13339 Hagers Ferry Road

Huntersville, NC 28078-7929

McGuire Nuclear Complex - MG03A2

Phone: 980-875-5245 Fax: 980-875-4349

Order Summary Report

Analytical Laboratory

Order Number: J10090177

Lab Contact: Jason C Perkins

Date: 11/18/2010

Customer Address: 253 Plant Allen Road

Customer Name(s): Don Scruggs, Robbin Jolly, Ray Lidke, Bill Kennedy

Belmont, NC 28012

Phone: 980-875-5348

Report Authorized By:

(Signature)

Program Comments:

Allen Test Burn #1 - October 5

Data Flags & Calculations:

Any analytical tests or individual analytes within a test flagged with an "X" or "1" indicate a deviation from the method quality 

system or quality control requirement. All results are reported on a dry weight basis unless otherwise noted.

Data Package:

This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of 

the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except 

in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The 

order of individual sections within this report is as follows:

Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,

Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & 

Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)

Certification:

The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina 

(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of 

specific methods. 

The results in this report meet NELAP requirements through New York State Department of Health Certification # 11717. 

Certified parameters are designated with an "N" in the analytical report.

Analytical Laboratory 

Page 1 of 15
Sample ID's & Descriptions:

Sample ID Plant/Station

Collection 

Date and Time Collected By Sample Description

2010009141 ALLEN 05-Oct-10 8:30 AM Chris Greene FGD Purge Eff 

2010009143 ALLEN 05-Oct-10 8:35 AM Jeff Womack EQ Tank Eff 

2010009144 ALLEN 05-Oct-10 8:39 AM Jeremy D. BioReactor 1 Inf 

2010009145 ALLEN 05-Oct-10 8:48 AM Jeff Womack BioReactor 2 Inf 

2010009146 ALLEN 05-Oct-10 8:38 AM Jeff Womack BioReactor 2 Eff 

2010009147 ALLEN 30-Sep-10 10:50 AM L. Davis Filter Blk 

2010009148 ALLEN 30-Sep-10 10:50 AM L. Davis Metals Trip Blank 

7 Total Samples

Analytical Laboratory 

Page 2 of 15
COC and .pdf report are in agreement with sample totals 

and analyses (compliance programs and procedures).

All Results are less than the laboratory reporting limits.

All laboratory QA/QC requirements are acceptable.

The Vendor Laboratories have been qualified by the 

Analytical Laboratory

Yes No

Technical Validation Review

Checklist:

Yes No

Yes No

Report Sections Included:

Job Summary Report Sub-contracted Laboratory Results

Sample Identification Customer Specific Data Sheets, Reports, & Documentation

Technical Validation of Data Package Customer Database Entries

Analytical Laboratory Certificate of Analysis Test Case Narratives

Analytical Laboratory QC Report Chain of Custody

Reviewed By: Jenny A Herman Date: 11/18/2010

Yes

Electronic Data Deliverable (EDD) Sent Separately

Analytical Laboratory 

Page 3 of 15
Certificate of Laboratory Analysis

This report shall not be reproduced, except in full.

Order # J10090177

2010009141

Collection Date: 05-Oct-10 8:30 AM

Site: FGD Purge Eff 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

MERCURY (COLD VAPOR) IN WATER

Mercury (Hg) 35.4 ug/L EPA 245.1 18-Oct-10 10:35 N 2.5 TLINN

TOTAL RECOVERABLE METALS BY ICP

Aluminum (Al) 96.6 mg/L SW 6010 18-Oct-10 11:59 N 0.05 MHH7131

Barium (Ba) 1.10 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131

Beryllium (Be) 0.015 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131

Boron (B) 107 mg/L N 0.5 SW 6010 18-Oct-10 11:59 MHH7131

Calcium (Ca) 2120 mg/L N 0.1 SW 6010 18-Oct-10 11:59 MHH7131

Cobalt (Co) 0.087 mg/L N 0.005 SW 6010 18-Oct-10 11:59 MHH7131

Iron (Fe) 106 mg/L N 0.1 SW 6010 18-Oct-10 11:59 MHH7131

Magnesium (Mg) 861 mg/L N 0.05 SW 6010 18-Oct-10 11:59 MHH7131

Manganese (Mn) 3.86 mg/L N 0.005 SW 6010 18-Oct-10 11:59 MHH7131

Molybdenum (Mo) 0.027 mg/L 0.005 SW 6010 18-Oct-10 11:59 MHH7131

Sodium (Na) 43.2 mg/L N 0.05 SW 6010 18-Oct-10 11:59 MHH7131

Tin (Sn) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 11:59 MHH7131

Titanium (Ti) 2.15 mg/L N 0.005 SW 6010 18-Oct-10 11:59 MHH7131

Zinc (Zn) 0.447 mg/L N 0.005 SW 6010 18-Oct-10 11:59 MHH7131

DISSOLVED METALS BY ICP-MS

Selenium (Se) 978 ug/L EPA 200.8 19-Oct-10 12:17 N 5 KRICHAR

TOTAL RECOVERABLE METALS BY ICP-MS

Antimony (Sb) 10.7 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR

Arsenic (As) 162 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Cadmium (Cd) < 10 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Chromium (Cr) 151 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Copper (Cu) 172 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Lead (Pb) 135 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Nickel (Ni) 281 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Selenium (Se) 1320 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Silver (Ag) < 10 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Thallium (Tl) < 10 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Vanadium (V) 168 ug/L N 10 EPA 200.8 28-Oct-10 11:10 KRICHAR

Zinc (Zn) 384 ug/L N 20 EPA 200.8 28-Oct-10 11:10 KRICHAR

TOTAL DISSOLVED SOLIDS

Vendor Parameter Complete V_PRISM

Analytical Laboratory 

Page 4 of 15
Certificate of Laboratory Analysis

This report shall not be reproduced, except in full.

Order # J10090177

2010009143

Collection Date: 05-Oct-10 8:35 AM

Site: EQ Tank Eff 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

MERCURY (COLD VAPOR) IN WATER

Mercury (Hg) 16.4 ug/L EPA 245.1 18-Oct-10 10:37 N 2.5 TLINN

TOTAL RECOVERABLE METALS BY ICP

Aluminum (Al) 41.0 mg/L SW 6010 18-Oct-10 12:03 N 0.05 MHH7131

Barium (Ba) 0.642 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131

Beryllium (Be) 0.006 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131

Boron (B) 82.8 mg/L N 0.05 SW 6010 18-Oct-10 12:03 MHH7131

Calcium (Ca) 2030 mg/L N 0.1 SW 6010 18-Oct-10 12:03 MHH7131

Cobalt (Co) 0.038 mg/L N 0.005 SW 6010 18-Oct-10 12:03 MHH7131

Iron (Fe) 41.6 mg/L N 0.01 SW 6010 18-Oct-10 12:03 MHH7131

Magnesium (Mg) 78.7 mg/L N 0.05 SW 6010 18-Oct-10 12:03 MHH7131

Manganese (Mn) 1.76 mg/L N 0.005 SW 6010 18-Oct-10 12:03 MHH7131

Molybdenum (Mo) 0.018 mg/L 0.005 SW 6010 18-Oct-10 12:03 MHH7131

Sodium (Na) 39.1 mg/L N 0.5 SW 6010 18-Oct-10 12:03 MHH7131

Tin (Sn) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 12:03 MHH7131

Titanium (Ti) 1.10 mg/L N 0.005 SW 6010 18-Oct-10 12:03 MHH7131

DISSOLVED METALS BY ICP-MS

Selenium (Se) 596 ug/L EPA 200.8 19-Oct-10 12:21 N 5 KRICHAR

TOTAL RECOVERABLE METALS BY ICP-MS

Antimony (Sb) < 10 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR

Arsenic (As) 75.9 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR

Cadmium (Cd) < 10 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR

Chromium (Cr) 65.7 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Copper (Cu) 65.8 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Lead (Pb) 62.6 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Nickel (Ni) 114 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Selenium (Se) 870 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Silver (Ag) < 10 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Thallium (Tl) < 10 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Vanadium (V) 72.2 ug/L N 10 EPA 200.8 28-Oct-10 11:21 KRICHAR

Zinc (Zn) 145 ug/L N 20 EPA 200.8 28-Oct-10 11:21 KRICHAR

2010009144

Collection Date: 05-Oct-10 8:39 AM

Site: BioReactor 1 Inf 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

TOTAL RECOVERABLE METALS BY ICP

Aluminum (Al) 0.011 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

Barium (Ba) 0.186 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

Beryllium (Be) < 0.005 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

Analytical Laboratory 

Page 5 of 15
Certificate of Laboratory Analysis

This report shall not be reproduced, except in full.

Order # J10090177

Boron (B) 72.2 mg/L SW 6010 18-Oct-10 12:07 N 0.5 MHH7131

Calcium (Ca) 1830 mg/L SW 6010 18-Oct-10 12:07 N 0.1 MHH7131

Cobalt (Co) < 0.005 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

Iron (Fe) < 0.01 mg/L SW 6010 18-Oct-10 12:07 N 0.01 MHH7131

Magnesium (Mg) 743 mg/L SW 6010 18-Oct-10 12:07 N 0.05 MHH7131

Manganese (Mn) 0.210 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

Molybdenum (Mo) 0.008 mg/L SW 6010 18-Oct-10 12:07 0.005 MHH7131

Sodium (Na) 37.1 mg/L SW 6010 18-Oct-10 12:07 N 0.5 MHH7131

Tin (Sn) < 0.05 mg/L SW 6010 18-Oct-10 12:07 N 0.05 MHH7131

Titanium (Ti) < 0.005 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

DISSOLVED METALS BY ICP-MS

Selenium (Se) 495 ug/L EPA 200.8 19-Oct-10 12:24 N 5 KRICHAR

TOTAL RECOVERABLE METALS BY ICP-MS

Antimony (Sb) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR

Arsenic (As) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR

Cadmium (Cd) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR

Chromium (Cr) < 10 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Copper (Cu) < 10 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Lead (Pb) < 10 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Nickel (Ni) 13.9 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Selenium (Se) 666 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Silver (Ag) < 10 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Thallium (Tl) < 10 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Vanadium (V) < 10 ug/L N 10 EPA 200.8 27-Oct-10 15:27 KRICHAR

Zinc (Zn) < 20 ug/L N 20 EPA 200.8 27-Oct-10 15:27 KRICHAR

2010009145

Collection Date: 05-Oct-10 8:48 AM

Site: BioReactor 2 Inf 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

TOTAL RECOVERABLE METALS BY ICP

Aluminum (Al) 0.066 mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131

Barium (Ba) 0.196 mg/L N 0.005 SW 6010 18-Oct-10 12:11 MHH7131

Beryllium (Be) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 12:11 MHH7131

Boron (B) 70.4 mg/L N 0.5 SW 6010 18-Oct-10 12:11 MHH7131

Calcium (Ca) 1920 mg/L N 0.1 SW 6010 18-Oct-10 12:11 MHH7131

Cobalt (Co) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 12:11 MHH7131

Iron (Fe) 0.209 mg/L N 0.01 SW 6010 18-Oct-10 12:11 MHH7131

Magnesium (Mg) 745 mg/L N 0.05 SW 6010 18-Oct-10 12:11 MHH7131

Manganese (Mn) 0.374 mg/L N 0.005 SW 6010 18-Oct-10 12:11 MHH7131

Molybdenum (Mo) 0.022 mg/L 0.005 SW 6010 18-Oct-10 12:11 MHH7131

Sodium (Na) 37.3 mg/L N 0.5 SW 6010 18-Oct-10 12:11 MHH7131

Tin (Sn) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 12:11 MHH7131

Titanium (Ti) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 12:11 MHH7131

TOTAL RECOVERABLE METALS BY ICP-MS

Analytical Laboratory 

Page 6 of 15
Certificate of Laboratory Analysis

This report shall not be reproduced, except in full.

Order # J10090177

Antimony (Sb) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Arsenic (As) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Cadmium (Cd) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Chromium (Cr) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Copper (Cu) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Lead (Pb) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Nickel (Ni) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Selenium (Se) 92.3 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Silver (Ag) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Thallium (Tl) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Vanadium (V) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR

Zinc (Zn) 53.9 ug/L EPA 200.8 27-Oct-10 15:32 N 20 KRICHAR

2010009146

Collection Date: 05-Oct-10 8:38 AM

Site: BioReactor 2 Eff 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

MERCURY (COLD VAPOR) IN WATER

Mercury (Hg) < 1 ug/L EPA 245.1 18-Oct-10 10:40 N 1 TLINN

TOTAL RECOVERABLE METALS BY ICP

Aluminum (Al) 0.040 mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131

Barium (Ba) 0.216 mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131

Beryllium (Be) < 0.005 mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131

Boron (B) 74.9 mg/L N 0.5 SW 6010 18-Oct-10 11:55 MHH7131

Calcium (Ca) 1960 mg/L N 0.1 SW 6010 18-Oct-10 11:55 MHH7131

Cobalt (Co) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 11:55 MHH7131

Iron (Fe) 0.523 mg/L N 0.01 SW 6010 18-Oct-10 11:55 MHH7131

Magnesium (Mg) 736 mg/L N 0.05 SW 6010 18-Oct-10 11:55 MHH7131

Manganese (Mn) 0.465 mg/L N 0.005 SW 6010 18-Oct-10 11:55 MHH7131

Molybdenum (Mo) 0.028 mg/L 0.005 SW 6010 18-Oct-10 11:55 MHH7131

Sodium (Na) 36.6 mg/L N 0.5 SW 6010 18-Oct-10 11:55 MHH7131

Tin (Sn) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 11:55 MHH7131

Titanium (Ti) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 11:55 MHH7131

TOTAL RECOVERABLE METALS BY ICP-MS

Antimony (Sb) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Arsenic (As) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Cadmium (Cd) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Chromium (Cr) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Copper (Cu) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Lead (Pb) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Nickel (Ni) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Selenium (Se) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Silver (Ag) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Thallium (Tl) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Vanadium (V) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR

Zinc (Zn) < 10 ug/L EPA 200.8 27-Oct-10 15:00 N 10 KRICHAR

Analytical Laboratory 

Page 7 of 15
Certificate of Laboratory Analysis

This report shall not be reproduced, except in full.

Order # J10090177

2010009147

Collection Date: 30-Sep-10 10:50 AM

Site: Filter Blk 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

DISSOLVED METALS BY ICP-MS

Selenium (Se) < 1 ug/L EPA 200.8 19-Oct-10 12:28 N 1 KRICHAR

2010009148

Collection Date: 30-Sep-10 10:50 AM

Site: Metals Trip Blank 

Matrix: OTHER

Analyte Result Units Qualifiers RDL Method Analysis Date/Time

Sample #:

Analyst

TOTAL RECOVERABLE METALS BY ICP

Aluminum (Al) < 0.005 mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131

Barium (Ba) < 0.005 mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131

Beryllium (Be) < 0.005 mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131

Boron (B) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 11:15 MHH7131

Calcium (Ca) < 0.01 mg/L N 0.01 SW 6010 18-Oct-10 11:15 MHH7131

Cobalt (Co) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 11:15 MHH7131

Iron (Fe) < 0.01 mg/L N 0.01 SW 6010 18-Oct-10 11:15 MHH7131

Magnesium (Mg) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 11:15 MHH7131

Manganese (Mn) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 11:15 MHH7131

Molybdenum (Mo) < 0.005 mg/L 0.005 SW 6010 18-Oct-10 11:15 MHH7131

Sodium (Na) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 11:15 MHH7131

Tin (Sn) < 0.05 mg/L N 0.05 SW 6010 18-Oct-10 11:15 MHH7131

Titanium (Ti) < 0.005 mg/L N 0.005 SW 6010 18-Oct-10 11:15 MHH7131

TOTAL RECOVERABLE METALS BY ICP-MS

Antimony (Sb) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR

Arsenic (As) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Cadmium (Cd) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Chromium (Cr) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Copper (Cu) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Lead (Pb) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Nickel (Ni) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Selenium (Se) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Silver (Ag) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Thallium (Tl) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Vanadium (V) < 1 ug/L N 1 EPA 200.8 27-Oct-10 15:37 KRICHAR

Zinc (Zn) 3.00 ug/L N 2 EPA 200.8 27-Oct-10 15:37 KRICHAR

Analytical Laboratory 

Page 8 of 15
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample 

Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed 

according to the referenced methods. 

Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case 

narrative.

NC Certification No. 402

SC Certification No. 99012

NC Drinking Water Cert No. 37735

Case Narrative

11/17/2010

Duke Energy Corporation

Jay Perkins

13339 Hagers Ferry Road

Huntersville, NC 28078

Project: Allen - FGD Alternative Fuels Test Burn #1 Daily

Project No.: J10090177

Lab Submittal Date: 10/06/2010

Prism Work Order: 0100197

This is a Revised Report and supercedes the original laboratory report dated 10/13/10. Client Sample ID 

were revised at the request of the client.

Narrative Notes:

Please call if you have any questions relating to this analytical report.

Respectfully,

PRISM LABORATORIES, INC.

VP Laboratory Services Reviewed By

Data Qualifiers Key Reference:

MDL Method Detection Limit

BRL Below Reporting Limit

RPD Relative Percent Difference

*

Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and 

reporting limit indicated with a J.

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543

Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 6

Analytical Laboratory 

Page 9 of 15
Sample Receipt Summary

11/17/2010

Prism Work Order: 0100197

Client Sample ID Lab Sample ID Matrix Date Sampled Date Received

2010009141/FGD Purge Eff 0100197-01 Water 10/05/10 10/06/10

Samples received in good condition at 1.5 degrees C unless otherwise noted.

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543

Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 6

Analytical Laboratory 

Page 10 of 15
Laboratory Report

11/17/2010

Parameter Result Batch

ID

Report

Limit

Analysis

Date/Time

Dilution Method

Factor

Units MDL Analyst

13339 Hagers Ferry Road Project No.: J10090177

Project: Allen - FGD Alternative Fuels 

Test Burn #1 Daily

Duke Energy Corporation

Huntersville, NC 28078

Attn: Jay Perkins

Sample Matrix: Water

Client Sample ID: 2010009141/FGD Purge E

Prism Sample ID: 0100197-01

Prism Work Order: 0100197

Time Collected: 10/05/10 08:30

Time Submitted: 10/06/10 16:25

General Chemistry Parameters

Total Dissolved Solids 8800 mg/L 50 8.7 1 *SM2540 C 10/7/10 13:25 JAB P0J0158

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543

Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 6

Analytical Laboratory 

Page 11 of 15
11/17/10

Level II QC Report

13339 Hagers Ferry Road Project No: J10090177

Project: Allen - FGD Alternative Fuels 

Test Burn #1 Daily

Duke Energy Corporation

Huntersville, NC 28078

Attn: Jay Perkins

Prism Work Order: 0100197

Time Submitted: 10/6/10 4:25:00PM

Result Limit

Reporting

Units Level

Spike

Result

Source

%REC

%REC

Limits RPD

RPD

 Analyte Limit Notes 

General Chemistry Parameters - Quality Control

Batch P0J0158 - NO PREP

Blank (P0J0158-BLK1) Prepared & Analyzed: 10/07/10 

Total Dissolved Solids BRL 50 mg/L

LCS (P0J0158-BS1) Prepared & Analyzed: 10/07/10 

Total Dissolved Solids 972 50 mg/L 1000 97 90-110

Duplicate (P0J0158-DUP1) Source: 0100197-01 Prepared & Analyzed: 10/07/10 

Total Dissolved Solids 8930 50 mg/L 8800 2 20

Sample Extraction Data

NO PREP

Lab Number Batch Initial Final Date

0100197-01 P0J0158 50 mL 50 mL 10/07/10

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543

Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 6

Analytical Laboratory 

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Page 5 of 6

Analytical Laboratory 

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Page 6 of 6

Analytical Laboratory 

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Analytical Laboratory 

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