## 13339 Hagers Ferry Road Huntersville, NC 28078-7929 McGuire Nuclear Complex - MG03A2 Phone: 980-875-5245 Fax: 980-875-4349 

# Order Summary Report

Analytical Laboratory

Order Number: J10090177

Lab Contact: Jason C Perkins 

## Date: 11/18/2010 Customer Address: 253 Plant Allen Road Customer Name(s): Don Scruggs, Robbin Jolly, Ray Lidke, Bill Kennedy

Belmont, NC 28012

Phone: 980-875-5348 Report Authorized By: (Signature)


## Program Comments: Allen Test Burn #1 - October 5 Data Flags & Calculations: Any analytical tests or individual analytes within a test flagged with an "X" or "1" indicate a deviation from the method quality system or quality control requirement. All results are reported on a dry weight basis unless otherwise noted. Data Package: This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report isavailable upon request. This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions.The order of individual sections within this report is as follows: Job Summary Report, Sample Identification,Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC) Certification: The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina (DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods. The results in this report meet NELAP requirements throughNew York State Department of Health Certification # 11717. Certified parameters are designated with an "N" in the analytical report.

## Sample ID's & Descriptions: Sample ID Plant/Station Collection Date and Time Collected By Sample Description 2010009141 ALLEN 05-Oct-10 8:30 AM Chris Greene FGD Purge Eff 2010009143 ALLEN 05-Oct-10 8:35 AM Jeff Womack EQ Tank Eff 2010009144 ALLEN 05-Oct-10 8:39 AM Jeremy D. BioReactor 1 Inf 2010009145 ALLEN 05-Oct-10 8:48 AM Jeff Womack BioReactor 2 Inf 2010009146 ALLEN 05-Oct-10 8:38 AM Jeff Womack BioReactor 2 Eff 2010009147 ALLEN 30-Sep-10 10:50 AM L. Davis Filter Blk 2010009148 ALLEN 30-Sep-10 10:50 AM L. Davis Metals Trip Blank 7 Total Samples

### COC and .pdf report are in agreement with sample totals and analyses (compliance programs and procedures). All Results are less than the laboratory reporting limits. All laboratory QA/QC requirements are acceptable. The Vendor Laboratories have been qualified by the Analytical Laboratory Yes No 

# Technical Validation Review Checklist:

Yes No
Yes No



## Report Sections Included: Job Summary Report Sub-contracted Laboratory Results Sample Identification Customer Specific Data Sheets, Reports, & Documentation Technical Validation of Data Package Customer Database Entries Analytical Laboratory Certificate of Analysis Test Case Narratives Analytical Laboratory QC Report Chain of Custody

Reviewed By:

### Jenny A Herman Date:

### 11/18/2010Yes

Electronic Data Deliverable (EDD) Sent Separately

# Certificate of Laboratory Analysis This re port shall not be re produced, exce pt in full. 

## Order # J10090177

2010009141 Collection Date: 05-Oct-10 8:30 AM 

### Site: FGD Purge Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst MERCURY (COLD VAPOR) IN WATER Mercury (Hg) 35.4 ug/L EPA 245.1 18-Oct-10 10:35 N 2.5 TLINN TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 96.6 mg/L SW 6010 18-Oct-10 11:59 N 0.05 MHH7131 Barium (Ba) 1.10 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131 Beryllium (Be) 0.015 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131 Boron (B) 107 mg/L SW 6010 18-Oct-10 11:59 N 0.5 MHH7131 Calcium (Ca) 2120 mg/L SW 6010 18-Oct-10 11:59 N 0.1 MHH7131 Cobalt (Co) 0.087 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131 Iron (Fe) 106 mg/L SW 6010 18-Oct-10 11:59 N 0.1 MHH7131 Magnesium (Mg) 861 mg/L SW 6010 18-Oct-10 11:59 N 0.05 MHH7131 Manganese (Mn) 3.86 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131 Molybdenum (Mo) 0.027 mg/L SW 6010 18-Oct-10 11:59 0.005 MHH7131 Sodium (Na) 43.2 mg/L SW 6010 18-Oct-10 11:59 N 0.05 MHH7131 Tin (Sn) < 0.05mg/L SW 6010 18-Oct-10 11:59 N 0.05 MHH7131 Titanium (Ti) 2.15 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131 Zinc (Zn) 0.447 mg/L SW 6010 18-Oct-10 11:59 N 0.005 MHH7131 DISSOLVED METALS BY ICP-MS Selenium (Se) 978 ug/L EPA 200.8 19-Oct-10 12:17 N 5 KRICHAR TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) 10.7 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Arsenic (As) 162 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Cadmium (Cd) < 10 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Chromium (Cr) 151 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Copper (Cu) 172 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Lead (Pb) 135 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Nickel (Ni) 281 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Selenium (Se) 1320 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Silver (Ag) < 10 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Thallium (Tl) < 10 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Vanadium (V) 168 ug/L EPA 200.8 28-Oct-10 11:10 N 10 KRICHAR Zinc (Zn) 384 ug/L EPA 200.8 28-Oct-10 11:10 N 20 KRICHAR TOTAL DISSOLVED SOLIDS Vendor Parameter Complete V_PRISM

