SW-846 UPDATE V REFERENCE TABLE

Method/Chapter Reference # in Up V Reference 

Method 1030 1

"Test Methods for Readily Combustible Solids. Burning Rate Test." (14.2.2.5). Recommendations on the Transport of Dangerous Goods, Fifth Revised Edition, United 

Nations, New York, 1988.

Method 1030 2 49 CFR, Appendix E to Part 173 (12-31-91 Edition), pp. 597-598.

http://ecfr.gpoaccess.gidx?c=ecfr;sid=75f5fbcv5;view=text;node=49%

Method 1030 3 "Flammability (solids). Method A.10," Official Journal of the European Communities, No. L251/63, September 19, 1984. http://www.intermed.it/

Method 1030 4

Foster Wheeler Enviresponse, Inc., Edison, NJ. "Validation of Ignitability Method for Solids," submitted to the Office of Solid Waste, U.S. Environmental Protection Agency, February 1994.

Method 1030 5 Internal Report (AMFA Report), North Carolina Department of Environmental Health and Natural Resources (Bill Hamner).

Method 3200 1

 Bloom, N. S.; Gill, G. A.; Cappellino, S.; Dobbs, C.; McShea, L.; Driscoll, C.; Mason, R.; Rudd, J., "Speciation and Cycling of Mercury in Lavaca Bay, Texas, Sediments." Environ. Sci. Technol., 1999, 33, (1), 7-13.

http://pubs.acs.org/doi/

Method 3200 2

Templeton, D.; Ariese, F.; Cornelis, R.; Danielsson, L. G.; Muntau, H.; van Leeuvan, H. 

P.; Lobinski, R., "Guidelines for terms related to chemical speciation and fractionation of elements: Definitions, structural aspects, and methodological approaches." Pure Appl. Chem. , 2000, 72, (8), 1453-1470.

http://www.iupac.org/o

Method 3200 3

Hintelmann, H.; Falter, R.; Ilgen, G.; Evans R. D., "Determination of Artifactual Formation of Monomethylmercury (CH3Hg+) in Environmental Samples Using Stable 

Hg2+ Isotopes with ICP-MS Detection: Calculation of Contents Applying Species 

Specific Isotope Additions." Fresenius J. Anal. Chem. , 1997, 358, (3), 363-370.

http://www.springerlink

Method 3200 4

Bloom, N. S.; Coleman, J. A.; Barber, L., "Artifact formation of methyl mercury during aqueous distillation and alternative techniques for the extraction of methyl mercury from environmental samples." Fresenius J. Anal. Chem. , 1997, 358, (3), 371-377.

http://www.springerlink

Method 3200 5

Rahman, G. M. M.; Kingston, H. M. S.; Bhandari, S., "Synthesis and Characterization of Isotopically Enriched Methylmercury (CH3201Hg+)." Appl. Organomet. Chem. , 2003, 17, 

(12), 913-920.

http://onlinelibrary.wile

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SW-846 UPDATE V REFERENCE TABLE

Method 3200 6

Han, Y.; Kingston, H. M.; Boylan, H. M.; Rahman, G. M. M.; Shah, S.; Richter, R. C.; Link, D. D.; Bhandari, S., "Speciation of mercury in soil and sediment by selective solvent and acid extraction." Anal. Bioanal. Chem. , 2003, 375, (3), 428-436.

http://www.springerlink

Method 3200 7

Huo, D.; Kingston, H. M. S.; Larget, B., "Application of Isotope Dilution in Elemental Speciation: Speciated Isotope Dilution Mass Spectrometry (SIDMS)." In: Comprehensive Analytical Chemistry, Volume 33 (Elemental Speciation: New 

Approaches for Trace Element Analysis), Elsevier, New York, 2000; 277-313.

http://www.sciencedire00800203

Method 3200 8

Rahman, G. M. M.; Kingston, H. M. S., "Application of Speciated Isotope Dilution Mass Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and Sediments." Anal. Chem. , 2004, 76, (13), 3548-3555.

http://www.ncbi.nlm.nih

Method 3200 9

Rahman, G. M. M.; Kingston, H. M. S.; Kern, J. C.; Hartwell, S. W.; Anderson, R. F.; Yang, S. -Y., "Inter-laboratory Validation of EPA Method 3200 for Mercury Speciation Analysis using Prepared Soil Reference Materials." Appl. Organomet. Chem. , 2005, 19, 

301-307.

http://onlinelibrary.wile

Method 3200 10 Labor, U.S. Department of, Occupational Health Guideline for Organo (Alkyl) Mercury, Occupational Safety and Health Adminstration, Washington, D.C., 1978. http://www.cdc.gov/nio

Method 3200 11

Nierenberg, D. W.; Nordgren, R. E.; Chang, M. B.; Siegler, R. W.; Blayney, M. B.; Hochberg, F.; Toribara, T. Y.; Cernichiari, E.; Clarkson, T., "Delayed Cerebellar Disease and Death after Accidental Exposure to Dimethylmercury." New Engl. J. Med. , 1993, 

338, 1672-1675.

http://www.nejm.org/do5

Method 3200 12

Kingston, H. M.; Haswell, S. J., Microwave Enhanced Chemistry: Fundamentals, Sample Preparation, and Applications, 10th ed.; American Chemical Society, 

Washington, DC, 1997.

Method 3200 13 Applied Isotope Technologies, Inc., www.sidms.com, e-mail: info@sidms.com.Method 3200 14 Kingston, H. M. Speciated Isotope Dilution Mass Spectrometry of Reactive Species and Related Methods. US Patent 6 790 673 B1 , September 14, 2004. http://www.findthatpate

ass_spectrometry_of_3.html

Method 3200 15

Jain, W.; McLeod, C. W., "Rapid Sequential Determination of Inorganic Mercury and Methylmercury in Natural Waters by Flow-injection - Cold Vapor-Atomic-Fluorescence Spectrometry." Talanta , 1992, 39, (11), 1537-1542.

http://www.sciencedire801384

Method 3200 16

Rahman, G. M. M.; Kingston, H. M. S., "Development of Microwave-Assisted Extraction Method and Isotopic Validation of Mercury Species in Soils and Sediments." J. Anal. At. Spectrom. , 2005, 20, 183-191.

Method's Archive Box 

Method 3200 17

Rahman, G. M. M. "Development, Research and Validation of Environmental Speciation Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in Mercury and Chromium Speciation Analysis." Ph. D. Dissertation , Duquesne University, Pittsburgh, 

PA, 2004.

http://digital.library.duqspiritan/document.php?&REC=1

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SW-846 UPDATE V REFERENCE TABLE

Method 3200 18

Fischer, E.; Tu, Q.; Nagourney, S.; England, R.; Buckley, B. "Microwave-assisted Solvent Extraction for Quantitative Simultaneous Extraction of Inorganic Mercury and Methylmercury from Soils." 20 th Annual National Environmental Monitoring Conference , 

Washington, DC, July 19-23, 2004; Washington, DC, July 19-23, 2004.

Method 3200 19 Jain, W.; McLeod, C. W., "Field Sampling Technique for Mercury Speciation." Anal. Proc. , 1991, 293-294.

Method 3200 20

Lee, Y. H.; Mowrer, J., "Determination of Methylmercury in Natural Waters at the Subnanograms-per-litre Level by Capillary Gas Chromatography after Adsorbent Preconcentration." Anal. Chim. Acta , 1989, 221, (2), 259-268. http://www.sciencedire

0819625

Method 3200 21

Mena, M. L.; McLeod, C. W., "Mercury Species Immobilized on Sulphydryl Cotton: A New Candidate Reference Material for Mercury Speciation." Mikrochim. Acta. , 1996, 

123, (1-4), 103-108.

http://www.springerlinkext.pdf

Method 3200 22

Boylan, H. M.; Richter, R. C.; Kingston, H. M.; Ricotta, A. C., "Rapid Analysis for the Field: Method Development and Application to Natural Gas Utility Sites." Water Air Soil Poll. , 2001, 127, (1-4), 255-270.

Method Archive Box 3

Method 3200 23

Davis, A. Bloom, N. S.; Hee, Q.; Shane, S., "The Environmental Geochemistry and Bioaccessibility of Mercury in Soils and Sediments-A Review." Risk Anal. , 1997, 17, (5), 

105-113.

http://onlinelibrary.wile6924.1997.tb00897.x/a

Method 3200 24

Revis, N. W.; Osborne, T. R.; Holdworth, G.; Hadden, C., "Distribution of Mercury Species in Soil from a Mercury-Contaminated Site." Water Air Soil Poll. , 1989, 17, (5), 

557-569.

Method Archive Box 3

Method 3200 25

Revis, N. W.; Osborne, T. R.; Sedgely, D.; King, A., "Quantitative Method for Determining the Concentration of Mercury (II) Sulphide in Soils and Sediments." Analyst , 1989, 114, 823-826.

http://pubs.rsc.org/en/C91400823

Method 3200 26

Rahman, G. M.; Fahrenholz, T. M.; Kingston, H. M. Skip; Pamuku, M.; Hwang, J. D.; Young, L.A., "Speciation of Mercury in Crude Oil uisng Speciated Isotope Dilution Mass Spectrometry." Spectroscopy , 2010, 25(1), 36-45.

http://spectroscopyonli/Feature/Speciation-of-Speciated/ArticleStand

Method 3200 27

Rahman, G.M.; Fahrenholz, T.M.; Kingston, H. M. Skip, "Application of Speciated Isotope Dilution Mass Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of Mercury Species Transformation in Human Hair." J. Anal. At. Spectrom., 2009, 24, 83-92.

http://pubs.rsc.org/en/C49b

Method 3200 28

Reyes, L. H.; Rahman, G. M.; Fahrenholz, T.; Kingston, H. M. Skip, "Comparison of Methods with Respect to Efficiencies, Recoveries, and Quantitation of Mercury Species Interconversions in Food Demonstrated using Tuna Fish." Anal. Bioanal. Chem. , 2008, 

390, 2123-2132.

http://www.ncbi.nlm.nih

Method 3511 1 "Simultaneous Analysis of Monocyclic Aromatic Hydrocarbons in Water by Microextraction." EPRI Report TR-Research Project, April 1997.Method 3511 2 D. M. Munro. "Simultaneous Determination of Volatile and Semivolatile Organic Compounds in Soil." Remediation Journal, 10, pp. 65-81, 2000. http://onlinelibrary.wile

df

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SW-846 UPDATE V REFERENCE TABLE

Method 3572 1

Applicable documents to support the occupational health program when dealing with chemical agents include AR11-34 (The Army Respiratory Protection Program; AR 40-5 (Preventive Medicine); DA Pam 40-8 (Occupational Health guidelines for the evaluation and Control of Occupational Exposure to Nerve Agents GA, GB, GC, and VX.) and DA Pam 40-173 (Occupational Health Guidelines for the Evaluation and Control of Occupational Exposure to Mustard Agents H, HD, and HT).

http://www.apd.army.mhttp://www.apd.army.mhttp://www.apd.army.m

Method 3572 2

Development and Evaluation of an Analytical Method for Determination of GB, VX, and HD in Concrete, SwRI Final Report to PM-ECW, William S. Williamson, Jr. Joseph H. Brewer.

Method 3572 3

Development and Evaluation of an Analytical Method for Determination of GB, VX, and HD in Coral, SwRI Final Report to PM-ECW, William S. Williamson, Jr., Joseph H. Brewer.

Method 3572 4

Development and Evaluation of an Analytical Method for Determination of GB, VX, and HD in Charcoal, SwRI Final Report to PM-ECW, Michael G. MacNaughton, Ph.D., P.E., William S. Williamson, Jr., Joseph H. Brewer.

Method 3572 5 Development and Evaluation of an Analytical Method for Determination of GB, VX, and HD on Surfaces, SwRI Final Report to PM-ECW, Carter Crigler.Method 3572 6 Laboratory Monitoring and Quality Assurance Plan dated June 2004, Department of Army, Chemical Material Agency.

Method 3620C 1

A.J. Gordon and R.A. Ford, The Chemist's Companion: A Handbook of Practical Data, 

Techniques, and References, New York: John Wiley & Sons, Inc., pp. 372, 374, and 

375, 1972.

Method 3620C 2 Floridin of ITT System, Florisil: Properties, Application, Bibliography, Pittsburgh, Pennsylvania, 5M381DW.

Method 3620C 3

P.A. Mills, "Variation of Florisil Activity; Simple Method for Measuring Absorbent Capacity and Its Use in Standardizing Florisil Columns," Journal of the Association of Official Analytical Chemists , 51, 29, 1968.

Method 3620C 4 U.S. Food and Drug Association, Pesticides Analytical Manual (Volume 1), July 1985. http://www.fda.gov/Foo

ds/PesticideAnalysisM

Method 3620C 5

V. Lopez-Avila, J. Milanes, N.S. Dodhiwala, and W.F. Beckert, "Cleanup of Environmental Sample Extracts Using Florisil Solid-Phase Extraction Cartridges," J. Chrom. Sci. 27, 209-215, 1989.

http://chromsci.oxfordjo

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SW-846 UPDATE V REFERENCE TABLE

Method 3620C 6 U.S. EPA, "Evaluation of Sample Extract Cleanup Using Solid-Phase Extraction Cartridges," Project Report, December 1989.

http://nepis.epa.gov/EPxe/2000AKCX.PDF?Zy86 Thru 1990&File=D%3A%5C6THRU90%5CTXT%5=&SearchMethod=1&F&Password=anonymoup=0&ExtQFieldOp=0&

Method 3620C 7 U.S. EPA, Method 650, "Aniline and Selected Substituted Derivatives."Method 3620C 8

W.F. Beckert and V. Lopez-Avila, "Evaluation of SW-846 Method 8060 for Phthalate Esters," Proceedings of the Fifth Annual Waste Testing and Quality Assurance Symposium, 1989, pp. 144-156.

http://nepis.epa.gov/EPxe/9100CUG4.PDF?Zy86 Thru 1990&File=D%3A%5C6THRU90%5CTXT%5=&SearchMethod=1&F&Password=anonymoup=0&ExtQFieldOp=0&

Method 3620C 9 U.S. EPA, Method 608, Organochlorine Pesticides and PCBs, 40 CFR 136, October 26, 1984. http://www.caslab.com

Method 4025 1 DF1 High Performance Dioxin/Furan Immunoassay Kit (CAPE Technologies), www.cape-tech.com. Method 4025 2 CAPE Technologies Application Notes and related product literature (www.cape- tech.com)

Method 4025 3

Carlson, Robert, E., Harrison, Robert, O., Measurement of PCDD/F TEQ by Immunoassay: Concept Development and Validation. Organohalogen Compounds, vol. 5, Stockholm, Sweden (1998).

Method's Archive Box 

Method 4025 4

Harrison, Robert, O., Carlson, Robert, E., Measurement of PCDD/F TEQ by 

Immunoassay: Demonstration Using Real World Samples, Organohalogen Compounds, vol. 5, Stockholm, Sweden (1998).

http://www.cape-tech.c

Method 4025 5

Harrison, Robert, O., Role of Quality Assurance in Immunoassay Methods Used for Field Screening. Immunochemical Technology for Environmental Applications, American Chemical Society, Washington D.C. (1997).

http://pubs.acs.org/doi/

Method 4025 6

Van den Berg, et. al., “The 2005 World Health Organization Re-evaluation of Human and Mammalian Toxic Equivalency Factors (TEFs) of Dioxins and Dioxin-like Compounds,” Toxicological Sciences, 93(2): 223-241, July 7, 2006.

http://toxsci.oxfordjourn

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SW-846 UPDATE V REFERENCE TABLE

Method 4025 7 “Correlation between EIA Results and GC-MS TEQ,” revised Figure 2 from document listed in Ref. 8. (www.cape-tech.com, Tech References). www.cape-tech.com

Method 4025 8

“Performance of the CAPE Technologies DF1 Dioxin/Furan Immunoassy Kit for Soil and Sediment Samples,” EPA 540/R-08/002, February 2008. (www.cape-tech.com, Tech References).

www.cape-tech.com

Method 4025 9

“Technologies for Monitoring and Measurement of Dioxin and Dioxin-like Compounds in 

Soil and Sediment (CAPE Technologies LLC, DF1; Dioxin/Furan Immunoassay Kit; PCB TEQ Immunoassy Kit),” EPA 540/R-05/004, March 2005. (www.cape-tech.com).

www.cape-tech.com

Method 4025 10 Technical Note TN-005, CAPE Technologies (www.cape-tech.com, Technical Notes) www.cape-tech.com

Method 4025 11 Application Note AN-008, CAPE Technologies (www.cape-tech.com, Application Notes) www.cape-tech.com

Method 4025 12 “An Efficient and Green Cleanup System for Analysis of Dioxins/Furans, Dioxin-like PCBs and PBDES,” (www.cape-tech.com) www.cape-tech.com

Method 4025 13 Immunoassy Sample Prep Kit SP3-60, CAPE Technologies (www.cape-tech.com, Material Lists). www.cape-tech.com

Method 4025 14 Sample Prep Starter Kit SP3-ST, CAPE Technologies (www.cape-tech.com, Material Lists). www.cape-tech.comMethod 4430 1 Dioxins and Furans in Soil and Sediment, Eichrom Method DFS01, www.eichrom.com/dioxin/products. www.eichrom.com/diox

Method 4430 2

M. Van den Berg, L. S. Birnbaum, M. Denison, M. De Vito, W. Farland, M. Feeley, H. Fiedler, H. Hakansson, A. Hanberg, L. Haws, M. Rose, S. Safe, D. Schrenk, C. Tohyama, A. Tritscher, J. Tuomisto, M. Tysklind, N. Walker, and R. E. Peterson; “The 2005 World Health Organization Reevaluation of Human and Mammalian Toxicity Equivalency Factors for Dioxins and Dioxin-like Compounds,” Toxicol. Sci. 2006, 93[2] , 

223-241.

http://toxsci.oxfordjourn

Method 4430 3 R. L. Allen, J. J. Willey; “Novel Real-Time PCR Assay for the Detection of Dioxins and Furans,” Organohalogen Compd. 2002, 58 , 341-343.

Method 4430 4

D. R. McAlister, M. J. Fern, R. L.; Allen, K. Sakata, B. Le Bizec, P. Marchand; “Sample Preparation for the Measurement of Polychlorinated Dioxins and Furans by the Procept Rapid Dioxin Assay,” Organohalogen Compnd. 2006, 68 , 940-943.

http://www.dioxin20xx.

Method 4430 5

Y. Z. Gu, J. B. Hogenesch, C. A. Bradfield; “The PAS Superfamily: Sensors of Environmental and Developmental Signals,” Annu. Rev. Pharmacol. Toxicol. 2000, 40 , 

519-561.

http://mcardle.oncology

Method 4430 6 D. R. McAlister, M. J. Fern; “Soil Screening at 50 pg/g Using a Novel Aryl Hydrocarbon Receptor-based PCR Assay,” Organohalogen Compd ., 2007, 69 , 1230-1233.

Method 4430 7 D. R. McAlister, M. J. Fern; “Cross-reactivity of Compounds on the Procept Rapid Dioxin Assay,” Organohalogen Compd ., 2007, 69 , 1226-1229.

Method 4430 8

S. Heid, R. Pollenz, H. Swanson; “Role of Heat Shock Protein 90 Dissociation in Mediating Agonist-induced Activation of the Aryl Hydrocarbon Receptor,” Mol. Pharmacol. 2000, 57[1] , 82-92.

http://molpharm.aspetj

SW-846 Update V References - 6 
SW-846 UPDATE V REFERENCE TABLE

Method 4430 9 Fed. Reg. 2006, 71 , 78441, Update to ATSDR Policy Guideline for Dioxins and Dioxin- Like Compounds in Residential Soil. http://edocket.access.g

Method 4430 10 C. A. Foy, H. C. Parkes; “Emerging Homogeneous DNA-based Technologies in the Clinical Laboratory,” Clin. Chem. 2000, 47(6) , 990-1000. http://www.clinchem.or

Method 4430 11

D. R. McAlister, M. J. Fern, R. L. Allen; “Rapid Aryl Hydrocarbon Receptor-based Polymerase Chain Reaction Screening Assay for Polychlorinated Dibenzo-p -Dioxins 

and Furans in Soil and Sediment,” Talanta , 2007, in press, doi.org/10.1016/j.talanta.2007.08.005.

Method 4435 1

Arrieta, D. E., Ontiveros, C., Denison, M.S., and Washburn, B.S. (2000). "Ah Receptor Mediated Effects of Particulate Organic Extracts from the Paso Del Morte Airshed Along the U.S. - Mexico Border." Organohalogen Compounds 45: 212 - 215.

http://www.ncbi.nlm.nihhp0111-001299.pdf

Method 4435 2

Behnisch, P. A., Allen, R., Anderson, J., Brouwer, A., Brown, D., Campbell, T. C., Goeyens, L., Harrison, R. O., Hoogenboom, R., Overmeire, I.V., Traag, W., and Malisch, R. (2001). "Harmonised Quality Criteria for Chemical and Bioassays Analyses of PCDDs/PCDFs in Feed and Food Part 2: General Considerations, Bioassay Methods." Organohalogen Compounds 45.

http://www.dioxins.com

Method 4435 3

Brown, D. J., M. D. Chu, et al. (2001). "Determination of REP Values for the CALUX bioassay and comparison to the WHO TEF Values." Organohalogen Compounds 53: 211- 214.

http://www.dioxins.com

Method 4435 4

Brown, D. J., Goeyens, L., Van Overmeire, I., Chu, M., Murata, H., and Clark, G.C. (2001). "Quality control criteria implemented for monitoring the CALUX bioassay." Organohalogen Compounds 54: 32-35.

http://www.dioxins.com

Method 4435 5

Brown, D. J., Kishimoto, Y., Ikeno, O., Chu, M., Nomura, J., Murakami, T., and Murata, H. (2000). "Validation Study for the use of the Dioxin Responsive CALUX Assay for Analysis of Japanese Ash and Soil Samples." Organohalogen Compounds 45: 200-203.

http://www.dioxins.com

Method 4435 6

Brown, D. J., Nakamura, M., Chu, M.D., Denison, M.S., Murata, H., and Clark, G.C. (2002). "Recovery determinations for bioassay analysis: Considerations and results." Organohalogen Compounds 58: 357-360.

http://www.dioxins.com

Method 4435 7

Brown, D. J., Van Overmeire, I., Goeyens, L., Chu, M.D., Denison, M.S., and Clark, G.C. (2002). "Elimination of interfering compounds in preparation for analysis by an Ah receptor based bioassay." Organohalogen Compounds 58: 401-404.

http://www.dioxins.com

Method 4435 8

Clark, G., V. Garry, et al. (2002). "Relationships between exposure to dioxin-like chemicals, testosterone levels, and sex of the children of pesticide applicators." Organohalogen Compounds 56: 73-76.

http://www.dioxins.com

Method 4435 9

Clark, G. C., Brown, D.J., Seidel, S.D., Phelan, D., Denison, M.S. (1999). "Characterization of the CALUX and GRAB bioassays for sensitivity and specificity in detection of phamacological agents that activate the Ah Receptor signaling system." Organohalogen Compounds 42: 309-312.

http://www.dioxins.com

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SW-846 UPDATE V REFERENCE TABLE

Method 4435 10

Clark, G. C., Chu, M., Touati, D., Rayfield, B., Stone, J., Cooke, M. (1999). "A Novel LowCost Air Sampling Device (AmbStack Sampler) and Detection System (CALUX Bioassay) for Measuring Air Emissions of Dioxin, Furan, and PCB on a TEQ Basis Tested With a Model Industrial Boiler." Organohalogen Compounds 42: 309-312.

http://www.dioxins.com

Method 4435 11

Denison, M. S., Nagy, S.R., Clark, G.C., Chu, M., Brown, D.J., Murata, H., Shan, G., Sanborn, J.R., and Hammock, B.D. (2001). "Bioanalytical approaches for the Detection of Dioxin and Related Halogenated Aromatic Hydrocarbons." Organohalogen Compounds 45.

http://www.crcnetbase8.ch33, 11. http://www

Method 4435 12

Denison, M. S., Seidel, S.D., Ziccardi, M., Rogers, W.J., Brown, D.J., and Clark, G.C. (1999). "Ah receptor-based bioassays for dioxins and related chemicals: Applications and limitations." Organohalogen Compounds 40: 27-30.

http://toxsci.oxfordjourn

Method 4435 13

Denison, M.S., Zhao, B., Baston, D.S., Clark, G.C., Murata, H. and Han, D.-H. (2004). Recombinant Cell Bioassay Systems for the Detection and Relative Quantitation of Halogenated Dioxins and Related Chemicals, Talanta 63: 1123-1133.

http://www.sciencedire4002978

Method 4435 14

Denison, M.S. Nagy, S.R., Ziccardi, M., Clark, G.C., Chu, M., Brown, D.J., Shan, G., Sugawara, Y., Shirley J. Gee, S.J., James Sanborn, J. and Hammock, B.D. (2002) Bioanalytical approaches for the detection of dioxin and related halogenated aromatic hydrocarbons, in: Technology-Driven Biomarkers Development and Application in Environmentally-Associated Diseases, Wilson, D. and W. Suk, W., eds., pp. 483-494, Lewis Press, Boca Raton, FL.

Method 4435 15

Garrison, P.M., Tullis, K., Aarts, J.M.M.J.G., Brouwer, A. and Giesy, J.P. and Denison, M.S. (1996) Species-specific recombinant cell lines as bioassay systems for the detection of 2,3,7,8-tetrachlorodibenzo-p-dioxin-like chemicals, Fund. Appl. Toxicol. 30, 194-203.

http://toxsci.oxfordjourn

Method 4435 16 Han, D.-H., Nagy, S.R. and Denison, M.S. (2004) Comparison of recombinant cell Bioassays for the detection of Ah receptor agonists, Biofactors 20, 11-22. https://iospress.metapr

resource-secured/?targ

Method 4435 17

Han, D., Nagy, S.R., and Denison, M.S. (2002). "Recombinant cell lines for the detection of dioxins and Ah Receptor ligands- Not all assays are created equal." Organohalogen Compounds 58: 421-424.

http://www.dioxins.com

Method 4435 18

Hoogenboom, R., Portier, L., Ontenk, C., Polman, T., Hamers, A., and Traag, W. (2000). "Determination of Dioxins and Planar PCBs in Fish Using the GC/MS and CALUX Bioassay." Organohalogen Compounds 45: 180 - 184.

http://www.dioxin20xx.

Method 4435 19

Hooper, K., G. Clark, et al. (2002). "Using the CALUX Assay to select high-TCDD mothers in Southern Kazakhstan and map time-course of TCDD elimination via breast milk." Organohalogen Compounds 58: 377-380.

http://www.dioxin20xx.

Method 4435 20

Hooper, K., Hayward, D., Anderson, M., Farland, W., Lucier, G., Clark, G. (2000). "CALUX results correlate with GC/MS/MS data from Kazakhstan breast milk samples." Organohalogen Compounds 45: 236-239.

http://www.dioxin20xx.

Method 4435 21

Huwe, J. K., Clark, G., Chu, A., and Garry, V. (2003). "CALUX and High Resolution GC/MS Analysis of Dioxin-Like Compounds in Chlorophenoxy Pesticide Formulations." Organohalogen Compounds 60 - 65.

http://www.dioxins.com

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SW-846 UPDATE V REFERENCE TABLE

Method 4435 22

Kayama, F., Hammatsu, A., Sagisaka, K., Brown, D., Clark, G., and Suzuki, T. (2001). "CALUX assay is applicable to human epidemiological studies." Organohalogen Compounds 54: 48-50.

http://www.dioxins.com

Method 4435 23

Kayama, F., Horiguchi, H., Kunisue, T., Tanabe, S., Fukatsu, H., Yamazaki, N., Nakamura, M., Yabushita, H., Fujino, J., and Clark, G. (2003). "Dioxin and Organochlorine Pesticide Concentrations of Breast Milk in China and Japan." Organohalogen Compounds 60 -65.

http://www.dioxins.com

Method 4435 24

Kayama, F., Horiguchi, H., Oguma, E., Fujino, J., Yabushita, H., Brown, D., Clark, G. (2002). "Regional differences of blood dioxins and organchlorine pesticides concentrations of Japanese female farmers.-Application of CALUX assay for epidemiological study-." Organohalogen Compounds 55: 275-278.

http://www.dioxins.com

Method 4435 25

Nakamura T, Nakamura M, Suzuki S, Takahashi M, Fujino J, Yabushita H, Yamamoto T, Brown DJ, Nakai K, Satoh H (2002)" A COMPARATIVE ANALYSIS OF CERTIFIED ENVIRONMENTAL REFERENCE MATERIALS USING CALUXTM ASSAY AND HIGH 

RESOLUTION GC/MS". Organohalogen Compounds 58: 381-384.

http://www.dioxin20xx.

Method 4435 26

Overmeire, I. V., Carbonnelle, S., Loco, J.V., Roos, P., Brown, D., Chu, M., Clark, G., and Goeyens, L. (2002). "Validation of the CALUX Bioassay: Quantitative Screening Approach." Organohalogen Compounds 58: 353 - 356.

http://www.dioxins.com

Method 4435 27

Overmeire, I. V., Chu, M., Brown, D., Clark, G., Carbonnelle, S. and Goeyens, L. (2001). "Application of the CALUX Bioassay for the Determination of Low TEQ Values in Milk Samples." Organohalogen Compounds 45.

http://www.dioxins.com

Method 4435 28

Overmeire, I. V., Goeyens, L., Beernaert, H., Srebrink, S., De Poorter, G., Baeyens, W., Clark, G., Chu, M., Chu, A., Chu, D., Morris, R., and Brown, D. (2000). "A Comparitive Study of GC-HRMS and CALUX TEQ Determinations in Food Samples by the Belgian Federal Ministries of Public Health and Agriculture." Organohalogen Compounds 45: 196 - 200.

http://www.dioxins.com

Method 4435 29

Pence, L. M., Archer, J.C., Bluhm, Earnheart, C., Clark, G., Chu, A., Lovell, R., and Eckert, J. (2003). "Inter-Laboratory CALUX Comparison Data at Low Levels with Traditional GC-HRMS Confirmations." Organohalogen Compounds 60 - 65.

http://www.dioxin20xx.

Method 4435 30

Shaw, S. D., Brenner, D., Mahaffey, C.A., Guise, S.D., Perkins, C.R., Denison, M.S., and Waring, G.T. (2003). "Persistent Organic Pollutants (POPs) and Immune Function in US Atlantic Coast Harbor Seals." Organohalogen Compounds 60 - 65.

http://www.dioxins.com

Method 4435 31

Warner M., E., B., Patterson, D.G., Clark, G., Turner, W.E., Bonsignore, L., Mocarelli, P., and Gerthoux, P.M. (2003). "Comparison of the CALUX Bioassay and IDHRGC/HRMS as Measures of Dioxin Toxic Equivalents in Serum." Organohalogen Compounds 60 - 65.

http://www.dioxins.com

Method 4435 32

Windal, I., Schroijen, C., Wouwe, N.V., Carbonnelle, S., Overmeire, I.V., Brown, D., Clark, G., Baeyens, W., and Goeyens, L. (2003). "Non Additive Interactions in CALUX." Organohalogen Compounds 60 - 65.

 http://www.dioxins.com

SW-846 Update V References - 9 
SW-846 UPDATE V REFERENCE TABLE

Method 4435 33 Windal, I., I. Van Overmeire, et al. (2002). "Variables that affect TEQ determinations by CALUX and GC-HRMS." Organohalogen Compounds 58: 389-392. http://www.dioxins.com

Method 4435 34

Ziccardi, M.H., Gardner, I.A. and Denison, M.S. (2002) Application of the luciferase recombinant cell culture bioassay system for the analysis of polycyclic aromatic hydrocarbons, Environ. Toxicol. & Chem. 21, 2027-2033.

http://onlinelibrary.wilel

Method 4435 35

Windal, I., Dennison, M. S, Birnbaum L. S., Van Wouwe, N., Baeyens, W. Goeyens L. (2005). “Chemically Activated Luciferase Gene Expression (CALUX) Cell Bioassay Analysis for the Estimation of Doxin-Like Activity: Critical Parameters of the CALUX Procedure that Impact Assay Results, Environ.” Sci. Technol., 3, 7357-7364.

www.vliz.be/imisdocs/p

Method 4435 36

Behnisch, P.A., Hosoe, K., Sakai, S-i. (2003). “Brominated dioxin-like compounds in vitro assessment in comparison to classical dioxin-like compounds and other polyaromatic compounds.” Environment International 29 , 861-877.

http://www.pops.int/docAnnexE_2007/Toxicity20Council.pdf

Method 4435 37

Schroijen, C.,Windal, I., Goeyens, L, Baeyens, W. (2004). “Study of the interference problems of dioxin-like chemicals with the bio-analytical method CALUX.” Talanta 63, 1261-1268.

http://www.vub.ac.be/A0al_2004.pdf

Method 4435 38

Van den Berg et al., (2006). “The 2005 World Health Organization Reevaluation of Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-Like Compounds.” Toxicological Sciences 93(2):223-241.

http://toxsci.oxfordjourn

Method 4435 39

Brown, D.J., Orelien, J., Gordon, J.D., Chu, A.C., Chu, M.D., Nakamura, M., Handa, H., Kayama, F., Denison, M.S., and Clark, G.C. (2007) “Mathematical Model Developed for Environmental Samples: Prediction of GC/MS Dioxin TEQ from XDS-CALUX Bioassay Data,” accepted Environmental Science and Technology Nov. 2007.

http://journals.ohiolink.sue=v41i0012&article=

Method 4435 40

USEPA, “Report on the Comparison of Cell Based Assays with Mass SpectrometryMethods for the Analysis of PCDDs/PCDFs and PCBs in Biosolids. U.S. EPA Report from the Office of Water and Office of Science and Technology, Engineering and Analysis Division on Biosolids, June 2002.

Method 4435 41

Denison, Michael S., Brouwer, Abraham, Clark, George C. "Bioassay for detecting 2,3,7,8-tetrachlorodibenzo-para-dioxin and TCDD-like compounds and novel recombinant cell line useful therefor," U.S. patent # 5,854,010, December 29, 1998.

http://patft.uspto.gov/nParser?Sect1=PTO1&Fnetahtml%2FPTO%2854,010.PN.&OS=PN/

Method 4435 42

Chu, Michael D, Clark, George C. "Methods and apparatus for separating and detecting specific polyhalogenated diaromatic hydrocarbons," U.S. patent # 6,720,431, April 13, 2004.

http://patft.uspto.gov/nParser?Sect1=PTO1&Fnetahtml%2FPTO%2720,431.PN.&OS=PN/

SW-846 Update V References - 10 
SW-846 UPDATE V REFERENCE TABLE

Method 5021A 1

P. Flores, and T. Bellar, "Determination of Volatile Organic Compounds in Soils using Equilibrium Headspace Analysis and Capillary Column Gas Chromatography/Mass Spectrometry," U.S. Environmental Protection Agency, Office of Research and Development, Environmental Monitoring Systems Laboratory, Cincinnati, OH, December, 1992.

Method's Archive Box 

Method 5021A 2 B. V. Loffe, and A. G. Vitenberg, "Headspace Analysis and Related Methods in Gas Chromatography," John Wiley and Sons, 1984.Method 5021A 3

R. J. Pirkle, and R. P. McLoughlin, “The Analysis of Selected Components of Reformulated Gasoline in Environmental Samples” from MTBE Handbook, ed. Kostecki, P. and Moyer, E. Amherst Scientific Publishers, 2002.

Method 5021A 4 USEPA OUST, Environmental Fact Sheet: Analytical Methods for Fuel Oxygenates, EPA 510-F-03-001, April, 2003. http://www.epa.gov/ou

Method 5021A 5

H. White, B. Lesnik, and J. T. Wilson, “Analytical Methods for Fuel Oxygenates”, LUSTLine (Bulletin #42), October, 2002, http://www.epa.gov/oust/mtbe/LL42Analytical.pdf

Method 5021A 6 RCRA Organic Methods Workgroup Meeting Minutes, March 20, 2012. Method Contract ArchiMethod 5021A 7 RCRA Organic Methods Workgroup Meeting Minutes, March 22, 2012. Method Contract ArchiMethod 5021A 8

RCRA Organic Methods Workgroup Meeting presentation describing changes to method 5021, “Proposed Changes to SW-846 method 5021A, VOCs by Static Headspace”, March 1, 2012. 

Method Contract Archi

Method 6010D 1

C.L. Jones, et al ., "An Interlaboratory Study of Inductively Coupled Plasma Atomic 

Emission Spectroscopy Method 6010 and Digestion Method 3050," EPA-600/4-87-032, U.S. Environmental Protection Agency, Las Vegas, NV, 1987.

http://nepis.epa.gov/Ex

Method 6010D 2 Taylor, J. K., “Quality Assurance of Chemical Measurements”, Lewis Publishers (1987).Method 6010D 3

Federal Advisory Committee on Detection and Quantitation Approaches and Uses in Clean Water Act Programs, Final Report, http://water.epa.gov/scitech/methods/cwa/det/index.cfm (December 28, 2007).

Method 6020B 1

Horlick, G., et al., "The effect of plasma operating parameters on analyte signals in inductively coupled plasma-mass spectrometry" Spectrochim. Acta Part B: Atomic Spectroscopy, 40(10-12), 1555-1572 (1985).

http://www.sciencedire801786

Method 6020B 2

Gray, A.L., "The ICP as an ion source-origins, achievements and prospects/Mass spectrometry with an inductively coupled plasma as an ion source: the influence on ultratrace analysis of background and matrix response" Spectrochim. Acta 40B, 1525 (1985); 41B, 151 (1986).

http://www.sciencedire801762 ; http://www.sciencedire801471

Method 6020B 3 Tan, S.H., and Horlick, G., "Background Spectral Features in Inductively Coupled Plasma/Mass Spectrometry" Appl. Spectrosc. 40(4), 445-460 (1986). http://www.opticsinfoba

445

Method 6020B 4

Vaughan, M.A., and Horlick, G., "Oxide, Hydroxide, and Doubly Charged Analyte 

Species in Inductively Coupled Plasma/Mass Spectrometry" Appl. Spectrosc. 40(4), 434-445 (1986).

http://www.opticsinfoba434

SW-846 Update V References - 11 
SW-846 UPDATE V REFERENCE TABLE

Method 6020B 5 Holden, N.E., "Table of the Isotopes," in Lide, D.R., Ed., CRC Handbook of Chemistry and Physics, 74th Ed., CRC Press, Boca Raton, FL, 1993.Method 6020B 6 Hinners, T.A., Heithmar, E., Rissmann, E., and Smith, D., Winter Conference on Plasma Spectrochemistry, Abstract THP18; p. 237, San Diego, CA (1994). http://pubs.rsc.org/en/c

90051n

Method 6020B 7 Lichte, F.E., et al., Anal. Chem. 59, 1150 (1987). http://pubs.acs.org/doi/Method 6020B 8

Evans E.H., and Ebdon, L., "Simple approach to reducing polyatomic ion interferences on arsenic and selenium in inductively coupled plasma mass spectrometry" J. Anal. At. Spectrom. 1989, 4, 299-300.

http://pubs.rsc.org/en/c00299

Method 6020B 9 Beauchemin, D., et al., "Study of the effects of concomitant elements in inductively coupled plasmamass spectrometry" Spectrochim. Acta Part B, 42(3), 1987, 467-490. http://www.sciencedire

800241

Method 6020B 10 Houk, R.S., "Mass Spectrometry of inductively coupled plasmas" Anal. Chem. 58(1), 97A-105A (Jan. 1986). http://pubs.acs.org/doi/

Method 6020B 11 Thompson, J.J., and Houk, R.S., "A Study of Internal Standardization in Inductively Coupled Plasma-Mass Spectrometry" Appl. Spectrosc. 41, 801 (1987). http://www.opticsinfoba

801&seq=0

Method 6020B 12

Newberry, W.R., Butler, L.C., Hurd, M.L., Laing, G.A., Stapanian, M.A., Aleckson, K.A., Dobb, D.E., Rowan, J.T., and Garner, F.C., Final Report of the Multi-Laboratory Evaluation of Method 6020 CLP-M Inductively Coupled Plasma-Mass Spectrometry (1989).

Method 6020B 13

Taylor, Daniel B., Kingston, H.M., Nogay, Donald J., Koller, Dagmar, and Hutton, Robert. On-Line Solid-phase Chelation for the Determination of Eight Metals in Environmental Waters by Inductively Coupled Plasma Mass Spectrometry.

Method's Archive Box 

Method 6020B 14

Kingston, H. M., Siriraks, A., and Riviello, J. M., Patent Number 5,126,272, "A Method and Apparatus for Detecting Transition and Rare Earth Elements in a Matrix", U.S. Patent, Filed U.S. Patent Office, March 1989, 31 pages, Granted June 30, 1992, Patent held by US Government.

Method 6020B 15

Kingston, H. M., Siriraks, A., and Riviello, J. M., Patent Number 5,244,634 , "A Method and Apparatus for Detecting Transition and Rare Earth Elements in a Matrix", U.S. Patent , Filed U.S. Patent Office, March 1989, 31 pages, Granted Sept. 14, 1993, Patent held by US Government.

Method 6020B 16

Dobb, David E., Rowan, J.T., and Cardenas, D., Lockheed Environmental Systems and Technologies Co., Las Vegas, NV; and Butler, L.C., and Heithmar, E.M., U.S.EPA, Las Vegas, NV; Determination of Mercury by ICP-MS.

Method's Archive Box 

Method 6020B 17 Taylor, J. K., “Quality Assurance of Chemical Measurements”, Lewis Publishers (1987).Method 6020B 18

Federal Advisory Committee on Detection and Quantitation Approaches and Uses in CleanWaterActPrograms,FinalReport,http://water.epa.gov/scitech/methods/cwa/det/inde

x.cfm (December 28, 2007).

Method 6800, Sec 

13 1 K. E. Jarvis, A. L. Gray and R. S. Houk, Handbook of Inductively Coupled Plasma Mass Spectrometry; Blackie Academic & Professional: London, U.K. 1992, p-315. http://www.springerlink

SW-846 Update V References - 12 
SW-846 UPDATE V REFERENCE TABLE

Method 6800, Sec 

13 2 G. P. Russ III, J. M. Bazan, Spectrochim. Acta, Part B 1987, 42B, 49- 62. http://www.sciencedire

800496

Method 6800, Sec 

13 3 H. E. Taylor, Inductively Coupled Plasma Mass Spectrometry: Practice and Techniques, Academic Press: San Diego, CA, USA, 2001, p-48. http://www.sciencedire

Method 6800, Sec 

13 4

M. Sargent, R. Harte and C. Harrington, Guidelines for Achieving High Accuracy in Isotope Dilution Mass Spectrometry, The Royal Society of Chemistry: Cambridge, UK, 2002.

http://books.google.comng_high_accuracy_i.ht

Method 6800, Sec 

13 5

“Characterization of waste – State of the art document – Chromium VI specification in 

solid matrices” PD CEN/TR 14589:2003, British Standards, EU publication “International Standards Correspondence Index, Technical Report CEN Technical Committee CEN/TC 292, European Committee for Standardization, 2003.

http://shop.bsigroup.co095298

Method 6800, Sec 

13 6

The web sites: http://www.epa.gov/epaoswer/hazwaste/test/new-meth.htm contains Method 6800 and www.sampleprep.duq.edu and www.sidms.com, contain SIDMS/Method 6800 analysis aids, tutorials, update information and applications (Ref. 27).

Method 6800, Sec 

16 1 J. D. Fasset and P. J. Paulsen, "Isotope Dilution Mass Spectrometry," Anal. Chem . 1989, 61(10), 643A-649A.

Method 6800, Sec 

16 2 H. M. Kingston, "Method of Speciated Isotope Dilution Mass Spectrometry," US Patent Number: 5,414,259, 1995.

http://patft.uspto.gov/nParser?Sect1=PTO1&Fnetahtml%2FPTO%2414,259.PN.&OS=PN/

Method 6800, Sec 

16 3

D. Huo and H. M. Kingston, "Correction of Species Transformations in the Analysis of Cr(VI) in Solid Environmental Samples Using Speciated Isotope Dilution Mass Spectrometry," Anal. Chem. 2000, 72(20), 5047-5054 . http://pubs.acs.org/doi/

Method 6800, Sec 

16 4

B. R. James, J. C. Petura, R. J. Vitale and G. R. Mussoline, "Hexavalent Chromium Extraction from Soils: A Comparison of Five Methods," Environ. Sci. Tech. 1995, 29(9), 

2377-2381.

http://cat.inist.fr/?aMod

Method 6800, Sec 

16 5

H. M. Kingston, D. Huo, Y. Lu and S. Chalk, "Accuracy in Species Analysis. Speciated Isotope Dilution Mass Spectrometry (SIDMS) Exemplified by the Evaluation of Chromium Species," Spectrochim. Acta, Part B: Atomic Spectroscopy , 1998, 53B(2), 

299-309.

http://www.sciencedire7001432

Method 6800, Sec 

16 6

D. Huo, H. M. Kingston and B. Larget, “Application of Isotope Dilution in Elemental Speciation: Speciated Isotope Dilution Mass Spectrometry (SIDMS),” In: Comprehensive Analytical Chemistry, J. A. Caruso, K. L. Sutton and K. L. Ackley (eds.), 

Vol. 33 (Elemental Speciation: New Approaches for Trace Element Analysis), Elsevier, New York, USA, 2000, p-277-313.

http://www.sciencedire00800203

Method 6800, Sec 

16 7

H. M. Kingston, D. Huo, S. Chalk and P. Walter, "The Accurate Determination of Species by Speciated Isotope Dilution Mass Spectrometry: Exemplified by the Evaluation of Chromium (VI) in Soil," The Twelfth Annual Waste Testing & Quality Assurance Symposium; Washington, DC, July 23-26, 1996, 112-119.

Method's Archive Box 

SW-846 Update V References - 13 
SW-846 UPDATE V REFERENCE TABLE

Method 6800, Sec 

16 8

D. Huo, Y. Lu and H. M. Kingston, "Determination and Correction of Analytical Biases and Study on Chemical Mechanisms in the Analysis of Cr(VI) in Soil Samples Using EPA Protocols," Environ. Sci. Tech. , 1998, 32(21), 3418-3423.

http://pubs.acs.org/doi/

Method 6800, Sec 

16 9

G. N. Bowers, Jr., J. D. Fassett and E. V. White, "IDMS and the National Reference System: Accuracy Transfer in Clinical Chemistry," Anal. Chem. , 1993, 65(12), 475 - 

479.

 http://pubs.acs.org/do

Method 6800, Sec 

16 10

L. J. Moore, H. M. Kingston and T. J. Murphy, "The Use of Isotope Dilution Mass Spectrometry for the Certification of Standard Reference Materials," Environ. Intern. , 

1984, 10(2), 169-173.

Method's Archive Box 

Method 6800, Sec 

16 11

H. M. ‘Skip’ Kingston, D. Huo, G. M. M. Rahman, and P. Walter, SamplePrep Web [Homepage of SamplePrep Web], Available: http://www.sampleprep.duq.edu/, referenced 2011.

Method 6800, Sec 

16 12

D. Huo, “The Development of Methods in Speciated Isotope Dilution Mass Spectrometry (SIDMS) for Elemental Speciation of Chromium in Environmental Samples Using LCICP-MS,” Doctoral Dissertation , Duquesne University, July 30, 1999.

Method 6800, Sec 

16 13

G. M. M. Rahman, H. M. Skip Kingston, T. G. Towns, R. J. Vitale and K. R. Clay, “Determination of hexavalent chromium by using speciated isotope-dilution mass spectrometry after microwave speciated extraction of environmental and other solid materials,” Anal. Bioanal. Chem ., 2005, 382(4), 1111-1120.

http://www.springerlink

Method 6800, Sec 

16 14

H. M. “Skip” Kingston, R. Cain, D. Huo and G. M. M. Rahman, “Determination and 

evaluation of hexavalent chromium in power plant coal combustion by-products and costeffective environmental remediation solutions using acid mine drainage,” J. Environ. Monit. , 2005, 7, 899-905.

http://pubs.rsc.org/en/C724b

Method 6800, Sec 

16 15

G. M. M. Rahman and H. M. ‘Skip’ Kingston, “Development of a microwave-assisted extraction method and isotopic validation of mercury species in soils and sediments,” J. 

Anal. At. Spectrom. , 2005, 20, 183-191.

http://pubs.rsc.org/en/C81e

Method 6800, Sec 

16 16

G. M. M. Rahman, H. M. ‘Skip’ Kingston, John Kern, Sarah W. Hartwell, Ramond F. Anderson and Shen-yi Yang, “Inter-laboratory Validation of EPA Method 3200 for mercury species analysis using prepared soil reference materials,” J. Applied 

Organometallic Chem. , 2005, 19, 301-307.

http://onlinelibrary.wile

Method 6800, Sec 

16 17

G. M. M. Rahman and H. M. ‘Skip’ Kingston, “Application of Speciated Isotope Dilution Mass Spectrometry to Evaluate Extraction Methods for Determining Mercury Speciation in Soils and Sediments,” Anal. Chem ., 2004, 76, 3548-3555.

http://pubs.acs.org/doi/

Method 6800, Sec 

16 18

H. M. Kingston, “Speciated isotope dilution mass spectrometry of reactive species and related methods,” US Patent Number 6 790 673 B1, 2004 and PCT Int. Appl . January 

28, 1999, Patent No. WO 9939198.

Method's Archive Box 

Method 6800, Sec 

16 19 H. M. Skip Kingston, U.S. Patent Number 6,974,951 B1, “Automated In-Process Ratio Mass Spectrometry” Dec 13, 2005.

Method 6800, Sec 

16 20

L. Hinojosa Reyes, G. M. M. Rahman, H. M. Skip Kingston, Robust microwave-assisted extraction protocol for determination of total mercury and methylmercury in fish tissues, Analytica Chemica Acta, 631, 121-128, 2009.

http://www.sciencedire8018229

SW-846 Update V References - 14 
SW-846 UPDATE V REFERENCE TABLE

Method 6800, Sec 

16 21

G. M. M. Rahman, T. Fahrenholz and H. M. Skip Kingston, “Application of Speciated Isotope Dilution Mass Spectrometry to Evaluate Methods for Efficiencies, Recoveries, and Quantification of Mercury Speciation Transformations in Human Hair” Journal of Analytical Atomic Spectrometry, 24, 83-92, 2009.

http://pubs.rsc.org/en/C49b

Method 6800, Sec 

16 22

Lu. Yang, E. Ciceri, Z. Mester and R. E. Sturgeon, “Application of Double Spike Isotope Dilution for the Accurate Determination of Cr(III), Cr(VI) and Total Cr in Yeast”, Anal. 

Bioanal. Chem ., 2006, (Published online on September 05, 2006, DOI: 10.1007 /s00216-006-0756-z).

http://www.springerlink

Method 6800, Sec 

16 23

H. M. Skip Kingston, Robert McDonald, Ye Han, Jason Wang, June Wang, Michael West, Larry Stewart, Bob Ormond, and Rudy Mui, “Automated, On-Line, Trace Contamination and Chemical Species Analysis For the Semiconductor Industry,” American Institute of Physics (AIP), Conference Proceedings, Proceedings form the 2003 Characterization and Metrology for ULSI Technology Conference, Volume 683, Melville, NY, 2003.

http://scitation.aip.org/g=pdf&id=APCPCS0006ps&prog=normal&bypa

Method 6800, Sec 

16 24

G. M. Mizanur Rahman, “Development, Research and Validation of Environmental Speciation Methods: Evaluation by Speciated Isotope Dilution Mass Spectrometry in 

Mercury and Chromium Speciation Analysis.” Duquesne University, Pittsburgh, PA USA, 2004.

http://digital.library.duqspiritan/results.php?CIARCHALL&CISOROO

Method 6800, Sec 

16 25

Juris Meija, Lu Yang, Joseph A. Caruso, Zoltan Mester, “Calculations of Double Spike Isotope Dilution Results Revisited.” J. Analytical Atomic Spectrometry, 2006 (Referenced on-line Aug. 2006).

http://www.uc.edu/plase%20Spike%20for%20

Method 6800, Sec 

16 26

Gonzalo Manchego, G. M. Mizanur Rahman, Laura Reyes, Panxi Zhao, H. M. Skip Kingston, “Testing is an Essential Part of International Environmental Regulation and Commerce Compliance”, Washington DC, NEMC Presentation 2008.

Method 6800, Sec 

16 27 http://www.epa.gov/epaoswer/hazwaste/test/new-meth.htm and www.sampleprep.duq.edu and www.sidms.com.

Method 6800, Sec 

16 28

John Kern, C. Toews, H. M. Skip Kingston, G. M. M. Rahman, J. Sun, L. H. Reyes, Accurate, Explicit Determinations in Speciated Isotope Dilution Mass Spectrometry without Calibration Curves, in revision 2010.

Method 6800, Sec 

16 29

C. Toews, J. Kern, H. M. Kingston and M. Rahman, “Sensitivity Analysis for Speciated Isotope Dilution Mass Spectrometry” Journal of Analytical and Atomic Spectrometry, 25, 196-200, 2010.

http://math.pugetsoundevision.pdf

Method 6800, Sec 

16 30

G. M. Mizanur Rahman, Timothy M. Fahrenholz, H. M. Skip Kingston, Matt Puku, J. David Hwang, and Lyman A. Young, “Speciation of Mercury in Crude Oil Using Speciated Isotope Dilution Mass Spectrometry” Spectroscopy, 25,1, 36-45, 2010.

http://spectroscopyonli/Feature/Speciation-of-Speciated/ArticleStand

Method 6800, Sec 

16 31

G. M. Mizanur Rahman, Timothy M. Fahrenholz, Matt Puku, Panxi Zhao, Laura Reyes, Scott Faber, H. M. Skip Kingston, “Speciation of Mercury in whole human blood by SIDMS SPME-GC-ICP-MS with Microwave Assisted Equilibration and Extraction” (in preparation 2010).

SW-846 Update V References - 15 
SW-846 UPDATE V REFERENCE TABLE

Method 6800, Sec 

16 32

Laura H. Reyes, G. M. Mizanur Rahman, Timothy Fahrenholz, H. M. Skip Kingston, “Comparison of methods with respect to efficiencies, recoveries, and quantitation of mercury species interconversions in food demonstrated using tuna fish” Analytical Bioanalytical Chemistry, 390, 2123-2132, 2008.

http://www.ncbi.nlm.nih

Method 6800, Sec 

16 33

Gregory M. Zinn, G. M. Mizanur Rahman, Curtis Frantz, Larry Newman, Scott Faber, H. M. Skip Kingston, “Zinc Dietary Supplement Contamination with Toxic Antimony Species, (in preparation 2010).

Method 6800, Sec 

16 34

Rebecca L. Wagner, Stephanie J. Wetzel, Matt Puku, H. M. Skip Kingston, “Glyphosate by IDMS and i-Spike IDMS as for Automated and Safe Toxic MS Analysis” (in preparation 2010).

Method 6800, Sec 

16 35

Timothy Fahrenholz, Hemasudha Chatragadda, Scott Faber, H. M. Skip Kingston, “Glutathione analysis as a biomarker for immune stress and autism” (in preparation 2011).

http://www.liebertonline

Method 6800, Sec 

16 36

Michael Passineau, Timothy Fahrenholz, Laurie Machen, Zourelias Lee, Katherine Nega, Rachel Paul, Mary MacDougall, Olga Mamaeva, Raymond Benza, Richard Steet, Jarrod Barnes, H. M. Skip Kingston. Human Gene Therapy, (Submitted 2010).

Method 6800, Sec 

16 37 NIST Certificate of Analysis SRM 2701 “Hexavalent Chromium in Contaminated Soil (High Level)” (2009). https://www-s.nist.gov/

Method 6800, Sec 

16 38

Stuart Nagourney, Stephen A. Wilson, Brian Buckley, H. M. Skip Kingston, Shen-Yi Yang and Stephen E. Long. Journal of Analytical Atomic Spectroscopy, 23, 1550-1554, 2008.

http://pubs.rsc.org/en/C88b

Method 6800, Sec 

16 39

“Characterization of waste – Stat of the art document – Chromium VI specification in 

solid matrices” PD CEN/TR 14589:2003, British Standards, EU publication “International Standards Correspondence Index, Technical Report CEN Technical Committee CEN/TC 292, European Committee for Standardization, 2003.

http://shop.bsigroup.co095298

Method 6800, Sec 

16 40

Gregory M. Zinn, G. M. Mizanur Rahman, H. M. Skip Kingston, “Sodium Azide 

Quantification for homeland defense by isotope dilution mass spectrometry EPA Method 6800 (in preparation 2011).

Method 6800, Sec 

16 41

Eva Krupp, Bruce Milne, Adrin Mestrot, Andrew Meharg and Jorg Feldmann, “Investigation into mercury bound to biothiols: structural identification using ESI-ion-trap MS and introduction of a method for their HPLC separation with simultaneous detection by ICP-MS and ESI-MS.” Analytical Bioanalytical Chemistry, 390, 1753-1764, 2008.

http://www.springerlinkext.pdf

Method 6800, Sec 

16 42

US AIR FORCE Task Reports for the Homeland Security and Homeland Defense: extension of EPA Method 6800 conducted between 2007 and 2010 with funding from the Headquarters of the US Air Force Surgeon General under the awards, No.FA7014-07-0014 and No.FA7014-08-C-0029. Report authors: H. M. Skip Kingston, M. Puku, M. Rahman, G. M. Zinn, R. L. Wagner.

Method 6800, Sec 

16 43

Timothy Fahrenholz, Scott Faber, H. M. Skip Kingston, John Kern, Matt Pamuku, Hemasudha Chatragadda, Becky Pekar, “Quantification Glutathione Biomarkers in Autism” (in preparation 2012).

SW-846 Update V References - 16 
SW-846 UPDATE V REFERENCE TABLE

Method 6800, Sec 

16 44

Rebecca L. Wagner, Stephanie Wetzel, H. M. Skip Kingston“ Direct Speciated Isotope Dilution Mass Spectrometry of Analytical Methodology of Illicit Drug in Urine Using Timeof-Flight Mass Spectrometry” (in review 2012).

Method 8000D 1 References for poor performing compounds can be found at: Department of Defense: http://www.a2la.org/forms/DoD_ELAP_Appendix_G1.doc www.a2la.org/forms/Do

Method 8000D 2 “Quality Systems Manual for Environmental Laboratories”, Version 5.0 http://www.denix.osd.m

FINAL.pdf

Method 8000D 3 U.S.E.P.A Contract Laboratory Program SOM 1.2 at: http://www.epa.gov/superfund/programs/clp/som1.htm www.epa.gov/superfunMethod 8000D 4 A list of quantitation limits for poor performing volatile compounds can be found in Table App D XIII-1 at: http://www.epa.gov/region1/oeme/appendc.pdf www.epa.gov/region1/Method 8000D 5 A list of quantation limits for poor performing semivolatile compounds can be found in Table App E XIII-1 at: http://www.epa.gov/region1/oeme/appendd.pdf www.epa.gov/region1/

Method 8021B 1

"Volatile Organic Compounds in Water by Purge-and-Trap Capillary Column Gas Chromatography with Photoionization and Electrolytic Conductivity Detectors in Series, Method 502.2, Rev. 2.0 (1989); Methods for the Determination of Organic Compounds in Drinking Water," U.S. Environmental Protection Agency, Environmental Monitoring Systems Laboratory, Cincinnati, OH, EPA/600/4-88/039, December 1988.

http://www.caslab.com

Method 8021B 2

"The Determination of Halogenated Chemicals in Water by the Purge and Trap Method," Method 502.1; U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, September 1986.

Method 8021B 3

"Volatile Aromatic and Unsaturated Organic Compounds in Water by Purge and Trap Gas Chromatography, Method 503.1;" U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH, September 1986.

Method 8021B 4 J. A. Glaser, D. L. Forest, G. D. McKee, S. A. Quave, W. L. Budde, "Trace Analyses for Wastewaters," Environ. Sci. Technol. 1981, 15, 1426. http://pubs.acs.org/doi/

Method 8021B 5

T. A. Bellar, J. J. Lichtenberg, "The Determination of Synthetic Organic Compounds in Water by Purge and Sequential Trapping Capillary Column Gas Chromatography," U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268.

http://books.google.com_Synthetic_Organic_C

Method 8111 1

V. Lopez-Avila, E. Baldin, J. Benedicto, J. Milanes, W. F. Beckert, "Application of OpenTubular Columns to SW-846 GC Methods," Final Report to the US EPA on Contract 68-03-3511, Mid-Pacific Environmental Laboratory, Mountain View, CA, 1990.

Method 8111 2

S. Tsang, P. Marsden, N. Chau, "Performance Data for Methods 8041, 8091, 8111, and 8121A," Draft Report to US EPA on Contract 68-W9-0011, Science Applications International Corp., San Diego, CA, 1992.

SW-846 Update V References - 17 
SW-846 UPDATE V REFERENCE TABLE

Method 8270D 1

J. W. Eichelberger, L. E. Harris, and W. L. Budde, "Reference Compound to Calibrate Ion Abundance Measurement in Gas Chromatography-Mass Spectrometry Systems," Analytical Chemistry, 47, 995-1000, 1975.

http://pubs.acs.org/doi/

Method 8270D 2 P. Olynk, W. L. Budde, and J. W. Eichelberger, "Method Detection Limit for Methods 624 and 625," unpublished report, October 1980.Method 8270D 3 "Interlaboratory Method Study for EPA Method 625-Base/Neutrals, Acids, and Pesticides," Final Report for EPA Contract 68-03-3102.Method 8270D 4

J. A. Burke, "Gas Chromatography for Pesticide Residue Analysis: Some Practical Aspects," Journal of the Association of Official Analytical Chemists (AOAC), 48, 1037, 1965.

Method 8270D 5

S. V. Lucas, R. A. Kornfeld, "GC-MS Suitability Testing of RCRA Appendix VIII and Michigan List Analytes," U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, February 20, 1987, Contract No. 68-03-3224.

http://books.google.comsting_of_RCRA_Appen

Method 8270D 6

T. M. Engel, R. A. Kornfeld, J. S. Warner, and K. D. Andrews, "Screening of Semivolatile Organic Compounds by Extractability and Aqueous Stability by SW-846, Method 3510," U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Cincinnati, OH 45268, June 5, 1987, Contract 68-03-3224.

http://nepis.epa.gov/ExonD=ZyDocument&Cliocs=&Query=&Time=&strict=n&Toc=&TocEntnth=&QFieldDay=&IntQry=&File=D%3A%5Czy%5CTxt%5C00000011OUS&Password=anon&MaximumDocuments75g8/r75g8/x150y150gge=x&SearchBack=Zy=Results%20page&Mage=x&ZyPURL

Method 8270D 7

V. Lopez-Avila (W. Beckert, Project Officer); "Development of a Soxtec Extraction Procedure for Extraction of Organic Compounds from Soils and Sediments," U.S. Environmental Protection Agency, Environmental Monitoring and Support Laboratory, Las Vegas, NV, October 1991; EPA 600/X-91/140.

http://books.google.comxtec_Extraction_Proce

SW-846 Update V References - 18 
SW-846 UPDATE V REFERENCE TABLE

Method 8270D 8

J. Bursey, R. Merrill, R. McAllister, and J. McGaughey, "Laboratory Validation of VOST and SemiVOST for Halogenated Hydrocarbons from the Clean Air Act Amendments List," Vol. 1 and 2, U.S. Environmental Protection Agency, EPA 600/R-93/123a and b, (NTIS PB 93-227163 and 93-27171), Research Triangle Park, NC, July 1993.

http://nepis.epa.gov/ExtionD=ZyDocument&CDocs=&Query=&Time=estrict=n&Toc=&TocEnonth=&QFieldDay=&Inery=&File=D%3A%5Cz4%5CTxt%5C0000000MOUS&Password=ano&MaximumDocuments75g8/r75g8/x150y150gge=x&SearchBack=Zy=Results%20page&Mage=x&ZyPURL

Method 8270D 9

B. Richter, J. Ezzell, and D. Felix, "Single Laboratory Method Validation Report: Extraction of Target Compound List/Priority Pollutant List BNAs and Pesticides Using Accelerated Solvent Extraction (ASE) with Analytical Validation by GC/MS and GC/ECD," Document 101124, Dionex Corporation, Salt Lake City, UT, June 16, 1994.

Method 8270D 10

H. B. Lee, T. E. Peart, R. L. Hong-You, and D. R. Gere, "Supercritical Carbon Dioxide Extraction of Polycyclic Aromatic Hydrocarbons from Sediments," J. Chromatography A, 653, 83-91 (1993).

http://www.sciencedire80394N

Method 8270D 11

S. Warner, "SFE Extraction of PNAs from Solid Matrices Using the Dionex 703M SFE 

Extractor and a Liquid Trap," EPA Region III, Central Regional Laboratory, 839 Bestgate Road, Annapolis, MD 21401, December 12, 1994.

Method 8270D 12 C. Markell, "3M Data Submission to EPA," letter to B. Lesnik, June 27, 1995.Method 8270D 13

USEPA Method 525.2, "Determination of Organic Compounds in Drinking Water by Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry," Environmental Monitoring Systems Laboratory, Office of Research and Development, US EPA, Cincinnati, OH, Revision 2.0, March 1995.

http://water.epa.gov/scSOCs.pdf

Method 8270D 14

USEPA, Superfund Analytical Services/Contract Laboratory Program (CLP), MultiMedia, Multi-Concentration Organics Analysis, SOM01.X, Exhibit D - Analytical Methods, "Analytical Method for the Analysis of Semivolatile Organic Compounds," November, 2003.

Method 8276 1 A. G. Harrison (2nd ed.), Chemical Ionization Mass Spectrometry, CRC Press, Boca Raton, FL, 1992.Method 8276 2

W. C. Brumley, C. M. Brownrigg, and A. H. Grange, "Determination of Toxaphene in Soil by Electron-Capture Negative Ion Mass Spectrometry After Fractionation by HighPerformance Gel Permeation Chromatography," J. Chromatogr., 633, 177-183, 1993. http://www.epa.gov/esd

anal/reports/toxpf/toxp

SW-846 Update V References - 19 
SW-846 UPDATE V REFERENCE TABLE

Method 8276 3

Brumley, W. C. "Analytical Protocol (GC/NIMS) for OSWER's Response to OIG Report (2005-P-00022) on Toxaphene Analysis." EPA/600/R-08/048. (TIP # 08-069, Published Report) U.S. Environmental Protection Agency, Washington, DC, 2008.

http://nepis.epa.gov/Ad

Method 8276 4

V. Lopez-Avila, E. Baldin, J. Benedicto, J. Milanes, W. F. Beckert, "Application of OpenTubular Columns to SW-846 GC Methods," Report for the U.S. Environmental Protection Agency, Contract 68-03-3511, Mid-Pacific Environmental Laboratory, Mountain View, CA, 1990.

http://nepis.epa.gov/ExonD=ZyDocument&Cliocs=&Query=&Time=&strict=n&Toc=&TocEntnth=&QFieldDay=&IntQry=&File=D%3A%5Czy%5CTxt%5C00000006OUS&Password=anon&MaximumDocuments75g8/r75g8/x150y150gge=x&SearchBack=Zy=Results%20page&Mage=x&ZyPURL

Method 8276 5

"Development and Application of Test Procedures for Specific Organic Toxic Substances in Wastewaters," Category 10, Pesicides and PCB Report for the U.S. Environmental Protection Agency, Contract 68-03-2606

http://nepis.epa.gov/ExonD=ZyDocument&Cliocs=&Query=&Time=&strict=n&Toc=&TocEntnth=&QFieldDay=&IntQry=&File=D%3A%5Czy%5CTxt%5C00000006US&Password=anonym&MaximumDocuments75g8/r75g8/x150y150gge=x&SearchBack=Zy=Results%20page&Mage=x&ZyPURL

Method 8276 6 D. F. Goerlitz, L. M. Law, "Removal of Elemental Sulfur Interferences from Sediment Extracts for Pesticide Analysis," Bull. Environ. Contam. Toxicol., 6, 9, 1971. http://www.springerlink

Method 8276 7

S. Jensen, L. Renberg, L. Reutergardth, "Residue Analysis of Sediment and Sewage Sludge for Organochlorines in the Presence of Elemental Sulfur," Anal. Chem. 49, 316-318, 1977.

http://pubs.acs.org/doi/

Method 8276 8

R. H. Wise, D. F. Bishop, R. T. Williams, B. M. Austern, "Gel Permeation Chromatography in the GC/MS Analysis of Organics in Sludges," U.S. Environmental Protection Agency, Cincinnati, OH.

SW-846 Update V References - 20 
SW-846 UPDATE V REFERENCE TABLE

Method 8276 9 H. B. Pionke, G. Chesters, D. E. Armstrong, "Extraction of Chlorinated Hydrocarbon Insecticides from Soil," Agron. J., 60, 289, 1968. https://www.agronomy

600030289

Method 8276 10 J. A. Burke, P. A. Mills, D. C. Bostwick, "Experiments with Evaporation of Solutions of Chlorinated Pesticides," J. Assoc. Off. Anal. Chem., 49, 999, 1966.Method 8276 11 J. A. Glazer, et. al., "Trace Analyses for Wastewaters," Environ. Sci. and Technol., 15, 1426, 1981. http://pubs.acs.org/doi/

Method 8276 12 P. J. Marsden, "Performance Data for SW-846 Methods 8270, 8081, and 8141," U.S. Environmental Protection Agency, EMSL-Las Vegas, EPA/600/4-90/015.

http://nepis.epa.gov/ExD=ZyDocument&Clien0&Docs=&Query=&TimcRestrict=n&Toc=&TocdMonth=&QFieldDay=eldOp=0&XmlQuery=&%20DATA%5C86THRCV89.txt&User=ANONtMethod=h%7C

Method 8276 13

V. Lopez-Avila, (Beckert, W., Project Officer), "Development of a Soxtec Extraction Procedure for Extracting Organic Compounds from Soils and Sediments," EPA 600/X91/140, U.S. Environmental Protection Agency, Environmental Monitoring Systems Laboratory, Las Vegas, NV, October 1991.

Method 8276 14 C. Markell, "Solid-Phase Extraction of TCLP Leachates," Proceedings of the Tenth Annual Waste Testing and Quality Assurance Symposium, Arlington, VA, July, 1994.Method 8276 15

D. Bennett, B. Lesnik, S. M. Lee, "Supercritical Fluid Extraction of Organochlorine Pesticide Residues from Soils," Proceedings of the Tenth Annual Waste Testing and Quality Assurance Symposium, Arlington, VA, July, 1994.

Method 8276 16 C. Markell, "3M Data Submission to EPA," Letter to B. Lesnik, June 27, 1995.Method 8276 17

B. Richter, J. Ezzell, D. Felix, "Single Laboratory Method Validation Report - Extraction of Organophosphorus Pesticides, Herbicides, and Polychlorinated Biphenyls Using Accelerated Solvent Extraction (ASE) with Analytical Validation by GC/NPD and GC/ECD," Dionex, Salt Lake City, UT, Document 101124, December 2, 1994.

Method 8276 18

K. Li, J. M. R. Bélanger, M. P. Llompart, R. D. Turpin, R. Singhvi, and J. R. J. Paré. Evaluation of Rapid Solid Sample Extraction Using the Microwave-Assisted Process (MAPTM) Under Closed-Vessel Conditions. Spectros. Int. J. 13 (1), 1-14, 1997.

http://www.cem.de/doc

Method 8276 19

L. D. Betowski, H. M. Webb, and A. D. Sauter. Pulsed Positive Ion Negative Ion Chemical Ionization Mass Spectrometric Applications to Environmental and Hazardous Waste Analysis. Biomed. Mass Spectrom. 10, 369, 1983.

SW-846 Update V References - 21 
SW-846 UPDATE V REFERENCE TABLE

Method 8276 20

Science Applications International Corporation, "Interlaboratory Study Plan for Validation of Method 8276," Submitted to U.S. Environmental Protection Agency, November 2008.

Method 8276 21 USEPA Region 4 Modified Method 3545A Standard Operating Procedure (SOP) for Pressurized Fluid Extraction (PFE), Revision 4.1, November 5, 2010.Method 8276 22 USEPA Region 4 Modified Method 3620C, SOP for Florisil® Cleanup, Revision 3.0, August 23, 2010.Method 8276 23 USEPA Region 4 Modified Method 3630C SOP for Silica Gel Cleanup, Revision 3.1, August 10, 2011.Method 8276 24 TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Study Plan," Submitted to U.S. Environmental Protection Agency, September 2011.Method 8276 25 TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Analytical Data Report," Submitted to U.S. Environmental Protection Agency, May 2012.Method 8276 26 TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Data Validation Report," Submitted to U.S. Environmental Protection Agency, May 2012.Method 8276 27 TechLaw Incorporated, "Inter-laboratory Validation for Fish Tissue Statistical Analysis Report," Submitted to U.S. Environmental Protection Agency, May 2012.Method 8276 28

H. Parlar, D. Angerhöfer, M. Coelhan, L. Kimmel, "HRGC and HRGC-ECNI Determination of Toxaphene Residues in Fish with a New 22 Components Standard," Organohalogen Compd., 26, 357, 1995.

http://www.dioxin20xx.

Method 8410 1

Handbook for Analytical Quality Control in Water and Wastewater Laboratories ; U.S. 

Environmental Protection Agency. Environmental Monitoring and Support Laboratory. ORD Publication Offices of Center for Environmental Research Information: Cincinnati, 

OH, March 1979; Sec. 4, EPA-600/4-79-019.

http://nepis.epa.gov/Exxt

Method 8410 2 R. R. Freeman, Hewlett Packard Application Note: Quantitative Analysis Using a Purged Splitless Injection Technique; ANGC 7-76.

Method 8410 3 R. H. Cole, Tables of Wavenumbers for the Calibration of Infrared Spectrometers ; Pergamon: New York, 1977. http://books.google.com

ers_for_the_calibratio.

Method 8410 4 J. G. Grasselli, P. R. Griffiths, R. W. Hannah, "Criteria for Presentation of Spectra from Computerized IR Instruments"; Appl. Spectrosc. 1982, 36, 87. http://www.opticsinfoba

Method 8410 5 R. A. Nyquist, The Interpretation of Vapor-Phase Infrared Spectra. Group Frequency Data; Volume I. Sadtler Laboratories: Philadelphia, PA, 1984.

Method 8410 6 G. Socrates, Infrared Characteristic Group Frequencies; John Wiley and Sons: New York, NY, 1980. http://www.amazon.co

Frequencies-Socrates/

SW-846 Update V References - 22 
SW-846 UPDATE V REFERENCE TABLE

Method 8410 7 L. J. Bellamy, The Infrared Spectra of Complex Organic Molecules; 2nd ed.; John Wiley and Sons: New York, NY, 1958.

http://www.amazon.comolecules/dp/B007T3Zqid=1355851489&sr=1red+spectra+complex+

Method 8410 8 H. A. Szymanski, Infrared Band Handbook, Volumes I and II; Plenum: New York, NY, 1965.

Method 8410 9

D. F. Gurka, "Interim Protocol for the Automated Analysis of Semivolatile Organic Compounds by Gas Chromatography/Fourier Transform-Infrared Spectrometry"; Appl. 

Spectrosc. 1985, 39, 826.

http://www.opticsinfoba827

Method 8410 10 P. R. Griffiths, J. A. de Haseth, L. V. Azarraga, "Capillary GC/FT-IR"; Anal. Chem. 1983, 55, 1361A. http://pubs.acs.org/doi/

Method 8410 11 P. R. Griffiths, J. A. de Haseth, Fourier Transform-Infrared Spectrometry; Wiley- Interscience: New York, NY, 1986. http://onlinelibrary.wile

matter/pdf

Method 8410 12

D. F. Gurka, I. Farnham, B. B. Potter, S. Pyle, R. Titus, W. Duncan, "Quantitation Capability of a Directly Linked Gas Chromatography/Fourier Transform Infrared/Mass Spectrometry System"; Anal. Chem. 1989, 61, 1584.

http://pubs.acs.org/doi/

Method 8430 1

W. D. Payne, T. W. Collette, "Identification of Bis(2-chloroethyl) ether Hydrolysis Products by Direct Aqueous Injection GC/FT-IR," J. of High Res. Chrom., 12, 693-696, 

1989.

http://onlinelibrary.wilebstract

Method 9013A 1 American Society for Testing and Materials, "Understanding Cyanide Species," D 6696, ASTM International, 2004. www.astm.org

Method 9013A 2 R. S. Ghosh, D. A. Dzombak, R. G. Luthy, "Equilibrium Precipitation and Dissolution of Iron Cyanide Solids in Water," Environ. Eng. Sci., Vol. 16, 293-313, 1999.Method 9013A 3

J. C. L. Meeussen, M. G. Keizer, W. H. van Riemsdijk, F. A. M. de Haan, "Dissolution 

Behavior of Iron Cyanide (Prussian Blue) in Contaminated Soils," Environ. Sci. Technol., Vol. 26, 1832-1838, 1992.

Method 9013A 4

J. C. L Meeussen, W. H. Keizer, F. A. M. de Haan, "Chemical Stability and Decomposition Rate of Iron Cyanide Complexes in Soil Solutions," Environ. Sci. Technol., Vol. 26, 511-516, 1992.

Method 9013A 5 J. T. Bushey, D. A. Dzombak, "Ferrocyanide Adsorption on Aluminum Oxides," J. Coll. Int. Sci., Vol. 272, 46-51, 2004.Method 9013A 6 T. L. Theis, M. L West, "Effects of Cyanide Complexation on the Adsorption of Trace Metals at the Surface of Goethite," Environ. Technol. Letters, Vol. 7, 309-318, 1986.Method 9013A 7 The RETEC Group, Inc., "Metal Cyanide Complexes by Anion Exchange Chromatography and UV Detection Method Validation Summary Report," March, 2004.

Method 9014 There are no references directly related to this method. References on total and amenable cyanide can be found in Method 9010.

SW-846 Update V References - 23 
SW-846 UPDATE V REFERENCE TABLE

Method 9015 1

American Society for Testing and Materials, "Standard Test Method for Determination of Metal Cyanide Complexes in Wastewater, Surface Water, Groundwater and Drinking Water using Anion Exchange Chromatography with UV Detection," D 6994, ASTM International, 2004. This reference can be purchased on line at ASTM’s web site: http://www.astm.org

www.astm.org

Method 9015 2 Dionex Corporation, "Determination of Metal Cyanides," Dionex Application Note No. 55, November, 1989. http://www.dionex.com

Method 9015 3

American Society for Testing and Materials, "Standard Guide for Understanding 

Cyanide Species," D 6696, ASTM International, 2004. This reference can be purchased on line at ASTM’s web site: http://www.astm.org

Method 9015 4 R. S. Ghosh, D. A. Dzombak, R. G. Luthy, "Equilibrium Precipitation and Dissolution of Iron Cyanide Solids in Water," Environ. Eng. Sci. , Vol. 16, 293-313, 1999. http://cat.inist.fr/?aModMethod 9015 5

J. C. L. Meeussen, W. H. Keizer, F. A. M. de Haan, "Chemical Stability and Decomposition Rate of Iron Cyanide Complexes in Soil Solutions," Environ. Sci. Technol. , Vol. 26, 511-516, 1992.

http://pubs.acs.org/doi/

Method 9015 6

J. C. L. Meeussen, M. G. Keizer, W. H. van Riemsdijk, F. A. M. de Haan "Dissolution Behavior of Iron Cyanide (Prussian Blue) in Contaminated Soils," Environ. Sci. Technol. , Vol. 26, 1832-1838, 1992.

Method 9015 7 U.S. Environmental Protection Agency, "Cyanide Extraction Procedure for Solids and Oils, Method 9013" U.S. EPA Office of Solid Waste SW-846 Manual.Method 9015 8 P. Doudoroff, "Toxicity to Fish of Cyanides and Related Compounds: A Review," EPA Report No. 600/3-76-038, 1976. http://books.google.com

&source=gbs_toc_r&ca

Method 9015 9 U.S. Environmental Protection Agency, "Total and Amenable Cyanide: Distillation, Method 9010" U.S. EPA Office of Solid Waste SW-846 Manual.Method 9015 10

American Society for Testing and Materials, "Standard Test Methods for Cyanides in Water," D 2036, ASTM International, 2004. This reference can be purchased on line at ASTM’s web site: http://www.astm.org

Method 9015 11 American Public Health Association, "Standard Methods for the Examination of Water and Wastewater," 20th Edition, 1998.

Method 9015 12

R. A. Wetzel, C. L. Anderson, H. Schleicher, G. D. Crook, "Determination of Trace Level Ions by Ion Chromatography with Concentrator Columns," Analytical Chemistry , Vol. 15, 

No. 9, 1532-1535, 1979.

http://pubs.acs.org/doi/

Method 9015 13

W. S. Rader, L. Solujic, E. B. Milosavljevic, J. L. Hendrix, "Sunlight-Induced Photochemistry of Aqueous Solutions of Hexacyanoferrate(II) and –(III) Ions," Environ. Sci. Technol. , Volume 27, 1875-1879, 1993.

http://pubs.acs.org/doi/

Method 9015 14 L. Moggi, F. Bolletta, V. Balzani, F. Scandola, "Photochemistry of Co-ordination Compounds_XV," J. inorg. Nucl. Chem. , Vol. 28, 2589-2597, 1966. http://www.sciencedire

803834

Method 9015 15

Dionex Corporation, "Product Manual IonPacÒ ATC-3 2-mm Anion Trap Column IonPac ATC-3 4-mm Anion Trap Column IonPac ATC-HC Anion Trap Column," Document No. 032697, Revision 08, July 12, 2002.

http://www.dionex.com08_IonPacATC-HC_3_

SW-846 Update V References - 24 
SW-846 UPDATE V REFERENCE TABLE

Method 9015 16

Dionex Corporation, "Product Manual IonPacÒ AG2 Guard Column IonPacÒ AG3 Guard Column IonPacÒ AG4 Guard Column IonPacÒ AG5 Guard Column IonPacÒ CG2 Guard Column IonPacÒ AS2 Analytical Column IonPacÒ AS3 Analytical Column IonPacÒ AS4 Analytical Column IonPacÒ AS5 Analytical Column IonPacÒ CS2 Analytical Column," Document No. 032226, Revision 14, May 12, 2002.

http://www.dionex.com14_AS2345_CS2_V17

Method 9015 17 Dionex Corporation, "Product Manual IonPacÒ AG11 Guard Column IonPacÒ AS11 Analytical Column," Document No. 034791, Revision 08, May 14, 2003. http://www.dionex.com

IonPac-AS11-Apr10.pd

Method 9015 18 Dionex Corporation, "Dionex Installation and Troubleshooting Guide for the IonPacÒ MFC-1 Metal-Free Trap Column," Document No. 034990, Revision 02, June 26, 1998. http://www.dionex.com

04_IP_MFC_V30.pdf

Method 9015 19 U.S. Environmental Protection Agency, "Determinative Chromatographic Separations, Method 8000" U.S. EPA Office of Solid Waste SW-846 Manual.Method 9015 20

R. M. Smith, A. E. Martell, "NIST Critically Selected Stability Constants of Metal Complexes Database, Version 5.0 Database Software" NIST Standard Reference Database 46, U.S. Department of Commerce, Gaithersburg, Maryland, 1998.

http://www.nist.gov/srd

Method 9015 21

D. D. Wagman, W. H. Evans, V. B. Parker, R. H. Shumm, I. Halow, S. M. Bailey, K. L. Churney, R. L. Nuttal, "The NBS Tables of Chemical Thermodynamic Properties, Selected Values for Inorganic and C1 and C2 Organic Substances in SI Units," Journal 

of Physical and Chemical Reference Data , Vol. 11, Supplement 2, 1-392, 1982.

http://jpcrd.aip.org/jpcr

Method 9015 22 The RETEC Group, Inc., "Metal Cyanide Complexes by Anion Exchange Chromatography and UV Detection Method Validation Summary Report," March, 2004.Method 9015 23

U.S. Environmental Protection Agency, "Total and Amenable Cyanide (Automated Colorimetric, with Off-Line Distillation), Method 9012" U.S. EPA Office of Solid Waste SW-846 Manual.

Method 9320 1

Greenberg, A.E., J.J. Connors, and D.J. Jenkens, eds., Standard Methods for the Examination of Water and Wastewater, 15 th ed., American Public Health Assoc., 

Washington, D.C., Method 707, p. 600, 1980.

http://www.standardme

Method 9320 2

Johnson, J.O., Determination of Radium 228 in Natural Waters. Radiochemical Analysis of Water. U.S. Geol. Surv., Water Supply Paper 1696-G. U.S. Govt. Printing Office, Washington, D.C., 1971.

http://pubs.usgs.gov/w

Method 9320 3

Krieger, H.L., Prescribed Procedures for Measurement of Radioactivity in Drinking Water, Environmental Monitoring and Support Laboratory, U.S. EPA, Cincinnati, OH, EPA-600/4-75-008, 1976.

http://nepis.epa.gov/

Chapter 1 1

USEPA. Guidance on Systematic Planning Using the Data Quality Objectives Process, EPA QA/G-4 . Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006. 

http://www.epa.gov/qu

SW-846 Update V References - 25 
SW-846 UPDATE V REFERENCE TABLE

Chapter 1 2

USEPA. EPA Quality Manual for Environmental Programs CIO 2105-P-01-0 . Office of 

Environmental Information Quality Staff, United States Environmental Protection Agency, Washington, D.C. May 5, 2000. 

http://www.epa.gov/irm

Chapter 1 3

USEPA. Guidance on Choosing a Sampling Design for Environmental Data Collection, EPA QA/G-5S. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. December 2002.

http://www.epa.gov/qu

Chapter 1 4

USEPA. Guidance on Environmental Data Verification and Data Validation , EPA QA/G8. Quality Staff, Office of Environmental Information, United States Environmental 

Protection Agency, Washington, D.C. November 2002. 

http://www.epa.gov/qu

Chapter 1 5

USEPA. Data Quality Assessment: A Reviewer’s Guide , QA/G-9R. Quality Staff, 

Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006.

http://www.epa.gov/qu

Chapter 1 6

USEPA. Data Quality Assessment: Statistical Tools For Practitioners , QA/G-9S. 

Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. February 2006. 

http://www.epa.gov/qu

Chapter 1 7

USEPA. Guidance for Preparing Standard Operating Procedures , EPA QA/G-6. Quality 

Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. April 2007. 

http://www.epa.gov/qu

Chapter 1 8 USEPA. RCRA Waste Sampling Draft Technical Guidance. Office of Solid Waste, United States Environmental Protection Agency, Washington, D.C. August 2002. http://www.epa.gov/wa

wsdtg_a.pdf

Chapter 1 9

USPEA. Guidance for Quality Assurance Project Plans , EPA QA/G-5. Quality Staff, 

Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. December 2002. 

http://www.epa.gov/qu

Chapter 1 10

USEPA. EPA Requirements for Quality Assurance Project Plans , EPA QA/R-5. Quality 

Staff, Office of Environmental Information. United States Environmental Protection Agency, Washington, D.C. March 2001. 

http://www.epa.gov/qu

Chapter 1 11 USEPA. RCRA Delisting Program Guidance Manual for the Petitioner . United States http://www.epa.gov/regChapter 1 12

USEPA. Waste Analysis at Facilities That Generate, Treat, Store and Dispose of Hazardous Wastes , ECDIC 2002-011. Office of Waste Programs Enforcement, United States Environmental Protection Agency. April 1994. 

http://www.epa.gov/cowasteanalygman-rpt.pd

Chapter 1 13

USEPA. Guidance on Technical Audits and Related Assessments for Environmental Data Operations , QA/G-7. Quality Staff, Office of Environmental Information, United States Environmental Protection Agency, Washington, D.C. January 2000. 

http://www.epa.gov/qu

Chapter 2 1 M. J. Barcelona, "TOC Determinations in Ground Water," Ground Water 1984, 22(1), 18- http://info.ngwa.org/gwChapter 2 2

R. Riggin, et al.; Development and Evaluation of Methods for Total Organic Halide and 

Purgeable Organic Halide in Wastewater; U.S. Environmental Protection Agency; Office of Research and Development; Environmental Monitoring and Support Laboratory; ORD Publication Offices of Center for Environmental Research Information; Cincinnati, OH, 1984; EPA-600/4-84-008.

http://nepis.epa.gov/Ex

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Chapter 2 3

G. McKee, et al.; Determination of Inorganic Anions in Water by Ion Chromatography 

(Technical addition to Methods for Chemical Analysis of Water and Wastewater, EPA 600/4-79-020); U.S. Environmental Protection Agency; Environmental Monitoring and Support Laboratory; ORD Publication Offices of Center for Environmental Research Information; Cincinnati, OH, 1984; EPA-600/4-84-017.

Chapter 3 1 Skoog, D. A., "Principles of Instrumental Analysis," 3rd ed, Saunders College Publishing, Philadelphia, PA, 1985. http://www.4shared.co

_Principles_of_Instrum

Chapter 3 2

EPA, U.S., "Sampling Ambient Water for Trace Metals at EPA Water Quality Criteria Levels, Method 1669, U.S. Environmental Protection Agency, Office of Water, Washington, D.C., 1996.

http://www.ecy.wa.gov69.pdf

Chapter 3 3 Adeloju, S. B. and Bond, A. M., "Influence of Laboratory Environment on the Precision and Accuracy of Trace Element Analysis," Anal. Chem. , 1985, 57, 1728-1733. http://pubs.acs.org/doi/

Chapter 3 4

Kingston, S. H. M., et al., "Microwave Enhanced Chemistry: Fundamentals, Sample Preparation, and Applications," American Chemical Society, Washington, DC, 1997, p. 257-279.

Chapter 3 5 Moody, J. R., "NBS Clean Laboratories for Trace Element Analysis," Anal. Chem. , 1982, 54, 1358A-1376A.

Chapter 3 6

Murphy, T., "National Bureau of Standards Special Publication 422 Accuracy in Trace Analysis: Sampling, Sample Handling, and Analysis," National Bureau of Standards, Gaithersburg, MD, 1976, p. 509-539.

Chapter 3 7 Tolg, G. and Tschopel, P., "Determination of Trace Elements," VCH, New York, NY, 1994, p. 1-38.Chapter 3 8 Zief, M. and Mitchell, J. W., "Chemical Analysis, Vol. 47, John Wiley & Sons, New York, NY, 1976.Chapter 3 9 Kuehner, E. C., et al., "Production and Analysis of Special High-Purity Acids Purified by Sub-Boiling Distillation," Anal. Chem. , 1972, 44, 2050-2056. http://pubs.acs.org/doi/

Chapter 3 10 Moody, J. R., "Purified Reagents for Trace Metal Analysis," Talanta , 1982, 29, 1003- 1010. http://www.sciencedire

802415

Chapter 3 11 Kuehner, E. C. and Freeman, D. H., "Purification of Inorganic and Organic Materials," Marcel Dekker, New York, NY, 1969, p. 297-306. http://onlinelibrary.wile

stract

Chapter 3 12 Moody, J. R., "The Sampling, Handling and Storage of Materials for Trace Analysis," Philos. Trans. R. Soc. London , 1982, 305, 669-680. http://www.jstor.org/ps

Chapter 3 13 Moody, J. R. and Lindstrom, R. M., "Selection and Cleaning of Plastic Containers for Storage of Trace Element Samples," Anal. Chem. , 1977, 49, 2264-2267. http://chemgroups.nort

odyLindstrom1977.pdf

Chapter 3 14 Prevatt, F. J., "Clean Chemistry for Trace Analysis," Environmental Testing and Analysis , 1995, 4, 24-27.

Chapter 3 15

Skelly, E. M. and DiStefano, F. T., "Clean Room and Microwave Digestion Techniques: Improvement in Detection Limits for Aluminum Determination by GF-AAS," Appl. Spectrosc. , 1988, 42, 1302-1306.

http://www.cem.de/doc06.PDF

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Chapter 3 16 Rabinowitz, M. B. and Wetherill, G. W., "Identifying Sources of Lead Contamination by Stable Isotope Techniques," Environ. Sci. Technol. , 1972, 6, 705-709. http://pubs.acs.org/doi/

Chapter 3 17 Maienthal, E. J., "U.S. National Bureau of Standards Technical Note 545," National Bureau of Standards, Gaithersburg, MD, 1970, p. 53-54. http://babel.hathitrust.o

00&id=mdp.390150013

Chapter 3 18 Boothe, P. N. and Nicolau, B.A. "The Coastal Bend Bays Project," 26th Annual Conference on Analysis of Pollutants in the Environment , Chicago, IL 2003. http://www.epa.gov/em

sia/symp2004/presenta

Chapter 3 19 Miller, G. T., "Living in the Environment, Wadsworth Inc., Belmont, CA, 1994. http://www.coursesma

enhanced-homework/m

Chapter 3 20 Gy, P., "Sampling for Analytical Purposes" Wiley, New York, NY, 1998.

Chapter 3 21 Pitard, F.F. "Pierre Gy's Sampling Theory and Sampling Practice," Second Edition, CRC Chapter 3 22 EPA, U.S., "Correct Sampling Using the Theories of Pierre Gy," Office of Research and Development, Las Vegas, NV, 1999. http://www.epa.gov/esdChapter 3 23 EPA, U.S., "Guidance for Obtaining Representative Laboratory Analytical Subsamples from Particulate Laboratory Samples." Office of Research and Development, 2003. http://www.epa.gov/osChapter 4 1

 A. B. Dindal, R. A. Jenkins, and C. K. Bayne. "Summary Report - Evaluation of the Impact of Post-Holding Time Analyte Degradation on Regulatory Decision-Making - VOCs in Water," Oak Ridge National Laboratory. 2001.

Chapter 4 2

ASTM Standard D4841, 1988 (2008). Standard Practice for Estimation of Holding Time for Water Samples Containing Organic and Inorganic Constituents. ASTM International, West Conshohocken, PA, 2003, DOI: 10.1520/D4841-88R08, www.astm.org

Chapter 4 3

J. T. Love, G. C., Deltzer, S. R. Abney, and J. S. Zogorski. “Study Design and Analytical Results Used to Evaluate Stability of Volatile Organic Compounds in Water Matrices.” United States Geological Survey Open-File Report 98-637. 1999.

Chapter 4 4

M. P. Maskarinec, C. K. Bayne, L. H. Johnson, S. K. Holladay, and R. A. Jenkins. “Stability of Volatile Organics in Environmental Water Samples: Storage and Preservation.” Oak Ridge National Laboratory ORNL/TM-11300. 1989.

http://www.dtic.mil/cgi-

Chapter 4 5

O. R. West, C. K. Bayne, R. L. Siegrist, W. L. Holden, S. S. Scarborough, and D. W. Bottrell. “Stability of VOCs in Water samples During Pre-analytical Holding. Part 1. Analyses by a Commercial Laboratory.” Oak Ridge National Laboratory ORNL/TM13240/V1. 1996.

Chapter 4 6

O. R. West, C. K. Bayne, R. L. Siegrist, W. L. Holden, and D. W. Bottrell. “Stability of VOCs in Water samples During Pre-analytical Holding. Part 2. Analyses by an EPA Regional Laboratory.” Oak Ridge National Laboratory ORNL/TM-13240/V2. 1997.

http://www.osti.gov/brid6XVR0S/webviewable/

Chapter 4 7

C. K. Bayne, D. D. Schmoyer, and R. A. Jenkins. “Practical Reporting Times for Environmental Samples.” Environmental Science and Technology, 28: 1430-1436. 1994.

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Chapter 4 8

M. P. Maskarinec, C. K. Bayne, R. A. Jenkins, L. H. Johnson, and S. K. Holladay. “Final Report - Stablity of Volatile Organics in Environmental Soil samples.” Oak Ridge National Laboratory ORNL/TM-12128. 1992.

Chapter 4 9 Preservation and Holding Times Study for Vinyl Chloride, Styrene in Industrial Wastewater provided by Test America, January 2012.Chapter 4 10

Preservation and Holding Times Study for Vinyl Chloride, Styrene in Municipal Wastewater provided by the Hampton Roads Sanitation District in Virginia Beach, Virginia, January 2012.

Chapter 4 11

ASTM Guide D4547, 1991 (2009). Standard Guide for Sampling Waste and Soils for Volatile Organic Compounds. ASTM International, West Conshohocken, PA, 2003, DOI: 10.1520/D4547-09, www.astm.org

Chapter 4 12 U.S. Environmental Protection Agency. “Sample Holding Time Re-evaluation.” http://www.epa.gov/esd

Chapter 4 13 U.S. Environmental Protection Agency. “Performance of Hydrochloric Acid and http://www.epa.gov/nrmChapter 4 14 ASTM Standard Practice D6418, 2003 (2009). Standard Practice for Using the Chapter 4 15 U.S. Environmental Protection Agency. “Integrity of VOA Vial Seals.” EPA/600/R- 00/066. 2000. http://www.epa.gov/esdChapter 5 No references listed in Chapter.

End of Update V References

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