### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

-
5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date

54634 St. Nicholas Cogen Unit ID 1 4/15/2010Fuel Type 1 Fuel Type 2 Fuel Type 3

coal refuse (culm or gob)Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

54634 St. Nicholas Cogen Unit ID 1 As Received Higher Heating Value 54634 St. Nicholas Cogen Unit ID 1 As Received % Moisture 54634 St. Nicholas Cogen Unit ID 1 As Received % Ash 54634 St. Nicholas Cogen Unit ID 1 As Received % Sulfur 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Higher Heating Value 54634 St. Nicholas Cogen Unit ID 1 Dry

basis % Moisture 54634 St. Nicholas Cogen Unit ID 1 Dry

basis % Ash 54634 St. Nicholas Cogen Unit ID 1 Dry

basis % Sulfur 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Antim ony 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Arsenic 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Beryllium 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Cadmium 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Chlorine 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Chromium 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Cobalt 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Fluorine 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Lead 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Manganese 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Mercury 54634 St. Nicholas Cogen Unit ID 1 Dry

basis Nickel 54634 St. Nicholas Cogen Unit ID 1 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D5142 ASTM D5142 ASTM D4239 ASTM D5865 ASTM D5142 ASTM D5142 ASTM D4239EIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 54634 St. Nicholas Cogen Unit ID 1 M0011, M18, M25A, M10

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 1 4/15/2010 4039.00 Btu/lb 6.28 2 4/15/2010 3810.00 Btu/lb 6.64 3 4/15/2010 3788.00 Btu/lb 7.30 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 62.65 0.48 4310 Btu/lb 66.85 0.51 63.68 0.47 4081 Btu/lb 68.21 0.50 62.76 0.5 4087 Btu/lb 67.71 0.54Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm