APPENDI X D CEM S AN D CM S QUALIT Y ASSURANC E PLAN S

### CONTINUOU S EMISSION S MONITORIN G SYSTE M QUALIT Y ASSURANC E PLA N

Prepare dfor : Veoli aE S Technica l Solutions , LL C

Sauget , Illinoi s

Prepare dby : Frankli n Engineerin g Group , Inc . Franklin , Tennesse e

Octobe r 200

8TABL E O F CONTENT S

1. 0 INTRODUCTIO N AN D BACKGROUN D 1

1. 1 DESCRIPTIO N O F CEM S 1 1. 2 OVERVIE W O F REGULATOR Y REQUIREMENT S 2 2. 0 CEM S CALIBRATION S AN D PERFORMANC E 5

2. 1 DAIL Y DRIF T CHECK S 5 2. 2 CALIBRATIO N 8 2. 3 ABSOLUT E CALIBRATIO N AUDI T 1 0 2. 4 INTERFERENC E RESPONS E TES T 1 0 2. 5 RELATIV E ACCURAC Y TES T AUDI T 1 1 3. 0 CEM S MAINTENANC E 1 4

3. 1 DAIL Y SYSTE M AUDI T 1 4 3. 2 SPAR E PART S INVENTOR Y 1 4 3. 3 CALIBRATIO N GA S SUPPL Y AN D CERTIFICATIO N 1 5 3. 4 CORRECTIV E ACTIO N FO RMALFUNCTIONIN G CEM S 1 7 4.0 . INTEGRATIO N O F TH E CEM S WIT H TH E AWFC O SYSTE M 1 8

4. 1 EMISSIO N STANDARD S 1 8 4. 2 DRIF T LIMIT S 1 8 5.0 . RECORDKEEPIN G AN D QUALIT Y ASSURANC E REVIEW S 1 9 6. 0 OPERATO RTRAININ G AN D CERTIFICATIO N 2 1

iINDE X O F TABLE S
TABL E 1 - 1 REGULATOR Y REQUIREMENT S FO RTH E CEM S Q C PROGRA M AN D TH E

CEM S QAPLA N 3 TABL E 2- 1 OVERVIE W O F CEM S PERFORMANC E REQUIREMENT S 6 TABL E 3 - 1 SUMMAR Y O F CONCENTRATIO N REQUIREMENT S FO RCALIBRATIO N GASE S 1 6

LIS T O F APPENDICE S APPENDI X A CEM S DAT A SHEET S AN D CHECKLIST S

i i1. 0 INTRODUCTIO N

Veoli aE S Technica l Solutions , LL C (Veolia ) own s an doperate s tw o fixe dhearth incinerator s (Unit s 2 an d3 ) an datransportabl e rotar y kil n incinerato r (Uni t 4 ) a t it s facilit y locate di n Sauget , Illinois . Thes e incinerator s ar e subjec t

to th e Nationa l Emission s Standard s fo r Hazardou s Ai r

Pollutant s (NESHAP ) fo r Hazardou s Wast e Combustor s (HWCs) , Par t 63 , Subpar

t EE E (§§63.120 0 to 63.1221) . Th e NESHA P fo r HWC s specifie s emission s standard s whic h reflec t emission s performanc e o f maximu m achievabl e contro l technologie s (MACT) , an di s commonl y referre dto a s th e HW C MACT . Fo r eac h incinerator , Veoli autilize s acontinuou s emission s monitorin g syste m(CEMS ) fo r demonstratin g on-goin g complianc e wit h th e carbo n monoxid e (CO ) emissio n standard . Thes e CEM S ar e subjec t to th e requirement s o f th e Appendi x to 4 0 CF RPart 63 , Subpart

EEE— Qualit

y Assurance Procedures for Continuous Emissions Monitors Used for Hazardous Waste Combustors. Thi s pla n ha s bee n develope dper th e CEM S qualit y assuranc e (QA)/qualit y contro l (QC ) requirements . Implementatio n o f thi s pla n wil l ensure tha

t th e CEM S generates , collects , an dreport s vali ddat atha t i s precise , accurate , complete , an do f aqualit y tha

t meet s the requiremen t o f th e HW C MAC T Standar dan dth e applicabl e performanc e specification . 1. 1 Descriptio n o

f CEM S Eac h incinerato r

i s equippe dwit h an EcoChe mAnalytic s MC 3 CEMS , whic h consist s o f th e followin g majo r

components :

• Heate dstac k

sampl e prob e
• Heate dtrace dumbilica l

• Heate dsampl e pump
• EcoChe mMC 3 multicomponen t infrare d(IR ) ga s analyze r
• Zirconiu moxide-base doxyge n analyze r
• Syste mcontrolle r

an ddat aacquisitio n syste m Hot , we t stac k ga s i s draw n throug h th e heate dstac k sampl e prob e an dhea t trace d umbilica l usin g aheate dsampl e pump . Th e samplin g locatio n i s downstreamo f th e induce ddraf

t (ID ) fan . Th e umbilica l supplie s instrumen t ai r to th e filte r

prob e to allo w fo r automate dperiodi c blowback . I t als o supplie s calibratio n gase s throug h the samplin g system . Th e stac k

ga s sampl e i s maintaine da t approximatel y 185° C throug h th e

1samplin g equipmen t an danalyze r

sampl e cel l to preven t th e remova l o f

pollutant s from th e sampl e throug h contac t wit h condense dmoisture . Th e sampl e cel l consist s o f multipl e mirror s tha

t wer e adjuste dan daligne da t th e factor y to se t th e path length appropriat e fo r th e specifi c application . Th e MC 3 multicomponen t I Rphotomete r

use s aGa s Filte r

Correlatio n analytica l techniqu e to continuousl y monito r th e stac k

ga s concentration s o f HC l an dCO . Th e Singl e Bea mDua l Wavelengt h analytica l techniqu e i s use dto continuousl y monito r stac k ga s wate r

vapo r (H2O ) concentrations . A technica l descriptio n an dspecificatio n fo r th e CEM S i s presente di n Sectio n 2. 0 o f th e MC 3 Operations Guide, Section 2.1. 1 document s th e lowes t rang e fo r

eac h componen t an da n accurac y o f

±2 % o f full-scal e value . Th e lowe r threshol di s 1 % o f

th e lowes t range . Thes e technica l specification s documen t tha t th e CEM S i s capabl e o f meetin g th e requirement s o f

th e Appendi x to Part

63 , Subpar

t EE E an dPerformanc e Specificatio n 4 B o f 4 0 CF RPart

60 , Appendi x B . Th e syste mcontrolle r control s th e samplin g syste mtemperatures , purge/blowback , calibratio n checks , dat ahandling , messaging , an dalarms . Th e CEM S controlle r i s integrate dwit h th e incinerato r dat aacquisitio n system , automati c waste fee dcutof f (AWFCO ) system , an dth e mai n contro l system . A l l thre e incinerator s ar e equippe dwit h COS A mode l ZFN-11YA1-2Z 1 O 2 analyzers . Thes e analyzer s ar

e zirconiu moxid e cell s an dar e locate ddownstrea mo f th e I D fan . 1. 2 Overview of

Regulator

y Requirement

s Cross-reference s an dsummarie s o f the applicabl e regulator y requirement s ar e presente d i n Tabl e 1-1 . Thi s tabl e indicate s th e sections , tables , an dfigure s o f thi s documen t

tha t addres s eac h particula r

requirement .

2Tabl e 1- 1

Regulator

y Requirement

s fo rth e CEM S Q C Progra m an d th e CEM S Q A Pla n Regulator

y Reference : Appendi x t

o SubpartEE E of

Par t6 3 Descriptio n CEM S Q A Pla n Section Sectio n 3.1.a. l Check s fo r componen t

failures , leaks , an dother abnorma l condition s 3. 0 3. 1 Sectio n 3.1.a. 2 Calibratio n o f CEM S 2. 2 Sectio n 3.1.a. 3 Calibratio n Drif t determinatio n an dadjustmen t o f CEM S 2.1,2. 2 Appendi x A Sectio n 3.1.a. 4 Integratio n o f CEM S wit h th e AWFC O syste m 4. 0 Sectio n 3.1.a. 5 Preventiv e Maintenanc e o f CEM S (includin g spar e part s inventory ) 3. 0 Appendi x A Sectio n 3.1.a. 6 Dat arecording , calculations , an dreportin g 4. 1 5. 0 Sectio n 3.1.a. 7 Check s o f recor dkeepin g 5. 0 Sectio n 3 . La . 8 Accurac y audi t procedures , includin g samplin g an danalysi s method s 2.3,2. 5 Appendi x A Sectio n 3.1.a. 9 Progra mo f correctiv e actio n fo r

malfunctionin g CEM S 3. 4 Sectio n 3.1.a . 1 0 Operato r trainin g an dcertificatio n 6. 0 Sectio n 3.1. b Reportin g o f excessiv e inaccuracie s 5. 0 Sectio n 3.2. 1 Q A responsibilitie s 5. 0 Sectio n 3.2. 2 Schedule s for : (1 ) dail y check s (2 ) periodi c audit s (3 ) preventiv e maintenanc e (1 ) 3.0,3. 1 (2 ) 2.0 , Tabl e 2- 1 (3 ) 3. 0 Sectio n 3.2. 3 Chec k list s an ddat asheet s Appendi x A Sectio n 3.2. 4 Preventiv e maintenanc e procedure s 3. 0

3Tabl e 1- 1 (Continued ) Regulator

y Requirement

s fo rth e CEM S Q C Progra m and th e CEM S Q A Pla n Regulatory Reference : Appendi x t

o Subpar tEE E of

Par t6 3 Descriptio n CEM S Q A Pla n Section Sectio n 3.2. 5 Descriptio n o f th e media , format , an dlocatio n o f al l record s an dreport s 5. 0 Sectio n 3.2. 6 Provision s fo r revie w o f

th e CEM S data ; revision s o r

update s o f

th e Q A pla n base do n revie w 5. 0 Sectio n 4. 1 Check , record , quantify : (1 ) Zer o Drif t (2 ) Calibratio n Drif t 2. 1 Sectio n 4. 2 Recordin g Requirement s for : (1 ) Zer o Drif t (2 ) Calibratio n Drif t 2. 1 Appendi x A Sectio n 4. 3 Dail y Syste mAudi t 3. 1 Sectio n 4. 4 Dat arecordin g an dreportin g 5. 0 Sectio n 5. 1 Relativ e Accurac y Tes t Audi t (RATA ) 2. 5 Sectio n 5. 2 Absolut e Calibratio n Audi t (ACA ) 2. 3 Sectio n 5. 3 Interferenc e Respons e Tes t (IRT ) 2. 4 Sectio n 5. 4 Excessiv e audi t inaccuracie s Tabl e 2- 1 2. 3 2. 5

42.

0 CEM S CALIBRATION S AN D PERFORMANC E Th e CEM S mus t

b e operated , calibrated , an dmaintaine dto ensur e conformanc e wit h th e Appendi x to Part

63 , Subpar

t EE E an dth e EP A Performanc e Specificatio n 4 B (P S 4B) . Calibratio n drif

t check s an dperformanc e demonstration s ar e performe dperiodicall y o n th e CEM S base do n th e followin g schedule :

• Dail y calibratio n check s fo r determinatio n o f

Calibratio n Drif t

(CD ) an dZer o Drif t (ZD) . • Quarterl y Absolut e Calibratio n Audi t (ACA ) fo r

determinin g calibratio n erro r (CE ) fo r 0 2 , CO , an dHCl . • Annua l Relativ e Accurac y Tes t Audi t (RATA ) fo r

determinin g th e CEM S relativ e accurac y (RA ) fo r

C O emissions . Th e procedures , Q C criteria , correctiv e actions , an drecordkeepin g associate dwit h thes e drif t check s an daudit s ar

e describe di n thi s section . A summary o f th e Q C criteri aan d correctiv e action s i s presente di n Tabl e 2-1 . Blan k dat asheet s ar

e provide di n Appendi x A . 2. 1 Dail y Drif

tChecks Dail y drif

t check s ar

e automaticall y initiate db y th e CEM S controller . Durin g th e automate dcalibratio n sequence , calibratio n gase s ar e injecte dfro mpressurize dcylinder s throug h th e samplin g system . Th e sequenc e start s wit h th e I Ranalyze r zer o ga s tha

t i s fre e o f an y o f th e constituent s analyze db y th e I Ranalyzer . Thi s zer o ga s ma y als o serv e as th e spa n ga s fo r

the integrate dO 2 analyzer . Th e zer o gas flow s throug h th e syste m wit h enoug h tim e allowe dfo r th e analyze r

to full y respon dto th e gas . The n th e analyze r respons e to th e zer o ga s i s recorde dfo r on e minut e an daveraged . Th e nex t calibratio n ga s i n th e calibratio n sequenc e i s th e firs t I Ranalyze r

spa n gas . Thi s span ga s i s a calibratio n standardtha t ha s on e o r

mor e constituen t

concentration s a

t th e analyze r

span valu e (thi s gas ma y als o b e use das th e zer o ga s fo r th e O 2 analyzer) . Th e firs t span ga s flow s throug h th e syste mto allo w th e analyze r enoug h tim e to full y respon dto th e gas . The n th e analyze r

respons e to th e firs t

span ga s i s recorde dfo r on e minut e an daveraged . Thi s i s the n repeate dfo r th e secon dspan ga s an dthe n possibl y athir dspan gas dependin g upo n th e compositio n o f th e span gases . Th e tota l duratio n o f thi s calibratio n sequenc e ha s bee n designe dto no t excee dth e 2 0 minut e maximu mallowabl e CEM S downtim e whil e burnin g hazardou s waste .

5Tabl e 2- 1 Overview of

CEM S Performanc e Requirement s Analyze r Paramete r (Spa n Value ) Q C Paramete r Minimu m Frequency Q C Limi t Correctiv e Actio n H 2 0 (60%) Z D Dail y ±2 % o f span Zer o Adjustmen t

0 2 (25%) Z D an dC D Dail y ±0.5 % 0 2 Zero/Spa n Adjustmen t 0 2 (25%) C D Dail y ±1.0 % 0 2 Shu t of f waste , service/calibrate , conduc t A C A 0 2 (25%) Cumulativ e Spa n

Adjustmen t Pe r

Adjustmen t ±1.5 % 0 2 Shu t of f waste , service/calibrate , conduc t AC A 0 2 (25%) C E Quarterl y 1 0.5 % 0 2 Shu t of f waste , service/calibrate , conduc t RAT A 0 2 (25%)
R A Annuall y 1.0 % 0 2 Shu t of f waste , service/calibrate , repea t RAT A

C O (20 0 ppm) Z D an dC D Dail y ±3% o o f spa n Zero/Spa n Adjustmen t

C O (20 0 ppm) C D Dail y ±5 % o f span fo r 6 out o f 7 da y Shu t

of f waste , service/calibrate , conduc t AC A C O (20 0 ppm) C D Dail y ±6 % o f span Shu t

of f waste , service/calibrate , conduc t AC A C O (20 0 ppm) Cumulativ e Spa n

Adjustmen t Pe r

Adjustmen t ±9 % o f span Shu t

of f waste , service/calibrate , conduc t AC A C O (20 0 ppm) C E Quarterl y 1 5 % Shu t of f waste , service/calibrate , conduc t RAT A C O (20 0 ppm)

R A 2 Annuall y 5 ppmd v @ 7% > O 2 (Se e Sectio n 2.5 ) Shu t of f waste , service/calibrate , conduc t RAT A Th e ACA s fo r

determinin g th e O 2 an dC O C E ar e conducte dquarterly , excep t i n aquarter

whe n aRAT A i s conducte dinstead . Th e R A accurac y fo r

C O i s base do n th e unit s o f th e C O emissio n standard(ppmd v @ 7 % O2) . C O dat acollecte dfro mth e analyze r durin g th e RAT A wil l includ e lo w an do r hig h rang e value s pe r

th e norma l operatin g requirements . 6Tabl e 2- 1 (continued) Overview o

f CEM S Performanc e Requirement s Analyze r Paramete r (Spa n Value ) Q C Paramete r Minimu m Frequency Q C Limi t Correctiv e Actio n

C O (300 0 ppm) Z D an dC D Dail y ± 3 % o f span Zero/Spa n Adjustmen t C O (300 0 ppm) C D Dail y ±5 % o f span fo r 6 ou t o f 7 day Shu t

of f waste , service/calibrate , conduc t AC A C O (300 0 ppm) C D Dail y ±6 % o f span Shu t

of f waste , service/calibrate , conduc t AC A C O (300 0 ppm) Cumulativ e Spa n

Adjustmen t Pe r Adjustmen t ±9 % o f span Shu t

of f waste , service/calibrate , conduc t AC A C O (300 0 ppm) C E Quarterly 3 5 % Shu t of f waste , service/calibrate , conduc t RAT A

HC l (100 0 ppm) Z D an dC D Dail y ± 3 % o f span Zero/Spa n Adjustmen t HC l (100 0 ppm) C D Dail y ±5 % o f span fo r 6 out o f 7 da y Shu t

of f waste , service/calibrate , conduc t AC A HC l (100 0 ppm) C D Dail y ±6 % o f span Shu t

of f waste , service/calibrate , conduc t AC A HC l (100 0 ppm) Cumulativ e Spa n

Adjustmen t Pe r Adjustmen t ±9 % o f span Shu t

of f waste , service/calibrate , conduc t AC A HC l (100 0 ppm) C E Quarterly 4 5 % Shu t of f waste , service/calibrate , conduc t AC A Th e ACA s fo r

determinin g th e O 2 an dC O C E ar e conducte dquarterly , excep t i n aquarter

whe n aRAT A i s conducte dinstead . A RAT A fo r

HC l ma y b e performe dannuall y i n lie u o f performin g a n AC A i n tha t quarter .

7Th e drif t fo r eac h stac k

ga s constituen t

i s determine das th e differenc e betwee n th e know n constituen t

concentratio n i n the calibratio n ga s an dth e analyze r reading . Z D i s th e drif t determine dusin g zer o gas . C D i s th e drif t determine dusin g span gases . Z D an d C D ar e determine ddail y fo r

0 2 , CO , an dHCl . Z D fo r H 2 0 i s als o determine ddaily . Th e Z D an dC D ar

e recorde db y th e CEM S datalogge r a s apercen t

o f full-scal e deviatio n (Dev%) . Give n tha

t the "spa n value " i s equa l to the "full-scale " value , Dev % i s calculate das follows : Dev% = \Drift

%\
^,, „, reference concetration - analyzer responce , Drift % = — - • 100

span value Fo r C O an d0 2 , i f

Dev % fo r

C D exceed s th e limit s specifie di n th e applicabl e Performanc e Specification s i n 4 0 CF RPart 60 , Appendi x B , th e analyze r mus t b e calibrated . I f

th e Dev % fo r

C D i s greate

r than th e prese t

toleranc e (Tol% ) th e instrumen t technicia n wil l notify th e incinerato r operato r

an dwaste feed s wil l b e shut of f unti l correctiv e measure s hav e bee n taken . Th e C D tolerance s fo r bot h 0 2an dC O hav e bee n se t a t th e tw o time s th e performanc e specificatio n limits . A calibratio n failur e alar m indicate s tha

t th e analyze r

i s out-of-contro l an dmus t b e service dan drecalibrated . A n A C A mus t

b e conducte dt o documen t tha t th e analyze r

i s withi n th e performanc e specification s prio r

to resumin g hazardou s waste burning . Fo r CO , i f th e Dev % fo r

C D i s greater

than 5 % fo r

6 out o f 7 days , the n th e analyze r i s out-of-contro l an dmus t b e service dan drecalibrated . A n AC A mus t b e conducte dto documen t

tha t th e analyze r

i s withi n th e performanc e specification s prio r to resumin g hazardou s wast e burning . Simila r requirement s fo r

drif t limit s appl y to HCl , excep t tha t n o performanc e specification s hav e bee n promulgate dfo r CEM S monitorin g thes e parameters . I n lie u o f limit s specifie db y a n EP A Performanc e Specification , Veoli aha s develope dself

impose dperformanc e specificatio n limit s fo r HCl . Thes e limit s ar

e specifie di n Tabl e 2

- 1 . 2. 2 Calibratio n Calibratio n o f

th e analyze r

wil l b e conducte dperiodicall y to ensure tha t the result s o f drif t checks , ACAs , o r

RATA s meet

th e applicabl e performanc e specifications . 8Calibratio n fo r eac h I Rchanne l (H 2 0 , CO , an dHCl ) ma y b e performe ddail y durin g th e automate dcalibratio n sequenc e use dto determin e calibratio n drift . Fo r eac h calibratio n ga s use ddurin g th e automate dsequence , the automati c calibratio n wil l reset th e analyze r respons e to correspon dwit h th e know n referenc e concentrations . An y automate d calibratio n adjustmen t wil l b e mad e immediatel y afte r th e analyze r

respons e to th e calibratio n gas i s recorde delectronically . Th e drif t determine dimmediatel y prio r to a calibratio n adjustmen t

i s equa l to th e magnitud e o f th e adjustment . Th e oxyge n analyze r use s atwo-poin t

calibratio n curve . Th e firs t calibratio n poin t

reset s th e measure d concentratio n o f

ai r to 20.94% . Th e secon dcalibratio n poin t reset s th e measure d concentratio n o f

alo w concentratio n calibratio n ga s to it s know n concentration . Thi s calibratio n i s performe dmanually . T o document th e calibratio n adjustment , th e actua l measurement

a t eac h calibratio n poin t

prio r to adjustmen t

wil l b e recorded . Followin g servic e to th e MC 3 analyze r tha t coul daffec t

it s calibration , eac h I Rchannel , an dth e 0 2analyze r

wil l b e calibrated . Th e CEM S Drif t an dCalibratio n Dat aSheet i n th e Appendi x to thi s documen t wil l b e use dto trac k th e cumulativ e span adjustment s (i.e. , chang e i n th e calibratio n factor) . Sectio n 5. 5 o f th e MC 3 CEM S Operations Guide an dSectio n 4. 4 o f

th e MC 3 CEM S System Guide shoul db e referre dto as neede dfo r additiona l detai l regardin g calibratio n o f the CEMS . I f th e cumulativ e calibratio n adjustmen t fo r C D i s thre e time s th e performanc e specificatio n limit s a

t an y time , hazardou s wast e burnin g wil l b e cutoff . Th e analyze r wil l b e serviced , recalibrated , an dan AC A wil l documen t tha t hazardou s wast e burnin g ca n recommence . A calibratio n facto r tha t ha s bee n verifie dthroug h a n AC A wil l becom e the ne w referenc e poin t fo r assessin g the cumulativ e adjustment s mad e to correc t fo r calibratio n drift . Th e incinerato r

ca n remai n o n hazardou s wast e durin g CEM S drif t checks , calibrations , purges , an dcorrectiv e action s fo r CEM S failure s provide dtha t th e CEM S downtim e doe s no t excee d2 0 minutes . Durin g thes e times , th e instantaneou s value s use dto determin e one-minut e average s o f dry , oxyge n correcte dconcentration s o f C O ar e discarded . Thi s allowanc e i s provide db y Sectio n 6. 2 an d6.5. 1 o f th e Appendi x to Subpar t EEE . Th e applicabl e regulator y requirement s do no t limi t the frequenc y tha

t thi s allowanc e ca n b e utilized . Typically , thi s allowanc e wil l onl y b e utilize donc e pe r day fo r th e dail y drif

t checks . Sinc e th e oxyge n analyze r canno t b e calibrate ddurin g th e automati c calibratio n o f th e I Rchannels , calibratio n o f th e oxyge n analyze r

wil l requir e additiona l downtime .

9I f

athere i s aCEM S failure , th e incinerato r ma y remai n o n hazardou s waste provide dtha t th e CEM S ca n b e restore dwithi n 2 0 minutes . Followin g downtime , the CEM S mus t b e withi n th e performanc e specification s describe d i n thi s document . Otherwise , hazardou s waste burnin g wil l ceas e unti l th e appropriat e correctiv e measure s can b e taken . T o ensure tha t th e hourl y rollin g averag e (HRA ) fo r C O i s representativ e o f curren t operatin g conditions , CEM S dat avalidit y mus t b e a t leas t 75 % (i.e. , 6 0 vali don e minut e average s pe r 8 0 minute s o f

norma l operations) . 2. 3 Absolute Calibratio n Audi t A n AC A i s conducte dquarterl y fo r 02 , C O (hig h an dlo w range) , an dHCl . Fo r O 2 an d CO , a n AC A i s no t

conducte di n th e quarte r tha t th e require dannua l RAT A i s performed . Th e AC A i s conducte daccordin g to th e calibratio n erro r (CE ) tes t

procedur e describe di n th e Performanc e Specification s 4B . Durin g th e ACA , th e analyze r i s challenge dove r eac h rang e wit h EP A Protoco l 1 cylinde r gases . Th e EP A Protoco l 1 cylinde r gase s ar e NIS T traceabl e calibratio n standards . Fo r agive n parameter , th e analyze r respons e i s recorde da

t thre e measurement

points . Thi s i s the n repeate dtwic e to giv e thre e sets o f data . Th e C E a

t eac h measurement

poin t i s determine da s follows : CE = d FS •100% wher e di s th e mea n differenc e betwee n th e CEM S respons e an dth e know n referenc e concentratio n an dF S i s th e span value . Fo r C O an dHCl , th e C E determine da t eac h measuremen t

poin t canno t excee d5% . Fo r 0 2 , C E canno t

excee d2% . I f

an AC A fail s to pas s th e Q C criterio n (i.e. , th e audi t indicate s excessiv e inaccuracy) , the n hazardou s waste burnin g canno t resum e unti l correctiv e measure s hav e bee n taken an daRAT A demonstrate s tha t th e CEM S i s operatin g withi n th e performanc e specifications . 2. 4 Interference Response Tes t Th e MC 3 analyze r

correct s fo r

interference s usin g additiv e an dmultiplicativ e interferenc e tables . Thes e table s wer e generate dpe r th e manufacturer' s procedur e a t th e initia l setup o f

th e CEM S system . A n Interferenc e Respons e Tes t (IRT ) i s liste di n th e Appendi x t o Subpar

t EEE , however , th e Performanc e Specificatio n 4 B doe s no t includ e requirement s o r

acceptanc e criteri afo r a n interferenc e respons e test . Veoli awil l perfor m 1 0Interferenc e Respons e Test s a t suc h tim e a

s U S EP A specifie s th e tes t procedure s an d acceptabl e criteri afo r

an Interferenc e Respons e Test . 2. 5 Relative Accurac y Tes tAudi t Th e Relativ e Accurac y Tes t Audi t (RATA ) i s require dannuall y fo r 0 2an dC O CEMS . Th e Relativ e Accurac y (RA ) tes t procedure s require db y Sectio n 7. 2 o f P S 4 B reference s incorrec t section s o f

P S 3 (fo r

0 2 ) an dP S 4 A (fo r

CO) . Th e applicabl e section s o f th e performanc e specification s are :

• RAT A procedures : Section s 8.4. 3 throug h 8.4. 5 o f P S 2 . • 0 2referenc e methods : Sectio n 8. 2 o f P S 3

• C O referenc e methods : Sectio n 8. 2 o f P S 4A . • 0 2R A calculations : Sectio n 12. 0 o f P S 3

• C O R A calculations : Sectio n 12. 0 o f P S 2

• 0 2R A criterion : Sectio n 13. 2 o f P S 3

• C O R A criteria : Sectio n 13. 2 o f P S 4 A A brie f summary o f

th e applicabl e referenc e method s ar e provide dbelow : U S EP A Metho d3/3 A (Stac k Ga s Compositio n an dMolecula r Weight ) Th e samplin g an danalytica l procedure s outline di n thi s metho dwil l b e use dto determin e th e 0 2compositio n o f th e stac k

ga s durin g th e RATA . Usin g thi s method , aga s sampl e i s extracte dfro mth e stac k a t aconstan t

rate fo r determinatio n o f

O2 , C0 2an dmolecula r weight . Th e integrate dgasba g collectio n optio n wil l b e employed . Th e gasbag s wil l b e analyze dusin g a n Orsat analyzer . A s an alternative , th e Metho d3 A (instrumenta l analyzer ) metho dma y b e use dfo r analysi s o f

th e sample . U S EP A Metho d4 (Stac k Ga s Moistur e Content ) I f necessary , th e samplin g an danalytica l procedure s outline di n thi s metho dwil l b e use d to determin e th e moistur e content o f th e stac k

ga s durin g th e RATA . Usin g thi s method , aga s sampl e i s extracte dfro mth e stack . Th e ga s passe s throug h aserie s o f impinger s tha t contai n reagents . Th e impinger s ar e connecte di n serie s an dar e containe di n an ic e bath i n orde r

to assur e condensatio n o f

th e moistur e i n th e ga s stream . An y moistur e tha t i s no t condense di n th e impinger s i s capture di n th e silic agel , ensurin g tha t al l moistur e ca n b e weighe dan dentere dint o moistur e calculations . U S EP A Metho d1 0 (Carbo n Monoxid e CEMS ) 1 1A continuou s emission s monito r wil l b e use dto continuousl y sampl e exhaus t ga s fo r carbo n monoxid e analysi s as describe di n EP A Metho d10 . Usin g thi s method , a continuou s gas sampl e i s extracte dfro mth e exhaus t gas , an di s analyze dfo r carbo n monoxid e (CO ) usin g aLuft-typ e Non-Dispersiv e Infrare dAnalyze r (NDIR) , o r

another equivalen t

analyzer . Thi s samplin g an danalysi s wil l occur continuousl y throughou t th e duratio n o f

eac h ru n o f

th e RATA . Durin g ates t

ru n o f th e RATA , U S EP A referenc e method s ar e utilize dto obtai n stac k ga s data . Thes e dat aare use dto calculat e th e stac k ga s dr y 0 2concentratio n an dth e stac k ga s C O concentratio n correcte dto seve n percen t oxyge n i n unit s o f

part s pe r million , dr y volum e (i.e. , i n th e unit s o f th e emissio n standard , 10 0 ppmd v C O @ 7 % O2) . Th e averag e stac k ga s O 2 (% , dry ) an dC O (ppmdv , @ 7 % O2 ) concentrations—a s calculate dfro mth e installe dCEM S ove r th e duratio n o f

th e run—are compare dto th e valu e obtaine dusin g th e referenc e methods . Th e RAT A consist s o f aminimu mo f

9 tes t runs . I f mor e tes t

run s ar e conducted , a

t leas t 9 dat aset s wil l b e use dto determin e RA , an dn o mor e than thre e set s o f dat awil l b e rejected . Th e O 2 an dC O R A calculation s an d acceptanc e criteri aar

e presente dbelow . RA. oxygen

^00= <1.0%O 2 ,dry

+ \CC\ RM • 100% < 10%...for RM > 50ppmdv @ 7% 0 2 d + \CC\<5ppmdv @ 7% 0 2 ...for RM < 50ppmdv @ 7% 0 2 where , 

### d = -•Y J 

### {RM

i 

### -CEMS i 

### ) n j n = numbe r

o f tes t run s RMj= the concentratio n determine db y th e referenc e metho dfo r th e i t htes t

ru n CEMSj= th e concentratio n determine db y th e CEM S fo r th e i t htes t

ru n CC = th e 2. 5 percen t erro r confidenc e coefficien t (se e Sectio n 12. 4 o f

P S 2 )

I f aRAT A fail s to pas s th e Q C criterio n (i.e. , th e audi t indicate s excessiv e inaccuracy) , the n hazardou s waste burnin g canno t resum e unti l correctiv e measure s hav e bee n take n an daRAT A demonstrate s tha t th e CEM S i s operatin g withi n the performanc e 1 2specifications . I f C O emissio n level s ar

e significantl y low , i t

ma y b e difficul t

to produc e meaningfu l result s usin g th e R A tes t procedure . Unde r

thes e circumstances , Veoli awil l reques t approva l t o utiliz e th e Alternativ e R A Procedur e prescribe db y Sectio n 7. 3 o f P S 4B .

1 33.

0 CEM S MAINTENANC E Veoli aha s develope dapreventativ e maintenanc e progra mfo r th e CEMS . Thi s progra m include s frequen t

inspection s o f

th e CEM S i n orde r

to identif

y potentia l componen t failures , leaks , an ddat aqualit y issues . Th e CEM S preventativ e maintenanc e progra m als o include s schedule dreplacemen t o f critica l component s an dmaintenanc e o f spar e part s inventory . Al l schedule dan dunschedule dmaintenanc e o f the CEM S wil l b e documente di n aCEM S logboo k maintaine dfo r

eac h incinerator . Sectio n 8. 0 o f th e MC 3 CEM S Operations Guide provide s detail s fo r daily , weekly , monthly , quarterly , an d annua l inspectio n an dmaintenanc e activities . Procedure s an drecordkeepin g fo r th e specifi c inspectio n an dmaintenanc e activitie s ar e describe dbelow . 3. 1 Dail y Syste

m Audi t Th e Dail y Syste mAudi t includes :

• Revie w o f

the dail y drif

t chec k dat a
• Inspectio n o f

th e recordin g syste m
• Chec k

fo r controlle r

alarm s an derror/warnin g message s
• Chec k

expecte dcalibratio n value s
• Chec k

o f curren t dat astatu s
• Chec k

o f calibratio n ga s cylinde r pressure s
• Chec k

calibratio n ga s pressur e regulato r setting s
• Inspectio n o f

th e instrumen t

ai r pressure
• Inspectio n o f

th e stac k

ga s samplin g syste m Th e Dail y Syste mAudi t Checklis t

wil l b e use dto documen t th e finding s fro mth e dail y syste maudit . A CEM S Drif t an dCalibratio n Dat aSheet wil l b e complete ddurin g the dail y syste maudi t

i n order

to trac k

an devaluat e drif

t an dadjustment s mad e to th e CEMS . 3. 2 Spare Part

s Inventor

y CEM S spar

e part s ar

e maintaine di n sufficien t quantitie s on-sit e to perfor mroutin e maintenanc e activities . I t i s anticipate dtha

t thes e spar

e part s an dtypica l maintenanc e supplie s wil l b e adequat e to servic e the CEMS . Som e service s an dreplacemen t o f component s mus t

b e performe db y an EcoChe mAnalytic s Servic e Enginee r to avoi d violatio n o f

th e syste mcertification .

1 4Th e followin g consumabl e part s hav e bee n targete dfo r periodi c inspectio n an d replacemen t

fo r maintainin g th e CEMS :

• Ai r conditione r

filter s fo r

CEM S shelter
• Instrumen t

ai r coalescin g filter s
• Sampl e pum p Teflo n diaphrag m
• Sampl e pum p Teflo n flappe r valv e
• Sampl e prob e interna l filte r
• Sampl e prob e gasket s
• Probe-ti p filte r Th e followin g spare part s ar e no t part o f routin e maintenanc e an dwoul db e replac e b y a n EcoChe mServic e Engineer :

• Cel l fron t

cove r gaske t

• Cel l inle t

filte r
• Cel l window s wit h o-rin g gasket s
• Cel l mirror s Th e CEM S Calibratio n Ga s an dSpare Part s Lo g i s provide di n Appendi x A an dwil l b e use da s neede dt o kee p trac k

o f inventory . 3. 3 Calibratio n Gas Suppl y an d Certificatio n A summary o f

th e calibratio n gase s neede dto perfor mth e dail y drif t checks , calibrations , an dACA s i s presente di n Tabl e 3-1 . Th e numbe r o f ga s cylinder s maintaine don-sit e depend s o n the specifi c mixtur e o f gase s i n eac h cylinde r an dth e lea dtim e require dfo r placin g orders . A n inventor y o f calibratio n gase s wil l b e conducte di n conjunctio n wit h th e spar e part s inventor y to ensure tha t th e appropriat e gase s ar e availabl e fo r

use . Certificatio n fro mth e supplie r o f calibratio n gas qualit y wil l b e kep t wit h th e mos t

recen t spar e part s inventor y documentation . Eac h calibratio n sequenc e deplete s approximatel y 4 0 psi , an dacylinde r wit h les s tha n 15 0 ps i shoul db e replaced . Th e dail y syste maudi t include s inspectio n o f th e calibratio n ga s cylinde r

pressure s an dwil l b e use dtrac k usag e an dto predic t

whe n to reorder .

1 5Tabl e 3- 1 Summar

y of Concentratio n Requirement s fo rCalibratio n Gase s Constituent Q C

Paramete r Concentratio n

Requirement Accurac y H 2 0 Z D 0 % pe r ga s supplie r 

# o 2 Z D 0 % pe r gas supplie r 

# o 2 C D 25 % pe r gas supplie r 

# o 2 A C A 0-2 % E P A Protoco l 1/NIS T Traceabl e 

# o 2 A C A 8-10 % E P A Protoco l 1/NIS T Traceabl e 

# o 2

A C A 14-16 % E P A Protoco l 1/NIS T Traceabl e C O (lo w range ) Z D 0 pp m pe r gas supplie r C O (lo w range ) C D 20 0 pp m pe r gas supplie r C O (lo w range ) A C A 0-4 0 pp m E P A Protoco l 1/NIS T Traceabl e C O (lo w range ) A C A 60-8 0 pp m E P A Protoco l 1/NIS T Traceabl e C O (lo w range )

A C A 140-16 0 pp m E P A Protoco l 1/NIS T Traceabl e C O (hig h range ) Z D 0 pp m pe r gas supplie r C O (hig h range ) C D 300 0 pp m pe r ga s supplie r C O (hig h range ) A C A 0-60 0 pp m E P A Protoco l 1/NIS T Traceabl e C O (hig h range ) A C A 900-120 0 pp m E P A Protoco l 1/NIS T Traceabl e C O (hig h range )

A C A 2100-240 0 pp m E P A Protoco l 1/NIS T Traceabl e H C l Z D 0 pp m pe r gas supplie r l C D 100 0 pp m pe r gas supplie r H C l A C A 0-20 0 pp m E P A Protoco l 1/NIS T Traceabl e H C l A C A 300-40 0 pp m E P A Protoco l 1/NIS T Traceabl e H C l

A C A 700-80 0 pp m E P A Protoco l 1/NIS T Traceabl e

1 63.

4 Correctiv e Actio n fo r Malfunctionin g CEM S I t i s Veolia' s polic y to minimiz e th e occurrenc e o f malfunction s b y takin g aproactiv e approac h to facilit y maintenance . Proactiv e measure s includ e th e preventiv e maintenanc e describe di n thi s section , an dth e calibratio n an dperformanc e testin g describe di n Sectio n 2.0 . Frequen t inspection s an davailabilit y o f spar e part s allo w fo r th e timel y completio n o f as neede dservic e to th e CEM S prio r to amajo r

malfunction . Operatin g an dmaintainin g th e incinerato r durin g amalfunctio n wil l b e conformanc e wit h th e Startup, Shutdown, and Malfunction Plan (SSMP) . Attachmen t 4 to th e SSM P i s th e Program of

Corrective Action for Malfunctions. Sectio n 9. 2 o f th e Program of Corrective Action for

Malfunctions addresse s correctiv e action s fo r malfunctionin g CEMS . Sectio n 9. 0 throug h 9. 2 o f th e MC 3 CEM S Operations Guide ma y b e referre dto a s neede dfo r

troubleshootin g an dcorrectiv e maintenanc e o f th e CEMS .

1 74.0 . INTEGRATIO N O F TH E CEM S WIT H TH E AWFC O SYSTE M

Th e CEM S i s integrate dwit h th e automati c wast e fee dcutof f (AWFCO ) syste mt o assur e on-goin g complianc e wit h C O emissio n standards . Th e AWFC O syste mi s designe dt o immediatel y an dautomaticall y shut o f al l wast e to the incinerato r i n th e event

o f a n exceedanc e o f

an emissio n o r

operatin g limit . Th e CEM S i s integrate dwit h AWFC O syste mthroug h interlocks . Thes e interlock s ar e condition s whic h trigge r arela y causin g th e AWFC O syste mt o activate . Thi s sectio n describe s th e AWFC O interlock s associate d wit h th e CEMS . 4. 1 Emissio n Standard s Th e CEM S ra w dat afo r O z( % vol) , H 2 0 ( % vol) , an dC O (ppmv ) consist s o f instantaneou s value s whic h hav e no t bee n smoothe do r

averaged , evaluate donc e ever y 1 5 seconds . Thes e value s ar e use dt o calculat e C O emission s i n th e unit s o f emissio n standards . Calculation s equivalen t t o th e followin g procedure s ar e performe dt o compar e th e stac k ga s emission s to th e C O emissio n standard . Firs t 15-secon ddat ai n th e unit s o f th e emissio n standard s ar e calculated : ( \ CO@7% O 2 ,ppmdv = CO, ppmv IOO%-(H 2 O,%) 14%

21%- 

# o 7



# ,% 100%-{H 2 O,%) Th e calculate d15-secon ddat aar e the n use dt o calculat e one-minut e average s (OMAs) . Th e curren t

minut e OM A i s average dwit h th e previou s 5 9 OMA s t o generat e an hourl y rollin g averag e (HRA) . Al l roundin g i s avoide dfo r th e number s use dto calculat e HRAs . Th e HR A o f

C O emission s ar

e rounde dt o tw o significan t figures . I f the HR A C O emissio n concentratio n exceed s th e C O emissio n standardo f 10 0 ppmd v @ 7 % 0 2 , a n AWFC O wil l occur . 4. 2 Drif

tLimits A s describe di n Sectio n 2.1 , wast e feed s wil l b e manuall y shut of f i n cas e adrif

t limi t i s exceeded . Fo r

C O an d0 2 , drif

t limit s ar

e equa l to 2 time s th e performanc e specifications . Comparabl e drif t limit s hav e bee n establishe dfo r excessiv e H 2 0 drift .

1 85.0. RECORDKEEPIN G AN D QUALIT Y ASSURANC E REVIEW S

Documentatio n generate dfro mCEM S QA/Q C procedure s an dmonitorin g wil l b e kep t on-sit e fo r

aperio do f

fiv e years . Th e dat aan ddocumentatio n tha t i s generate dan d reviewe di s kep t

i n variou s location s a t th e Veoli afacility . Tabl e 6- 1 belo w list s th e storag e locatio n an dforma t o f thi s documentation . Maintenanc e an dInstrumen t Technician s hav e th e primar y responsibilit y fo r creatin g an d organizin g CEM S dat asheets , dail y syste maudi t checklists , maintenanc e logbook , an d spar e part inventor y records . Th e Environmenta l Engineer/Specialis t o r designe e wil l chec k thes e record s quarterl y to verif y completio n an dorganization . Thi s revie w wil l als o conside r

th e followin g requirements : 1 . Wheneve r

excessiv e audi t

inaccuracie s occu r

fo r tw o consecutiv e quarters , th e current writte n procedure s wil l b e revise do r th e CEM S modifie do r replace dto correc t th e deficienc y causin g th e excessiv e inaccuracies . Previou s version s o f writte n procedure s wil l b e kep t o n recor dan dmad e availabl e fo r inspection . 2 . I f the Z D and/o r

C D exceed(s ) tw o time s th e limit s i n th e Performanc e Specifications , o r

i f th e cumulativ e adjustmen t to th e Z D and/o r

C D exceed(s ) thre e time s th e limit s i n the Performanc e Specifications , th e CEM S i s considere d "out-of-control " (a s define di n 4 0 CF R63.8(c)(7)) , an dthe event wil l b e reporte d i n the facility' s semi-annua l "Exces s Emission s an dCM S Performanc e Report" . Furthe r detai l o n thi s repor

t ca n b e foun di n th e facilit y CM S Qualit y Assuranc e Program . O n an annua l basi s th e Environmenta l Engineer/Specialis t o r designe e wil l revie w al l CEM S dat agenerate dfo r the previou s 1 2 month s an dprepare abrie f interna l report/mem o summarizin g findings . Base do n thi s review , the Environmenta l Engineer/Specialis t

o r designe e wil l solici t

recommendation s fo r

revision s to th e CEM S Qualit y Assuranc e Plan . Th e CEM S Qualit y Assuranc e Pla n wil l b e revise das neede dt o maintai n QA/Q C o f

th e CEMS . Al l version s o f thi s pla n fo r

th e las t fiv e year s remai n i n th e operatin g record .

1 9Tabl e 5- 1 CEM S Records an d Report s Record/Report Storag e Locatio n Media/Format 1 CEM S Q A Pla n

- Curren t

Versio n

- Previou s Versio n Incinerato r Manager' s Offic e Operatin g Record s Archive s H D and/o r P R D CEM S Reading s an dHR A

- Previou s yea

r throug h yea

r to dat e

- Remainin g archive s Dat aHistoria n Operatin g Record s Archive s H D and/o r R D R D Drif t an dCalibratio n Data :

- Previou s yea

r throug h yea

r t o dat e

- Remainin g archive s Operatin g Record s Archive s P and/o r R D Absolut e Calibratio n Audi t

- Previou s yea

r thoug h yea

r to dat e

- Remainin g archive s Operatin g Recor dArchive s P and/o r R D Relativ e Accurac y Tes t Audi t

- Previou s yea

r throug h yea

r t o dat e

- Remainin g archive s Operatin g Recor dArchive s P and/o r R D Dail y Syste mAudi t

- Previou s yea

r throug h yea

r t o dat e

- Remainin g archive s Operatin g Recor dArchive s P and/o r R D Preventiv e Maintenanc e Logboo k

- Previou s yea

r throug h yea

r to dat e

- Remainin g archive s Operatin g Record s Archive s P and/o r R D Spar e Part s Inventor y

- Previou s yea

r throug h yea

r to dat e

- Remainin g archive s Operatin g Record s Archive s P and/o r R D

Annua l Revie w o f

CEM S Dat a Operatin g Records Archive s P and/o r H D and/o r R D

1 Medi aFormat : H D - Compute r o r network har ddriv e R D - Removabl e driv e (floppy , CD , backu p tape ) P - Pape r documentatio n 2 06.

0 OPERATO RTRAININ G AN D CERTIFICATIO N Trainin g i s provide dto Veoli aemployee s o n th e basi s o f thei r jo b title . Individual s specificall y involve di n th e operatio n o f th e incinerato r

an dassociate dCEM S ar e th e Instrumen t

Technicians , Incinerato r Operators , an dEnvironmenta l Engineer/Specialist . Th e Veoli aoperato r

trainin g an dcertificatio n progra mmeet s th e requirement s outline di n 4 0 CF R63.1206(c)(6) . Documentatio n o f employe e trainin g an dcertificatio n i s kep t wit h th e Trainin g Director , an di s availabl e fo r revie w upo n request .

2 1APPENDI X A CEM S DAT A SHEET S AN D CHECKLIST S

NOTE : TH E FOLLOWIN G SHEET S AR E FO REXAMPL E PURPOSE S ONLY . VEOLI A MA Y UTILIZ E EQUIVALEN T DOCUMENTATIO N FO RAN Y O FTH E SHEET S INCLUDED .CEM S DRIF T AN D CALIBRATIO N DAT A SHEE T Paramete

r (Spa n Value ) Dat

e & Tim e Concentratio n Drif t% Adjustmen t% Cumulativ

e Adjustmen

t% Paramete

r (Spa n Value ) Dat

e & Tim e Referenc

e Analyze

r Drif

t% Adjustmen t% Cumulativ

e Adjustmen

t% H z O (6 0 % ) Zero O z(25% ) Zero Calibratio n C O (20 0 ppm ) Zero Calibratio n C O (300 0 ppm ) Zero Calibratio n HC l (100 0 ppm ) Zer o Calibratio n
Drif t % = RfifeW0C * - AmlyZer . 100 %

Spa n Valu e (Nam e & Title ) Adjustmen

t % = Drif t % (i f zero/spa n wa s rese t during drif

t check ) Cumulativ e Adjustmen

t % = (Previou s Cumulativ e Adjustmen t % ) + (Curren

t Adjustmen

t % ) (Signature)ABSOLUT E CALIBRATIO N AUDI T (ACA ) DAT A SHEE T

Paramete r



## •o 2 E H CO-lo w range f~ l CO-hig h range • HC l NIS T Traceabl e Calibratio n Standard s Paramete r



## •o 2 E H CO-lo w range f~ l CO-hig h range • HC l Gas Concentratio n Paramete r



## •o 2 E H CO-lo w range f~ l CO-hig h range • HC l Lo w (Zero ) 

### ± Paramete r



## •o 2 E H CO-lo w range f~ l CO-hig h range • HC l M i d 

### ± Paramete r



## •o 2 E H CO-lo w range f~ l CO-hig h range • HC l Hig h 

### ± RU N NUMBE R Concentratio n Differenc e RU N NUMBE R Referenc e Analyze r Lo w Mi d Hig h 1 - Lo w — — 2-Mi d ~ 3 - Hig h — 

## - 4-Lo w — — 5-Mi d ~ — 6 - Hig h ~ ~ 7-Lo w — — 8-Mi d — — 9 - Hig h — MEA N DIFFERENC E = CALIBRATIO N ERRO R= MEA N DIFFERENC E = CALIBRATIO N ERRO R= % % % Calibratio n Erro r

= ^ e a nDifferenc e * ^Q Q Span Valu e

(Name ) (Title ) (Signature) (Date )RELATIV E ACCURAC Y TES T AUDI T RAT A DAT A SHEE T Referenc e Metho d CEM S Differenc e Referenc e Metho d CEM S Differenc e Run H 2 0 , % (i f applicable ) 0 2 , % we

t (i f applicable ) 0 2 , % dr

y 0 2 , % dr

y 0 2 , % dr

y C O ppm

v (i f applicable ) C O ppmd v C O ppmd

v @ 7 % 0 2 C O ppmd v @ 7 % 0 2 C O ppmd

v @ 7 % 0 2 1 2 3 4 5 6 7 8 9 1 0 1 1 1 2 0 2 R A Mean Differenc e Standar dDeviatio n Confidenc e Coefficien t COR A (Name) (Title ) (Signature) (Date)CEM S DAIL Y SYSTE M AUDI T Initial s

Verify tha

t th e mos t recen t drif t checks an

dcalibratio n adjustments ar e withi n limits . Complet e Drif t an dCalibratio n Dat aSheet . Correctiv e Actions : Verif y prope r operatio n o f

CEM S dat

arecordin g an

dprintin g Correctiv e Actions : Chec k fo r controller alarm s anderror/warning message s Correctiv e Actions : Chec k expectedcalibratio n value s Correctiv e Actions : Chec k curren t emission s dat

astatu s Correctiv e Actions : Verif y calibratio n ga

s cylinde r pressure s (>15 0 psi ) Correctiv e Actions : Verify pressur

e regulator

setting s (approximately 25-3 5 psi ) Correctiv e Actions : Verif y prope r instrumen

t air pressur e t o CEM S umbilica l Correctiv e Actions : Performvisua l inspectio n o f th e stac k ga s sampling syste

m Correctiv e Actions :

(Name) (Signature) (Title ) (Date)CEM S CALIBRATIO N GA S AN D SPAR E PART S LO G

CALIBRATIO N GASES : (Attac h al l certificatio n forms ) Zer o gas : Spa n ga s 1 Span ga s 2 Spa n ga s 3 A C A Gases : cylinder s cylinder s cylinder s cylinder s Composition :

Composition : Composition : Composition :

PARTS : Ai r conditione r

filter s fo r

CEM S shelte r Instrument

ai r coalescin g filter s Sampl e pum p Teflo n diaphrag m Sampl e pum p Teflo n flappe r valv e Sampl e probe interna l filte r Sampl e prob e gasket s Probe-ti p filte r Cel l fron t

cove r gaske t Cel l inle t filte r Cel l window s wit h o-rin g gaskets _ Cel l mirror s Tubin g Fitting s ____ _ Solenoi dValue s Thermocouple s Electroni c part s

Othe r spare part s

Inventory take n by : Date :

### CONTINUOU S MONITORIN G SYSTE M QUALIT Y CONTRO L PROGRA M

Prepare dfor : Veoli aE S Technica l Solutions , LL C

Sauget , Illinoi s

Prepare dby : Frankli n Engineerin g Group , Inc . Franklin , Tennesse e

Octobe r 200

8TABL E O F CONTENT S

1. 0 INTRODUCTIO N AN D BACKGROUN D 1 1. 1 SUMMAR Y O F FACILIT Y INFORMATIO N 4 1.1.1 Fixed

Hearth Incinerators 4 1.1.2 Rotary Kiln Incinerator 5 1. 2 CM S INSTRUMENTATIO N 6 2. 0 CM S CALIBRATIO N AN D PREVENTIV E MAINTENANC E 1 3 2. 1 CM S CALIBRATIO N 1 3 2.1.1 Initial

CMS Calibration 13 2.1.2 Subsequent

CMS Calibration 13 2.1.3 CEMS

Calibration Audits and Calibration 14 2. 2 CM S CALIBRATIO N AUDIT S 1 4 2. 3 PREVENTIV E MAINTENANC E 1 9 3. 0 CM S RECORDKEEPIN G AN D REPORTIN G 2 0 3. 1 RECORDKEEPIN G 2 0 3. 2 REPORTIN G 2 1 4. 0 CM S CORRECTIV E ACTION S 2 4

i iINDE X O F TABLE S

TABL E 1- 1 REGULATOR Y CHECKLIS T FO RTH E CM S Q A PROGRA M 2 TABL E 1 - 2 CM S INSTRUMEN T SPECIFICATION S 7 TABL E 2- 1 CM S CALIBRATIO N AUDI T REQUIREMENT S 1 5 TABL E 3 - 1 REPORTIN G REQUIREMENT S 2 3

ii i1.

0 INTRODUCTIO N AN D BACKGROUN D Veoli aE S Teclinica l Solutions , LL C (Veolia ) own s an doperate s tw o fixe dheart h incinerator s (Unit s 2 an d3 ) an darotary kil n incinerato r (Uni t 4 ) a t it s facilit y locate di n Sauget , Illinois . Th e incinerator s ar e subjec t to th e Nationa l Emission s Standard s fo r Hazardou s Ai r

Pollutant s (NESHAP ) fo r Hazardou s Wast e Combustor s (HWC) , Part 63 , Subpar t EE E ( § 63.120 0 to § 63.1221) . Th e NESHA P specifie s emission s standard s whic h reflec t

emission s performanc e o f Maximu mAchievabl e Contro l Technologie s (MACT) , an di s commonl y referre dto a s the HW C MACT . Hazardou s waste combustor s ar e require d[pe

r § 63.8(d)(2) ] to establis h an dimplemen t a Continuou s Monitorin g Syste m(CMS ) Qualit y Contro l (QC ) Program . Th e purpos e o f th e Q C Progra mi s to outlin e procedure s use dto verify tha t th e CM S ar

e properl y installed , calibrated , an dcollectin g accurate dat ao n a n ongoin g basis . Th e CM S performanc e evaluatio n tes t pla n wa s submitte das par t o f th e Comprehensiv e Performanc e Tes t

Plan . Th e Q C Progra mdemonstrate s Veolia' s complianc e wit h th e requirement s se t fort h i n § 63.8(d)(2) , as wel l a s th e additiona l qualit y assuranc e (QA ) requirements . Th e Q C Progra mi s require dto contai n description s o f initia l an dsubsequent CM S calibration , calibratio n drift , preventiv e maintenance , dat arecording , calculation s an dreporting ; an d acorrectiv e actio n pla n fo r malfunctionin g CMS . Tabl e 1- 1 present s the regulatory reference s relate dt

o th e Q C program , followe db y the sectio n o f thi s pla n tha

t addresse s eac h specifi c requirement . Som e reference s ar e mad e to othe

r HW C MAC T require dfacilit y operatin g plans . Thi s Q C Progra mi s intende dto fulfil l th e requirement s o f § 63.8(d)(2) , an dinclude s informatio n relate dto th e procedure s fo r eac h o f th e followin g operations :

• Initia l an dsubsequen t calibratio n o f

the CM S

• Detenriinatio n an dadjustment o f the calibratio n drif

t o f the CM S

• Preventiv e maintenanc e o f the CMS , includin g spar e part s inventory • Dat arecording , calculations , andreportin g
• Programo f

correctiv e actio n fo r

malfunctionin g CMS .

1Tabl e 1- 1 Regulator

y Checklis tfo rth

e CM S Q A Progra m Regulatory Citatio n Descriptio n Plan Section § 63.8(c)(l)(i ) Operatio n an dmaintenanc e o f eac h CM S Sectio n 1 .2 , 2. 3 O & M Pla n CEM S Pla n § 63.8(c)(l)(iii ) Startup , shutdown , an dmalfunctio n pla n fo r CM S SSM P Pla n § 63.8(c)(3 ) Verificatio n o f operationa l statu s CM S PE T Pla n § 63.8(c)(7)(ii ) Out-of-contro l CM S dat awil l no t b e use di n average s an dcalculations . Sectio n 4. 0 § 63.8(c)(7)(h ) Correctiv e action s fo r an out-of-contro l CM S Sectio n 4. 0 an d SSM P Pla n § 63.8(c)(8 ) Out-of-contro l CM S informatio n to b e submitte d Sectio n 4. 0 § 63.8(d)(2 ) Develo p an dimplemen t Q C portio n o f

CM S Q A progra m Sectio n 1. 0 § 63.8(d)(2 ) Q A progra minclude s th e developmen t an dsubmitta l o f the performanc e evaluatio n tes t pla n Sectio n 2.1. 1 § 63.8(d)(2)(f

) Develo p writte n procedure s fo r initia l an dsubsequent calibration s Section s 2 .1.1 , 2 .1 . 2 § 63.8(d)(2)(h ) Develo p writte n procedure s fo r determinatio n an d adjustmen t

o f calibratio n drift s Sectio n 2. 2 § 63.8(d)(2 )(iii ) Develo p writte n procedure s fo r preventiv e maintenanc e an dspar e part s inventor y Sectio n 2. 3 § 63.8(d)(2)(iv ) Dat arecording , calculations , an dreportin g Section s 3 .1 , 3. 2 § 63.8(d)(2 )(vi ) Correctiv e action s fo r malfunctionin g CM S Sectio n 4. 0 § 63.8(e)(3 ) Performanc e evaluatio n o f CM S CM S PE T Pla n § 63.8(g ) Reductio n o f monitorin g dat a Sectio n 3. 2 § 63 .10 (b )(1 ) Maintainin g file s Sectio n 3 . 1 §63 .10 (b)(2)(ix ) Maintai n record s o f measurement s fro mperformanc e evaluation s Sectio n 3 . 1 § 63 .10 (b)(2)(vi ) Maintai n record s o f eac h perio ddurin g whic h aCM S i s malfunctioning , o r

inoperativ e an dou t

o f contro l Sectio n 4. 0 an d SSM P Pla n §63.10(b)(2 )(vii ) Maintai n record s o f measurement s to demonstrate complianc e Sectio n 3 . 1 § 63 .10 (b)(2)(viii ) Maintai n record s o f result s o f

CM S performanc e evaluation s an dopacit y an dvisibl e emissio n observation s Sectio n 3 . 1 §63.10(b)(2)(x ) Maintai n record s o f CM S calibratio n check s Sectio n 2 .1 . 2

2Tabl e 1- 1 (continued) Regulator

y Checklis tfo r th

e CM S Q A Progra m Regulator

y Citatio n Descriptio n Pla n Section §63.10(b)(2)(xi ) Maintai n record s o f al l adjustment s an dmaintenanc e performe do n th e CM S Sectio n 3. 1 § 63.10(c)(1 ) Recordkeepin g requirement s fo r CM S measurement s (includin g unavoidabl e breakdown s an dout-of-contro l situations ) Sectio n 3. 1 §63.10(c)(13 ) Maintai n record s o f tota l proces s operatin g tim e durin g th e reportin g perio d Sectio n 3. 1 §63.10(c)(14 ) Develo p an dimplemen t CM S Q A progra mprocedure s Sectio n 1. 0 § 63.10(c)(5 ) Maintai n record s o f dat e an dtim e fo r

CM S Sectio n 3. 1 § 63.10(c)(5 ) inoperabilit y (excep t fo r zer o an dhigh-leve l checks ) Sectio n 3. 1 § 63.10(c)(6 ) Maintai n record s o f dat e an dtim e fo r

CM S out-of

contro l period s Sectio n 3. 1 Maintai n record s o f

identificatio n o f

eac h tim e perio d § 63.10(c)(8 ) o f

exceedance s - doe s no t includ e period s o f

Startup , Shutdown , Malfunctio n (SSM ) Sectio n 3. 1 §63.10(e)(3)(i ) Submitta l o f semiannua l exces s emission s an dCM S Sectio n 3. 1 §63.10(e)(3)(i ) performanc e report Sectio n 3. 1 §63.10(e)(3)(v ) Conten t an dsubmitta l dat ao f

exces s emission s an d CM S performanc e repor t Sectio n 3. 2 §63.10(e)(3)(vi ) Conten t o f summar y report

require db y (e)(3)(vii ) an d (e)(3)(viii ) to thi s sectio n Sectio n 3. 2 §63.10(e)(3)(vii ) Conditio n fo r submittin g onl y th e summary repor t Sectio n 3. 2 §63.10(e)(3)(viii ) Conditio n fo r submittin g bot h th e summary repor t an d exces s emission s an dCM S performanc e repor t Sectio n 3. 2 § 63.1209(b)(2)(i ) Calibratio n o f thermocouple s an dpyrometer s Sectio n 2. 1 § 63.1209(b)(3 ) Frequenc y o f CM S sampling , evaluation , computing , an drecordin g o f

regulate dparameter Sectio n 3. 1 § 63.1209(b)(5 ) Calculatio n o f rollin g average s Sectio n 3. 1 § 63.1209(f)(1 ) § 63.1211(c ) require s tha t CM S ar e installed , calibrated , an doperationa l b y th e complianc e dat e CM S PE T Pla n
Notes : PE T Performanc e Evaluatio n Tes t SSM P Startup , Shutdown , Malfunctio n Plan SD P Standar

dDivisio n Practice s

3Th e dat acollecte dfro mCM S instrumentatio n i s use dto demonstrate th e unit' s

complianc e wit h th e performanc e requirement s promulgate di n th e Interi mHW C Maximu mAchievabl e Contro l Technolog y (MACT ) standard . Th e Q A Progra moutline s procedure s use dto verify tha t th e CM S ar

e properl y calibrate dan dcollectin g accurate dat ao n a n ongoin g basis . Du e to th e similarit y o f th e thre e CM S system s (on e fo r eac h incinerato r

system) , general reference s to aCM S syste mo r incinerato r

syste mi n thi s documen t wil l impl y al l thre e systems . Informatio n tha t i s onl y applicabl e to on e o r tw o o f th e thre e system s wil l b e clearl y identified . Thi s documen t

i s organize da

s follows : Sectio n 1. 0 Introductio n an dBackgroun d Sectio n 2. 0 CM S Calibratio n an dPreventiv e Maintenanc e Sectio n 3. 0 CM S Recordkeepin g an dReportin g Sectio n 4. 0 CM S Correctiv e Action s Thi s pla n als o assimilate s informatio n an dprocedure s foun di n other documents . A s require db y § 63.6(e)(3)(vi) , othe r document s containin g procedure s o r informatio n referre dt o i n thi s pla n wil l b e mad e availabl e fo r inspectio n whe n requeste db y th e Administrator . Th e remainde r

o f thi s sectio n provide s a n overvie w o f th e incineratio n syste mfollowe d b y adiscussio n o n th e CM S instrumentation . Sectio n 2. 0 discusse s CM S initia l an d continuin g calibratio n an dpreventiv e maintenanc e requirements . Sectio n 3. 0 addresse s requirement s relate dto facilit y documentatio n an dreporting . Sectio n 4. 0 define s an d discusse s nonstandar doperation s o f th e CM S an dapplicabl e correctiv e actions . 1. 1 Summar

y of Facility Informatio n Brie f summarie s whic h describ e th e fixe dheart h incinerator s an dth e rotar y kil n incinerato r

ar e presente di n thi s section . 1.1.1 Fixed

Hearth Incinerators Eac h o f th e fixe dheart

h incinerator s include s th e followin g components :

• Fee dequipmen t

4• Primar y an dsecondary combustio n chamber s
• Lim e injectio n syste m
• Spra y drye r

absorber (SDA )

• Fabri c filte r

baghous e
• Solid s an das h remova l system s
• Induce ddraf

t (ID ) fa n an dstac k

• Instrumentation , controls , an ddat aacquisitio n system s Variou s soli dan dliqui dwaste s an dgaseou s feedstream s ar e thermall y treate di n th e fixe dhearth incinerators . Soli dwast e i s fe dto th e primar y (lower ) combustio n chambe r vi aafee dconveyo r

syste man dpneumati c ram . Liqui dwaste fro mtank s an dtanke r truck s are fe dto th e primar y combustio n chambe r throug h tw o atomize dliqui dinjectors . Liqui dwast e fro mcontainer s ar e fe dto th e primar y combustio n chambe r throug h a specialt y fee dinjector . A gaseou s feedstreami s fe dto th e Uni t 2 primar y combustio n chambe r directl y fro mga s cylinders . Of f gase s fro mahoode dfee demissio n contro l syste man dfro mawast e handlin g glov e bo x ar e fe ddirectl y to th e Uni t 3 secondary combustio n chamber . Combustio n chambe r temperature s ar

e maintaine dusin g natura l ga s fire dto adedicate dburne r i n bot h th e primar y an dsecondary chambers . Combustio n ga s exit s th e secondary combustio n chambe r an denter s th e SDA , whic h provide s aci dgas remova l an dcoolin g o f th e combustio n gas . Combustio n gas exit s th e SD A an di s distribute dto th e fabri c filte r baghouses , whic h provid e particulat e matter removal . Th e induce ddraf t fan , locate ddownstrea mo f th e baghouses , move s th e combustio n gas throug h th e syste man dexhaust s th e ga s throug h th e mai n stack . Hot , we t gas i s extracte ddownstreamo f th e baghous e throug h acontinuou s emission s monitorin g system . Thi s syste mfeature s amulti-componen t infrare dga s analyze r

tha t detect s hydroge n chloride , carbo n monoxide , an dwate r vapo r concentrations . A n integrate dzirconiu moxide-base danalyze r detect s oxyge n concentrations . 1.1.2 Rotary Kiln Incinerator Th e rotar y kil n incinerato r include s th e followin g components :

• Wast e fee dsyste m
• Primar y an dsecondary combustio n chamber s
• Temperin g chambe r
• Lim e injectio n syste m
• Spra y drye r

absorbe r

5• Carbo n injectio n syste m
• Fabri c filte r

baghous e
• Solid s an das h remova l system s
• I D fa n an dstac k

• Instrumentation , controls , an ddat aacquisitio n system s Variou s soli dan dliqui dwaste s ar e thermall y treate di n th e rotar y kil n incinerator . Soli d waste s ar

e fe dto ara mfeede r

vi aaclamshell , adru mfee dconveyor , an dan auxiliar y fee dconveyor . A hydrauli c ra mpushe s th e soli dwaste int o the kiln . Liqui dwaste fro m tank s an dtanke r

truck s i s fe dto th e primar y an dsecondary combustio n chamber s throug h atomize dliqui dinjectors . Combustio n chambe r temperature s ar

e maintaine dusin g natura l gas fire dt o adedicate dburne r i n bot h th e primar y an dsecondary chambers . Combustio n ga s exit s th e secondary combustio n chambe r an denter s th e temperin g chamber , whic h provide s coolin g o f th e combustio n gases . Th e combustio n ga s exit s th e temperin g chambe r

an di s distribute dbetwee n tw o identica l SDAs , whic h provid e aci d ga s remova l an dadditiona l ga s cooling . A carbo n injectio n syste mi s utilize dfo r controllin g dioxin/fura n an dmercur y emissions . Th e activate dcarbo n i s ai r injecte dint o th e combustio n ga s immediatel y downstrea mo f the convergenc e o f

combustio n gase s fro mth e SDAs . Fro mth e SDAs , combustio n gas i s distribute dt o fabri c filte r baghouses , whic h provid e particulat e matter removal . Th e I D fan , locate ddownstreamo f th e baghouses , move s th e combustio n ga s throug h th e syste man dexhaust s th e gas throug h th e mai n stack . Hot , we t ga s i s extracte ddownstrea mo f th e I D fa n throug h acontinuou s emission s monitorin g system . Thi s syste mfeature s amulti-componen t infrare dga s analyze r

tha t detect s hydroge n chloride , carbo n monoxide , an dwate r vapo r concentrations . A n integrate dzirconiu moxide-base danalyze r detect s oxyge n concentrations . 1. 2 CM S Instrumentatio n Thi s sectio n describe s th e CM S instrument s use dmonito r regulate dproces s parameter s fo r demonstratin g on-goin g complianc e wit h the Interi mHW C MAC T emissio n standards . A summary o f specification s fo r

CM S instrumentatio n i s provide di n Tabl e 1-2 . Th e Interi mHW C MAC T standardrequire s al l CMS' s b e installe di n location s tha t provid e representativ e measurement s o f emission s o r

proces s parameters . Al l CM S

6Tabl e 1- 2 CM S Instrumen

tSpecifications Applicatio

n Instrumen t Ta

g Numbe r Manufacture

r Mode

l Operatin

g Rang e Locatio

n Uni tNo . 2 Hig h BT U Liqui dFeedrat e Mas s Flowmete r FT-21 5 Micr o Motio n D 40S-S S 0-3,600 lb/hr Fee dLin e Hig h BT U Liqui dDirec t

Injectio n Feedrat e Scal e WT-215D I Weigh-Troni x WI-.13 0 0-60,000 lb Fee dLin e Lo w BT U Liqui dFeedrat e Mas s Flowmete r FT-21 6 Micr o Motio n D 40S-S S 0-3,600 lb/h r Fee dLin e Lo w BT U Liqui dDirec t

Injectio n Feedrat e Scal e WT-215D I Weigh-Troni x WI-.13 0 0-60,000 l b Fee dLin e Specialt y Fee dWeight Weig h Scal e WT-20 4 Toled o 8140 EX P 0-4,000 lb #20 4 Specialt y Feede r Drumme dSolid s Fee dWeight Weig h Scal e WT-21 0 Toled o A14 0 0-40 0 l b Soli dCharg e

Conveyo r Cylinde r Ga s Feedrat

e d

P Cel l FT-21 7 Yokogaw a YA11 F 0-1 0 in . w.c . (0-60 lb/min ) Cylinde r Ga s Fee dSyste

m PC C Temperatur

e Type K

Thermocoupl e TT-200A/ B Modico n B883-20 0 0-250 0 ° F Primar

y Chambe r SC C Temperatur

e Type K

Thermocoupl e TT-219A/ B Modico n B883-20 0 0-250 0 ° F Secondar

y Chambe r PC C Pressur

e Pressur e Transmitte

r PT-20 0 Rosemon t 1151D P -7. 5 t o 2. 5 in . w.c . Primar y Chambe r ES V Positio n Positio n Switc h ZS-22 4 Square- D 900 7 CG2B 2 open/clos e Emergenc y Stac k Baghous e Inlet

Temperatur

e Typ e K Thermocoupl e TT-27 0 Modico n 833-200 0-2500 ° F SD A Outle t Combustio n Ga s Flo w Rat e dPCel l FT-28 3 Rosemoun t 1151D R 0-20,000 acf m Stac

k Stack Ga s Oxyge n Concentratio n Zirconiu mOxid e Analyze r AT-28 9 COS A ZFN-11YA1-2Z 1 0-25 % CEM S Buildin g Stack Ga s Carbo n Monoxid e Concentratio n Multicomponent Infrare d Photomete

r AT-288 E EcoChe m MC 3 0-20 0 / 0-300 0 ppm v CEM S Buildin g Stac k Hydroge n Chlorid e Concentratio n Multicomponent Infrare d Photomete

r AT-288 E EcoChe m MC 3 0-1000 ppm v CEM S

Buildin g Stac k Ga s Moisture Concentratio n Multicomponent Infrare d Photomete

r AT-288 E EcoChe m MC 3 0-60 % CEM S Buildin g Lim e Slurr

y Flo w Rat

e Mag . Flowmete r FT-28 8 Fischer & Porte r 10D147 5 0-1 0 GP M SD A Penthous e Lim e Slurr

y Densit y Densit

y Transduce r AT-96 8 Solartro n Mobre y 784 6 0-10 0 Lb/Ft 3 SD A Penthous e

7Tabl e 1- 2 (continued) CM S Instrumen

tSpecifications Applicatio

n Instrumen t Ta

g Numbe r Manufacture

r Mode

l Operatin

g Rang e Locatio

n Uni tNo . 3 Hig h BT U Liqui dFeedrat e Mas s Flowmete r FT-31 5 Micr o Motio n DS-04 0 0-3,600 lb/h r Fee dLin e Hig h BT U Liqui dDirec t

Injectio n Feedrat e Scal e WT-315D I Weigh-Troni x WI-13 0 0-60,000 lb Fee dLin e Lo w BT U Liqui dFeedrat e Mas s Flowmete r FT-31 6 Micr o Motio n DS-04 0 0-3,600 lb/hr Fee dLin e Lo w BT U Liqui dDirec t

Injectio n Feedrat e Scal e WT-315D I Weigh-Troni x WI-13 0 0-60,000 lb Fee dLin e Specialt y Fee dWeight Weig h Scal e WT-30 4 Toled o AI40EX P 0-2,000 l b #30

4 Hoode d Feede r Drumme dSolid s Fee dWeigh t Weig h Scal e WT-31 0 Toled o A14 0 0-40 0 lb Soli dCharg e

Conveyor PC C Temperatur

e Typ e K

Thermocoupl e TT-300A/ B Modico n 883-200 0-2500 ° F Primar y Chambe r SC C Temperatur

e Type K

Thermocouple TT-319A/ B Modico n 883-200 0-250 0 ° F Secondar

y Chambe r PC C Pressur

e Pressur e Transmitte

r PT-30 0 Rosemoun t 115 1 d

P -7. 5 t

o 2. 5 in . w.c . Fee dLin e TR V Positio n Positio n Switc h ZS-32 4 Square- D 900 7 CG2B 2 open/clos e Emergenc y Stac k Baghous e Inle

t Temperatur

e Type K

Thermocoupl e TT-37 0 Modico n 833-200 0-250 0 ° F SD A Outlet Combustio n Ga s Flo w Rat e dPCel l FT-38 3 Rosemoun t 115 1 D R 0-20,000 acf m Stac

k Stac k Ga s Oxyge n Concentratio n Zirconiu mOxid e Analyze r AT-38 9 COS A ZFN-11YA1-2Z 1 0-25 % CEM S Buildin g Stac k Ga s Carbo n Monoxid e Concentratio n Multicomponent Infrare d Photomete

r AT-388 E EcoChe m MC 3 0-20 0 / 0-300 0 ppm v CEM S

Buildin g Stac k Hydroge n Chlorid e Concentratio n Multicomponent Infrare d Photomete

r AT-388 E EcoChe m MC 3 0-100 0 ppm v CEM S

Buildin g Stac k Ga s Moisture Concentratio n Multicomponent Infrare d Photomete

r AT-388 E EcoChe m MC 3 0-60 % CEM S Buildin g Lim e Slurry Flo w Rat

e Mag . Flowmete r FT-38 8 Fischer & Porte r 10D147 5 0-1 0 GP M SD A Penthous e Lim e Slurr

y Densit y Densit

y Transduce r AT-96 9 Solartro n Mobre y 784 6 0 - 10 0 Lb/Ft 3 SD A Penthous e

8Tabl e 1 (continued) CM S Instrumen

tSpecifications Applicatio

n Instrumen t Ta

g Numbe r Manufacture

r Mode

l Operatin

g Rang e Locatio

n Uni tNo . 4 Wast e Feedrat e t o X-1 0 Nozzl e Mas s Flowmete r FT-12 9 Micr o Motio n DS100 S 12 8 0-7,00

0 lb/h r Fee dLin e Wast e Feedrat e t o X- l 1 Nozzl e Mas s Flowmete r FT-13 8 Micr o Motio n D100S-H Y 0-6,000 lb/h r Fee dLin e Wast e Feedrat e t o X-l 2 Nozzl e Mas s Flowmeter FT-14 5 Micr o Motio n DL100S-S S 0-8,000 lb/hr Fee dLin e Wast e Feedrat e t o X-2 2 Nozzl e Mas s Flowmete r FT-21 2 Micr o Motio n D1D00S-S S 0-7,000 lb/hr Fee dLin e Cla mShel l Fee dWeight (shredde dsolids ) Loa dCel l WT-00 1 Toled o 8140 0-2,000 lb RamFee d Hopper Dru mConveyo r

Solid s Weight Loa dCel l WT-014 A Toled o 8140 0-1,000 lb Dru m Conveyo r Auxiliar y Conveyo r

Solid s Weight Loa dCel l WT-14 B Toled o 8140 0-20 0 lb Auxiliar y

Conveyo r PC C Temperatur

e Pyromete r TT-305A/ B Irco n Modline 4 44-99-F

1-0- 1 0-3,000 ° F Kil n Outlet SC C Temperatur

e Type R

Thermocoupl e TT-317A/ B Chesse l 351 0 0-3,000 ° F SC C Outlet PC C Pressur

e Pressur e Transmitte

r PT-30 0 Rosemoun t 1151DR2 F -9. 0 t o 1. 0 in . w.c . Kil n Hoo d Surge Ven t

Positio n Positio n Switc h ZSC-02 6 Square- D 9007 CG2B 2 open/clos e Kil n Fac e TR V Positio n Positio n Switc h ZSC-31 6 Square- D 900 7 CG2B 2 open/clos e Emergenc y Stac k Carbo n Feedrat

e Feede r C-1 7 K-Tro n K2T3 5 0-10 0 Carbo n Inject .

Syste m Carbo n Injectio n Carrier

Ga s Suppl y Pressur

e Pressur e Switc h PSL-438 A Dwye r 333 0 Tri p Points : ± 5 in . w.c . Carbo n

Injectio n Lin e Carbo n Feede

r Discharg e Pressur

e Pressur

e Switc h PSH-438 B Dwye r 321 5 Tri p Points : < 3 psi g > 1 3 psi g Carbo n

Injectio n Lin e

9Tabl e 1 (continued) CM S Instrumen

tSpecifications Applicatio

n Instrumen t Ta

g Numbe r Manufacture

r Mode

l Operatin

g Rang e Locatio

n Uni tNo . 4 (continued

) SD A X-l 8 Outle

t Temperatur

e (Baghous e Inlet

Temperature) Type K

Thermocoupl e TT-417A/ B Modico n B883-20 0 0-2,50 0 ° F SD A X- l 8

Outle t SD A X-l 9 Outlet

Temperatur

e (Baghous e Inle

t Temperature) Type K

Thermocouple TT-418A/ B Modico n B883-20 0 0-2,500 ° F SD A X-l 9 Outle t Combustio n Ga s Flowrat e Pito t

Tube/d P Cel l FT-559A/ B Automatio n Servic e 1151DRF228 3 0-55,000 acf m Stac

k Stac k Ga s Oxyge n Concentratio n Zirconiu mOxid e Analyze r AT-560A/ B COS A ZFN-11YA1-2Z 1 0-20 % CEM S Buildin g Stack Ga s Carbo n Monoxid e Concentratio n Multicomponent Infrare d Photomete

r AT-556 E EcoChe m MC 3 0-20 0 / 0-300 0 ppm v CEM S Buildin g Stac k Hydroge n Chlorid e Concentratio n Multicomponent Infrare d Photomete

r AT-556 E EcoChe m MC 3 0-100 0 ppm v CEM S

Buildin g Stac k Ga s Moisture Concentratio n Multicomponent Infrare d Photomete

r AT-556 E EcoChe m MC 3 0-60 % CEM S Buildin g

Lim e Slurr

y Flo w Rat

e Mag . Flowmete r FT-61 5 Fischer & Porte r 10D147 5 0-8 0 GP M SD A Nozzle s Lim e Slurr

y Densit y Densit

y Transduce r DIT-60 9 Solartro n Mobre y 784 6 0 - 10 0 Lb/Ft 3 Lim e Sil o

1 0operatin g parameter measurement

device s a

t th e Veoli afacilit y ar

e installe di n complianc e wit h thi s requirement . A descriptio n o f th e type s o f

CM S instrumentatio n follows : Mass/Feedrat

e Monitors : Liqui dwaste feedrate s fro mtank s ar e measure db y corioli s mas s flowmeters . Direc t

injec t liqui dfeedrate s fro mtanke r truc k ar e calculate dusin g th e continuousl y monitore dweigh t

o f th e tanker . Al l soli dwaste charge s ar e weighe dusin g ascale/loa dcel l prio r to bein g fee dto th e incinerator . Thes e measurement s ar e use dto calculat e pumpabl e waste , tota l waste , an dconstituen t

feedrates . Fo r Uni t 4 , th e outpu t

o f acalibrate dfeede r

i s utilize dto calculat e th e feedrate o f powdere d activate dcarbon , whic h i s injecte dint o th e plenu mupstreamo f th e baghouses . Pressure/Differential Pressur e Monitors : Primar y combustio n chambe r pressure i s measure d b y diaphrag mactuate dpressure transmitters . Th e positio n o f th e dampe r

immediatel y upstream o f th e I D fa n i s varie dto contro l stac k ga s flowrat e an dt o maintai n kil n combustio n chambe r negativ e pressur e (draft) . Th e primar y combustio n chamber pressur e i s interlocke dwit h waste feeds . Fo r Uni t 2 , pressur e dro p i n th e cylinde r ga s feedstrea mi s measure dan dconverte dto afeedrate . Th e feedrat e i s use dto calculat e thi s feedstream' s contributio n to th e chlorine , lo w volatil e metals , an dsemivolatil e metal s feedrate s to th e incinerator . Fo r Uni t 4 , pressure switche s ar e utilize dto ensure tha

t th e carbo n feede r

discharg e pressure , an d th e carbo n injectio n ai r blowe r discharg e pressur e ar

e withi n th e desig n limits . Th e pressur e dro p acros s apito t tub e i n th e stac k

i s continuousl y monitore dan duse dto calculat e th e stac k ga s flowrate . Temperature Monitors : Fo r Unit s 2 an d3 , redundan t thermocouple s ar

e use dto measure the temperature i n bot h combustio n chambers . A thermocoupl e i s als o locate da t the exi t to th e SD A an di s th e primar y elemen t fo r th e SD A exi t

temperature contro l loop . Uni t 4 i s equippe dwit h redundan t pyrometer s i n th e primar y chambe r an dredundan t thermocouple s i n th e secondary chamber . Eac h SD A outle t i s equippe dwit h redundan t thermocouple s use dfo r temperature contro l an dmonitorin g o f th e baghous e inle t

temperature .

1 1Emergency Safet y Ven tPositio n Monitors : Th e positio n o f th e emergenc y safet y ven t (ESV ) i s indicate da s ope n o r close db y apositio n transmitter . N o waste o r fue l can b e fe di f

the ES V positio n i s "open" . Th e Emergenc y Safet y Ven t (ESV ) Pla n provide s detail s o n th e ES V systems . Ba g Lea k Detectio n System : A triboelectri c senso r i s locate ddownstrea mo f the I D fa n an d monitor s th e relativ e particulat e matter loadin g o f

th e combustio n ga s exitin g th e baghouses . Alarm s an dinterlock s base do n thi s relativ e measuremen t ar e indication s o f

apotentia l ba g lea k o r failure . Procedure s fo r setu p an dadjustment s to th e ba g lea k detectio n syste mar

e no t covere d b y thi s Q C program . Th e Operatio n an dMaintenanc e Pla n provide s detail s o n th e ba g lea k detectio n system . Continuou s Emission s Monitorin g System : Th e CEM S continuousl y sample s an danalyze s stac k gas fo r th e concentration s o f carbo n monoxid e (CO) , Hydroge n Chlorid e (HCl) , an d moistur e usin g amulticomponen t infrare dphotometer . Th e oxyge n concentratio n i s analyze d simultaneousl y usin g azirconiu moxid e analyzer . Thes e dat aar e use dt o calculat e th e stac k ga s C O concentratio n o n adr y basis , correcte dto 7 % 0 2 . Th e CEM S Q A Pla n provide s additiona l detail s o n th e CEMS .

1 22.

0 CM S CALIBRATIO N AN D PREVENTIV E MAINTENANC E Thi s sectio n discusse s th e calibratio n an dpreventiv e maintenanc e requirement s t o meet th e requirement s o f

§ 63.8(d) . 2. 1 CM S Calibratio n T o ensur e ongoin g complianc e wit h th e Interi mHW C MAC T standard , i t i s essentia l tha

t th e dat acollecte dfro mth e CM S b e measure dan drecorde di n an accurat e manner . Initia l calibrations , subsequent calibration , an dCEM S calibration s ar e describe di n thi s section . 2.1.1 Initial

CMS Calibration A s par t o f Veolia' s Qualit y Contro l Program , th e CM S instrument s wer e initiall y calibrate dprio r to th e Interi mHW C MAC T complianc e date . Calibratio n prio r to th e complianc e dat e i s require ds o tha

t al l collecte ddat aar

e reliabl e an daccurate . Al l initia l calibratio n dat aar e par t o f th e operatin g record . Initia l calibration s o f new/replacemen t

instrument s wil l b e performe dpe r th e manufacture' s writte n procedures . I n lie u o f an initia l calibratio n fo r new/replacemen t instrument s o r

instrumen t

components , th e facilit y ma y us e amanufacturer' s certification . 2.1.2 Subsequent

CMS Calibration Subsequent

calibration s o n CM S instrumentatio n wil l b e performe da s neede dan di n accordanc e wit h th e manufacture' s writte n procedures . Calibration s wil l b e performe das correctiv e measure s fo r

hig h calibratio n drift . Calibration s ma y b e require dwhe n restorin g CM S instrument s afte r

maintenanc e o r

repairs . Al l calibratio n adjustment s wil l b e documente db y record s o f

th e calibratio n drif

t determine dbefor e an dafte r th e instrumen t

wa s serviced . Som e instrument s suc h as differentia l pressure cell s mus t b e remove dfro mservic e an dbenc h calibrated . T o minimiz e downtim e thes e instrument s ma y b e replace dwit h acalibrate dspare . Th e Uni t 4 primar y combustio n chambe r pyrometer s wil l b e replace da t leas t annuall y wit h a factor y calibrate dpyrometer . Electroni c check s an dreplacement s o f thermocouple s wil l b e performe dpe r

th e facility' s Thermocoupl e Calibration , Operation , an dReplacemen t Procedure . A calibratio n recor dfor mi s availabl e fo r eac h CM S instrumen t

an dwil l b e use dto documen t calibratio n audits , calibrations , an dreplacements . Th e mos t recentl y complete dcalibratio n recor ddocument s tha

t th e instrumen t

i n servic e meet s th e qualit y contro l criteri ase t fort h b y thi s program . Thes e calibratio n record s contai n "calibratio n notes " whic h provid e th e instrumen t technicia n wit h procedure s specifi c to agive n instrument . Th e calibratio n recor dform s fo r CM S instrument s ar

e incorporate di n thi s Q C Progra mb y reference .

1 32.1.3 CEMS Calibration Audits and Calibration CEM S QA/Q C procedure s ar e provide db y th e Continuous Emission Monitoring System Quality Assurance Plan. Thes e procedure s ar e maintaine da

t th e facilit y an ddescrib e th e requirement s fo r CEM S drif

t checks , audits , calibrations , preventiv e maintenance , an drecordkeeping . 2. 2 CM S Calibratio n Audit s C M S calibratio n audit s ar e performe dto determin e th e calibratio n drif t (CD ) o f

CM S instruments . Calibratio n Drif t (CD ) i s th e bia s betwee n th e CM S instrumen t readin g an da calibratio n reference . Tabl e 2- 1 present s th e requirement s fo r CM S calibratio n audits . Eac h C M S instrumen t

wil l b e subjecte dacalibratio n audi t a t th e frequenc y indicate di n Tabl e 2-1 . Th e calibratio n audi t

wil l b e performe da

t th e low-leve l (zero ) an dhigh-leve l check s indicated . Th e calibratio n chec k

wil l confir mtha

t al l proces s variabl e indication s (e.g. , loca l reading , contro l roo mdisplay ) a t th e high-leve l valu e agre e wit h th e calibratio n referenc e withi n Vi o f th e require dtolerance . Calibratio n adjustments/correctiv e action s mus t b e take n i f

thi s calibratio n drift i s greater

tha n Vi o f

th e require dtolerance . I f th e calibratio n drif

t exceed s th e require d tolerance , th e instrumen t i s considere dout-of-control . Sectio n 4. 0 describe s th e correctiv e action s fo r

out-of-control , inoperative , an dmalfunctionin g CMS . I f th e accurac y o f

aCM S instrumen t

i s i n question , th e C D i s determine dan ddocumente dprio r t o performin g maintenance , repairs , o r adjustments . Th e troubleshooting/calibration s o f CM S instrument s wil l b e performe di n amanne r consisten t

wit h th e manufacturer' s writte n procedure s an drecommendations . Th e C D determine dafte r calibrations/correctiv e action s hav e bee n take n wil l documen t

the effect s o f

the adjustment s an ddemonstrate tha t th e instrumen t

i s performin g properly . Calibratio n record s wil l documen t CD , whic h i s an indicato r o f th e stabilit y o f

the CM S calibratio n ove r

time . Th e amount

o f drif t an dstabilit y i s dependant o n the typ e o f

instrumen t an dth e calibratio n frequency . Veoli ama y increas e o r decreas e th e frequenc y o f particula r calibratio n audit s to th e extent warrante db y an assessment o f an instrument' s stability . Veoli a wil l maintai n regularl y schedule dcalibratio n audi t interval s fo r

eac h CM S instrument . Calibration s wil l b e performe dto preven t excessiv e C D an dto maintai n the validit y o f the dat a collecte dfro mth e monitorin g system .

1 4T V .2- 1 CM S Calibratio n Audi tRequirement s Applicatio

n Instrumen t Ta

g Numbe r Frequenc

y o f Calibratio

n Audit Lo

w Leve l Chec k Poin t Hig

h Leve l Chec k Poin t Toleranc

e Uni tNo . 2 Hig h BT U Liqui dFeedrat e Mas s Flowmete r FT-21 5 Annuall y 0- 5 lb/mi n 15-2 5 lb/mi n 10 % Hig h BT U Liqui dDirec t Injectio n Feedrat e Scal e WT-215D I Quarterly 01 b 25,000 lb 10 % Lo w BT U Liqui dFeedrat e Mas s Flowmete r FT-21 6 Annuall y 0- 5 lb/mi n 15-2 5 lb/mi n 10% Lo w BT U Liqui dDirec t

Injectio n Feedrat e Scal e WT-215D I Quarterly 01 b 25,000 lb 10 % Specialt y Fee dWeight Weig h Scal e WT-20 4 Quarterly 01 b -50 0 lb 10 % Drumme dSolid s Fee dWeight Weig h Scal e WT-21 0 Quarterly 01 b -5 0 lb 10 % Cylinde r Ga s Feedrat

e d

P Cel l FT-21 7 Annuall y 0 in . w.c . 1 0 in . w.c . 10% Primar y Combustio n Chambe

r Temperatur

e Type K Thermocoupl e TT-200A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur

e Secondar y Combustio n Chambe

r Temperatur

e Type K Thermocoupl e TT-219A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e Primar y Combustio n Chambe

r Pressur e Pressur e Transmitte

r PT-20 0 Quarterly -7. 5 t o -6. 5 1.

5 t o 2. 5 i n w.c . 10 % ES V Positio n Positio n Switc h ZS-22 4 Annuall y AWFC O interloc k energize dwhen ope

n Pas s Baghous e Inlet

Temperatur

e Typ e K

Thermocoupl e TT-27 0 Se e Calibratio n RecordForm Combustio n Ga s Flo w Rat e d

P Cel l FT-28 3 Annuall y 0-0.05 in . w.c . 0.45-0.5 0 in . w.c . 10 % Lim e Slurry Flo w Rat

e Mag . Flowmete r FT-28 8 Annuall y 0 gpm 1-1 0 gp m 10% Lim e Slurr

y Densit y Densit

y Transduce

r AT-96 8 Replace , a s required , with factory service dtransduce r Stack Ga s Oxyge n Concentratio n Zirconiu mOxid e Analyze r AT-28 9 Per CEM S QAPla n Stack Ga s Carbo n Monoxid e Concentratio n Multicomponent Infrare d Photomete

r AT-288 E Per CEM S QAPla n Stac k Hydroge n Chlorid e Concentratio n Multicomponent Infrare d Photomete

r AT-288 E Per CEM S QAPla n Stac k Ga s Moisture Concentratio n Multicomponent Infrare d Photomete

r AT-288 E Per CEM S QAPla n

1 5Tabl e 2- 1 (continued) CM S Calibratio n Audi tRequirement s Applicatio

n Instrumen t Ta

g Numbe r Frequenc

y o f Calibratio

n Audi t Lo w Leve l Chec k Poin t Hig

h Leve l Chec k Poin t Toleranc

e Uni tNo . 3 Hig h BT U Liqui dFeedrat e Mas s Flowmete r FT-31 5 Annuall y 0-5 lb/mi n 15-2 5 lb/mi n 10 % Hig h BT U Liqui dDirec t Injectio n Feedrat e Scal e WT-315D I Annuall y 01 b 25,000 lb 10 % Lo w BT U Liqui dFeedrat e Mas s Flowmete r FT-31 6 Annuall y 0- 5 lb/h r 15-2

5 lb/mi n 10 % Lo w BT U Liqui dDirec t

Injectio n Feedrat e Scal e WT-315D I Annuall y 01 b 25,000 lb 10 % Specialt y Fee dWeight Weig h Scal e WT-30 4 Quarterly 01 b -20 0 lb 10 % Drumme dSolid s Fee dWeight Weig h Scal e WT-31 0 Quarterly 01 b -5 0 lb 10 % Primar y Combustio n Chambe

r Temperatur

e Type K Thermocoupl e TT-300A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e Secondar y Combustio n Chambe

r Temperatur

e Type K Thermocoupl e TT-319A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e Primar y Combustio n Chambe

r Pressur e Pressur e Transmitte

r PT-30 0 Quarterly -7. 5 t o -6. 5 1.

5 t o 2. 5 i n w.c . 10 % ES V Positio n Positio n Switc h ZS-32 4 Annuall y AWFC O interloc k energize dwhen ope

n Pas s Baghous e Inle

t Temperatur

e Typ e K

Thermocouple TT-37 0 Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e Combustio n Ga s Flo w Rat e d

P Cel l FT-38 3 Annuall y 0-0.0 5 in . w.c . 0.45-0.5 0 in . w.c . 10 % Lim e Slurr

y Flo w Rat

e Mag . Flowmete r FT-38 8 Annuall y 0 gpm 1-1 0 gpm 10 % Lim e Slurr

y Densit y Densit

y Transduce

r AT-96 9 Replace , a s required , with factor

y service dtransduce

r Stac k Ga s Oxyge n Concentratio n Zirconiu mOxid e Analyze r AT-38 9 Pe r CEM S QAPla n Stac k Ga s Carbo n Monoxid e Concentratio n Multicomponent Infrare d Photomete

r AT-388 E Per CEM S Q A Plan Stac k Hydroge n Chlorid e Concentratio n Multicomponent Infrare d Photomete

r AT-388 E Per CEM S Q A Plan Stac k Ga s Moisture Concentratio n Multicomponent Infrare d Photomete

r AT-388 E Per CEM S Q A Plan

1 6Tabl e 2-

_continued ) CM S Calibratio n Audi tRequirement s Applicatio

n Instrumen t Ta

g Numbe r Frequenc

y o f Drif t Check/Accurac

y Audi t Lo

w Leve l Chec k Poin t Hig

h Leve l Chec k Poin t Toleranc

e Uni tNo . 4 Wast e Feedrat e t o X-l 0 Nozzl e Mas s Flowmete r FT-12 9 Annuall y 0- 5 lb/mi n 15-2 5 lb/mi n 10 % Wast e Feedrat e t o X- l 1 Nozzl e Mas s Flowmete r FT-13 8 Annuall y 01 b 21,000 lb 10 % Wast e Feedrat e t o X-l 2 Nozzl e Mas s Flowmete r FT-14 5 Annuall y 0-5 lb/mi n 15-2 5 lb/mi n 10 % Wast e Feedrat e t o X-2 2 Nozzl e Mas s Flowmete r FT-21 2 Annuall y 01 b 21,000 lb 10 % Cla mShel l Fee dWeight (shredde dsolids ) Loa dCel l WT-00 1 Quarterly 01 b -20 0 lb 10 % Dru mConveyo r

Solid s Weight Loa dCel l WT-014 A Quarterly 01 b -10 0 lb 10 % Auxiliar y Conveyo r

Solid s Weight Loa dCel l WT-14 B Quarterly 01 b -5 0 l b 10 % Primar y Combustio n Chambe

r Temperatur

e Pyromete r TT-305A/ B Replac e a t least annually with factor

y calibrate dPyromete

r Secondar y Combustio n Chambe

r Temperatur

e Typ e R Thermocoupl e TT-317A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e Primar y Combustio n Chambe

r Pressur e Pressur e Transmitte

r PT-30 0 Quarterly -9. 0 t o -8. 0 in . w.c . 0 t

o 1. 0 in . w.c . 10 % Surge Ven t

Positio n Positio n Switc h ZS-02 6 Annuall y AWFC O interloc k energize dwhen ope

n Pas s ES V Positio n Positio n Switc h ZS-32 4 Annuall y AWFC O interloc k energize dwhen open Pas s Carbo n Feedrat

e Feede r WT-43 8 Quarterly 0 lb/mi n 6-3 0 lb/mi n 10 % Carbo n Injectio n Carrier

Ga s Lo w Pressur e Pressur e Switc h PSL-438 A Annuall y Energiz e Switc h Pas s Carbo n Injectio n Carrier

Ga s Hig h Pressur

e Pressur e Switc h PSH-438 B Annuall y Energiz e Switc h Pas s

1 7Tabl e 2- 1 (continued) CM S Calibratio n Audi tRequirement s Applicatio

n Instrumen t Ta

g Numbe r Frequenc

y o f Drif t Check/Accurac

y Audi t Lo

w Leve l Chec k Poin t Hig

h Leve l Chec k Poin t Toleranc e Uni tNo . 4 (continued

) SD A X- l 8 Outlet

Temperatur

e (Baghous e Inlet

Temperature) Type K

Thermocouple TT-417A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e SD A X-l 9 Outle

t Temperatur

e (Baghous e Inlet

Temperature) Type K

Thermocouple TT-418A/ B Refe r t o th e Thermocoupl e Calibration , Operation , an dReplacemen

t Procedur e Combustio n Ga s Flowrate Pito t Tube/d P Cel l FT-559A/ B Annuall y 0 in . w.c . 1.7 4 i n w.c . 10 % Lim e Slurr

y Flo w Rat

e Mag . Flowmete r FT-61 5 Annuall y 0 gpm 1-1 0 gp m 10 % Lim e Slurr

y Densit y Densit

y Transduce

r DIT-60 9 Replace , a s required , with factor

y service dtransduce

r Stac k Ga s Oxyge n Concentratio n Zirconiu mOxid e Analyze r AT-560A/ B Per CEM S Q A Plan Stac k Ga s Carbo n Monoxid e Concentratio n Multicomponent Infrare dPhotomete

r AT-556 E Pe r CEM S QAPla n Stac k Hydroge n Chlorid e Concentratio n Multicomponent Infrare dPhotomete

r AT-556 E Pe r CEM S QAPla n Stac k Ga s Moisture Concentratio n Multicomponent Infrare dPhotomete

r AT-556 E Pe r CEM S QAPla n

1 82.

3 Preventive Maintenanc e Veoli atake s dail y proactiv e measure s to assur e tha t potentia l problem s wit h th e CM S ar e quickl y identifie dan davoided , i f possible . Dail y maintenanc e check s include :

• Verificatio n tha

t proces s variable s ar

e reasonabl e
• Compariso n o f

reading s fro mredundant instrument s
• Cleanin g an dvisua l chec k o f monitorin g equipmen t

• Communicatio n betwee n operator s an dinstrumen t technician s Thes e check s ar

e documente do n adail y logshee t fo r eac h incinerator . Th e preventiv e maintenanc e o n the CM S als o include s th e calibratio n audit s previousl y described . Al l necessar y part s fo r routin e repair s o f

th e affecte dCM S equipmen t ar e mad e readil y availabl e onsite . A spar e part s inventor y fo r

eac h componen t

o f th e CM S i s include di n th e record s maintaine db y th e Maintenanc e Department . Additiona l detail s regardin g preventiv e maintenanc e applicabl e to th e CM S ar

e provide di n th e facility' s Operatio n an dMaintenanc e Pla n an dth e CEM S Q A Plan .

1 93.

0 CM S RECORDKEEPIN G AN D REPORTIN G Thi s sectio n discusse s recordkeepin g an dreportin g requirement s fo r CM S instrumentatio n a

s specifie db y § 63.1211 . 3. 1 Recordkeepin g Veoli awil l follo w th e recordkeepin g requirement s as specifie di n § 63.10(b) , includin g th e semiannua l exces s emission s an dCM S performanc e report . Veoli awil l maintai n thes e record s o f

CM S dat afo r

aminimu mo f

5 year s followin g the dat e o f eac h occurrence , measurement , maintenance , correctiv e action , report , o r record . A t

a minimum , th e mos t

recen t 2 year s o f

dat awil l b e retaine donsite . Belo w i s abrie f summar y o f

thes e requirements . Veoli awil l maintai n record s o n the following :

• Th e occurrenc e an dduratio n o f eac h startup , shutdown , o r malfunctio n o f operation . • Th e occurrenc e an dduratio n o f eac h malfunctio n o f

th e ai r pollutio n contro l an dmonitorin g equipment . Maintenanc e performe do n the ai r pollutio n contro l an dmonitorin g equipmen t
• Action s take n durin g period s o f startup , shutdown , an dmalfunctio n (includin g correctiv e action s to restore th e proces s o r ai r pollutio n contro l syste mto norma l operation ) whe n suc h action s ar e differen t

th e procedure s outline di n th e SSM P

• Al l informatio n necessar y to demonstrate conformanc e wit h the SSM P

• Eac h perio di n whic h aCM S i s malfunctionin g o r inoperativ e (includin g out of-contro l periods )

• Al l require dmeasurement s neede dto demonstrate complianc e wit h arelevan t standard . • Al l result s o f

performanc e tests , CM S performanc e evaluations , an dopacit y an dvisibl e emissio n observation s • Al l CM S calibratio n check s
• Al l adjustment s an dmaintenanc e performe do n CM S

• Al l require dCM S measurement s (includin g dat arecorde ddurin g unavoidabl e CM S breakdown s an dout-of-contro l periods )

• Th e dat

e an dtim e identifyin g eac h perio ddurin g whic h th e CM S wa s inoperativ e excep t

fo r zer o (lo w level ) an dhig h leve l check s

2 0• Th e dat e an dtim e identifyin g eac h perio ddurin g whic h th e CM S wa s out-of

contro l as define db y § 63.8(c)(7 )

• Th e specifi c identificatio n (dat e an dtim e o f

commencemen t

an dcompletion ) o f eac h perio do f

exces s emission s an dparameter monitorin g exceedances , a s define di n th e relevan t

standard , tha

t occur s durin g period s other tha n startup , shutdowns , an dmalfunctions . • Th e nature an dcaus e o f an y malfunctio n
• Th e correctiv e actio n taken o r preventive measure s adopte d

• Th e nature o f

th e repair s o r

adjustment s to the CM S tha t wa s inoperativ e o r out-of-contro l

• Th e tota l proces s operatin g tim e durin g th e reportin g perio d

• Al l procedure s tha t ar e par t o f qualit y contro l progra mdevelope dan d implemente dfo r

CM S unde r

§ 63.8(d) . A l l CM S instrumentatio n wil l b e operate do n acontinuou s basis . Th e detecto r respons e wil l b e evaluate da

t leas t ever y 1 5 seconds , an dthes e value s wil l b e use dto calculat e regulate dparameters . Fo r parameter s interlocke dwit h th e AWFC O syste mo n an hourl y rollin g averag e basis , ra w dat awil l b e average dan drecorde da t leas t onc e pe r

minute . On e minut e average s wil l b e use dto calculat e th e hourl y rollin g averages . Th e pumpabl e waste , tota l waste , an dconstituen t feedrat e operatin g parameter limit s ar

e base s o n rollin g total s i n lie u o f

rollin g averages . A n integra l par

t o f th e CM S i s th e dat aacquisitio n an ddat ahistoria n systems , whic h record s al l operatin g dat agenerate db y the CM S instruments . Th e dat ahistoria n an d associate darchiv e file s ar e par t o f th e operatin g record . CM S instrumen t calibrations , maintenanc e activities , an dcorrectiv e action s ar e recorde dan dkep t

i n th e operatin g record . Al l dat acollecte ddurin g CM S PET s ar e recorde dan dkep t

i n th e operatin g record . 3. 2 Reportin g Veoli awil l follo w th e reportin g requirement s as specifie di n § 63.10 . I n addition , Veoli a wil l develo p an dinclud e i n th e operatin g recor daDocumentatio n o f Complianc e (DOC ) pe r § 63.1211(c) . Th e DO C mus t includ e asigne dan ddate dcertificatio n tha t th e CEM S an dCM S ar

e installed , calibrated , an dcontinuousl y operatin g i n complianc e wit h th e requirement s o f

Subpar t EEE .

2 1Ra w dat afro mth e CM S wil l b e collected , reducedas describe di n § 63.8(g) , an d

include di n th e CM S PE T report . Thi s dat awil l b e analyze dto determin e complianc e wit h th e HW C MAC T an dth e result s wil l b e submitte das par t o f the notificatio n o f complianc e require db y § 63.1207(j) . Th e conten t

an ddeadlin e requirement s fo r the exces s emission s an dmonitorin g syste m performanc e report s ar e specifie di n § 63.10(e)(3)(v) . Th e requirement s fo r the summary report are give n i n § 63.10(e)(3)(vi) . A s note di n § 63.10(e)(3)(vii) , Veoli ai s require dt o onl y submi t th e summar y repor

t i f th e tota l duratio n o f

exces s emission s o r

proces s o r

contro l syste mparamete r exceedance s fo r th e reportin g perio di s les s tha n on e percen t o f th e tota l operatin g tim e fo r the reportin g period , an dCM S downtim e fo r th e reportin g perio di s les s than fiv e percen t o f th e tota l operatin g tim e fo r

th e reportin g period . Conversely , additiona l reportin g i s require db y § 63.10(e)(3)(viii ) i f

th e tota l duratio n o f

exceedances , o r

the tota l CM S downtim e durin g th e reportin g period , i s greater tha n th e allowabl e percentag e o f th e reportin g period . Tabl e 3- 1 provide s alis t o f Veolia' s reportin g requirements .

2 2Tabl e 3- 1 Reportin g Requirement s Regulatory Citatio n Descriptio n Frequency § 63.1211(c ) Recor dDocumentatio n o f Complianc e i n th e operatin g recor d Onc e § 63.10(d)(2 ) Befor e Titl e V permi t ha s bee n issued , owne r operato r mus t submi t result s o f

performanc e test . B y th e 60th day followin g ever y performanc e tes t § 63.10(d)(2 ) Afte r Titl e V permi t

ha s bee n issued , owne r operato r mus t submi t result s o f

require dperformanc e tests . B y th e 60t h day followin g require d performanc e tes t § 63.10(d)(4 ) Progres s report s A s specifie di n writte n extensio n o f complianc e § 63.10(d)(5)(i ) Periodi c startup , shutdown , an dmalfunctio n report s

(durin g reportin g period ) Submitte d simultaneou s wit h exces s emissio n repor

t §63.10(d)(5)(ii ) Startup , shutdown , an dmalfunctio n report s whe n

action s ar

e take n tha

t ar e inconsisten t

wit h SSMP . 2 workin g day s fro m commencemen t

o f action , followe dwit h a lette r explainin g extent withi n 7 workin g days . § 63.10(e)(3)(i ) Submitta l o f semiannua l exces s emission s an dCM S performanc e repor

t Semiannuall y - b y th e 30th day followin g th e en do f eac h calenda

r hal f performanc e tes t

234.0 CM S CORRECTIV E ACTION S

I f aCM S i s foun dto b e out-of-control , inoperative , o r malfunctioning ; correctiv e action s mus t b e take n to retur n th e CM S to norma l operation . Definition s use di n determinin g th e typ e o f

correctiv e actio n require dar e give n below . Out-of-control: A CM S i s out-of-contro l if :

• Th e zer o (lo w level) , mid-level , o r high-leve l calibratio n drif t exceed s tw o time s th e applicabl e C D specificatio n i n th e applicabl e performanc e specificatio n o r

procedure ; o r
• Th e CM S fail s aperformanc e tes t audit , relativ e accurac y audit , relativ e accurac y tes t

audit , o r linearit y tes t

audit . Th e onl y applicabl e performanc e specificatio n to th e CM S i s Performanc e Specificatio n (PS ) 4 B o f

4 0 CF RPart

63 , Appendi x B . P S 4 B applie s to th e 0 2an dC O CEMS . Th e requirement s o f

P S 4 B an dadditiona l requirement s Veoli aimpose s o n th e CEM S ar e detaile di n th e CEM S Q A Plan . I n th e absenc e o f promulgate dperformanc e specificatio n applicabl e to non-CEM S CM S instruments , Veoli aha s self-impose dahigh-leve l C D specification , as describe di n Sectio n 2.0 . Whe n aCM S i s out-of-control , Veoli awil l take th e necessary correctiv e actio n an dshal l repea t al l necessary test s whic h indicat e tha t th e syste mi s out-of-control . Correctiv e action s an dretestin g wil l continu e unti l th e CM S i s returne dto norma l operation . Th e beginnin g o f

th e out-of-contro l perio di s the hou r tha t th e calibratio n drif

t indicate s tha

t th e CM S ha s exceede dit s performanc e specifications . Th e en do f th e out-of-contro l perio di s th e hou r

followin g th e completio n o f correctiv e actio n an dsuccessfu l demonstratio n tha

t the CM S i s withi n it s allowabl e limits . Durin g th e perio dth e CM S i s out-of-control , recorde ddat ashal l no t b e use di n dat aaverage s an dcalculations , o r t o mee t an y dat aavailabilit y requiremen t establishe dunde r

thi s part . Veoli awil l submi t

al l informatio n concernin g out-of-contro l periods , includin g star t an d en ddate s an dhours , an ddescription s o f correctiv e action s taken , i n th e exces s emission s an dcontinuou s monitorin g syste mperformanc e repor t require db y § 63.10(e)(3) . Malfunction: Fo r

us e i n thi s plan , malfunctio n i s define das an y sudden , infrequent , an d no t reasonabl y preventabl e failur e o f ai r pollutio n contro l o r

monitorin g equipment .

2 4Malfunctio n als o include s th e failur e o f aproces s o r

an y proces s equipmen t to operat

e i n anorma l o r

usua l manner . Failure s tha t ar e cause di n par

t b y poo r

maintenanc e o r careles s operatio n ar

e no t malfunctions . Th e Program of

Corrective Actions for

Malfunctions i s Attachmen t 4 o f the SSM P Plan . Thi s progra maddresse s ho w th e incinerato r wil l b e operate dan dmaintaine ddurin g malfunctions . I n thi s program , potentia l malfunction s ar e liste dfo r

eac h portio n o f

th e incinerato r

system . Th e malfunction s ar e event s tha

t ar e recognize db y th e operator , o r indicate db y a n alarm , an dthreate n to caus e a n exceedance . I n th e respons e to th e malfunctio n and/o r

alarms , th e operato r

wil l appl y discretio n an dattemp t to maintai n th e incinerato r

syste mwithi n regulator y limits . I n th e progra mo f correctiv e actions , potentia l cause s o f

eac h malfunctio n ar

e listed . Th e operato r wil l utiliz e proces s knowledge , jo b experience , and , i f needed , assistanc e fro mother personne l to identif

y th e caus e o f th e malfunction . Fo r eac h potentia l cause , action s to correc t th e failur e are listed . Th e correctiv e action s prescribe dma y requir e th e collaboratio n o f multi

discipline dpersonne l wh o ar e qualifie dto return th e incinerato r syste mto prope r

workin g condition s (i.e. , maintenanc e personnel , instrumen t technicians , engineering )

2 5