# Certificate of Laboratory Analysis This re port shall not be re produced, exce pt in full. 

## Order # J10090177

2010009143 Collection Date: 05-Oct-10 8:35 AM 

### Site: EQ Tank Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst MERCURY (COLD VAPOR) IN WATER Mercury (Hg) 16.4 ug/L EPA 245.1 18-Oct-10 10:37 N 2.5 TLINN TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 41.0 mg/L SW 6010 18-Oct-10 12:03 N 0.05 MHH7131 Barium (Ba) 0.642 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131 Beryllium (Be) 0.006 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131 Boron (B) 82.8 mg/L SW 6010 18-Oct-10 12:03 N 0.05 MHH7131 Calcium (Ca) 2030 mg/L SW 6010 18-Oct-10 12:03 N 0.1 MHH7131 Cobalt (Co) 0.038 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131 Iron (Fe) 41.6 mg/L SW 6010 18-Oct-10 12:03 N 0.01 MHH7131 Magnesium (Mg) 78.7 mg/L SW 6010 18-Oct-10 12:03 N 0.05 MHH7131 Manganese (Mn) 1.76 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131 Molybdenum (Mo) 0.018 mg/L SW 6010 18-Oct-10 12:03 0.005 MHH7131 Sodium (Na) 39.1 mg/L SW 6010 18-Oct-10 12:03 N 0.5 MHH7131 Tin (Sn) < 0.05mg/L SW 6010 18-Oct-10 12:03 N 0.05 MHH7131 Titanium (Ti) 1.10 mg/L SW 6010 18-Oct-10 12:03 N 0.005 MHH7131 DISSOLVED METALS BY ICP-MS Selenium (Se) 596 ug/L EPA 200.8 19-Oct-10 12:21 N 5 KRICHAR TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 10 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Arsenic (As) 75.9 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Cadmium (Cd) < 10 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Chromium (Cr) 65.7 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Copper (Cu) 65.8 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Lead (Pb) 62.6 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Nickel (Ni) 114 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Selenium (Se) 870 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Silver (Ag) < 10 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Thallium (Tl) < 10 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Vanadium (V) 72.2 ug/L EPA 200.8 28-Oct-10 11:21 N 10 KRICHAR Zinc (Zn) 145 ug/L EPA 200.8 28-Oct-10 11:21 N 20 KRICHAR 

### 2010009144 Collection Date: 05-Oct-10 8:39 AM 

### Site: BioReactor 1 Inf Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 0.011 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131 Barium (Ba) 0.186 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131 Beryllium (Be) < 0.005mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131

# Certificate of Laboratory Analysis This re port shall not be re produced, exce pt in full. 

## Order # J10090177

Boron (B) 72.2 mg/L SW 6010 18-Oct-10 12:07 N 0.5 MHH7131 Calcium (Ca) 1830 mg/L SW 6010 18-Oct-10 12:07 N 0.1 MHH7131 Cobalt (Co) < 0.005mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131 Iron (Fe) < 0.01 mg/L SW 6010 18-Oct-10 12:07 N 0.01 MHH7131 Magnesium (Mg) 743 mg/L SW 6010 18-Oct-10 12:07 N 0.05 MHH7131 Manganese (Mn) 0.210 mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131 Molybdenum (Mo) 0.008 mg/L SW 6010 18-Oct-10 12:07 0.005 MHH7131 Sodium (Na) 37.1 mg/L SW 6010 18-Oct-10 12:07 N 0.5 MHH7131 Tin (Sn) < 0.05 mg/L SW 6010 18-Oct-10 12:07 N 0.05 MHH7131 Titanium (Ti) < 0.005mg/L SW 6010 18-Oct-10 12:07 N 0.005 MHH7131 DISSOLVED METALS BY ICP-MS Selenium (Se) 495 ug/L EPA 200.8 19-Oct-10 12:24 N 5 KRICHAR TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Arsenic (As) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Cadmium (Cd) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Chromium (Cr) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Copper (Cu) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Lead (Pb) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Nickel (Ni) 13.9 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Selenium (Se) 666 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Silver (Ag) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Thallium (Tl) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Vanadium (V) < 10 ug/L EPA 200.8 27-Oct-10 15:27 N 10 KRICHAR Zinc (Zn) < 20 ug/L EPA 200.8 27-Oct-10 15:27 N 20 KRICHAR 

### 2010009145 Collection Date: 05-Oct-10 8:48 AM 

### Site: BioReactor 2 Inf Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 0.066 mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131 Barium (Ba) 0.196 mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131 Beryllium (Be) < 0.005mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131 Boron (B) 70.4 mg/L SW 6010 18-Oct-10 12:11 N 0.5 MHH7131 Calcium (Ca) 1920 mg/L SW 6010 18-Oct-10 12:11 N 0.1 MHH7131 Cobalt (Co) < 0.005mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131 Iron (Fe) 0.209 mg/L SW 6010 18-Oct-10 12:11 N 0.01 MHH7131 Magnesium (Mg) 745 mg/L SW 6010 18-Oct-10 12:11 N 0.05 MHH7131 Manganese (Mn) 0.374 mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131 Molybdenum (Mo) 0.022 mg/L SW 6010 18-Oct-10 12:11 0.005 MHH7131 Sodium (Na) 37.3 mg/L SW 6010 18-Oct-10 12:11 N 0.5 MHH7131 Tin (Sn) < 0.05mg/L SW 6010 18-Oct-10 12:11 N 0.05 MHH7131 Titanium (Ti) < 0.005mg/L SW 6010 18-Oct-10 12:11 N 0.005 MHH7131 TOTAL RECOVERABLE METALS BY ICP-MS

# Certificate of Laboratory Analysis This re port shall not be re produced, exce pt in full. 

## Order # J10090177

Antimony (Sb) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Arsenic (As) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Cadmium (Cd) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Chromium (Cr) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Copper (Cu) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Lead (Pb) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Nickel (Ni) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Selenium (Se) 92.3 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Silver (Ag) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Thallium (Tl) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Vanadium (V) < 10 ug/L EPA 200.8 27-Oct-10 15:32 N 10 KRICHAR Zinc (Zn) 53.9 ug/L EPA 200.8 27-Oct-10 15:32 N 20 KRICHAR 

### 2010009146 Collection Date: 05-Oct-10 8:38 AM 

### Site: BioReactor 2 Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst MERCURY (COLD VAPOR) IN WATER Mercury (Hg) < 1 ug/L EPA 245.1 18-Oct-10 10:40 N 1 TLINN TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 0.040 mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131 Barium (Ba) 0.216 mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131 Beryllium (Be) < 0.005mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131 Boron (B) 74.9 mg/L SW 6010 18-Oct-10 11:55 N 0.5 MHH7131 Calcium (Ca) 1960 mg/L SW 6010 18-Oct-10 11:55 N 0.1 MHH7131 Cobalt (Co) < 0.005mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131 Iron (Fe) 0.523 mg/L SW 6010 18-Oct-10 11:55 N 0.01 MHH7131 Magnesium (Mg) 736 mg/L SW 6010 18-Oct-10 11:55 N 0.05 MHH7131 Manganese (Mn) 0.465 mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131 Molybdenum (Mo) 0.028 mg/L SW 6010 18-Oct-10 11:55 0.005 MHH7131 Sodium (Na) 36.6 mg/L SW 6010 18-Oct-10 11:55 N 0.5 MHH7131 Tin (Sn) < 0.05mg/L SW 6010 18-Oct-10 11:55 N 0.05 MHH7131 Titanium (Ti) < 0.005mg/L SW 6010 18-Oct-10 11:55 N 0.005 MHH7131 TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Arsenic (As) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Cadmium (Cd) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Chromium (Cr) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Copper (Cu) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Lead (Pb) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Nickel (Ni) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Selenium (Se) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Silver (Ag) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Thallium (Tl) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Vanadium (V) < 5 ug/L EPA 200.8 27-Oct-10 15:00 N 5 KRICHAR Zinc (Zn) < 10 ug/L EPA 200.8 27-Oct-10 15:00 N 10 KRICHAR

# Certificate of Laboratory Analysis This re port shall not be re produced, exce pt in full. 

## Order # J10090177

2010009147 Collection Date: 30-Sep-10 10:50 AM 

### Site: Filter Blk Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst DISSOLVED METALS BY ICP-MS Selenium (Se) < 1 ug/L EPA 200.8 19-Oct-10 12:28 N 1 KRICHAR 

### 2010009148 Collection Date: 30-Sep-10 10:50 AM 

### Site: Metals Trip Blank Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

### Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 Barium (Ba) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 Beryllium (Be) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 Boron (B) < 0.05 mg/L SW 6010 18-Oct-10 11:15 N 0.05 MHH7131 Calcium (Ca) < 0.01 mg/L SW 6010 18-Oct-10 11:15 N 0.01 MHH7131 Cobalt (Co) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 Iron (Fe) < 0.01 mg/L SW 6010 18-Oct-10 11:15 N 0.01 MHH7131 Magnesium (Mg) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 Manganese (Mn) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 Molybdenum (Mo) < 0.005mg/L SW 6010 18-Oct-10 11:15 0.005 MHH7131 Sodium (Na) < 0.05 mg/L SW 6010 18-Oct-10 11:15 N 0.05 MHH7131 Tin (Sn) < 0.05 mg/L SW 6010 18-Oct-10 11:15 N 0.05 MHH7131 Titanium (Ti) < 0.005mg/L SW 6010 18-Oct-10 11:15 N 0.005 MHH7131 TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Arsenic (As) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Cadmium (Cd) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Chromium (Cr) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Copper (Cu) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Lead (Pb) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Nickel (Ni) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Selenium (Se) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Silver (Ag) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Thallium (Tl) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Vanadium (V) < 1 ug/L EPA 200.8 27-Oct-10 15:37 N 1 KRICHAR Zinc (Zn) 3.00 ug/L EPA 200.8 27-Oct-10 15:37 N 2 KRICHAR

### This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert No. 37735 

# Case Narrative 11/17/2010

Duke Energy Corporation Jay Perkins 13339 Hagers Ferry Road Huntersville, NC 28078 Project: Allen - FGD Alternative Fuels Test Burn #1 Daily Project No.: J10090177 Lab Submittal Date: 10/06/2010 Prism Work Order: 0100197

This is a Revised Report and supercedes the original laboratory report dated 10/13/10. Client Sample ID were revised at the request of the client. 

## Narrative Notes:

Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC.



### VP Laboratory Services Reviewed By

Data Qualifiers Key Reference:



### Method Detection Limit MDL Below Reporting Limit BRL
Relative Percent Difference RPD


## * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J.

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 1 of 6

# Sample Receipt Summary 11/17/2010 

## Prism Work Order: 0100197 Client Sample ID Matrix Lab Sample ID Date Sampled Date Received 

### 0100197-01 10/05/10 2010009141/FGD Purge Eff 10/06/10 Water Samples received in good condition at 1.5 degrees C unless otherwise noted.

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 2 of 6

# Laboratory Report 11/17/2010

Result Parameter Batch ID Report Limit Analysis Date/Time Method Dilution Factor Units MDL Analyst 

### 13339 Hagers Ferry Road Project No.: J10090177 Project: Allen - FGD Alternative Fuels Test Burn #1 Daily Duke Energy Corporation
Huntersville, NC 28078 Attn: Jay Perkins Sample Matrix: Water Client Sample ID: 2010009141/FGD Purge E Prism Sample ID: 0100197-01 Prism Work Order: 0100197 Time Collected: 10/05/10 08:30 Time Submitted: 10/06/10 16:25

General Chemistry Parameters 8800 *SM2540 C P0J0158 1 50 10/7/10 13:25JAB mg/L 8.7 Total Dissolved Solids

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 3 of 6

### 11/17/10 

## Level II QC Report

13339 Hagers Ferry Road Project No: J10090177 Project: Allen - FGD Alternative Fuels Test Burn #1 Daily Duke Energy Corporation
Huntersville, NC 28078 Attn: Jay Perkins Prism Work Order: 0100197 Time Submitted: 10/6/10 4:25:00PM

Result Limit

ReportingUnits Level SpikeResult

Source%REC%REC LimitsRPDRPD Limit Notes Analyte General Chemistry Parameters - Quality Control



### Batch P0J0158 - NO PREP Blank (P0J0158-BLK1) 

### Prepared & Analyzed: 10/07/10 Total Dissolved Solids mg/L BRL 50 LCS (P0J0158-BS1) 

### Prepared & Analyzed: 10/07/10 Total Dissolved Solids mg/L 972 50 1000 90-110 97 Duplicate (P0J0158-DUP1) 

### Prepared & Analyzed: 10/07/10 Source: 0100197-01 Total Dissolved Solids mg/L 8930 50 8800 20 2


### Sample Extraction Data
NO PREP Lab Number Batch Date Initial Final P0J0158 0100197-01 10/07/10 50 50 mL mL

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 4 of 6

## Page 5 of 6

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