Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet If you choose "other" please provide a description of the fuel in the Other Fuel Description column

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mincomposite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop‐down boxes to fill in the unit

Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop‐down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention:

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.3. Please choose the type of fuel being sampled using the drop‐down in the fuel column of the Boiler Information

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865‐04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell).

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mincomposite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop‐down boxes to fill in the unit

measure.
EIA Facility Code Facility Name Boiler ID Fuel Type 1

7213 Clover 1 bituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

7213 Clover 1 As Received Higher Heating Value

7213 Clover 1 As Received % Moisture

7213 Clover 1 As Received % Ash

7213 Clover 1 As Received % Sulfur

7213 Clover 1 Dry basis Higher Heating Value

7213 Clover 1 Dry basis % Ash

7213 Clover 1 Dry basis % Sulfur

7213 Clover 1 Dry basis Antimony

7213 Clover 1 Dry basis Arsenic

7213 Clover 1 Dry basis Beryllium

7213 Clover 1 Dry basis Cadmium

7213 Clover 1 Dry basis Chlorine

7213 Clover 1 Dry basis Chromium

7213 Clover 1 Dry basis Cobalt

7213 Clover 1 Dry basis Fluorine

7213 Clover 1 Dry basis Lead

7213 Clover 1 Dry basis Manganese

7213 Clover 1 Dry basis Mercury

7213 Clover 1 Dry basis Nickel

7213 Clover 1 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D2015

ASTM D‐3173

ASTM D‐3174

ASTM D 4239

ASTM D2015

ASTM D‐3174

ASTM D 4239

SW 846 7041

SW 846 7060A

SW 846 6010B

SW 846 6010B

ASTM D4208

SW 846 6010B

SW 846 6010B

ASTM D3761

SW 846 6010B

SW 846 6010B

EPA 7473

SW 846 6010B

SW 846 7740
EIA Facility Code Facility Name Boiler ID

7213 Clover 1

Sample Number (minimum 

of 3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value 

(HHV)

(as received)

Unit 1 PM/MTL-1 3/29/2010 3/29/2010 12711.00

Unit 1 Run 1 PM/MTL-2 3/30/2010 3/30/2010 12636.00

Unit 1 Run 2 PM/MTL-3 3/30/2010 3/30/2010 12378.00

 Fuel Testing Results
HAPs Test Group

Mercury and non‐mercury metalic HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 5.78 9.57 1.01 13500

Btu/lb 5.97 9.67 1.69 13400

Btu/lb 7.4 9.52 1.26 13400
HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Btu/lb 10.15 1.07 1849 ppm 0.077 PPM

Btu/lb 10.28 1.79 1111 ppm 0.14 PPM

Btu/lb 10.28 1.36 1431 ppm 0.109 PPM
Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

1.06 PPM 6.71 PPM < 5.00 PPM < 1.00 PPM 21.1

1.17 PPM 27.3 PPM < 5.00 PPM < 1.00 PPM 19.2

1.25 PPM 13.4 PPM < 5.00 PPM < 1.00 PPM 20
Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

PPM 9.33 PPM 17 PPM 17.6 PPM 3.45 PPM

PPM 10.9 PPM 19.9 PPM 15.8 PPM 2.86 PPM

PPM 9.21 PPM 22.1 PPM 16.1 PPM 4.36 PPM
Note the Proximate/Ultimate data below

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon

68.6 ppm 10.5 PPM 5 10.15

59.5 ppm 9.81 PPM 5.3 10.28

103 ppm 9.55 PPM 6.65 10.28

Proximate Analyses, % by wt
w should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

79.55 5.34 1.43 1.07 2.45

78.56 5.34 1.37 1.79 2.66

79.04 5.41 1.35 1.36 2.55

Ultimate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID

7213 Clover 1

Sample Number (minimum of 

3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received)

Unit 1 Run 1 NDF/AG-1 4/2/2010 4/2/2010 12840.00

Unit 1 Run 2 NDF/AG-1 4/2/2010 4/2/2010 12617.00

Unit 1 Run 1 NDF/AG-2 4/3/2010 4/3/2010 12736.00

Unit 1 Run 1 NDF/AG-3 4/3/2010 4/3/2010 12980.00

 Fuel Testing Results
HAPs Test Group

Acid gas HAPs

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 3.99 9.73 1.06 13400

Btu/lb 3.92 9.44 0.91 13100

Btu/lb 3.87 9.42 0.92 13200

Btu/lb 3.39 8.97 0.83 13400
HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Btu/lb 10.13 1.1 1690 ppm 0.081 PPM

Btu/lb 9.83 0.95 1834 ppm 0.049 PPM

Btu/lb 9.8 0.96 1586 ppm 0.063 PPM

Btu/lb 9.28 0.86 1759 ppm 0.04 PPM
Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

5.79 PPM 5.79 PPM < 5.00 PPM < 1.00 PPM 25.9 PPM

1.96 PPM 3.79 PPM < 5.00 PPM < 1.00 PPM 25.4 PPM

1.58 PPM 3.92 PPM < 5.00 PPM < 1.00 PPM 24.6 PPM

1.2 PPM 3.14 PPM < 5.00 PPM < 1.00 PPM 19.6 PPM
Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

10.8 PPM 9.21 PPM 25.3 PPM 1.8 PPM 61 ppm

10.6 PPM 7.59 PPM 22.1 PPM 3.57 PPM 55.4 ppm

6.95 PPM 11.9 PPM 21.8 PPM 3.49 PPM 54.6 ppm

9.49 PPM 6.85 PPM 16.1 PPM 3.37 PPM 53 ppm
Note the Proximate/Ultimate data below should be rec

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen

14.9 PPM 3 10.13 77.29 5.23

12.9 PPM 2.85 9.83 77.05 5.27

11.6 PPM 2.85 9.8 77.82 5.23

10.7 PPM 2.4 9.28 78.69 5.26

Proximate Analyses, % by wt Ultim
corded on a dry basis (including ash).

Nitrogen Total Sulfur Oxygen

1.48 1.1 4.77

1.47 0.95 5.44

1.41 0.96 4.77

1.42 0.86 4.48

mate Analyses, % by wt
EIA Facility Code Facility Name Boiler ID

7213 Clover 1

 Fuel Testing Results

Sample Number (minimum of 

3 composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received)

Unit 1 Run 1 NDF/AG-1 4/2/2010 4/2/2010 12840.00

Unit 1 Run 2 NDF/AG-1 4/2/2010 4/2/2010 12617.00

Unit 1 Run 1 NDF/AG-2 4/3/2010 4/3/2010 12736.00

Unit 1 Run 1 NDF/AG-3 4/3/2010 4/3/2010 12980.00
HAPs Test Group

Non‐dioxin/furan organic HAPs

Higher 

HHV Units

% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Heating 

Value (HHV)

(Dry Basis)

Btu/lb 3.99 9.73 1.06 13400

Btu/lb 3.92 9.44 0.91 13100

Btu/lb 3.87 9.42 0.92 13200

Btu/lb 3.39 8.97 0.83 13400
HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Btu/lb 10.13 1.1 1690 ppm 0.081 PPM

Btu/lb 9.83 0.95 1834 ppm 0.049 PPM

Btu/lb 9.8 0.96 1586 ppm 0.063 PPM

Btu/lb 9.28 0.86 1759 ppm 0.04 PPM
Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

5.79 PPM 5.79 PPM < 5.00 PPM < 1.00 PPM 25.9 PPM

1.96 PPM 3.79 PPM < 5.00 PPM < 1.00 PPM 25.4 PPM

1.58 PPM 3.92 PPM < 5.00 PPM < 1.00 PPM 24.6 PPM

1.2 PPM 3.14 PPM < 5.00 PPM < 1.00 PPM 19.6 PPM
Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

10.8 PPM 9.21 PPM 25.3 PPM 1.8 PPM 61 ppm

10.6 PPM 7.59 PPM 22.1 PPM 3.57 PPM 55.4 ppm

6.95 PPM 11.9 PPM 21.8 PPM 3.49 PPM 54.6 ppm

9.49 PPM 6.85 PPM 16.1 PPM 3.37 PPM 53 ppm
Note the Proximate/Ultimate data below should be rec

Proximate Analyses, % by wt Ultim

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen

14.9 PPM 3 10.13 77.29 5.23

12.9 PPM 2.85 9.83 77.05 5.27

11.6 PPM 2.85 9.8 77.82 5.23

10.7 PPM 2.4 9.28 78.69 5.26
corded on a dry basis (including ash).

mate Analyses, % by wt

Nitrogen Total Sulfur Oxygen

1.48 1.1 4.77

1.47 0.95 5.44

1.41 0.96 4.77

1.42 0.86 4.48
EIA Facility Code Facility Name Boiler ID HAPs Test Group

7213 Clover 1

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

 Fuel Testing Results
% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury 

(Dry Basis)

Mercury 

Units

Antimony 

(Dry Basis)

Antimony 

Units

Arsenic (Dry 

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units
Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry 

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry 

Basis) Nickel Units
Note the Proximate/U

Selenium 

(Dry Basis)

Selenium 

Units

Fluorine 

(Dry Basis)

Fluorine 

Units

Cobalt (Dry 

Basis) Cobalt Units Total Moisture Volatiles Ash

Proximate Analyses, % by w
ltimate data below should be recorded on a dry basis (including ash).

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

wt Ultimate Analyses, % by wt
Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

PPM
re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm