## Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

## Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units of

### EIA

Facility Code Facility Name Boiler ID Fuel Type 1

PPL Montour Station

031 - Unit 1 bitum inous

### Fuel Type 2 Fuel Type 3 Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte

0 PPL Montour Station

031 - Unit 1

As Received Higher Heating Value 0 PPL Montour Station

031 - Unit 1

As Received % Moisture 0 PPL Montour Station

031 - Unit 1

As Received % Ash 0 PPL Montour Station

031 - Unit 1

As Received % Sulfur 0 PPL Montour Station

031 - Unit 1Dry

basis Higher Heating Value 0 PPL Montour Station

031 - Unit 1Dry

basis % Ash 0 PPL Montour Station

031 - Unit 1Dry

basis % Sulfur 0 PPL Montour Station

031 - Unit 1Dry

basis Antim ony 0 PPL Montour Station

031 - Unit 1Dry

basis Arsenic 0 PPL Montour Station

031 - Unit 1Dry

basis Bery llium 0 PPL Montour Station

031 - Unit 1Dry

basis Cadmium 0 PPL Montour Station

031 - Unit 1Dry

basis Chlorine 0 PPL Montour Station

031 - Unit 1Dry

basis Chromium 0 PPL Montour Station

031 - Unit 1Dry

basis Cobalt 0 PPL Montour Station

031 - Unit 1Dry

basis Fluorine 0 PPL Montour Station

031 - Unit 1Dry

basis Lead 0 PPL Montour Station

031 - Unit 1Dry

basis Manganese 0 PPL Montour Station

031 - Unit 1Dry

basis Mercury 0 PPL Montour Station

031 - Unit 1Dry

basis Nickel 0 PPL Montour Station

031 - Unit 1Dry

basis Selenium

### An alysis M ethod for each A nalyte

(example: ASTM D5865-04)EIA Facility Code Facility

Name Boiler ID HA Ps Test Group 0 PPL Montour Station 031 - Unit 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Test 1 1.2D 3/16/2010 3/16/2010 15148.00 Btu/lb 1.62 8.74 2.425 Test 2 1.2D 3/16/2010 3/16/2010 15151.90 Btu/lb 1.53 8.9 2.43 Test 3 1.2D 3/17/2010 3/17/2010 15117.30 Btu/lb 1.51 8.66 2.366 Fuel Testing Results% Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic Units Bery llium (Dry Basis) Bery llium

Units Cadmium

(Dry Basis) 8.88 2.465 0.12 % 0.06903 ppm <4.96 ppm 3.28 ppm <0.04 ppm <0.05 9.03 2.468 0.12 % 0.07319 ppm <4.98 ppm 2.58 ppm <0.04 ppm <0.05 8.79 2.402 0.12 % 0.06774 ppm <4.94 ppm 2.47 ppm <0.04 ppm <0.05Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units ppm 15.1 ppm 4.21 ppm 14.4 ppm 4.66 ppm 0.88 ppm <0.25 ppm ppm 14.3 ppm 4.76 ppm 13.8 ppm 5.22 ppm 0.59 ppm <0.25 ppm ppm 16 ppm 4.79 ppm 14.8 ppm 6.97 ppm 0.76 ppm <0.25 ppmEIA Facility Code Facility

Name Boiler ID HA Ps Test Group 0 PPL Montour Station 031 - Unit 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units Test 3 1.2C 3/18/2010 3/18/2010 15206.60 Btu/lb 1.16 7.56 2.694 Test 4 1.2C 3/18/2010 3/18/2010 15197.30 Btu/lb 1.17 7.69 2.515 Test 5 1.2C 3/18/2010 3/18/2010 15224.20 Btu/lb 1.17 7.79 2.105 Fuel Testing Results% Moisture

(Dry Basis) % Ash

(Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony (Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic Units Bery llium (Dry Basis) Bery llium

Units Cadmium

(Dry Basis) 7.65 2.726 0.1 % 7.78 2.545 0.11 % 7.88 2.13 0.11 %Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 0 PPL Montour Station 031 - Unit 1

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBery llium

(Dry Basis) Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### HA Ps Test Group 0 PPL Montour Station 031 - Unit 1

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### Fuel Testing Results% Moisture

(as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis)% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony (Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic UnitsBery llium

(Dry Basis) Bery llium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis)Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add y our own unit of measure to the orange hightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm