SW-846 UPDATE V REFERENCE TABLEMethod/ChapterReference #in Up VReferenceLocation**Method 1030 1 "Test Methods for Readily Combustible Solids. Burning Rate Test." (14.2.2.5).** **Recommendations on the Transport of Dangerous Goods , Fifth Revised Edition, United** **Nations, New York, 1988. Method 1030 2 49 CFR, Appendix E to Part 173 (12-31-91 Edition), pp. 597-598.** **http://ecfr.gpoaccess.gov/cgi/t/text/text idx?c=ecfr;sid=75f5fbc866580ef2bc4bc1a8b340a5ab;rgn=di** **v5;view=text;node=49%3A2.1.1.3.9;idno=49;cc=ecfr Method 1030 3** **"Flammability (solids). Method A.10," Official Journal of the European Communities ,** **No. L251/63, September 19, 1984. http://www.intermed.it/istbiotech/reach/A10web1992.pdf** **Method 1030 4 Foster Wheeler Enviresponse, Inc., Edison, NJ. "Validation of Ignitability Method for** **Solids," submitted to the Office of Solid Waste, U.S. Environmental Protection Agency, February 1994.** **Method 1030 5 Internal Report (AMFA Report), North Carolina Department of Environmental Health and** **Natural Resources (Bill Hamner). Method 3200 1** **Bloom, N. S.; Gill, G. A.; Cappellino, S.; Dobbs, C.; McShea, L.; Driscoll, C.; Mason, R.; Rudd, J., "Speciation and Cycling of Mercury in Lavaca Bay, Texas, Sediments."** **Environ. Sci. Technol., 1999, 33, (1), 7-13. http://pubs.acs.org/doi/abs/10.1021/es980379d** **Method 3200 2 Templeton, D.; Ariese, F.; Cornelis, R.; Danielsson, L. G.; Muntau, H.; van Leeuvan, H.** **P.; Lobinski, R., "Guidelines for terms related to chemical speciation and fractionation of elements: Definitions, structural aspects, and methodological approaches."** Pure Appl.Chem.**,**2000,**72, (8), 1453-1470. http://www.iupac.org/objID/Article/pac7208x1453** **Method 3200 3 Hintelmann, H.; Falter, R.; Ilgen, G.; Evans R. D., "Determination of Artifactual** **Formation of Monomethylmercury (CH 3** **Hg +** **) in Environmental Samples Using Stable Hg** **2+ Isotopes with ICP-MS Detection: Calculation of Contents Applying Species** **Specific Isotope Additions."**Fresenius J. Anal. Chem.**,**1997,**358, (3), 363-370. http://www.springerlink.com/content/m7dpx89cxqke7fq6/** **Method 3200 4 Bloom, N. S.; Coleman, J. A.; Barber, L., "Artifact formation of methyl mercury during** **aqueous distillation and alternative techniques for the extraction of methyl mercury from environmental samples."** Fresenius J. Anal. Chem.**,**1997,**358, (3), 371-377. http://www.springerlink.com/content/35jq2nrwbqn08e3x/** **Method 3200 5 Rahman, G. M. M.; Kingston, H. M. S.; Bhandari, S., "Synthesis and Characterization of** **Isotopically Enriched Methylmercury (CH 3** **201 Hg** **+ )."** Appl. Organomet. Chem.**,**2003,**17, (12), 913-920.** **http://onlinelibrary.wiley.com/doi/10.1002/aoc.551/pdf**SW-846 Update VReferences - 1July 2014SW-846 UPDATE V REFERENCE TABLE**Method 3200 6 Han, Y.; Kingston, H. M.; Boylan, H. M.; Rahman, G. M. M.; Shah, S.; Richter, R. C.;** **Link, D. D.; Bhandari, S., "Speciation of mercury in soil and sediment by selective solvent and acid extraction."** Anal. Bioanal. Chem.**,**2003,**375, (3), 428-436. http://www.springerlink.com/content/m45jmrqf9kac67fw/** **Method 3200 7 Huo, D.; Kingston, H. M. S.; Larget, B., "Application of Isotope Dilution in Elemental** **Speciation: Speciated Isotope Dilution Mass Spectrometry (SIDMS)." In: Comprehensive Analytical Chemistry, Volume 33 (Elemental Speciation: New** **Approaches for Trace Element Analysis) , Elsevier, New York, 2000; 277-313.** **http://www.sciencedirect.com/science/article/pii/S0166526X 00800203** **Method 3200 8 Rahman, G. M. M.; Kingston, H. M. S., "Application of Speciated Isotope Dilution Mass** **Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and Sediments."** Anal. Chem.**,**2004,**76, (13), 3548-3555. http://www.ncbi.nlm.nih.gov/pubmed/15228324** **Method 3200 9 Rahman, G. M. M.; Kingston, H. M. S.; Kern, J. C.; Hartwell, S. W.; Anderson, R. F.;** **Yang, S. -Y., "Inter-laboratory Validation of EPA Method 3200 for Mercury Speciation Analysis using Prepared Soil Reference Materials."** Appl. Organomet. Chem.**,**2005,**19, 301-307.** **http://onlinelibrary.wiley.com/doi/10.1002/aoc.816/abstract Method 3200 10** **Labor, U.S. Department of, Occupational Health Guideline for Organo (Alkyl) Mercury ,** **Occupational Safety and Health Adminstration, Washington, D.C., 1978. http://www.cdc.gov/niosh/docs/81-123/pdfs/0384.pdf** **Method 3200 11 Nierenberg, D. W.; Nordgren, R. E.; Chang, M. B.; Siegler, R. W.; Blayney, M. B.;** **Hochberg, F.; Toribara, T. Y.; Cernichiari, E.; Clarkson, T., "Delayed Cerebellar Disease and Death after Accidental Exposure to Dimethylmercury."** New Engl. J. Med.**,**1993,**338, 1672-1675. http://www.nejm.org/doi/full/10.1056/NEJM19980604338230** **5 Method 3200 12** **Kingston, H. M.; Haswell, S. J., Microwave Enhanced Chemistry: Fundamentals, Sample Preparation, and Applications** **, 10th ed.; American Chemical Society, Washington, DC, 1997.** **Method 3200 13 Applied Isotope Technologies, Inc., www.sidms.com, e-mail: info@sidms.com. Method 3200 14** **Kingston, H. M. Speciated Isotope Dilution Mass Spectrometry of Reactive Species and Related Methods.** US Patent 6 790 673 B1**, September 14, 2004. http://www.findthatpatent.com/Speciated_isotope_dilution_m** **ass_spectrometry_of_reactive_species_and_related,679067 3.html** **Method 3200 15 Jain, W.; McLeod, C. W., "Rapid Sequential Determination of Inorganic Mercury and** **Methylmercury in Natural Waters by Flow-injection - Cold Vapor-Atomic-Fluorescence Spectrometry."** Talanta**,**1992,**39, (11), 1537-1542. http://www.sciencedirect.com/science/article/pii/0039914092** **801384 Method 3200 16** **Rahman, G. M. M.; Kingston, H. M. S., "Development of Microwave-Assisted Extraction Method and Isotopic Validation of Mercury Species in Soils and Sediments."** J. Anal. At.Spectrom.**,**2005,**20, 183-191. Method's Archive Box 22** **Method 3200 17 Rahman, G. M. M. "Development, Research and Validation of Environmental Speciation** **Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in Mercury and Chromium Speciation Analysis."** Ph. D. Dissertation**, Duquesne University, Pittsburgh, PA, 2004.** **http://digital.library.duq.edu/cdm spiritan/document.php?CISOROOT=/etd&CISOPTR=74238** **&REC=1**SW-846 Update VReferences - 2July 2014SW-846 UPDATE V REFERENCE TABLE**Method 3200 18 Fischer, E.; Tu, Q.; Nagourney, S.; England, R.; Buckley, B. "Microwave-assisted** **Solvent Extraction for Quantitative Simultaneous Extraction of Inorganic Mercury and Methylmercury from Soils."** 20thAnnual National Environmental Monitoring Conference**, Washington, DC, July 19-23, 2004; Washington, DC, July 19-23, 2004.** **Method 3200 19 Jain, W.; McLeod, C. W., "Field Sampling Technique for Mercury Speciation."** Anal.Proc.**,**1991**, 293-294. Method 3200 20** **Lee, Y. H.; Mowrer, J., "Determination of Methylmercury in Natural Waters at the Sub nanograms-per-litre Level by Capillary Gas Chromatography after Adsorbent Pre** **concentration."**Anal. Chim. Acta**,**1989,**221, (2), 259-268. http://www.sciencedirect.com/science/article/pii/S000326700** **0819625 Method 3200 21** **Mena, M. L.; McLeod, C. W., "Mercury Species Immobilized on Sulphydryl Cotton: A New Candidate Reference Material for Mercury Speciation."** Mikrochim. Acta.**,**1996,**123, (1-4), 103-108. http://www.springerlink.com/content/v5261u5642445451/fullt** **ext.pdf Method 3200 22** **Boylan, H. M.; Richter, R. C.; Kingston, H. M.; Ricotta, A. C., "Rapid Analysis for the Field: Method Development and Application to Natural Gas Utility Sites."** Water Air SoilPoll.**,**2001,**127, (1-4), 255-270. Method Archive Box 3** **Method 3200 23 Davis, A. Bloom, N. S.; Hee, Q.; Shane, S., "The Environmental Geochemistry and** **Bioaccessibility of Mercury in Soils and Sediments-A Review."**Risk Anal.**,**1997,**17, (5), 105-113.** **http://onlinelibrary.wiley.com/doi/10.1111/j.1539- 6924.1997.tb00897.x/abstract** **Method 3200 24 Revis, N. W.; Osborne, T. R.; Holdworth, G.; Hadden, C., "Distribution of Mercury** **Species in Soil from a Mercury-Contaminated Site."**Water Air Soil Poll.**,**1989,**17, (5), 557-569.** **Method Archive Box 3 Method 3200 25** **Revis, N. W.; Osborne, T. R.; Sedgely, D.; King, A., "Quantitative Method for Determining the Concentration of Mercury (II) Sulphide in Soils and Sediments."** Analyst**,**1989,**114, 823-826. http://pubs.rsc.org/en/Content/ArticleLanding/1989/AN/an98** **91400823 Method 3200 26** **Rahman, G. M.; Fahrenholz, T. M.; Kingston, H. M. Skip; Pamuku, M.; Hwang, J. D.; Young, L.A., "Speciation of Mercury in Crude Oil uisng Speciated Isotope Dilution Mass** **Spectrometry."**Spectroscopy**, 2010, 25(1), 36-45. http://spectroscopyonline.findanalytichem.com/spectroscopy** **/Feature/Speciation-of-Mercury-in-Crude-Oil-Using Speciated/ArticleStandard/Article/detail/655117** **Method 3200 27 Rahman, G.M.; Fahrenholz, T.M.; Kingston, H. M. Skip, "Application of Speciated** **Isotope Dilution Mass Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of Mercury Species Transformation in Human Hair."** J. Anal. At.Spectrom.,**2009, 24, 83-92. http://pubs.rsc.org/en/Content/ArticleLanding/2009/JA/b8052** **49b Method 3200 28** **Reyes, L. H.; Rahman, G. M.; Fahrenholz, T.; Kingston, H. M. Skip, "Comparison of Methods with Respect to Efficiencies, Recoveries, and Quantitation of Mercury Species** **Interconversions in Food Demonstrated using Tuna Fish."**Anal. Bioanal. Chem.**, 2008, 390, 2123-2132.** **http://www.ncbi.nlm.nih.gov/pubmed/18317738 Method 3511 1** **"Simultaneous Analysis of Monocyclic Aromatic Hydrocarbons in Water by Microextraction." EPRI Report TR-Research Project, April 1997.** **Method 3511 2 D. M. Munro. "Simultaneous Determination of Volatile and Semivolatile Organic** **Compounds in Soil."**Remediation Journal,**10, pp. 65-81, 2000. http://onlinelibrary.wiley.com/doi/10.1002/rem.3440100408/p** **df**SW-846 Update VReferences - 3July 2014SW-846 UPDATE V REFERENCE TABLE**Method 3572 1 Applicable documents to support the occupational health program when dealing with** **chemical agents include AR11-34 (The Army Respiratory Protection Program; AR 40-5 (Preventive Medicine); DA Pam 40-8 (Occupational Health guidelines for the evaluation** **and Control of Occupational Exposure to Nerve Agents GA, GB, GC, and VX.) and DA Pam 40-173 (Occupational Health Guidelines for the Evaluation and Control of** **Occupational Exposure to Mustard Agents H, HD, and HT). http://www.apd.army.mil/pdffiles/r11_34.pdf, b.** **http://www.apd.army.mil/pdffiles/p40_8.pdf c. http://www.apd.army.mil/pdffiles/p40_173.pdf** **Method 3572 2 Development and Evaluation of an Analytical Method for Determination of GB, VX, and** **HD in Concrete, SwRI Final Report to PM-ECW, William S. Williamson, Jr. Joseph H. Brewer.** **Method 3572 3 Development and Evaluation of an Analytical Method for Determination of GB, VX, and** **HD in Coral, SwRI Final Report to PM-ECW, William S. Williamson, Jr., Joseph H. Brewer.** **Method 3572 4 Development and Evaluation of an Analytical Method for Determination of GB, VX, and** **HD in Charcoal, SwRI Final Report to PM-ECW, Michael G. MacNaughton, Ph.D., P.E., William S. Williamson, Jr., Joseph H. Brewer.** **Method 3572 5 Development and Evaluation of an Analytical Method for Determination of GB, VX, and** **HD on Surfaces, SwRI Final Report to PM-ECW, Carter Crigler. Method 3572 6** **Laboratory Monitoring and Quality Assurance Plan dated June 2004, Department of Army, Chemical Material Agency.** **Method 3620C 1 A.J. Gordon and R.A. Ford, The Chemist's Companion: A Handbook of Practical Data,** **Techniques , and References, New York: John Wiley & Sons, Inc., pp. 372, 374, and** **375, 1972. Method 3620C 2** **Floridin of ITT System, Florisil: Properties, Application, Bibliography , Pittsburgh,** **Pennsylvania, 5M381DW. Method 3620C 3** **P.A. Mills, "Variation of Florisil Activity; Simple Method for Measuring Absorbent Capacity and Its Use in Standardizing Florisil Columns,"** Journal of the Association ofOfficial Analytical Chemists**, 51, 29, 1968. Method 3620C 4 U.S. Food and Drug Association, Pesticides Analytical Manual** **(Volume 1), July 1985. http://www.fda.gov/Food/ScienceResearch/LaboratoryMetho** **ds/PesticideAnalysisManualPAM/ucm111455.htm Method 3620C 5** **V. Lopez-Avila, J. Milanes, N.S. Dodhiwala, and W.F. Beckert, "Cleanup of Environmental Sample Extracts Using Florisil Solid-Phase Extraction Cartridges,"** J.Chrom. Sci.**27, 209-215, 1989. http://chromsci.oxfordjournals.org/content/27/5/209.abstract** SW-846 Update VReferences - 4July 2014SW-846 UPDATE V REFERENCE TABLE**Method 3620C 6 U.S. EPA, "Evaluation of Sample Extract Cleanup Using Solid-Phase Extraction** **Cartridges," Project Report, December 1989. http://nepis.epa.gov/EPA/html/DLwait.htm?url=/Exe/ZyNET.e** **xe/2000AKCX.PDF?ZyActionP=PDF&Client=EPA&Index=19 86 Thru** **1990&File=D%3A%5CZYFILES%5CINDEX%20DATA%5C8 6THRU90%5CTXT%5C00000003%5C2000AKCX.txt&Query** **=&SearchMethod=1&FuzzyDegree=0&User=ANONYMOUS &Password=anonymous&QField=&UseQField=&IntQFieldO** **p=0&ExtQFieldOp=0&Docs= Method 3620C 7 U.S. EPA, Method 650, "Aniline and Selected Substituted Derivatives."** **Method 3620C 8 W.F. Beckert and V. Lopez-Avila, "Evaluation of SW-846 Method 8060 for Phthalate** **Esters," Proceedings of the Fifth Annual Waste Testing and Quality Assurance Symposium, 1989, pp. 144-156.** **http://nepis.epa.gov/EPA/html/DLwait.htm?url=/Exe/ZyNET.e xe/9100CUG4.PDF?ZyActionP=PDF&Client=EPA&Index=19** **86 Thru 1990&File=D%3A%5CZYFILES%5CINDEX%20DATA%5C8** **6THRU90%5CTXT%5C00000020%5C9100CUG4.txt&Query =&SearchMethod=1&FuzzyDegree=0&User=ANONYMOUS** **&Password=anonymous&QField=&UseQField=&IntQFieldO p=0&ExtQFieldOp=0&Docs=** **Method 3620C 9 U.S. EPA, Method 608, Organochlorine Pesticides and PCBs, 40 CFR 136, October 26,** **1984. http://www.caslab.com/EPA-Methods/PDF/608.pdf** **Method 4025 1 DF1 High Performance Dioxin/Furan Immunoassay Kit (CAPE Technologies),** **www.cape-tech.com .** **Method 4025 2 CAPE Technologies Application Notes and related product literature (www.cape-** **tech.com) Method 4025 3** **Carlson, Robert, E., Harrison, Robert, O., Measurement of PCDD/F TEQ by Immunoassay: Concept Development and Validation. Organohalogen Compounds,** **vol. 5, Stockholm, Sweden (1998). Method's Archive Box 36** **Method 4025 4 Harrison, Robert, O., Carlson, Robert, E., Measurement of PCDD/F TEQ by** **Immunoassay: Demonstration Using Real World Samples, Organohalogen Compounds, vol. 5, Stockholm, Sweden (1998).** **http://www.cape-tech.com/TR-001.pdf Method 4025 5** **Harrison, Robert, O., Role of Quality Assurance in Immunoassay Methods Used for Field Screening. Immunochemical Technology for Environmental Applications,** **American Chemical Society, Washington D.C. (1997). http://pubs.acs.org/doi/abs/10.1021/bk-1997-0657.ch029** **Method 4025 6 Van den Berg, et. al., “The 2005 World Health Organization Re-evaluation of Human** **and Mammalian Toxic Equivalency Factors (TEFs) of Dioxins and Dioxin-like Compounds,” Toxicological Sciences, 93(2): 223-241, July 7, 2006.** **http://toxsci.oxfordjournals.org/content/93/2/223.full.pdf+html**SW-846 Update VReferences - 5July 2014SW-846 UPDATE V REFERENCE TABLE**Method 4025 7 “Correlation between EIA Results and GC-MS TEQ,” revised Figure 2 from document** **listed in Ref. 8. (www.cape-tech.com, Tech References). www.cape-tech.com** **Method 4025 8 “Performance of the CAPE Technologies DF1 Dioxin/Furan Immunoassy Kit for Soil and** **Sediment Samples,” EPA 540/R-08/002, February 2008. (www.cape-tech.com, Tech References).** **www.cape-tech.com Method 4025 9** **“Technologies for Monitoring and Measurement of Dioxin and Dioxin-like Compounds in Soil and Sediment (CAPE Technologies LLC, DF1; Dioxin/Furan Immunoassay Kit; PCB** **TEQ Immunoassy Kit),” EPA 540/R-05/004, March 2005. (www.cape-tech.com). www.cape-tech.com** **Method 4025 10 Technical Note TN-005, CAPE Technologies (www.cape-tech.com, Technical Notes ) www.cape-tech.com** **Method 4025 11 Application Note AN-008, CAPE Technologies (www.cape-tech.com, Application Notes) www.cape-tech.com** **Method 4025 12 “An Efficient and Green Cleanup System for Analysis of Dioxins/Furans, Dioxin-like** **PCBs and PBDES,” (www.cape-tech.com) www.cape-tech.com** **Method 4025 13 Immunoassy Sample Prep Kit SP3-60, CAPE Technologies (www.cape-tech.com** **, Material Lists).** **www.cape-tech.com Method 4025 14** **Sample Prep Starter Kit SP3-ST, CAPE Technologies (www.cape-tech.com , Material** **Lists). www.cape-tech.com** **Method 4430 1 Dioxins and Furans in Soil and Sediment, Eichrom Method DFS01,** **www.eichrom.com/dioxin/products .** **www.eichrom.com/dioxin/products. Method 4430 2** **M. Van den Berg, L. S. Birnbaum, M. Denison, M. De Vito, W. Farland, M. Feeley, H. Fiedler, H. Hakansson, A. Hanberg, L. Haws, M. Rose, S. Safe, D. Schrenk, C.** **Tohyama, A. Tritscher, J. Tuomisto, M. Tysklind, N. Walker, and R. E. Peterson; “The 2005 World Health Organization Reevaluation of Human and Mammalian Toxicity** **Equivalency Factors for Dioxins and Dioxin-like Compounds,”**Toxicol. Sci.2006**,**93[2]**, 223-241.** **http://toxsci.oxfordjournals.org/content/93/2/223.full.pdf+html Method 4430 3** **R. L. Allen, J. J. Willey; “Novel Real-Time PCR Assay for the Detection of Dioxins and Furans,”** Organohalogen Compd.2002**,**58**, 341-343. Method 4430 4** **D. R. McAlister, M. J. Fern, R. L.; Allen, K. Sakata, B. Le Bizec, P. Marchand; “Sample Preparation for the Measurement of Polychlorinated Dioxins and Furans by the Procept** **Rapid Dioxin Assay,”**Organohalogen Compnd.2006**,**68**, 940-943. http://www.dioxin20xx.org/pdfs/2006/06-138.pdf** **Method 4430 5 Y. Z. Gu, J. B. Hogenesch, C. A. Bradfield; “The PAS Superfamily: Sensors of** **Environmental and Developmental Signals,”**Annu. Rev. Pharmacol. Toxicol.2000**,**40**, 519-561.** **http://mcardle.oncology.wisc.edu/bradfield/519.pdf Method 4430 6** **D. R. McAlister, M. J. Fern; “Soil Screening at 50 pg/g Using a Novel Aryl Hydrocarbon Receptor-based PCR Assay,”** Organohalogen Compd**.,**2007**,**69**, 1230-1233. Method 4430 7** **D. R. McAlister, M. J. Fern; “Cross-reactivity of Compounds on the Procept Rapid Dioxin Assay,”** Organohalogen Compd**.,**2007**,**69**, 1226-1229. Method 4430 8** **S. Heid, R. Pollenz, H. Swanson; “Role of Heat Shock Protein 90 Dissociation in Mediating Agonist-induced Activation of the Aryl Hydrocarbon Receptor,”** Mol.Pharmacol.2000**,**57[1]**, 82-92. http://molpharm.aspetjournals.org/content/57/1/82.full.pdf** SW-846 Update VReferences - 6July 2014SW-846 UPDATE V REFERENCE TABLE**Method 4430 9**Fed. Reg.2006**,**71**, 78441, Update to ATSDR Policy Guideline for Dioxins and Dioxin- Like Compounds in Residential Soil.** **http://edocket.access.gpo.gov/2006/pdf/E6-22388.pdf Method 4430 10** **C. A. Foy, H. C. Parkes; “Emerging Homogeneous DNA-based Technologies in the Clinical Laboratory,”** Clin. Chem.2000**,**47(6)**, 990-1000. http://www.clinchem.org/cgi/reprint/47/6/990** **Method 4430 11 D. R. McAlister, M. J. Fern, R. L. Allen; “Rapid Aryl Hydrocarbon Receptor-based** **Polymerase Chain Reaction Screening Assay for Polychlorinated Dibenzo-**p**-Dioxins and Furans in Soil and Sediment,”** Talanta**,**2007**, in press, doi.org/10.1016/j.talanta.2007.08.005.** **Method 4435 1 Arrieta, D. E., Ontiveros, C., Denison, M.S., and Washburn, B.S. (2000). "Ah Receptor** **Mediated Effects of Particulate Organic Extracts from the Paso Del Morte Airshed Along the U.S. - Mexico Border." Organohalogen Compounds 45: 212 - 215.** **http://www.ncbi.nlm.nih.gov/pmc/articles/PMC1241610/pdf/e hp0111-001299.pdf** **Method 4435 2 Behnisch, P. A., Allen, R., Anderson, J., Brouwer, A., Brown, D., Campbell, T. C.,** **Goeyens, L., Harrison, R. O., Hoogenboom, R., Overmeire, I.V., Traag, W., and Malisch, R. (2001). "Harmonised Quality Criteria for Chemical and Bioassays Analyses** **of PCDDs/PCDFs in Feed and Food Part 2: General Considerations, Bioassay Methods." Organohalogen Compounds 45.** **http://www.dioxins.com/pdf/feedstuffs/feed04.pdf Method 4435 3** **Brown, D. J., M. D. Chu, et al. (2001). "Determination of REP Values for the CALUX bioassay and comparison to the WHO TEF Values." Organohalogen Compounds 53:** **211- 214. http://www.dioxins.com/pdf/compounds/compound02.pdf** **Method 4435 4 Brown, D. J., Goeyens, L., Van Overmeire, I., Chu, M., Murata, H., and Clark, G.C.** **(2001). "Quality control criteria implemented for monitoring the CALUX bioassay." Organohalogen Compounds 54: 32-35.** **http://www.dioxins.com/pdf/environment/environment01.pdf Method 4435 5** **Brown, D. J., Kishimoto, Y., Ikeno, O., Chu, M., Nomura, J., Murakami, T., and Murata, H. (2000). "Validation Study for the use of the Dioxin Responsive CALUX Assay for** **Analysis of Japanese Ash and Soil Samples." Organohalogen Compounds 45: 200-203. http://www.dioxins.com/pdf/environment/environment10.pdf** **Method 4435 6 Brown, D. J., Nakamura, M., Chu, M.D., Denison, M.S., Murata, H., and Clark, G.C.** **(2002). "Recovery determinations for bioassay analysis: Considerations and results." Organohalogen Compounds 58: 357-360.** **http://www.dioxins.com/pdf/compounds/compound03.pdf Method 4435 7** **Brown, D. J., Van Overmeire, I., Goeyens, L., Chu, M.D., Denison, M.S., and Clark, G.C. (2002). "Elimination of interfering compounds in preparation for analysis by an Ah** **receptor based bioassay." Organohalogen Compounds 58: 401-404. http://www.dioxins.com/pdf/compounds/compound04.pdf** **Method 4435 8 Clark, G., V. Garry, et al. (2002). "Relationships between exposure to dioxin-like** **chemicals, testosterone levels, and sex of the children of pesticide applicators." Organohalogen Compounds 56: 73-76.** **http://www.dioxins.com/pdf/compounds/compound07.pdf Method 4435 9** **Clark, G. C., Brown, D.J., Seidel, S.D., Phelan, D., Denison, M.S. (1999). "Characterization of the CALUX and GRAB bioassays for sensitivity and specificity in** **detection of phamacological agents that activate the Ah Receptor signaling system." Organohalogen Compounds 42: 309-312.** **http://www.dioxins.com/pdf/compounds/compound09.pdf**SW-846 Update VReferences - 7July 2014SW-846 UPDATE V REFERENCE TABLE**Method 4435 10 Clark, G. C., Chu, M., Touati, D., Rayfield, B., Stone, J., Cooke, M. (1999). "A Novel Low** **Cost Air Sampling Device (AmbStack Sampler) and Detection System (CALUX Bioassay) for Measuring Air Emissions of Dioxin, Furan, and PCB on a TEQ Basis** **Tested With a Model Industrial Boiler." Organohalogen Compounds 42: 309-312. http://www.dioxins.com/pdf/environment/environment09.pdf** **Method 4435 11 Denison, M. S., Nagy, S.R., Clark, G.C., Chu, M., Brown, D.J., Murata, H., Shan, G.,** **Sanborn, J.R., and Hammock, B.D. (2001). "Bioanalytical approaches for the Detection of Dioxin and Related Halogenated Aromatic Hydrocarbons." Organohalogen** **Compounds 45. http://www.crcnetbase.com/doi/abs/10.1201/978142003220** **8.ch33, 11. http://www.dioxin20xx.org/pdfs/2001/01-82.pdf Method 4435 12** **Denison, M. S., Seidel, S.D., Ziccardi, M., Rogers, W.J., Brown, D.J., and Clark, G.C. (1999). "Ah receptor-based bioassays for dioxins and related chemicals: Applications** **and limitations." Organohalogen Compounds 40: 27-30. http://toxsci.oxfordjournals.org/content/55/1/107.full.pdf** **Method 4435 13 Denison, M.S., Zhao, B., Baston, D.S., Clark, G.C., Murata, H. and Han, D.-H. (2004).** **Recombinant Cell Bioassay Systems for the Detection and Relative Quantitation of Halogenated Dioxins and Related Chemicals, Talanta 63: 1123-1133.** **http://www.sciencedirect.com/science/article/pii/S003991400 4002978** **Method 4435 14 Denison, M.S. Nagy, S.R., Ziccardi, M., Clark, G.C., Chu, M., Brown, D.J., Shan, G.,** **Sugawara, Y., Shirley J. Gee, S.J., James Sanborn, J. and Hammock, B.D. (2002) Bioanalytical approaches for the detection of dioxin and related halogenated aromatic** **hydrocarbons, in: Technology-Driven Biomarkers Development and Application in Environmentally-Associated Diseases, Wilson, D. and W. Suk, W., eds., pp. 483-494,** **Lewis Press, Boca Raton, FL. Method 4435 15** **Garrison, P.M., Tullis, K., Aarts, J.M.M.J.G., Brouwer, A. and Giesy, J.P. and Denison, M.S. (1996) Species-specific recombinant cell lines as bioassay systems for the** **detection of 2,3,7,8-tetrachlorodibenzo-p-dioxin-like chemicals, Fund. Appl. Toxicol. 30, 194-203.** **http://toxsci.oxfordjournals.org/content/30/2/194.full.pdf+html Method 4435 16** **Han, D.-H., Nagy, S.R. and Denison, M.S. (2004) Comparison of recombinant cell Bioassays for the detection of Ah receptor agonists, Biofactors 20, 11-22.** **https://iospress.metapress.com/content/458qmdj2gu4mc7ef/ resource-secured/?target=fulltext.pdf** **Method 4435 17 Han, D., Nagy, S.R., and Denison, M.S. (2002). "Recombinant cell lines for the** **detection of dioxins and Ah Receptor ligands- Not all assays are created equal." Organohalogen Compounds 58: 421-424.** **http://www.dioxins.com/pdf/compounds/compound05.pdf Method 4435 18** **Hoogenboom, R., Portier, L., Ontenk, C., Polman, T., Hamers, A., and Traag, W. (2000). "Determination of Dioxins and Planar PCBs in Fish Using the GC/MS and** **CALUX Bioassay." Organohalogen Compounds 45: 180 - 184. http://www.dioxin20xx.org/pdfs/2000/00-212.pdf** **Method 4435 19 Hooper, K., G. Clark, et al. (2002). "Using the CALUX Assay to select high-TCDD** **mothers in Southern Kazakhstan and map time-course of TCDD elimination via breast milk." Organohalogen Compounds 58: 377-380.** **http://www.dioxin20xx.org/pdfs/2002/02-467.pdf Method 4435 20** **Hooper, K., Hayward, D., Anderson, M., Farland, W., Lucier, G., Clark, G. (2000). "CALUX results correlate with GC/MS/MS data from Kazakhstan breast milk samples."** **Organohalogen Compounds 45: 236-239. http://www.dioxin20xx.org/pdfs/2000/00-214.pdf** **Method 4435 21 Huwe, J. K., Clark, G., Chu, A., and Garry, V. (2003). "CALUX and High Resolution** **GC/MS Analysis of Dioxin-Like Compounds in Chlorophenoxy Pesticide Formulations." Organohalogen Compounds 60 - 65.** **http://www.dioxins.com/pdf/environment/environment04.pdf**SW-846 Update VReferences - 8July 2014SW-846 UPDATE V REFERENCE TABLE**Method 4435 22 Kayama, F., Hammatsu, A., Sagisaka, K., Brown, D., Clark, G., and Suzuki, T. (2001).** **"CALUX assay is applicable to human epidemiological studies." Organohalogen Compounds 54: 48-50.** **http://www.dioxins.com/pdf/biological/biological02.pdf Method 4435 23** **Kayama, F., Horiguchi, H., Kunisue, T., Tanabe, S., Fukatsu, H., Yamazaki, N., Nakamura, M., Yabushita, H., Fujino, J., and Clark, G. (2003). "Dioxin and** **Organochlorine Pesticide Concentrations of Breast Milk in China and Japan." Organohalogen Compounds 60 -65.** **http://www.dioxins.com/pdf/biological/biological06.pdf Method 4435 24** **Kayama, F., Horiguchi, H., Oguma, E., Fujino, J., Yabushita, H., Brown, D., Clark, G. (2002). "Regional differences of blood dioxins and organchlorine pesticides** **concentrations of Japanese female farmers.-Application of CALUX assay for epidemiological study-." Organohalogen Compounds 55: 275-278.** **http://www.dioxins.com/pdf/biological/biological03.pdf Method 4435 25** **Nakamura T, Nakamura M, Suzuki S, Takahashi M, Fujino J, Yabushita H, Yamamoto T, Brown DJ, Nakai K, Satoh H (2002)" A COMPARATIVE ANALYSIS OF CERTIFIED** **ENVIRONMENTAL REFERENCE MATERIALS USING CALUX TM** **ASSAY AND HIGH RESOLUTION GC/MS". Organohalogen Compounds 58: 381-384.** **http://www.dioxin20xx.org/pdfs/2002/02-468.pdf Method 4435 26** **Overmeire, I. V., Carbonnelle, S., Loco, J.V., Roos, P., Brown, D., Chu, M., Clark, G., and Goeyens, L. (2002). "Validation of the CALUX Bioassay: Quantitative Screening** **Approach." Organohalogen Compounds 58: 353 - 356. http://www.dioxins.com/pdf/environment/environment02.pdf** **Method 4435 27 Overmeire, I. V., Chu, M., Brown, D., Clark, G., Carbonnelle, S. and Goeyens, L. (2001).** **"Application of the CALUX Bioassay for the Determination of Low TEQ Values in Milk Samples." Organohalogen Compounds 45.** **http://www.dioxins.com/pdf/biological/biological08.pdf Method 4435 28** **Overmeire, I. V., Goeyens, L., Beernaert, H., Srebrink, S., De Poorter, G., Baeyens, W., Clark, G., Chu, M., Chu, A., Chu, D., Morris, R., and Brown, D. (2000). "A Comparitive** **Study of GC-HRMS and CALUX TEQ Determinations in Food Samples by the Belgian Federal Ministries of Public Health and Agriculture." Organohalogen Compounds 45:** **196 - 200. http://www.dioxins.com/pdf/feedstuffs/feed02.pdf** **Method 4435 29 Pence, L. M., Archer, J.C., Bluhm, Earnheart, C., Clark, G., Chu, A., Lovell, R., and** **Eckert, J. (2003). "Inter-Laboratory CALUX Comparison Data at Low Levels with Traditional GC-HRMS Confirmations." Organohalogen Compounds 60 - 65.** **http://www.dioxin20xx.org/pdfs/2003/03-65.pdf Method 4435 30** **Shaw, S. D., Brenner, D., Mahaffey, C.A., Guise, S.D., Perkins, C.R., Denison, M.S., and Waring, G.T. (2003). "Persistent Organic Pollutants (POPs) and Immune Function** **in US Atlantic Coast Harbor Seals." Organohalogen Compounds 60 - 65. http://www.dioxins.com/pdf/biological/biological05.pdf** **Method 4435 31 Warner M., E., B., Patterson, D.G., Clark, G., Turner, W.E., Bonsignore, L., Mocarelli,** **P., and Gerthoux, P.M. (2003). "Comparison of the CALUX Bioassay and ID HRGC/HRMS as Measures of Dioxin Toxic Equivalents in Serum." Organohalogen** **Compounds 60 - 65. http://www.dioxins.com/pdf/biological/biological04.pdf** **Method 4435 32 Windal, I., Schroijen, C., Wouwe, N.V., Carbonnelle, S., Overmeire, I.V., Brown, D.,** **Clark, G., Baeyens, W., and Goeyens, L. (2003). "Non Additive Interactions in CALUX." Organohalogen Compounds 60 - 65.** **http://www.dioxins.com/pdf/compounds/compound06.pdf**SW-846 Update VReferences - 9July 2014SW-846 UPDATE V REFERENCE TABLE**Method 4435 33 Windal, I., I. Van Overmeire, et al. (2002). "Variables that affect TEQ determinations by** **CALUX and GC-HRMS." Organohalogen Compounds 58: 389-392. http://www.dioxins.com/pdf/environment/environment03.pdf** **Method 4435 34 Ziccardi, M.H., Gardner, I.A. and Denison, M.S. (2002) Application of the luciferase** **recombinant cell culture bioassay system for the analysis of polycyclic aromatic hydrocarbons, Environ. Toxicol. & Chem. 21, 2027-2033.** **http://onlinelibrary.wiley.com/doi/10.1002/etc.5620211004/ful l** **Method 4435 35 Windal, I., Dennison, M. S, Birnbaum L. S., Van Wouwe, N., Baeyens, W. Goeyens L.** **(2005). “Chemically Activated Luciferase Gene Expression (CALUX) Cell Bioassay Analysis for the Estimation of Doxin-Like Activity: Critical Parameters of the CALUX** **Procedure that Impact Assay Results, Environ.” Sci. Technol.,**3,**7357-7364. www.vliz.be/imisdocs/publications/103941.pdf** **Method 4435 36 Behnisch, P.A., Hosoe, K., Sakai, S-i. (2003). “Brominated dioxin-like compounds in** **vitro assessment in comparison to classical dioxin-like compounds and other polyaromatic compounds.” Environment International** 29**, 861-877. http://www.pops.int/documents/meetings/poprc/submissions/** **AnnexE_2007/Toxicity%20studies%20World%20Chlorine% 20Council.pdf** **Method 4435 37 Schroijen, C.,Windal, I., Goeyens, L, Baeyens, W. (2004). “Study of the interference** **problems of dioxin-like chemicals with the bio-analytical method CALUX.” Talanta 63, 1261-1268.** **http://www.vub.ac.be/ANCH/publications/Schroijen%20et%2 0al_2004.pdf** **Method 4435 38 Van den Berg et al., (2006). “The 2005 World Health Organization Reevaluation of** **Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-Like Compounds.” Toxicological Sciences 93(2):223-241.** **http://toxsci.oxfordjournals.org/content/93/2/223.full.pdf+html Method 4435 39** **Brown, D.J., Orelien, J., Gordon, J.D., Chu, A.C., Chu, M.D., Nakamura, M., Handa, H., Kayama, F., Denison, M.S., and Clark, G.C. (2007) “Mathematical Model Developed for** **Environmental Samples: Prediction of GC/MS Dioxin TEQ from XDS-CALUX Bioassay Data,” accepted Environmental Science and Technology Nov. 2007.** **http://journals.ohiolink.edu/ejc/article.cgi?issn=0013936x&is sue=v41i0012&article=4354_mmdfesdtfxbd** **Method 4435 40 USEPA, “Report on the Comparison of Cell Based Assays with Mass** **SpectrometryMethods for the Analysis of PCDDs/PCDFs and PCBs in Biosolids. U.S. EPA Report from the Office of Water and Office of Science and Technology,** **Engineering and Analysis Division on Biosolids, June 2002. Method 4435 41** **Denison, Michael S., Brouwer, Abraham, Clark, George C. "Bioassay for detecting 2,3,7,8-tetrachlorodibenzo-para-dioxin and TCDD-like compounds and novel** **recombinant cell line useful therefor," U.S. patent # 5,854,010, December 29, 1998. http://patft.uspto.gov/netacgi/nph** **Parser?Sect1=PTO1&Sect2=HITOFF&d=PALL&p=1&u=%2 Fnetahtml%2FPTO%2Fsrchnum.htm&r=1&f=G&l=50&s1=5,** **854,010.PN.&OS=PN/5,854,010&RS=PN/5,854,010 Method 4435 42** **Chu, Michael D, Clark, George C. "Methods and apparatus for separating and detecting specific polyhalogenated diaromatic hydrocarbons," U.S. patent # 6,720,431,** **April 13, 2004. http://patft.uspto.gov/netacgi/nph** **Parser?Sect1=PTO1&Sect2=HITOFF&d=PALL&p=1&u=%2 Fnetahtml%2FPTO%2Fsrchnum.htm&r=1&f=G&l=50&s1=6,** **720,431.PN.&OS=PN/6,720,431&RS=PN/6,720,431**SW-846 Update VReferences - 10July 2014SW-846 UPDATE V REFERENCE TABLE**Method 5021A 1 P. Flores, and T. Bellar, "Determination of Volatile Organic Compounds in Soils using** **Equilibrium Headspace Analysis and Capillary Column Gas Chromatography/Mass Spectrometry," U.S. Environmental Protection Agency, Office of Research and** **Development, Environmental Monitoring Systems Laboratory, Cincinnati, OH, December, 1992.** **Method's Archive Box 6 Method 5021A 2** **B. V. Loffe, and A. G. Vitenberg, "Headspace Analysis and Related Methods in Gas Chromatography," John Wiley and Sons, 1984.** **Method 5021A 3 R. J. Pirkle, and R. P. McLoughlin, “The Analysis of Selected Components of** **Reformulated Gasoline in Environmental Samples” from MTBE Handbook, ed. Kostecki, P. and Moyer, E. Amherst Scientific Publishers, 2002.** **Method 5021A 4 USEPA OUST, Environmental Fact Sheet: Analytical Methods for Fuel Oxygenates,** **EPA 510-F-03-001, April, 2003. http://www.epa.gov/oust/mtbe/omethods.pdf** **Method 5021A 5 H. White, B. Lesnik, and J. T. Wilson, “Analytical Methods for Fuel Oxygenates”,** **LUSTLine (Bulletin #42), October, 2002, http://www.epa.gov/oust/mtbe/LL42Analytical.pdf** **Method 5021A 6 RCRA Organic Methods Workgroup Meeting Minutes, March 20, 2012. Method Contract Archives Method 5021A 7 RCRA Organic Methods Workgroup Meeting Minutes, March 22, 2012. Method Contract Archives** **Method 5021A 8 RCRA Organic Methods Workgroup Meeting presentation describing changes to** **method 5021, “Proposed Changes to SW-846 method 5021A, VOCs by Static Headspace** ”**, March 1, 2012. Method Contract Archives** **Method 6010D 1 C.L. Jones,** et al**., "An Interlaboratory Study of Inductively Coupled Plasma Atomic Emission Spectroscopy Method 6010 and Digestion Method 3050," EPA-600/4-87-032,** **U.S. Environmental Protection Agency, Las Vegas, NV, 1987. http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=91009D89.txt** **Method 6010D 2 Taylor, J. K., “Quality Assurance of Chemical Measurements”, Lewis Publishers (1987). Method 6010D 3** **Federal Advisory Committee on Detection and Quantitation Approaches and Uses in Clean Water Act Programs, Final Report,** **http://water.epa.gov/scitech/methods/cwa/det/index.cfm (December 28, 2007). Method 6020B 1** **Horlick, G., et al., "The effect of plasma operating parameters on analyte signals in inductively coupled plasma-mass spectrometry" Spectrochim. Acta Part B: Atomic** **Spectroscopy, 40(10-12), 1555-1572 (1985). http://www.sciencedirect.com/science/article/pii/0584854785** **801786 Method 6020B 2** **Gray, A.L., "The ICP as an ion source-origins, achievements and prospects/Mass spectrometry with an inductively coupled plasma as an ion source: the influence on** **ultratrace analysis of background and matrix response" Spectrochim. Acta 40B, 1525 (1985); 41B, 151 (1986).** **http://www.sciencedirect.com/science/article/pii/0584854785 801762 ;** **http://www.sciencedirect.com/science/article/pii/0584854786 801471** **Method 6020B 3 Tan, S.H., and Horlick, G., "Background Spectral Features in Inductively Coupled** **Plasma/Mass Spectrometry" Appl. Spectrosc. 40(4), 445-460 (1986). http://www.opticsinfobase.org/as/abstract.cfm?uri=as-40-4-** **445 Method 6020B 4** **Vaughan, M.A., and Horlick, G., "Oxide, Hydroxide, and Doubly Charged Analyte Species in Inductively Coupled Plasma/Mass Spectrometry" Appl. Spectrosc. 40(4), 434-** **445 (1986). http://www.opticsinfobase.org/abstract.cfm?URI=as-40-4-** **434**SW-846 Update VReferences - 11July 2014SW-846 UPDATE V REFERENCE TABLE**Method 6020B 5 Holden, N.E., "Table of the Isotopes," in Lide, D.R., Ed., CRC Handbook of Chemistry** **and Physics, 74th Ed., CRC Press, Boca Raton, FL, 1993. Method 6020B 6** **Hinners, T.A., Heithmar, E., Rissmann, E., and Smith, D., Winter Conference on Plasma Spectrochemistry, Abstract THP18; p. 237, San Diego, CA (1994).** **http://pubs.rsc.org/en/content/articlelanding/1994/JA/ja9940 90051n** **Method 6020B 7 Lichte, F.E., et al., Anal. Chem. 59, 1150 (1987). http://pubs.acs.org/doi/abs/10.1021/ac00135a018** **Method 6020B 8 Evans E.H., and Ebdon, L., "Simple approach to reducing polyatomic ion interferences** **on arsenic and selenium in inductively coupled plasma mass spectrometry" J. Anal. At. Spectrom. 1989, 4, 299-300.** **http://pubs.rsc.org/en/content/articlelanding/1989/ja/ja98904 00299** **Method 6020B 9 Beauchemin, D., et al., "Study of the effects of concomitant elements in inductively** **coupled plasmamass spectrometry" Spectrochim. Acta Part B, 42(3), 1987, 467-490. http://www.sciencedirect.com/science/article/pii/0584854787** **800241 Method 6020B 10** **Houk, R.S., "Mass Spectrometry of inductively coupled plasmas" Anal. Chem. 58(1), 97A-105A (Jan. 1986).** **http://pubs.acs.org/doi/pdf/10.1021/ac00292a003 Method 6020B 11** **Thompson, J.J., and Houk, R.S., "A Study of Internal Standardization in Inductively Coupled Plasma-Mass Spectrometry" Appl. Spectrosc. 41, 801 (1987).** **http://www.opticsinfobase.org/viewmedia.cfm?uri=as-41-5- 801&seq=0** **Method 6020B 12 Newberry, W.R., Butler, L.C., Hurd, M.L., Laing, G.A., Stapanian, M.A., Aleckson, K.A.,** **Dobb, D.E., Rowan, J.T., and Garner, F.C., Final Report of the Multi-Laboratory Evaluation of Method 6020 CLP-M Inductively Coupled Plasma-Mass Spectrometry** **(1989). Method 6020B 13** **Taylor, Daniel B., Kingston, H.M., Nogay, Donald J., Koller, Dagmar, and Hutton, Robert. On-Line Solid-phase Chelation for the Determination of Eight Metals in** **Environmental Waters by Inductively Coupled Plasma Mass Spectrometry. Method's Archive Box 7** **Method 6020B 14 Kingston, H. M., Siriraks, A., and Riviello, J. M., Patent Number 5,126,272, "A Method** **and Apparatus for Detecting Transition and Rare Earth Elements in a Matrix", U.S. Patent, Filed U.S. Patent Office, March 1989, 31 pages, Granted June 30, 1992, Patent** **held by US Government. Method 6020B 15** **Kingston, H. M., Siriraks, A., and Riviello, J. M., Patent Number 5,244,634 , "A Method and Apparatus for Detecting Transition and Rare Earth Elements in a Matrix", U.S.** **Patent , Filed U.S. Patent Office, March 1989, 31 pages, Granted Sept. 14, 1993, Patent held by US Government.** **Method 6020B 16 Dobb, David E., Rowan, J.T., and Cardenas, D., Lockheed Environmental Systems and** **Technologies Co., Las Vegas, NV; and Butler, L.C., and Heithmar, E.M., U.S.EPA, Las Vegas, NV; Determination of Mercury by ICP-MS.** **Method's Archive Box 7 Method 6020B 17 Taylor, J. K., “Quality Assurance of Chemical Measurements”, Lewis Publishers (1987).** **Method 6020B 18 Federal Advisory Committee on Detection and Quantitation Approaches and Uses in** **CleanWaterActPrograms,FinalReport,http://water.epa.gov/scitech/methods/cwa/det/inde x.cfm (December 28, 2007).** **Method 6800, Sec 13** **1 K. E. Jarvis, A. L. Gray and R. S. Houk, Handbook of Inductively Coupled Plasma Mass** **Spectrometry; Blackie Academic & Professional: London, U.K. 1992, p-315. http://www.springerlink.com/content/h62264k1r26m4071/** SW-846 Update VReferences - 12July 2014SW-846 UPDATE V REFERENCE TABLE**Method 6800, Sec 13** **2 G. P. Russ III, J. M. Bazan, Spectrochim. Acta, Part B 1987, 42B, 49- 62. http://www.sciencedirect.com/science/article/pii/0584854787** **800496 Method 6800, Sec** **13 3** **H. E. Taylor, Inductively Coupled Plasma Mass Spectrometry: Practice and Techniques, Academic Press: San Diego, CA, USA, 2001, p-48.** **http://www.sciencedirect.com/science/book/9780126838657 Method 6800, Sec** **13 4** **M. Sargent, R. Harte and C. Harrington, Guidelines for Achieving High Accuracy in Isotope Dilution Mass Spectrometry, The Royal Society of Chemistry: Cambridge, UK,** **2002. http://books.google.com/books/about/Guidelines_for_achievi** **ng_high_accuracy_i.html?id=9wwLS5pcD9sC Method 6800, Sec** **13 5** **“Characterization of waste – State of the art document – Chromium VI specification in solid matrices” PD CEN/TR 14589:2003, British Standards, EU publication “International** **Standards Correspondence Index, Technical Report CEN Technical Committee CEN/TC 292, European Committee for Standardization, 2003.** **http://shop.bsigroup.com/ProductDetail/?pid=000000000030 095298** **Method 6800, Sec 13** **6 The web sites: http://www.epa.gov/epaoswer/hazwaste/test/new-meth.htm contains** **Method 6800 and www.sampleprep.duq.edu and www.sidms.com, contain SIDMS/Method 6800 analysis aids, tutorials, update information and applications (Ref.** **27). Method 6800, Sec** **16 1** **J. D. Fasset and P. J. Paulsen, "Isotope Dilution Mass Spectrometry,"**Anal. Chem**. 1989, 61(10), 643A-649A.** **Method 6800, Sec 16** **2 H. M. Kingston, "Method of Speciated Isotope Dilution Mass Spectrometry," US Patent** **Number: 5,414,259, 1995. http://patft.uspto.gov/netacgi/nph** **Parser?Sect1=PTO1&Sect2=HITOFF&d=PALL&p=1&u=%2 Fnetahtml%2FPTO%2Fsrchnum.htm&r=1&f=G&l=50&s1=5,** **414,259.PN.&OS=PN/5,414,259&RS=PN/5,414,259 Method 6800, Sec** **16 3** **D. Huo and H. M. Kingston, "Correction of Species Transformations in the Analysis of Cr(VI) in Solid Environmental Samples Using Speciated Isotope Dilution Mass** **Spectrometry,"**Anal. Chem. 2000, 72(20), 5047-5054**. http://pubs.acs.org/doi/abs/10.1021/ac000008r** **Method 6800, Sec 16** **4 B. R. James, J. C. Petura, R. J. Vitale and G. R. Mussoline, "Hexavalent Chromium** **Extraction from Soils: A Comparison of Five Methods,"**Environ. Sci. Tech.**1995, 29(9)**,**2377-2381. http://cat.inist.fr/?aModele=afficheN&cpsidt=3643033** **Method 6800, Sec 16** **5 H. M. Kingston, D. Huo, Y. Lu and S. Chalk, "Accuracy in Species Analysis. Speciated** **Isotope Dilution Mass Spectrometry (SIDMS) Exemplified by the Evaluation of Chromium Species,"** Spectrochim. Acta, Part B: Atomic Spectroscopy**, 1998, 53B(2), 299-309.** **http://www.sciencedirect.com/science/article/pii/S058485479 7001432** **Method 6800, Sec 16** **6 D. Huo, H. M. Kingston and B. Larget, “Application of Isotope Dilution in Elemental** **Speciation: Speciated Isotope Dilution Mass Spectrometry (SIDMS),” In:**Comprehensive Analytical Chemistry,**J. A. Caruso, K. L. Sutton and K. L. Ackley (eds.), Vol. 33 (Elemental Speciation: New Approaches for Trace Element Analysis), Elsevier,** **New York, USA, 2000, p-277-313. http://www.sciencedirect.com/science/article/pii/S0166526X** **00800203 Method 6800, Sec** **16 7** **H. M. Kingston, D. Huo, S. Chalk and P. Walter, "The Accurate Determination of Species by Speciated Isotope Dilution Mass Spectrometry: Exemplified by the** **Evaluation of Chromium (VI) in Soil," The Twelfth Annual Waste Testing & Quality Assurance Symposium; Washington, DC, July 23-26, 1996, 112-119.** **Method's Archive Box 7**SW-846 Update VReferences - 13July 2014SW-846 UPDATE V REFERENCE TABLE**Method 6800, Sec 16** **8 D. Huo, Y. Lu and H. M. Kingston, "Determination and Correction of Analytical Biases** **and Study on Chemical Mechanisms in the Analysis of Cr(VI) in Soil Samples Using EPA Protocols,"** Environ. Sci. Tech.**, 1998, 32(21), 3418-3423. http://pubs.acs.org/doi/abs/10.1021/es971029e** **Method 6800, Sec 16** **9 G. N. Bowers, Jr., J. D. Fassett and E. V. White, "IDMS and the National Reference** **System: Accuracy Transfer in Clinical Chemistry,"**Anal. Chem.**, 1993, 65(12), 475 - 479.** **http://pubs.acs.org/doi/abs/10.1021/ac00060a620 Method 6800, Sec** **16 10** **L. J. Moore, H. M. Kingston and T. J. Murphy, "The Use of Isotope Dilution Mass Spectrometry for the Certification of Standard Reference Materials,"** Environ. Intern.**, 1984, 10(2), 169-173.** **Method's Archive Box 7 Method 6800, Sec** **16 11** **H. M. ‘Skip’ Kingston, D. Huo, G. M. M. Rahman, and P. Walter, SamplePrep Web [Homepage of SamplePrep Web], Available: http://www.sampleprep.duq.edu/,** **referenced 2011. Method 6800, Sec** **16 12** **D. Huo, “The Development of Methods in Speciated Isotope Dilution Mass Spectrometry (SIDMS) for Elemental Speciation of Chromium in Environmental Samples Using LC** **ICP-MS,”**Doctoral Dissertation**, Duquesne University, July 30, 1999. Method 6800, Sec** **16 13** **G. M. M. Rahman, H. M. Skip Kingston, T. G. Towns, R. J. Vitale and K. R. Clay, “Determination of hexavalent chromium by using speciated isotope-dilution mass** **spectrometry after microwave speciated extraction of environmental and other solid materials,”** Anal. Bioanal. Chem**., 2005, 382(4), 1111-1120. http://www.springerlink.com/content/lh1m670w184184rr/** **Method 6800, Sec 16** **14 H. M. “Skip” Kingston, R. Cain, D. Huo and G. M. M. Rahman, “Determination and** **evaluation of hexavalent chromium in power plant coal combustion by-products and cost effective environmental remediation solutions using acid mine drainage,”** J. Environ.Monit.**, 2005, 7, 899-905. http://pubs.rsc.org/en/Content/ArticleLanding/2005/EM/b504** **724b Method 6800, Sec** **16 15** **G. M. M. Rahman and H. M. ‘Skip’ Kingston, “Development of a microwave-assisted extraction method and isotopic validation of mercury species in soils and sediments,”** J.Anal. At. Spectrom.**, 2005, 20, 183-191. http://pubs.rsc.org/en/Content/ArticleLanding/2005/JA/b4045** **81e Method 6800, Sec** **16 16** **G. M. M. Rahman, H. M. ‘Skip’ Kingston, John Kern, Sarah W. Hartwell, Ramond F. Anderson and Shen-yi Yang, “Inter-laboratory Validation of EPA Method 3200 for** **mercury species analysis using prepared soil reference materials,”**J. AppliedOrganometallic Chem.**, 2005, 19, 301-307. http://onlinelibrary.wiley.com/doi/10.1002/aoc.816/abstract** **Method 6800, Sec 16** **17 G. M. M. Rahman and H. M. ‘Skip’ Kingston, “Application of Speciated Isotope Dilution** **Mass Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and Sediments,”** Anal. Chem**., 2004, 76, 3548-3555. http://pubs.acs.org/doi/abs/10.1021/ac030407x** **Method 6800, Sec 16** **18 H. M. Kingston, “Speciated isotope dilution mass spectrometry of reactive species and** **related methods,” US Patent Number 6 790 673 B1, 2004 and**PCT Int. Appl**. January 28, 1999, Patent No. WO 9939198.** **Method's Archive Box 7 Method 6800, Sec** **16 19** **H. M. Skip Kingston, U.S. Patent Number 6,974,951 B1, “Automated In-Process Ratio Mass Spectrometry” Dec 13, 2005.** **Method 6800, Sec 16** **20 L. Hinojosa Reyes, G. M. M. Rahman, H. M. Skip Kingston, Robust microwave-assisted** **extraction protocol for determination of total mercury and methylmercury in fish tissues, Analytica Chemica Acta, 631, 121-128, 2009.** **http://www.sciencedirect.com/science/article/pii/S000326700 8018229** SW-846 Update VReferences - 14July 2014SW-846 UPDATE V REFERENCE TABLE**Method 6800, Sec 16** **21 G. M. M. Rahman, T. Fahrenholz and H. M. Skip Kingston, “Application of Speciated** **Isotope Dilution Mass Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of Mercury Speciation Transformations in Human Hair” Journal of** **Analytical Atomic Spectrometry, 24, 83-92, 2009. http://pubs.rsc.org/en/Content/ArticleLanding/2009/JA/b8052** **49b Method 6800, Sec** **16 22** **Lu. Yang, E. Ciceri, Z. Mester and R. E. Sturgeon, “Application of Double Spike Isotope Dilution for the Accurate Determination of Cr(III), Cr(VI) and Total Cr in Yeast”,** Anal.Bioanal. Chem**., 2006, (Published online on September 05, 2006, DOI: 10.1007 /s00216-006-0756-z).** **http://www.springerlink.com/content/6871v185q61j2v47/ Method 6800, Sec** **16 23** **H. M. Skip Kingston, Robert McDonald, Ye Han, Jason Wang, June Wang, Michael West, Larry Stewart, Bob Ormond, and Rudy Mui, “Automated, On-Line, Trace** **Contamination and Chemical Species Analysis For the Semiconductor Industry,” American Institute of Physics (AIP), Conference Proceedings, Proceedings form the** **2003 Characterization and Metrology for ULSI Technology Conference, Volume 683, Melville, NY, 2003.** **http://scitation.aip.org/getpdf/servlet/GetPDFServlet?filetype =pdf&id=APCPCS000683000001000592000001&idtype=cvi** **ps&prog=normal&bypassSSO=1 Method 6800, Sec** **16 24** **G. M. Mizanur Rahman, “Development, Research and Validation of Environmental Speciation Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in** **Mercury and Chromium Speciation Analysis.” Duquesne University, Pittsburgh, PA USA, 2004.** **http://digital.library.duq.edu/cdm spiritan/results.php?CISOOP1=any&CISOFIELD1=CISOSE** **ARCHALL&CISOROOT=/etd&CISOBOX1=isotope Method 6800, Sec** **16 25** **Juris Meija, Lu Yang, Joseph A. Caruso, Zoltan Mester, “Calculations of Double Spike Isotope Dilution Results Revisited.” J. Analytical Atomic Spectrometry, 2006** **(Referenced on-line Aug. 2006). http://www.uc.edu/plasmachem/Documents/webpdfs1/Doubl** **e%20Spike%20for%20Isotope%20Ratios.pdf Method 6800, Sec** **16 26** **Gonzalo Manchego, G. M. Mizanur Rahman, Laura Reyes, Panxi Zhao, H. M. Skip Kingston, “Testing is an Essential Part of International Environmental Regulation and** **Commerce Compliance”, Washington DC, NEMC Presentation 2008. Method 6800, Sec** **16 27** **http://www.epa.gov/epaoswer/hazwaste/test/new-meth.htm and www.sampleprep.duq.edu and www.sidms.com.** **Method 6800, Sec 16** **28 John Kern, C. Toews, H. M. Skip Kingston, G. M. M. Rahman, J. Sun, L. H. Reyes,** **Accurate, Explicit Determinations in Speciated Isotope Dilution Mass Spectrometry without Calibration Curves, in revision 2010.** **Method 6800, Sec 16** **29 C. Toews, J. Kern, H. M. Kingston and M. Rahman, “Sensitivity Analysis for Speciated** **Isotope Dilution Mass Spectrometry” Journal of Analytical and Atomic Spectrometry, 25, 196-200, 2010.** **http://math.pugetsound.edu/~ctoews/research/publications/r evision.pdf** **Method 6800, Sec 16** **30 G. M. Mizanur Rahman, Timothy M. Fahrenholz, H. M. Skip Kingston, Matt Puku, J.** **David Hwang, and Lyman A. Young, “Speciation of Mercury in Crude Oil Using Speciated Isotope Dilution Mass Spectrometry” Spectroscopy, 25,1, 36-45, 2010.** **http://spectroscopyonline.findanalytichem.com/spectroscopy /Feature/Speciation-of-Mercury-in-Crude-Oil-Using** **Speciated/ArticleStandard/Article/detail/655117 Method 6800, Sec** **16 31** **G. M. Mizanur Rahman, Timothy M. Fahrenholz, Matt Puku, Panxi Zhao, Laura Reyes, Scott Faber, H. M. Skip Kingston, “Speciation of Mercury in whole human blood by** **SIDMS SPME-GC-ICP-MS with Microwave Assisted Equilibration and Extraction” (in preparation 2010).** SW-846 Update VReferences - 15July 2014SW-846 UPDATE V REFERENCE TABLE**Method 6800, Sec 16** **32 Laura H. Reyes, G. M. Mizanur Rahman, Timothy Fahrenholz, H. M. Skip Kingston,** **“Comparison of methods with respect to efficiencies, recoveries, and quantitation of mercury species interconversions in food demonstrated using tuna fish” Analytical** **Bioanalytical Chemistry, 390, 2123-2132, 2008. http://www.ncbi.nlm.nih.gov/pubmed/18317738** **Method 6800, Sec 16** **33 Gregory M. Zinn, G. M. Mizanur Rahman, Curtis Frantz, Larry Newman, Scott Faber, H.** **M. Skip Kingston, “Zinc Dietary Supplement Contamination with Toxic Antimony Species, (in preparation 2010).** **Method 6800, Sec 16** **34 Rebecca L. Wagner, Stephanie J. Wetzel, Matt Puku, H. M. Skip Kingston, “Glyphosate** **by IDMS and i-Spike IDMS as for Automated and Safe Toxic MS Analysis” (in preparation 2010).** **Method 6800, Sec 16** **35 Timothy Fahrenholz, Hemasudha Chatragadda, Scott Faber, H. M. Skip Kingston,** **“Glutathione analysis as a biomarker for immune stress and autism” (in preparation 2011).** **http://www.liebertonline.com/toc/hum/22/3 Method 6800, Sec** **16 36** **Michael Passineau, Timothy Fahrenholz, Laurie Machen, Zourelias Lee, Katherine Nega, Rachel Paul, Mary MacDougall, Olga Mamaeva, Raymond Benza, Richard Steet,** **Jarrod Barnes, H. M. Skip Kingston. Human Gene Therapy, (Submitted 2010). Method 6800, Sec** **16 37** **NIST Certificate of Analysis SRM 2701 “Hexavalent Chromium in Contaminated Soil (High Level)” (2009).** **https://www-s.nist.gov/srmors/view_detail.cfm?srm=2701 Method 6800, Sec** **16 38** **Stuart Nagourney, Stephen A. Wilson, Brian Buckley, H. M. Skip Kingston, Shen-Yi Yang and Stephen E. Long. Journal of Analytical Atomic Spectroscopy, 23, 1550-1554,** **2008. http://pubs.rsc.org/en/Content/ArticleLanding/2008/JA/b8084** **88b Method 6800, Sec** **16 39** **“Characterization of waste – Stat of the art document – Chromium VI specification in solid matrices” PD CEN/TR 14589:2003, British Standards, EU publication “International** **Standards Correspondence Index, Technical Report CEN Technical Committee CEN/TC 292, European Committee for Standardization, 2003.** **http://shop.bsigroup.com/ProductDetail/?pid=000000000030 095298** **Method 6800, Sec 16** **40 Gregory M. Zinn, G. M. Mizanur Rahman, H. M. Skip Kingston, “Sodium Azide** **Quantification for homeland defense by isotope dilution mass spectrometry EPA Method 6800 (in preparation 2011).** **Method 6800, Sec 16** **41 Eva Krupp, Bruce Milne, Adrin Mestrot, Andrew Meharg and Jorg Feldmann,** **“Investigation into mercury bound to biothiols: structural identification using ESI-ion-trap MS and introduction of a method for their HPLC separation with simultaneous detection** **by ICP-MS and ESI-MS.” Analytical Bioanalytical Chemistry, 390, 1753-1764, 2008. http://www.springerlink.com/content/y7276028411l8p53/fullt** **ext.pdf Method 6800, Sec** **16 42** **US AIR FORCE Task Reports for the Homeland Security and Homeland Defense: extension of EPA Method 6800 conducted between 2007 and 2010 with funding from** **the Headquarters of the US Air Force Surgeon General under the awards, No.FA7014- 07-0014 and No.FA7014-08-C-0029. Report authors: H. M. Skip Kingston, M. Puku, M.** **Rahman, G. M. Zinn, R. L. Wagner. Method 6800, Sec** **16 43** **Timothy Fahrenholz, Scott Faber, H. M. Skip Kingston, John Kern, Matt Pamuku, Hemasudha Chatragadda, Becky Pekar, “Quantification Glutathione Biomarkers in** **Autism” (in preparation 2012).**SW-846 Update VReferences - 16July 2014SW-846 UPDATE V REFERENCE TABLE**Method 6800, Sec 16** **44 Rebecca L. Wagner, Stephanie Wetzel, H. M. Skip Kingston“ Direct Speciated Isotope** **Dilution Mass Spectrometry of Analytical Methodology of Illicit Drug in Urine Using Time of-Flight Mass Spectrometry” (in review 2012).** **Method 8000D 1 References for poor performing compounds can be found at: Department of Defense:** **http://www.a2la.org/forms/DoD_ELAP_Appendix_G1.doc www.a2la.org/forms/DoD_ELAP_Appendix_G1.doc** **Method 8000D 2 “Quality Systems Manual for Environmental Laboratories”, Version 5.0 http://www.denix.osd.mil/edqw/upload/QSM-Version-5-0-** **FINAL.pdf Method 8000D 3** **U.S.E.P.A Contract Laboratory Program SOM 1.2 at: http://www.epa.gov/superfund/programs/clp/som1.htm** **www.epa.gov/superfund/programs/clp/som1.htm Method 8000D 4** **A list of quantitation limits for poor performing volatile compounds can be found in Table App D XIII-1 at: http://www.epa.gov/region1/oeme/appendc.pdf** **www.epa.gov/region1/oeme/appendc.pdf Method 8000D 5** **A list of quantation limits for poor performing semivolatile compounds can be found in Table App E XIII-1 at: http://www.epa.gov/region1/oeme/appendd.pdf** **www.epa.gov/region1/oeme/appendd.pdf Method 8021B 1** **"Volatile Organic Compounds in Water by Purge-and-Trap Capillary Column Gas Chromatography with Photoionization and Electrolytic Conductivity Detectors in Series,** **Method 502.2, Rev. 2.0 (1989); Methods for the Determination of Organic Compounds in Drinking Water," U.S. Environmental Protection Agency, Environmental Monitoring** **Systems Laboratory, Cincinnati, OH, EPA/600/4-88/039, December 1988. http://www.caslab.com/EPA-Methods/PDF/502_2.pdf** **Method 8021B 2 "The Determination of Halogenated Chemicals in Water by the Purge and Trap** **Method," Method 502.1; U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, September 1986.** **Method 8021B 3 "Volatile Aromatic and Unsaturated Organic Compounds in Water by Purge and Trap** **Gas Chromatography, Method 503.1;" U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH, September 1986.** **Method 8021B 4 J. A. Glaser, D. L. Forest, G. D. McKee, S. A. Quave, W. L. Budde, "Trace Analyses for** **Wastewaters," Environ. Sci. Technol. 1981, 15, 1426. http://pubs.acs.org/doi/abs/10.1021/es00094a002** **Method 8021B 5 T. A. Bellar, J. J. Lichtenberg, "The Determination of Synthetic Organic Compounds in** **Water by Purge and Sequential Trapping Capillary Column Gas Chromatography," U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory,** **Cincinnati, OH 45268. http://books.google.com/books/about/The_Determination_of** **_Synthetic_Organic_C.html?id=Sdr5GwAACAAJ Method 8111 1** **V. Lopez-Avila, E. Baldin, J. Benedicto, J. Milanes, W. F. Beckert, "Application of Open Tubular Columns to SW-846 GC Methods," Final Report to the US EPA on Contract 68-** **03-3511, Mid-Pacific Environmental Laboratory, Mountain View, CA, 1990. Method 8111 2** **S. Tsang, P. Marsden, N. Chau, "Performance Data for Methods 8041, 8091, 8111, and 8121A," Draft Report to US EPA on Contract 68-W9-0011, Science Applications** **International Corp., San Diego, CA, 1992.**SW-846 Update VReferences - 17July 2014SW-846 UPDATE V REFERENCE TABLE**Method 8270D 1 J. W. Eichelberger, L. E. Harris, and W. L. Budde, "Reference Compound to Calibrate** **Ion Abundance Measurement in Gas Chromatography-Mass Spectrometry Systems," Analytical Chemistry, 47, 995-1000, 1975.** **http://pubs.acs.org/doi/abs/10.1021/ac60357a061 Method 8270D 2** **P. Olynk, W. L. Budde, and J. W. Eichelberger, "Method Detection Limit for Methods 624 and 625," unpublished report, October 1980.** **Method 8270D 3 "Interlaboratory Method Study for EPA Method 625-Base/Neutrals, Acids, and** **Pesticides," Final Report for EPA Contract 68-03-3102. Method 8270D 4** **J. A. Burke, "Gas Chromatography for Pesticide Residue Analysis: Some Practical Aspects," Journal of the Association of Official Analytical Chemists (AOAC), 48, 1037,** **1965. Method 8270D 5** **S. V. Lucas, R. A. Kornfeld, "GC-MS Suitability Testing of RCRA Appendix VIII and Michigan List Analytes," U.S. Environmental Protection Agency, Environmental** **Monitoring and Support Laboratory, Cincinnati, OH 45268, February 20, 1987, Contract No. 68-03-3224.** **http://books.google.com/books/about/GC_MS_Suitability_Te sting_of_RCRA_Append.html?id=d6yqSgAACAAJ** **Method 8270D 6 T. M. Engel, R. A. Kornfeld, J. S. Warner, and K. D. Andrews, "Screening of** **Semivolatile Organic Compounds by Extractability and Aqueous Stability by SW-846, Method 3510," U.S. Environmental Protection Agency, Environmental Monitoring and** **Support Laboratory, Cincinnati, OH 45268, June 5, 1987, Contract 68-03-3224. http://nepis.epa.gov/Exe/ZyNET.exe/2000TMKH.TXT?ZyActi** **onD=ZyDocument&Client=EPA&Index=1986+Thru+1990&D ocs=&Query=&Time=&EndTime=&SearchMethod=1&TocRe** **strict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMo nth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQue** **ry=&File=D%3A%5Czyfiles%5CIndex%20Data%5C86thru90 %5CTxt%5C00000011%5C2000TMKH.txt&User=ANONYM** **OUS&Password=anonymous&SortMethod=h%7C- &MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r** **75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPa ge=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc** **=Results%20page&MaximumPages=1&ZyEntry=1&SeekPa ge=x&ZyPURL** **Method 8270D 7 V. Lopez-Avila (W. Beckert, Project Officer); "Development of a Soxtec Extraction** **Procedure for Extraction of Organic Compounds from Soils and Sediments," U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory,** **Las Vegas, NV, October 1991; EPA 600/X-91/140. http://books.google.com/books/about/Development_of_a_So** **xtec_Extraction_Proce.html?id=SsA8twAACAAJ**SW-846 Update VReferences - 18July 2014SW-846 UPDATE V REFERENCE TABLE**Method 8270D 8 J. Bursey, R. Merrill, R. McAllister, and J. McGaughey, "Laboratory Validation of VOST** **and SemiVOST for Halogenated Hydrocarbons from the Clean Air Act Amendments List," Vol. 1 and 2, U.S. Environmental Protection Agency, EPA 600/R-93/123a and b,** **(NTIS PB 93-227163 and 93-27171), Research Triangle Park, NC, July 1993. http://nepis.epa.gov/Exe/ZyNET.exe/30003WHW.TXT?ZyAc** **tionD=ZyDocument&Client=EPA&Index=1991+Thru+1994& Docs=&Query=&Time=&EndTime=&SearchMethod=1&TocR** **estrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldM onth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQu** **ery=&File=D%3A%5Czyfiles%5CIndex%20Data%5C91thru9 4%5CTxt%5C00000009%5C30003WHW.txt&User=ANONY** **MOUS&Password=anonymous&SortMethod=h%7C- &MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r** **75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPa ge=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc** **=Results%20page&MaximumPages=1&ZyEntry=1&SeekPa ge=x&ZyPURL** **Method 8270D 9 B. Richter, J. Ezzell, and D. Felix, "Single Laboratory Method Validation Report:** **Extraction of Target Compound List/Priority Pollutant List BNAs and Pesticides Using Accelerated Solvent Extraction (ASE) with Analytical Validation by GC/MS and** **GC/ECD," Document 101124, Dionex Corporation, Salt Lake City, UT, June 16, 1994. Method 8270D 10** **H. B. Lee, T. E. Peart, R. L. Hong-You, and D. R. Gere, "Supercritical Carbon Dioxide Extraction of Polycyclic Aromatic Hydrocarbons from Sediments," J. Chromatography A,** **653, 83-91 (1993). http://www.sciencedirect.com/science/article/pii/0021967393** **80394N Method 8270D 11** **S. Warner, "SFE Extraction of PNAs from Solid Matrices Using the Dionex 703M SFE Extractor and a Liquid Trap," EPA Region III, Central Regional Laboratory, 839 Bestgate** **Road, Annapolis, MD 21401, December 12, 1994. Method 8270D 12 C. Markell, "3M Data Submission to EPA," letter to B. Lesnik, June 27, 1995.** **Method 8270D 13 USEPA Method 525.2, "Determination of Organic Compounds in Drinking Water by** **Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry," Environmental Monitoring Systems Laboratory, Office of Research and** **Development, US EPA, Cincinnati, OH, Revision 2.0, March 1995. http://water.epa.gov/scitech/methods/cwa/upload/525_2-** **SOCs.pdf Method 8270D 14** **USEPA, Superfund Analytical Services/Contract Laboratory Program (CLP), Multi Media, Multi-Concentration Organics Analysis, SOM01.X, Exhibit D - Analytical** **Methods, "Analytical Method for the Analysis of Semivolatile Organic Compounds," November, 2003.** **Method 8276 1 A. G. Harrison (2nd ed.), Chemical Ionization Mass Spectrometry, CRC Press, Boca** **Raton, FL, 1992. Method 8276 2** **W. C. Brumley, C. M. Brownrigg, and A. H. Grange, "Determination of Toxaphene in Soil by Electron-Capture Negative Ion Mass Spectrometry After Fractionation by High** **Performance Gel Permeation Chromatography," J. Chromatogr., 633, 177-183, 1993. http://www.epa.gov/esd/chemistry/org-** **anal/reports/toxpf/toxpf.htm**SW-846 Update VReferences - 19July 2014SW-846 UPDATE V REFERENCE TABLE**Method 8276 3 Brumley, W. C. "Analytical Protocol (GC/NIMS) for OSWER's Response to OIG Report** **(2005-P-00022) on Toxaphene Analysis." EPA/600/R-08/048. (TIP # 08-069, Published Report) U.S. Environmental Protection Agency, Washington, DC, 2008.** **http://nepis.epa.gov/Adobe/PDF/9100D5NZ.PDF Method 8276 4** **V. Lopez-Avila, E. Baldin, J. Benedicto, J. Milanes, W. F. Beckert, "Application of Open Tubular Columns to SW-846 GC Methods," Report for the U.S. Environmental** **Protection Agency, Contract 68-03-3511, Mid-Pacific Environmental Laboratory, Mountain View, CA, 1990.** **http://nepis.epa.gov/Exe/ZyNET.exe/30003UMO.TXT?ZyActi onD=ZyDocument&Client=EPA&Index=1986+Thru+1990&D** **ocs=&Query=&Time=&EndTime=&SearchMethod=1&TocRe strict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMo** **nth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQue ry=&File=D%3A%5Czyfiles%5CIndex%20Data%5C86thru90** **%5CTxt%5C00000006%5C30003UMO.txt&User=ANONYM OUS&Password=anonymous&SortMethod=h%7C-** **&MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r 75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPa** **ge=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc =Results%20page&MaximumPages=1&ZyEntry=1&SeekPa** **ge=x&ZyPURL Method 8276 5** **"Development and Application of Test Procedures for Specific Organic Toxic Substances in Wastewaters," Category 10, Pesicides and PCB Report for the U.S.** **Environmental Protection Agency, Contract 68-03-2606 http://nepis.epa.gov/Exe/ZyNET.exe/2000V0S8.TXT?ZyActi** **onD=ZyDocument&Client=EPA&Index=1976+Thru+1980&D ocs=&Query=&Time=&EndTime=&SearchMethod=1&TocRe** **strict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFieldMo nth=&QFieldDay=&IntQFieldOp=0&ExtQFieldOp=0&XmlQue** **ry=&File=D%3A%5Czyfiles%5CIndex%20Data%5C76thru80 %5CTxt%5C00000006%5C2000V0S8.txt&User=ANONYMO** **US&Password=anonymous&SortMethod=h%7C- &MaximumDocuments=1&FuzzyDegree=0&ImageQuality=r** **75g8/r75g8/x150y150g16/i425&Display=p%7Cf&DefSeekPa ge=x&SearchBack=ZyActionL&Back=ZyActionS&BackDesc** **=Results%20page&MaximumPages=1&ZyEntry=1&SeekPa ge=x&ZyPURL** **Method 8276 6 D. F. Goerlitz, L. M. Law, "Removal of Elemental Sulfur Interferences from Sediment** **Extracts for Pesticide Analysis," Bull. Environ. Contam. Toxicol., 6, 9, 1971. http://www.springerlink.com/content/v4u6174186w55721/** **Method 8276 7 S. Jensen, L. Renberg, L. Reutergardth, "Residue Analysis of Sediment and Sewage** **Sludge for Organochlorines in the Presence of Elemental Sulfur," Anal. Chem. 49, 316- 318, 1977.** **http://pubs.acs.org/doi/abs/10.1021/ac50010a033 Method 8276 8** **R. H. Wise, D. F. Bishop, R. T. Williams, B. M. Austern, "Gel Permeation Chromatography in the GC/MS Analysis of Organics in Sludges," U.S. Environmental** **Protection Agency, Cincinnati, OH.**SW-846 Update VReferences - 20July 2014SW-846 UPDATE V REFERENCE TABLE**Method 8276 9 H. B. Pionke, G. Chesters, D. E. Armstrong, "Extraction of Chlorinated Hydrocarbon** **Insecticides from Soil," Agron. J., 60, 289, 1968. https://www.agronomy.org/publications/aj/abstracts/60/3/AJ0** **600030289 Method 8276 10** **J. A. Burke, P. A. Mills, D. C. Bostwick, "Experiments with Evaporation of Solutions of Chlorinated Pesticides," J. Assoc. Off. Anal. Chem., 49, 999, 1966.** **Method 8276 11 J. A. Glazer, et. al., "Trace Analyses for Wastewaters," Environ. Sci. and Technol., 15,** **1426, 1981. http://pubs.acs.org/doi/abs/10.1021/es00094a002** **Method 8276 12 P. J. Marsden, "Performance Data for SW-846 Methods 8270, 8081, and 8141," U.S.** **Environmental Protection Agency, EMSL-Las Vegas, EPA/600/4-90/015. http://nepis.epa.gov/Exe/ZyNET.exe/9100CV89.txt?ZyAction** **D=ZyDocument&Client=EPA&Index=1986%20Thru%20199 0&Docs=&Query=&Time=&EndTime=&SearchMethod=1&To** **cRestrict=n&Toc=&TocEntry=&QField=&QFieldYear=&QFiel dMonth=&QFieldDay=&UseQField=&IntQFieldOp=0&ExtQFi** **eldOp=0&XmlQuery=&File=D%3A%5CZYFILES%5CINDEX %20DATA%5C86THRU90%5CTXT%5C00000020%5C9100** **CV89.txt&User=ANONYMOUS&Password=anonymous&Sor tMethod=h%7C** **Method 8276 13 V. Lopez-Avila, (Beckert, W., Project Officer), "Development of a Soxtec Extraction** **Procedure for Extracting Organic Compounds from Soils and Sediments," EPA 600/X 91/140, U.S. Environmental Protection Agency, Environmental Monitoring Systems** **Laboratory, Las Vegas, NV, October 1991. Method 8276 14** **C. Markell, "Solid-Phase Extraction of TCLP Leachates," Proceedings of the Tenth Annual Waste Testing and Quality Assurance Symposium, Arlington, VA, July, 1994.** **Method 8276 15 D. Bennett, B. Lesnik, S. M. Lee, "Supercritical Fluid Extraction of Organochlorine** **Pesticide Residues from Soils," Proceedings of the Tenth Annual Waste Testing and Quality Assurance Symposium, Arlington, VA, July, 1994.** **Method 8276 16 C. Markell, "3M Data Submission to EPA," Letter to B. Lesnik, June 27, 1995. Method 8276 17** **B. Richter, J. Ezzell, D. Felix, "Single Laboratory Method Validation Report - Extraction of Organophosphorus Pesticides, Herbicides, and Polychlorinated Biphenyls Using** **Accelerated Solvent Extraction (ASE) with Analytical Validation by GC/NPD and GC/ECD," Dionex, Salt Lake City, UT, Document 101124, December 2, 1994.** **Method 8276 18 K. Li, J. M. R. Bélanger, M. P. Llompart, R. D. Turpin, R. Singhvi, and J. R. J. Paré.** **Evaluation of Rapid Solid Sample Extraction Using the Microwave-Assisted Process (MAP** **TM ) Under Closed-Vessel Conditions. Spectros. Int. J. 13 (1), 1-14, 1997.** **http://www.cem.de/documents/pdf/RE/RE036.PDF Method 8276 19** **L. D. Betowski, H. M. Webb, and A. D. Sauter. Pulsed Positive Ion Negative Ion Chemical Ionization Mass Spectrometric Applications to Environmental and Hazardous** **Waste Analysis. Biomed. Mass Spectrom. 10, 369, 1983.**SW-846 Update VReferences - 21July 2014SW-846 UPDATE V REFERENCE TABLE**Method 8276 20 Science Applications International Corporation, "Interlaboratory Study Plan for** **Validation of Method 8276," Submitted to U.S. Environmental Protection Agency, November 2008.** **Method 8276 21 USEPA Region 4 Modified Method 3545A Standard Operating Procedure (SOP) for** **Pressurized Fluid Extraction (PFE), Revision 4.1, November 5, 2010. Method 8276 22** **USEPA Region 4 Modified Method 3620C, SOP for Florisil® Cleanup, Revision 3.0, August 23, 2010.** **Method 8276 23 USEPA Region 4 Modified Method 3630C SOP for Silica Gel Cleanup, Revision 3.1,** **August 10, 2011. Method 8276 24** **TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Study Plan," Submitted to U.S. Environmental Protection Agency, September 2011.** **Method 8276 25 TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Analytical Data** **Report," Submitted to U.S. Environmental Protection Agency, May 2012. Method 8276 26** **TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Data Validation Report," Submitted to U.S. Environmental Protection Agency, May 2012.** **Method 8276 27 TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Statistical Analysis** **Report," Submitted to U.S. Environmental Protection Agency, May 2012. Method 8276 28** **H. Parlar, D. Angerhöfer, M. Coelhan, L. Kimmel, "HRGC and HRGC-ECNI Determination of Toxaphene Residues in Fish with a New 22 Components Standard,"** **Organohalogen Compd., 26, 357, 1995. http://www.dioxin20xx.org/pdfs/1995/95-279.pdf** **Method 8410 1 Handbook for Analytical Quality Control in Water and Wastewater Laboratories** **; U.S. Environmental Protection Agency. Environmental Monitoring and Support Laboratory.** **ORD Publication Offices of Center for Environmental Research Information: Cincinnati, OH, March 1979; Sec. 4, EPA-600/4-79-019.** **http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=30000PWG.t xt** **Method 8410 2 R. R. Freeman, Hewlett Packard Application Note: Quantitative Analysis Using a** **Purged Splitless Injection Technique ; ANGC 7-76.** **Method 8410 3 R. H. Cole, Tables of Wavenumbers for the Calibration of Infrared Spectrometers** **; Pergamon: New York, 1977.** **http://books.google.com/books/about/Tables_of_wavenumb ers_for_the_calibratio.html?id=i7_vAAAAMAAJ** **Method 8410 4 J. G. Grasselli, P. R. Griffiths, R. W. Hannah, "Criteria for Presentation of Spectra from** **Computerized IR Instruments"; Appl. Spectrosc. 1982, 36** **, 87. http://www.opticsinfobase.org/as/abstract.cfm?id=127579** **Method 8410 5 R. A. Nyquist, The Interpretation of Vapor-Phase Infrared Spectra** **. Group Frequency Data** **; Volume I. Sadtler Laboratories: Philadelphia, PA, 1984. Method 8410 6** **G. Socrates, Infrared Characteristic Group Frequencies ; John Wiley and Sons: New** **York, NY, 1980. http://www.amazon.com/Infrared-Characteristic-Group-** **Frequencies-Socrates/dp/0471275921**SW-846 Update VReferences - 22July 2014SW-846 UPDATE V REFERENCE TABLE**Method 8410 7 L. J. Bellamy, The Infrared Spectra of Complex Organic Molecules** **; 2nd ed.; John Wiley and Sons: New York, NY, 1958.** **http://www.amazon.com/infra-red-spectra-complex molecules/dp/B007T3ZVP0/ref=sr_1_2?s=books&ie=UTF8&** **qid=1355851489&sr=1-2&keywords=infra red+spectra+complex+molecules** **Method 8410 8 H. A. Szymanski, Infrared Band Handbook** **, Volumes I and II; Plenum: New York, NY, 1965.** **Method 8410 9 D. F. Gurka, "Interim Protocol for the Automated Analysis of Semivolatile Organic** **Compounds by Gas Chromatography/Fourier Transform-Infrared Spectrometry"; Appl. Spectrosc.** **1985, 39 , 826.** **http://www.opticsinfobase.org/as/abstract.cfm?uri=as-39-5- 827** **Method 8410 10 P. R. Griffiths, J. A. de Haseth, L. V. Azarraga, "Capillary GC/FT-IR"; Anal. Chem.** **1983, 55** **, 1361A. http://pubs.acs.org/doi/abs/10.1021/ac00263a784** **Method 8410 11 P. R. Griffiths, J. A. de Haseth, Fourier Transform-Infrared Spectrometry** **; Wiley- Interscience: New York, NY, 1986.** **http://onlinelibrary.wiley.com/doi/10.1002/9780470106310.f matter/pdf** **Method 8410 12 D. F. Gurka, I. Farnham, B. B. Potter, S. Pyle, R. Titus, W. Duncan, "Quantitation** **Capability of a Directly Linked Gas Chromatography/Fourier Transform Infrared/Mass Spectrometry System"; Anal. Chem.** **1989, 61 , 1584.** **http://pubs.acs.org/doi/pdf/10.1021/ac00189a022 Method 8430 1** **W. D. Payne, T. W. Collette, "Identification of Bis(2-chloroethyl) ether Hydrolysis Products by Direct Aqueous Injection GC/FT-IR," J. of High Res. Chrom.** **, 12, 693-696, 1989.** **http://onlinelibrary.wiley.com/doi/10.1002/jhrc.1240121016/a bstract** **Method 9013A 1 American Society for Testing and Materials, "Understanding Cyanide Species," D 6696,** **ASTM International, 2004. www.astm.org** **Method 9013A 2 R. S. Ghosh, D. A. Dzombak, R. G. Luthy, "Equilibrium Precipitation and Dissolution of** **Iron Cyanide Solids in Water," Environ. Eng. Sci., Vol. 16, 293-313, 1999. Method 9013A 3** **J. C. L. Meeussen, M. G. Keizer, W. H. van Riemsdijk, F. A. M. de Haan, "Dissolution Behavior of Iron Cyanide (Prussian Blue) in Contaminated Soils," Environ. Sci. Technol.,** **Vol. 26, 1832-1838, 1992. Method 9013A 4** **J. C. L Meeussen, W. H. Keizer, F. A. M. de Haan, "Chemical Stability and Decomposition Rate of Iron Cyanide Complexes in Soil Solutions," Environ. Sci.** **Technol., Vol. 26, 511-516, 1992. Method 9013A 5** **J. T. Bushey, D. A. Dzombak, "Ferrocyanide Adsorption on Aluminum Oxides," J. Coll. Int. Sci., Vol. 272, 46-51, 2004.** **Method 9013A 6 T. L. Theis, M. L West, "Effects of Cyanide Complexation on the Adsorption of Trace** **Metals at the Surface of Goethite," Environ. Technol. Letters, Vol. 7, 309-318, 1986. Method 9013A 7** **The RETEC Group, Inc., "Metal Cyanide Complexes by Anion Exchange Chromatography and UV Detection Method Validation Summary Report," March, 2004.** **Method 9014 There are no references directly related to this method. References on total and** **amenable cyanide can be found in Method 9010.**SW-846 Update VReferences - 23July 2014SW-846 UPDATE V REFERENCE TABLE**Method 9015 1 American Society for Testing and Materials, "Standard Test Method for Determination of** **Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water using Anion Exchange Chromatography with UV Detection," D 6994, ASTM** **International, 2004. This reference can be purchased on line at ASTM’s web site: http://www.astm.org** **www.astm.org Method 9015 2** **Dionex Corporation, "Determination of Metal Cyanides," Dionex Application Note No. 55, November, 1989.** **http://www.dionex.com/en-us/webdocs/4151-AN55_V15.pdf Method 9015 3** **American Society for Testing and Materials, "Standard Guide for Understanding Cyanide Species," D 6696, ASTM International, 2004. This reference can be purchased** **on line at ASTM’s web site: http://www.astm.org Method 9015 4** **R. S. Ghosh, D. A. Dzombak, R. G. Luthy, "Equilibrium Precipitation and Dissolution of Iron Cyanide Solids in Water,"** Environ. Eng. Sci.**, Vol. 16, 293-313, 1999. http://cat.inist.fr/?aModele=afficheN&cpsidt=1890662** **Method 9015 5 J. C. L. Meeussen, W. H. Keizer, F. A. M. de Haan, "Chemical Stability and** **Decomposition Rate of Iron Cyanide Complexes in Soil Solutions,"**Environ. Sci.Technol.**, Vol. 26, 511-516, 1992. http://pubs.acs.org/doi/abs/10.1021/es00027a010** **Method 9015 6 J. C. L. Meeussen, M. G. Keizer, W. H. van Riemsdijk, F. A. M. de Haan "Dissolution** **Behavior of Iron Cyanide (Prussian Blue) in Contaminated Soils,"**Environ. Sci.Technol.**, Vol. 26, 1832-1838, 1992. Method 9015 7** **U.S. Environmental Protection Agency, "Cyanide Extraction Procedure for Solids and Oils, Method 9013" U.S. EPA Office of Solid Waste SW-846 Manual.** **Method 9015 8 P. Doudoroff, "Toxicity to Fish of Cyanides and Related Compounds: A Review," EPA** **Report No. 600/3-76-038, 1976. http://books.google.com/books?id=bXaxa306tpwC&pg=PR7** **&source=gbs_toc_r&cad=4#v=onepage&q&f=false Method 9015 9** **U.S. Environmental Protection Agency, "Total and Amenable Cyanide: Distillation, Method 9010" U.S. EPA Office of Solid Waste SW-846 Manual.** **Method 9015 10 American Society for Testing and Materials, "Standard Test Methods for Cyanides in** **Water," D 2036, ASTM International, 2004. This reference can be purchased on line at ASTM’s web site: http://www.astm.org** **Method 9015 11 American Public Health Association, "Standard Methods for the Examination of Water** **and Wastewater," 20 th** **Edition, 1998. Method 9015 12** **R. A. Wetzel, C. L. Anderson, H. Schleicher, G. D. Crook, "Determination of Trace Level Ions by Ion Chromatography with Concentrator Columns,"** Analytical Chemistry**, Vol. 15, No. 9, 1532-1535, 1979.** **http://pubs.acs.org/doi/abs/10.1021/ac50045a040 Method 9015 13** **W. S. Rader, L. Solujic, E. B. Milosavljevic, J. L. Hendrix, "Sunlight-Induced Photochemistry of Aqueous Solutions of Hexacyanoferrate(II) and –(III) Ions,"** Environ.Sci. Technol.**, Volume 27, 1875-1879, 1993. http://pubs.acs.org/doi/abs/10.1021/es00046a016** **Method 9015 14 L. Moggi, F. Bolletta, V. Balzani, F. Scandola, "Photochemistry of Co-ordination** **Compounds_XV,"**J. inorg. Nucl. Chem.**, Vol. 28, 2589-2597, 1966. http://www.sciencedirect.com/science/article/pii/0022190266** **803834 Method 9015 15** **Dionex Corporation, "Product Manual IonPacÒ ATC-3 2-mm Anion Trap Column IonPac ATC-3 4-mm Anion Trap Column IonPac ATC-HC Anion Trap Column," Document No.** **032697, Revision 08, July 12, 2002. http://www.dionex.com/en-us/webdocs/40850-32697-** **08_IonPacATC-HC_3_MAN_V16.pdf**SW-846 Update VReferences - 24July 2014SW-846 UPDATE V REFERENCE TABLE**Method 9015 16 Dionex Corporation, "Product Manual IonPacÒ AG2 Guard Column IonPacÒ AG3** **Guard Column IonPacÒ AG4 Guard Column IonPacÒ AG5 Guard Column IonPacÒ CG2 Guard Column IonPacÒ AS2 Analytical Column IonPacÒ AS3 Analytical Column** **IonPacÒ AS4 Analytical Column IonPacÒ AS5 Analytical Column IonPacÒ CS2 Analytical Column," Document No. 032226, Revision 14, May 12, 2002.** **http://www.dionex.com/en-us/webdocs/4395-32226- 14_AS2345_CS2_V17.pdf** **Method 9015 17 Dionex Corporation, "Product Manual IonPacÒ AG11 Guard Column IonPacÒ AS11** **Analytical Column," Document No. 034791, Revision 08, May 14, 2003. http://www.dionex.com/en-us/webdocs/4445-Man-034791-12-** **IonPac-AS11-Apr10.pdf Method 9015 18** **Dionex Corporation, "Dionex Installation and Troubleshooting Guide for the IonPacÒ MFC-1 Metal-Free Trap Column," Document No. 034990, Revision 02, June 26, 1998.** **http://www.dionex.com/en-us/webdocs/4463-34990- 04_IP_MFC_V30.pdf** **Method 9015 19 U.S. Environmental Protection Agency, "Determinative Chromatographic Separations,** **Method 8000" U.S. EPA Office of Solid Waste SW-846 Manual. Method 9015 20** **R. M. Smith, A. E. Martell, "NIST Critically Selected Stability Constants of Metal Complexes Database, Version 5.0 Database Software" NIST Standard Reference** **Database 46, U.S. Department of Commerce, Gaithersburg, Maryland, 1998. http://www.nist.gov/srd/nist46.cfm** **Method 9015 21 D. D. Wagman, W. H. Evans, V. B. Parker, R. H. Shumm, I. Halow, S. M. Bailey, K. L.** **Churney, R. L. Nuttal, "The NBS Tables of Chemical Thermodynamic Properties, Selected Values for Inorganic and C** **1 and C** **2 Organic Substances in SI Units,"** Journalof Physical and Chemical Reference Data**, Vol. 11, Supplement 2, 1-392, 1982. http://jpcrd.aip.org/jpcrbu/v18/i4/p1807_s1?isAuthorized=no** **Method 9015 22 The RETEC Group, Inc., "Metal Cyanide Complexes by Anion Exchange** **Chromatography and UV Detection Method Validation Summary Report," March, 2004. Method 9015 23** **U.S. Environmental Protection Agency, "Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation), Method 9012" U.S. EPA Office of Solid Waste** **SW-846 Manual. Method 9320 1** **Greenberg, A.E., J.J. Connors, and D.J. Jenkens, eds., Standard Methods for the Examination of Water and Wastewater, 15** **th ed., American Public Health Assoc.,** **Washington, D.C., Method 707, p. 600, 1980. http://www.standardmethods.org/** **Method 9320 2 Johnson, J.O., Determination of Radium 228 in Natural Waters. Radiochemical** **Analysis of Water. U.S. Geol. Surv., Water Supply Paper 1696-G. U.S. Govt. Printing Office, Washington, D.C., 1971.** **http://pubs.usgs.gov/wsp/1696g/report.pdf Method 9320 3** **Krieger, H.L., Prescribed Procedures for Measurement of Radioactivity in Drinking Water, Environmental Monitoring and Support Laboratory, U.S. EPA, Cincinnati, OH,** **EPA-600/4-75-008, 1976. http://nepis.epa.gov/** **Chapter 1 1 USEPA.** Guidance on Systematic Planning Using the Data Quality Objectives Process,EPA QA/G-4**. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006.** **http://www.epa.gov/quality/qs-docs/g4-final.pdf**SW-846 Update VReferences - 25July 2014SW-846 UPDATE V REFERENCE TABLE**Chapter 1 2 USEPA.** EPA Quality Manual for Environmental Programs CIO 2105-P-01-0**. Office of Environmental Information Quality Staff, United States Environmental Protection** **Agency, Washington, D.C. May 5, 2000. http://www.epa.gov/irmpoli8/policies/2105P010.pdf.** **Chapter 1 3 USEPA.** Guidance on Choosing a Sampling Design for Environmental Data Collection,**EPA QA/G-5S. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. December 2002.** **http://www.epa.gov/quality/qs-docs/g5s-final.pdf Chapter 1 4** **USEPA.**Guidance on Environmental Data Verification and Data Validation**, EPA QA/G 8** .**Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. November 2002.** **http://www.epa.gov/quality/qs-docs/g8-final.pdf Chapter 1 5** **USEPA.**Data Quality Assessment: A Reviewer’s Guide**, QA/G-9R. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. February 2006. http://www.epa.gov/quality/qs-docs/g9r-final.pdf** **Chapter 1 6 USEPA.** Data Quality Assessment: Statistical Tools For Practitioners**, QA/G-9S. Quality Staff, Office of Environmental Information, United States Environmental** **Protection Agency, Washington, D.C. February 2006. http://www.epa.gov/quality/qs-docs/g9s-final.pdf** **Chapter 1 7 USEPA.** Guidance for Preparing Standard Operating Procedures**, EPA QA/G-6** .**Quality Staff, Office of Environmental Information, United States Environmental Protection** **Agency, Washington, D.C. April 2007. http://www.epa.gov/quality/qs-docs/g6-final.pdf** **Chapter 1 8 USEPA.** RCRA Waste Sampling Draft Technical Guidance.**Office of Solid Waste, United States Environmental Protection Agency, Washington, D.C. August 2002.** **http://www.epa.gov/wastes/hazard/testmethods/sw846/pdfs/r wsdtg_a.pdf** **Chapter 1 9 USPEA.** Guidance for Quality Assurance Project Plans**, EPA QA/G-5. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency,** **Washington, D.C. December 2002. http://www.epa.gov/quality/qs-docs/g5-final.pdf** **Chapter 1 10 USEPA.** EPA Requirements for Quality Assurance Project Plans**, EPA QA/R-5. Quality Staff, Office of Environmental Information. United States Environmental Protection** **Agency, Washington, D.C. March 2001. http://www.epa.gov/quality/qs-docs/r5-final.pdf** **Chapter 1 11** **USEPA.**RCRA Delisting Program Guidance Manual for the Petitioner**. United States http://www.epa.gov/region6/6pd/rcra_c/pd-o/delist23.pdf** **Chapter 1 12 USEPA.** Waste Analysis at Facilities That Generate, Treat, Store and Dispose ofHazardous Wastes**, ECDIC 2002-011. Office of Waste Programs Enforcement, United States Environmental Protection Agency. April 1994.** **http://www.epa.gov/compliance/resources/policies/civil/rcra/ wasteanalygman-rpt.pdf** **Chapter 1 13 USEPA.** Guidance on Technical Audits and Related Assessments for EnvironmentalData Operations**, QA/G-7. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. January 2000.** **http://www.epa.gov/quality/qs-docs/g7-final.pdf Chapter 2** **1 M. J. Barcelona, "TOC Determinations in Ground Water,"** **Ground Water** **1984, 22(1)** **, 18- http://info.ngwa.org/gwol/pdf/840629056.PDF** **Chapter 2 2 R. Riggin, et al.; Development and Evaluation of Methods for Total Organic Halide and** **Purgeable Organic Halide in Wastewater ; U.S. Environmental Protection Agency; Office** **of Research and Development; Environmental Monitoring and Support Laboratory; ORD Publication Offices of Center for Environmental Research Information; Cincinnati, OH,** **1984; EPA-600/4-84-008. http://nepis.epa.gov/Exe/ZyPURL.cgi?Dockey=500024JK.txt** SW-846 Update VReferences - 26July 2014SW-846 UPDATE V REFERENCE TABLE**Chapter 2 3 G. McKee, et al.; Determination of Inorganic Anions in Water by Ion Chromatography** **(Technical addition to Methods for Chemical Analysis of Water and Wastewater, EPA 600/4-79-020); U.S. Environmental Protection Agency; Environmental Monitoring and** **Support Laboratory; ORD Publication Offices of Center for Environmental Research Information; Cincinnati, OH, 1984; EPA-600/4-84-017.** **Chapter 3 1 Skoog, D. A., "Principles of Instrumental Analysis," 3rd ed, Saunders College** **Publishing, Philadelphia, PA, 1985. http://www.4shared.com/get/C9SkaLKp/Skoog_-** **_Principles_of_Instrume.html Chapter 3 2** **EPA, U.S., "Sampling Ambient Water for Trace Metals at EPA Water Quality Criteria Levels, Method 1669, U.S. Environmental Protection Agency, Office of Water,** **Washington, D.C., 1996. http://www.ecy.wa.gov/programs/wq/wastewater/method_16** **69.pdf Chapter 3 3** **Adeloju, S. B. and Bond, A. M., "Influence of Laboratory Environment on the Precision and Accuracy of Trace Element Analysis,"** Anal. Chem.**, 1985,**57**, 1728-1733. http://pubs.acs.org/doi/abs/10.1021/ac00285a050** **Chapter 3 4 Kingston, S. H. M., et al., "Microwave Enhanced Chemistry: Fundamentals, Sample** **Preparation, and Applications," American Chemical Society, Washington, DC, 1997, p. 257-279.** **Chapter 3 5 Moody, J. R., "NBS Clean Laboratories for Trace Element Analysis,"** Anal. Chem.**, 1982,** 54**, 1358A-1376A. Chapter 3 6** **Murphy, T., "National Bureau of Standards Special Publication 422 Accuracy in Trace Analysis: Sampling, Sample Handling, and Analysis," National Bureau of Standards,** **Gaithersburg, MD, 1976, p. 509-539. Chapter 3 7** **Tolg, G. and Tschopel, P., "Determination of Trace Elements," VCH, New York, NY, 1994, p. 1-38.** **Chapter 3 8 Zief, M. and Mitchell, J. W., "Chemical Analysis, Vol. 47, John Wiley & Sons, New York,** **NY, 1976. Chapter 3 9** **Kuehner, E. C., et al., "Production and Analysis of Special High-Purity Acids Purified by Sub-Boiling Distillation,"** Anal. Chem.**, 1972,**44**, 2050-2056. http://pubs.acs.org/doi/abs/10.1021/ac60320a016** **Chapter 3 10 Moody, J. R., "Purified Reagents for Trace Metal Analysis,"** Talanta**, 1982,**29**, 1003- 1010.** **http://www.sciencedirect.com/science/article/pii/0039914082 802415** **Chapter 3 11 Kuehner, E. C. and Freeman, D. H., "Purification of Inorganic and Organic Materials,"** **Marcel Dekker, New York, NY, 1969, p. 297-306. http://onlinelibrary.wiley.com/doi/10.1002/jps.2600590137/ab** **stract Chapter 3 12** **Moody, J. R., "The Sampling, Handling and Storage of Materials for Trace Analysis,"**Philos. Trans. R. Soc. London**, 1982,**305**, 669-680. http://www.jstor.org/pss/37123** **Chapter 3 13 Moody, J. R. and Lindstrom, R. M., "Selection and Cleaning of Plastic Containers for** **Storage of Trace Element Samples,"**Anal. Chem.**, 1977,**49**, 2264-2267. http://chemgroups.northwestern.edu/ohalloran/grouponly/Mo** **odyLindstrom1977.pdf Chapter 3 14** **Prevatt, F. J., "Clean Chemistry for Trace Analysis,"**Environmental Testing andAnalysis**, 1995,**4**, 24-27. Chapter 3 15** **Skelly, E. M. and DiStefano, F. T., "Clean Room and Microwave Digestion Techniques: Improvement in Detection Limits for Aluminum Determination by GF-AAS,"** Appl.Spectrosc.**, 1988,**42**, 1302-1306. http://www.cem.de/documents/pdf/publikation/digestion/RD0** **06.PDF**SW-846 Update VReferences - 27July 2014SW-846 UPDATE V REFERENCE TABLE**Chapter 3 16 Rabinowitz, M. B. and Wetherill, G. W., "Identifying Sources of Lead Contamination by** **Stable Isotope Techniques,"**Environ. Sci. Technol.**, 1972,**6**, 705-709. http://pubs.acs.org/doi/abs/10.1021/es60067a003** **Chapter 3 17 Maienthal, E. J., "U.S. National Bureau of Standards Technical Note 545," National** **Bureau of Standards, Gaithersburg, MD, 1970, p. 53-54. http://babel.hathitrust.org/cgi/pt?seq=1&view=image&size=1** **00&id=mdp.39015001325276&page=root&orient=0 Chapter 3 18** **Boothe, P. N. and Nicolau, B.A. "The Coastal Bend Bays Project,"**26th AnnualConference on Analysis of Pollutants in the Environment**, Chicago, IL 2003. http://www.epa.gov/emap/html/pubs/docs/groupdocs/sympo** **sia/symp2004/presentations/BrienNicolau.pdf Chapter 3 19 Miller, G. T., "Living in the Environment, Wadsworth Inc., Belmont, CA, 1994.** **http://www.coursesmart.com/living-in-the-environment- enhanced-homework/miller/dp/9780495387633** **Chapter 3 20 Gy, P., "Sampling for Analytical Purposes" Wiley, New York, NY, 1998. Chapter 3** **21 Pitard, F.F. "Pierre Gy's Sampling Theory and Sampling Practice," Second Edition, CRC** **Chapter 3 22 EPA, U.S., "Correct Sampling Using the Theories of Pierre Gy," Office of Research and** **Development, Las Vegas, NV, 1999. http://www.epa.gov/esd/factsheets/csutpg.pdf** **Chapter 3 23 EPA, U.S., "Guidance for Obtaining Representative Laboratory Analytical Subsamples** **from Particulate Laboratory Samples." Office of Research and Development, 2003. http://www.epa.gov/osp/hstl/tsc/Gerlach2003.pdf** **Chapter 4 1 A. B. Dindal, R. A. Jenkins, and C. K. Bayne. "Summary Report - Evaluation of the** **Impact of Post-Holding Time Analyte Degradation on Regulatory Decision-Making - VOCs in Water," Oak Ridge National Laboratory. 2001.** **Chapter 4 2 ASTM Standard D4841, 1988 (2008). Standard Practice for Estimation of Holding Time** **for Water Samples Containing Organic and Inorganic Constituents. ASTM International, West Conshohocken, PA, 2003, DOI: 10.1520/D4841-88R08, www.astm.org** **Chapter 4 3 J. T. Love, G. C., Deltzer, S. R. Abney, and J. S. Zogorski. “Study Design and Analytical** **Results Used to Evaluate Stability of Volatile Organic Compounds in Water Matrices.” United States Geological Survey Open-File Report 98-637. 1999.** **Chapter 4 4 M. P. Maskarinec, C. K. Bayne, L. H. Johnson, S. K. Holladay, and R. A. Jenkins.** **“Stability of Volatile Organics in Environmental Water Samples: Storage and Preservation.” Oak Ridge National Laboratory ORNL/TM-11300. 1989.** **http://www.dtic.mil/cgi-bin/GetTRDoc?AD=ADA412461 Chapter 4 5** **O. R. West, C. K. Bayne, R. L. Siegrist, W. L. Holden, S. S. Scarborough, and D. W. Bottrell. “Stability of VOCs in Water samples During Pre-analytical Holding. Part 1.** **Analyses by a Commercial Laboratory.” Oak Ridge National Laboratory ORNL/TM 13240/V1. 1996.** **Chapter 4 6 O. R. West, C. K. Bayne, R. L. Siegrist, W. L. Holden, and D. W. Bottrell. “Stability of** **VOCs in Water samples During Pre-analytical Holding. Part 2. Analyses by an EPA Regional Laboratory.” Oak Ridge National Laboratory ORNL/TM-13240/V2. 1997.** **http://www.osti.gov/bridge/servlets/purl/656450- 6XVR0S/webviewable/656450.pdf** **Chapter 4 7 C. K. Bayne, D. D. Schmoyer, and R. A. Jenkins. “Practical Reporting Times for** **Environmental Samples.” Environmental Science and Technology, 28: 1430-1436. 1994.** SW-846 Update VReferences - 28July 2014SW-846 UPDATE V REFERENCE TABLE**Chapter 4 8 M. P. Maskarinec, C. K. Bayne, R. A. Jenkins, L. H. Johnson, and S. K. Holladay. “Final** **Report - Stablity of Volatile Organics in Environmental Soil samples.” Oak Ridge National Laboratory ORNL/TM-12128. 1992.** **Chapter 4 9 Preservation and Holding Times Study for Vinyl Chloride, Styrene in Industrial** **Wastewater provided by Test America, January 2012. Chapter 4 10** **Preservation and Holding Times Study for Vinyl Chloride, Styrene in Municipal Wastewater provided by the Hampton Roads Sanitation District in Virginia Beach,** **Virginia, January 2012. Chapter 4 11** **ASTM Guide D4547, 1991 (2009). Standard Guide for Sampling Waste and Soils for Volatile Organic Compounds. ASTM International, West Conshohocken, PA, 2003, DOI:** **10.1520/D4547-09, www.astm.org Chapter 4 12** **U.S. Environmental Protection Agency. “Sample Holding Time Re-evaluation.” http://www.epa.gov/esd/cmb/research/bs_033cmb06.pdf** **Chapter 4 13 U.S. Environmental Protection Agency. “Performance of Hydrochloric Acid and** **http://www.epa.gov/nrmrl/pubs/600r08148/600r08148.pdf Chapter 4 14** **ASTM Standard Practice D6418, 2003 (2009). Standard Practice for Using the Chapter 4 15** **U.S. Environmental Protection Agency. “Integrity of VOA Vial Seals.” EPA/600/R- 00/066. 2000.** **http://www.epa.gov/esd/cmb/research/papers/bs124.pdf Chapter 5 No references listed in Chapter.** **End of Update V References**SW-846 Update VReferences - 29July 2014