# AIR QUALITY TECHIVICAL SERVICES, IIVC.



# COMPLIANCE REPORT
FLUORIDE EMISSION COMPLIANCE PROGRAM

for BRICK MANUFACTURING PROCESS

Submitted for: VERMONT BRICK MANUFACTURING, L.P.

P. O. Box 330 Highgate Center, Vermont 05459

18 Morse Drive, Essex Junction, Vermont 05452 (802) 879-1800

# COMPLIANCE REPORT
FLUORIDE EMISSION COMPLIANCE PROGRAM



# for BRICK MANUFACTURING PROCESS

Submitted for: VERMONT BRICK MANUFACTURING, L.P.

P. O. Box 330 Highgate Center, Vermont 05459
P. O. Number: Verbal
Submitted to: AGENCY OF NATURAL RESOURCES DEPARTMENT OF ENVIRONMENTAL CONSERVATION

AIR POLLUTION CONTROL DIVIS[ON -

103 South Main Street Waterbury, Vermont 05671-0402

Submitted by: AIR QUALtTY TECHNICAL SERVICES, INC.

18 Morse Drive Essex Junction, Vermont 05452 Project: 021304 November 25, 2002

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# FOREWORD

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# Air Quality Technical Services, Inc., an environmental consulting company specializing

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# in air resource management and air quality assessment, was contracted by Vermont Brick

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# Manufacturing, L.P. to conduct a source emission compliance program at the facility which it

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# owns and operates in Highgate, Vermont. The source involved in the program was the M 

# emission control system that services the Water Struck Brick Manufacturing Process.

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# This report presents results, test and analytical data, sampling and analytical methods,

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# and other relevant data pertaining to the program.



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# ' Air Quality Technical Services, Inc. 18 Morse Drive Essex Junction, Vermont 05452 Telephone: 802-879-1800 Fax: 802-879-8875

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FOREWORD
1.0 INTRODUCTION 2.0 SOURCE DESCRIPTION 2.1 KILN PROCESS
3.0 PROGRAM STRUCTURE 3.1 SAMPLING APPROACH
4.0 SUMMARY OF RESULTS TABLE OF CONTENTS Vermont Brick Highgate, VT

1
2 2
5 

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_ 8 5.0 COMPLIANCE PROCEDURES 9 5.1 SAMPLING LOCATION 10 5.1.1 Velocity Head Measurements 10 5.1.2 Fluoride Measurements 10 5.2 FLUORIDE MEASUREMENT PROCEDURES 12 5.2.1 Sampling 12 5.2.1.1 Sampling Apparatus 12 5.2.1.2 Quality Control/Quality Assurance 14 5.2.1.2.1 Equipment Calibration 14 5.2.1.2.1.1 Nozzle 14 5.2.1.2.1.2 Critical Orifice 14 5.2.1.2.1.3 Dry Gas Meter 14 5.2.1.2.2 Leak Checks 14 5.2.1.2.2.1 Sample train 14 5.2.1.3 Sample Recovery 15 5.2.2 Analytical Procedures 15 

# 5.3 GAS VELOCITYIVOLUMETRIC FLOW 16 5.3.1 Measurement Apparatus 16 5.3.1.1 Quality Control/Quality Assurance 16 5.3.1.1.1 Equipment Calibration 16 5.3.1:1.1.1 Pitot Tubes 16 5.3.1.1.1.2 Thermocouple Probe 16

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# TABLE OF CONTENTS (cont'd) 5.3.1.1.2 Leak Checks 17 5.3.1.1.2.1 Pitot Tubes 17 5.4 GAS COMPOSITION 18 5.5 MOISTURE CONTENT 19
APPENDIX A: APPENDIX B: APPENDIX C: APPENDIX D: APPENDIX E: APPENDIX F: APPENDIX G: Equation Format

Summary Of Results Test Data Summary Sheets Computerized Field Test Data Sheets Analytical Data Operating Data Log Equipment Calibration Sheets



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# 1.0 INTRODUCTION 0 

# 1 Vermont Brick Manufacturing, L.P. (Vermont Brick), operates a clay mining and brick

manufacturing plant in Highgate, Vermont. The brick manufacturing process involves operation of a periodic kiln which generates exhaust gases containing emissions of fluoride. Vermont Brick was issued an original Air Pollution Control Permit on October 25, 1995, and, an amended Permit (#AP-95-009a) on October 17, 1996, by the State of Vermont Agency of Natural Resources, Department of Environmental Conservation, Air Pollution Control Division (APCD). Condition (6) of the amended Permit requires that Vermont Brick install, operate, and maintain an Ohlmann limestone scrubber/adsorber, or equivalent device to control the fluoride emissions from the periodic brick kiln when the kiln temperatures are in excess of 752

_ °F. Condition (8) of the amended Permit limits emissions of total fluoride, including elemental fluoride and ali fluoride compounds from the periodic kiln to a maximum of 24.8 pounds per complete kiln cycle or 0.18 pounds per ton of dry brick produced. Condition (12) of the amended Permit requires that Vermont Brick perform emission testing for total fluorides, including elemental fluoride and all fluoride compounds, from the periodic kiln exhaust. An initial compliance test program was conducted March 15 - 17, 2000. Based on fluoride concentrations measured during testing, the APCD calculated that emissions from the kiln were in violation of the permitted allowable limits. As a resuft a NOTICE OF ALLEGED VIOLATION was issued and corrective measures that would bring the source into compliance were requested to he taken. A second compliance test program was required to evaluate the impact of these measures upon completion. The field portion of the second compliance test program was performed October 1- 3, 2002. The major on-site representatives that participated in the program and their respective 

# affiliations were:
Vermont Brick Mark Kellner - Operations Manager Air Quality Technical Services, Inc. John Jasko - Project Director Dave Evans - Technician



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## Project: 021304 Vermont Brick Highgate, VT 

# 2.0 SOURCE DESCRIPTION Clay is mined on the facility grounds and transported to a building for storage while awaiting processing. When it is taken from storage the clay is placed in a hopper and metered out to a conveyor, where approximately 14 to 15 percent sand is added, that carries 'it to a pug mill. At the pug mill barium carbonate is added to the clay/sand mixture in the respective ratio of forty ounces per ton. The combined product is worked in the pummel and then conveyed to a second horizontal pummel for additional blending. The clay mixture is transferred from the second horizontal pummel to a Posey brick machine for molding. *The Posey brick machine is metered by variab(e frequency drive to ram press the clay mixture into water wetted molds, each of which contains forms for seven brick, at a rate of one mold every five seconds. As the ram lifts after loading a mold, a blade sweeps across the top of the mold box thus "striking" off excess clay. As the loaded mold box slides out from under the press, a new mold box slides under the press. The loaded mold box is then flipped over emptying the seven wet or "green" brick onto a small drying pallet. The green brick are loaded on drier cars and dried at a temperature of 200 °F for a period of thirty hours using indirect steam heat generated by recovering heat from the kifn process of natural gas . One days green brick production equals forty-four dryer cars or 32,032 brick.
2.1 KILN PROCESS The dry brick are transferred to kiln cars with 7800 brick per car. The brick are set on the kiln cars in a manner that leaves spaces between the individual bricks to facilitate even heat flow through the racks during the kiln cycle. The kiln has three independently controlled temperature zones fired on natural gas, and is loaded with seven kiln cars holding approximately 54,600 brick. A typical kiln cycle lasts forty-two to fifty-one hours depending on desired finished product with an additional ten to fifteen hours for cool down. After loading, the kiln is ramped to a set point temperature of approximately 300 °F over a period of about thirty minutes. The kiln maintains this "soak" temperature for an additional thirty minutes. During this initial heat up phase, the exhaust gases from the kiln are ducted directly to a primary induced draft fan at the base of the stack and are vented to the atmosphere. The kiln enters cycle segment 1 as it is ramped to a set point temperature of approximately 1800 °F over a period of about ten hours. V11hen the kiln reaches a temperature of 350 °F during this phase, system dampers divert the exhaust gases through a recovery boiler 

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# for heat reclamation with the assist of an secondary induced draft fan. When the kiln attains a temperature of 700 °F during this phase, additional system dampers direct the flow of the exhaust gases in the system after the recovery boiler through the limestone scrubberladsorber for control of fluoride emissions before passing through the primary induced draft fan and being discharged to the atmosphere. 

# At the end of the ten hour ramp when the 1800 °F set point is achieved, the kiln enters ' cycle segment 2, a 12 hour soak designed to burnout the carbon in the clay body.

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# At the end of cycle segment 2, the kiln enters cycle segment 3, a ramp of 2 hour

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# duration that brings the kiln to a set point temperature of 1910 °F at which product shrinkage ;.

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# and densification occur. f The kiln maintains this finishing "soak" temperature, cycle segment 4, for an additiona( ! 20 to 25 hours depending on the rate of shrinkage of the desired finished product.

# ► After the curing cycle is complete, the kiln enters a cool down phase, cycle segment 5, 1 during which the temperature is allowed gradualiy drop. Approximatefy 15 hours into the cool 1 down phase, when the temperature drops below 700 °F the system dampers that diverted 1 exhaust gas flow through the scrub be r/adso rber are reset and the exhaust gas flow is vented 1 directly to the atmosphere.

A schematic of the kiln and exhaust systern configuration is shown in Figure 2-1.

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# Project: 021304 Vermont Brick Highgate, VT 

# 3.0 PROGRAM STRUCTURE 

# For the purpose of conducting a sampling program that would result in a representative evaluation of emissions of fluoride over the lengthy duration of the kilning, the entire cycle was to be separated into process events as follows: • Segment I 

# - Ramp 

# Initial startup firing of burners and ramping of temperature to 1800 °F. Targeted program duration 10 hours. Approximate clock time from 10:30 to 20:30 (10101/02). Note: Exhaust flow diverted through scrubber around 17:00. • Segment 2 

# - Initial Soak



# _ Temperature held at 1800 °F for carbon burnout. Targeted program duration 12 hours. Approximate clock time from 20:30 (10/01/02) to 08:30 (10/02/02). • Segment 3 

# - Ramp 

# Ramping of temperature to 1910 °F. Targeted program duration 2 hour. Approximate clock time from 08:30 to 10:30 (10/02102). • Segment 4 

# - Final Soak 

# Curing of brick to achieve desired shrinkage. Targeted program duration 25 hours. Targeted approximate clock time from 10:30 (10102/02) to 11:30 (10/03102). • Segment 5 

# - Cool Down 

# Gradual cooling of kiln. Targeted approximate clock time from 11:30 (10/03l02) to approximately 15 hours later when temperature drops below 700 °F and exhaust flow is redirected to bypass scrubber.

_ Page 5 AIR QUALITY TECHI111CAL SERVICES, INC.

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# 3.1 SAfVIPLING APPROACH Sampling of emissions was conducted with a sample train that was controlled with a delay-on-make timing mechanism to cycle between off and on on a sixty minute schedule. Based on the preliminary measurements of exhaust conditions (i.e. average velocity head pressure, temperature, gas composition, and an estimated moisture content) made November 17, 1999, and July 25, 2002, with the kiln operating in a Segment 4- Soak condition, and, data collected during the first compliance test program, an average sample rate was calculated that would satisfy isokinetic requirements. A critical orifice was selected ,to be placed in line prior to the sample control console that would control sample flow at this predetermined isokinetic rate 10 percent) for the nozzle size used. When the process system achieved the 700 °F set point at approximately 17:00 on October 1, causing the exhaust flow to be directed through the scrubber, the initial sampfing cycle was initiated by activating the control timer. The first hour of the cycle was an "off' period; the second hour of the cycle was an "on" period. This "off' and "on" alternating of the sampling system continued through the course of the three and one half hour duration remaining of Segment 1 and, unfortunately, into the first half hour of Segment 2 resuiting in a total of two hours of active sample collection. At the end of the first sampling cycle the control timer was deactivated and the composite sampfe representing Segment 1, but including a thirty minute portion of Segment 2, was recovered. The same "off' and "on" alternating of the sampling system continued over the remaining course of Segment 2 starting at 21:10, forty minutes into the Segment, and continuing until 08:10 (10/02/02) resulting in a total of five hours of active sample collection during the twelve hour Segment duration. At the end of the second sampling cycle, the control timer was deactivated and the composite sample representing Segment 2 was recovered. A representative sample was not coilected for Segment 3 due to its short duration and the lack of time needed to prepare the sampie system. A new sampling cycle was initiated by again activating the control timer at 09:30 during the last hour of Segment 2 as an "off' period. As the process entered Segment 4 at 10:30 the control timer entered an "on" period and active sampling started. For this round of sampling the cycling of the sampling continued over the course of the first eleven hours of Segment 4 terminating at 21:30, resuiting in a total of six hours of active sample collection. At the end of this third sampling the control timer was allowed to remain active while the composite samp(e representing the first portion of Segment 4 was recovered. . By the time the next "on" period for the control timer was reached at 22:30 the recovery was complete and the sample train was prepared for the ensuing sample round. For this round _ Page 6 A1R QUAd.17"Y 1'ECHIdICAL SERI/ICES, 1111C.
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# of sampling the cycling of the sampling continued over the course of the last thirteen hours of Segment 4 terminating at 11:30 (10/03/02), resulting in a total of seven hours of active sample collection. At the end of this fourth sampling the control timer was deactivated while the composite sample representing the second portion of Segment 4 was recovered. A final sampling cycle was initiated by again activating the control timer at 11:30 at the start of Segment 5, the kiln cool down, as an "off' period. For this round of sampling the cycling of the sampling continued over the course of the first four hours of Segment 5 terminating at 

# 15:30, resulting in a total of two hours of active sample collection.

Page 7



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# 4.0 

# SUMMARY OF RESULTS

For the purpose of determining representative emissions of fluoride for each process segment composite samples of either two or four hour duration were collected at a sample rate of approximately 0.25 cfm.


# TOTAL FLUORIDE Test 1 2 3 4 5 Date 10/01 10/01-02 10/02 10/02-03 10/03 Cycle Segment 1 2 4 4 5 Cycle Clock Time (24 hour) 17:00-20:30 20:30-08:30 10:30-21:30 21:30-11:30 11:30-? Test Period Time (24 hour) 16:57-20:5721:10-08:10 10:30-21:30 21:30-11:30 11:30-15:30 Active Sample lntervals 2 5 6 7 2 Sample Duration (minutes) 120 300 360 420 120 Average Test Measurements Isokinetics (%) 104.0 108.1 105.5 101.9 85.5* Moisture Content (%) 15.2 12.0 8.9 

# 4 • 4 0.7 Velocity Hear Pressure ("H 2 0) 0.24 0.25 0.26 0.27 0.36 Temperature (OF) 274.5 427.2 513.9 539.4 491.4 Gas Composition - CO 2 (%) 6.6 5.1 3.9 3.4 0.1

0 2 (%) 9.8 12.7 14.3 15.2 20.7 CO (%} 0 0 0 0 0 N z(%} 83.6 82.2 81.8 81.4 79.2 Gas Velocity (fps) 33.2 37.1 39.5 40.5 45.2 Gas Volumetric Flow (dscfm) 5726 5498 5516 5780 7117 (acfm) 9454 10565 11248 11533 12871 Emission Determinations Total Fluoride: Concentration: (μgldscf) 15.511 64.293 383.376 94.210 23.459



# (Ibs/dcsf) 4.082x10 -8 1.418x10

- ' 8.453x10

- ' 2.077X10

- ' 5.173x10 -8 Emission Rate: (Ibs/hr) 0.014 0.047 0.280 0.072 0.022 * Note: Test 5 fell outside of the isokinetic range due to an unexpected large increase in velocity head pressure during Segment 5 beyond those measured for the other Segments (0.36 as opposed to 0.24-0.27) that the expected that isokinetic rate calculations were based upon.
Page 8

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# 5.0 

# COMPLIANCE PROCEDURES Due to the unconventional nature of the emission compliance program, the procedures used were conducted in accordance with, or using as guidelines, the Reference Methods described in Appendix A of 40 CFR Part 60, as revised July 1, 2001. Any deviations made to these Reference Method procedures were not considered to adversely impact the results of the sampling program. The test methods to be used for the determination of compliance are referenced as follows: Method 1 - Sample and Velocity Traverses for Stationary Sources; Method 2 - Determination of Stack Gas Velocity and Volumetric Fiow Rate (Standard Type Pitot Tube Option); Method 3 - Gas Analysis for the Determination of Dry Molecular Weight; Method 4 - Determination of Moisture Content in Stack Gases; Method 13B - Determination of Total Fluoride Emissions from Stationary Sources - Specific lon Electrode Method.

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# 5.1 SAMPLING LOCATION The sampling location was positioned according to the guidelines set forth in Method 1, "Sample and Velocity Traverses for Stationary Sources" . .. The sample ports were located in the stack approximately 32.0 feet downstream from juncture of the induced draft (ID) fan discharge duct with the stack and approximately 5.5 feet upstream from the outlet of the stack. At the sampling location the stack had an inside diameter of 29.5 inches. This positioned the sampling location approximately 13.0 diameters downstream and approximately 2.2 diameters upstream from the appropriate ffow disturbances.
5.1.1 Velocity Head Measurements The Method 1 required minimum of 8 traverse points used for preliminary velocity head ° measurements conducted November 17, 1999, and July 25, 2002, indicated that a very even profile existed across the face of the stack at the sample port location.

. In consideration of this fact, the velocity head pressure measurements recorded during compliance testing were monitored at a single point located at the center of the stack.
5.1.2 Fluoride Measurements Samples used for the determination of the fluoride content of the exhaust stream were 

# acquired from a single point of average velocity located near the center of the stack. A schematic of the sample port location and the velocity and sample point layout can be found in Figure 4-1.



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# SAMPLING LOCATION



# F(GURE 5-1



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# 5.2 FLUORIDE MEASUREMENT PROCEDURES Fluoride sampling was conducted in accordance with Method 1313, Determination of Total Fluoride Emissions from Stationary Sources - Specific Ion Electrode Method. 5.2.1 Sampling 5.2.1.1 Sampling Apparatus The sample train consisted of: a) a stainless steel nozzle sized to provide an average isokinetic sample rate;

_ b) a borosilicate glass-lined probe heated to a temperature of 248 °F, ± 25 °F; c) a sample trainlmoisture condensing unit with four 500 ml glass impingers immersed in an ice water bath: a modified Greenburg-Smith type impinger containing approximately 100 ml of distilledldeionized water and weighed to establish a known starting weight, a Greenburg-Smith type containing approximately 100 ml of distilledldeionized water and weighed to establish a known starting weight, a modified Greenburg-Smith type impinger empty and weighed to establish a known starting weight, a Whatman No. 1 paper filter encased in a glass filter holder, and, a modified Greenburg-Smith type impinger containing approximately 200 grams of silica gel and weighed to estab(ish a known starting weight; d) a vacuum sample line; e) a critical orifice sized to an average isokinetic sarnple rate; f) a vacuum sampling pump adjusted to provide a critical vacuum to the orifice; g) a calibrated dry gas meter for totalizing sample volume, and, h) a timing relay to activate the sampling pump at preset intervals. A EurothermlChessel Data Logger was used to continuously record the dry gas meter inlet and outlet, impinger outlet and probe temperatures during testing. A schematic of the sample train is depicted in Figure 5-2. Page 12



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# 5.2.1.2 Quality ControllQuality Assurance 5.2.1.2.1 Equipment Calibration
5.2.1.2.1.1 Nozzle The nozzle used in compliance program was calibrated according to procedures outlined in Method 5, Section 5- Calibration (§5.1 Probe Nozzie).
5.2.1.2.1.2 CriticalOrifice
The orifice was calibrated to establish the critical flow rate and the vacuum needed to achieve the choked ffow. A sample train, configured to duplicate the trains to be used in the sampling portion of the program, from the tirst impinger back, was connected to a wet test meter and a series of three volumetric flow observations were made over a set time interval. These observations were recorded on a calibration data sheet afong with readings of ineter temperature and barometric pressure. The three observations were averaged to obtain a average critical flow rate. 5.2.1.2.1.3 Dry Gas Meter Dry gas meters undergo semiannual calibration according to procedures outlined in Method 5, Section 5- Calibration (§5.3 Metering System, §5.3.1 Cafibration Prior to Use). After completion of the compliance program, the dry gas meter calibration was rechecked for accuracy according to procedures outlined in Method 5, Section 5- Calibration (§5.3 Metering System, §5.3.2 Caiibration After Use).
5.2.1.2.2 Leak Checks 5.2.1.2.2.1 Sample Train The sample trains were leak checked according to procedures outlined in Method 5, Section 4- Procedure (§4.1 Sampling, §4.1.4 Leak-Check Procedures). Before the start of each test series, the infet of the probe nozzle was sealed off with a section of gum rubber tubing and a tubing clamp, and the predetermined vacuum (approximately 15" Hg) needed to operate the orifice at critical flow was applied upstream of the orifice. In each instance this 

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# resulted in a vacuum of <2 "Hg. on the sample train downstream of the orifice. The metering dial on the dry gas meter was then timed for a period of one minute and any movement during that period was noted and recorded. At the end of each test series, the same procedure was followed. 5.2.1.3 Sample Recovery At the completion of each test series the sample train was processed and recovered as follows: • Nozzlelprobe - The nozzle and probe was internally brushed and rinsed in triplicate with distiiled/deionized water. The rinses were collected in a polyethylene storage bottle. • Water (mpingers - The first three impingers were reweighed to determine the net weight gain resuiting from the volume of condensate collected from the

.. sample stream. The contents was then -added to the polyethylene storage bottle used to collect the nozzle/probe rinses. The Impingers and connecting glassware up to the front half of the filter holder was rinsed in triplicate with distilled/deionized water and the rinses were added to the storage bottle. • Filter - The filter paper was removed from the filter holder and added to the polyethylene storage bottle.♦ 

# Silica Gel Impinger - The fourth impinger was reweighed to determine the net weight gain attributable to any additional water vapor absorbed from the sample stream. 5.2.2 Analytical Procedures Analysis was performed by Oxford Laboratories of Wilmington, North Carolina according to all procedures for sample fusion, digestion and ion specific electrode analysis as required by Method 13B.



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# 5.3 GAS VELOCITYIVOLUiVIETRIC FLOW 

# Measurements of stack gas velocity and volumetric flow was performed using procedures outlined in EPA Test Method 2 as a guideline. Veiocity head pressure was monitored at a single point at the center of the stack over the course of each fluoride sampiing period. The monitored pressures showed no variation over the course of each individual sampling period and very little variation over the course of 

# the entire program with the exception of Segment 5, the cool down cycle. These monitored pressures were used for the determination of mass emission rate. 5.3.1 Measurement Apparatus The apparatus used,to measure stack differential pressure and temperature profiles consisted of: a) a S-type pitot tube with an assigned design coefficient of 0.84 connected to an inclined manometer; and, b) a Type-K thermocouple probe connected to a EurothermlChessel Data Logger to continuously record stack temperature. 5.3.1.1 Quality ControllQuality Assurance 5.3.1.1.1 Equipment Calibration
5.3.1.1.1.1 Pitot Tubes The S-type pitot tube assembly used for velocity head measurement was checked for conformity with the design specifications listed in Method 2(4. Calibration, §4.1 Type S Pitot Tube, §4.1.1 Type S Pitot Tube Assemblies). 5.3.1.1.1.2 Thermocouple Probe The thermocouple probe used in the test program underwent annual calibration according to procedures outlined in the Quality Assurance Handbook, Section 3.1 - Method 2( §3.1.2 Calibration of Apparatus).

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# 5.3.1.1.2 Leak Checks
5.3.1.2.2.1 Pitot Tubes Pitot tubes were leak checked according to procedures outlined in Method 2(§3. Procedure, §3.1). Prior to placement in the stack befoi
- e the start of the sampling program, the pitot tubes were subjected to a leak check. A length of tubing attached to the impact opening of a pitot was pressurized until a minimum pressure of 3" H 2 0 registered on the inclined 

# manometer. The tubing was then closed off and the manometer (evel reading observed. The reading had to remain stable for a period of 15 seconds to be accepted. The same procedure was used to check the static pressure side of the pitot by applying vacuum to the static

_ opening. After the end of the sampling program the pitot.tubes were removed from the stack, allowed to cool, and the
- same leak check procedure was conducted. '

,. r . .



# Page 17 

# AIR QUALITX TECHN{CAL SERUICES, INC. bo„f-tir,n \IPI'Rlflllt 1 1: 

### 7L1 r ip 

## f Rnpl 879-1800

# Ptoject: 021304 Vermont Brick Highgate, VT 

# 5.4 GAS COMPOSITION Carbon dioxide (CO 2 ) and oxygen (0 2 ) sample collection and analyses was performed according to procedures outlined in using EPA Test Method 3A - Determination of Oxygen and Carbon Dioxide Concentrations in Emissions from Stationary Sources (Instrumental Analyzer Procedure). During testing a continuous sample stream was withdrawn form a single point in the stack, conditioned to remove moisture, and conveyed to analyzers to measure the CO Zand O Z concentrations. The proportional electronic output of the analyzers was relayed to a data logging system for recording of the appropriate concentrations on a one minute basis over the course of each test period. The one minute readings were averaged to calcufate the average

_ concentrations for the test period. The balance of the gas composition will be considered N Z

. The results were used to determine the dry molecular weight of the exhaust stream.



# • '

Page 18 TECHNlCAL SERVICES Ifi1C. AIR

~ 

# UALITY ~ 

# ~ :.. I a nn,,,.od nnk„o Fccnr . li inrrtinn 

### 1/armnnt fl,ri45? 

## 18021 879-1800

## Project: 021304 Vermont Brick Highgate, VT 

# 5.5 

# lVIOiSTURE CONTENT The stack gas moisture content was performed according to procedures outlined in EPA Test Method 4- Determination of Moisture Content in Stack. The net weight gains determined from the initial and final impinger weights, in conjunction with the corrected metered sample volumes, were used to calculate the moisture content of the process exhaust stream.

Page 19



# A1R QUALITY TECHMICd1L SERVICES, IIVC. ` ` . - . . - r,_:..,, c-,.-v . Ii inrtinn 

### 1/armnnt 

## f15452 t8021 879-1800

# ~ ~ 

# r ~ ' '

# ►►► i 

# / 1
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# 1 1 1 1 1
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# 1
~ ~ ~

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# M APPENDiX A Equation Format



# ~ i

# METHOD 5 PARTIC U LATE EQUATIO N FO RMAT Volume of dry gas sampled at standard conditions, 68 °F, 29.92 "Hg - Vm s , d ( 

# scf):

Pb + 3 

# Vmstd = 17.65 (Vm) (Y) Tm + 460 

# Stack gas moisture condensed at standard conditions - Vwstd (scf): Vwstd = 0.04707 (Vlc) Decima) fraction stack gas proportion of water by volume - Bwo BWo = Vwsld



### Vw Si d + Vmstd 

# Stack gas dry molecular weight - MW d (Ib/lb-mole): MWd = 0.44 (%CO2) + 0.32 (%02) + 0.28 (°/vN2 + %CO) Stack gas molecular weight - MWs (Ib/Ib-mole): MWs = MWd (1 - Bwo) + 18 (Bwo) Pressure of stack - Ps (in. Hg): Ps = Pb + (Pst/13.6) Stack gas velocity at stack conditions - Vs (fps): Vs = 85.49 (Cp) ( FAP )av Ts + 

## 4so g (Ps) (MW S ) 

# Stack gas volumetric flow rate at standard conditions - Qs s (scfm):

QSs 

# = 60 (Vs) (As) ( Ts + 460 )( 29.92 } 

# Stack gas vo(umetric flow rate at actual conditions - Qsa (acfm): Qsa = 60 (Vs) (As) Stack gas. volumetric flow at dry standard conditions - Qsd(dscfm): QSd = ( 

# 60) (1 - BWO) (VS) (AS) { Ts + 460 } { 29.92 ) 

# (df"; inE`) 

# () -1.

# Concentration of particulate matter in stack gas, dry basis, standard conditions - Cs

(gr/dscf) Cs = 15.432 ( MP

# ~

vms

~ 

## a 

# Emission rate of particulate matter, dry basis, standard conditions - ER (lbslhr) ER = 0.00857 (Qsd) (Cs) Isokinetic variation - Iso (%) 17.33 (Ts + 460) [0.04707 (Vlc) + VmStd ] Iso = g (Vs) (Ps) (Dn 2 ) 

# Where: As = Cross section area of stack (ft2) Cp = Pitot tube coefficient Dn = Diameter of nozzle (in.) oH = Pressure differential across orifice (in. H20) Mp = Mass of particulate in grams Pb = Barometric pressure (in. Hg) Pst = Static pressure of stack (in. H20) Pstd = Standard pressure, 29.92 (in. H20) OP = Stack difFerential pressure (in. H20) Tm = Average temperature of dry gas meter (°F) Ts = Average stack temperature (OF) Tstd = Standard temperture, 68 (°F) Vlc = Volume of liquid condensate (ml) Vm = Volume of dry gas sample metered (ft 3 ) Y= Dry gas meter correction factor 8 = Sample duration (min.) 0.00857 = Conversion factor, gr to !bs and min. to hr. 0.04707 = Conversion factor, ml to ft 3 0.264 = ratio of 0 2 to N2 in air, v/v 15.432 = Conversion factor, g/ft 3 to gr/ft 3 17.65 = Conversion factor, standard temperature and pressure 17.33 = Isokinetic constant from factoring 18 = Molecuiar weight of water 85.49 = Pitot tube constant



# 0 00 ~

# APPENDIX B Summary Of Results

# VERMONT BR1CK HIGHGATE CENTER, VT PROJECT: 021304 BRICK KILN

FLUORIDE SAMPLE CONCENTRATION AND EMISSION DATA SUMMARY

SAMPLE. NET SAMPLE . SAMPLE EMISSION . VOLUMETRIC EMISSION 

## SAMPLE TEST ,: °_ MASS MASS VOLUME..' '.. CONCENTRATION . FLOW - RATE ID RUN (ug) (ug) (dscf) (dscfm) (Ibslhr) (ug/dsc0 (Ibsldscf) 

## C905 1 554.0 ; 554.00 ! 29.928 18.511 4.082E-008 5726 ' 0.014 I t C906 2 5030.0 5030.00 I 78.236 ~ 

## 64.293 1.418E-007 5498 0.047 ~ 

## C907 3 ; 35100.0 35100.00 I 91.555 383.376 8.453E-007 5516 0.280 : C908 C909 4 ! 10200.0 I

5 ; 732.0 ` 10200.00

732.00 j 108.269

31.204 94.21 .2.077E-007

23.459 ; 5.173E-008 ~ 

## 5780 7117 i 0.072 i

0.022 ! C910 BLANK i <105 AVERAGE I I I I i 5630 i

~►



### ~

~

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## I I I I

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## a' 1 I 

# ij'n'{~0"

# APPENDIX C Test Data Summary Sheets R

~~ 

# `:

# FIELD DATA TEST RESULTS

CLIENT: Vermont Brick FACILITY: Highgate Center, VT PROJECT: 021304 UNIT: Brick Kiln TEST DATE: October 1, 2002 TEST RUN: 1-1 

## TEST DATA SUMMARY INPUT VALUES Pitot Coefficient

- 

## Cp: 0.84 No2zle Diameter

- 

## Dn (in): 0.191 Dry Gas Meter Cal. (Y): 1.014 Stack Area (ftz): 4.746 Barometric Press.

- 

## Pb ("Hg): 29.74 Static Press.

- 

## Pst ("Hg): -0.18 Sample Duration (min.): 120 Volume of Gas Metered

- 

## Vm (ft'): 30.478 Volume of Water Condensed

- 

## Vlc (g.): 114.3 Oxygen

- 

## 0 2(%): 

## 9.8 Carbon Dioxide

- 

## CO 2(%): 

## 6.6 Carbon Monoxide

- 

## CO 

# (%): 0 Nitrogen

- 

## N z

# (%): 83.6 Average AP ("H 2 0): 0.24 Average aH ("H Z O): 0.19 Stack Temperature - Ts (°F): 274.5 Meter Temperature - Tm (°F): 81.8 Average 

## 4oP: 0.490 Mass of Particulate Callected - Mp -(g.):

11



## OUTPUT VALUES Dry Gas Volume (Standard) - Vmstd (dscf): Volume of Water (Standard) - Vwstd (scf): Stack Gas Water Proportion by Volume - Bwo: Molecular Weight of Dry Stack Gas - MWd (Ib/Ib-mole): Molecular Weight of Stack Gas - MWs (Ib/lb-mole): Pressure of Stack - Ps ("Hg.): Velocity of Stack Gas - Vs (fps): Dry Standard Volumetric Flow of Stack Gas - Qdscfm: Actual Volumetric Flow of Stack Gas - Qacfm: Test lsokinetic Sample Rate (%): 29.928 5.38 0.152 29.45 - 27.71 29.73 33.2 5726 9454 104

# FIELD DATA TEST RESULTS

CLIENT: Vermont Brick FACILITY: Highgate Center, VT PROJECT: 021304 

## UNIT: Brick Kiln TEST DATE: October 1-2, 2002 TEST RUN: 1-2 

# TEST DATA SUMMARY
INPUT VALUES Pitot Coefficient - Cp: 0.84 Average AP ("H Z O): 0.25 Nozzle Diameter - Dn (in): 0.191 Average oH ("H 2 0): 0.18 Dry Gas Meter Cal. (Y): 1.014 Stack Temperature - Ts (°F): 427.2 Stack Area (ftz): 4.746 Meter Temperature - Tm (°F): 97.2 Barometric Press. - Pb ("Hg): 29.74 Average 4oP: 0.500 

## ' Static Press. - Pst ("Hg): -0.18 Mass of Particulate Collected - Mp -(g.): Sample Duration (min.): 300 Volume of Gas Metered - Vm (ft'): 78.236 Volume of Water Condensed - Vic (g.): 215.4 Oxygen - 0 2

(%): 12.7 Carbon Dioxide - CO z(%}: 5.1 Carbon Monoxide - CO (%}: 0 Nitrogen - N 2

(%): 82.2

OUTPUT VALUES Dry Gas Volume (Standard) - Vmstd (dscf): 74.701 Volume of Water (Standard) - Vwstd (scf): 10.139 = Stack Gas Water Proportion by Volume - Bwo: 0.12 Molecular Weight of Dry Stack Gas - MWd (Ibllb-mole): 29.32 Molecular Weight of Stack Gas - MWs (Ib/Ib-mole): 27.96 Pressure of Stack - Ps ("Hg.): 29.73 Velocity of Stack Gas - Vs (fps): 37.1 Dry Standard Volumetric Flow of Stack Gas - Qdscfm: 5498 Actual Volumetric Flow of Stack Gas - Qacfm: 10565 Test Isokinetic Sample Rate (%): 108.1

~~~• ~~r=~'"

# FIELD DATA TEST RESULTS

CLIENT: Verrnont Brick FACILITY: Highgate Center, VT PROJECT: 021304 UNIT: Brick Kiln TEST DATE: October 2, 2002 TEST RUN: 1-3 

# TEST DATA SUMIVIARY INPUT VALUES Pitot Coefficient

- 

## Cp: 0.84 Noszle Diameter

- 

## Dn (in): 0.191 Dry Gas Meter Cal. (Y): 1.014 Stack Area (ft 2 ): 4.746 Barometric Press.

- 

## Pb ("Hg): 29.72 Static Press.

- 

## Pst ("Hg): -0.18 Sample Duration'(min.): 360 Volume of Gas Metered

- 

## Vm (ft'): 91.555 Volume of Water Condensed

- 

## Vlc (g.): 182.6 Oxygen

- 

## 0 2(%): 14.3 Carbon Dioxide

- 

## CO 2(%): 3.9 Carbon Monoxide

- 

## CO (°/a): 0 Nitrogen

- 

# N 2 (%): 81.8 Average AP ("H 2 0): 0.26 Average bH ("H 2 0): 0.2 Stack Temperature - Ts (°F): 513.9 Meter Temperature - Tm (°F): 94.5 Average 40P: 0.510 Mass of Particulate Collected - Mp -(g.):

OUTPUT VALUES Dry Gas Volume (Standard) - Vmstd (dscf): Volume of Water (Standard) - Vwstd (scf): Stack Gas Water Proportion by Volume - Bwo: Molecular Weight of Dry Stack Gas - MWd (Ib/lb-mole): Molecular Weight of Stack Gas - MWs (Ib/lb-mole): Pressure of Stack - Ps ("Hg.): Velocity of Stack Gas - Vs (fps): Dry Standard Volumetric Flow of Stack Gas - Qdscfm: Actual Volumetric Flow of Stack Gas - Qacfm: Test lsokinetic Sample Rate (%): 87.785 8.595 0.089 29.2 28.2 29.71 39.5 5516 11248 105.5

# FIELD DATA TEST RESULTS

CLIENT: Vermont Brick FACILITY: Highgate Center, VT PROJECT: 021304 UNIT: Brick Kiln TEST DATE: October 2-3, 2002 TEST RUN: 1-4 

# TEST DATA SUMMARY
INPUT VALUES Pitot Coefficient - Cp: 0.84 Nozzle Diameter - Dn (in): 0.191 Dry Gas Meter Cal. (Y): 1.014 Stack Area (ft 2 ): 4.746 Barometric Press. - Pb ("Hg): 29.7 Static Press. - Pst ("Hg): -0.18 Sample Duration (min.): ~ 

## ' 420 Volume of Gas Metered - Vm (ft'): 108.269 Volume of Water Condensed - Vlc (g.): 100.3 Oxygen - O Z (%): 15.2 Carbon Dioxide - CO 2(%): 3.4 Carbon Monoxide - CO (%): 0 Nitrogen - N 2(%): 81.4 Average OP ("H 2 0): 0.27 Average OH ("H Z O): 0.2 Stack Temperature - Ts (°F): 539.4 Meter Temperature - Tm (°F): 95 Average qaP: 0.520 Mass of Particulate Collected - Mp -(g.):

OUTPUT VALUES Dry Gas Volume (Standard) - Vmstd (dscf): Volume of Water (Standard) - Vwstd (scf): Stack Gas Water Proportion by Volume - Bwo: 

# Molecular Weight of Dry Stack Gas - MWd (lb/lb-mole): Molecular Weight of Stack Gas - MWs (Ib/Ib-mole): Pressure of Stack - Ps ("Hg.): Velocity of Stack Gas - Vs (fps): Dry Standard Volumetric Flow of Stack Gas - Qdscfm: Actual Volumetric Flow of Stack Gas - Qacfm: Test Isokinetic Sample Rate (%): 103.647 4.721 0.044 29.15 28.66 29.69 40.5 

# 5780 11533 101.9



## ~~? ~ 

# 0 '~

# FIELD DATA TEST RESULTS

CLIENT: Vermont Brick FACILITY: Highgate Center, VT PROJECT: 021304 UNIT: Brick Kilri TEST DATE: October 3, 2002 TEST RUN: 1 

## - 5 

## TEST DATA SUMfVIARY INPUT VALUES Pitot Coefficient - Cp: 0.84 Nozzle Diameter - Dn (in): 0.191 Dry Gas Meter Cal. (Y): 1.014 Stack Area (ft 2 ): 4.746 Barometric Press. - Pb ("Hg): 30.03 Static Press. - Pst ("Hg): -0.18 

# Sample Duration (min.): 120 Volume of Gas Metered - Vm (ft'): 31.204 Volume of Water Condensed - Vlc (g.): 4.8 Oxygen - O Z (%): 20.7 Carbon Dioxide - CO 2 (%): 0.1 Carbon Monoxide - CO (%}: 0 Nitrogen - N 2 (%): 79.2 Average oP ("H 2 0): 0.36 Average AH ("H 2 0): 0.2 Stack Temperature - Ts (°F): 491.4 Meter Temperature - Tm (°F): 88.3 Average dOP: 0.600 Mass of Particulate Callected - Mp -(g.):

OUTPUT VALUES Dry Gas Volume (Standard) - Vmstd (dscf): Volume of Water (Standard) - Vwstd (scf): 

# Stack Gas Water Proportion by Volume - Bwo: Molecular Weight of Dry Stack Gas - MWd (Ibllb-mole): 

# Malecular Weight of Stack Gas - MWs (Ib/lb-mole): Pressure of Stack - Ps ("Hg.): Velocity of Stack Gas - Vs (fps): Dry Standard Volumetric Flow of Stack Gas - Odscfm: Actual Volumetric Flow of Stack Gas - Gacfm: Test lsokinetic Sample Rate (%): 30.573 0.226 0.007 28.84 28.76 30.02 45.2 

# 7117 12871 85.5

- ~ 

# 43~?~`~~

# APPENDIX D -Computefized Field Test Data Sheets I'll

## ISOK{NETIC STACK CALCULATOR (Revised 11l08/01) INPUT PARAMETERS PITOT COEFFICIENT (Cp): 0.84 METER TEMPERATURE (°F): 90 STACK TEMPERATURE (°F): 325 AVERAGE DELTA P ("H20): 0.25 MAXIMUM DELTA P ("H20): 0.34 ESTIMATED MOISTURE (%): 14 METER BOX NUMBER: 1284-2964

DELTA H @: 1.846 NOZZLE DIAMETER (Dn) DATA CALCULATED DIAMETER (in.): 0.3292 SELECTED SIZE (in.): 0.191 CALCULATED PARAMETERS K FACTOR = 0.8062 ISOKINETIC DELTA H ("H20) = 0.2 MAX DELTA H ("H20) = 0.27 SAMPLING PARAMETERS MIMIMUM SA(1'PLE VOLUME REQUIRED (ds 31.8 SAMPLE TIME REQUI .P.ED (min): 60 AVERAGE SAMPLE RATE (cfm): 0.25 MAX SAMPLE RATE (cfm): 0.29
PROJECT NUMBER: 021304 TEST RUN NUMBER: 1-1



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# Vermont BrickCompany


# ~ Highgate Center, VT

# ► Project: 021304


# ~ Periodic Kiln Compliance Initial Ramp - Hour 1


# ~ Date Time CO2 {%) 42 {%} I 10/01/2002 17:57 6.74 9.62


# ~ 10/01 /2002 17:58 6.73 9.53 1010112002 17:59 6.57 9.88


# ~ 10/01/2002 18:00 6.21 10.68

# ► 10101/2002 18:01 6.09 10.77


# ~ 10/01 /2002 18:02 5.76 10.75 10/01l2002 18:03 6.01 10.77


# ~ 10/01 /2002 18:04 5.89 10.77


# ~ 10/0112002 18:05 5.82 10.78 ( 10/01 /2002 18:06 5.79 10.81 10/01/2002 18:07 - 5.58 10.81


# ~ 10l01/2002 18:08 5.81 10.86

, 10101 /2002 18:09 5.95 10.87

, 10/01/2002 18:10 5.95 10.91-1 10101 /2002 18:11 5.66 10.92


# ~ 10/01/2002 18:12 5.92 10.95


# ~ 10101 /2002 18:13 5.71 10.93

10/01 /2002 18:14 5.88 10.92 

# ~ 10/01 /2002 18:15 6.01 10.9


# ~ 10/01 l2002 18:16 5.89 10.89


# ~ 10/01 /2002 18:17 5.97 10.86

10/01/2002 18:18 5.9 10.8


# ~ 10/01/2002 18:19 5.95 10.8


# ~ 10/01/2002 18:20 6.06 10.76


# ~ 10/01 /2002 18:21 6.02 10.71

10/01 /2002 18:22 6.19 10.72 10/01 l2002 18:23 6.19 10.69


# ~ 10/01 l2002 18:24 5.85 10.64



# ~ _ _10/01/2002 18:25 6.11 10.62



# ~ 10101 l2002 18:26 6.03 10.57

10/01/2002 18:27 6.16 10.53 ` 

# ~ 10101 /2002 18:28 6.07 10.51 `


# ~ 10/01 /2002 18:29 5.99 10.47

10/01/2002 18:30 6.06 10.44 ` 10/01/2002 18:31 6.48 10.42 10/01 /2002 18:32 6.07 10.38 10/01 /2002 18:33 6.47 10.35 10/01 /2002 18:34 6.68 10.31 10/01/2002 18:35 6.12 10.3

. ,:. 10101 /2002 18:36 6.4 10.24

10/01/2002 18:37 6.38 10.24 10/01/2002 18:38 6.47 10.21 t.. _ a 10/01 /2002 18:39 6.34 10.25



# ~ . Oot 

# ~~~ ;; :

## 10/01 /2002 18:40 6.28 10.23

10/01 /2002 18:41 6.4 10.24 10/01 /2002 18:42 6.37 10.22 10/01/2002 18:43 6.47 10.19 10I01 /2002 18:44 6.02 10.14 10101 /2002 18:45 6.42 10.13 10/01/2002 18:46 6.42 10.09 10101 /2002 18:47 6.13 10.06 10l01 /2002 18:48 6.29 10.05 

# 10l01 /2002 18:49 6.64 10 10/01 /2002 18:50 6.38 9.99 10/01 /2002 18: 51 6.84 9.99 10/01/2002 18:52 6.56 9.98 10/01/2002 18:53 6.29 9.96 10/01 /2002 18:54 6.55 9.93 10/01 /2002 18:55 6.46 9.92 1010112002 18:56
_ 6.3 9.92 Houriy Average CO2 (%) 02 (%) 6.2 10.4

z



# o ~~~~~~

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# Init'sal Ramp - Hour 2

Date Time CO2 (%) 02 (%) 10101 /2002 19:57 7.05 9.22 10/01 /2002 19:58 6.89 9.24 10/01 /2002 19:59 7.06 9.25 10/01 /2002 20:00 7.45 9.26 10/01 /2002 20:01 6.91 9.25 10101 /2002 20:02 7.15 9.26 10/01/2002 20:03 7.12 9.26 10/01l2002 20:04 7.02 9.27 10/0112002 20:05 7.19 9.28 10/01/2002 20:06 7.09 9.29 10/01/2002 20:07 6.98 9.24 10/01 /2002 20:08 7.11 9.26 10I01 /2002 20:09 7.08 9.27 10/01 /2002 20:10 7.31 9.26 10/01/2002 20:11

_ 6.74 9.25 10/01 /2002 20:12 7.03 9.24 10/01 /2002 20:13 6.9 9.23 10/01/2002 20:14 6.95 ~ 9.25 10/01 /2002 20:15 7.06 9.23 10/0112002 20:16 7.19 9.24 10/01 /2002 20:17 6.93 9.25 10/01/2002 20:18 7.16 9.25 10101 /2002 20:19 7.2 9.23 10101/2002 20:20 7.02 9.22 10101/2002 20:21 6.87 9.24 10/01/2002 20:22 6.88 9.24 1010112002 20:23 7.21 9.24 10/01 /2002 20:24 7.06 9.22 10/01 /2002 20:25 7.12 9.24 10/01/2002 20:26 7.39 9.25 10101 /2002 20:27 7.27 9.23 10/01/2002 20:28 6.99 9.25 10/01/2002 20:29 6.82 9.25
- - 10/0112002 20:30 7.28 9.28 10/0112002 20:31 7.02 9.26 10101/2002 20:32 7.05 9.29 10/01 /2002 20:33 7.26 9.28 10/01 /2002 20:34 6.99 9.26 10/0112002 20:35 6.9 9.23 10101/2002 20:36 7.07 9.26 10/01 /2002 20:37 7.14 9.25 10l01 /2002 20:38 6.96 9.23 10/0112002 20:39 7.11 9.26 10/01/2002 20:40 7.19 9.27 10/0112002 20:41 6.98 9.24 10101/2002 20:42 7.19 9.25 10/01 /2002 20:43 7.04 9.26 

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10/0112002 20:45 7.29 9.25 10101 /2002 20:46 7.05 9.26 10/01/2002 20:47 7.28 9.25 10/01l2002 20:48 7.2 9.25 10/01/2002 20:49 6.99 9.25 10/01/2002 20:50 6.9 9.24 10101/2002 20:51 6.94 9.25 10101 /2002 20:52 7.15 9.24 10/01/2002 20:53 6.78 9.24 10101 /2002 20:54 7.18 9.26 10/01/2002 20:55 6.77 9.25 10/0112002 20:56 7.19 9.26 

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# Test Average 6.6 9.8

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## 1SOKiNETIC STACK CALCULATOR (Revised 11/08/01) INPUT PARAMETERS 

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## PlTOT COEFFICIENT (Cp): 0.84 METER TEMPERATURE (°F): 90 STACK TEMPERATURE (°F): 450 AVERAGE DELTA P ("H20): 0•25 MAXIMUM DELTA P ("H20): 0.34 ESTIMATED MOISTURE (%}: 12 METER BOX NUMBER: 1284-2964

DELTA H @: 1.846 NOZZLE DIAMETER (Dn) DATA CALCULATED DIAMETER (in.): 0.3384 SELECTED SIZE (in.): 0.191 CALCULATED PARAMETERS K FACTOR = 0.7224 ISOKINETIC DELTA H ("H20) = 0.18 MAX DELTA H ("H20) = 0.25 SAMPLING PARAMETERS MIMIMUM SAMPLE VOLUME REQUiRED (ds 31.8 SAMPLE TIME REQUIRED (min): 60 , AVERAGE SAMPLE RATE (cfm): 0.23 MAX SAMPLE RATE (cfm): 0.28
PROJECT NUMBER: 021304 TEST RUN NUMBER: 1-2

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# Vermont Brick Company

Highgste Center, VT Project: 021304 Periodic Kiln Compliance Initial Soak - Hour 1 Date Time CO2 (%) 02 (%) 10101/2002 23:10 5.59 11.33 10/01/2002 23:11 6.1 11.35 10/01 /2002 23:12 6.26 11.34 10/0112002 23:13 6.14 11.33 10/01/2002 23:14 5.9 11.38 10101/2002 23:15 5.7 11.38 10101 /2002 23:16 6.31 11.39 10101/2002 23:17 6.31 11.39 10/01/2002 23:18 6.2 11.42 1010112002 23:19 5.55 11.4 10/01/2002 23:20 - 5.78 11.41 10l0112002 23:21 5.89 11.41 10/01/2002 23:22 5.91 11.4 10/01/2002 23:23 6.1 11.43 10/01/2002 23:24 5.74 11.48 10101/2002 23:25 6.04 11.51 10/01/2002 23:26 5.81 11.51 10/01/2002 23:27 5.72 11.52 10/01/2002 23:28 5.65 11.51 10101/2002 23:29 5.85 11.51 10l01 /2002 23:30 5.89 11.55 10101/2002 23:31 5.45 11.52 10/01/2002 23:32 5.74 11.53 10101l2002 23:33 5.65 11.57 10/01/2002 23:34 5.79 11.57 10/01/2002 23:35 5.8 11.58 10/0112002 23:36 5.79 11.61 10101/2002 23:37 5.39 11.6 10/0112002 23:38 5.84 11.56 10/01/2002 23:39 5.47 11.55 10101/2002 23:40 5.82 11.57 10/01 /2002 23:41 5.65 11.57 10/01/2002 23:42 5.71 11.62 10/01 /2002 23:43 5.69 11.66 10/0112002 23:44 5.42 11.69 10/01 /2002 23:45 5.51 11.74 10/0112002 23:46 5.68 11.74 10/01/2002 23:47 5.76 11.74 10/01/2002 23:48 5.68 11.74 10/0112002 23:49 5.4 11.75 10101/2002 23:50 5.75 11.74 1010112002 23:51 5.62 11.75 10/01/2002 23:52 5.1 11.77 

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# 1010112002 23:53 5.79 11.67

10/01l2002 23:54 6.03 11.64 10/01/2002 23:55 5.72 11.62 10101/2002 23:56 5.74 11.59 10101/2002 23:57 5.84 11.61 10101l2002 23:58 5.68 11.6 1010112002 23:59 5.73 11.62 10102t2002 0:00 5.51 11.68 10/02/2002 0:01 5.62 11.68 1010212002 0:02 5.4 11.79 1010212002 0:03 5.64 11.8 10102l2002 0:04 5.42 11.88 10/0212002 0:05 5.77 11.87 10102/2002 0:06 5.22 11.89 1010212002 0,07 5.53 11.9 1010212002 0:08 5.45 11.91 10/02/2002 0:09

- 

# 5.62 11.9 

# Hourly Average c02 (%) 02 (%) 5.7 11.6

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# lnitial Soak - Hour 2

Date Time CO2 (%) 02 (%) 

# 10/02/2002 1:10 5.48 12.23 10/02/2002 1:11 5.48 12.21 10/02l2002 1:12 5.35 12.23 10/02/2002 1:13 5.5 12.2 10/02/2002 1:14 5.54 12.2 10/02/2002 1:15 5.59 12.22 10102l2002 1:16 5.34 12.27 10102/2002 1:17 5.5 12.31 10l02/2002 1:18 5.62 12.33 10/02/2002 1:19 5.13 12.36 10l0212002 1:20 5.3 12.32 10/02/2002 1:21 5.38 12.32 10l02/2002 1:22 5.44 12.3 10/02/2002 1:23 5.2 12.31 10102/2002 1:24 

# - 5.15 12.33 1010212002 1:25 5.28 12.33 10/02/2002 1:26 5.62 12.36 10/02/2002 1:27 5.25 12.39 10102I2002 1:28 5.13 12.38 10/02/2002 1:29 5.51 12.42 10/02/2002 1:30 5.01 12.37 10/0212002 1:31 5.5 12.37 10/02J2002 1:32 5.24 12.35 10/02/2002 1:33 5.49 12.35 10/02/2002 1:34 5.6 12.37 10l02/2002 1:35 5.21 12.46 10/02/2002 1:36 5.3 12.51 10l02/2002 1:37 5.06 12.51 1010212002 1:38 5.29 12.52 10/02/2002 1:39 5.38 12.52 10l02/2002 1:40 5.34 12.5 10102/2002 1:41 5.27 12.45



# _ 10/0212002 1:42 5.27 12.43 10l0212002 1:43 5.34 12.43 10/02/2002 1:44 5.09 12.42 10102/2002 1:45 5.15 12.47 10/02/2002 1:46 5.38 12.47 10/02/2002 1:47 5.56 12.31 10102I2002 1:48 5.49 12.26 10/02/2002 1:49 5.28 12.18 10102I2002 1:50 5.72 12.25 1010212002 1: 51 5.28 12.23 10/02/2002 1:52 5.32 12.21 1010212002 1:53 5.4 12.26 10102l2002 1:54 5.42 12.26 10/02/2002 1:55 5.41 12.3 10IO212002 1:56 5.21 12.25 

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## 10/02/2002 1:57 5.22 12.34 10/02/2002 1:58 5.49 12.37 1010212002 1:59 5.04 12.47 10102/2002 2:00 5.51 12.51 10/0212002 2:01 5.36 12.49 10IO212002 2:02 5.11 12.52 10/02/2002 2:03 4.96 12.52 10/02/2002 2:04 5.55 12.58 10/02/2002 2:05 5.41 12.55 10r0212002 2:06 5.17 12,51 10102/2002 2:07 5.04 12.49 10/02/2002 2:08 4.89 12.49 10/02/2002 2:09 5.11 12.54 Hourly Average c02 (%) 02 (%) 5.3 12.4



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# Initial Soak - Hour 3

Date Tirne CO2 (%) 02 (%) 10/02/2002 3:10 5.14 12.69 10/02/2002 3:11 5.16 12.67 10/02/2002 3:12 5.19 12.65 10/02/2002 3:13 4.88 12.64 10/0212002 3:14 5.33 12.64 10/02/2002 3:15 5.14 12.62 10/0212002 3:16 5.38 12.63 10/02/2002 3:17 5.35 12.63 10/02/2002 3:18 5.05 12.68 10/02/2002 3:19 4.85 12.7 10/02/2002 3:20 4.81 12.71 10/02/2002 3:21 5.7 12.68 10l0212002 3:22 5.24 12.71 10/02/2002 3:23 5.43 12.73 10/02/2002 3:24 - 5.29 12.72 10/02/2002 3:25 5.14 12.72 10/02/2002 3:26 5.09 12.7 10/02/2002 3:27 5.26 12.71 10/02/2002 3:28 5.12 12.71 10/02/2002 3:29 5.01 12.76 10/02/2002 3:30 5.28 12.76 10102/2002 3:31 4.86 12.82 10/02/2002 3:32 5.27 12.76 10/02/2002 3:33 5.07 12.72 10/02/2002 3:34 5.19 12.72 10102/2002 3:35 5.08 12.7 10102/2002 3:36 5.29 12.73 1010212002 3:37 5.16 12.71 10/02/2002 3:38 4.9 12.75 10/02/2002 3:39 5.09 12.78 10/0212002 3:40 5.13 12.77 10/02/2002 3:41 5.12 12.75 10/02/2002 3:42 5.01 12.76 10/02/2002 3:43 5 12.77 10/02/2002 3:44 4.94 12.82 10/02/2002 3:45 4.88 12.79 10/02/2002 3:46 5.17 12.78 10/02/2002 3:47 4.96 12.77 10/02/2002 3:48 5.25 12.64 10/02/2002 3:49 5.11 12.61 10102/2002 3:50 5.05 12.54 10/02/2002 3:51 5.11 12.55 10/0212002 3:52 5.27 12.48 10/02/2002 3:53 5.05 12.46 10/02/2002 3:54 5.16 12.47 10/02/2002 3:55 5.34 12.5 10102/2002 3:56 5.52 12.53

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# 10l0212002 3:57 5.36 12.53

10/02/2002 3:58 5.34 12.58 10/02/2002 3:59 5.33 12.59 10IO2/2002 4:00 5.33 12.68 10/02/2002 4:01 5.16 12.7 10102/2002 4:02 5.15 12.71 10/02/2002 4:03 5.3 12.76 10102/2002 4:04 5.18 12.76 10/02/2002 4:05 5.17 12.74 10IO2/2002 4:06 5.17 12.71 10102/2002 4:07 5.25 12.7 10/02/2002 4:08 4.83 12.66 10102l2002 4:09 5.17 12.68 Hourly Average CO2 (%) 02 (%) 5.2 12.7

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# 000023

# Initial Soak - Hour 4

Date Time CO2 (%) 02 (%) 

# 10/0212002 5:10 5.07 12.9 10102/2002 5:11 4.81 12.91 10/02/2002 5:12 4.76 12.85 10/02/2002 5:13 5.11 12.88 10/0212002 5:14 4.88 12.85 10/02/2002 5:15 5.1 12.88 10/02l2002 5:16 4.73 12.86 

# 10/02/2002 5:17 5.02 12.86 10/02/2002 5:18 4.95 12.87 10/02/2002 5:19 5.01 12.84 10/02/2002 5:20 5 12.88 10/02/2002 5:21 4.57 12.89 10l0212002 5:22 4.95 12.9 10/02/2002 5:23 4.72 12.94 10/02/2002 5:24

- 

# 5.02 12.92 10/02/2002 5:25 5.06 12.92 10/02/2002 5:26 5.18 12.94 10/0212002 5:27 4.52 12.94 10102/2002 5:28 4.94 12.91 10/02/2002 5:29 4.94 12.95 10102/2002 5:30 4.71 12.95 10/02/2002 5:31 5.22 13.01 10/02/2002 5:32 4.81 13.02 10/02/2002 5:33 5.12 13.05 10/02/2002 5:34 4.75 13.01 10/0212002 5:35 5.01 12.99 10/02/2002 5:36 5 13.02 10/02/2002 5:37 11 

# 4.99 13.01 10/02/2002 5:38 5 13.03 10/02/2002 5:39 5.01 13.02 10/02/2002 5:40 4.98 13.03 10/02/2002 5:41 5.03 12.99 10/02/2002 5:42 4.89 13.02 10/02/2002 5:43 5.17 13.05 10/02/2002 5:44 4.77 13.03 1010212002 5:45 4.75 13.06 10102/2002 5:46 4.93 12.97 10/02/2002 5:47 4.77 12.92 10/02/2002 5:48 5.03 12.9 1010212002 5:49 5.03 12.86 10/02/2002 5:50 5.07 12.83 10/02/2002 5:51 4.9 12.76 10/02/2002 5:52 5.15 12.77 10/0212002 5:53 5.27 12.77 10/02/2002 5:54 4.87 12.75 10/02/2002 5:55 4.85 12.86 10/02/2002 5:56 4.73 13.05

## 10/0212002 5:57 4.81 13.09

10/0212002 5:58 4.6 13.12 10/0212002 5:59 4.63 13.21 10/0212002 6:00 4.84 13.21 10/0212002 6:01 4.88 13.2 10/02/2002 6:02 4.95 13.21 10/02I2002 6:03 5.36 13.21 10/0212002 6:04 4.2 13.17 

## 10102/2002 6:05 4.74 13.18 10102/2002 6:06 4.57 13.18 10/02/2002 6:07 5.12 13.15 10/02/2002 6:08 5.26 13.18 10/02/2002 6:09 4.55 13.14 Hourly Average CO2 (%) 02 (%) 4.9 13.0

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## Initial Soak - Hour 5

Date Time CO2 (%} 02 (%) 10/02/2002 7:10 3.72 13.81 10102/2002 7:11 4.31 13.82 10/02/2002 7:12 4.54 13.81 10/02/2002 7:13 4.37 13.79 10/02/2002 7:14 4.37 13.76 10/02/2002 7:15 4.41 13.77 10102/2002 7:16 4.8 13.76 10/02/2002 7:17 4.36 13.79 10102/2002 7:18 4.59 13.83 10102/2002 7:19 4.72 13.84 10/02/2002 7:20 4.06 13.84 10/02/2002 7:21 4.43 13.84 10/02J2002 7:22 4.43 13.83 10/02l2002 7:23 4.46 13.85 10102/2002 7:24 - 4.15 13.86 10102/2002 7:25 4.22 13.85 10/02/2002 7:26 4.16 13.84 10/02/2002 7:27 4.27 13.88 10/02/2002 7:28 4.47 13.87 10/02/2002 7:29 4.43 13.89 10/02/2002 7:30 4.11 13.87 1010212002 7:31 4.4 13.89 10/02/2002 7:32 4.19 13.89 10/0212002 7:33 4.07 13.92 10102/2002 7:34 4.47 13.93 10/02/2002 7:35 4.18 13.91 10/02/2002 7:36 3.96 13.94 10/02/2002 7:37 4.08 13.9 10/02/2002 7:38 4.36 13.86 10l02/2002 7:39 3.99 13.88 10/02/2002 7:40 4.2 13.92 10/02/2002 7:41 4.38 13.9 10102/2002 7:42 4.02 13.91 + 10/02/2002 7:43 4.24 13.9 10/02/2002 7:44 4.24 13.91 10/02/2002 7:45 4.16 13.9 10/02/2002 7:46 4.18 13.91 10/02/2002 7:47 3.94 13.89 10l02/2002 7:48 4.18 13.88 10/02/2002 7:49 4.26 13.91 10/0212002 7:50 3.8 13.91 10/02/2002 7:51 3.86 13.94 

# 10/0212002 7:52 4.19 13.91 10/02/2002 7:53 4.48 13.92 10/02/2002 7:54 4.45 13.92 10102/2002 7:55 4.3 13.93 10/0212002 7:56 4.24 13.91

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10/02l2002 7:58 10102/2002 7:59 10/02/2002 8:00 10r02/2002 8:01 10102/2002 8:02 10/0212002 8:03 10/02l2002 8:04 10t0212002 8:05 10102/2002 8:06 1 0102/2002 8:07 

# 10/02/2002 8:08 10/02/2002 8:09 4.59 13.9 4.5 13.92 4.4 13.94 4.09 13.94 4.14 13.94 4.25 13.92 4.4 13.94 4 13.95 4 13.97 4.25 13.99 4.4 14 4.36 13.98 4.03 13.94

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# Hourly Average CO2 (%) 02 (%) 4.3 13.9 Test Average 5.1 12.7

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~- ISOKINETIC STACK CALCULATOR (Revised 11108101) INPUT PARAMETERS PITOT COEFFICIENT (Cp): 0.84 METER TEMPERATURE (°F): 90 STACK TEMPERATURE (°F): 450 AVERAGE DELTA P ("H20): . 0.25 MAXIMUM DELTA P ("H20): 0.34 ESTIMATED MOISTURE (%): 8 METER BOX NUMBER: 1284-2964

DELTA H @: 1.846 NOZZLE DIAMETER (Dn) DATA CALCULATED DIAMETER (in.): 0.3322 SELECTED SIZE (in.): 0.191 CALCULATED PARAMETERS K FACTOR = 0.7772 ISOKINETIC DELTA H ("H20) = 0.19 MAX DELTA H ("H20) = 0.26 SAMPLING PARAMETERS MIMIMUM SAMPLE VOLUME REQUIRED (ds 31.8i SAMPLE TIME REQUIRED (min): 60 AVERAGE SAMPLE RATE (cfm): 0.24 MAK SAMPLE RATE (cfm): 0.28
PROJECT NUMBER: 021304 TEST RUN NUMBER: 1-3CR co "t Co ,r to w 0, csi C~ LL. IN u- C-4 co

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- 

# Hour 1 Date Time CO2 (%) 02 (%) 10/02/2002 10:30 4.3 13.68 10102/2002 10: 31 4.35 13.58 10102/2002 10:32 4.11 13.58 10/0212002 10:33 4.4 13.51 1010212002 10:34 4.16 13.51 10102/2002 10:35 4.46 13.52 10102/2002 *10:36 4.6 13.45 10/02/2002 10:37 4.78 13.39 1010212002 10:38 4.42 13.42 1010212002 10:39 4.67 13.38 10/0212002 10:40 4.2 13.39 10/0212002 10:41 r 4.5 13.37 10l02/2002 10:42 4.58 13.39 10/0212002 1 0:43 4.18 13.42 10/0212002 10:44 4.34 13.43 10102/2002 10:45 4.64 13.4 10/02/2002 10:46 4.3 13.45 10/0212002 10:47 4.52 13.47 10/02/2002 10:48 4.23 13.53 1010212002 10:49 3.96 13.57 10102/2002 10:50 4.35 13.59 1010 2/2002 10: 51 4.28 13.61 10102l2002 10:52 4.49 13.64 10/0212002 10:53 4.15 13.7 10/0212002 10:54 4.3 13.75 1010212002 10:55 3.79 13.76 10/02/2002 10:56 4.11 13.77 10/02/2002 10:57 4.18 13.8 10102/2002 10:58 4.03 13.83 10/02/2002 10:59 4.07 13.81 -10/02l2002 11:00 4.03 13.81 10/02/2002 1 'f :01 4.23 13.84 10102/2002 11:02 4.26 13.85 10102/2002 11:03 3.78 13.9 10/0212002 11:04 4.07 13.86 10/02/2002 11:05 4.12 13.88 1010212002 11:06 4.26 13.95 10102/2002 11:07 3.83 13.95 10l0212002 11:08 4.04 13.94 10/0212002 11:09 4.11 13.92 1010212002 11:10 4.55 13.92 1010212002 11:11 4.05 13.95 1010212002 11:12 3.84 13.95 10/02/2002 11:13 4.09 13.94 10102l2002 11:14 4.11 13.93 10102/2002 11:15 4.09 13.96 

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Date Time CO2 (%) 02 (%) 10/02/2002 12:30 4.35 14.18 10/0212002 12:31 3.93 14.18 10/02/2002 12:32 3.75 14.22 10/02/2002 12:33 3.88 14.19 10l02/2002 12:34 4.01 14.15 10/02/2002 12:35 3.88 14.15 10/02/2002 12:36 4.14 14.1 10/02/2002 12:37 3.94 14.05 10/0212002 12:38 3.69 13.99 10/02/2002 12:39 4.49 14.02 10/02/2002 12:40 3.46 13.96 10/02/2002 12:41 3.99 13.96 10/02/2002 12:42 4.06 13.97 10/02/2002 12:43 4.2 13.97 10/0212002 12:44 3.97
_ 13.97 10/02/2002 12:45 4.07 14 10/02/2002 12:46 3.97 14 10/02/2002 12:47 3.96 13.99 10/02/2002 12:48 4.36 14.02 10/02/2002 12:49 4 14 10/02/2002 12:50 4.12 14.05 10l02/2002 12: 51 3.84 14.03 10/02/2002 12:52 4.01 14.05 10/0212002 12:53 4.26 14.06 10/02l2002 12:54 4.11 14.06 10/02/2002 12:55 3.95 14.07 10/02/2002 12:56 3.98 14.07 10/02/2002 12:57 4.17 14.11 10/02/2002 12:58 4.49 14.12 10102/2002 12:59 3.75 14.12 10102/2002 13:00 3.93 14.11 10/02/2002 13 : 01 3.66 14.1 10/02/2002 13:02 3.91 14.14 10/0212002 13:03 3.96 14.19
- - 10/02/2002 13:04 4.09 14.2 10/02/2002 13:05 3.6 14.2 10/02/2002 13:06 3.96 14.19 10/02l2002 13:07 3.96 14.18 10/02/2002 13:08 4.02 14.18 10/0212002 13:09 3.86 14.21 10/0212002 13:10 3.82 14.21 10/02/2002 13:11 4.18 14.19 10/02/2002 13:12 4.25 14.21 10/02/2002 13:13 4.03 14.22 10/02/2002 13:14 3.97 14.22 10102/2002 13:15 3.95 14.2 10/02/2002 13:16 3.72 14.23 10/02/2002 13:17 3.66 14.24 10/02/2002 13:18 3.92 14.25 10/02/2002 13:19 3.52 14.24 

# r) 0 () 0341

## 1010212002 13:20 3.76 14.28

1010 212002 13 : 

## 21 3.62 14.27 10102/2002 13:22 3.79 14.27 10/02/2002 13:23 3.99 14.27 10/02/2002 13:24 3.83 14.27 10/02/2002 13:25 3.55 14.28 10/02/2002 13:26 3.53 14.34 10/02/2002 13:27 3.87 14.36 1010212002 13:28 3.73 14.4 10/02/2002 13:29 4,04 14.37 Hourly Average CO2 (°la) 02 {%a} 3.9 14,1



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~ 1 st half of Carbon Burnout Soak - Hour 3

Date Time CO2 (%) 02 (%) 10/02/2002 14:30 3.85 14.19 10/02/2002 14: 31 3.93 14.22 10/02/2002 14:32 3.88 14.19 10/0212002 14:33 3.76 14.25 10/02/2002 14:34 4.1 14.2 10102/2002 14:35 3.78 14.19 10/02/2002 1 4:36 3.74 14.18 1010212002 14:37 3.77 14.2 .10102/2002 14:38 4.12 14.2 10/02/2002 14:39 4.54 14.19 10/02/2002 14:40 3.92 14.15 1010212002 14:41 4.02 14.19 1010212002 14:42 3.87 14.18 10102/2002 14:43 3.59 14.16 10102/2002 14:44

_ 3.82 14.18 10102/2002 14:45 4.11 14.17 10102/2002 14:46 3.96 14.18 1010212002 14:47 3.88 14.18 10102/2002 14:48 3.98 14.19 10102/2002 14:49 3.75 14.2 10102/2002 14:50 3.85 14.25 10102/2002 14: 51 4.09 14.24 9 010212002 14:52 3.95 14.26 10102/2002 14:53 4.21 14.25 10102/2002 14:54 3.84 14.27 10/02/2002 14:55 3.74 14.28 10/02/2002 14:56 3.91 14.25 10/02/2002 14:57 4.11 14.27 10/0212002 14:58 3.79 14.25 10102/2002 14:59 3.74 14.26 10/0212002 15:00 3.93 14.24 10/02/2002 15: 01 3.94 14.23 10/0212002 15:02 3.75 14.26 10/0212002 15:03 4.08 14.27

- 

# 10/02/2002 15:04 3.95 14.26 10102/2002 15:05 3.95 14.25 10/02/2002 15:06 3.99 14.3 10/0212002 15:07 3.88 14.33 10/0212002 15:08 3.78 14.33 10/0212002 15:09 3.6 14.33 10/0212002 15:10 3.65 14.32 10/0212002 15:11 3.75 14.36 10/0212002 15:12 3.7 14.33 10/02/2002 15:13 3.89 14.35 10102/2002 15:14 3.72 14.36 10102/2002 15:15 4.17 14.34 10/0212002 15:1 fi 4.01 14.33 1010212002 15:17 4.02 14.33 10102/2002 15:18 3.84 14.35 10102/2002 15:19 4.01 14.34 

# ()0 iq=) 3 6i
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## 10/0212002 15:20 3.95 14.34

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## 10l0212002 1 5:21 4.01 14.34

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## 1010212002 15:22 3.9 14.37

1010212002 15:23 3.76 14.38 ' 10102/2002 15:24 3.97 14.4 1010212002 15:25 3.68 14.39 10102I2002 15:26 3.7 14.37 10102/2002 15:27 3.78 14.38 Hourly Average 10/0212002 15:28 4.18 14.34 CO2 (%) 02 (%) 10/02/2002 15:29 3.71 14.37 3.9 14.3

~



# - 000 0-3

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# 7

# 1 st half of Carbon Burnout Soak - Hour 4

Date Time CO2 (%) 02 (%) 10102/2002 16:30 3.87 14.59 10/02/2002 16 :31 3.69 14.57 10/0212002 1 fi:32 3.73 14.57 10/0212002 16:33 3.91 14.54 10102I2002 16:34 3.71 14.39 10102/2002 16:35 4.07 14.22 10102/2002 16:36 4.01 14.26 10l0212002 16:37 3.8 14.25 10/0212002 16:38 3.91 14.31 10/02/2002 16:39 4.02 14.33 10102/2002 16:40 4.12 14.34 10102/2002 16:41 3.9 14.33 10/02/2002 16:42 3.94 14.34 10l0212002 16:43 4.01 14.33 10/0212002 16:44 3.72

_ 14.35 10102/2002 16:45 3.65 14.36 10/02/2002 16:46 3.91 14.37 10102l2002 16:47 3.8 14.36 10102/2002 16:48 3.8 14.35 10/0212002 16:49 3.63 14.36 10/0212002 16:50 3.58 14.35 10/0212002 16: 51 3.72 14.36 10/02/2002 16:52 3.88 14.39 10102/2002 16:53 3.81 14.43 10102/2002 16:54 3.77 14.44 10102/2002 16:55 3.81 14.46 10102/2002 1 fi:56 3.78 14.44 1010212002 16:57 3.99 14.47 1010212002 16:58 3.93 14.49 10102/2002
- ' 16:59 3.76 14.46 10102/2002 17:00 3.67 14.5 10102/2002 17:01 3.79 14.49 10102/2002 17:02 3.83 14.48 10/0212002 17:03 3.54 14.47

_ _ 10/0212002 17:04 3.66 14.48 10102/2002 17:05 3.74 14.5 10102l2002 17:06 3.89 14.52 10/0212002 17:07 3.77 14.5 10/0212002 17:08 3.93 14.51 10l02/2002 17:09 3.59 14.52 10/02/2002 17:10 3.59 14.51 10/0212002 17 :11 3.82 14.49 10702/2002 17:12 3.93 14.52 10/0212002 17:13 3.89 14.49 10/0212002 17:14 3.56 14.49 10/0212002 17:15 3.76 14.49 10/0212002 17:1 fi 3.79 14.49 10102/2002 17:17 3.8 14.49 10102/2002 17:18 3.74 14.49 10l02/2002 17:19 3.89 14.49



# - ~~ 

# 00038

## 10l0212002 17:20 3.55 14.48

10102/2002 17 :21 4.03 14.49 10102/2002 17:22 3.64 14.5 1010212002 17:23 3.48 14.5 10/0212002 17:24 4 14.5 10/0212002 17:25 3.58 14.54 10/0212002 17:26 3.76 14.56 10/0212002 17:27 3.95 14.57 10/02/2002 17:28 3.55 14.59 10102/2002 17:29 3.93 14.55 Hourly Average CO2 (%) 02 (%) 3.8 14.5

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## 1 st half of Carbon Burnout Soak - Hour 5

Date Time CO2 (%) 02 (%) 10/02/2002 18:30 3.9 14.35 10/02/2002 18: 31 3.66 14.37 10102l2002 18:32 4.02 14.34 10/0212002 18:33 3.94 14.33 10/0212002 18:34 3.93 14.31 10l02/2002 18:35 3.8 14.33 10/02/2002 18:36 3.86 14.35 10/02/2002 18:37 3.52 14.41 10/02/2002 18:38 3.54 14.47 10IO212002 18:39 3.65 14.49 10l0212002 18:40 3.88 14.47 10/0212002 18:41 3.73 14.54 1010212002 18:42 3.48 14.61 10102/2002 18:43 3.65 14.6 10102I2002 18:44 3.92 14.63 10/02I2002 18:45 + 

## 3.26 14.59 10/0212002 18:46 3.94 14.6 10/0212002 18:47 3.67 14.6 10l0212002 18:48 3.88 14.59 10102l2002 18:49 3.87 14.57 10102l2002 18:50 3.52 14.57 10l0212002 18: 51 4.02 14.55 10l0212002 18:52 3.95 14.55 1010212002 18:53 3.54 14.51 10/02/2002 18:54 3.82 14.52 10/02/2002 18:55 3.79 14.54 10IO2/2002 18:56 3.85 14.52 10/02/2002 18:57 4.09 14.5 10/0212002 18:58 3.62 14.5 10102l2002 18:59 3.74 14.48 10/02/2002 19:00 3.7 14.48 1-0102/2002 19:01 3.59 14.48 1010212002 19:02 3.78 14.47 1010212002 19:03 3.84 14.49 10/02/2002 19:04 3.9 14.46 10J02l2002 19:05 3.81 14.46 10/02/2002 19:06 4.09 14.45 10l0212002 19:07 3.93 14.43 10102l2002 19:08 3.59 14.44 10102l2002 19:09 3.66 14.44 10102/2002 19:10 3.83 14.45 10/02/2002 19:11 3.91 14.44 10/0212002 19:12 4.02 14.44 10/02/2002 19:13 3.73 14.46 10102/2002 19:14 4.03 14.46 10/0212002 19:15 3.62 14.44 10i/0212002 19:16 3.78 14.47 10102/2002 19:17 4.27 14.46 10102/2002 19:18 3.63 14.47 10102/2002 19:19 3.6 14.46

I 11 

# 0i'0-16s0

# 10l02/2002 19:20 3.78 14.49

1 0/02/2002 19:21 3.77 14.47 10l0212002 19:22 3.76 14.49 10102l2002 19:23 3.72 14.5 10l02/2002 19:24 3.79 14.48 1010212002 19:25 3.61 14.51 10/0212002 19:26 3.7 14.52 10/4212002 19:27 3.82 14.51 10IO212002 1 9:28 3.58 14.51 10IO212002 19:29 3,71 14.54 Hourly Average CO2 (%) 02 (%) 3.8 14.5

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~ ~ 1 st half of Carbon Burnout Soak - Hour 6

Date Time CO2 (%) 02 (%) 10/0212002 20:30 3.92 14.44 10l02/2002 20:31 4.26 14.44 10/0212002 20:32 3.88 14.47 10/0212002 20:33 3.84 14.43 10/02/2002 20:34 3.79 14.46 1010212002 20:35 3.87 14.44 10/02/2002 20:36 3.64 14.45 1010212002 20:37 3.77 14.46 10102/2002 20:38 3.84 14.47 10/02/2002 20:39 3.73 14.46 1010212002 20:40 3.46 14.47 10/0212002 20:41 3.1 14.47 10/0212002 20:42 4.01 14.47 10/0212002 20:43 3.86 14.46 10/0212002 20:44

_ 3.58 14.48 10/02/2002 20:45 3.94 14.49 10l0212002 20:46 3.73 14.53 10102/2002 20:47 4.07 14.51 10/02/2002 20:48 3.39 14.51 1010212002 20:49 3.94 14.51 10/02/2002 20:50 3.6 14.54 10102/2002 20:51 3.77 14.52 10/0212002 20:52 3.67 14.53 10102/2002 20:53 3.77 14.53 10/02l2002 20:54 3.82 14.54 1010212002 20:55 3.71 14.56 10102/2002 20:56 3.94 14.55 10/02/2002 20:57 3.87. 14.56 10/0212002 20:58 3.69 14.58 10/02/2002 20:59 3.57 14.58 10/02J2002 21:00 4.15 14.6 10102/2002 21:01 3.81 14.57 10/02/2002 21:02 3.62 14.63 1010212002 21:03 3.65 14.63 10/02/2002 21:04 3.67 14.65 10/02/2002 21:05 3.91 14.66 1010212002 21:06 3.41 14.66 10/02/2002 21:07 3.85 14.65 10/02/2002 .21:08 3.69 14.68 10102/2002 21:09 3.57 14.65 10102l2002 21:10 3.77 14.7 10/02/2002 21:11 3.65 14.7 10/02/2002 21:12 3.65 14.71 10102/2002 21:13 3.57 14.71 10/02/2002 21:14 3.47 14.72 1-010212002 21:15 3.39 14.72 10/02l2002 21:16 3.71 14.75 10/02/2002 21:17 3.44 14.73 10/02/2002 21:18 3.46 14.74 10102l2002 21:19 3.53 14.74 

# 000 0 4 2

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~ 10/02/2002 21:20 3.67 14.73

10/02/2002 21:21 3.7 14.73 1010212002 21:22 3.89 14.75 10/02/2002 21:23 3.59 14.79 10/02/2002 21:24 3.87 14.79 10/02J2002 21:25 3.67 14.78 10l02/2002 21:26 3.6 14.77 10/02/2002 21:27 3.71 14.77 10/02/2002 21:28 3.45 14.77 10/02/2002 21:29 3.72 14.78 Hourly Average CO2 (%) 02 (%) 

## 3.7 14.6 Test Average CO2 (%) 02 (°IO) 3.9 14.3



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# - () 0 -fl0- 4 3

## ISOKINETIC STACK CALCULATOR (Revised 11108I01) INPUT PARAMETERS PITOT COEFFICIENT (Cp): 0.84 . • METER TEMPERATURE (°F): 90 STACK TEMPERATURE (°F): 500 AVERAGE DELTA P ("H20): 0.24 MAXlMUM DELTA P ("H20): 0.34 ESTIMATED MOISTURE (%): 6 METER BOX NUMBER: 1284-2964

DELTA H @: 1.846 NOZZLE DIAMETER (Dn) DATA CALCULATED DIAMETER (in.): 0.3372 SELECTED SIZE (in.): 0.191 CALCULATED PARAMETERS - K FACTO R = 0.7631 ISOKINETlC DELTA H ("H20) = 0.18 MAX DELTA H ("H20) = 0.26 SAMPLING PARAMETERS

~ 

## MIMIMUM SAMPLE VOLUME REQUIRED (ds 31.8

SAMPLE TIME REQUIRED (min): 60 AVERAGE SAMPLE RATE (cfm): 0.23 MAX SAMPLE RATE (cfm): 0.28
PROJECT NUMBER: 021304 TEST RUN NUMBER: 1-4



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# ~ Vermont BrickCompany 

# ~ Highgate Center, VT Project: 021304 

# ~ Periodic Kiln Compliance 

# ~ 2nd Half of Carbon Burnout Soak - Hour 1

Date Time CO2 (%) 02 (%) 

# ~ 10/02/2002 22:30 3.78 14.81 

# ~ 10l02/2002 22:31 3.83 14.76



# ~ 10/02l2002 22:32 3.85 14.61 1 fl102/2002 22:33 3.9 14.62 

# ~ 10/0212002 22:34 3.86 14.66 

# ~ 10J0212002 22:35 3.91 14.68 10/0212002 22:36 3.41 14.73 

# ~ 10J0212002 22:37 3.49 14.74 

# ~ 10102/2002 22:38 3.63 14.7 10/02/2002 22:39 3.64 14.74 

# ~ 10J02/2002 22:40

_ 3.51 14.72 

# ~ 10/02/2002 22:41 3.54 14.75 10J02/2002 22:42 3.36 14.72 

# ~ 10/02/2002 22:43 3.74 14.71 

# ~ 10/02/2002 22:44 3.78 14.71 

# ~ 10102/2002 22:45 3.64 14.71 10/02/2002 22:46 3.79 14.71 

# ~ 10J02/2002 22:47 3.49 14.72 

# ~ 10102/2002 22:48 3.55 14.69 10/02/2002 22:49 3.43 14.7 

# ~ 10/02/2002 22:50 3.58 14.72 b 10/02l2002 22:51 3.64 14.71 1010212002 22:52 3.85 14.72 

# ~ 10J02/2002 22:53 3.46 14.71 

# ~ 10/02/2002 22:54 3.78 14.71 

# ~ 10/02/2002 22:55 3.42 14.73 10/02/2002 22:56 3.23 14.74 

# ~ 10102/2002 22:57 3.69 14.72 

# ~ 10/02/2002 22:58 3.55 14.74 10/02/2002 22:59 3.24 14.71 

# ~ - -10/02/2002 23:00 3.55 14.73 ! 10J02/2002 23:01 3.6 14.74 10J02/2002 23:02 3.7 14.72 

# ~ 10102/2002 23:03 3.62 14.71 

# ~ 10/02/2002 23:04 3.54 14.73 

# ~ 10l0212002 23:05 3.81 14.73 10J0212002 23:06 3.69 14.7 

# ~ 10/02/2002 23:07 3.86 14.73 

# ~ 10/0212002 23:08 3.84 14.72 10/02/2002 23:09 3.7 14.74 

# ~ 10J02/2002 23:10 3.51 14.76 b 10/02/2002 23:11 3.55 14.73 10/0212002 23:12 3.3 14.72 4 10/02/2002 23:13 3.91 14.75 

# ~ 10/0212002 23:14 3.62 14.73

, 10/02/2002 23:15 3.44 14.73

# 10/02/2002 23:16 3.41 14.73

10/02/2002 23:17 3.57 14.75 10/02/2002 23:18 3.27 14.74 10/02/2002 23:19 3.36 14.72 1 0/02/2002 23:20 3.78 14.75 10/02/2002 23:21 3.28 14.73 10/02/2002 23:22 3.38 14.72 10/02/2002 23:23 3.82 14.72 10/0212002 23:24 3.84 14.74 10/02/2002 23:25 3.39 14.76 10/02/2002 23:26 3.74 14.77 10/02/2002 23:27 3.6 14.75 10/02/2002 23:28 3.39 14.76 10/02/2002 23:29 4 14.77 

# Hourly Average CO2 (%) 02 (%) 3.6 14.7



# ~~~~~~

# 2nd Half of Carbon Burnout Soak - Hour 2

Date Time CO2 (%) 02 (%) 10/0312002 0:30 3.5 14.91 1010312002 0:31 4.01 14.89 10/0312002 0:32 3.54 14.89 10/03/2002 0:33 3.29 14.89 10/03/2002 0:34 3.28 14.9 10/03/2002 0:35 3.65 14.9 10/0312002 0:36 3.75 14.9 10l03I2002 0:37 3.56 14.94 10/03/2002 0:38 3.36 14.91 10l0312002 0:39 3.65 14.92 10/03I2002 0:40 3.52 14.87 10103/2002 0:41 3.53 14.88 10/0312002 0:42 3.54 14.89 10/03/2002 0:43 3.73 14.88 10/0312002 0:44 3.6



# _ 14.88 10103l2002 0:45 3.51 14.88 10/0312002 0:46 3.66 14.91 10/03/2002 0:47 3.17 14.93 10/03/2002 0:48 3.46 14.88 10/03/2002 0:49 3.59 14.88 10/03/2002 0:50 3.56 14.88 1010312002 0:51 3.32 14.89 10103/2002 0:52 3.5 14.92 10/03/2002 0:53 3.5 14.92 10I0312002 0:54 3.76 14.94 10/03/2002 0:55 3.61 14.92 10/03/2002 0:56 3.61 14.94 10103/2002 0:57 3.3 14.92 10/03/2002 0:58 3.35 14.93 10103/2002 0:59 3.42 14.97 

# ' 10103/2002 1:00 3.66 14.93 10/0312002 1:01 3.71 14.92 10103/2002 1:02 3.52 14.93 1010312002 1:03 3.46 14.94 -10103/2002 1:04 3.65 14.93 10/03/2002 1:05 3.38 14.92 10/0312002 1:06 3.52 14.91 10103/2002 1:07 3.65 14.94 10/03/2002 1:08 3.58 14.95 1010312002 1:09 3.56 14.96 10/03I2002 1:10 3.6 14.95 10t0 3/2002 1:11 3.65 14.98 10/03/2002 1:12 3.57 14.94 10I0312002 1:13 3.61 14.95 10/03/2002 1:14 3.62 14.98 10103/2002 1: 15 3.54 14.98 10/0312002 1:16 3.6 14.98 10/03/2002 1:17 3.53 14.97 10/03/2002 1:18 3.8 14.99 10103/2002 1:19 3.79 14.96 

# 0O0O5 0

## 10/0312002 1:20 3.2 14.96

10103l2002 1: 21 3.13 14.97 10/0312002 1:22 3.5 14.97 10/03/2002 1:23 3.67 14.94 10/0312002 1:24 3.7 14.97 10/03I2002 1:25 3:46 14.95 10l03/2002 1:26 3.51 14.95 10/03/2002 1:27 3.57 14.95 10/0312002 1:28 3.86 14.97 10103l2002 1:29 3.6 14.98 Hour{y Average CO2 (%) 02 (%) 3.6 14.9



# 00~i~ 

# 051

# ~
~
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, 2nd Ha{f of Carbon Burnout Soak - Hour 3

Date Time CO2 (°fo) 02 (%)


# ~ 1410312002 2:30 3.33 15.03 ' 10/0312002 2:31 3.67 15.01 10103/2002 2:32 3.63 15.05 

# ~ 10/03/2002 2:33 3.34 15.03

, 10/03/2002 2:34 3.71 15.08 ` 10103/2002 2:35 3.62 15.02 10l0312002 2:36 3.91 15.03 

# ~ 10103/2002 2:37 3.64 15.04 

# ~ 10/03/2002 2:38 3.54 15.03 10/03/2002 2:39 3.47 15.04 1 10/0312002 2:40 3.45 15.03


# ~ 10/03/2002 2:41 3.59 15.07 10/0312002 2:42 3.29 15.07 

# ~ 10/0312002 2:43 3.09 15.05 ' 10/03/2002 2:44 3.52 15.04 

# ~ 10/03/2002 2:45 + 3.74 15.06 10/0312002 2:46 3.54 15.05 

# ~ 1010312002 2:47 3.34 15.08

, 10/03/2002 2:48 3.72 15.06 10103/2002 2:49 3.55 15.07 ` 1010312002 2:50 3.61 15.07 ' 10/03/2002 2:51 3.48 15.06 10/03/2002 2:52 3.51 15.04 

# ~ 10/03/2002 2:53 3.32 15.06 

# ~ 10/03/2002 2:54 3.67 15.06 

# ~ 10/0312002 2:55 3.53 15.05 10103/2002 2:56 3.51 15.05 

# ~ 10/0312002 2:57 3.6 15.04 

# ~ 10/03/2002 2:58 3.37 15.08 1010312002 2:59 3.35 15.07 

# ~ 10/0312002 3:00 3.21 15.05 

# ~ 1010312002 3:01 3.64 15.09 1010312002 3:02 3.56 15.08 

# ~ 1010312002 3:03 3.77 15.05 

# ~ - -10103/2002 3:04 3.5 15.09 

# ~ 10103/2002 3:05 3.37 15.09 10103/2002 3:06 3.37 15.05


# ~ 10/03/2002 3:07 3.48 15.08


# ~ 10/0312002 3:08 3.64 15.05

10/0312002 3:09 3.45 15.05 

# ~ 10/0312002 3:10 3.63 15.07


# ~ 1010312002 3:11 3.31 15.06 

# 1 1010312002 3:12 3.51 15.05

10103/2002 3:13 3.57 15:08


# ~ 10/03/2002 3:14 3.36 15.09


# ~ 101.0312002 3:15 3.48 15.09

10103/2002 3:16 3.38 15.08


# ~ 10I0312002 3:17 3.64 15.09


# ~ 10/0312002 3:18 3.94 15.08 0 10/0312002

. 3:19 3.95 15.08 

# 00,0052

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## 10/03/2002 3:20 3.9 15.07

10/03/2002 3:21 3.47 15.1 1010312002 3:22 3.65 15.07 1010312002 3:23 3.21 15.11 10103/2002 3;24 3.31 15.1 10103/2002 3:25 3.36 15.09 1010312002 3:26 3.46 15.08 1010312002 3:27 3.63 15.08 10I03I2002 3:28 3.56 15.1 10/03/2002 3:29 3.37 15.13 

# Hourly Average CO2 (%) 02 (%) 3.5 15.1



# - 0000'53

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~ ~ 2nd Half of Carbon Burnout Soak - Hour 4

Date Time CO2 (%) 02 (%) 1010312002 4:30 3.77 15.21 10/03/2002 4:31 3.4 15.24 10103/2002 4:32 3.4 15.23 1010312002 4:33 3.31 15.24 10/03/2002 4:34 3.47 15.24 10/03/2002 4:35 3.83 15.2 10/03l2002 4:36 3.54 15.22 10/03l2002 4:37 3.47 15.23 1010312002 4:38 3.57 15.23 10/0312002 4:39 3.53 15.22 1010312002 4:40 3.44 15.22 10/03/2002 4:41 3.45 15.24 10/03/2002 4:42 3.48 15.24 1010312002 4:43 3.51 15.19 10/0312002 4:44 3.75 15.23 10/03/2002 4:45 3.56 15.23 10103l2002 4:46 3.59 15.2 1010312002 4:47 3.39 15.22 10103/2002 4:48 3.06 15.24 1010312002 4:49 3.56 15.2 1010312002 4:50 3.5 15.23 1010312002 4:51 3.49 15.23 10/03/2002 4:52 3.04 15.23 10/03/2002 4:53 3.82 15.2 1010312002 4:54 3.7 15.24 10/0312002 4:55 3.3 15.25 10103/2002 4:56 3.51 15.25 10/03/2002 4:57 3.62 15.25 10l03l2002 4:58 3.35 15.24 10/03/2002 4:59 3.49 15.24 10l0312002 5:00 3.6 15.23 10103/2002 5:01 3.45 15.21 10/03l2002 5:02 3.57 15.21 1010312002 5:03 3.33 15.22

_ _1010312002 5:04 3.35 15.22 10/03/2002 5:05 3.28 15.23 10/0312002 5:06 3.26 15.27 10/03/2002 5:07 3.67 15.24 10/03/2002 5:08 3.68 15.22 10/03/2002 5:09 3.78 15.22 10/03/2002 5:10 3.37 15.22 10l0312002 5:11 3.22 15.21 10/0312002 5:12 3.43 15.23 1010312002 5:13 3.44 15.23 1010312002 5:14 3.47 15.23 10/03/2002 5:15 3.59 15.23 1 0Ib3l2002 5:16 3.49 15.22 1010312002 5:17 3.66 15.25 10/0312002 5:18 3.47 15.26 10/03/2002 5:19 3.27 15.27



# ~~ 

# O00,54

## 1010312002 5:20 3.47 15.26

1 0103/2002 5:21 3.1 15.26 10/0312002 5:22 3.75 15.26 10/0312002 5:23 3.52 15.26 1 0l0312002 5:24 3.4 15.27 10/03/2002 5:25 3.54 15.23 1 0/0312002 5:26 3.66 15.26 10/0312002 5:27 3.74 15.28 10t0312002 5:28 3.34 15.24 10/03l2002 5:29 3.13 15.26 

# Hourfy Average c02 (%) 02 (%) 3.5 15.2

.

# 2nd Half of Carbon Burnout Soak - Hour 5

Date Time CO2 (%) 02 (%) 10l03/2002 6:30 3.92 15.21 10/03/2002 6:31 3.58 15.23 10/0312002 6:32 3.81 15.21 10103/2002 6:33 3.53 15.21 1010312002 6:34 3.57 15.21 10/03/2002 6:35 . 3.3 15.23 10/03/2002 6:36 3.72 15.21 10103l2002 6:37 3.71 15.21 10l0312002 6:38 3.57 15.21 10103/2002 6:39 3.73 15.18 10l0312002 6:40 3.73 15.17 10/03/2002 6:41 3.38 15.18 1010312002 6:42 3.32 15.17 10103/2002 6:43 3.57 15.18 10/03/2002 6:44 3.53 15.17 10103l2002 6:45

~ 

# 3.55 15.17 10103/2002 6:46 3.4 15.2 10I0312002 6:47 3.37 15.15 10103/2002 6:48 3.3 15.18 10I03l2002 6:49 3.37 15.19 1010312002 6:50 3.21 15.17 10/03/2002 6:51 3.59 15.2 10103I2002 6:52 3.56 15.21 10I03l2002 6:53 3.54 15.2 10/03I2002 6:54 2.93 15.18 10I0312002 6:55 3.61 15.18 10l03I2002 6:56 3.59 15.21 10103/2002 6:57 3.2 15.21 10/03/2002 6:58 3.47 15.2 10/03/2002 6:59 3.2 15.2 10I0312002 7:00 3.65 15.2 10/03/2002 7:01 3.61 15.21 10103I2002 7:02 3.27 15.19 10l0312002 7:03 3.17 15.2 10I0312002 7:04 3.42 15.2 10103/2002 7:05 3.13 15.18 10103/2002 7:06 3.47 15.2 10/03l2002 7:07 3.44 15.19 10/03/2002 7:08 3.36 15.15 10/0312002 7:09 3.32 15.19 10l03/2002 7:10 3.63 15.15 10103l2002 7:11 3.69 15.17 10/03/2002 7:12 3.62 15.16 10I0312002 7:13 3.41 15.16 10/03/2002 7:14 3.56 15.15 10I0312002 7:15 3.53 15.15 10103/2002 7:16 3.41 15.16 10/03/2002 7:17 3.54 15.16 10/0312002 7:18 3.52 15.17 10/03/2002 7:19 3.25 15.19 .11

# 10/0312002 7:20 3.46 15.2

10l0312002 7:21 3.55 15,18 10/0312002 7:22 3.24 15.19 10103/2002 7:23 3.37 15.2 10103l2002 7:24 3.48 15,21 10103l2002 7:25 3.6 15.21 10/03/2002 7:26 3.65 15.21 1010312002 7:27 3.4 15.18 1010312002 7:28 3.43 15.18 10103l2002 7:29 3.53 15.19 

# Hourly Average c02 (%) 02 (%) 3.5 15.2



# ° ~ ~

# 2nd Half of Carbon Burnout Soak - Hour 6

Date Time CO2 (%) 02 (%) 10/03/2002 8:30 3.06 15.13 10/0312002 8:31 3.51 15.15 10/03/2002 8:32 3.18 15.14 10/03/2002 8:33 3.42 15.15 10103l2002 8:34 3.63 15.15 1010312002 8:35 3.37 15.16 10/0312002 8:36 3.33 15.14 10103/2002 8:37 3.33 15.17 10l03/2002 8:38 3.26 15.16 10/03/2002 8:39 3.43 15.17 10103I2002 8:40 3.33 15.12 10/03/2002 8:41 3.51 15.11 10103/2002 8:42 3.69 15.11 10103/2002 8:43 3.64 15.12 10/0312002 8:44 3.71 15.09 1010312002 8:45 3.81 15.1 10103I2002 8:46 3.4 15.1 10/0312002 8:47 3.95 15.1 10103/2002 8:48 3.09 15.1 10/03/2002 8:49 3.48 15.1 10I0312002 8:50 3.55 15.13 1 0/03/2002 8:51 3.09 15.13 10/0312002 8:52 3.69 15.14 10/03/2002 8:53 3.04 15.11 10/03/2002 8:54 3.42 15.11 10103I2002 8:55 3.35 15.1 1 0/0312002 8:56 3.83 15.1 10I0312002 8:57 3.37 15.1 10/03/2002 8:58 3.54 15.09 10/03/2002 8:59 3.21 15.1 10/0312002 9:00 3.88 15.09 10/03/2002 9:01 3.31 15.11 1010312002 9:02 3.6 15.12 10/03/2002 9:03 3.62 15.11



# _ 10/03/2002 9:04 3.7 15.14 10/03/2002 9:05 3.57 15.14 10/03l2002 9:06 3.57 15.15 10103/2002 9:07 3.63 15.12 10/03/2002 9:08 3.45 15.19 10/03/2002 9:09 3.21 15.16 10/0312002 9:10 3.32 15.16 10103/2002 9:11 3.22 15.16 10/03/2002 9:12 3.21 15.13 10/03/2002 9:13 4 15.15 10103/2002 9:14 3.66 15.15 10/03/2002 9:15 3.17 15.13 141 * 03/2002 9:16 3.66 15.12 10/0312002 9:17 3.56 15.1 10/0312002 9:18 3.48 15.12 10/03/2002 9:19 3.4 15.1 J



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# 0 2 9:20 3.54 3 

## 29 15.13

15.15 1 p103/2002 9 :21 3.46 15.16 10103/20 02 9 = 22 3 

## 49 15.16 1010312002 9:23 3.74 10103120 02 9:24 15.16 3.75 15.17 10/0312002 9:25 3.48 15.15 1010312002 9:26 3.38 15.15 10/03/2002 9:27 3,34 15.16 1 alo3120 02 9=28 3 24 15.18 10/0312002 9:29 Hourly Average CO2 (%) 02 (%) 

# 3.5 15.1

f 

# . ~ ~ .~ ~ 

# ( ) 0 f) r;. )5 9

# 2nd Half of Carbon Burnout Soak - Hour 7

Date Time CO2 (°fo) 02 (%) 10/03/2002 10:30 3.66 15.19 10/0312002 10:31 3.57 15.17 1 0/03/2002 10:32 3.51 15.16 10103/2002 10:33 3.49 15.12 10103/2002 10:34 3.55 15.17 10/0312002 10:35 3.21 15.21 1 0/03/2002 10:36 3.27 15.2 10/0312002 10:37 2.91 15.22 10/0312002 10:38 3.74 15.2 10103/2002 1 0:39 3.51 15.25 10/0312002 10:40 3.26 15.24 10/03/2002 10:41 3.61 15.22 10/0312002 10:42 3.44 15.23 10/03/2002 10:43 3.35 15.29 10/0312002 10:44 3.49 15.35 10103/2002 10:45 3.61 15.37 10/03/2002 10:46 3.5 15.36 10/03/2002 1 0:47 3.36 15.37 10/03/2002 10:48 3.29 15.39 1 0/03/2002 10:49 3.22 15.38 1010312002 10:50 3.37 15.38 10/03/2002 10:51 3.31 15.38 10/03/2002 10:52 3.45 15.4 10/03/2002 10:53 3.48 15.37 10/0312002 10:54 3.63 15.37 10/03/2002 10:55 3.13 15.39 10/03/2002 10:56 3.73 15.4 10103J2002 10:57 3.49 15.39 10/03/2002 10:58 3.44 15.4 10103/2002 1 

# 10:59 3.33 15.36 1010312002 11:00 3.57 15.39 10/03/2002 11:01 3.5 15.38 10/03/2002 11:02 3.52 15.38 10I03/2002 11:03 3.26 15.39 -10/03/2002 11:04 3.62 15.38 10/03/2002 11:05 3.56 15.36 10/03/2002 11:06 3.26 15.37 10/03/2002 11:07 3.4 15.37 10/03/2002 11:08 3.24 15.35 10/03/2002 11:09 3.61 15.38 10/03/2002 11:10 3.08 15.38 10/0312002 1 - 1:11 3.49 15.37 10/0312002 11:12 3.65 15.35 10/03/2002 11:13 3.22 15.36 10103/2002 11:14 3.18 15.37 10/03/2002 11:15 3.42 15.37 10/0312002 11:16 3.85 15.32 10/03/2002 11:17 3.62 15.35 10/03/2002 11:18 3.32 15.4 10/03/2002 Z 1:19 3.77 15.37 

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~ ~ 10/0312002 11:20 3.36 15.39 10l0312002 11:21 .09 33 4 15.38 10103/2002 11:22 15.4 15.4 10/0312002 11:23 3.14 10/03/2002 11:24 3.48 15.39 10/03/2002 11:25 3.48 15.31 10/03/2002 11:26 3.54 15.43 10l03/2002 11:27 358 3 37 15.3fi

15.3 10l0312002 11:28 15.39 10103/2002 11:29 3,42 Hourly Average CO2 (%) 02 (%) 3.4 15.3 Test Average CO2 (%) 02 (%) 3.4 15.4

## ISOKINETIC STACK CALCULATOR (Revised 11l08/01) 

## INPUT PARAMETERS PITOT COEFFICIENT (Cp): 0.84 METER TEMPERATURE (°F): 90 STACK TEMPERATURE (°F): 450 AVERAGE DELTA P ("H20): 0.25 MAXlMUM DELTA P ("H20): 0.34 ESTIMATED MOISTURE (%): 1 METER BOX NUMBER: 1284-29'64



## DELTA H @: 1.846 NOZZLE DIAMETER (Dn) DATA CALCULATED DIAMETER (in.): 0.3225 SELECTED SIZE (in.): 0.191 CALCULATED PARAMETERS K FACTOR = 0.876 ISOKINETIC DELTA H (71-120) = 0.22 MAX DELTA H ("H20) = 0.3 SAMPLING PARAMETERS MIMIMUM SAMPLE VOLUME REQUIRED (ds 31.8 SAMPLE TIME REQUIRED (min): 60 AVERAGE SAMPLE RATE (cfm): 0.26 MAX SAMPLE RATE (cfm): 0.3
PROJECT NUMBER: 021304 TEST RUN NUMBER: 1-5 

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# 0 0 IND 6 3

# Vermont BrickCompany

Highgate Center, VT Project: 021304 Periodic Kiin Compliance Cool Down

- 

# Hour 1 Date Time CO2 (%) 02 (%) 10/03/2002 12:30 0.16 20.74 10/03/2002 12:31 0.13 20.66 10/03/2002 12:32 0.1 20.63 10/03/2002 12:33 0.09 20.71 10/03/2002 12:34 0.12 20.67 10/03/2002 12:35 0.14 20.74 10/03/2002 12:36 0.23 20.76 10/03/2002 12:37 0.11 20.72 10/03/2002 12:38 0.13 20.69 10/03/2002 12:39 0.18 20.72 10/0312002 12:40 0.16 20.74 10/03/2002 12:41 0.14 20.7 10/03/2002 12:42 0.09 20.67 10/03/2002 12:43 0.12 20.68 10/03/2002 12:44 0.14 20.7 10/03/2002 12:45 0.04 20.69 10/03/2002 12:46 0 20.69 10/03/2002 12:47 0.01 20.71 10103/2002 12:48 0.11 20.69 1010312002 12:49 0.04 20.72 10/03/2002 12:50 0.21 20.72 10/03/2002 12:51 0.06 20.7 10/03/2002 12:52 0.02 20.69 10/03/2002 12:53 0.07 -20.72 10/03/2002 12:54 0.06 20.71 10103I2002 12:55 0.11 20.71 10/03l2002 12:56 0.08 20.69 10/03/2002 12:57 0.05 20.69 -10/0312002 12:58 0.32 20.68 10/03/2002 12:59 0.11 20.71 10/03/2002 13:00 0 20.68 10/0312002 13:01 0.21 20.66 14/03/2002 13:02 0.1 20.68 10/03/2002 13:03 0.13 20.65 10103/2002 13:04 0.07 20.7 14/03/2002 13:05 0.06 20.68 10/0312002 13:06 0.23 20.66 10/03/2002 13:07 0.19 20.66 10/03/2002 13:08 0.06 20.66 10103I2002 13:09 0.19 20.67 10/03/2002 13:10 0.21 20.66 10/03/2002 13:11 0.07 20.69 10/03/2002 13:12 0.09 20.67 414



# 00 ,0064

# 10/03/2002 13:13 0.15 20.66

10/03/2002 13:14 0.26 20.68 10/03/2002 13:15 0.32 20.67 10/03/2002 13:16 0.16 20.7 10/03/2002 13:17 0.15 20.68 10/0312002 13:18 0.3 20.66 10/03/2002 13:19 0.36 20.67 10/03/2002 13:20 0.26 20.67 10/03/2002 13:21 0.2 20.68 10/03/2002 13:22 0.06 20.67 10/0312002 13:23 0.09 20.69 10103/2002 13:24 0.05 20.68 10/03/2002 13:25 0.04 20.69 10/03/2002 13:26 0.03 20.7 10/03/2002 13:27 0.09 20.66 10/03/2002 13:28 0.19 20.67 10/03/2002 13:29

- 

# 0.17 20.68 0

Hour{y Average CO2 (%) 02 (%) 0.1 20.7



# 00 1

0065

## 10/03/2002 15:17 0.05 20.82

10103l2002 15:18 0.08 20.Z5 10/0312002 15:19 0.07 20.79 10/0312002 15:20 0.1 20.77 1010312002 15:21 0.06 20.84 10/0312002 15:22 0.04 20.81 10/03/2002 15:23 0.07 20.85 10103J2002 15:24 0.09 20.81 10/03/2002 15:25 0.11 20.87 10/0312002 15:26 0.13 20.79 10/03/2002 15:27 0.11 20.8 10103/2002 15:28 0.09 20.85 10/03/2002 15:29 0.04 20.83 Hourly Average CO2 (%) 02 (%) 0.1 20.8 Test Average CO2 (%) 02 (%) 0.1 20.7



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# ~. ~. ~ ~ ~ Cool Down - Hour 2

Date Time CO2 (%) 02 (%) 10/03/2002 14:30 0.11 20.75 10/03/2002 14:31 0.33 20.79 10/03/2002 14:32 0.08 20.82 10/03/2002 14:33 0.07 20.77 10103/2002 14:34 0.08 20.74 10/03/2002 14:35 0.02 20.76 10/03/2002 14:36 0.15 20.71 

## 10/03/2002 14:37 0.05 20.78 10/03/2002 14:38 0.06 20.8 10103/2002 14:39 0.05 20.82 1010312002 14:40 0.11 20.79 10/03/2002 14:41 0.06 20.84 10/03/2002 14:42 0.04 20.82 10/0312002 14:43 0.09 20.8 10/0312002 14:44 + 0.1 20.81 10/03/2002 14:45 0.12 20.77 10/03/2002 14:46 0.07 20.75 10/0312002 14:47 0.05 20.79 10/03/2002 14:48 0.06 20.86 10/03/2002 14:49 0.1 20.84 10/03/2002 14:50 0.11 20.86 10/03/2002 14:51 0.06 20.85 10/03/2002 14:52 0.09 20.81 10/03/2002 14:53 0.02 20.77 1010312002 14:54 0.08 20.72 10/03/2002 14:55 0.12 20.84 10/03/2002 14:56 0.13 20.87 10I03I2002 14:57 0.07 20.82 10/03/2002 14:58 0.04 20.79 10/03/2002 14:59 0.06 20.77 1010312002 15:00 0.1 20.83 1010312002 15:01 0.09 20.86 10/03/2002 15:02 0.13 20.81 1010312002 15:03 0.07 20.78 10/03/2002 15:04 0.09 20.84 10/03/2002 15:05 0.03 20.86 10/03/2002 15:06 0.05 20.79 10l0312002 15:07 0.02 20.8 10/03/2002 15:08 0.11 20.77 10/03/2002 15:09 0.1 20.84 10/03/2002 15:10 0.08 20.82 10/0312002 15:11 0.08 20.78 10/03/2002 15:12 0.04 20.75 10103/2002 15:13 0.09 20.83 10103/2002 15:14 0.12 20.88 10/03/2002 15:15 0.13 20.8 10/03J2002 15:16 0.08 20.84 

# -() 0, Pi: ~~.1 , 

# . . SAMPLE LOGICHAIN OF CUSTODY RECORD
AQTS CLIENT: Vermont Brick PROJECT: 021304 Sample Number Date

Collected Date

Received Test

Number Description 

# C905 10/01/02 10/04102 1-1 Fluoride impinger catch, backup filter, train rinses C906 10/02102 10104102 1-2 Fluoride impinger catch, backup filter, train rinses C907 10/02102 10I04/02 1-3 Fluoride impinger catch, backup filter, train rinses C908 10103102 10104102 1-4 Fluoride impinger catch, backup filter, train rinses C909 10/03/02 +10104102 1-5 Fluoride impinger catch, backup filter, trai 

## n rinses 

# C910 10l03/02 I 10/04/02 AII IDistilledldeionized water collection medium and rinse blank



# I

~ . . I " 

# I
~



# I = I I 

# I I
Samples Logged By: I John J. Jasko Date: 1 10/04102 1 Time: 1 08:30 

# 'S amples Relinquished :y: John J

.

## Jasko

r 1 - r r' -

## 1 - 

# `C

- )XFORD I.ABORATORIES

~ 

# 91 Division of Tritest t I 

# Analytical and Consulting Chemzsts 1316 South Fifth Street Wilmingtan, N.C. 28401

(910) 763-9793 

# Fax (910) 343-9688 

# DATE RECEIVED 10-08-02 1 DATE REPORTED 10-31-02

~ 

# 02T1079 I t 

# PAGE 1 OF 2►

~ 

# AIR QUALITY TECHNZCAL SERVICES INC. P.O. # 3133 18 MORSE DR.

~ 

# ESSEX JUNCTION, VT 05452

~ 

# ATTENTION: JOHN JASKfl

~ 

## 1 

# SAMPLE DESCRIPTION: M13B FLUORIDE 10-08-02 t 1. C905 1-1 2. C906 1-2

~ 

# 3. C907 1-3 ~ 

# E 4. C908 1-4 5. C909 1-5

~ 

# 6. C910 

# I

~ 

# RESULTS

~ 

# 1

} 

# Fluoride, as HF, Total ug 554 1 

# _Initial. Volume, mis 550 2 3 4 5 6 5030 35100 10200 732 <105 655 620 545 425 325



# ~`~~~0 6 9

# XFORD LBORATORIES

.. Division of Tritest 

# Analytical anci Consulting Chemists 1316 South Fifth StreeC Wilmington, N.C. 28401

(910) 763-9793 Fax (910) 343-9688 

# DATE RECEIVED 10-08-02 DATE REPORTED 10-31-02

02T1079
PAGE 2 OF 2

~ 

# AIR QUALITY TECHNICAL SERVICES INC. P.O. # 3133 18 MORSE DR. 1 ESSEX JUNCTION, VT 05452

~ 

# ATTENTION: JOHN JASKO 

# I

~ 

# SAMPLE DESCRIPTION:

# M13B FLUORIDE 10-08-02 1

~ 

# 7. METHOD 

# i 1 1

~ 

# Fluoride, as HF, Total ug 

# b i 1

~ 

# b

~ Q

~
~
~
~ ` ]

~ 1 

# RESULTS 7 

# 13B



# TERESA ADAMS, LAB MANAGER

# ! ~ I 1~ 

# Oxford Laboratdries 

# ~ a 

# Divrsion of Tritesf, Inc. 

# 1 Wet Laboratory Narrative Summary 

# ~ oxford Labs Sample Number: 02T1079 :

Report Date: 10I2512002 1



## , Client lnformation

Client: Air Quality Technicai Services

~ 

## Project #: 21304

Received Date: 10/8/2002 

## 1 Chain of custody: Yes 1 Shipped via: Federal Express

Comments upon receipt: Samples satisfactory

~ 

## Any observed discrepancies: No



# ~ Instrumentation ' Instrumentation Used: Accumet Fiuoride ISE Electrode Fisher Scientifc Accumet 25 meter 

# ~ Class A Glassware ! Analysis Requested: Fluoride



# ~ Sample Numbers: 01-06 

## Method of Analysis 13B



# ~ Quality Control Requirements 

# ~ QC Requirernents: QC recovery of 90-110%

QC Requirements Met: Yes 

# ~ Duplication: - Duplicates within +1-10% 

# ' Duplication Requirements Met: Yes

Spikes: Spikes within +/- 10% 

# ~ Spike Requirements Niet: Yes

Laboratory blanks within control: Yes 

# ~ Detection limits within controf: Yes ' Caiibration verifred with externa) QC standard: Yes



## ~ 

# Cafculations

S= observed sample value read from meter, ppm

~ 

## B= observed blank value read from meter, ppm ' V= sample value used for calculation, pprn (S-B)=V A= total volume distilled, ml

_ ~ 

## C= amount of sample distilled (grams or ml) ~ 

## 1 

# D= ml distillate analyzed (V)(A!C)(251D)=ppm Fluoride

, Calculation for total ug HF (in needed) 

# F= ppm Fluoride ` 1000= final sampie volume per method 1 1.053= factor to convert F to HF (F)(1000)(1.053)=Total ug HF 

## ` Additiona! comments Per Method 1313, all samples are brought to 1000 m L 

# t fnal voiume prior to fluoride distillation and analysis.

~ 

## All initial volumes are recorded and reported.

~ 

# Report compieted by: Chuck Williford Date 10125J2002 Signed
~ 

## V

# 1'GTAL uG ,5 PHI I tV= :l 1,853 = SPIxB TO1'AI, uG 1'OtnL uG 

# LEVEL FLUORIDe HP



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# Xf ; XULfIPL3


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# ~ 105 5 STD 25 1 l.4 5,010 5.010 5 -



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## 5010 -2DUP 250 270. / 4.410 / 4.753 -.58 5 4760



# ~ •2SPr, 25 250 l 270.0 / 9.400 

# ~ / 1a.152 53.80 / 5- 

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# ~ PpH 25 1 1.0 5.240 f 5.243 5 5 

## 4-1 25 250 250,0 1.080 / 1.123 S



# ~ 6-506 25 1 1.0 1.630 / 1.630 5 2 S , 1 1. 0 0. 00f/ ' < 10 S 

# ~ PPK 25 1 1.0 5.130 

# ~ 5.180 - 5



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## WXFORE) 1316 South r I M StreeE 

## aboratories W?1mi.ngtoQ. N.C. 28401 (910) 763-9793 nc. _ F'ex(9i0) 343-9688 

## PARAh{ETER: 

# `
~ 

# !2 

# 6 ANALYST 

# ~ t/tS REVIE7ED BY DATE BEGAN: 

# 1Q'`y'OZ, TIME:

# ~~Ja DATE COMPLETED: TIMF: 

## N 

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# ' I I

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# 74
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## i+4

# APPENDIX F Operating Data Log;



# ~ MAIN GA.S ME TER FIN I SH 411 

# J 2 1 1 l 

# a ~ BTART -'O( 3(obloS 

## O



# ~ TOTAI+ TOTAL ® 80ILER METER FINI9H 9oZ.• 

# ~ START



# ~ TOTAL TOTAL



# ~ SUH TOTAL •



# ~ -DRYER FINI3H 

# o 

# ~ ~ BTART



# ~ TOTAL a TOTAL p TOTAx. GAS k`OR KI LN ( MC F)



## ~ TOTAl+ HOURB BURNED
. 

# g ~ ~,~ ~ / TOTAL INCH. 

# E B 8E TTI.T 

## ~.D 

# q

~ SURNER SETTING6: TOP AIR 

# ~_ " GA3 " BOTTpM AIR 

# <<- _ " GAS • O"

~ 

# . . ®

~ ~ ®

~ ® ® ® ® ®

~

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# ®
~ ® ®

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# ~
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## o. . 4



# Prompt Fur

~ 

# ct bon Seg m e rrt Val ue Procnpt Fur

~ 

# ct bn Seg m e rit' V a I ue SiHi"SE-G Start Seg. SEG7RAMP Ramp Time 7 END SEG Erxi Seg. SEG8 SP Soak SP 8 RECYCLE.S Number ot



# Recycles SEG8TIME 

# Soak Time 8
S4AK DEY Deviation



# Value SEG9RAMP Ramp Time 9 

# ' 

# SFGI RAW Ranp Time 1 

# 10 SG1 o SP Spak S P 10 SF-G2 SP Soak SP 2 2 0a SG10 TIME Soak Time 10 i SEG2TIME Soa}c Time 2 2 . SG1 1 RAMP. ~ 

# • Ramp Time 11 

# I
SEaRAMP Ramp Ttme 3 ~ 

# SG12 SP Soak SP 12 SEG4 SP Soak SP 4 'g10 ' SG121'1ME Soak Time 12 SEG4TTME Soakc rrne 4 

# ~ D ~ r, STATE Pro9ram Corttroller 

# St at e SEGdRAIAP Rarnp Time 5 PROG ETtD CaMrol}er Status SEG6 SP 

# • So ak S P 6 RAM' LUT Engr. Unit 

# ior Ramp SEG611biE So ak Time 6

~



# ~ • 

# ~ 

# 1197 UDC 3000 Controller Product Manual

_ 127

~ • ~ ~ 

# r,;
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# NO.

ry



# A Q A&

## Honeywell Control Pressure

w " FE AR .9 

# t 

# FIMA M . 

# F u M



# M m 

# MA

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# ® 

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# WM. ~ ~ • j I 

# Fff*

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# ~~r®~~or~~►► .~

# APPENDIX G Equipment Calibration 

# Sheets

## ~

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~ I

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### 61' LLI l:J D LO L ~ '#:,.; flJ;r:;:G O N V) M G? ~ ~ ~} ~ Q ;•;. ~. , c ~

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ti c0 M C7 I ~ C 

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~ ' ~ t~ - :~. ::C; ~ •~ ::titiY N
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l!~ N N N :•::.:::i'i5: r O O O O O ~ O O O O O j$::fi:•ii:.} 0~~ O a O :ti~i ;: ~ :~:• •::ti~ : {::•: M T ~ CO (D CJ ••.. 0 T r r T r '::;~,: aaaaoo :~::, ~:: r r T r r r

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# _ c NOZZLE CALIBRATION DATA FORIVI

:

NOZZLE IDENTIFICATION NOZZLE DIAMETER (D) D diff. 

# D avg. A B C NUMBER (in.) (in.) (in.) (in.) (in.) C-3 0.191 0.190 0.191 0.001 0.191 Calibrated By: John J. Jasko Date: 10/01/02

1

~

# Stack Temperature Sensor Calibration

Date: 01112/2000 Barometric Pressure: 29.82 Ambient Temperature: 61 °F 

## Cafibrated by: John Jasko Thermocouple Id # : T.C-24-2 Reference Thermometer Tem erature °F Thermocouple Potentiometer Tem erature (°F) Temperature Difference % Reference Point Source 

## 1 lce Water 33 33 0.0 2 Warm Water 116 116 0.0 3 Hot Oil 245 247 -0.3



# 7--T 4 Hot Oil 396 396 0.0

~ ;

# ITOT' #



# re , "_ " ID2. DATE 

# OBSERVATIONS BY 

# ~ ,) A11 construction criter•ia for an isolated "S" type pitot are within given tolerances prescribed in Federal Register, Vol. 42, No. 160. Thursday,

~ 

# ugust 18, 1977. REOUIRED MEASUP,EMENTS

a. External tubing Ci.imeter, , D t , 0.23 in .< D t < 0.38 in .
. b. I3ase to plane opei:irg D; star,ce , Pa and PB, 0.40 in .< PA=Pg < 0.60 in .



# mo
~ PB= O

D t = 

# 0.376 PA= D. S(o ZS

. - UsE ax.= LQNG:TLID;` ~~-_~ G• ; ~ "


# .all assEn:blv criteria to prevEnt aerodynamic interference for a samoling arrangement )

~ .; . 

# ot an "S" type pitot, nozzi.e and thermocoisple, are within given rolerances prescribed 

# in Federa? Register, Vo1. 42, No. i60. Thursday, August 18, 1977. - 

# RE('U:11r.SD ; IEASliRE:`I E\TS

~ !!! 

# ~ ~ 

# a. External tubing di.ameter.- See l.a. above b. Pitot / nozz7.e sepa.ration, k, X> 0.73 in. ior nozzle d-ameter, D n= 0.50 in. 

# ~ ~ c. Plane of impact side oF pitot in relation to plzne of nozzle opening.



# ~ d. Thernocouple placement, Z, A-? > 0.75 in., a-W > 3.0 in., B-Z > 2.0 ir..

~ 

# . P1toL / Drobe s!'.eath di

~ 

# ta!lce, Y, Y > 3.0 1:7.



# ~

~•Iti
a. 

# -:`:E. '

~ 

# `._. • - 

# x ~ I~ 

# b . NOZZLE D O

~ 

# ~ ~

.



### ~ i - ' 

# B-Z

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# ~ rr?; 5?1 f07 tlsCl - ~ 7 rtiz:• cK6!

~ li

_ --•--

### i 

# ~ !tvE S P1TD1 T-AC 

# d . -- - 

# oR ~ 

# Y e. D n = o . /9/ .l' = 1.00 ` r 

# 7 = 0.8 

# ~~ ,, C . T
~~ 

### : L 

# Y \ ; 

# > 0.0 in. '

# ~ Nitrogen 99.998% Oxygen 5 ppm Moisture 3 ppm Total Hydrocarbons < 0.5 ppm 

# 99.998% < 5 ppm < 3 ppm < 0.5 ppm 

# ~ 

# ~ r 

# ~ 

# as,

. 

# r ®Speciatty Gases
' 325 MCCausland Court 

# ~ Ch:shire, C106410



# ~ (203) 250-6827 fAX:(203)250 -6842 / , 

# ~

, t



### , 

# CERTIFICATE OF BATCH ANALYSIS

Date: 05/16/00 

# Customer: Airgas East-Cheshire
~ 

## 325 McCausland Ct.
~ Cheshire, CT 06410

~ Record # 13935
~ P.O. # 249476

~ Grade of Product: Zero 4.8



# ~ 

# Cy(inder Number: Component
~

~ 

# ~ 677456D



# ~
~ 

# 9 Actual Concentration 

# Reguired Concentration

Lot # B00-128-003



# ~ Rest of Cylinders in Lot:

~ CC84025 CC98004 CC119403 CC119486 

# ~
~
~
~
~
~
~
~ CC116330 CC104423 CC96422



# ~ ~ Approva! Signature 

# '

~
~ . ' '



# ~

~► 

# —t ~ f-~~

# SPECTRR GiRSES 1NCw 3434 Route 22 West • 8ranchburg, NJ 08876 USA Tel.: (908) 252-9300 •(800) 932-0624 - Fax: (908) 252-0811 Shipped From: 80 Industrial Drive • Alpha, NJ 08865 f: t;;

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