### Instructions for filling in the Emission Test Template

This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate runs or sampling events for each of the requested constituents. This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. yellow are required. All cells that are shaded in green are populated using drop

- down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls (example: 8100_Unit_2_EmisTestMethods.xls).

Please refer to the following steps when using these spreadsheets.

Boiler Information Worksheet

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the control device configuration.

Emission Data Worksheets

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg Hg+2

### , or if the Ontario

- Hydro Method was used, you would need to enter Hg0

### , HgP, and Hg Volatile Organic HAP and Speciated Semi

-Volatile Organic HAP worksheets allow you to use a drop Constituent field to define as many records as needed to record each HAP that you have results for. General instructions follow for these worksheets:

Boiler Operation Information

1. Please provide the values of all requested parameters for each of test run/sample. 2. Please provide any other supporting information or comments in the Other Supporting Information field.

Fuel Information

1. Please enter what types of fuel are being used in your boiler using the drop

- downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples, then enter an input rate of zero. 2. Please enter the unit of measure using the drop down provided. 3. Please enter the test method used to determine the fuel input rate. 4. Please provide any other information that you feel may be important in the Other Supporting Information field.

Emission Data

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and ppmvd @ 7% O 2 

### (parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please also enter these data.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about emission data from fossil fuel burning power plants and which test methods were used to do so for cases where the test methods are not currently supported by the Electronic Reporting Tool (ERT). This spreadsheet should only be used if the method is not in the ERT or if you do not have access to a lab which performs methods that are in the ERT. You must complete at least 3 separate This spreadsheet is intended to be used for one boiler of one facility. Data for multiple boilers should be handled by using separate copies of this spreadsheet. Fields shaded in down lists. You do not need to populate cells shaded in gray, as they are automatically populated from the Boiler Information worksheet. Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_EmisTestMethods.xls

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

The emission data worksheets are provided for each constituent or constituent family required for this analysis. On each spreadsheet, you must enter boiler operating information during sampling, fuel input information, and emission test results. There are generally 1 to 3 emission test results records to be entered depending on the constituent or constituent family. For example, CO only requires 1 record with 3 sample events, while Mercury requires that you enter both Hg0 

### and , HgP, and Hg+2 

### . However, both the Speciated Volatile Organic HAP worksheets allow you to use a drop

- down provided in the Constituent field to define as many records as needed to record each HAP that you have results for. General instructions

2. Please provide any other supporting information or comments in the Other Supporting Information field.

downs in the Fuel Type Selection field. You may enter up to 4 fuel types. If you are not burning one or more of the fuel types entered in one or more samples,

4. Please provide any other information that you feel may be important in the Other Supporting Information field.

### 1. Some constituents ask for the emission rate results of each run in two different units of measure, while others do not. If emission rate results are requested in two different units of measure (ex. lb/MMBtu (Pounds per million BTU) and

(parts per million by volume dry basis at 7 percent oxygen)), you are required to provide both. 2. Please provide the test method used. This may or may not match the example given in the Test Method Used field. Please ensure that the name includes the owning organization of the test method (ex. U.S. EPA Method 0010). 3. Please provide any other information that you feel may be important in the Other Supporting Information field. 4. If data sheets and QA/QC documentation tables are provided for the test method you are entering data for please alsoEIA

Facility Code Facility Name Boiler ID

2451 San Juan Unit 3Control Device Configuraton

Listed (by

boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICRListed (by boiler) in the Configuration Order Section of the Facility Unit Configurations Section of the Electronic ICREIA

Facility Code Facility Name Boiler ID 2451 San Juan Unit 3

1 5/26/2010 8:10 1 5/26/2010 8:10 2 6/29/2010 10:45 2 6/29/2010 10:45 3 6/30/2010 8:35 3 6/30/2010 8:35 Run Number Test Start Date Test Start TimePlease note QA/QC documentation starting in Column "AI"

Measured Value (μg/dscm) Basis (Wet or Dry)

5/26/2010 11:10 0.071 Dry 5/26/2010 11:10 0.053 Dry 6/29/2010 13:45 0.035 Dry 6/29/2010 13:45 0.035 Dry 6/30/2010 11:35 0.086 Dry 6/30/2010 11:35 0.08 Dry

Test End Time Test End Date Total Vapor Phase Mercury Emission Test ResultsPlease note QA/QC documentation starting in Column "AI"

Test Method Used Data Flag (ADL, BDL, DDL) Test Method

Comments (lb/mmBtu)

U.S. EPA Method 30B 0.0000000607 2411 U.S. EPA Method 30B 0.0000000450 2411 U.S. EPA Method 30B 0.0000000300 2837 U.S. EPA Method 30B 0.0000000290 3837 U.S. EPA Method 30B 0.0000000717 3074 U.S. EPA Method 30B 0.0000000665 3074 Total Vapor Phase Mercury Emission Test Results Steam Output (1000 lb/hr)Fuel Input Rate

4014 16.5 13.4 5.9 1211393 126 403888 4014 16.5 13.4 5.9 1211393 126 403888 4901 13.5 13.7 5.4 1157212 119 496138 4901 13.5 13.7 5.4 1157212 119 496138 5440 13.8 13.6 5.5 1255382 120 540156 5440 13.8 13.6 5.5 1255382 120 540156 Flue Gas Temperature (F) Flue Gas CO 2(%) Flue Gas

O 2(%) Flue Gas

Flow Rate (dscfm) Flue Gas Moisture (%) Total Heat Input (mmBtu/hr)QA /QC Documentation

Fuel Type Units of

Measure Measurement

Method Trap ID Section 1 Mass (ng)
subbituminous lb/hour F-Factor 67759 30.3 subbituminous lb/hour F-Factor 66149 31.1 subbituminous lb/hour F-Factor 66225 23.5 subbituminous lb/hour F-Factor 66245 22.7 subbituminous lb/hour F-Factor 66101 31.6 subbituminous lb/hour F-Factor 67772 30.7

Fuel #1 Other Supporting InformationQA /QC Documentation

Section 2 Mass (ng) Total

Mass (ng) Initial

Spike (ng) Total NonSpike (ng) Sample

Volume (dscm) Volume

Difference (%) Volume Diff. Limit Breaktrough

(%)
1.1 31.4 20 11.4 0.1433 3.630363036 2.2 33.3 20 13.3 0.1455 7.073954984 2.7 26.2 20 6.2 0.1434 11.4893617 2.7 25.4 20 5.4 0.1455 11.89427313 1 32.6 20 12.6 0.1436 3.164556962 0.7 31.4 20 11.4 0.1457 2.280130293 ≤20% of field recovery test Trap #1Breaktrough

Limit Concentration

(μg/dscm) Trap ID Section 1 Mass Section 2

Mass Total

Mass Initial

Spike Total NonSpike
0.079553385 60905 11 0.7 11.7 0 11.7 0.091408935 60894 10 1.6 11.6 0 11.6 0.043235704 fgs01479 3.5 0.6 4.1 0 4.1 0.037113402 fgs01572 4.2 0.6 4.8 0 4.8 0.087743733 60877 11.7 0.5 12.2 0 12.2 0.078242965 fgs01566 11.3 0.5 11.8 0 11.8 ≤10% of Section 1 Hg

mass for Hg conc. >1
μg/dscm: or ≤ 20% of SectionSample

Volume Volume

Difference (%) Volume Diff. Limit Breaktrough (%) Breaktrough Limit Concentration

(μg/dscm)
0.1435 6.363636364 0.081533101 0.1448 16 0.080110497 0.1435 17.14285714 0.028571429 0.1447 14.28571429 0.03317208 0.1438 4.273504274 0.084840056 0.1449 4.424778761 0.081435473 ≤10% of Section 1 Hg mass for Hg conc. >1
μg/dscm: or ≤ 20% of Section 1 for Hg conc. ≤1 ≤20% of field recovery test Trap #2Abs. diff. RD (%) Limit C rec R (%) by Run Ravg(%) Limit

0.00198 1.228977 19.3234 96.6 0.011298 6.587264 21.0825 105.4 0.014664 20.42175 20.0009 100 0.003941 5.60759 18.54 92.3 0.002904 1.682474 19.846 99.2 0.003193 1.999336 19.3014 96.5

≥ 10 % RD mass for Hg conc. >1 μg/dscm: or
≤20% RD or ≤ 0.2 μg/dscm abs.diff. for Hg conc. ≤1 Average Recovery

, between 85 and 115% Measured Spike Recovery ( R )

98.33333333 Paired Trap Agreement (RD)EIA

Facility Code Facility Name Boiler ID

2451 San Juan Unit 3

1 6/29/2010 10:20 6/29/2010 2 6/30/2010 8:32 6/30/2010 3 7/1/2010 8:15 7/1/2010 Run Number Test Start Date Test Start Time Test End DateMeasured Value (ppm) Basis (Wet or Dry)
15:03 0.02 Dry 13:13 0.02 Dry 12:15 0.01 Dry Test End TimeTest Method Used Data Flag (ADL, BDL, DDL) Test Method

Comments U.S. EPA Conditional Test Method 033 (CTM-033) 0.0000175 U.S. EPA Method 320 0.0000154 U.S. EPA Conditional Test Method 033 (CTM-033) 0.0000113 Hydrogen Cyanide Emission Test Results Calculated Emission Rate (lb/mmBtu)2697 4579 10 15.2 4.0 70987500 120 3042 5208 13 13.4 6.0 81060249 125 3124 5313 13 13.5 5.9 82430500 126 Steam Output (1000 lb/hr) Total Heat

Input (mmBtu/hr) Flue Gas Temperature (F) Flue Gas Moisture (%) Flue Gas

CO 2(%) Flue Gas

O 2(%) Flue Gas

Flow Rate (dscfm)Fuel Input

Rate Fuel Type Units of Measure Measurement

Method 462228 subbituminous

lb/hour F-Factor 514532 subbituminous

lb/hour F-Factor 533133 subbituminous

lb/hour F-Factor Other Supporting Information Fuel #1EIA

Facility Code Facility Name Boiler ID 2451 San Juan Unit 3

1 6/29/10 10:49 2 6/30/10 8:35 3 7/1/10 8:15 Run Number Test Start Date Test Start TimeTotal Dissolved Solids (mg solids/liter) Total Suspended Solids (mg solids/liter)
6/29/2010 13:45 33780 153822 6/30/2010 11:35 44680 162854 7/1/2010 12:15 44200 160114

Test End Time Test End DateTest Method Used Data Flag (ADL, BDL, DDL)
Standard Test Method for Filterable and Nonfilterable Matter in W ater ASTM D5907 Standard Test Method for Filterable and Nonfilterable Matter in W ater ASTM D5907 Standard Test Method for Filterable and Nonfilterable Matter in W ater ASTM D5907 Constisuent Emission Test ResultsTest Method Comments

3837 4839 1157212 3074 5444 1255382 3164 5431 1144060 Steam Output (1000 lb/hr) Total Heat Input (mmBtu/hr) Flue Gas Flow Rate (dscfm)Fuel Input Rate Fuel Type Units of Measure Measurement

Method
119 496138 subbituminous lb/hour F-Factor 120 540156 subbituminous lb/hour F-Factor 122 462403 subbituminous lb/hour F-Factor Flue Gas Temperature (F) Fuel #1Other Supporting Information