Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

6017 Newton 2 subbituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

6017 Newton 2 As Received Higher Heating Value 6017 Newton 2 As Received % Moisture 6017 Newton 2 As Received % Ash 6017 Newton 2 As Received % Sulfur 6017 Newton 2 Dry basis Higher Heating Value 6017 Newton 2 Dry basis % Ash 6017 Newton 2 Dry basis % Sulfur 6017 Newton 2 Dry basis Antim ony 6017 Newton 2 Dry basis Arsenic 6017 Newton 2 Dry basis Beryllium 6017 Newton 2 Dry basis Cadmium 6017 Newton 2 Dry basis Chlorine 6017 Newton 2 Dry basis Chromium 6017 Newton 2 Dry basis Cobalt 6017 Newton 2 Dry basis Fluorine 6017 Newton 2 Dry basis Lead 6017 Newton 2 Dry basis Manganese 6017 Newton 2 Dry basis Mercury 6017 Newton 2 Dry basis Nickel 6017 Newton 2 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D5142 ASTM D5142 ASTM D4239 ASTM D5865 ASTM D5142 ASTM D5142 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357 ASTM D6722 ASTM D5987, ASTM D6357 ASTM D5987, ASTM D6357EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6017 Newton 2 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 6/17/10 15:30 6/17/2010 6/17/2010 8392 Btu/lb 6/18/10 17:10 6/18/2010 6/18/2010 8413 Btu/lb 6/23/10 9:55 6/23/2010 6/23/2010 8587 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 30.23 4.88 0.31 12028 Btu/lb 6.99 0.45 29.97 4.78 0.32 12013 Btu/lb 6.83 0.46 28.91 4.68 0.39 12079 Btu/lb 6.58 0.55Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 21.7 19.63 17.83 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 45.58 6.99 47.43 69.47 4.66 1 0.45 44.58 6.83 48.59 69.65 4.52 1.03 0.46 44.61 6.58 48.81 70.03 4.77 1.02 0.55 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

17.43 17.51 17.05EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6017 Newton 2 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 6/16/10 10:00 6/16/2010 6/16/2010 8263 Btu/lb 6/16/10 14:00 6/16/2010 6/16/2010 8333 Btu/lb 6/16/10 17:40 6/16/2010 6/16/2010 8244 Btu/lb 6/22/10 13:00 6/22/2010 6/22/2010 8599 Btu/lb 6/22/10 15:20 6/22/2010 6/22/2010 8519 Btu/lb 6/22/10 17:10 6/22/2010 6/22/2010 8363 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 30.28 5.10 0.36 11852 Btu/lb 7.31 0.52 30.14 4.83 0.38 11927 Btu/lb 6.91 0.54 30.71 4.76 0.38 11898 Btu/lb 6.87 0.55 28.29 4.68 0.33 11992 Btu/lb 6.53 0.46 29.08 4.51 0.33 12012 Btu/lb 6.36 0.46 29.72 4.91 0.36 11899 Btu/lb 6.98 0.51Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) <0.0015 % <0.0015 % <0.0015 % <0.0015 % <0.0015 % 0.0018 %Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units

74.12 μg/g 73.7 μg/g 69.59 μg/g 72.04 μg/g 69.44 μg/gNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

20.56 44.23 7.31 48.46 69.68 4.55 1.03 0.52 22.83 44.25 6.91 48.84 70.16 4.66 1.02 0.54 22.25 44.22 6.87 48.91 69.97 4.74 1.04 0.55 18.81 45.83 6.53 47.64 69.8 4.66 1.05 0.46 19.77 45.17 6.36 48.47 69.66 4.63 0.98 0.46 17.91 44.82 6.98 48.2 69.06 4.62 0.97 0.51 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 16.91 16.71 16.83 17.5 17.91 17.8582EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 6017 Newton 2 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher

Heating Value (HHV) (as received) HHV Units 6/16/10 10:00 6/16/2010 6/16/2010 8263 Btu/lb 6/17/10 10:00 6/17/2010 6/17/2010 8346 Btu/lb 6/18/10 10:05 6/18/2010 6/18/2010 8671 Btu/lb 6/22/10 13:00 6/22/2010 6/22/2010 8599 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 30.28 5.10 0.36 11852 Btu/lb 7.31 0.52 30.36 4.88 0.36 11984 Btu/lb 7.01 0.51 29.99 4.86 0.34 12386 Btu/lb 6.94 0.49 28.29 4.68 0.33 11992 Btu/lb 6.53 0.46Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) <0.0015 % 0.079 μg/g 0.228 μg/g 1.7 μg/g 0.315 0.0039 % 0.069 μg/g 0.174 μg/g 1.43 μg/g 0.256 0.0021 % 0.052 μg/g 0.175 μg/g 1.47 μg/g 0.258 <0.0015 % 0.063 μg/g 0.131 μg/g 1.07 μg/g 0.187Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units μg/g 0.0948 μg/g 5.99 μg/g 2.82 μg/g 12.8 μg/g μg/g 0.0992 μg/g 5.12 μg/g 3.18 μg/g 15 μg/g μg/g 0.0912 μg/g 5.44 μg/g 2.75 μg/g 10.5 μg/g μg/g 0.0702 μg/g 4.33 μg/g 2.11 μg/g 10.8 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 5.96 μg/g <1.1 μg/g 74.1 ppm 2.18 μg/g 30.28 5.55 μg/g <1.1 μg/g 73.7 ppm 1.87 μg/g 30.36 5.78 μg/g <1.1 μg/g 76 ppm 2.07 μg/g 29.99 4.03 μg/g <1.1 μg/g 69.6 ppm 1.42 μg/g 28.29 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 44.23 7.31 48.46 69.68 4.55 1.03 0.52 16.91 45.05 7.01 47.94 69.38 4.65 1.04 0.51 17.41 44.43 6.94 48.63 69.72 4.66 0.99 0.49 17.20 45.83 6.53 47.64 69.8 4.66 1.05 0.46 17.50 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm