p. 1



# OAR Box 1145 Prepped by Ollie Stewart



# Document

Number: 

# 10 ) F

. R

. Februar

y14 , 198 9
Docket Number: 

# A-87-1 5

Printed 4/23/20088:55:55AM

Sheet 10of 88P. 2 

# A-J7-JS
666 0 Federa l Registe r / Vo i 54 , No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s Th e Genera l Counse l ha s certifie dt o th e Chie f Counsel , fo r

Advocacy , Smal l Busines s Administratio ntha t th e rul e chang e i s no t

expecte dt o hav e a significan t

advers e economi c impac t o n asubstantia l numbe r

o f smal l entitie s (Regulator y Flexibilit y Act , Pub

. L
. 96

- 354 ) becaus e i nmerel y codifyin g th e inheren t righ t o f th e PT O t o reconside r it s decision s sua sponte, th e rul e extend s th e right

t o eac hpart y i naPT O disciplinar y proceedin g t o see k reconsideration

. Th e Paten t

an dTrademar k

Offic e ha s determine dtha t

thi s rul e chang e i s no t

a majo r rul e unde r

Executiv e Orde r

12291

. Th e annua l effec t

o nth e econom y wil l b e les s tha n$10 0 million

. Ther e wil l b e n o majo r increase s i ncost s o r

price s for

consumers.individua l industries

. Federal , Stat e o r

loca l governmen t agencies , o r

geographi c regions

. Ther e wil l b e n o advers e effect s o n competition , employment , investment , productivity , innovation , o r o nth e abilit y o f Unite dState s base d enterprise s t o compet e wit hforeign

base denterprise s i ndomesti c o r expor t markets

. Th e Paten t

an dTrademar k

Offic e ha s als o determine dtha t

thi s notic e ha s n o Federalis mimplication s affectin g th e relationshi p betwee nth e Nationa l governmen t

an dth e State s a s outline d i nExecutiv e Orde r

12612

. Thi s rul e chang e doe s no t contai na collectio no f

informatio nsubjec t

t o th e Paperwor k

Reductio n Act-o f

1980 , 4 4 U.S.C

. 350 1 et

seq. Lis t o f Subject s i n3 7 CF RPar t 1 0 Administrativ e practic e an d procedure , Courts , Invention s an d patents
. Lawyers , Trademarks

. Fo r th e reason s se t

ou t i nth e preambl e an dunde r

th e authorit y grante dt o the

. Commissione r o f Patent s an dTrademark s b y 3 5 U.S.C

. 6 , th e Paten t an dTrademar k

Offic e amend s 3 7 CFRPar t 1 0 a s follows : 

### PAR T 10—REPRESENTATIO N O F OTHER S BEFOR E THE PATEN T AN D TRADEMAR KOFFICE 1

. Th e authorit y citatio nfo r 3 7 CFR Par t 1 0 woul dcontinu e t o rea da s follows : Authority : 5 U.S.C

. 500 ; 1 5 U.S.C

. 1123 ; 3 5 U.S.C

. 6 , 31 , 32 , 41

. 2

. Sectio n10.15 6 i s amende db y revisin g paragrap h(a ) an daddin g ne w paragrap h(c ) t o rea da s follows : " §10.15 6 Decisio n o fth e Commissioner . (a ] A nappea l fro ma ninitia l decisio n o f th e administrativ e la w judg e shal l b e decide db y th e Commissioner

. Th e Commissione r

ma y affirm , revers e o r modif y th e initia l decisio no r reman dth e matte r t o th e administrativ e la w judg e fo r suc hfurthe r

proceeding s a s th e Commissione r

ma y dee mappropriate

. Subjec t t o paragrap h(c ) o f

thi s section , adecisio n b y th e Commissione r doe s - no t becom e afina l agenc y actio ni na disciplinar y proceedin g unti l 2 0 day s afte r i t i s entered

. I n makin g afina l decision , th e Commissione r shal l revie w th e recor do r

thos e portion s o f

th e recor da s ma y b e cite db y th e partie s i n orde r t o limi t th e issues

. Th e Commissione r

shal l transmi t

acop y o f th e fina l decisio nt o th e Directo r an dt o th e respondent

. **** * (c ) A singl e reques t

fo r reconsideratio no r

modificatio no f

th e Commissioner' s decisio nma y b e mad e b y th e responden t

o r th e Directo r

if file d withi n2 0 day s fro mth e dat e o f entr y o f th e decision

. Suc hareques t shal l hav e th e effec t o f stayin g th e effectiv e dat e o f th e decision

. Th e decisio nb y th e

_Commissione r

o nth e reques t

i s afina l agenc y actio n i n adisciplinar y proceedin g an di s effectiv e o nit s dat e o f entry
. Dated : January 11,1989

. Donal dJ
. Quigg , Assistant

Secretary

and Commissioner

of Patents and Trademarks. [F RDoc
. 89-346 5 File d2-13-89 ; 8:4 5 am ] BILLIN G COD E 3510-16- M ENVIRONMENTA L PROTECTIO N AGENC Y 4 0 CF R Part 6 0 [AD-FRL-3468-4 ] Standard s o f Performanc e fo r New Stationary Sources ; Amendment s t o Tes t Method s an d Procedure s AGENCY: Environmenta l Protectio n Agenc y (EPA)

. ACTION : Fina l rule

. SUMMARY

: O n Februar y 19,198 8 (5 3 FR 5082) , EP A propose damendment s t o th e tes t method s an dprocedure s section s o f th e subpart s i n4 0 CF RPar t 6 0 t o consolidat e al l tes t

method s an d procedure s necessar y t o determin e complianc e wit hth e applicabl e standard s o r

relate dmonitorin g requirement s an dt o clarif y certai n procedures

. Today' s actio n promulgate s thes e amendments ; • . •* EFFECTIV EDATE : Februar y 14,1989 ; * ^ Unde r sectio n 307(b)(1 ) o f

th e Clea n Ai r Act , judicia l revie w o f tri e action s take nb y thi s notic e i s availabl e only b y th e filin g o f

apetitio nfo r

revie w i nth e U.S

. Court s of

Appeal s fo r

th e Distric t

o f Columbi aCircui t withi n6 0 day s o f today' s publicatio no f

thi s rule

. Unde r sectio n307(b)(2 ) o f

th e Clea n Ai r

Act , th e requirement s tha t

ar e th e subjec t

o f today' s notic e ma y no t b e challenge d late r i ncivi l o r

crimina l proceeding s brough t b y EP A t o enforc e thes e requirements

. ADDRESSES : Docke t

No ! A-87-15 , containin g informatio n considere db y - EP A i n developin g th e promulgate drule , i s availabl e fo r

publi c inspectio n an d copyin g betwee n8:0 0 a.m . an d3:3 0 p.m. , Monda y throug hFriday , a t EPA' s Centra l Docke t

Section , Sout h Conferenc e Center , Roo m4 , 40 1 M Stree t SW. , Washington , D C 20460

. A reasonabl e fe e ma y b e charge dfo r copying

. FO R FURTHE R INFORMATIO N CONTACT : Roge r T
. Shigehara , Emissio n Measuremen t

Branc h(MD-19)

. Technica l Suppor t

Division , U.S

. EPA , Researc hTriangl e Park , N C 27711 , telephon e (919 ) 541-1058

. : SUPPLEMENTAR YINFORMATION : I
. Th e Rulemaking

. Th e tes t method s an dprocedure s sectio no f

eac hsubpar t

ha s bee n revise d primaril y t o clarif

y th e sectio n b y consolidatin g al l procedure s tha t pertai n t o on e measuremen t

(e.g. , particulat e matte r concentrations ) unde r on e paragraph , t o delet e repetition s o f method s alread y reference dwithi na cite dmetho d(e.g. , Method s 1 , 2 , an d3 ar e reference db y Metho d5 and , therefore , hav e no t

bee nliste dagain), , an dt o separat e alternativ e method s fro mreferenc e methods

. I n addition , othe r change s hav e bee n mad e fo r consistenc y fro mon e subpar t o r on e sectio nt o another ; procedure s tha t wer e overlooke di n th e : promulg atio n fo r requirement s alread y i nth e subpart s hav e bee nincluded i an dtechnica l error s hav e bee ncorrected

. Majo r amendment s beside s clarification s ar e liste dbelow : 1

. Section 60.2: Sinc e th e standard s ar e base do n referenc e methods , th e applicabl e subpar t

rathe r tha n Appendi x A i s bein g use dt o defin e th e referenc e methods

. Th e titl e o f Appendi x A i s bein g revise dfro m "Referenc e Methods " t o "Tes t Methods " i nanothe r

rulemakin g actio nt o allo w th e inclusio no f

alternativ e method s in Appendi x A

. 2

. Section 60.8(b) and(e): Certai n .-... phrase s o r

requirement s ar e repeate di n eac hsubpar t

o r i nanumbe r

o f subparts

. Sinc e the y ar e generall y applicabl e t o al l subparts , thes e phrase s an d requirement s hav e bee n incorporate d int o th o Genera l Provisions

.P. 4



### Federa l Registe r

/ Vol

. 54 , No
. 2 9 /Tuesday

. Februar y 14 , 198 9 / Rule s an dRegulation s 666 1 3

. Section 60.44a: Lignite fue l subjec t t o th e 34 0 ng/ J standar di s bein g adde d t o th e equatio nan daclarifyin g footnote i s bein g adde dt o th e table

. 4

. Sections 60.46

and 60.48a: Th e us e o f F,
. factor s ha s bee n incorporate dint o di e procedures

. Thi s chang e wa s th e resul t of comment s receive ddurin g proposal

. 5

. Section 60.54: A procedur e fo r Metho d3 for

afacility withou t

awe t scrubbe r i s bein g added ! Th e grab

samplin g techniqu e of

Metho d3 i s als o bein g added

. 6
. Sections 60.93, 60.123, and 60.133: Samplin g rat e i s bein g change dt o sampl e volume

. 7
. Sections 60.165,60.175, 60.185: Th e ' requiremen t

fo r compressin g th e ' recorde r scal e durin g th e performanc e evaluatio n tes t

i s bein g deleted

. 8

. Sections 60.166, 60.176 and 60.186: Th e specificatio nfo

r monitorin g syste m drif t no t t o excee d2 percen t

o f spa n valu e whic hi s i nSubpart Pan d overlooke dinSubpart s Q an dRi s bein g added

. Inaddition , dry basi s measurement s of

th e SO 2 concentratio n ar e bein g specified

. Subpart s Db

. J , EE
. MM
. QQ

. RR, SS , TT
. WW , an dFF

Far e no t bein g amende da t

thi s time

. It

ha s bee n determine dtha t

Subpart s K

, Ka , HHH , JJJ, an dKK

K requir e n o amendments

. Thi s rulemakin g doe s no t impos e emissio nmeasuremen t

requirement s beyon dthos e specifie dinth e curren t regulations, no r

doe s i t chang e any . emissio nstandard

. Rather , th e rulemakin g woul dsimpl y clarif y an di n som e instance s ad daprocedur e associate dwithemissio nmeasuremen t or proces s monitorin g requirement s that woul dappl y irrespectiv e O f thi s rulemaking

. H
. Publi c Participatio n Th e amendment s wer e propose din th e Federa l Register

o n February 19 , 198 8 (53.F R5082)

. T o provid e intereste d person s tiie opportunity fo r ora l presentatio n of

data , views , o r argument s concernin g th e propose d amendments , apubli c hearin g wa s schedule dfo

r Apri l 4,1988 , a t

th e ". Researc hTriangl e Park

. Nort hCarolina , bu t wa s not-held-.becaus e n o on e wishe d t o mak e a nora l presentation

. Th e publi c comment perio dwa s fro

mFebruary 19 , 1988 , t o Ma

y 4,1988

. Thre e commen t , letter s wer e received..

. . III
. Significant

Comment s an dChange s t o th e Propose dAmendment s Th e thre e comment

letter s o nth e . propose damendment s wer e from industr y an dautility ad

hoc group , an d al l comment s concerne donl y § 60.8 , Subpart D (Fossil-Fue l Fire dSteam Generators) , an dSubpar t D a(Electri c Utilit y SteamGeneratin g Units)

. Ther e wer e ndcomment s o nth e amendment s mad e t o th e othe r

3 9 subparts

. Al l thre e commenter s objecte dt o th e withdrawa l of

Method s 6A an d6

B primaril y becaus e n o clea r justificatio n wa s given

. Th e primary reaso nfor th e propose dwithdrawa l of

Method s 6A an d6 B fo r emissio nperformanc e test s an dcontinuou s monitorin g relativ e accurac y test s i s du e t o th e slightl y greate r variabilit y of

th e F c 

### facto r

tha n th e F d

### facto r

( 6 percen t

vs . 3 percent)

. Bot hMethod s 6A an d6

B ar e base do n th e F c 

### factor

. Th e firs t commente r

suggeste dtha t

i f th e differenc e betwee nth e F c 

### an dF d 

### factor s wa s of

concern, ultimat e analysi s of

coa l sample s coul db e use d t o prov e th e appropriatenes s o f th e F c 

### factor

. After

considerin g th e commenter' s suggestion , EP A ha s decide dt o allo w th e us e of Method s 6

A an d6 B a s alternativ e method s withon e restriction

. I

f th e averag e F c 

### facto r

in Metho d1 9 i s use dan dwhe nth e emissio nrat e i s from0^9

7 t o 1.0 0 o f th e emissio nstandar do r

th e relativ e accurac y i s fro

m1 7 an d20 percent , the n achec k of th e acceptabilit y of

th e F c 

### facto r i s made

. Thi s sam e commente r

suggeste dtha t Metho d8 an dMetiio d7D b e designate d a s alternative s t o Metho d6
. I nsectio n 2. 1 o f Metho d6 , Metho d8 i s designate d a s a nacceptabl e alternativ e t o Metho d6 provide dtha t

aheate dfilter

i s place d betwee nth e prob e an disopropano l impinge n Sinc e thi s applie s t o whereve r Metho d6 i s used , i t

i s unnecessar y t o repea t it s acceptabilit y a s a nalternativ e in§ 60.46(d)(3)

. Metho d7D canno t b e adde dwithou t

goin g throug hth e rulemakin g process . Th e Agenc y plan s t o conside r

thi s actio ni nth e nea r

future

. Th e secon dcommente r

State dtha t

th e propose damendmen t

t o § 60.8(e)(1 ) could , b e mad e cleare r

b y referencin g appropriat e section s of

Metho d1

. Th e Agenc y feel s tha t

paragrap h(e)(l)(i)

. whic hstate s "constructin g th e ai r pollutio ncontro l syste msuc htha t volumetri c flow rate s an dpollutan t emissio nrate s ca nb e accuratel y determine db y applicabl e tes t method s an dprocedures, " i s sufficientl y clea r t o giv e th e necessar y intent

. Inth e cas e o f , : 

### particulat e matter , Method s 1,2 , an d5 ar e th e applicabl e procedures , whic h contai ncriteri aan dprocedure s fo r

. ensurin g tha t

measurement s of

flo w ari d emissio nrate s ar e accurate
. Th e Agenc y agree s tha t

paragrap h(e)(1)(H

) coul db e

, mad e clearer

. It

ha s bee nrevise da s follows : "providin g astac k o r duc t fre e o f cycloni c flo w durin g performanc e tests , a s demonstrate db y applicabl e tes t method s an dprocedures. " : 

### Thi s sam e commente r suggeste dtha t § 60.45(f ) ca nb e shortene db y referencin g sectio n3 of

Metho d19

. Th e Agenc y agree s an dplan s t o revis e thi s paragrap hunde r

aseparat e action

. Thi s commente r

als o aske dwhethe r th e expression s "Th e owne r o r operato r ma y use " an d"a t

th e sol e discretio nof th e owne r an doperator " hav e th e sam e impac t t o EPA

. Bot

hexpression s mea n th e sam e thing

. Onl y th e sourc e owne r p r operato r ma y choos e t o us e th e alternativ e method s for

determinin g compliance

. However , i t

doe s no t mea n tha t onl y th e owne r

o r operato r ma y us e th e alternativ e methods

. Alternativ e method s ar e thos e tha t

hav e bee n show nt o produc e result s adequat e fo r determinin g complianc e an dmay hav e n o bias , apositiv e bias , o r aslightl y negativ e bias

. Th e inten t

o f suc h expressio nwa s t o indicat e tha t contro l agencies shoul dno t

mandat e th e us e of alternativ e method s i

f th e owne r

o r operato r choose s no t

t o us e them

. However , th e alternativ e statu s doe s no t preclud e th e contro l agenc y fromusin g th e metho dfo

r complianc e purposes ; it onl y mean s tha t

a nagenc y mus t conside r positiv e biases , if

an y (som e alternativ e method s hav e bee nshow n no t t o exhibi t

an y bias) , whe nusin g alternativ e methods

. Th e secon dcommente r

suggeste dtha t referenc e t o § 60.4 6 i n§ § 60. a(c)(4 ) an d (d)(1 ) b e deleted

. Th e referenc e wa s mad e t o § 60.4 6 t o indicat e tha t onl y F d 

### factor s shoul db e used

. However , with th e change s allowin g th e us e of tiie F c 

### factors , th e referenc e ha s bee ndeleted

. Thi s sam e commente r

state dtha t

th e first equatio ni n§ 60:43a(h)(2 ) ha s n o meanin g an dtherefor e i s unnecessary . Th e EP A realize s tha t

th e first equatio n woul dno t b e applicable

. Th e equatio n wa s include dt o satisf

y th e requirement s o f sectio n111(a

) o f th e CleanAi r

Act , a s amended

. Two o f th e commenter s pointe dou t severa l typesettin g errors . Thes e hav e bee nnoted

. A s aresul t

of an . EP A interna l review , th e propose dadditio nof

aminimum samplin g tim e of

120 minute s t o § § 60.386(b)(3 ) an d60.675(b)(3 ) ha s bee n rescinde dbecaus e a naveragin g tim e wa s riot considere dessentia l fo

r determinin g complianc e i nthes e subparts

. IV
. Administrative.

. A. Docket Th e docke t

i s a norganize dan d complet e file of

al l th e informatio n submitte dt o o r

otherwis e considere d EP A ir i th e developmen t

o f thi s rulemaking

. Th e docke t

i s adynami cP. 5

666 2 Federa l Registe r/ Vol . 54 , No . 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an d Regulation s file, sinc e materia l i s adde d throughou t th e rulemakin g development . Th e docketin g syste m i s intende d t o allo w member s o f

th e publi can d industrie s involve d t o identif

y readil y an d locat e document s s o the y ca n effectivel y participat e i n th e rulemakin g process . Alon g wit h di e statemen to f basi s an d purpos e o f

th e propose d an d promulgate d rule , an d EP A response s t o significan tcomments , th e content s o f th e docket , excep tfo rinteragenc y revie wmaterials , wil l serv e a s th e recor d i n cas e o f

judicia l revie w(Clea n Ai rAct , sectio n 307(d)(7)(A)) . B. Off ice of Management

and Budget Reviews Unde rExecutiv e Orde r12291 , EP A i s require d t o judg e whethe raregulatio n i s a"majo rrule " and , therefore , subjec tt o di e requirement s o f

aregulator y impac t analysis . Th e Agenc y ha s determine d tha tthi s regulatio n woul d resul ti n non e o f th e advers e economi ceffect s se tfort h i n sectio n 1 o f

th e Orde ra s ground s fo r findin g aregulatio n t o b e a"majo rrule. " Th e rulemakin g doe s no timpos e emissio n measuremen trequirement s beyon d thos e specifie d i n th e curren t regulations , bu tinstead , provide s simplificatio n an d clarificatio n i n th e tes tmethod s an d procedure s section s o f th e regulatio n tha twoul d appl y irrespectiv e o f

thi s rulemaking . Th e Agenc y has , therefore , conclude d tha t this regulatio n i s no ta"majo rrule " unde rExecutiv e Orde r12291 . A s require d b y Executiv e Orde r12291 , thi s Fina l Rul e ha s bee n reviewe d b y th e Offic e o f Managemen tan d Budge t (OMB) . An y writte n OMB comment s t o EP A an d EPA' s respons e t o thes e comment s wil l b e availabl e fo r inspectio n i n th e publi cdocke tfo rthis rulemaking . C. Regulatory Flexibility Act Compliance Th e Regulator y Flexibilit y Ac t(RFA ) o f 198 0 require s th e identificatio n o f potentiall y advers e impact s o f Federa l regulation s upo n smal l busines s entities . Th e Ac tspecificall y require s th e completio n o f

a n RFA i n thos e instance s wher e smal l busines s impact s ar e possible . Becaus e this rulemakin g impose s n o advers e economi cimpacts , a n RFA ha s no tbee n conducted . Pursuan tt o th e provision s o f 5 U.S.C . 605(b) , I hereb y certif

y tha tthi s promulgate d rul e wil l no thav e an y economi cimpac to n smal l entitie s becaus e n o change s ar e bein g mad e l o testin g requirements . Lis to f Subject s i n 4 0 CF

RPar t6 0 Ai rpollution . Electri cutilit y stea m generatin g units , Ga s turbines , • Incinerators , Incorporatio n b y reference , Intergovernmenta l relations , Phosphat e fertilizer , Portlan d cemen tplants , Primary coppe rsmelters , Primary lea d smelters . Primary zin csmelters . Reportin g an d recordkeepin g requirements , an d Woo l fiberglass insulation . Date : Februar

y 2,1989 . Jac kMoore, . Acting Administrator. ' . . 4 0 CF RPart6 0 i s amende d a s follows : PAR T60—[AMENDED ] 1 . Th e authorit y citatio n fo rPart6 0 continue s t o rea d a s follows : Authority : Section s 101 , 111 , 114,116 , and 30 1 o f the Clea n AirAct, a s amended (4

2 U.S.C . 7401 , 7411 , 7414, 7416, an d 7601) . §60. 2 [Amended ] 2 . Sectio n 60. 2 (Subpar tA ) i s amende d b y revisin g th e definitio n o f "Referenc e method " to read , '"Referenc e method ' mean s an y metho d o f

samplin g an d analyzin g fo ra n ai rpollutan ta s specifie d i n th e applicabl e subpart. " §60. 8 [Amended ] 3 . I n § 60.8(b) , th e firs tsentenc e i s amende d b y removin g th e wor d "on " befor e th e numbe r"(4)" , revisin g th e perio d a tth e en d o f

th e sentenc e t o a comma , an d b y addin g th e followin g phrase , t o rea d a s follows : (b ) * * * o r(5 ) approve s shorte r samplin g time s an d smalle rsampl e volume s whe n necessitate d b y proces s variable s o rothe rfactors . 4 . Sectio n 60. 8 i s amende d b y addin g th e followin g sentenc e t o th e en d o f paragrap h (e)(1 ) t o rea d a s follows : (e ) * * * (1 ) * * * Thi s include s (i ) constructin g th e ai rpollutio n contro l syste m suc h tha tvolumetri cflo w rate s an d pollutan temissio n rate s ca n b e accuratel y determine d b y applicabl e tes t method s an d procedure s an d (ii ) providin g astac ko rduc tfree o f cycloni c flo wdurin g performanc e tests , a s demonstrate d b y applicabl e tes t method s an d procedures . §60.4 5 (Amended ] 5 . Sectio n 60.45(c)(1 ) i s revise d t o rea d a s follows : (c ) * * * (1 ) Method s 6 , 7 , an d 3 , a s applicable , shal l b e use d fo rth e performanc e evaluation s o f

sulfu rdioxid e an d nitroge n oxide s continuou s monitorin g systems . Acceptabl e alternativ e method s fo rMethod s 6 , 7 , an d 3 ar e give n i n § 60.46(d) . 6 . I n § 60.45(f)(3) , di e word s "paragrap h (d) " ar e revise d t o rea d "paragrap h (a)" . 7 . Sectio n 60.4 6 i s revise d t o rea d a s follows : • " § 60.4 6 Tes tmethod s an d procedures. ' (a ) In conductin g th e performanc e test s require d i n § 60.8 , th e owne ro r operato rshal l us e a s referenc e method s an d procedure s th e tes tmethod s i n Appendi x A o f

thi s par to rothe r method s an d procedure s a s specifie d i n thi s section , excep ta s provide d i n § 60.8(b) . Acceptabl e alternativ e method s an d procedure s ar e give n i n paragrap h (d ) o f

thi s section . (b ) Th e owne ro roperato rshal l determin e complianc e wit h th e particulat e matter , SO2 , an d NO , standard s i n §§60.42 , 60.43 , an d 60.4 4 a s follows : (1 ) Th e emissio n rat e (E ) o f particulat e matter , SOi , o rNO , shal l b e compute d fo reac h ru n usin g th e followin g equation : E=CF d(20.9)/(20.9- % O. ) E = emissio n rat

e o f pollutant, ng/

J (lb / million Btu) . C = concentration o

f pollutant, ng/dscm (lb / dscf) . %0 2 = oxyge n concentration , percen tdr y basis . F d= factora s determined fro m Metho d 19 . (2 ) Metho d 5 shal l b e use d t o determin e th e particula rmatte r concentratio n (C ) a taffecte d facilitie s withou twe tflue-gas-desulfurizatio n (FGD ) system s an d Metho d 5B shal l b e use d t o determin e di e particulat e matte r concentratio n (C ) afte rFGD systems . (i ) Th e samplin g tim e an d sampl e volum e fo reac h run shal l b e a tleas t6 0 minute s an d 0.8 5 dsc m (3 0 dscf) . Th e prob e an d filte rholde rheatin g system s i n th e samplin g trai n ma y b e se tt o provid e aga s temperatur e n o greate r tha n 160±1 4 ° C (320±2 5 °F) . (ii ) The . emissio n rat e correctio n factor , integrate d o rgra b samplin g an d analysi s procedur e o f

Metho d 3 shal l b e use d t o determin e th e O 2 concentratio n (%0 2 ) . Th e O

2 sampl e shal l b e obtaine d simultaneousl y with , an d a tth e sam e travers e point s as , th e particulat e sample . I

f th e gra b samplin g procedur e i s used , th e O2 concentratio n fo rth e run shal l b e th e arithmeti cmea n o f al l th e individua l O

2 sampl e concentration s a t eac h travers e point . (iii ) I f th e particulat e run ha s mor e tha n 1 2 travers e points , th e O j travers e point s ma y b e reduce d t o 1 2 provide d tha tMetho d 1 i s use d t o locat e th e 1 2 O 2 travers e points . (3 ) Medio d 9 an d di e procedure s i n § 60.1 1 shal l b e use d t o determin e opacity . (4 ) Metho d 6 shal l b e use d t o determin e th e SO 2 concentration .P. 6

(i ) Th e samplin g sit e shal l b e th e sam e a s tha tselecte d fo rth e particulat e sample . Th e samplin g locatio n i n th e duc tshal l b e a tth e centroi d o f th e cros s sectio n o ra tapoin tn o close rt o th e wall s tha n 1 m (3.2 8 ft) . Th e samplin g tim e an d sampl e volum e fo reac h sampl e run shal l b e a tleas t2 0 minutes . an d 0.02 0 dsc m (0.7 1 dscf) . Tw o sample s shal l b e take n durin g a1-hou rperiod , wit h eac h sampl e take n withi n a30 - minut e interval . (ii ) Th e emissio n rat e correctio n factor , integrate d samplin g an d analysi s procedur e o f

Metho d 3 shal l b e use d t o determin e th e O

j concentratio n (%Oi) . Th e O 2 sampl e shal l b e take n simultaneousl y with , an d a tth e sam e poin tas , th e SQ» sample . Th e SO2 emissio n rat e shal l b e compute d fo r eac h pai ro f

SO 2 an d O

z samples . Th e SO 2 emissio n rat e (E) fo reac h run shal l b e di e aridimeti cmea n o f th e result s o f di e tw o pair s o f

samples . (5 ) Metho d 7 shal l b e use d to determin e th e NO „ concentration . (i ) Th e samplin g sit e an d locatio n shal l b e th e sam e a s fo rth e SO 2 sample . Eac h ru n shal l consis to f fou rgra b samples , wit h eac h sampl e take n a t abou t15-minut e intervals . (ii ) Fo reac h NO z sample , th e emissio n rat e correctio n factor , gra b samplin g an d analysi s procedur e o f

Metho d 3 shal l b e use d t o determin e th e O 2 concentratio n (%02) . Th e sampl e shal l b e take n simultaneousl y with , an d a tth e sam e poin tas , th e NO „ sample . (iii ) Th e NO „ emissio n rat e shal l b e compute d fo reac h pai ro f NO , an d O i samples . Th e NO , emissio n rat e (E) fo r eac h run shal l b e th e arithmeti cmea n o f th e result s o f

th e fou rpair s o f

samples . (c ) Whe n combination s o f fossi l fuel s o rfossi l fue l an d woo d residu e ar e fired , th e owne ro roperato r(i n orde rt o comput e th e prorate d standar d a s show n i n § § 60.43(b ) an d 60.44(b) ) shal l determin e th e percentag e (w , x . y , o rz )

. o f th e tota l hea tinpu tderive d from eac h typ e o f fue l a s follows : (1 ) Th e hea tinpu trat e o f eac h fue l shal l b e determine d b y multiplyin g th e gros s calorifi cvalu e o f

eac h fue l fire d b y th e rat e o f

eac h fue l burned . (2 ) AST M Mediod s D 2015-7 7 (soli d fuels) , D 240-7 6 (liqui d fuels) , o rD 1826 - 7 7 (gaseou s fuels ) (incorporate d b y reference—se e § 60.17 ) shal l b e use d t o determin e th e gros s calorifi cvalue s o f th e fuels . Th e metho d use d t o determin e th e calorifi cvalu e o f

woo d residu e mus t b e approve d b y th e Adrhinistrator . (3 ) Suitabl e method s shal l b e use d t o determin e th e rat e o f

eac h fue l burne d durin g eac h tes tperiod , an d amateria l balanc e ove rdi e stea m generatin g syste m shal l b e use d t o confirm th e rate . (d ) Th e owne ro roperato rma y us e th e followin g a s alternative s t o th e referenc e mediod s an d procedure s i n thi s sectio n o ri n othe rsection s a s specified : (1 ) Th e emissio n rat e (E) o f particulat e matter , SO 2 an d NO Kma y b e determine d b y usin g th e F cfactor , provide d tha tth e followin g procedur e i s used : (i ) Th e emissio n rat e (E) shal l b e compute d usin g th e followin g equation : E=CF c (100/%CO2 ) where : E=emissio n rat

e o f pollutant, ng/

J (lb/millio n Btu) . C=concentr e tion of

pollutant, hg/dsc m (lb / dscf) - %COi=carbon dioxid e concentration , percentdr

y basis . F c =facto ra s determined in appropriat e section s o f Metho d 19 . (ii ) I f an d onl y i f

th e averag e F cfacto r i n Metho d 1 9 i s use d t o calculat e E an d eitiie rE i s fro m 0.9 7 t o 1.0 0 o f th e emissio n standar d o rth e relativ e accurac y o f

acontinuou s emissio n monitorin g syste m i s from 1 7 t o 2 0 percent , the n thre e run s o f Medio d 3 shal l b e use d t o determin e di e O 2 an d CO 2 concentratio n accordin g t o th e procedure s i n paragrap h (b ) (2)(ii) , (4)(ii) , o r(5)(ii ) o f

thi s section . The n i f

F 0 (averag e o f

thre e runs) , a s calculate d fro m di e equatio n i n Metho d 3 , i s mor e tha n ± 3 percen ttha n tiie averag e F o value , a s determine d fro m di e averag e value s o f F dan d F ci n Metho d 19 , i.e. , F M =0.20 9 (Fda/FJ , the n th e followin g procedur e shal l b e followed : (A ) Whe n F 0 i s les s tha n 0.9 7 F oa , the n E shal l b e increase d b y tiiatproportio n unde r0.9 7 Foa

, e.g. , if F 0 i s 0.9 5 F oa , E shal l b e increase d b y 2 percent . Thi s recalculate d valu e shal l b e use d t o determin e complianc e with.th e emissio n standard . (B ) Whe n F

„ i s les s tha n 0.9 7 F Man d whe n th e averag e differenc e (3 ) betwee n th e continuou s monito rminu s th e referenc e mediod s i s negative , the n E shal l b e increase d b y tha tproportio n unde r0.9 7 Foa

, e.g. , if F 0 i s 0.9 5 F oa , E shal l b e increase d b y 2 percent . Thi s recalculate d valu e shal l b e use d t o determine.complianc e wit h th e relativ e accurac y specification . (C ) Whe n F

„ i s greate rtha n 1.03 F O T an d whe n th e averag e differenc e 3 i s

. positive , the n E shal l b e decrease d b y tha tproportio n ove r1.03 F oa , e.g. , if F 0 i s 1.05 !?„ „ E shal l b e decrease d b y 2 percent . Thi s recalculate d valu e shal l b e use d t o determin e complianc e wit h th e relativ e accurac y specification . (2 ) Fo rMetho d 5 o r5B , Metho d 1 7 ma y b e use d a tfacilitie s wit h o rwithou t we tFG D system s i f

th e stac kga s temperatur e a tth e samplin g locatio n doe s no texcee d a n averag e temperatur e o f 16 0 ° C (32 0 °F) . Th e procedure s o f section s 2. 1 an d 2. 3 o f

Metho d 5B ma y b e use d wit h Metho d 1 7 onl y i f i ti s use d afte rwe tFG D systems . Metho d 1 7 shal l no tb e use d afte rwe tFGD system s i f th e effluen tga s i s saturate d o rlade n wit h . wate rdroplets . (3 ) Particulat e matte ran d S0 2ma y b e determine d simultaneousl y wit h th e Metho d 5 trai n provide d tha tth e followin g change s ar e made : (i ) Th e filteran d impinge rapparatu s i n section s 2.1. 5 an d 2.1. 6 o f Metho d 8 i s use d i n plac e o f

th e condense r(sectio n 2.1.7 ) o f Metho d 5 . (ii ) Al l applicabl e procedure s i n Metho d 8 fo rth e determinatio n o f SO2 (includin g moisture ) ar e used : (4 ) Fo rMetho d 6 , Metho d 6 C ma y b e used . Metho d 6 A ma y als o b e use d wheneve rMethod s 6 an d 3 dat aar e specifie d t o detennin e th e SO2 emissio n rate , unde rth e condition s i n paragrap h (d)(1 ) o f thi s section' . (5 ) Fo rMetho d 7 , Metho d 7A . 7C , 7D , o r7 E ma y b e used . If

Metho d 7C , 7D , o r 7E i s used , th e samplin g tim e fo reac h ru n shal l b e a tleas t1 hou ran d th e integrate d samplin g approac h shal l b e use d t o determin e th e O 2 concentratio n (%0-j) fo rth e emissio n rat e correctio n factor . (6 ) Fo rMetho d 3 , Metho d 3 A ma y b e used . § 60.43 a[Amended ] 8 . Sectio n 60.43a(h)(l ) i s amende d b y revisin g bot h equation s t o rea d a s follows : E1 = (340 X +52 0 y)/l0 0 and %P,=1 0 9 . Sectio n 60.43a(h)(2 ) i s amende d by : a . Revisin g bot h equation s t o rea d a s follows : E S =(340X+52 0 y)/l0 0 an d %P 0 =(10X+30y)/lO O b . Revisin g th e firstter m i n th e nomenclatur e lis tt o rea d "E," . c . Revisin g th e secon d term i n th e nomenclatur e lis tt o rea d a s follows : %V, i s the percentage of

potentia l sulfu r dioxid e emissio n allowed . § 60.44 a [Amended ] . 10 . Sectio n 60.44a(a)(l) . No xemissio n limit s table , i s amende d by : a . Addin g afootnot e "2 " t o th e en d o f th e fift h ite m unde r"Fuel type"immediatel y afte rth e wor d "furnace " t o rea d "furnace 2 " . b . Revisin g th e sixt h ite m unde r'Fue l type " t o rea d a s follows : An y fue l containin g mor e tha n 25% , b y weight , lignit e no tsubjec tt o th e 34 0 ng/ J hea tinpu temissio n limit 2
.P. 7



### 666 4 Federa l Registe r/ Vol . 54 . No . 2 9 /

Tuesday . Februar y 14 , 198 9 / Rule s an d Regulation s

cAdding afootnote "2 " atdi e end of the tabl e to read a s follows : * An y fue l containin g les s tha n 25% , b y

. weigh tlignit e i s no tprorate d bu tit s percentag e i s adde d t o th e percentag

e o f th e predominan

tfuel - 11 . Sectio n 60.44a(c) i s amended by : a. Revising the equatio n t o read a s follows : E„=[8 6 W+130 X +210y+26 0 z+34 0 v]/l0 0 b . Revising the firstter

m i n di e nomenclatur

e lis tto read "En". c . Movin g the word "and " a tdi e end of di e ter m "y " t o di e en d o

f di e ter m "z"an d adding di e definitio n of di e ter m "v " t o di e en d o f

di e nomenclature lis tto read a s follows : v i s th e percentag

e o f tota l hea tinpu t delivere d from th e combustio

n o f fuel s subjec tt o th e 34 0 ng/ | hea tinpu t standard . § 60.46 a [Amended ] 

### 12 . I n § 60.46a(d)(3) , the paragrap h reference "(i) " i s revise d t o read "(h)" . 13 . I n § 60.46a(h) , di e phras e "section s 6.0 and 7.0 o f

Reference Method 1 9 (Appendix A) " i s revise d t o read : "sectio n 7 o

f Method 19. " 14 . Sectio n 60.47

ai s amended b y revisin g paragraph

s (f) . (h) , (i) introductor

y text , and (i)(l) , and (i)(2) , and b y adding ane wparagrap h (j ) t o rea d a s follows : § 60.47 aEmissio

n monitoring

.

- (f ) Th e owne ro roperatorshall obtain emissio n dat

afo ra tleas t1 8 hour

s in a t leas t2 2 ou to f 3 0 successiv e boile r operating days . I

f dii s minimu

m dat a requiremen

tcannotb e me

twit h a continuous monitoring system , di e owne ro roperatorshall supplemen t emissio n dat

awit h othermonitoring system s approved b y the Administrator o rdi e reference method s and procedures a s describe d in paragrap h (h ) o f thi s section . (h ) Whe n itbecome s necessary t

o supplemen

tcontinuous monitorin

g system dat

at o meetdi e minimu

m dat a requirement

s in paragrap

h (f ) o f dii s section , di e owne ro

roperatorshal l us e di e referenc

e method s and procedures a s specifie d in thi s paragraph. Acceptabl e alternative method s and procedures ar

e given i n pargrap

h (j ) of thi s section . (1 ) Mediod 6 shall b e use d t o determine di e SO

j concentratio n atthe same locatio n a s di e SO

z monitor. Samples shal l b e taken at60-minut e intervals . The sampling tim e and sample volume foreac h sampl e shal l b e atleas t 2 0 minutes and 0.02

0 dsc m (0.7 1 dscf) . Eac

h sampl e represent

s a1-hou r average . (2 ) Mediod 7 shal l b e use d t o determine the NO , concentratio n atdi e sam e locatio n a s di e NO z 

### monitor. Samples shal l b e taken at30-minut e intervals . The arithmeticaverage o f tw o consecutiv e sample s represents a1-hou r average . (3 ) The emissio n rat

e correction factor, integrated bag sampling an d analysi s procedur

e o f Method 3 shal l b e use d t o determine di e O

2 o rCC s concentratio n atdi e sam e locatio n a s the O 2 o rCO 2 monitor. Sample s shall b e taken fora

tleas t30 minutes in eac h hour . Eac h sampl e represents a1-hou r average . (4 ) The procedures i n Medio d 1 9 shal l b e use d t o comput e each 1-hou

raverage concentration in ng/ ] (lb/millio n Btu ) heatinput. (i) The owne ro roperato rshall us e mediod s and procedures i n dii s paragrap h t o conductmonitoring syste m performanc

e evaluation s under § 60.13(ic ) and calibration check s unde r § 60.13(d) . Acceptabl e alternativ e method s and procedures are give n i n paragrap h (j ) of thi s section . (1 ) Methods 6,7 , and 3 , a s applicable , shall b e use d t

o determine O2

, SO2 , and NO , concentrations . (2 ) SO 2 o rNO , (NO) , a s applicable , shall b e use d fo

rpreparin g di e calibration ga s mixtures (in N2 , a s applicable ) unde

rPerformanc

e Specificatio n 2 o

f Appendix B o f

dii s part . **** * (j ) Th e owne ro roperato rma

y us e di e following a s alternative s t o di e reference methods and procedures specifie d in dii s section : (1 ) Fo rMethod 6, Method 6

A or6 B (wheneve rMediod s 6 and 3 dat aar e used ) o r6C ma y b e used . Eac

h Medio d 6 B sampl e obtaine d ove r2 4 hour s represent s 241-houraverages . I

f Method 6 A o r6 B i s use d unde

rparagrap

h (i ) o f dii s section , di e condition s under § 60.46(d)(1 ) apply ; thes e condition s d o notapply unde

rparagrap

h (h ) o f dii s section . (2 ) Fo rMethod 7

, Metiiod 7A , 7C , 7D , o r7 E ma y b e used . I

f Metiio d 7C, 7D , or 7 E i s used , the sampling tim e fo reach ru n shall b e 1 hour

. (3 ) Fo rMediod 3 , Mediod 3

A ma y b e use d i f di e sampling time i s 1 hour . 15 . Sectio n 60.48ai s amended by redesignating paragrap

h (d) a s paragrap h (f) . b y adding ane wparagra h (d) , and b y revisin g paragraphs (a) , (b) , (c) , and (e ) t

o rea d a s follows : § 60.48aComplianc e determinatio

n tes t methods an

d procedures . (a) I n conducting di e performance test s required in § 60.8 , th e owne ror operato rshal l us e a s reference method s and procedures di e method s in Appendix A o f

dii s par to rth e mediod s an d procedures a s specifie d i n dii s section , excep ta s provided in § 60.8(b) . Sectio n 60.8(f

) doe s no tapply t

o thi s - sectio n forSO

2 and NO, . Acceptabl e alternativ e method s ar

e give n in paragrap h (e ) o f thi s section . (b ) Th e owne rd

roperato rshal l determine compliance with di e particulat e matterstandard s i n § 60.42 a. a s follows : (1 ) The dr y basi s F facto r(Oi) procedures i n Medio d 1 9 shal l b e use d t o comput e di e emissio n rat

e o f particulat e matter . (2 ) Fo rdi e particularmatter concentration , Medio d 5 shall b e use d a t affecte d facilitie s withoutwe tFG D system s and Metho d 5

B shal l b e use d afterwe tFG

D systems . (i ) The sampling time an d sampl e volume foreac h ru

n shal l b e a

tleas t120 minutes an d 1.7

0 dscm (60 dscf) . The prob e and filterholde rheating syste m in the sampling train ma

y b e se tt o provide a n average ga s temperatur e of n o greatertiian 160±1 4 "

C (320±2 5 *F). (ii ) Fo reac h particulat

e run , di e emissio n rat

e correction factor, integrated or

. gra b sampling and analysi s procedures o

f Medio d 3 shal l b e use d t o determine di e O

2 concentration . The O

2 sampl e shal l b e obtaine d simultaneousl y with , and atdi e sam e travers e points as , the particulat

e run. I f di e particulat

e ru n ha s mor e tha n 1 2 travers e points , di e O 2 travers e points ma

y b e reduced t

o 1 2 provided tiiatMethod 1 i s use d t o locat e the 1 2 Oi travers e points . I f di e gra b sampling procedur

e i s used , di e O

a concentratio n fordi e ru

n shal l b e di e aridimeti cmean o

f al l di e individua

l O i concentration s ateac h travers e poin t (3) Mediod 9 an d di e procedures in § 60.1 1 shall b e use d to determine opacity . (c) The owne ro roperato rshal l determine compliance wid i th e SO i standard s i n § 60.43aa s follows : (1 ) The percento f

potential SO

2 emission s (%P

a 

### ) t o di e atmosphere shal l b e computed usin g the followin g equation : %P.=[(10O—%R

J (100—%RJ]/10

0 where : %P,=percen

tof potential SO , emissions , percen t %R,=percen

treduction fro

m fue l pretreatment

, percent. %R,=percen

treduction b y SOi contro l 6ystem , percent.P. 8

Federal ; Registe r/

Vol . 54-,, No . 2 9 /

Tuesday/, , Februar y 14, , 198 9 / Rule s aud i Regulation s (2 ) Th e procedure s in.Metho d 19.ma y be . use d t o detennin e percen treduction' (%Rf) i o f sulfu rh y such , processes , a s fue l pretreatment(physica l coa l cleaning, , hydrodesulfurization : o f fue l oil, , etc.), . coaL pulverizers, , an d bottom : an d flyas h interactions. . Thi s determin atio n is s optioaa L (3 ) Th e procedure s i h Metho d 19 . shal l b e use d tO'determin e th e percen tSO * reductio n (%Rao f

an y SO i control , system . Alternatively, , a. combination , o f a n "a s fired " fue l monito ran d emissio n rate s measure d afte rdi e contro l system , .following ^ th e procedures ; ir o Medio d 1S\ ma y b e use d i f

the percen treduction ; is ; : calculate d using:m e averag e emissio n rat e from tile SO i control 1 device * and 1 th e averag e SO i inpu trat e from.di e "a s fired" fue l analysis - for30 ' successiv e boile roperating , days . (4 ) Th e appropriat e procedures , i h Metho d 1 9 shal l b e use d t o determin e th e emissio n rate . (5 ) Th e continuou s monitoring ; syste m i n § 60.47 a(b ) an d (d ) shall ) be : use d to) determin e di e concentrations ; o f SOi-an d CO-or02 . (d ) Th e owne ro roperato rshal l determin e complianc e with 1 th e NO, , standar d i n § 60.44 aa s follows : (1 ) Th e appropriat e procedure s i n Method'1 9 shall'B e use d t o determine , th e emissio n rat e o f

NO „ (2 ) Th e continou s monitoring ; system , i n § 60;47 a(c ) an d (d ) shal l b e use d t o determin e th e concentration s o f NO, , an d CO i o rOi . (e ) Theowne ro roperato rma y use : th e followin g as . alternative s t o die ; reference , mediods : an d procedures , specified : ih : diis ; section: : (1 ) Fo rMetho d 5 or5Bi . Method ! 1 7 ma y b e used : a tfacilities ; with ; o rwithou t we tFG Psystem s i f

me : stac k temperatur e at : th e samplin g location : does;not:excee d a n averag e temperature : o f 16 0 ° C (320'-F)l.The : procedures : o f §§2. 1 an d 2J'o f

Method . 5 E ma y b e use d i n Medio d 1 7 onl y i f

i ti s use d afte rwe t FG D systems . Method ; 1 7 shal l no tb e use d afte rwe tFGD systems;if - die ; effluent'i s saturate d o rlade n wit h wate r droplets: . (2 ) Th e F cfacto r(CO2) , procedure s i n Metho d 1 9 ma y b e use d t o compute , di e emissio n rat e o f

particulat e matte r unde rdi e stipulation s o f § 60.46(d)(1) . Th e COi . shal l b e determine d i n th e -same.manne ra s th e Ou.concentration i

* - * * • * *

. 16 . Sectio n 60.5 4 i s revise d f o read'a s follows : § 60.5 4 Tes tmethod s an d procedures , (ai) . In. conducting : th e performanc e test s require d i n § 60.8, , th e owne ro r operato rshal l us e a s referenc e method s and . procedures - the . tes tmethod s in . Appendi x A o f tiiiapar to rothe r method s an d procedures , a s specifie d i n

. thi s section, , excep tas . provide d i n (b ) Th e owne ro roper ato rshal l determine : compliance : with ; th e particulat e matte rstandar d i n §. 60.52 : a * follows t (1 ) The-emtssibn'rat e few^o f particulate - matter ; corrected ' to' 12 ' percen tCQ2 , shal l It e computed 1 fo reac h run using;di e fottbmh g equatibn r c, j = c „ (i2/%Goy ; where : c u = concentration o

f particulat

e matter,, corrected t

o 1 2 percen

tCO2 , g/d'sc m (gr / dscf) . c„=concentratio n o

f particulat

e matter,, g/ ' dscm . (gr/dscf}. . %COr =CO j concentration , percen tdr y basis . (2] : Metiiod'5"8hallbeusedt o determin e the . particulat e matte r concentratio n (cj . Th e sampling , time , an d sampl e volum e fo reac h ru ashal l be a tleas t6 0 minute s and.0.8 5 dsc m (3 0 dscf): . (3 ) Th e emissio n rat acorrectio n factor ; integrate d o rgrab-samplin g and : analysis;procedur e o f

Metho d 3 shall , be . use d to . determine : CO

2 concentration ; (%C02 ) i (i ) Th e CO

2 sampl e shal l b e obtaine d simultaneousl y with , an d a tdie . same , travers e points , as , die : particulate , run . If th e particulat e ru n ha s more . than . 1 2 travers e points * the CO2 . travers e point s ma y b e reduced ; t o 1 2 if Metho d 1 i s use d to locat e th e 12.CO* . traverse-points, . I f individual . CO2' . samples.ar e take n a t eac h traverse , point, , th e CO s concentration . (,%C02) ; use d i n th e correctio n equatio n shal l b e th e arithmeti cmean , o f

all , th e individua l CO 2 sampl e concentrations ; a teac h traverse , point- . (ii. ) I f samplin g i s conducte d afte ra we tscrubber. , an . "adjusted;'CO i concentr ation . [(^CGsJadiJi. which , account s fo rth e effectso f CO 2 absorptio n and . dilution , air * ma y b e use d instea d o f

th e GO2 . concentration , determine d i n thisparagraph.The adjuste d COr. concentration ; shal l b e determine d b y eithe ro f the:procedure s i n paragraph 1 (c) , o f

this . section . (c)'Th e owne ro roperato rmay-us e eithero f die;following:procedure s to' determin e th e adjuste d CO 2 . concentration: . (iliJ'The : volumetri'c.flbw/rates:af cthe : inlet , and . outle to f

die 1 we tscrubbe rand ; th e inle tCX)i

. concentration'ma y b e used i t o determin e th e adjuste d CO 2 concentratio n [(%C02) wU ] , usin g th e followin g equation : (%C0 2 U=(,%C02ta(.Q.i/Q U where: ; (^COJ^^djuste d outletCO concentration!,.percentdry ' baais. . (%GOa)

dl =CO i concentration . measured . before-the.scrubber ; percen tdr y basis . Q di=volumetri cflowrat

e of ; effluen tgas : befor e the we tscrubber ; dscm/'mi h (dscf/inin) . Qdo=volumetric

ffow rahrof

effluentgps afterthe we tscrubber, dscm/min'(dsef / imin) l (j) : At > th e outle tMetiiod i 5 i s use d to , determin e di e volumetri cflo wrat aQQio) ; of , th e effluen tgas . (iii) ; At l di e inlet . Metho d 2 . is : use d to ; determin e ths : volumetri cflowrate : (Qj,,) . o f th e effluen tga s a s follows: . Tw o ful l velocit y traverse s ar e conducted , on e immediatel y befor e an d on e immediately ; afte reach 1 particulate : ru n conducted : at

- die . outlet, , and . th e result s ar e averaged . (iii)f At : the : inlet , the : emission ; rate correctio n factor , integrated - samplin g and 1 analysis - procedure - o f Method ! 3

- i s use d t o determin e th e CO 2 concentration , [CftCOiJu

] a s follbws : A tleas tnin e samplin g points ' are - selected 1 randomly , from th e velbcitytravers e point' s an d are divide d randoml y into ; three - sets' , equal ' i n numbe ro f

points ^ th e first'seto f

three : o rmore - point s is - use d fo rth e firs trun ; th e second'se tfo rth e secon d run, , an d th e third se tfo rth e tiii'rd run . Th e C0 2 sample-i s take n simultaneously-wit h eac h particulat e run . being , conducte d a t the . outlet , b y traversing , th e three , samplin g point s (o rmore ) and : sampling , a teach , poin tfo requa l increment s o f time . (2)1 Excess,ai rmeasurements.mayb e use d to determin e theadjustiediGO j concentratio n [(%C02) at u ] usin g the 1 following : equation : (%C02) adj =(%C02) a i [(100+%EAi)/ (100+%EAo

) ] where : (%eOj).,u=adjusted outletCO i concentration ; percent 1 dry-basis : (%COj)i,=CO

i concentration - a tm e inleto f the wet'scrubber : percen

tdr y basis . %EA , = exces s ai rat ' the inleto f th e scrubber; . percent. %EA„.=exce8s-.ai

rat.the:outlet:of

the scrubber, , percent . (i j A ga s sampl e i s collecte d a s ihparagrap h (e)P)(iiO.'o f

thi s sectio n and ! th e ga s sample s a tbot h th e inle tand ' outle tlocation s ar e analyzed , fo rCOi, . O2 , an d N 2 . (ii ) Equatio n 3- 1 o f

Metho d 3 i s use d to compute , th e percentages , o f excess , ai r a tthe : inle tan d outlet : o f th e we t scrubber . 17 . Section'60.6 4 is,revised - t o rea d a s follows :

1 —1 if——--
- --^ ^P. 9

666 6 Federa l Registe r / Vol

. 54

. No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s § 60.6 4 Tes t

method s an dprocedures

. (a ) I nconductin g th e performanc e test s require di n§ 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r shal l determin e complianc e wit hth e particulat e matte r

standar di n§ 60.6 2 a s follows : (1 ) Th e emissio nrat e (E ) o f particulat e matte r shal l b e compute dfo r

eac hru n usin g th e followin g equation : E={c.Q*)/(PK ) where : E=emissio n rat e o

f particulat e matter , kg / metri c to n(lb/ton ) o

f kil nfeed

. c,=concentratio n o

f particulat e matter , g / dsc m(g/dscf)

. Q K! =yolumetri c flow rat e o f effluen t gas , dscm/h r (dscf/hr)

. P=tota l kil nfeed(dr

y basis ) rate , metri c ton / hr (ton/hr). ' K=conversio n factor , 100 0 g/kg (453. 6 g/lb)

. (2 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentratio n(c. ) an dth e volumetri c flow rat e (O^ ) o f

th e effluen t

gas . Th e samplin g time an dsampl e volum e fo r eac hru nshal l b e a t

leas t 6 0 minute s an d0.8 5 dsc m(30. 0 dscf ) fo r th e kil n an d a t leas t 6 0 minute s an d1.1 5 dsc m(40. 6 dscf ) fo r th e clinke r

cooler

. (3 ) Suitabl e method s shal l b e use dt o determin e th e kil nfee drat e (P) , excep t fuels , fo r eac hrun . Materia l balanc e ove r th e productio nsyste mshal l b e use dt o confir mth e fee drate
. (4 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. (18 ) Sectio n60.73(a ) i s revise dt o rea d a s follows : § 60.7 3 Emissio n monitoring . (a ) Th e sourc e owne r

o r operato r shal l install , calibrate , maintain , an doperat e acontinuou s monitorin g syste mfo r measurin g nitroge noxide s (NO,)

. Th e pollutan t ga s mixture s unde r Performanc e Specificatio n2 an dfo r calibratio ncheck s unde r § 60.13(d ) o f thi s par t shal l b e nitroge ndioxid e (NOa)

. Th e spa nvalu e shal l b e 50 0 pp mo f NO2

. Metho d7 shal l b e use dfo r th e performanc e evaluation s unde r § 60.13(c)

. Acceptabl e alternativ e method s t o Metho d7 ar e give ni n § 60.74(c)

. **** * 19

. Sectio n60.73(b ) i s amende db y removin g th e wor d"short " whereve r i t occur s i nth e first

an dthir dsentences
. 20

. Sectio n60.7 4 i s revise dt o rea da s follows : § 60.7 4 Tes t method s an dprocedures

. (a ) I nconductin g th e performanc e test s require di n § 60.8 , th e owne r o r ' operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r - method s an dprocedure s a s specifie di n dii s section , excep t

a s provide di n § 60.8(b)

. Acceptabl e alternativ e method s an dprocedure s ar e give n i n paragrap h(c ) o f

thi s section

. (b ) Th e owne r

o r operato r shal l determin e complianc e wit hth e NO / standar di n§ 60.7 2 a s follows : (1 ) Th e emissio n rat e (E ) o f NO , shal l b e compute dfo r

eac hru n usin g th e followin g equation : E=(C.Q„,)/(PK ) where : E=emissio n rat e o

f NO , a s NO2

. kg/metri c to n(lb/ton ) o

f 10 0 percen t nitri c acid

. C,=concentratio n o

f NO , a s NOa

. g/dsc m (lb/dscf)

. Q sd =volumetri c flow rat e o f effluen t gas , dscm/h r (dscf/hr)

. P=aci dproductio n rate , metri c ton/h r (ton / hr) o r 10 0 percen t nitri c acid

. K=conversio nfactor , 100 0 g/kg (1. 0 lb/lb)

. (2 ) Metho d7 shal l b e use dt o determin e th e NO , concentratio n o f eac hgra b sample

. Metho d1 shal l b e use dt o selec t

di e samplin g site , an dth e samplin g poin t

shal l b e th e centroi do f th e stac k o r duc t o r a t apoin t n o close r t o th e wall s tha n 1 m(3.2 8 ft)

. Fou r gra b sample s shal l b e take na t approximatel y 15-minut e intervals

. Th e arithmeti c mea n o f th e fou r sampl e concentration s shal l constitut e th e ru n valu e (C,)

. (3 ) Metho d2 shal l b e use dt o determin e th e volumetri c flo w rat e (QKJ ) o f th e effluen t

gas . Th e measuremen t - sit e shal l b e th e sam e a s fo r th e NO , sample

. A velocit y travers e shal l b e mad e onc e pe r

ru n withi nth e hou r

tha t th e NO , sample s ar e taken

. (4 ) Th e method s o f

§ 60.73(c ) shal l b e use dt o determin e th e productio nrat e (P ) o f 10 0 percen t

nitri c aci dfo r

eac h run . Materia l balanc e ove r th e productio nsyste mshal l b e use dt o confir mth e productio nrate
. (c ) Th e owne r

o r operato r

ma y us e th e followin g a s alternative s t o di e referenc e method s an dprocedure s specifie di n thi s section : (1 ) Fo r Metho d7
. Metho d7A

. 7B , 7C

. o r 7 D ma y b e used

. I

f Metho d7 C o r

7 D i s used , th e samplin g tim e shal l b e a t leas t 1 hour

. (d ) Th e owne r

o r operato r shal l us e th e procedur e i n§ 60.73(b ) t o determin e th e conversio nfacto r

fo r convertin g di e monitorin g dat at o th e unit s o f th e standard

. § 60.8 4 [Amended ] 21

. I n § 60.84(a) , th e thir dsentenc e i s amende db y removin g th e wor d "Reference " befor e di e word s "Method s 8" ; an dth e fourt hsentenc e i s amende d b y addin g th e wor d"value " afte r th e wor d"span"

. 22

. I n§ 60.84(b) , th e firs t sentenc e an d definitio no f

C Fi n nomenclature , lis t ar e amende db y removin g th e wor d"short " befor e th e wor d"ton " i nth e tw o place s i t occurs . 23

. Sectio n 60.84(d ) i s amende db y revisin g th e equatio n an dnomenclatur e lis t t o rea da s follows : (d ) *

. * • E,=(C.S)/[0.265-(0.12 6 %Oi)-[A%CO-i)] where : E,=emissio n rat e o

f SO* , kg/metri c to n (lb / ton ) o f 10 0 percen t o f H 2 SO« produced

. C.=concentratio n o

f SO» , kg/dsc m(lb/dscf)

. S=aci dproductio n rat e factor , 36 8 dscm/ metri c to n (11,80

0 dscf/ton ) o

f 10 0 percen t H2SO 4 produced

. %0 2 =oxyge nconcentration , percen t dry basis

. A=auxiliar y fue

l factor

. =0.0 0 fo r n o fuel

. =0.022 6 fo

r methane

. =0.021 7 fo

r natura l gas . =0.019 6 fo

r propane . =0.017 2 fo

r N o 2 oil

. =0.016 1 fo

r N o 8 oil

. =0.014 8 fo

r coal

. =0.012 6 fo

r coke

. %C0 2 = carbo ndioxid e concentration , ' percen t dr y basis

.

* * • * * * 24

. Sectio n 60.8 5 i s revise dt o rea da s follows : § 60.8 5 Tes t method s an d procedures . (a ) I nconductin g di e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s di e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. Acceptabl e alternativ e method s an dprocedure s ar e give n i n paragrap h(c ) o f

thi s section

. (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hdi e SO 2 aci d mist , an dvisibl e emissio n standard s i n § § 60.8 2 aii d60.8 3 a s follows : (1 ) Th e emissio nrat e (E ) o f aci dmis t o r SO 2 shal l b e compute dfo r eac hru n usin g th e followin g equation : t F^fCCW/fPK ) where : E=emissio nrat e o

f aci dmisto r

SO 2 kg / metri c to n(lb/ton ) o

f 10 0 percen t H j S O 4 produced

. C=concentratio no

f aci dmis t o r SO a , g/dsc m (lb/dscf). . ..,•"• • Qsd=volumetri c flow rat e o f th e effluen

t gas, . dscm/h r (dscf/hr)

. P=productio n rat e o

f 10 0 percen t ILSO4 , metri c ton/h r

(ton/hr)

. K = conversio n factor , 100

0 g/kg (1: 0 lb/lb)

. (2 ) Metho d8 shal l b e use dt o determin e th e aci dmis t an dSO 2 concentration s (C's ) an dth e volumetri cP.1 0

Federa l Registe r

/ Vol.

. 54,

. No ; 29

< / ' Tuesday , Februar y 14 v 1989 ; / Rule s an dRegulation s 666 7 flo w rat e (Gjsd

) o f the

- effluen t

gas u Th e moistur e content ; ma y b e considered : to> b e zerc u Th e samplin g tim e an dsampl e volum e fo r

eac hnu nshal l be

. at
. leas t 6 0 minutes,affld)l.U 5 dsc m(40.6

. dscf) : (3: ) Suitabl e method s shal l b e used-

. to > determine : th e production , rat e (P ) o f WO i percen t H2SO4 fo r

eac hrun . Materia l balance , over , th e productio n syste m shall : b e used

. to

> confirm

- the

- production , rate
. (4)

. Method. 9 an dth e procedures ; in ; § 60.1 1 shal l b e used : to
. determin e opacity.

. (c)

. Th e owne r

o r operato r

ma y us e th e following , as . afterhatLv.es ; t o di e referenc e method' s an dprocedure s specifie di nthi s section : Clj i If asourc e processe s elementa l sulfu r o r arr or e tha t contain s elementa l sulfu r an duse s ai r

to suppl y oxygen; , th e followfiig , procedur e ma y b e use d instea do f

determinin g th e volumetri c flo w rat e an dproductio nrate : (j) ; The : integrate dtechnique

- o f Kferho d 3 i s use dt o determin e th e O i \ concentratio n and, , i f

required ; COi : concentration

. (ii ) Th e SO 2 o r

aci dmis t

emissio n rat e i s calculate da s describe di n § 60.84(d) , substitutin g th e aci dmis t concentratio n fo r C , a s appropriate

. 25

. Sectio n60.93

. i s revised't o read , as fofl'ovvs:

. §60:9 3 Tesi'metiiod s an dprocedures

. (a ) I nconductin g th e performanc e test s required 1 i n£60:8 , th e owne r o r operato r shal l us e a s referenc e medi o Js ' an dprocedures , the

. tes t method s in

. Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provided ' i h § 60.8fb) \ (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n § 60.9 2 a s follows : (1 ) Metho d5 shal l b e use dt o determine

- th e particulat e matte r concentration

. Th e sampling ' time and ' sampl e volume

- for ' eac hru nshall 1 b e a t leas t 6f f minute s an d0'.90 dsc m(31.8 ' dscf)

. (2 ) Method 1 9 1 and ' th e procedure s i n § 60.1 1 shal l be- use dt o determin e opacity

. 26

. Sectio n 60.123 1 is

- revise dt o rea da s follows: ' §60.12 3 Testmethods-an dprocedures.

. (ta)In i conducting : th e performanc e test s required ! nm§;60i8* ; th e owne r o r operato r shal l use : a s reference : methods : an dprocedure s th e tes t methods'i n Appendia aA of

i diis ? par t

o c otiie r methods : am i procedures : as : specified ! in : thi s section, , excep t

as ; provided : i

m § 60.8(b)

. (b ) Th e owne r o r operato r shal l determin e complianc e wit hth e particulat e matte r

standard s i

m§ 60:12 2 a s follows : (li ) Method 1 5 shall ' B e used ! t o determin e th e particulat e matter ' concentratio ndurin g representative , periods , of

. furnac e operation , includin g chargin g an dtapping

. Th e sampling- , tim e an dsampl e volum e fo r each

- run- , shal l b e a t leas t 6 0 minute s an d0.9 0 dsc m(31. 8 dscf)

. - (2 ) Method. 9 an dth e procedure s i n § 6U1 1 shalT.be

. use dt o determine , opacity.

. 27

. Sectio n 6O113 3 i s revise dt o rea da s follows:

. § 60.13 3 Tes t method s aficf procedures ; (a) ' I nconductin g performanc e test s require di n § 60.8 ; th e owne r Or

. operato r shal l us e a s referenc e method s and ' procedure s th e tes t

method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specified ' ih

. thi s section , excep t

a s provide di n §6U8(fc) l (b),Th e owne r

o r operator'shall , determin e complianc e with i th e particulate , matte r

standards : h i §'60;13 2 as . follows : (I) : Metho d5

^ shal l b e use dto ' determin e th e particulate

- matte r concentratio n durin g representativ e period s o f

chargin g an drefining, , but

. no t durin g pourin g o f

th e heat

. Th e samplin g tim e an dsampl e volum e fo r eac hrun shal l b e a t

leas t 120 1 minute s an d1.8 0 dsc mf83>. 8 dscf) : (2)' : Method 1 9 : an dth e procedure s in

- : § 60.11 ' shal l b e used'ro : determin e opacity

. §60.14 3 [Amended] ! 28

. I n § 6 9 J43(b)(S), , th e referenc e " § 60.13(bi)(a) V isirevisedt o read : " § 60.13(b)"

. 29

. I n§ 60.143(c) , th e reference s "(b)(1)(A ) o r

(b)(2)(A) " ar e revise dt o rea d"(b)(l)(i ) o r

(b)(2)(i)"

.

. 30

. Sectio n60.14 4 i s revise dt o rea da s follows : § 60.14 4 Tes t

method s an dprocedures

. (a ) I nconductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

tiifs par t

o r othe r mediod s and-procedure s a s specifie di n thi s section , excep t

a s provide dini

. § 60,8(:b);

. (ft) : Th e owne r

o r operato r shall ' determin e complianc e wit hth e particulat e matte r

standard s i n §'60.14 2 a s follows : (1) ! Th e time-measuring ' instrumen t o f § 60.14 3 shal l b e use dto : documen t the : time : and * duration i o f

eac hsteel ? productio n Gyel e an deach ' diversio n perio ddurin g eac hrun . (2) : Metho d5

- shaf

t b e use dto* determiiieth e particulat e matte r concentration ; Th e samplin g tim e and 1 sampl e volum e fo r

eac hrun ' shall

- b e a t least %® minutesan d1.50dsc m(53'dscf)

. Samplin g shal l be : discontinued 1 durin g period s o f

diversions

. (i ) For

- affected ' facilitie s that

commence dconstruction ; modification ; o r reconstructio n ©WO Tbefor e Januar y 2011983 ; thesamplin g for eac hrun-shal l continu e fbran i integral ' numbe r o f steel 1 production ' cycles'

. A cycl e shal l star t a t th e • beginnin g o f

either ' th e scrap s prehe at o r th e oxyge n blo w and 1 shal l terminate ' immediatel y before ' tapping : (ii ) Fo r affecte dfacHfties tha t commenced 1 construction , modification ; o r reecmsn-uctib n after-Januar y 20V1983 V th e sampl&ig'ro r

eac hran sftatf

continu e fo r a nintegral 5 numbe r

o f primar y oxyge n blows

- (3 ) Metho d9 and ' th e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity : Observation s take n durin g a diversio nperiod ! shall 1 no t b e use di n determining ' complianc e with

- th e opacit y standard'

. Opacit y observations

- take n a t 15-secon dintervals-immediatel y before : an dafte r adiversion

- o f

exhaust

- gase s fro mth e stac k

ma y b e considere dto-b e consecutiv e fo r

th e purpos e o f computin g an - averag e opacit y fo r a6- minute : period

. fc ) T o eompl y wit h§ 60;143(c) ; th e Owne r oroperatOrsha- n us e th e monitorin g device s o f

§ 60.143(b ) (1 ) and ! (2 ) durihgth e particulate : run s t o detennin e th e 3-hou r

average s o f

th e require dmeasurements. " 31

. Sectio n60.144 ai s amende db y redesignatin g paragraph s (d)(1) : an d(2 ) a s (c ) (1) : and 1 f2) : an db y revising ' paragraphs ' fa-)

i (b) „ (c) 1 mtroduefor y text , and * (d ) to' read : as : follows: § 60.144 aTes t

method s an dprocedures

. (a ) I nconductin g di e performanc e test s require di n§ 60.8 , th e ownero r operato r shal l us e a s referenc e method s and : procedure s th e test method s i n Appendi x A o f

this : par t

o r otiie r methods-and.procedure s a s specified 1 i n thi s section , excep t

as : provide di n § 60.8(b).

. (b ) The'ownero r

operato r

shaff i determin e compliance-with i tfie

particulat e mattter'standard s ih ' § 60:142 a a s follows : (1 ) Star t an den dtimes o f

each-stee l productio n cycl e durin g each

- run - shall ' b e recorded ' (se e f

60;145aC«J : an dfd) ! fo r th e definition s o f

star t and'entf

- time s o f acycle) ; (2) ! Metho d5 shafl i b e used 1 to determin e th e particulat e matter 1

.P.1 1

666 8 Federa l Registe r / Vol

. 54 , No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s concentration

. Samplin g shal l b e conducte donl y durin g th e stee l productio ncycl e an dfo r asufficien t numbe r o f stee l productio ncycle s t o obtai natota l sampl e volum e o f a t leas t 5.6 7 dsc m(20 0 dscf) fo r eac hrun . (3 ) Metho d9 an dth e procedure s o f § 60.1 1 shal l b e use dt o determiri e opacity , excep t

section s 2. 4 an d2. 5 o f Metho d9 shal l b e replace dwit hth e followin g instruction s fo r recordin g observation s an dreducin g data : {i ) Section 2.4. Opacit y observation s shal l b e recorde dt o th e neares t 5 percent..a t

15-secon dintervals

. Durin g th e initia l performanc e tes t conducte d pursuan t t o § 60.8 , observation s shal l b e mad e an drecorde di nthi s manne r fo r a minimu mo f

thre e stee l productio n cycles

. Durin g an y subsequen t Complianc e test , observation s ma y b e mad e fo r an y numbe r

o f stee l productio n cycles , although , wher e conditions

. permit , observation s wil l generall y b e ' : mad e fo r aminimu mo f

thre e stee l productio ncycles

. (ii ) Section 2.5. Opacit y shal l b e determine da s a naverag e o f 1 2 consecutiv e observation s recorde da t 15-secon dintervals

. Fo r eac hstee l productio ncycle , divid e th e observation s recorde dint o set s o f 1 2 consecutiv e observations

. Sets-nee dno t be

. consecutiv e i ntime , an di nn o cas e shal l tw o set s overlap

. Fo r eac hse t o f 1 2 observations , calculat e th e averag e b y summin g th e opacit y o f 1 2 consecutiv e observation s an ddividin g thi s su mb y 12

. (c ) I ncomplyin g wit hth e requirement s o f § 60.143a(c) , th e owne r o r operato r shal l conduc t

a ninitia l tes t

a s follows : • . *

. « * * (d ) T o compl y wit h§ 60.143 a(d ) o r (e)

. th e owne r

o r operato r shal l us e th e monitorin g devic e o f

§ 60.143a(a ) to , determin e th e exhaus t

ventilatio nrate s o r level s durin g th e particulat e matte r run s an dt o determin e a3-hou r average . 32

. Sectio n60.15 4 i s revise dt o rea da s follows : §60.15 4 Tes t

method s an dprocedures

. (a ) I n conductin g th e performanc e test s require diri § 60.8 , di e owne r o r operato r shal l us e a s referenc e method s an dprocedure s di e tes t method s i n Appendi x A o f

thi s par t o r othe r "

. method s an dprocedure s a s specifie di n tins section , excep t

a s provide dfo r

i n 160.8(b)

. (b ) Th e owne r

o r operato r shal l determin e compliance , wit hth e particulat e matte r

emissio n standard s i n § 60.15 2 a s follows : .... ' (i ) Th e emissio nrat e (E ) o f particulat e matte r fo r eac hru nshal l b e compute d usin g th e followin g equation : E=R(c.Q s<1 )/ S where : - E=emissio n rat e o

f particulat e matter , g/k g (lb/ton ) o f dr y sludg e inpu t c,=concentratio n of

particulat e matter , g / dsc m(g/dscf)

. Q«d=volumetri c flow rat e o f effluen t gas , dscm/h r (dscf/hr)

. S=chargin g rat e of

dry sludg e durin g the-run , kg/h r (lb/hr)

. Reconversio n factor , 1.0 g/ g (4.40 9 lb s /(g

-
• ' .ton)] . ' •-., • .,•:.;:..-•.'•• •

. (2 ) Metho d5 shal l b e use dt o ' determin e th e particulat e matte r . concentratio n(c„ ) an dth e volumetri c flo w rat e (QKI ) o f

th e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r eac hru nshal l b e a t

leas t 6 0 minute s an d 0.9 0 dsc m(31. 8 dscf)

. (3 ) Th e dr y sludg e chargin g rat e (S ) fo r eac hru nshal l b e compute dusin g eithe r o f th e followin g equations : S=R

—S mRa

m/ 0 S=K „ S v R dv /

0 where : S=chargin g rat e o

f dry sludge , kg/h r

(lb/hr)

. S m =tota l mas s o

f sludg e charged , k

g (lb)

. Rara =averag e mas s o

f dr y sludg e pe r

uni t mas s o f sludg e charged , mg/mg (lb/lb)

. 0=duratio n o

f run , min

. K m =conversio n factor , 60 min/hr

. S,=tota l volume o

f sludg e charged , m 3

. (gal)

. R <v =averag e mas s o

f dry sludg e pe r

uni t volume o f sludg e charged , mg/liter

(lb /

. ft 3 )

. Reconversio n factor , 60xl0~'(liter*kg

- , - min)/(m 3 -mg-hr) [8.02 1 (ft 3 -min)/(gal-hr)]

. (4 ) Th e flo w measurin g devic e o f § 60.153(a)(1 ) shal l b e use dt o determin e di e tota l mas s (S„i ) o r

volum e (S» ) o f sludg e charge dt o th e incinerato r durin g eac hrun . I

f the.flo w measurin g devic e i s o natim e rat e basis , reading s shal l b e take nan drecorde da t

5-minut e interval s durin g th e ru n an dth e tota l charg e o f sludg e shal l b e compute dusin g the : followin g equations , a s applicable :

n. S „ = 2 Qml« l i= l n S , = 2 Q«0\ i= l where : Q ml =averag e mas s flow rat e calculate db y averagin g th e flow rate s a t th e beginnin g an den do f eac hinterva l "i" , kg/mi n (lb / min)

. Qvi=averag e volume flow rat e calculate db y averagin g th e flo

w rate s a t th e beginning " an den do f eac hinterval "i" , m 3 /mi n (gal/min)

. 0i=duratio n o

f interva l "i" , min

. (5 ) Sample s o f

th e sludg e charge dt o di e incinerato r

shal l b e collecte di n nonporou s jar s a t

th e beginnin g o f

eac h ru n an da t

approximatel y 1-hou r interval s thereafte r

unti l th e tes t

ends , an d"20 9 F
. Metho dfo r Soli dan d: Semisoli dSamples " (incorporate db y references-se e § 60,17 ) shal l b e use dt o determin e dr y sludg e conten t o f eac h sampl e (tota l solid s residue) , excep t that : ..<:•••.'.' . (i ) Evaporatin g dishe s shal l b e ignite d t o a t leas t 10 3 " C rathe r

tha n th e 55 0 " C specifie di nste p 3(a)(1) : ; ; - ! (ii ) Determinatio no f

volatil e residue , ste p 3(b ) ma y b e deleted

. (iii ) Th e quantit y o f

dr y sludge|pe r uni t sludg e charge dshallb e deteririine d i n term s o f

mg/lite r (lb/ft 3 ) o r

mg/m g (lb/lb)

. (iv ) Th e averag e dr y sludg e conten t : shal l b e th e arithmeti c averag e o f al l th e sample s take ndurin g th e run . (6 ) Metho d9 ari dth e procedure s ir i • § 60.1 1 shal l b e use dt o determin e opacity. ' § § 60.165,60.175 , an d60.18 5 , [Amended ] 33

. Section s 60.165(b)(2)(i) , ' 60.175(a)(2)(i) , an d60.185(a)(2)(i ) ar c amende db y removin g th e secon dan d' thir dsentences
. 34 i Tn§§60.165(b)(2)(ii) , ' 60,175(a)(2)(ii) , ari d60.185(a)(2)(ii) , th o word s "Fiel dTes t

fo r Accurac y (Relative) " ar e revise dt o rea d"Relativ e Accurac y Tes t

Procedure" , an dth e wor d "Reference " jus t

befor e "Metho d6 " i s removed

. 35

. Sectio n 60.16 6 i s revise dt o rea da s follows : .''..
. §60.16 6 Tes t

method s an dprocedures

. (a ) I nconductin g performanc e test s require di n§ 60.8 , th e owne r o r operato r shal l us e a s refereric e method s an d procedure s the , tes t

method s i n Appendi x A o f

thi s par t o r otiie r method s ari dprocedure s a s specifie dir i thi s section , excep t

a s provide di n § 60.8(b) :

, (b ) Th e owne r

o r operato r

shall ' determin e complianc e wit hth e particulat e rnattcr , sulfu r dioxid e (SO2 ) an dvisibl e emissio n standard s i n .§§'60.162 , 60.163 , an d60il6 4 a s follows :
: (1 ) Metho d5 shal l b e Use dt o : determin e th e particulat e matter'

. concentration

. Th e samplin g tim e an d

. sampl e volum e fo r

eac hru n shal l b e a t leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (2 ) Th e continuou s monitorin g system ' o f § 60.165(b)(2 ) shal l b e use dt o determin e th e SO 2 concentration s o n a dr y basis

. Th e samplin g tim'efo r eac hy : ru nshal l b e 6 hours , ari dth e averag e SO 2 concentratio nshal l b e compute dfo r th e 6-hou r

perio da s i n§ 60.165(c) : Th e ' monitoring , system-drif t durin g th e ru n • • ma y no t exceie d2 percen t

o f th e spa n value

. :•'••. •P.1 2

Federa l Registe r

/ Vol

. 54 , No
. 2 9 /

Tuesday , Februar y 14

. 198 9 / Rule s an dRegulation s 666 9 •ii^HHaiii^^KK,i^^^^MBMHMMjBiii^^^^^WaaBHMii^^^ ^ (3 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. 36

. Sectio n 60.17 6 i s revise dt o rea da s follows : §60.17 6 Tes t method s an d procedures . (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t rnethod s i n Appendi x A o f

thi s par t

o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r

shal l determin e coriiplianc e wit hth e particulat e matter , sulfu r dioxid e (S0 2 J , an dvisibl e emissio n standard s i n § § 60.172 , 60.173 , an d60.17 4 a s follows ; (1 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentration

. Th e samplin g tim e an d sampl e volum e fo r

eac hru n shal l b e a t leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (2 ) Th e continuou s monitorin g syste m o f § 60.175(a)(2 ) shal l b e use dt o determin e th e SO 2 concentration s o n a dr y basis

. Th e samplin g tim e fo r eac h ru n shal l b e 2 hours , an dth e averag e SO 2 concentratio n fo r

th e 2-hou r

perio d shal l b e compute da s i n § 60.175(b)

. Th e monitorin g syste mdrif t durin g th e ru n ma y no t excee d2 percen t

o f th e spa n value

. (3 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. 37

. Sectio n 60.18 6 i s revise dt o rea da s follows : §60.18 6 Tes t

methods , an dprocedures

. (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s ' an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section ; excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matter , sulfu r dioxid e {SO2) , .an dvisibl e emissio n standard s i n § § 60.182 , 60.183 ; an d60.18 4 a s follows : (1 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentration

. Th e samplin g tim e an d sampl e volum e fo r

eac hru n shal l b e a t

, leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (2 ) Th e continuou s monitorin g syste m o f § 60.185(a)(2 ) shal l b e use dt o determin e th e SO j concentration s o n a dr y basis

. Th e samplin g tim e fo r eac h ru n shal l b e 2 hours , an dth e averag e SO 2 concentratio n fo r

th e 2-hou r

perio d shal l b e compute da s i n § 60.185(b)

. Th e monitorin g syste mdrif t durin g th e ru n ma y no t excee d2 percen t

o f th e spa n value

. (3 ) Metho d9 an dth e procedure s i n . § 60.1 1 shal l b e use dt o determin e opacity

. § § 60.19 4 an d 60.19 5 [Amended ] 38

. Sectio n 60.19 5 i s amende db y redesignatin g § 60.195(a ) a s § 60.194(c ) an d§ 60.195(b ) a s § 60.194(d) ; 39

. Sectio n 60.19 5 i s revise dt o rea da s follows : § 60.19 5 Tes t method s an d procedures . (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t

o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n . § 60.8(b)

. (b ) Th e owne r

o r operato r

shal l : determin e complianc e wit hth e total , fluoride s an dvisibl e emissio n standard s i n §§60.19 2 an d60,19 3 a s follows : (1 ) Th e emissio n rat e (Ep ) o f tota l fluoride s fro mpotroo mgroup s shal l b e compute dfo r

eac hru n usin g th e followin g equation : EP=1(C.Q«,),+(C,Q r t ) 2 ]/(PR ) where : E„=emissio n rat e o

f tota l fluoride s fro

ma potroo mgroup , kg/M g (lb/ton)

. C,=concentratio n o

f tota l fluorides , mg/dsc m (mg/dscf)

. Q M = volumetric flow rat e o f effluen t gas . dscm/h r (dscf/hr)

. P=aluminu mproductio n rate
. Mg/h r (ton/hr)

. K=conversio n factor

. 10 " mg/k g (453,60 0 mg / lb)

. 1=subscrip t

fo r primary contro l syste m effluen t gas . 2— subscript

fo r secondar y contro l syste mo r roof monito r effluen t gas . (2 ) Th e emissio n rat e (Et, ) o f tota l - fluoride s fro manod e bak e plant s shal l b e compute dfo r

eac hrur i usin g th e followin g equation : E b =(C.Q sd )/(P.R ) where : Eu=emissio n rat e o

f tota l fluorides , kg/M g (lb/ton ) of

aluminu mequivalent. C,=concenrratio n o

f tota l fluorides , mg/dsc m (mg/dscf)

. Qsd=volumetri c flow rat e o f effluen t gas , dscm/h r (dscf/hr)

. P«=aluminu mequivalen t fo r anod e productio n rate , Mg/h r

(ton/hr)

. K=conversio n factor , 10"mg/k g (453,60 0 mg/ lb)

. (3 ) Method s 13 A o r

13 B shal l b e use d fo r duct s o r stacks , an dMetho d1 4 fo r roo f monitor s no t

employin g stack s o r pollutan t collectio n systems , t o determin e th e tota l fluoride s concentratio n (C J an dvolumetri c flo w rat e (Q s( i ) o f

th e effluen t

gas . Th e samplin g time an dsampl e volurii e fo r eac hru n shal l b e a t

leas t 8 hour s an d 6.8 0 dsc m(24 0 dscf ) fo r potroo mgroup s an da t leas t 4 hour s an d3.4 0 dscm(12 0 dscf ) fo r anod e bak e plants

. (4 ) Th e monitorin g device s o f § 60.194(a ) shal l b e use dt o determin e th e dail y weigh t

o f aluminu mari danod e produced

. (i ) Th e aluminu mproductio n rat e (P ) shal l b e determine db y dividin g 72 0 hour s int o th e weigh t

o f aluminu m tappe dfro mth e affecte dfacilit y durin g aperio do f

3 0 day s befor e an dincludin g th e final ru n o f

aperformanc e test
. (ii ) Th e aluminu mequivalen t productio n rat e (P e ) fo r anode s shal l b e determine da s 2 time s th e averag e weigh t o f ariod e produce ddurin g a representativ e ove n cycl e divide db y th e cycl e time

. A n owne r

o r operato r

ma y establis hamultiplicatio n facto r othe r tha n 2 b y submittin g productio n record s o f th e amoun t

o f aluminu mproduce d an dth e concurren t

weigh t o f anode s consume db y th e potrooms
. (5 ) Metho d9 an dth e procedure s in , § 60.1 1 shal l b e use dt o determin e opacity

. §60.20 3 [Amended ] 40

. I n § 60.203(b) , th e referenc e " § 60.204(d)(2 ) i s revise dt o rea d
" § 60.204(b)(3)"

. 41

. Sectio n 60.20 4 i s revise dt o rea da s follows : § 60.20 4 Tes t

method s an dprocedures

. (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t

o r other

method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e tota l fluoride s standar di n § 60.20 2 a s follows : (1 ) Th e emissio n rat e (E ) o f tota l fluoride s shal l b e compute dfo r eac hru n usin g tiie.following equation :

N E= ( 2

. i= l C „ Q«,i)/(PK

)

where : E=emissio n rat e o

f tota l fluorides , g/metric , to n (lb/ton ) o

f equivalen t

PiO s feed

. Cs i = concentratio n o

f tota l fluoride s fro

m emissio n poin t

"i,' ! mg/dsc m(mg/dscf)

.P.1 3



### 667 0 Federa

l Register/

Vol

. 54 , No
. 2

9 / Tuesday , February 14 , 198 9 / Rule s an dRegulation s Qsdi=volumetri c flow rat e o f effluen t ga s fro memission.point

"i. " dscm/h r

(dscf / hr)

. N = number

o f emissio npoint s associate d wit hth e affecte dfacility

. P=equivalen t

PiO s feed-rate , metri c ton/h r (ton/hr)

. R=conversio nfactor

. 100 0 mg/ g (453.60 0 mg / lb)

. (2 ) Metho d13 A o r

13 B shal l b e use dt o determin e th e tota l fluoride s concentratio n(C^ ) an dvolumetri c flo w rat e (Q„D. ) o f

th e effluen t

ga s fro meac h o f th e emissio npoints

. Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (3 ) Th e equivalen t

P 2 0 5 fee drat e (P ) shal l b e compute dfo r

eac hru nusin g th e followin g equation : P=M B RI > where : M p =tota l mas s flow rat e o f phosphorus

bearin g feed , metri c ton/h r (ton/hr)

. R 0 =Pj0 5 content , decimal fraction

. (i ) Th e accountabilit y syste mo f § 60.203(a ) shal l b e use dt o determin e th e mas s flo w rat e (M p ) of th e phosphorus-bearin g feed

. (ii ) Th e Associatio no f

Officia l Analytica l Chemist s (AOAC ) Metho d9 (incorporate db y reference—se e § 60.17 ) shal l b e use dt o determin e th e P2O 5 conten t (R p ) of th e feed

. §60.21 3 [Amended ] 42

. I n§ 60.213(b) , th e referenc e " § 60.214(d)(2) " i s revise dt o rea d
" § 60.214(b)(3)"

. 43

. Sectio n60.21 4 i s revise dt o rea da s follows : § 60.21 4 Tes t method s an d procedures . (a ) I nconductin g th e performanc e test s require di n§ 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. •(b) Th e owne r

o r operato r shal l determin e compliance'wit hth e tota l fluorides standar di n§ 60.21 2 a s follows : (1 ) Th e emmissio nrat e (E) o f tota l fluoride s shal l b e compute dfo r eac hru n usin g th e followin g equation :

N '( 2 C „ Q M

)/(PR ) i= l
where : E=emissio nrat e o f tota l fluorides , g/metri c ton (lb/ton ) o

f equivalen t

P2O 5 feed

. C5i=concentratio n o

f tota l fluoride s fro

m emissio npoint

"i, " mg/dsc m(mg/dscf)

. Qsdi=volumetri c flo

w rat e o f effluen t ga s fro memissio n point

"i, " dscm/h r

(dscf / hr)

. N= number

o f emissio n point s associate d wit hth e affecte dfacility

. P=equivalen t

P2O 5 feedrate , metri c ton/h r (ton/hr)

. R=co n versio nfactor , 100 0 mg/g (453.60

0 mg/ lb)

. (2 ) Metho d13 A o r

13 B shal l b e use dt o determin e th e tota l fluoride s concentratio n (C, ^ an dvolumetri c flo w rat e (Qsai) o f

th e effluen t

ga s fro meac h o f th e emissio n points

. Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (3 ) Th e equivalen t

P2O5 fee drat e (P ) shal l b e compute dfo r

eac hru nusin g th e followin g equation : P=M P R P where : M p =tota l mas s flow rat e o f phosphorus

bearin g feed , metri c ton/h r (ton/hr)

. R p =P 2 O s content , decimal fraction

. (i ) Th e accountabilit y syste mo f § 60.213(a ) shal l b e use dt o determin e th e mas s flo w rat e (M p ) o f th e phosphorus-bearin g feed

. (it) Th e Associatio no f

Officia l Analytica l Chemist s (AOAC ) Metho d9 (incorporate db y reference—se e § 60.17 ) shal l b e use dt o determin e th e P2O 5 conten t (Rp ) o f th e feed

. §60.22 3 [Amended ] 44

. I n§ 60.223(b) , th e referenc e " § 60.224(d)(2) " i s revise dt o rea d
" § 60.224(b)(3)"

. 45

. Sectio n60.22 4 i s revise dt o rea da s follows : § 60.22 4 Tes t method s an d procedures . (a ) I n conductin g th e performanc e test s require di n§ 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e tota l fluoride s standar di n § 60.22 2 a s follows : (1 ) Th e emissio nrat e (E ) o f tota l fluoride s shal l b e compute dfo r eac hru n usin g di e followin g equation :

N E= [ 2 C aQ^JA PR

) i = l where : E=emissio n rat e o

f tota l fluorides , g/metri c to n (lb/ton ) o

f equivalen t

PjO s feed

. . C s i = concentratio no

f tota l fluoride s fro

m emissio n point

"i, " mg/dsc m(mg/dscf)

. Qs<i i = volumetri c flow rat e o

f effluen t ga s fro memissio n poin t

"i, " dscm/h r

(dscf / hr)

. N = number

o f emissio npoint s associate d wit hth e affecte dfacility

. P=equivalen t

P2O 5 feed-rate , metri c ton/h r (ton/hr)

. R=conversio nfactor , 100 0 mg/g .(453.60

0 mg / lb). , (2 ) Metho d13 A o r

13 B shal l b e use dt o determin e th e tota l fluoride s concentratio n(C 8l ) an dvolumetri c flo w rat e (Q sd i ) o f

th e effluen t

ga s fro meac h o f th e emissio n points

. Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf).

. (3 ) Th e equivalen t

P2O5 fee drat e (P ) shal l b e compute dfo r

eac hru nusin g th e followin g equation : P=M p R p where : M p =totalmas s flow rat e o f phosphorus

bearin g feed , metri c ton/h r (ton/hr)

. R„=P 2 O s content , decimal fraction

. (i ) Th e accountabilit y syste mo f § 60.223(a ) shal l b e use dt o determin e th e mas s flo w rat e (M p ) o f th e phosphorus^bearin g feed

. (ii ) Th e Associatio no f

Officia l Analytica l Chemist s (AOAC ) Metho d9 (incorporte db y reference—se e § 60.17 ) shal l b e use dt o determin e th e P2O 5 conten t (R p ) o f th e feed

. §60.23 3 [Amended ] 46

. I n § 60.233(b) , th e referenc e " § 60.234(d)(2) " i s revise dt o rea d
" § 60.234(b)(3)"

. 47

. Sectio n60.23 4 i s revise dt o rea da s follows : § 60.23 4 Tes t method s an d procedures . (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide din § 60.8(b)

. (b ) Th e owne r

o r operato r shal l determin e complianc e wit hth e tota l fluoride s standard s i n §'60.23 2 a s follows : (l)'Th e emissio nrat e (E ) o f tota l fluoride s shal l b e compute dfo r eac hru n usin g th e followin g equation :P.1 4

Federa l Registe r

/ Vol

. 54 , No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s 6G7 1

N _E=(IC

- Q^i)/(PR ) i = l
where : E=emissio nrat e o

f tota l fluorides , g/metri c to n(lb/ton ) o

f equivalen t

P2O 5 feed

. Cd=concentratio n o

f tota l fluoride s fro

m emissio npoin t

"i, " mg/dsc m(mg/dscf)

. Qsdi=volumetri c flo w rat e of effluen t ga s fro memissio n poin t

"i, " dscm/h r

(dscf / ' hr)

. N=numbe r

o f emissio n point s in th e affecte d facility

. P=equivalen t

P2O 5 fee drate , metri c ton/h r (ton/hr)

. K=conversio n factor , 100 0 mg/g (453.60

0 mg/ lb)

. (2 ) Metho d13 A o r

13 b shal l b e use dt o determin e th e tota l fluoride s concentratio n(C dan dvolumetri c flo w rat e (Q«H ) o f

th e effluen t

ga s fro meac h o f th e emissio n points

. Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (3 ) Th e equivalen t

P 2 O s fee drat e (P ) shal l b e compute dfo r

eac hru n usin g th e followin g equation : P= M , R „ where : Mp total mas s flow rat e o

f phosphorus

bearin g feed , metri c ton/h r (ton/hr)

. R p =P20 s content , decimal fraction

. (i ) Th e accountabilit y systeir i o f § 60.233(a ) shal l b e use dt o determin e th e mas s flo w rat e (M p ) o f th e phosphorus-bearin g feed

. (ii ) Th e Associatio no f

Officia l Analytica l Chemist s (AOAC ) Metho d9 (incorporate db y reference—se e § 60.17 ) shal l b e use dt o determin e th e P2O 5 conten t (R„2) o f th e feed

. §60.24 3 [Amended ] 48

. I n § 60.243(b) , th e referenc e "60.244(f)(2) " i s revise dt o rea d "60.244(c)(3)"

. 49

. Sectio n60.24 4 i s revise dt o rea da s follows : § 60.24 4 Tes t

method s an dprocedures

. (a ) Th e owne r

o r operato r shal l conduc t performanc e test s require di n § 60. 8 onl y whe n th e followin g quantitie s o f

produc t ar e bein g cure do r store di n th e facility

. (1 ) Tota l granula r

tripl e superphosphat e i s a t

leas t 1 0 percen t

o f th e buildin g capacit y an d (2 ) Fres hgranula r

tripl e superphosphat e i s a t

leas t 2 0 percen t

o f th e tota l amoun t

o f tripl e superphosphat e or , (3 ) If th e provisio ni n paragraphia)^ ) o f thi s sectio nexceed s productio n capabilitie s fo r fres hgranula r

tripl e superphosphate , fres hgranula r tripl e superphosphat e i s equa l t o a t leas t 5 day s maximu mproduction

. (b ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (c ) Th e owne r

o r operato r shal l

. determin e complianc e wit hth e tota l fluorides standar di n § 60.24 2 a s follows : (1 ) Th e emissio nrat e (E ) o f tota l fluoride s shal l b e compute dfo r eac hru n usin g th e followin g equation :

N E=(2C r i Q^)/(PR ) i = l

where : E=emissio n rat e of

tota l fluorides , g/hr / metri c to n (lb/hr/ton ) o

f equivalen t

P 2 0 5 stored

. 'C,i=concentratio n o

f tota l fluoride s fro

m emissio n poin t

"i, " mg/dsc m(mg/dscf)

. Qau^volumetri c flow rat e of effluent ga s fro memissio npoin t

"i, " dscm/h r

(dscf / hr)

. N=numbe r

o f emissio n point s i n th e affecte d facility

. P=equivalen t

P2O 3 stored , metri c ton s (tons)

. K=conversio n factor , 100 0 mg/g (453,60

0 mg / lb) . (2 ) Metho d13 A o r

13 B shal l b e use dt o determin e th e tota l fluoride s concentratio n(CM ) an dvolumetri c flo w rat e (Q^i ) o f

th e effluen t

ga s fro meac h o f th e emissio n points

. Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (3 ) Th e equivalen t

P2O5 fee drat e (P ) shal l b e compute dfo r

eac hru n usin g th e followin g equation : P=M P R P where : M p =amoun t

o f produc t in storage , metri c to n (ton)

. R 0 =PjO s conten t

o f produc t i n storage , weight fraction

. (i ) Th e accountabilit y syste mo f § 60.243(a ) shal l b e use dt o determin e th e amoun t

o f produc t (M„ ) i n storage
. (ii ) Th e Associatio n o f

Officia l Analytica l Chemist s (AOAC ) Metho d9 (incorporate db y reference—se e § 60.17 ) shal l b e use dt o determin e th e P2O5 conten t (R p ) o f th e produc t

i n storage
. §60.25 3 [Amended ]

50

. I n § 60.253(b) , th e las t lin e i s amende d.b y revisin g th e referenc e " § 60.13(b)(3) " t o rea d" § 60.13(b)"

. 51

. Sectio n 60.25 4 i s revise dt o rea da s follows: , § 60.25 4 Tes t

method s an dprocedures

. (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operator , shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

this.par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r shal l determin e complianc e wit hth e particula r

matte r standard s i n § 60.25 2 a s follows : (1 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentration

. Th e samplin g tim e an d

. sampl e volum e fo r

eac hru n shal l b e a t leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. Samplin g shal l begi n n o les s tha n 3 0 minute s afte r

startu p an dshal l terminat e befor e shutdow n procedure s begin

. (2 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. 52

. Sectio n60.26 6 i s revise dt o rea da s follows : § 60.2S 6 Tes t

method s an dprocedures

. (a ) Durin g an y performanc e tes t require di n § 60.8 , th e owne r o r operato r shal l no t allo w gaseou s diluent s t o b e adde dt o th e effluen t

ga s strea mafte r th e fabri c i n a n ope npressurize dfabri c filte r collecto r

unles s th e tota l ga s volum e flo w fro mth e collecto r i s accuratel y determine dan dconsidere d i n th e determinatio no f emissions

. (b ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide din

. § 60.8(b)

. (c ) Th e owne r

o r bperato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n § 60.26 2 a s follows: ' (1 ) Th e emissio nrat e (E ) o f particulat e matte r shal l b e compute dfo r eac hru n usin g th e followin g equation :

N E= PC,Q»„)/(PK ) i= l vhere :P.1 5

667 2 Federa l Registe r/ Vol

. 54 , No
. 2 9 /

Tuesday,

- Februar y 14 , 198 9 / Rule s an dRegulation s E=emissio nrat e o

f particulat e matter , kg / MW-h r (lb/MW-hr)

. n=tota l nuniber

o f exhaus t stream s a t

whic h emission s i s quantified

. d=concentratio n o

f particulat e matte r

fro m exhaus t strea m"i'Vg/dsc m(g/dscf)

. 0^1=volumetri c flow rat e o f effluen t ga s fro mexhaus t

stream"i" , dscm/h r

(dscf / hr)

. P=averag e furnac e powe r input , MW
. K=conversio n factor

. 100 0 g/k g (453. 6 g/lb)

. (2 ) Metho d5 shal l b e use dt o determine'th e particulat e matte r concentratio n (Cd

) an d^volumetri c flow rat e (Q„ii ) o f

th e effluen t

gas , excepttha t di e heatin g system s specifie di n section s 2.1. 2 an d2.1. 6 ar e no t

t o b e use dwhe n th e carbo n monoxid e conten t o f th e ga s strea mexceed s 1 0 percen t b y volume , dr y basis

. 3 f

aflar e i s use dt o compl y wid i § 60.263 , th e samplin g sit e shal l b e upstrea mo f

ith e flare. Th e samplin g tim e shal l includea nintegra l numbe r o f furnac e cycles

. (i ) Whe nsamplin g emission s fro m ope nelectri c submerge dar c furnace s wit hwe t scrubbe r

contro l devices , seale delectri c submerge dar c furnaces , o r semienclose delectri c ar c furnaces , th e samplin g tim e an dsampl e volum e fo r eac hru nshal l b e a t

leas t 6 0 minute s an d1.8 0 dsc m(63. 6 dscf)

- (ii ) Whe nsamplin g emission s fro m othe r type s o f installations , th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 20 0 minute s an d5.7 0 dsc m(20 0 dscf)

. (3 ) Th e measuremen t

devic e o f § 60.265(b ) shal l b e use dt o determin e th e averag e furnac e powe r inpu t (P ) durin g eac hrun . (4 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. (5 ) Th e emissio nrat e correctio n factor , integrate dsamplin g procedur e o f Metho d3 shal l b e use dt o determin e th e C O concentration

. Th e sampl e shal l b e take nsimultaneousl y wit heac h particulate.matte r

sample

. (d ) Durin g di e particulat e matte r run , th e maximu mope nhoo dare a(i nhood s wit hsegmente do r

otherwis e moveabl e sides ) unde r

whic hth e proces s i s expecte dt o b e operate dand-remaini n complianc e wit hal l standard s shal l b e recorded

. An y futur e operatio n o f th e hoodin g syste mwit hope narea s i n exces s o f th e maximu mi s no t

permitted

. (e ) T o compl y wit h§ 60.26 5 (d ) o r (f)

. th e owne r

o r operato r shal l us e th e monitorin g device s ir

i § 60.26 5 (c ) o r

(e ) t o mak e tiie require dmeasurement s a s determine ddurin g th e performanc e test
. §60.27 3 [Amended ] 53

. Sectio n60.273(c ) i s revise dt o rea d a s follows : (c ) A continuou s monitorin g syste mi s no t require do nan y modular , multiple

stack , negative-pressur e o r positive

pressur e fabri c filter

i f observation s o f th e opacit y o f

tiie visibl e emission s fro m th e contro l devic e ar e performe db y a certifie dvisibl e emissio n observe r a s follows : Visibl e emissio n observation s shal l b e conducted.a t

leas t onc e pe r

da y whe ntiie furnac e i s operatin g i n th e meltin g an drefinin g period

. Thes e observation s shal l b e take n i n accordanc e wit hMetho d9 , and ; fo r a t leas t thre e 6-minut e periods , th e opacit y shal l b e recorde dfo r

an y point(s ) wher e visibl e emission s ar e observed

. Wher e i t i s possibl e t o determin e tha t anumbe r o f visibl e emissio n site s relat e t o onl y on e inciden t

o f th e visibl e emission , only-on e se t

o f thre e (6-minut e observation s wil l b e required

. I n thi s case , Metho d9 observation s mus t b e mad e fo r th e sit e o f

highes t opacit y tha t directl y relate s t o di e caus e (o r location ) o f visibl e emission s observe ddurin g a singl e incident

. Record s shal l b e maintaine do f

an y 6-minut e averag e tha t i s i nexces s o f

th e emissio n limi t specifie di n§ 60.272(a ) o f thi s subpart

. 54

. Sectio n 60.27 5 i s amende db y redesignatin g paragrap h(c ) a s § 60.276(c) , b y revisin g paragraph s (a) , (b) , (d) , (e),an d(f) , an db y addin g ane w paragrap h(c ) t o rea da s follows : § 60.27 5 Tes t

method s an dprocedures

. (a ) Durin g performanc e test s require d i n§ 60.8 , th e owne r

o r operato r

shal l no t ad dgaseou s diluen t

t o th e effluen t

ga s afte r th e fabri c i n an y pressurize dfabri c collector , unles s th e amoun t o f dilutio n i s separatel y determine dan dconsidere d i nth e determinatio n o f

emissions

. (d ) Whe nemission s fro man y EAF(s ) ar e combine dwit hemission s fro m facilitie s no t

subjec t t o th e provision s o f dii s subpar t

bu t controlle db y acommo n captur e syste man dcontro l device , th e owne r o r operato r shal l us e eithe r

o r bot ho f th e followin g procedure s durin g aperformanc e tes t

(se e als o § 60.276(b)) : (1 ) Determin e complianc e usin g th e combine demissions

. (2 ) Us e amedio dtha t

i s acceptabl e t o th e Administrato r

an dtha t

compensate s fo r th e emission s fro mdi e facilitie s no t subjec t t o th e provision s o f

thi s subpar t (c ) Whe nemission s fro man y EAF(s ) ar e combine dwit hemission s fro m facilitie s no t

subjec t t o th e provision s o f thi s subpart , th e owne r o r operato r shal l us e eithe r

o r bot ho f th e followin g procedure s t o demonstrat e complianc e wit h§ 60.272(a)(3) : (1 ) Determin e complianc e usin g th e combine demissions

. (2 ) Shu t dow noperatio no f

facilitie s no t subjec t t o th e provision s o f

thi s subpar t durin g th e performanc e test
. (d ) I n conductin g th e performanc e test s require di n§ 60.8 , th e owne r o r operato r

shal l us e a s referenc e method s an dprocedure s th e tes t method s i n . Appendi x A o f

thi s par t o r othe r i method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n §60.8(b)

. (e ) Th e owne r

o r operato r

shal l j determin e complianc e wit hth e . particulat e matte r

standard s i n § 60.27 2 a s follows : (1 ) Metho d5 shal l b e use dfo r negative-pressur e fabri c filter s an dothe r type s o f contro l device s an dMetho dS D shal l b e use dfo r

positive-pressur e fabri c filter s t o determin e th e particula r matte r concentratio nand , if

applicable , th e volumetri c flow rat e o f di e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r eac hru nshal l b e a t

leas t 4 hour s an d 4. 5 dsc m(16 0 dscf) and , whe n asingl e EA Fi s sampled , th e samplin g tim e shal l includ e a n integra l numbe r o f heats

. (2 ) Whe nmor e the n on e contro l devic e serve s th e EAF(s ) bein g tested , th e concentratio no f

particulat e matte r shal l b e determine dusin g di e followin g equation :
nn

C r t =[IC

- Q« a )]/2Q« l t i = l »= 1 where : c,,=averageconcentratio n o f particulat e matter , mg/dsc m(gr/dscf)

. ^^concentratio n o

f particulat e matte r

fro m contro l devic e "i" , mg/dsc m(gr/dscf)

- n= tota l numbe r

o f contro l device s tested

. Qs«u=volumetri c flow rat e o f stac k ga s from contro l devic e "i" , dscm/h r (dscf/hr)

. (3 ) Metho d9 an dth e procedure s o f § 60.1 1 shal l b e use dt o determin e opacity

. (4 ) T o demonstrat e complianc e wit h § 60.272(a ) (1) , (2) , an d(3) , th e tes t run s shal l b e conducte dconcurrently , unles s inclemen t

weathe r interferes

. (f ) T o compl y wit h§ 60.27 4 (c)

. (f) , (g) , an d(i) , th e owne r

o r operato r

shal l obtai n th e informatio n i n thes e paragraph s durin g th e particulat e matte r runs . §60.27 6 [Amended ] 55

. I n§ 60.276(b) , th e referenc e |
" § 60.275(g)(2 ) o r

(g)(3) " i s revise dt o 1 rea d" § 60.275(b)(2 ) o r

acombinatio n o f

. (b)(1 ) an d(b)(2)"

. j § 60.273 a[Amended ] j 56

. Sectio n60.273a(c ) i s revise dt o j rea da s follows : j (c ) A continuou s monitorin g syste mj fo r th e measuremen t

o f opacit y i s no t

! require do nmodular , multiple-stack

. ' ( negative-pressur e o r

positive-pressur e j fabri c filters if

observation s o f

th e ! opacit y o f

th e visibl e emission s fro mth eP.1 6

Federa l Registe r

/ Vol

. 54 , No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s 667 3
contro l devic e ar e performe db y a certifie dvisibl e emissio n observe r a s follows : Visibl e emissio nobservation s ar e conducte da t

leas t onc e pe r

da y whe nth e furnac e i s operatin g i nth e meltin g an drefinin g perio dThes e observation s shal l b e take n i n accordanc e wit hMedio d9 , and , fo r a t leas t thre e 6-minut e periods , di e opacit y shal l b e recorde dfo r

an y point(s ) wher e visibl e emission s ar e observed

. Wher e i t i s possibl e t o determin e tha t anumbe r o f visibl e emissio nsite s relat e t o onl y on e inciden t

o f di e visibl e emissions , onl y on e se t

o f thre e 6-minut e observation s wil l b e required

. I nthi s case , Metho d9 observation s mus t b e mad e fo r th e sit e o f

highes t opacit y tha t directl y relate s t o th e caus e (o r location ) o f visibl e emission s observe ddurin g a singl e incident

. Record s shal l b e maintaine do f

an y 6-minut e averag e tha t i s i nexces s o f

di e emissio nlimi t specifie di n§ 60.272a(a ) o f thi s subpart

. 57

. Sectio n60.275 ai s amende db y redesignatin g paragrap h(d ) a s § 60.276a(f), b y revising paragraph s (a) , (b) , (c) , (e) , an d(f)

. an db y addin g ne w paragrap h(d ) t o rea da s follows : § 60.275 a Tes t method s an d procedures . (a ) Durin g performanc e test s require d i n§ 60.8 , th e owne r

o r operato r shal l no t ad dgaseou s diluent s t o th e effluen t ga s strea mafte r

th e fabri c i nan y pressurize dfabri c filter collector , unles s th e amoun t

o f dilutio n i s separatel y determine dan dconsidere di nth e determinatio no f

emissions

. (b ) Whe nemission s froman y EAF(s ) o r AO D vessel(s ) ar e combine dwit h emission s fromfacilitie s no t subjec t t o th e provision s o f

thi s subpar t

bu t controlle db y acommo ncaptur e syste m an dcontro l device , di e owne r o r operato r shal l us e eithe r

O r bot ho f th e followin g procedure s durin g a performanc e tes t

(se e als o § 60.276a(e)) : (1 ) Determin e complianc e usin g th e combine demissions

. (2 ) Us e ametho dtha t

i s acceptabl e t o th e Administrato r

an dtha t compensate s fo r di e emission s fromdi e facilitie s no t subjec t t o th e provision s o f

thi s subpart

. (c ) Whe nemissio n fro man y EAF(s ) o r AO D vessel(s ) ar e combine dwit h emission s fromfacilitie s no t subjec t t o th e provision s o f

thi s subpart , di e owne r o r operato r shal l demonstrat e complianc e wit h§ 60.272(a)(3 ) base do n emission s fro monl y th e affecte d facility(ies)

. (d ) I nconductin g di e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e mediod s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t a s provide di n 560.8(b)

. (e ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n§ 60.272 a a s follows : (1 ) Medio d5 shal l b e use dfo r negative-pressur e fabri c filters an dothe r type s o f contro l device s an dMetho d5 D shal l b e use dfo r

positive-pressur e fabri c filters t o determin e di e particulat e matte r concentratio n an dvolumetri c flow rat e o f

th e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 4 hour s an d 4.5 0 dsc m(16 0 dscf) and , whe nasingl e EA Fo r AO D vesse l i s sampled , th e samplin g tim e shal l includ e a nintegra l numbe r o f heats

. (2 ) Whe nmor e tha n on e contro l devic e serve s di e EAF(s ) bein g tested , th e concentratio n o f

particulat e matte r shal l b e determine dusin g di e followin g equation :

nn

=[2C..CU)]/XQ. B i = l 1= 1

where : Crt=averag e concentratio no f particulat e matter , mg/dsc m(gr/dscf)

. c»j=concentratio n of

particulat e matte r

fro m contro l devic e "i" , mg/dsc m(gr/dscf)

. n=tota l numbe r

o f contro l device s tested

. Q.di=volumetri c flo w rat e of stac k ga s fro m contro l devic e "i" , dscm/h r (dscf/hr)

. (3 ) Metho d9 an dth e procedure s o f § 60.1 1 shal l b e use dt o determin e opacity

. (4 ) T o demonstrat e complianc e wit h § 60.272a(a ) (1) , (2) , an d(3) , th e tes t run s shal l b e conducte dconcurrently , unles s inclemen t

weathe r interferes

. (f ) T o compl y wit h§ 60.274 a(c) , (f) , (g) , an d(h) , th e owne r

o r operato r

shal l obtai n th e informatio nrequire di nthes e paragraph s durin g th e particulat e matte r runs . § 60.276 a[Amended ] 58

. I n 60.276a(e)

. th e referenc e " § 6U275a(h)(2 ) o r

(h)(3) " i s revise dt o rea d" § 60.275(b)(2 ) o r

acombinatio no f (b)(1 ) an d(b)(2)"

. 59

. Sectio n 60.28 5 i s revise dt o rea da s follows : § 60.28 5 Tes t

method s an dprocedures

. (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

dii s par t o r othe r method s an dprocedure s i n thi s section ,

excep t a s provide di n § 60.8(b)

. Acceptabl e alternativ e method s an d procedure s ar e give n i n paragrap h(f ) o f thi s section

. (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n § 60.282(a ) (1 ) an d(3 ) a s follows : (1 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentration

. Th e samplin g tim e an d sampl e volum e fo r

eac hru nshal l b e a t leas t 6 0 minute s an d0.9 0 dsc m(31. 8 dscf)

. Wate r

shal l b e use da s th e cleanu p solven t

instea do f

aceton e i n th e sampl e recover y procedure

. Th e particulat e concentratio n shal l b e correcte dt o th e appropriat e oxyge n concentratio naccordin g t o § 60.284(c)(3)

. (2 ) Th e emissio nrat e correctio n factor , integrate dsamplin g an danalysi s procedur e o f

Metho d3 shal l b e use dt o determin e di e oxyge n concentration

. Th e ga s sampl e shal l b e take n a t th e sam e tim e an da t

th e sam e travers e ~ point s a s th e particulat e sample

. (3 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. (c ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particula r

matte r standar di n § 60.282(a)(2 ) a s follows : (1 ) Th e emissio nrat e (E ) o f particulat e matte r shal l b e compute dfo r

eac hru n usin g th e followin g equation : E=c e Q Jrf /BL S where : E=emissio n rat e o

f particulat e matter,'g/k g (lb/ton ) o f BLS.

_ C„=concentratio n o f

particulat e matter , g/ds m(lb/dscf)

. Qxs= volumetric flow rat e of effluen t gas , dscm/h r (dscf/hr)

. BLS=blac k

liquo r solid s (dry weight) fee d rate , kg/h r

(ton/hr)

. (2 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentratio n(C„ ) an dth e volumetri c flo w rat e (Q. J o f

th e effluen t

gas . Th e samplin g tim e an dsampl e volum e shal l b e a t leas t 6 0 minute s an d0.9 0 dsc m (31. 8 dscf)

. Wate r

shal l b e use dinstea d o f aceton e i n th e sampl e recovery . (3 ) Proces s dat ashal l b e use dt o determin e th e blac k

liquo r solid s (BLS ) fee drat e o n adr y weigh t basis

. (d ) Th e owne r

o r operato r

shal l detennin e complianc e wit hth e TR S standard s i n§ 60.283 , excep t § 60.283(a)(l)(vi ) an d(4) , a s follows : (1 ) Metho d1 6 shal l b e use dt o determin e th e TR S concentration

. Th e - TR S concentratio nshal l b e correcte dt o th e appropriat e oxyge n concentratio n usin g th e procedur e i n § 60.284(c)(3)

. Th eP.1 7

667 4 Federa l Registe r / Vol

. 54 , No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s samplin g tim e shal l b e a t leas t 3 hours , bu t n o longe r

tha n 6 hours

. (2 ) Th e emissio n rat e correctio n factor , integrate dsamplin g an danalysi s procedur e o f

Metho d3 shal l b e use dt o determin e th e oxyge n concentration

. Th e sampl e shal l b e take n ove r th e sam e tim e perio da s th e TR S samples

. (3 ) Whe n determinin g whethe r a furnac e i s astraigh t

kraf t recover y furnac e o r

acros s recover y furnace , TAPP I Metho dT.62 4 (incorporate db y reference—se e § 60.17 ) shal l b e use dt o determin e sodiu msulfide , sodiu m hydroxide , an dsodiu mcarbonate

. Thes e determination s shal l b e mad e 3 time s dail y fromdi e gree n liquor , an ddi e dail y averag e value s shal l b e converte d t o sodiu moxid e (Nac^O ) an dsubstitute d int o th e followin g equatio n t o determin e th e gree n liquo r

sulfidity : GL S = 10 0 CNa a S/(C NA2 S -r-C N .oH-fC Ntfc0 3 ) Where : GLS=gree n liquo r

sulfidity , percent
. C N .2 S =concentratio n o

f Na2 S a s Na 2 0 , mg/ lite r (gr/gal)

. CN«OH=concentratio no

f NaO H a s Na 2 0 , mg

/ lite r (gr/gal)

. C K ,2co3=concentratio n o

f Na2C0 3 a s Na 2 0 , mg/liter (gr/gal)

. (e ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e TR S standard s i n § 60.283(a)(l)(vi ) an d(4 ) a s follows : (1 ) Th e emissio n rat e (E ) o f TR S shal l b e compute dfo r

eac hru n usin g th e followin g equation : E=C TI1 S F0,,,/ P where : E=emissio n rat e o

f TRS , g/kg (lb/ton ) o

f BL S o r ADP

. C TRS =averag e combine dconcentratio n o f TRS , ppm . F=conversio n factor

. 0.00141 7 g HjS/m 3 ppm (0.0844X10" 6 lb HsS/ft 3 ppm)

. Qsd—volumetric flow rat e o f stac k gas , dscm/ h r (dscf/hr)

. P=blac k liquo r solid s feedo r

pulp productio n rate , kg/h r

(ton/hr)

. (2 ) Medio d1 6 shal l b e use dt o determin e th e TR S concentratio n (Cms)

- (3 ) Metho d2 shal l b e use dt o determin e di e volumetri c flo w rat e (Q„j ) o f th e effluen t

gas . (4 ) Proces s dat ashal l b e use dt o determin e th e blac k

liquo r fee drat e o r th e pul p productio n rat e (P)

. (f ) Th e owne r

o r operato r

ma y us e th e followin g a s alternative s t o th e referenc e method s an dprocedure s specifie di n thi s section : (1 ) Fo r Metho d5 , Metho d1 7 ma y b e use di f aconstan t

valu e o f 0.00 9 g/dsc m (0.00 4 gr/dscf ) i s adde dt o di e result s o f Metho d1 7 an dth e stac k temperatur e i s n o greate r

tha n 20 5 ° C (40 0 °F)

. (2 ) Fo r Metho d16 , Metho d16 A o r 16 B ma y b e use dif

th e samplin g tim e i s 6 0 minutes

. §60.29 2 [Amended ] 60

. I n § 60.292(a)(2) , th e definitio n o f "Y " i s amende db y revisin g th e word s "Decima l percent " t o rea d"Decima l fraction " an drevisin g di e referenc e " § 60.296(f) " t o rea d" § 60.296(b)"

. 61

. Sectio n 60.29 6 i s revise dt o rea da s follows : §60.29 6 Tes t

method s an dprocedures

. (a ) If aglas s meltin g furnac e wit h modifie dprocesse s i s change dt o on e withou t modifie dprocesse s o r if aglas s meltin g furnac e withou t modifie d: processe s i s change dt o on e wid i ; modifie dprocesses , th e owne r o r operato r shal l notif

y th e Administrato r a t leas t 6 0 day s befor e th e chang e i s schedule dt o occur . (b ) Whe n gaseou s an dliqui dfuel s ar e firedsimultaneousl y i n aglas s meltin g furnace , th e owne r

o r operato r

shal l determin e th e applicabl e standar dunde r § 60.292(a)(2 ) a s follows : (1 ) Th e rati o (Y ) o f

liqui dfue l heatin g valu e t o tota l (gaseou s an dliquid ) fue l heatin g valu e fire di n th e glas s meltin g furnace s shal l b e compute dfo r eac hru n usin g th e followin g equation : Y=(H I L)/H 1 L+H,G ) where : Y=decima l fraction o

f liqui dfue l heatin g valu e t o tota l fue

l heatin g value.

- H|=gros s calorifi c valu e o f liqui dfuel , J/kg

. H,=gros s calorifi c valu e o f gaseou s fuel , J

/ kg

L=liqui dflow rate , kg/hr

. G=gaseou s flo w rate , kg/hr

. (2 ) Suitabl e method s shal l b e use dt o determin e th e rate s (Lan dG ) o f fuel s burne ddurin g eac htes t perio dan da materia l balanc e ove r

th e glas s meltin g furnac e shal l b e use dt o confir mth e rates
. (3 ) America n Societ y o f Testin g an d Material s (ASTM ) Metho dD 240-7 6 (liqui dfuels ) an dD 1826-7 7 (gaseou s fuels ) (incorporate db y reference—se e § 60.17) , a s applicable , shal l b e use dt o determin e th e gros s calorifi c values i (c ) I n conductin g th e performanc e test s requiredi n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r

. method s an dprocedure s a s specifie di n ' thi s section , excep t

a s provide di n § 60.8(b)

. (d ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n § § 60.29 2 an d60.29 3 a s follows : (1 ) Th e emissio n rat e (E ) o f particulat e matte r shal l b e compute dfo r eac hru n usin g th e followin g equation : E=(c.W^-A)/ P where : E=emissio n rat e o

f particulat e matter , g/kg

. c,=concentratio n o

f particulat e matter , g / dsm

. Q sd =volumetri c flow rate , dscm/hr

. A=zer o productio n rat e correctio n = 22 7 g/h r fo r containe r

glass , presse dan d blow n (soda-lime an dlead ) glass , an d presse dan dblow n (othe r tha n borosilicate , soda-lime , an dlead ) glass

. =45 4 g/h r fo r presse dan dblow n

. (borosilicate ) glass , woo l fiberglass , an d fla t glass

. P=glas s productio n rate , kg/hr

. (2 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r concentratio n (c, ) an dvolumetri c flow rat e (0^ ) o f

di e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d 0.9 0 dsc m(31. 8 dscf)

. Th e prob e an d filter holde r heatin g syste mma y b e se t t o provid e aga s temperatur e n o greate r tha n 177±1 4 " C (350±2 5 °F)

. excep t unde r th e condition s specifie di n § 60.293(e)

. (3 ) Direc t

measuremen t

o r materia l balanc e usin g goo dengineerin g practic e shal l b e use dt o detennin e th e amoun t o f glas s pulle ddurin g th e performanc e test
. Th e rat e o f

glas s produce di s define da s th e weigh t

o f glas s pulle dfro mth e affecte dfacilit y durin g th e performanc e tes t divide db y th e numbe r o f hour s take n t o perfor mth e performanc e test
. (4 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determine ' opacity

. 62

. Sectio n 60.30 3 i s revise dt o rea da s follows : § 60.30 3 Tes t

method s an dprocedures

. (a ) I n conductin g th e performanc e test s require di n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

tiiis par t

o r otiie r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. Acceptabl e alternativ e method s an dprocedure s ar e give n i n paragrap h(c ) o f

thi s section

. (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hdi e particulat e matte r

standard s i n § 60.30 2 a s follows : (1 ) Metho d5 shal l b e use dt o determin e th e particulat e matte r , concentratio n an ddi e volumetri c flow rat e o f th e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d1.7 0 dsc m(6 0 dscf)

. Th e prob e an dfilte r holde r shal l b e operate dwithout

. . heaters

. (2 ) Metho d2 shal l b e use dt o determin e th e ventilatio n volumetri c flow rate
. (3 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. (c ) Th e owne r

o r operato r

ma y us e th e followin g a s alternative s t o th eP.1 8

Federa l Registe r/

Vol . 54 , No . 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an d Regulation s 667 5 referenc e method s an d procedure s specifie d i n thi s section : (1 ) Fo rMetho d 5 , Metho d 1 7 ma y b e used . 63 . Sectio n 60.33 5 i s revise d t o rea d a s follows : §60.33 5 Tes tJTivsiiMKt

e an d e»ro<^dijr®o

. (a ) T o comput e di e riitroge n oxide s emissions , th e owne ro roperato rshal l us e analytica l method s an d procedure s tha tar e accurat e t o withi n 5 percen tan d ar e approve d b y th e Administrato rt o determin e th e nitroge n conten to f th e fue l bein g fired. (b ) I n conductin g th e performanc e test s require d i n § 60.8 , th e owne ro r operato rshal l us e a s referenc e method s an d procedure s th e tes tmethod s i n Appendi x A o f

thi s par to rothe r method s an d procedure s a s specifie d i n thi asection , excep ta s provide d fo ri n § 60.8(b) . Acceptabl e alternativ e mediod s an d procedure s ar e give n i n paragrap h (f

) o f thi s section . (c ) Th e owne ro roperato rshal l determin e compUanc e wit h th e nitroge n oxide s an d sulfu rdioxid e standard s i n § § 60.33 2 an d 80.333(a ) a s follows : (1 ) Th e nitroge n oxide s emissio n rat e (NOx) shal l b e compute d fo reac h ru n usin g th e followin g equation : NO„=(NO IO ) (P,/PJ a«e>««*>-»«« M (288*K/T

J 1.5 3 where : NO,=emissio n rat

e o f NO , a t1 5 percen

tO 2 and ISO standar

d ambien tconditions , volume percent. NO,,,=observe d NO , concentration , pp m by volume . P r = referenc

e combustorinletabsolute pressur e at101.3 kilopascal s ambien t pressure , m

m Hg. P 0 =observe d combustorinletabsolut e pressur e a ttest , m m Hg. Ho=observe d humidit

y o f ambien tair, g HjO/gair . e=transcendental constan t2.718 . T.=ambien ttemperature, *K . (2 ) Th e monitorin g devic e o f § 60.334(a ) shal l b e use d t o determin e th e fue l consumptio n an d th e water-to fue l rati o necessar y t o compl y wit h § 60.33 2 a t30 , 50 , 75 , an d 10 0 percen to f pea kloa d o ra tfou rpoint s i n th e norma l operatin g rang e o f

th e ga s turbine , includin g th e minimu m poin ti n th e rang e an d pea kload . Al l load s shal l b e correcte d t o IS O condition s usin g th e appropriat e equation s supplie d b y th e manufacturer . (3 ) Metho d 2 0 shal l b e use d t o determin e th e nitroge n oxides , sulfu r dioxide , an d oxyge n concentrations . Th e spa n value s shal l b e 30 0 pp m o f nitroge n oxid e an d 2 1 percen toxygen . Th e NO , emission s shal l b e determine d a teac h o f th e loa d condition s specifie d i n paragrap h (c)(2 ) o f

this section . (d ) Th e owne ro roperato rshal l determin e complianc e wit h th e sulfu r conten tstandar d i n § 60.333(b ) a s follows : AST M D 2880-7 1 shal l b e use d

- t o determin e th e sulfu rconten to f liqui d fuel s an d AST M D 1072-80 , D 3031-81 . D 4084-82 , o rD 3246-8 1 shal l b e use d fo r th e sulfu rconten to f

gaseou s fuel s (incorporate d b y reference—se e § 60.17) . Th e applicabl e range s o f som e AST M method s mentione d abov e ar e no t adequat e t o measur e th e level s o f sulfu r i n som e fue l gases . Dilutio n o f sample s befor e analysi s (wit h verificatio n o f di e dilutio n ratio ) ma y b e used , subjec tt o th e approva l o f

th e Administrator . (e ) T o mee tdi e requirement s o f § 60.334(b) , th e owne ro roperato rshal l us e th e method s specifie d i n paragraph s (a ) an d (d ) o f

thi s sectio n t o determin e th e nitroge n ari d sulfu rcontent s o f the ' fue l bein g burned . Th e analysi s ma y b e performe d b y th e owne ro roperator , a . servic e contracto rretaine d b y th e owne r o roperator , th e fue l vendor , o ran y otiie r qualifie d agency . (f ) Th e owne ro roperato rma y us e th e followin g a s alternative s t o th e referenc e method s an d procedure s specifie d i n thi s section : (1 ) Instea d o f

usin g di e equatio n i n paragrap h (b)(1 ) o f

thi s section , manufacturer s ma y develo p ambien t conditio n correctio n factor s t o adjus tth e nitroge n oxide s emissio n leve l measure d b y th e performanc e tes ta s provide d i n § 60. 8 t o IS O standar d da y conditions . Thes e factor s ar e develope d fo reac h ga s turbin e mode l the y manufactur e i n term s o f combustio n inle tpressure , ambien tai rpressure , ambien tai r humidity , an d ambieri tai rtemperature . The y shal l b e substantiate d wit h dat a an d mus tb e approve d fo rus e b y th e Administrato rbefor e th e initia l performanc e tes trequire d b y § 60.8. ' Notice s o f

approva l o f

custo m ambien t conditio n correctio n factor s wil l b e publishe d i n th e Federa l Register . §60.34 3 (Amended ] 64 . I n § 60.343(e) , th e las tsentenc e i s revised t o rea d a s follows : "I f visibl e emissio n Observation s ar e mad e

- accordin g t o paragrap h (b ) o f thi s section , reports o f

exces s emission s shal l b e submitte d semiannually. " 65 . Sectio n 60.34 4 i s revised t o rea d a s follows : § 60.34 4 Tes t method s an d procedures . (a ) I n conductin g th e performance. , test s require d i n § 60.8 , th e owne ror ' operato rshal l us e a s referenc e method s an d procedure s th e tes tmethod s i n Appendi x A o f

thi s parto rothe r method s an d procedure s a s specifie d i n this section , excep ta s provide d i n § 60.8(b) . (b ) Th e owne ro roperato rshal l determin e complianc e wit h th e . particulat e matte rstandard s i n § 60.342(a ) a s follows : (1 ) Th e emissio n rat e (E ) o f particulat e matte rshal l b e compute d fo reac h run usin g th e followin g equation : E=(c„Qrt)/PK) where : • . E=emissio n rat

e o f particulat

e matter, kg/M g (lb/ton ) o f ston e feed . c,=concentratio n o

f particulat

e matter, g/dsc m (g/dscf) . Q«i=volumetri cflo wrat

e o f effluen tgas , - dscm/h r(dscf/hr) . P=ston e fee d rate , Mg/hr(ton/hr) . R=conversio n factor, 100 0 g/k g (453. 6 g/lb) . (2 ) Metho d 5 shal l b e use d a tnegative pressur e fabri cfilters an d othe rtype s o f contro l device s an d Metho d 5 D shal l b e use d a s positive-pressur e fabri cfilters t o determin e th e particulat e matte r concentratio n (c 8 ) ari d th e volumetri c flo wrat e (Qs J o f

th e effluen tgas . Th e samplin g tim e an d sampl e volum e fo r eac h ru n shal l b e a tleas t6 0 minute s an d 0.9 0 dsc m (31. 8 dscf) . (3 ) Th e monitorin g devic e o f § 60.343(d ) shal l b e use d t o detennin e th e ston e fee d rat e (P ) fo reac h run . (4 ) Metho d 9 an d th e procedure s i n § 60.1 1 shal l b e use d t o determin e opacity . (c ) Durin g th e particulat e matte rrun , th e owne ro roperato rshal l us e th e monitorin g device s i n § 60.343(c ) (1 ) an d (2 ) to determin e th e averag e pressur e los s o f th e ga s strea m throug h th e scrubbe ran d di e averag e scrubbin g liqui d suppl y pressure . 66 . Sectio n 60.37 4 i s revise d t o rea d a s follows : § 60.37 4 Tes tmethod s an d procedures . (a ) I n conductin g th e performanc e test s require d i n § 60.8 , th e owne ro r operato rshal l us e a s referenc e method s an d procedure s th e tes tmethod s i n Appendi x A o f

dii s parto rothe r method s an d procedure s a s specifie d i n thi s section , excep ta s provide d i n § 60.8(b) . (b ) Th e owne ro roperato rshall , determin e complianc e wit h th e lea d standard s i n § 60.372 , excep t § 60.372(a)(4) , a s follows ; (1 ) Metho d 1 2 shal l b e use d t o determin e th e lea d concentratio n and , i f applicable , th e volurnetri cflowrate . (Qsda ) o f th e effluen tgas . Th e samplin g tim e an d sampl e volum e fo reac h ru n shal l b e a tleas t6 0 minute s an d 0.8 5 dsc m (3 0 dscf) . (2 ) Whe n differen toperation s i n a three-proces s operatio n facilit y ar e ducte d t o separat e contro l devices , th e lea d emissio n concentratio n (C ) fro m th e facilit y shal l b e determine d a s follows :P.1 9

667 6 Federa l Registe r / Vol

. 54 , No
. 2 9 /

Tuesday

. Februar y 14 , 198 9 / Rule s an dRegulation s

NN : C= ( X (C.OdJ] /

I C U a= l a = l

where : C=concentratio no

f lea demission s fo

r th e entir e facility , mg/dsc m(gr/dscf)

. C,=concentratio n oflea demission s fro m facilit y "a" , mg/dsc m(gr/dscf)

. Q^=yolurnetricflo w rat e o f effluen t ga s fro mfacilit y "a" , dscm/h r

(dscf/hr)

. N=tota l number

o f contro l device s t o whic h separat e operation s i nth e facilit y ar e

. ducted

. • (3 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. Th e opacit y number s shal l b e rounde dof

f t o di e neares t

whol e percentage
. (c ) Th e owne r

o r operato r shal l determin e complianc e wit hth e lea d standar di n§ 60.372(a)(4 ) a s follows : (1 ) Th e emissio n rat e (E ) fro mlea d oxid e manufacturin g facilit y shal l b e compute dfo r

eac hru n usin g th e followin g equation :

E= ( M

I i= l CPMCUM PK )

where : E=emissio nrat e oflead , mg/kg (lb/ton ) o f lea dcharged

. Cpn=concentratio n o

f lea dfro memissio n point "i, " mg/dscm

. Q«ti=volumetri c flow rat e o f effluen t ga s fro memissio n point

"i, " dscm/h r

(sdcf / hr)

. M=numbe r

o f emissio npoint s i

nth e affecte d facility

. P=lea dfeedrat e t o th e facility , kg/h r (ton / hr)

. K=conversio nfactor , 1.0 mg/mg (453.60 0 mg / lb)

. (2 ) Metho d1 2 shal l b e use dt o detennin e th e lea dconcentratio n(Cp^ ) ari dth e volumetri c flo w rat e (Qsd ) o f th e

- effluen t gas . Th e samplin g tim e an d sampl e volum e fo r

eac hru nshal l b e a t leas t 6 0 minute s an d0.8 5 dsc m(3 0 dscf)

. (3 ) Th e averag e lea dfee drat e (P ) shal l b e determine dfo r

eac hru nusin g th e followin g equation : P=NW/ 0 where : N=numbe r

o f lea dpig s (ingots ) charged

. W=averag e mas s o

f apig

. k g (ton)

. ©=duratio n o

f run , hr

. §60.38 5 [Amended ] 67
. I n§ 60.385(c)

. th e word s "those measurement s recorded " ar e revise dto
. . rea d"th e averag e obtained"

. 68

. Sectio n60.38 6 i s revise dt o rea da s follows : . ]. § 60.38 6 Tes t method s an d procedures ! (a ) I nconductin g th e performanc e test s require di n§ 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s tiie tes t mediod s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r shal l determin e complanc e wit htile particulat e matte r

standard s § 60.38 2 a s follows : (1 ) Metho d5 o r

1 7 shal l b e use dt o determin e th e particulat e matte r concentration

. Th e sampl e volum e fo r eac hru nshal l b e a t

leas t 1.7 0 dsc m(6 0 dscf)

. Th e samplin g prob e an dfilte r holde r o f Metho d5 ma y b e operated : withou t heater s if

th e ga s strea mbein g sample di s a t

ambien t ternperature : Fo r ga s stream s abov e ambien t temperature , th e Metho d5 samplin g trai n shal l b e operate dwit haprob e an dfilter temperatur e slighd y abov e th e effluen t
. temperatur e (u p t o amaximu mfilte r temperatur e o f

121° C (250"F) ) i n orde r t o preven t wate r condensatio n o nth e filter. (2 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacit y fro mstac k

emission s an d proces s fugitiv e emissions

. Th e observe r shal l rea dopacit y onl y whe n emissions , ar e clearl y identifie da s emanatin g solel y fro mth e affecte dfacilit y bein g observed

. {c ) T o compl y wit h§ 60.385(c)

. the

. . owne r o r operato r

shal l us e tiie; . monitorin g device s i n § 60.3284(a ) an d (b ) t o determin e th e pressur e los s o f th e ga s strea mthroug hth e scrubbe r ari d scrubbin g liqui dflow rat e a t an y tim e durin g eac hparticulat e matte r run , an d

. th e averag e o f

tile thre e determination s ' shal l b e computed

. 69
. Sectio n60-404 i s revise dt o rea da s follows : § 60.40 4 Tes t method s an d procedures . (a ) I n conductin g th e performanc e .. . test s require di n§ 60.8 , th e owne r o r operato r

shal l us e a s referenc e method s , an dprocedure s th e tes t method s i n Appendi x A o f

thi s part , o r

othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide dfo r

i n. « §60.8(b).•'.,.',

- :

. . ,

• . • , ; •],-• ' : ,;{b ) Th e owne r

o r operato r

shal l -i

. ' determin e complianc e wit hth e '•• particulate , matte r

standard s i n § 60.40 2 a s follows : .•••• • (1 ) Th e emissio nrat e (E ) o f particulat e matte r shal l b e compute dfo r

eac hru n usin g th e followin g equation : E=(c > Q Jd )/(PK )

. where : E=emissio n rat e o

f particulat e matter , kb / M g (lb/ton ) o

f phosphat e rock

feed...

. c b =concentratio n o

f particulat e matter , g / dsc m(g/dscf) ; Q l o=volumetri c flow rat e of effluen t gas , dscm/h r (dscf/hr) : P=phosphat e roc k

fee drate , Mg/hr

(ton/hr)

. K=conversio n factor , 100 0 g/k g (453.6.g/lb)

. (2 ) Metho d5 shal l b e use dt o determiri e th e particulat e rriatte r concentratio n (e j an dvolumetri c flow rat e (QJ) o f

th e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r eac hru n shal l b e a t

leas t 6 0 minute s an d 0.8 5 dsc m(3 0 dscf)

. (3 ) Th e devic e o f

§ 60.403(d ) shal l b e use dt o determin e th e phosphat e roc k fee drat e (P ) fo r

eac hrun . (4 ) Metho d9 an dth e procedure s i n §60.1 1 shal l b e use dt o determin e opacity

. (c ) T o compl y wit h§ 60.403(f) , if applicable , th e owne r

o r operato r

shajl

. us e th e monitorin g devicesi n § 60.403(c ) (1 ) an d(2 ) t o determin e th e averag e pressur e los s o f

th e ga s strea mthroug h th e scrubbe r

an dth e averag e scrubbin g • suppl y pressur e durin g tiie particulat e matte r runs . . , . , . : . , . , ;

.: 70

. Sectio n 60.42 4 i s revise dt o rea da s • •follows:' : •'

. •;' • \

. \ { •'..•.•.- -

. - . § 60.42 4 Tes t method s an d procedures . (a ) Iri.conduttirig'th e performanc e test s require di n§ 60.8 , th e owne r or . operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n , ; § 60.8(b)

. ''••.:•' :P.2 0



### Federa l JRegister

. /

Vol.

. 54 , No
. 2

9 /Tuesday , February

. 14 , 198 9 /Rule s an dRegulations , ; 

### 667 7 (b ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n § 60.42 2 a s follows : (1 ) Th e emissio n rat e (E ) o f particulat e matte r shal l b e compute dfo r eac hru n usin g th e followin g equation : [ E=(c,Q^)/(PK ) .,;,.

_: : f •„-'. ; .....-...'.

. V where : E=emissio n rat e o

f particulat e matter , kg/M g (lb/ton ) o f ammoniumsulfate produced

. :

. c,=concentratio n o

f particulat e matter , g / dsc m(g/dscf)

. . QM= volumetric flow rat e o f effluen t gas , dscm/h r (dscf/hr)

.

. P=productiorirat e o

f ammoniumsulfate , Mg/ hr (ton/hr)

. Reconversio n factor ! 100 0 g/k g (453. 6 g/lb)

. (2 ) Metho d5 shal l b e use dt o determiri e th e particulat e matte r concentratio n (c dan dvolumetri c flow, rat e (Q„i ) o f

th e effluen t

gas . Th e samplin g tim e an dsampl e volum e fo r . eac hru n shal l b e a t

leas t 6 0 minute s an d 1.5 0 dsc m(5 3 dscf)

. (3 ) Direc t

measuremen t

usin g produc t weig hscale s o r

compute dfro mmateria l balanc e shal l b e use dt o determin e th e rat e (P ) o f

th e ammoniu msulfat e production

. I f

productio n rat e i s determine db y materia l balance , th e followin g equation s shal l b e used : (i ) Fo r syntheti c an dcok e ove n by

produc t ammoniu msulfat e plants:

. P=ABCI C where : A=sulfuricaidflowrat e t o thereactor / crystallize r

average dove r

th e tim e . perio dtake n to conduc t

th e run , liter

/

. min

. B=aci ddensity ( afunctio n o f aci dstrengt

h an dtemperature) , g/cc

. C=aci dstrength , decimal fraction ;

. K'=conversio n factor , 0.080 8 (Mg-niin-cc)/(g

hr-liter) [0.089 1 (ton-min-cc)/(g-hr-liter)]

. (ii ) Fo r caprolacta mby-produc t ammoniu msulfat e plants : • . . . P=DEFK " where:

. ! ' D=tota l combine dfee dstrea mflow rat e t o th e ammoniumcrystallize r befor e th e

- point wher e an y recycl e stream s ente r th e strea maverage dover th e time perio d take n t o conduc t

th e tes t run , liter/min , E=densit y o

f th e proces s strea msolution , g/

. liter

. F=percen t

mas s o f ammoniumsulfate i n th e proces s solution , decimal fraction

. Reconversio n factoi

d6. 0 x IO" 5 (Mg-min) /

• (g-hr ) [&61 4 xl0- s (ton-miri)/(g-hr)]

. (3 ) Metho d9 an dthe procedure s i n § 60.1 1 shal l b e use dt o determin e th e opacity

. 71

. Sectio n 60.47 4 i s revise dt o rea da s follows : § 60.47 4 Tes t method s an dprocedures

. (a ) Fo r saturators , th e owne r

o r operato r shal l conduc t

performanc e . test s require di n § 60. 8 a s follows : (1 ) I f th e final produc t

i s shingl e o r mineral-surface drol l roofing , th e test s shal l b e conducte dwhil e 106.6-kg (235 : lb ) shingl e i s bein g produced

. (2 ) I f th e final produc t

i s saturate dFel

t o r srfiooth-surfacedrol l roofing , the'test s shal l b e conducte dwhil e 6.8-kg (15-lb ) fel t i s bein g produced

. (3 ) If th e final produc t

i s fiberglass shingle , th e tes t

shal l b e conducte d whil e anomina l 100-k g (220-lb ) shingl e i s bein g produced.

. (b ) Iri conductin g th e performanc e test s requiredi n § 60.8 , th e owne r o r operato r shal l us e a s referenc e methods , an dprocedure s th e tes t methods , in ' Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (c ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standard s i n §60.47 2 - a s follows : (1 ) Th e emissio n rat e (E ) o f particulate , matte r shal l b e compute dfo r eac hru n usin g th e followin g equation : E=(c,Q 8Q )/(PK) where : - E=emissio n rat e o

f particulat e matter , kg/ Mg
. c s =concentratio n o

f particulat e matter , g / dsc m(g/dscf)

. Q sd =volumetri c flow rat e o f effluen t gas , dscm/h r (dscf/hr)

. P=asphal t

roofing productio n rat e or asphalt ' chargin g rate , Mg/h r

(ton/hr)

. K=conversio n factor , 100 0 g/kg (907.2/(g

Mg)/{kg-ton)]

. (2 ) Metho d5 A shal l b e use dt o determin e th e particulat e rnatte r concentratio n (c s ) ari dvolumetri c flo w ' rat e (Qsd ) o f th e effluen t

gas . Fo r a saturator , th e samplin g time ari dsampl e ; volum e fo r

eac hru n shal l b e a t

leas t 120

. minute s an d3-00 dsc m(10 6 dscf) , ari d fo r th e blowin g still , a t

leas t 9 0 minute s o r th e duratio n o f

th e coatin g blo w o r non-coatin g blow , whicheve r i s greater , an d2.2 5 dsc m(79. 4 dscf)

. (3 ) Fo r th e saturator , th e asphal t roofin g productio n rat e (P ) fo r eac hru n shal l b e determine da s follovys ; Th e amoun t o f asphal t roofin g produce do n th e shingl e o r

saturate dfel t

proces s line s shal l b e obtaine db y direc t measurement
. Th e asphal t roofin g productio n rat e i s th e amoun t produce d divide db y th e tim e take n fo r th e run . (4 ) Fo r th e blowin g still , th e asphal t chargin g rat e (P ) shal l b e compute dfo r eac hru n usin g th e followin g equation : P=(Vd)/(K ' 0) where : P=asphal t chargin g rat e to blowin g still , Mg/ h r (ton/hr)

. V=volum e o

f asphal t charged , m'fft 3 )

. d=densit y o

f asphalt , kg/m 3 (lib/ft 3 )

. K ' = conversio n factor , 100

0 kg/M g (20

0 lb / ton)

. 0= duratio n o

f tes t run , hr

. (i ) Th e volum e (V ) o f

asphal t charge d shal l b e measure db y an y means , accurat e t o withi n 1 0 percent. ' (ii ) Th e densit y (d ) o f

th e asphal t

shal l b e compute dusin g th e followin g equation : d= K " (1056. 1 ^0.617 6 °C) where : °C = temperatur e at

th e star t o f th e blow

. °C K " = 1.0 (0.0624 3 (lb-mVlft'-kg)

. (5 ) Metho d9 an dth e procedures ' i n § 60.1 1 shal l b e use dt o deterrnin e opacity

. (d ) Th e Administrato r

wil l determin e complianc e wit hth e standard s i n § 60.472(a)(3 ) b y usin g Metho d22 , modifie ds o tha t

reading s ar e recorde d ever y 15.second s fo r

aperio do f consecutiv e observation s durin g representativ e condition s (i n accordanc e wit h§ 60.8(c) ) totalin g 6 0 minutes

. A performanc e tes t

shal l consis t

o f on e run . (e ) Th e owne r

o r operato r

shal l us e th e monitorin g devic e i n § 60.473 (a ) o r (b ) t o monito r

an drecor dcontinuousl y th e temperatur e durin g th e particulat e matte r ru n an dshal l repor t

th e result s t o th e Administrato r

wit hth e performanc e tes t results

. (f ) If a t alate r dat e th e Owne r

o r operato r believe s th e emissio n limit s i n § 60.47 2 (a ) an d(b ) ar e bein g me t eve n

. thoug hth e temperatur e rneasu're din. , accordanc e with.§60.47 3 (a ) an d(b ) i s . exceedin g tha t

measure ddurin g th e . . performanc e test , h e ma y submi t a. writte n reques t

t o th e Administrato r

to ' repea t the'performanc e tes t

an d procedur e outline di n paragrap h(c ) df ; thi s section

. " " '
• (g ) If fue l oi l i s t o b e use dt o fir e an ' afterburne r

use dt o contro l emission s fro mablowin g still , th e owne r o r operato r ma y petitio n th e Administrato r i n accordanc e wit h§ 60.11(e ) o f th e Genera l Provision s t o establis ha n opacit y standar dfo r

th e blowin g stil l
• tha t wil l b e th e opacit y standar dwhe n . fue l oi l i s use dt o fir e th e afterburner

. T o obtai n thi s opacit y standard , th e owne r o r operato r

mus t reques t th e Administrato r

t o determin e opacit y

. durin g a n initial , o r

subsequent , performanc e tes t

whe n fue l oi l i s use dt o fir e th e afterburner

. Upo n receip t o f th e result s o f

th e performanc e test , th e Administrato r

wil l mak e afindin g concernin g complianc e wit hth e mas s standar dfo r

th e blowin g still

. I

f th e Administrato r

find s tha t

th e facilit y wa sP.2 1

667 8 Federa l Registe r/ Vol . 54 , No . 2 9 /

Tuesday , Februar y 14 , 1989 / Rule s an d Regulation s i n complianc e wit h th e mas s standar d durin g th e performanc e tes tbutfaile d t o mee tth e zer o opacit y standard , th e Administrato rwil l establis h an d promulgat e i n th e Federa l Registe ra n opacit y standar d fo rtiie blowin g stil l tha twil l b e th e opacit y standar d whe n fue l oi l i s use d t o fire th e afterburner . Whe n th e afterburne ri s fire d wit h natura l gas , th e zer o percen topacit y remain s th e applicabl e opacit y standard . 72 . Sectio n 60.48 5 i s revise d t o rea d a s follows : § 60.48 5 Tes tmethod s an d procedures . (a ) I n conductin g th e performanc e test s require d i n § 60.8 , th e owne ro r operato rshal l us e a s referenc e method s an d procedure s th e tes tmethod s i n Appendi x A o f

thi s par to rothe r method s an d procedure s a s specifie d i n thi s section , excep ta s provide d i n § 60.8(b) . (b ) Th e owne ro roperato rshal l determin e complianc e wit h th e standard s i n §§60.482,60.483 , an d 60.48 4 a s follows : (1 ) Metho d 2 1 shal l b e use d t o determin e th e presenc e o f leakin g sources . Th e instrumen tshal l b e calibrate d befor e us e eac h da y o f it s us e b y th e procedure s specifie d i n Metho d 21 . Th e followin g calibratio n gase s shal l b e used : (i ) Zer o ai r(les s tha n 1 0 pp m o f hydrocarbo n i n air) ; an d (ii ) A mixtur e o f

methan e o rn-hexan e an d ai ra taconcentratio n o f about , bu t les s than , 10,00 0 pp m methan e o rn hexane . (c ) Th e owne ro roperato rshal l determin e complianc e wit h th e n o detectabl e emissio n standard s i n § § 60.482-2(e) . 60.482-3(i) , 60.482-4 , 60.482-7(f) , an d 60.482-10(e ) a s follows : (1 ) Th e requirement s o f paragrap h (b ) shal l apply . (2 ) Metho d 2 1 shal l b e use d t o determin e th e backgroun d level . Al l potentia l lea kinterface s shal l b e traverse d a s clos e t o tile interfac e a s possible . Th e arithmeti cdifferenc e betwee n th e maximu m concentratio n indicate s b y th e instrumen tan d th e backgroun d leve l i s compare d wit h 50 0 pp m fo rdeterminin g compliance . (d ) Th e owne ro roperato rshal l tes t eac h piec e o f

equipmen tunles s h e demonstrate s tha taproces s uni ti s no t i n VO C series , i.e. , tha tth e VO C conten t woul d neve rb e reasonabl y expecte d to excee d 1 0 percen tb y weight . Fo r purpose s o f

thi s demonstration , th e followin g method s an d procedure s shal l b e used : (1 ) Procedure s tha tconfor m t o th e genera l method s i n AST M E-260 , E-168 , E-16 9 (incorporate d b y reference—se e § 60.17 ) shal l b e use d t o determin e th e percen tVO C conten ti n th e proces s flui d tha ti s containe d i n o rcontact s apiec e o f equipment . (2 ) Organi ccompound s tha tar e considere d b y th e Administrato rt o hav e negligibl e photochemica l reactivit y ma y b e exclude d fro m th e tota l quantit y o f organi ccompound s i n determinin g th e . VO C conten to f

th e proces s fluid. (3 ) Engineerin g judgmen tma y b e use d t o estimat e th e VO C content , i f apiec e o f equipmen tha d no tbee n show n previousl y t o b e i n service . I f th e Administrato rdisagree s wit h th e judgment , paragraph s (d ) (1 ) an d (2 ) o f thi s sectio n shal l b e use d t o resolv e th e disagreemen t (e ) Th e owne ro roperato rshal l demonstrat e tha ta n equipmen ti s i n ligh tliqui d servic e b y showin g tha tal l th e followin g condition s apply : (1 ) Th e vapo rpressur e o f on e o rmor e o f th e component s i s greate rtha n 0. 3 kP aa t2 0 * C Standar d referenc e text s o r AST M D-287 9 (incorporate d b y reference—se e § 60.17 ) shal l b e use d t o determin e th e vapo rpressures . (2 ) Th e tota l concentratio n o f th e pur e component s havin g avapo rpressur e greate rtha n 0. 3 kP aa t2 0 " C i s equa l t o o rgreate rtha n 2 0 percen tb y weight . (3 ) Th e fluid i s aliqui d a toperatin g conditions . (f ) Sample s use d i n conjunctio n wit h paragraph s (d) , (e) , an d (g ) shal l b e representativ e o f

th e proces s fluid tha t i s containe d i n o rcontact s th e equipmen to rdi e ga s bein g combuste d i n th e flare . (g ) Th e owne ro roperato rshal l determin e complianc e wit h th e standard s o f

flare s a s follows : (1 ) Metho d 2 2 shal l b e use d t o determin e visibl e emissions . (2 ) A thermocoupl e o ran y othe r equivalen tdevic e shal l b e use d t o monito rth e presenc e o f apilo tflam e i n th e flare . (3 ) Th e maximu m permitte d velocit y (Vouu J fo rair-assiste d flare s shal l b e compute d usin g th e followin g equation : VnMI=8.706-|-0.708 4 H T where : V ram =maximum permitte d velocity , m/sec . H T =ne theating valu e of

the ga s being combusted , MJ/scm . (4 ) Th e ne theatin g valu e (H T ) o f th e ga s bein g combuste d i n aflar e shal l b e compute d a s follows :

H T =KC,H , i = l where : K=conversio n constant , 1.740X10'((g -

. mole)(M])]/[(ppm)(scm)(kcal) . Q=concentratio n o

f sampl e componen

t"i" , • ppm. H,=ne theato

f combustion o

f sample componen

t"i " at2 5 * C and 760 m

m Hg , kcal/g-mole . • (5 ) Metiio d 1 8 an d AST M D2504^ 7 (incorporate d b y reference—se e § 60.17 ) shal l b e use d t o determin e th e concentratio n o f

sampl e componen t"L " (6 ) AST M D 2382-7 6 (incorporate d b y reference—se e § 60.17 ) shal l b e use d t o determin e th e ne thea to f combustio n o f

. componen t"i " i f

publishe d value s ar e no tavailabl e o rcanno tb e calculated . (7 ) Metho d 2 . 2A , 2C , o r2D , a s appropriate , shal l b e use d t o determin e th e actua l exi tvelocit y o f aflare. If needed , th e unobstructe d (free ) cross sectiona l are ao f

th e flare tip shal l b e used . §60.50 2 [Amended ] 73 . In § 60.502(h) , th e referenc e " § 60.503(b) " i s revise d t o rea d " § 60.503(d)" . 74 . Sectio n 60.50 3 i s revise d t o rea d a s follows : § 60.50 3 Tes tmethod s an d procedures . (a ) I n conductin g th e performanc e test s require d i n § 60.8 , th e owne ro r operato rshal l us e a s referenc e method s an d procedure s th e tes tmethod s i n Appendi x A o f

thi s par to rothe r method s an d procedure s a s specifie d i n . thi s section , excep ta s provide d i n § 60.8(b) . Th e three-ru n requiremen to f § 60.8(f ) doe s no tappl y t o thi s subpart . (b ) "Immediatel y befor e th e performanc e tes trequire d t o determin e complianc e wit h § 60.50 2 (b) , (c) , an d (h) , th e owne ro roperato rshal l us e Metho d 2 1 t o monito rfo rleakag e o f vapo ral l potentia l source s i n th e terminal' s vapo rcollectio n syste m equipmen twhil e agasolin e tan ktrucki s bein g loaded . Th e owne ro roperato r shal l repai ral l leak s wit h reading s o f 10,00 0 pp m (a s methane ) o rgreate r befor e conductin g th e performanc e test . (c ) Th e owne ro roperato rshal l determin e complianc e wit h th e standard s i n § 60.50 2 (b ) an d (c ) a s follows : (1 ) Th e performanc e tes tshal l b e 6 hour s lon g durin g whic h a tleas t300,00 0 liter s o f gasolin e i s loaded . I

f thi s i s no t possible , th e tes tma y b e continue d th e sam e da y unti l 300,00 0 liter s o f gasolin e i s loade d o rth e tes tma y b e resume d th e nex tda y wit h anothe rcomplet e 6-hou r period . I n di e latte rcase , th e 300,000 - lite rcriterio n nee d no tb e met . However , a s muc h a s possible , testin g shoul d b e conducte d durin g th e 6-hou rperio d i nP.2 2

Federa l Registe r/

Vol

. 54 , No
. 2 9 /

Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s 667 9 whic hth e highes t

throughpu t

normall y occurs . (2 ) If th e vapo r

processin g syste mi s intermitten t

i noperation , th e performanc e tes t

shal l begi n a t

a referenc e vapo r

holde r leve l an dshal l en da t th e sam e referenc e poin t Th e tes t shal l includ e a t

leas t tw o startup s an d shutdown s o f

th e vapo r

processor . If

thi s doe s no t occu r unde r automaticall y controlle doperations , th e syste mshal l b e manuall y controlled

. (3 ) Th e emissio nrat e (E ) o f tota l organi c compound s shal l b e compute d usin g th e followin g equation :

E=K 2 (V ^ C d ) /

(L106 ) i = l

where : E=emissio n rat e o

f tota l organi c compounds , mg/liter o f gasolin e loaded

. V esl =volum e o

f air-vapo r mixture exhauste d at eac hinterva l "i" , sem . C« 1 =concentratio n o

f tota l organi c compound s a t

eac hinterva l "i" , ppm . L=tota l volume o

f gasolin e loaded , liters , n=numbe r

of testin g intervals

. i— emissio ntestin g interva l o f 5 minutes

. K=densit y o

f calibratio n gas , 1.83X 10 " fo r propan e an d2.41xi0 6 fo r

butane , mg / sem . (4 ) Th e performanc e tes t shal l b e conducte di ninterval s o f 5 minutes

. Fo r eac hinterva l "i" , reading s fro meac h measuremen t

shal l b e recorded , an dth e volum e exhauste d(V^, ) an dth e correspondin g averag e tota l organi c compound s concentratio n(C ci ) shal l b e determined

. Th e samplin g syste m respons e tim e shal l b e considere di n determinin g th e averag e tota l organi c compound s concentratio ncorrespondin g t o th e volum e exhausted

. (5 ) Th e followin g method s shal l b e use dt o determin e th e volum e (V^ ) air

vapo r mixtur e exhauste da t

eac h interval : (i ) Metho d2 B shal l b e use dfo r combustio nvapo r

processin g systems
. (ii ) Metho d2 A shal l b e use dfo r al l othe r vapo r processin g systems
. (6 ) Metho d25 A o r

25 B shal l b e use d fo r determinin g th e tota l organi c compound s concentratio n (C ef ) a t eac h interval

. Th e calibratio nga s shal l b e eithe r propan e o r

butane

. Th e owne r

o r operato r ma y exclud e th e methan e an d ethan e conten t

i nth e exhaus t

ven t b y an y metho d(e.g. , Metho d18 ) approve d b y th e Administrator

. (7 ) T o determin e th e volum e (L) o f gasolin e dispense ddurin g th e performanc e tes t

perio da t

al l loadin g rack s whos e vapo r

emission s ar e controlle db y th e processin g syste m bein g tested , termina l record s o r reading s fro mgasolin e dispensin g meter s a t

eac hloadin g rac k

shal l b e used

. (d ) Th e owne r

o r operato r shal l determin e complianc e wit hth e standar d i n§ 60.502(h ) a s follows : (1 ) A pressur e measuremen t devic e (liqui drhanbmeter , magneheli c gauge , o r equivalen t

instrument) , capabl e o f measurin g u p t o 50 0 m mo f wate r gaug e pressur e wit h±2. 5 m mo f wate r precision , shal l b e calibrate dan d installe do nth e terminal's , vapo r collectio nsyste ma t

apressur e ta p locate da s clos e a s possibl e t o th e connectio nwit hth e gasolin e tan k truck

. (2 ) Durin g th e performanc e lest , th e pressur e shal l b e recorde dever y 5 minute s whil e agasolin e truc k i s bein g loaded ; th e highes t

instantaneou s pressur e tha t

occur s durin g eac hloadin g shal l als o b e recorded

. Ever y loadin g positio nmus t

b e teste da t

leas t onc e durin g th e performanc e test
. §60.64 3 [Amended ] 75

. Sectio n60.643(b ) i s revise da s follows : (b ) Th e emissio nreductio n efficienc y (R ) achieve db y th e sulfu r reductio n technolog y shal l b e determine dusin g th e procedure s i n§ 60.644(c)(1)

. § 60.64 5 [Remove dan dReserved ] 76
. Sectio n60.64 5 i s remove dan d reserved , an d§ 60.64 4 i s revise dt o rea d a s follows : § 60.64 4 Tes t

method s an dprocedures

. (a ) I nconductin g th e performanc e test s requiredi n § 60.8 , th e owne r o r operato r shal l us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

thi s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide d: n paragrap h§ 60.8(b)

. (b ) Durin g aperformanc e tes t require d b y § 60.8 , th e owne r

o r operato r shal l determin e th e minimu mrequire d reductio nefficiencie s (Z ) o f SO 2 emission s a s require di n § 60.64 2 (a ) an d (b ) a s follows : (1 ) Th e averag e sulfu r

fee drat e (X ) shal l b e compute da s follows :

X=KQ, Y where : X=averag e sulfu

r feedrate , lon g ton/day

. Q„=averag e volumetri c flow rate.o f aci dga s fro msweetenin g unit , dscf/day

. Y = averag e H2

S concentratio n i naci dga s feedfro msweetenin g unit , percen t b y volume

. K=(3 2 lb S/lb-mole)/[(100%)(385.3 6 dscf/lb

mole)(2240 lb/lon g ton) ] =3.707X10" ' (2 ) Th e continuou s reading s fromth e proces s flowmeter

shal l b e use dt o determin e th e averag e volumetri c flow rat e (Q„ ) i ndscf/da y o f th e aci dga s fro mth e sweetenin g uni t fo r eac hrun . (3 ) Th e Tutwile r

procedur e i n§ 60.64 8 o r achromatographi c procedur e followin g AST M E-26 0 (incorporate db y reference—se e § 60.17 ) shal l b e use dt o determin e th e H2 S concentratio n i nth e aci dga s fee dfro mth e sweetenin g unit

. A t leas t on e sampl e pe r

hou r (a t equall y space dintervals ) shal l b e take n durin g eac h4-hou r

run . Th e arithmeti c mea no f al l sample s shal l b e th e averag e H2 S concentratio n(Y ) o nadr y basi s fo r th e run . B y multiplyin g th e resul t fro mth e Tutwile r procedur e b y 1.6 2 X IO" 3 , th e unit s gr/10 0 sc f

ar e converte dt o volum e percent
. (4 ) Usin g th e informatio n fro m paragraph s (b ) (1 ) ari d(3) , Table s 1 an d 2 shal l b e use dt o determin e th e require d initia l (Zj ) an dcontinuou s (Z J reductio n efficiencie s o f

SO 2 emissions

. (c ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e SO 2 standard s i n§ 60.64 2 (a ) o r (b ) a s follows : (1 ) Th e emissio n reductio n efficienc y (R ) achieve db y th e sulfu r recover y technolog y shal l b e compute dfo r eac h~ ru nusin g th e followin g equation : . R=(100S)/(S+E ) (2 ) Th e leve l indicator s o r manua l sounding s shal l b e use dt o measur e th e liqui dsulfu r

accumulatio n rat e i nth e produc t storag e tanks

. Reading s take n a t th e beginnin g an den do f eac hrun , th e tan k geometry , sulfu r

densit y a t

th e storag e temperature , an dsampl e duratio nshal l b e use dt o determin e th e sulfu r productio nrat e (S ) i n kg/h r fo r eac hrun . (3 ) Th e emissio nrat e (E ) o f sulfu r shal l b e compute dfo r

eac hru n a s follows : E=CQ*/K

where : C e= concentratio no

f sulfu r equivalen t {SO2+TRS) , g/dscm

. Q«i=volumetri c flow rat e o f effluen t gas , • dscm/hr

. K=conversio n factor , 100 0 g/kg

. (4 ) Th e concentratio n (C c ) o f sulfu r equivalen t

shal l b e th e su mo f

th e SO 2 an dTR S concentrations , afte r bein g converte dt o sulfu r

equivalents

. Fo r

eac h ru nan deac ho f

th e tes t method s specifie di nthi s paragrap h(c ) o f thi s section , th e samplin g tim e shal l b e a t leas t 4 hours

. Metho d1 shal l b e use dt o selec t th e samplin g site

. Th e samplin g poin t i nth e duc t

shal l b e a t

th e centroi dP.2 3

668 0 Federa l Registe r / Vol

. 54 , Nd i 2 9 /Tuesday , Februar y 14 , 198 9 / Rule s and

. Regulation s

o f th e cross-sectio nif

th e are ai s les s tha n5 m 2 (5 4 ft2 ) o r

a t apoin t n o close r t o th e wall s tha n1 m(3 9 in. ) if th e cross sectiona l are ai s 5 m 2 o r more , an dth e centroi di s mor e tha n1 mf 3 9 in. ) fro m th e wall

. (i ) Metho d6 shal l b e use dt o . determin e th e SO 2 concentration

. Eigh t sample s o f

2 0 minute s eac hshal l b e take na t 30-minut e intervals

. T?h e arithmeti c averag e i n mg/dsc mshal l b e th e concentratio nfo r

th e run . Th e concentratio ni nmg/dsc msha'U'b e multiplie db y O. S t o conver t th e result s t o sulfu r equivalent

. - . • - • (ii ) Metho d1 5 shal l b e use dt o determin e th e TR S concentratio nfrom reduction-typ e device s o r wher e th e oxyge nconten t

o f th e effluen t

ga s i s les s tha nI D percen t

b y volume

. Th e samplin g rat e shal l b e a t leas t 3 liters / mi n(0. 1 ft 3 /min ) t o insur e minimu m residenc e tim e i nth e sampl e line

. Sixtee nsample s shal l b e take na t 15

- minut e intervals

. Th e arithmeti c averag e o f al l th e sample s shal l b e th e concentratio nfo r

th e run . Th e concentratio ni npp mTR S a s H2 S shal l b e multiplie db y 1.35 2 x 10~ 6 t o conver t th e result s t o sulfu r

equivalent

. (iii ) Metho d16 A shal l b e use dt o determin e th e TR S concentratio nfro m oxidation-typ e device s o r wher e th e oxyge ncontent.o f

th e effluen t

ga s i s greate r tha n1. 0 percen t

b y volume

. Eigh t sample s o f

2 0 minute s eac hshal l b e take na t 30-minut e intervals

. Th e arithmeti c averag e shal l b e th e concentratio nfo r

th e run . Th e concentratio ni npp mTR S a s H2 S shal l b e multiplie db y 1.35 2 X 10" 6 t o conver t th e result s t o sulfu r

equivalent

. (iv ) Metho d2 shal l b e use dt o determin e th e volumetri c flo w rat e o f th e effluen t

gas . A velocit y travers e shal l b e conducte da t

th e beginnin g an d en do f eac hrun . Th e arithmeti c averag e o f th e tw o measurement s shal l b e use d t o calculat e th e volumetri c flo w rat e (Qui dfo r th e run . Fo r

th e determinatio n o f th e effluen t

ga s molecula r

weight , a singl e integrate dsampl e ove r th e 4-hou r perio dma y b e take nan danalyze do r gra b sample s a t

1-hou r interval s ma y b e taken , analyzed , an daveraged

. Fo r th e moistur e conten t

tw o sample s o f

a t leas t 0.1 0 dsc m(0.3 5 dscf

) an d1 0 minute s shal l b e take n a t th e beginnin g o f th e 4-hou r

ru nan dnea r

th e en do f

th e tim e period

. Th e aridimeti c averag e of th e tw o run s shal l b e th e moistur e conten t fo r di e run . (d ) T o compl y wit h§ 60.646(d)

. th e owne r o r operato r shal l obtai n th e informatio nrequire db y usin g th e monitorin g device s i nparagrap h(b ) of i'f. ) o f thi s section

. §60;64 6 [Amended ] 77. I n § 60.646(a)(2) , th e referenc e " § 60/645(a)(8)"i s revise dt o rea d
" § 6ffl:644(b)(l)"

. 78

. I n § 60.646(a)(4) , th e referenc e " § 60.644(a)(45 " i s revisedt o rea d• " § 60.644(!b){3T

. 79
. I n§ 60:646(d) , th e referenc e "§ : 60v643(b) " i s revise dt o rea d"
" § 60.644(c)(1)"

. 80 : Sectio n60.67 5 i s revise dt o rea da s follows : §60:67 5 Tes t

.method s an dprocedures

. (a ) I n conductin g th e performanc e test s require di n §

. 60.fi , th e owne r o r operato r shal l use^a s referenc e method s ari dprocedures-*i5h: e tes t method s i n . - / Appendi x A o f

thf e par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 6G:'8(b)

. Acceptabl e alternativ e method s an dprocedure s ar e give n i n paragrap h(e ) of

. thi s section

. |t> ) Th e owne r

o r operato r shal l deteomin e compfianc e wit hth e particulat e matte r

standard s i n § 60.272(a ) a s follows : (1 ) Metho d5 o r

Metho d1 7 shal l b e use dt o determin e th e particulat e matte r concentration

. Th e sampl e volum e shal l b e a t leas t 1.7 0 dsc m(6 0 dscf)

. Fo r Metho d'5

. i f

th e ga s strea mbein g sample di s a t

ambien t temperature , th e samplin g prob e an dfilte r ma y b e operate dwithou t

heaters

. If

th e ga s strea mi s abov e ambien t temperature , th e samplin g prob e an dfilter ma y b e operate da t

atemperatur e hig henough , bu t n o highe r

tha n12 1 ° C (25 0 °F)

. t o preven t wate r condensatio n o nth e filter. (2 ) Metho d9 an dth e procedure s i n § 60.1 1 shal l b e use dt o determin e opacity

. (c ) I n determinin g complianc e wit hth e particulat e matte r

.standard s i n§ 60.67 2 (b ) an d(c) , th e owne r

o r operato r shal l us e Metho d9 an dith e procedure s i n § 60.il , wit hth e followin g additions : (1 ) Th e minimu mdistanc e betwee n th e observe r

an dth e emissio n sourc e shal l b e 4.5 7 meter s (1 5 feet)

. (2 ) Th e observe r

shall , whe n possible , selec t apositio n tha t

minimize s interferenc e fro mothe r fugitiv e emissio n source s (e.g. , roa ddust)

. Th e required observe r positio n relativ e t o th e su n (Metho d9 , Sectio n 2.1 ) mus t b e followed

. (3 ) Fo r affecte dfacilitie s usin g we t dus t suppressio nfo r

particulat e matte r control , avisibl e mis t

i s sometime s generate db y th e spray . Th e wate r mis t mus t no t b e confuse dwit hparticulat e matte r emission s an di s no t

t o b e considere davisibl e emission

. Whe na wate r mis t o f thi s natur e i s present , th e observatio no f

emission s i s t o b e mad e a t apoin t i n th e plum e whereth e mis t i s n o longe r

visible

. (d ) I ndeterminin g complianc e wit h § 60.672(e) , th e owne r

o r operato r

shal l us e Metho d2 2 t o determin e fugitiv e emissions

. Th e performanc e tes t shal l b e conducte dwhil e al l affecte dfacilitie s insid e th e buildin g ar e operating

. Th e performance.tes t

foreae hbuildin g shal l b e a t leas t 7 5 minute s i nduration ; wit h eac hsid e o f

the

. buildin g ari dth e roo f bein g observe dfo r

a t leas t 1 5 minutes

. (e ) Th e owne r

o r operato r

ma y us e the ' followin g a s alternative s t o the , " reference method s ari dprocedure s specifie di n thi s section : (1 ) Fo r th e metho dan dprocedur e o f paragrap h(c ) o f

thi s section , i f emission s fro mtw o o r

mor e facilitie s continuousl y interfer e s o tha t th e opacit y o f

fugitiv e emission s fro ma n

. individua l affecte dfacilit y canno t b e read , eithe r

o f th e followin g procedure s ma y b e used : (i ) Us e fo r

th e combine demissio n strea mth e highes t

fugitiv e opacit y standar dapplicabl e t o an y o f th e individua l affecte dfacilitie s contributin g t o th e emission s stream
. (ii ) Separat e th e emission s s o tha t th e opacit y o f

emission s fro meac haffecte d facilit y ca nb e read

. (f ) f o compl y wit h§ 60.676(d)

. th e owne r o r operato r shal l recor dth e measurement s a s require d§ 60.676(c ) usin g th e monitorin g device s i n § 60.67 4 (a ) an d(b ) durin g eac hparticulat e matte r ru n an dshal l determin e th e averages . §60.67 6 [Amended ] 81

. I n§ 60.676(d)

. th e word s "thos e measurement s recorded " ar e revise dt o rea d"th e average ddetermined"

. 82

. Sectio n60.68 5 i s revise dt o rea da s follows : § 60.68 5 Tes t

method s an dprocedures

. (a ) I nconductin g th e performanc e test s require di n§ 60.8 , th e owne r o r operato r shall.us e a s referenc e method s an dprocedure s th e tes t method s i n Appendi x A o f

dii s par t o r othe r method s an dprocedure s a s specifie di n thi s section , excep t

a s provide di n § 60.8(b)

. (b ) Th e owne r

o r operato r shal l conduc t performanc e test s whil e th e produc t wit hth e highes t

los s o n ignitio n (LOI ) expecte dt o b e produced.b y th e affecte dfacilit y i s bein g manufactured

. (c ) Th e owne r

o r operato r

shal l determin e complianc e wit hth e particulat e matte r

standar di n § 60.68 2 a s follows : (1 ) Th e emissio n rat e (E ) o f particulat e matte r shal l b e compute dfo r

eac hru n usin g th e followin g equation :P.2 4

Federa l Registe r

/ Vol

. 54, No
. 2 9 •'/

. Tuesday , Februar y 14 , 198 9 / Rule s an dRegulation s 668 1 E=(C,0 J d)/(P. v .K ) where : E=emissio n rat e o

f particulat e matter , kg/M g (lb/ton)

. C,=concentratio n o

f particulat e matter
. g/dsc m(g/dscf) : Q«i=volumetri c flow.rate o f effluen t gas , dscm/h r (dscf/hr) : P. v .=averageglas s pul l rate; Mg/h r (tori/hr)

. K=conversion : factor , 100 0 g/k g (453. 6 g/lb) ; (2 ) Metho d5 Eshal l b e use dt o determin e di e particulateinatte r concentratio n(C J an dthe

. volumetri c flo w fat e (Qai ) o f

th e effluen t

gas . Th e sampling , tim e an dsampl e volum e shal l b e a t leas t 12 0 minute s an d2.5 5 dsc m (90dscf)

. (3 ) Th e averag e glas s pul l rat e (P.,-, ) fo r th e manufacturin g lin e shal l b e th e arithmeti c averag e o f thre e glas s pul l rat e (P J determination s take na t interval s o f

a t leas t 3 0 minute s durin g eac hrun . Th e individua l glas s pul l rate s (P J shal l b e compute dusin g th e followin g equation : p,=K ' L , WmM (i.p-.fJLpi/ioo) ] ,.;,; ' where : P t =glas s pul l rat e a t

interva l "i" , Mg/h r

(ton/ hr)

. L,=lin e speed, m/mi n (ft/min) , W m .=trimmedma t

width , m(ft)

. . . M=ma t gra mweight,.g/m , Hb/ft3

. LOI=los s on . ignition , weigh t percent.
. K'=conversio n factor,6X10" 5 (min-Mg) / (hr

g ) [3X10" * (min-ton)/lhrrlbl] ' (i ) ASTM'Standar dTes t Metho d D2584-6 8 (Reapprbve d1979 ) (incorporate db y reference—se e § 60.17) , shal l b e use dt o determin e th e LO I fo r eac hrun . (ii ) Lin e spee d(L,) , trimriie dma t widt h (W m ) „ an dma t

gra mweigh t

(M)

. shal l b e determine dfo r

eac hru n fromthe : . proces s informatio no r fro mdirec t measurements
. :. , • • (d ) T o compl y with

- §6p:684(d) , th e owne r o r operato r

shal l record measurement s a s require diri § 60.684.(a ) an d(b ) using , th e monitorin g device s i n § 60.683 (a ) an d(b ) durin g th e particulatematterruns

. > -.'"

- [F RDoc
. 89-3064,File d2^-13-89:8:45 am]:
. -. , • BILLING COD E 6560-50- M .