Exhaust Emissions Sampling 

Dal-Italia, Muskogee, OK 

Kiln Scrubber Exhaust 

May 3, 2006 

Armstrong Environmental, Inc. 

Project W-2498-06 

Report Prepared For: 

Bob Hurt 

Daltile 

7834 C. F. Hawn Freeway 

Dallas, TX 75217 

Report Prepared May 22, 2006 By: 

Arnzstrong Environmental, Inc. 

7715 Sovereign Row 

Dallas, Texas 75247 

(214) 631-0021 
TABLE OF CONTENTS 

Page 

1. Yntroduction 1 

H. Summary 2-3 

III. Procedures 4-5 

I'V. Appendices 

A. Caiculation Summaries 6-8 

B. Analytical Summaries 9- 14 

C. Field Data Sheets 15 - l.8 

D. Equipment Calibrations 19 - 25 
1. INTRODUCTION 

A series of tests was perfoizned on the exhaust associated with the Kiln Scrubber at the 

Dal-Italia facility in Muskogee, OK on May 3, 2006. 

The purpose of this test series was to deterrnine the exhaust einission rate of particulate in 

terms of lbslhr. 

Testing followed procedures detailed in Title 40: Code of FederaI Regulations (40:CFR). 

Sampling was perforrned by Richard Taylor, Gilbert Salinas and Tom Armstrong of 

Armstrong Environmental, Inc. using an Apex Method 5 sampling train. 

Three one hour test repetitions were perforrned according to the following schedule: 

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5I3/06 8:25 AM .2:07 PM 

Submitted by: 
IL SUMMARY 

A series of tests was performed on the exhatist associated with the Kiln Scnibber at the 

Dal-Italia facility in Muskogee, OK on May 3, 2006. 

Sampling was perfon-ned -followiiig procedures detailed -in Title 40: Code of Federal 

Regulations. 

Results of this test series are summarized in Table 1. 

Results indicate the following particulate emission rates: 

i"IX 

A 

5/3/06 Exhaust, lbs/hr 3.371 3.470 2.905 3.249 

Sampling was interrupted for approximately 95 minutes during Run #3 on 5/3/06. 

2 
SUMMARY OF EMISSIONS TEST DATA 

Table : 1 

Plant : Dal-Italia, Muskogee, OK 

Location : Kiln Scrubber Exhaust 

Operator : R. Taylor 

Test Date : 3-May-06 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 137.7 138.1 138.1 

Velocity, fps 29.12 29.31 29.18 

Volume Flow, acfm 33737.6 33958.9 33805.1 

scfm 23899.3 24072.5 23989.6 

scfh 1433955 1444349 1439374 

Moisture, % 18.63% 18.52°'Jo 18.43% 

CO2, % 2.50 2.50 3.00 

02, % 18.00 18.00 18.00 

SAMPLE 

Start Time, hrs:min 8:25 AM 9:55 AM 11:30 AM 

Finish Time, hrs:min 9:27 AM 10:27 AM 2:05 PM 

Sample Volume, scf 38.059 38.275 37.965 

Isokinetic Ratio, % 101.5394 101.3814 100.9073 

PARTICULATE 

~_ 

ront Ha ~l 

Samp e eight, mg 38.64 36.11 29.75 

Concentration, gr/scf 0.015665 0.014557 0.012091 

Emissions, Ibs/hr 3.210118 3.004605 2.487039 

Back Half 

Sample Weight, mg 1.94 5.59 5.00 

Concentration, gr/scf 0.000787 0.002253 0.002032 

Emissions, Ibs/hr 0.161171 0.465127 0.41799 

Total Particulate, Ibs/hr 3.371288 3.469732 2.905029 

3 
III. PROCEDURES 

The procedure for emissions sampling followed USEPA test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method Title 

1 Sample arnd Velocity Traverses for Stationary Sources 

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

3 Gas Analysis for the Determination of Dry Molecular Weight 

5 Determination of Particulate Emissions from Stationary Sources 

202 Determination of Condensible Particulate Emissions from Stationary 

Sources 

02 and CO2 were determined using FyRite Analyzers. 

PM sampling was performed on the scrubber exhaust for 3 minutes at each of 20 points, 

10 points per traverse, making a total run duration of 60 minutes. A schematic of the 

sampling location is shown in Figure 1. The sampling train was configured as follows: 

Stainless Steel Sampling Nozzle 

Heated Glass Lined Probe 

Heated glass fiber filter 

Impinger #1 - 100 mis H20 

Impinger #2 - 100 mis H20 

Impinger 43 - 100 mis H20 

Impinger #4 - Empty 

Impinger #5 - 200 grams silica Gel 

C! 
Figure I- Kiln Scrubber Exhuast 

Ln 

StcLl, Diemeter - 59.5 inclhes 

Roint #1 -1.S inci'ies 

Point #2 - 4.9 incliesPoint #3 = 3.7 inches 

Point #4 - 13.4 inclies 

Point #S - 20.3 Inches 

f'oint #6 - 39.1 inches 

Poiilt #7 - 46.1 inches 

Point M3 - 50.6 in t,,hes 

Point #9 - 511.6 inclies 

Point #10 - -56 inchps 
Appendix A : 
EMISStON TEST SUMMARY 

PLANT : Dal•Italia. Muskogee. 0K 

DATE : 3-May-06 

PLACE : Kiln Scruhber Exhaiust 

RUN#: 1 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 185.1 

NOZZLE DiAMETER (INCH.) : 0.3043 PARTICULATE WEIGHT (Front hall rng) : 38.64 

METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Back hali mg) : 1.94 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (En. H20) : •0.2 

uAS METER VOL.(Cu.Ft.) : 39.8 PERCENT CO2 2.5 

BAROMETRIC PRESSURE 29.5 PERCENT 02 18 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (leet): 0.000505 STACK AREA (Sq.FI.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 3B.0593 

VOLUME OF WATER VAPOR (STD. CU.FT.): 8.7127 

FRACTIONAL MOiSTURE CONTENT (QJo): 0.1863 

DRY BASE: 79.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.0486 

STACK PRESSURE (inch Hg): 29.4853 

STACK GAS VELOCITY (ft/sec.}: 29.1207 

ACTUAL STACK GAS FLOW RATE (ACFM): 33737.6354 

STANDARD STACK GAS FLOW RATE (SCFH): 1433955.26 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0157 

PARTICULATE CONCENTRATION (LBS/SCF): 2.24E-06 

PARTICULATE EMISSION (LBS/HR): 3.2101 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0,0008 

PARTICULATE CONCENTRATION (LBS/SCF): 1.12E-07 

PARTICULATE EMISSION (LBS/HR): 0.1612 

ISOKINETIC RATIO (%): 101.5394 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 137 0.22 0.469042 1.10 77 77 

2 138 0.20 0.447214 1.00 82 77 

3 138 0.22 0.469042 1.10 84 78 

4 138 0.22 0.469042 1.10 86 79 

5 138 0.25 0.5 1.25 88 80 

6 138 0.25 0.5 1.25 90 81 

7 138 0.23 0.479583 1.20 92 81 

8 138 0.23 0.479583 1.20 92 82 - 

9 137 0.21 0.458258 1.10 92 82 

10 137 0.15 0.387298 0.75 92 82 

11 137 0.24 0.489898 1.20 85 83 

12 138 0.25 0.5 1.30 92 84 

13 137 0.26 0.509902 1.30 92 84 

14 137 0.25 0.5 1.20 93 84 

15 138 0.23 0.479583 1.10 92 84 

16 138 0.22 0.469042 1.10 52 35 

17 138 0.23 0.479583 1.10 91 85 

18 138 0.21 0.458258 1,00 91 85 

19 138 0.19 0.43589 0.94 90 85 

20 138 0.15 0.387298 0.74 91 85 

137.7 0.4684 1.1015 89.2000 82.1500 85.6750 

R 
EMISSION TEST SUMMARY 

PLANT : aal•Italia. Masl<o;ee. OK 

DATE : 3-May-06 

PLACE : Y.iln ScrubGer Exhaust 

RUN#: 2 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 184.8 

NOZZLE DIAMETER (INCH.) : 0.3043 PARTICULATE WEIGHT (Front half mg) : 36.11 

METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Back half mg) : 5.59 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.2 

GAS METER VOL.(Cu.Ft.) : 39.989 PERCENT CO2 2.5 

BAROMETRIC PRESSURE 29.5 PERCENT 02 18 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inches) : 

NOZZLE AREA (teet): 0.000505 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 38.2755 

VOLUME OF WATER VAPOR (STD. CU .FT.): 8.6985 

FRACTIONAL MOISTURE CONTENT (qo): 0.1852 

DRY BASE: 79.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT, OF STACK GAS (WET BASE): 27.0608 

STACK PRESSURE (inch Hg): 29.4853 

STACK GAS VELOCITY (ft/sec.): 29.3117 

ACTUAL STACK GAS FLOW RATE (ACFM): 33958.9176 

STANDARD STACK GAS FLOW RATE (SCFH): 1444348.7 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0146 

PARTICULATE CONCENTRATION (LBS/SCF): 2.08E-06 

PARTICULATE EMISSION (LBS/HR): 3.0046 

BACK HALF ~ 

PARTICULATE CONCENTRATION (GR./SCF): 0.0023 

PARTICULATE CONCENTRATION (LBS/SCF): 3.22E•07 

PARTICULATE EMISSION (LBS/HR): 0.4651 

ISOKINETIC RATIO (%): 101.3814 

POINTS STACK T. DELTA P SQUAR O.P DELTA H METER T. METER T. 

deg F INLET OUTLET 

1 138 0.19 0.43589 0.94 82 82 

2 139 0.20 0.447214 0.99 84 82 

3 138 0.23 0.479583 1.10 88 82 

4 138 0.21 0.458258 1.00 86 82 

5 138 0.23 0.479583 1.10 86 82 

6 138 0.23 0.479583 1.10 87 82 

7 138 0.22 0.469042 1.10 87 82 

8 138 0.23 0.479583 1.10 88 82 

9 138 0.23 0.479583 1.10 88 82 

10 138 0.20 0.447214 0.99 88 82 

11 13!9 0.24 0.489898 1.20 85 82 

12 138 0.23 0.479583 1.10 90 83 

13 138 0.25 0.5 1.20 90 83 

14 138 0.26 0.509902 1.30 90 83 

15 138 0.27 0.519615 1.30 90 83 

16 138 0.24 0.489898 1.20 90 83 

17 138 0.23 0.479583 1.10 90 83 

18 138 0.22 0.469042 1,10 90 83 

19 138 0.19 0.43589 0.94 89 83 

20 133 0.16 0.4 0.79 89 83 

138.1 0.4714 1.0875 87.8500 82.4500 85.1500 

~''~ 
EM1SSlON TEST SlJMMARY 

PLANT : ual•lialia. i'rSusisol;pe. Ott 

UATE : 3•May•06 

PLACE : Y,itn Scrtihber Exhiust 

RUNi; : 3 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (m1s) : 182.2 

NOZZLE OIAMETER (INCH.) : 0.3043 PARTICULATE WEIGHT (Front hall mg) : 29.75 

METER COEFFICIENT (Y) : 1 PARTICULATE WEIGHT (Sack half mg) : 5 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (fn. H20) : •0.21 

GAS METER VOL.(Cu.Ft.) : 40.03 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.5 PERCENT 02 18 

PERCENT CO . 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 59.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 19.30907 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000505 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 19.30907 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 37.9653 

VOLUME OF WATER VAPOR (STD. CU .FT.): 8.5762 

FRACTIONAL MOISTURE CONTENT (°Jo): 0.1843 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.2000 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.1362 

STACK PRESSURE (inch Hg): 29.4846 

STACK GAS VELOCITY (ft/sec.): 29.1790 

ACTUAL STACK GAS FLOW RA7E (ACFM): 33805.1152 

STANDARD STACK GAS FLOW RATE (SCFH): 1439374.08 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATIOIV (GR./SCF): 0.0121 

PARTICULATE CONCENTRATION (LBS/SCF): 1.73E•06 

PARTICULATE EMISSION (LBS/HR): 2.4870 

BACK HALF 

PARTICULATE CONCENTRATION (GR./SCF): 0.0020 

PARTICULATE CONCENTRATION (LBS/SCF): 2.90F•07 

PARTICULATE EMISSION (LBS/HR): 0.4180 

1SOKINETIC RATIO (%): 100.9073 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. 

deg F 1NLET OUTLET 

1 139 0.22 0.469042 1.10 83 83 

2 ] 39 0.22 0.469042 1.10 86 84 

3 138 0.22 0.469042 1.10 88 84 

4 138 0.23 0.479583 1.10 90 85 

5 138 0.24 0.489898 1.20 92 85 

6 138 0.24 0.489898 1.20 93 86 

7 138 0.22 0.469042 1.10 94 86 

8 138 0.21 0.458258 1.00 94 87 

9 138 0.20 0.447214 0.99 95 87 

10 138 0:15 0.387298 0.75 89 88 

11 138 0,26 0.509902 1.30 90 89 

12 I38 0.26 0.509902 1.30 94 89 

13 138 0.25 0.5 1.30 95 89 

14 138 0.26 0.509902 1.30 95 89 

15 138 0.26 0.509902 1.30 96 29 

16 138 0.24 0.489898 1.20 96 90 

17 138 0.21 0,458258 1.10 96 91 

18 138 0.20 0.447214 1.00 96 91 

19 138 0.19 0.43589 0.97 96 91 

20 138 0.16 0.4 0.81 96 91 

138.1 0.4700 1.1110 92.7000 87.7000 90.2000 

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Time M. 

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FILTER ANALITICAL DATA 

Company: Dal-Italia, Muskogee, OK 

Date: 5/3106 

Location: Kiln Scrubber Exhaust 

Run 1 Run 2 Run 3 

Filter ID Number 

Date of Weighing a~SfQi~: :a~~1.0~ :5f~~4~F'i: 

Time 0~:i~M : 

Gross Filter Wt. 7~:~: 

Date of Weighing 

Time ... M: 

Gross Filter Wt. 

Ave. Gross Filter Wt. 0.3699 0.3712 0.3714 

Date of Weighing 

0

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Time :~,~?:Af~I :~` :.i ~ ~`3... ~. AN[: 

Filter Tare Wt. 

•i 

Date of Weighing :i.I~~~O~ ::~~~1i~6 

Time 

Filter Tare Wt. 

Ave. Filter Tare V1/t. 0.3514 0.3506 0.3511 

Wt. of PM on Filter (grams) 0.0185 0.0206 0.0203 

Total Weight of Particulate (mg) 18.5 20.6 20.3 

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Time 

Time 

Time 

Time 

1 1 
PARTICULATE ANALYTICAL DATA FORM 

Company: Dal•Italia, Muskogee, 0K 

Date: 5/3/06 

Location: Kiln Scrubber Exhaust 

Run 1 Run 2 Run 3 

Density (Pa) 

Blank Concentration (Ca) 

Rinse Volume (Vaw) 

Residue in Rinse (Wa) = Ca•Vaw*Pa 0.0004 0.0004 . 0.0004 

Date of Weighing 

Time 

Gross Weight 

Date of Weighing 

Time p 

Gross Weight i i 55, 89: io 4 - 11 1 

Date of Weighing ...... ~ r 

Time 

Beaker Tare Weight .... . 6,2 

Date of Weighing 6- Q.: 

Time j 2:..M 

Beaker Tare Weight 116.24-2 2, 2. 9 5 

Average Gross Weight 95.0989 116.2479 101.3031 

Less Blank Residue (Wa) 0.0004 0.0004 0.0004 

Average Beaker Tare Weight 95.0968 116.2422 101.2998 

Weight of Particulate in Rinse (mg) 1.68 5.33 2.88 

H20 BLANK ANALYTICAL DATA FORM 

Blank Volume (Va) 

Date of Weighing .. ...... v 

Time 

Gross Weight 

Date of Weighing 

Time 

Gross Weight 

Average Gross Weight 98.22075 

Date of Weighing 

Time 

Tare Weight 

Date of Weighing 

Time 

Tare Weight 

Average Tare Weight 

Weight of Blank (Ma) 

Ca= Ma/(Va"Pa) = g/g 

98.2204 

1.4E•06 

Note: In no case should a blank residue greater than 0.01 i-ng/g or 0.001% of the blank 1.2 

,weight be subtracted from the sample weight. 

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()PERATOR: 

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METER BOX ~: /0 

BAROMETRIC PRESSi7RE: 

AMBrENT TEMPERATURE 7 ~ 

ASSUIOED IviOISTURE f ~ 

PROBE LENGTH: ta 

NOZZLE DLAMETER: - 3 ,t5 13 

! STACK D IAMETER: 57~7. fMETER H: / y 1 4 

C FACTOR: . E q 

METER CO-EF'FICTENT: 

FILTER TARE C,7.351 

PRE-TEST LEAK CHECK.. 

Meter:c5 •ol 5'__cu.ft. @ IS in. HG 

Pitots: .1-. (a ~ -; •~ in. H2O. 

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F I-EL~ 

PL.ANT: ~.,. , .? f; •? •, :,,t.`f _• . 

DATE: ,S~ ~ a~ 

REPETITION: ~ 

LOCATION (SOURCE 

OPERATOR: 

S AMPLE TRAIN 

Iv1ETER BOX k / J - 

BAROMETRIC PRESSURE: 

AMBIENT TEMPERATURE: 7 ~ 

ASSUNIED MOISTURE: 1~ 

PROBE LENGTH: 6 ' 

NOZZLE DLA.METER: 3~ J' 3 

STACK DIAMETER: 

METER H: 1. e-/ f Z 

C FACTOR: - *6 "t 

METER CO-EFFICIENT: 

FII.,TER TARE: - 3`! S:;Z-Y410 

PRE-TEST LEAK CHECK 

Meter: Q r cu.ft. @ ~ S in. HG 

Pitots: "r~ (~a, ~~, ~ in. H20 

i~PI~IGERS 

Initiai Fi.nai 

W 

T.2 

'.`3/ 9' 

P-4 

u~ 

=6 

CO2 02 

o ~ ~ 1 13 

POST-TEST LEAK CHECK 

Meter: 6, o 09 cu.ft. @ in. HG 

Pitots: v (a), ~ '~ in. H20 

I 3 .5q 35o.6cb ql 6 v qq- 72, 3 

f~ . Z - qq 3SL.5° ~`~ ~ Z S~- 6~ ~ 

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PLANT: 

DATE: 

REPETITION: 

LOCATION (SOURCEP): rJViPINGERS 

OPERATOR: iiiitial Fiiial 

SAMPLE TRAIN #r: 

METER BOX 4: / 0 

17 

4. 2 j 

BAROMETRIC PRESSURE: 2~-7, #3 

AN,f BIE-NT TENIPERATURE: ?, Z- -ral 4 

ASSUMED MOISTURE: '77`5 

PROBE LENGTH: or ' 

NOZZLE DLtMETER: , 3,013 

-rr6 

STACK DIAMETER:• --S.' 5— 

METER H: CO2 02 

.CFACTORMETER CO-EFFICIENT 3 8 

FILTER TARE: Q. 

PRE-TEST LEAK CHECK POST-TEST LEAK CH- ECK 

Meter;0.-0,,!VS c .u.ft. @ /5'in. HG - Meter: 0. 005-cu.ft. @ 5- in. HG 

A,_~ , ~rl - Pitots: i-11 A - -.-) -L in. H20 Pitots: (-), "*.fin. iUC) 

r)p (f )/;s7 

37 

13 

.7 

31 

q o 

1 13:33 • q- 11 . o? 1 13,357 13S L q 

Z_ -39 9• q 6 1 

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q51 

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lio ut 6 

q.71 7, 

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FLOW DATA 

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~~~~~~ 

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- ~~~~~ 

~~~~~~. 

~~~~~~. 

~~~_ 

~~~~ 

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PLANT: 

DATE: S% i ~~ 

RUN 44: 

LOCATION (SOURCE rr 

OPERATOR: 

AMBIENT TEMPER-AiXURE:

BAROMETRIC PRESSURE: 2--r-7. ✓ CO2 .02 

ASSUAIED NIOISTURE: 

STACK DIANIETER: S5-7- 

C F.A C T 0 R:, I 

COMMENTS: 
! 
APE Armslrong Environmental Inc. CONVERSION FACTORS 

EPA Method 5 

522 Series Meter Box Calibralion 1 mm Hg : 0.13330 kPa 

Pre-Test Oririce Method 1 cm z 0.39370 lnch 

English Meter Box Units, English K Factor 1 mm = 0.03937 inch 

1 cu ft a 28.32 lilers 

:ter Box i. 10 Dale: ----------- ------------- > 03/15/06 

!rial tt: 30272 Baromelric Pressure: --- -- --- --> 29.95 (in. Hg) 

Theorelical Crilical Vacuum: --- > 14.13 (in. Hg) 

Iill! 

~1 0RTAN For valid tesl resuits, the Aclual Vacuum sliould be 1 to 2 In. Hg greaier lhan the Theoretica) Crilical Vacuum shown above. 

'ORTAN The Critical Orifice Coefficienl. W. musl be entered in English units, (ft) 1,3'(deg R)^0.5/((in.Hg)'(min)). 

!ili! 

---------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGS- 

-- Average Temperatures -- 

Vofunie Volume Volunie Initial Temps. Final Temps. Orifice K' Oritice Acluat -- Ambient Temperalure -- DGM DGM Anibient 

dH Tirzie Inilial Final Total Inlet Outlet Inlel Oullet Sarial# Coefficient Vacuum Initial Flnal Average Outlet Overall Temp 

H20) (r1iin) (cu tt) (cu (t) (cu it) (deg F) (deg F) (deg F) . (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.24 5.00 652.700 654.270 1.570 66.0 65.0 66.0 65.0 40 0.242 23.0 64.0 64.0 64.0 525.0 525.5 524.0 

0.50 5.00 654.600 656.847 2.247 66.0 66.0 66.0 66.0 48 0.344 21.0 63.0 64.0 63.5 526.0 526.0 523.5 

0.93 5.00 657.500 660.520 3.020 66.0 66.0 67.0 66.0 55 0.464 19.5 64.0 64.0 64.0 526.0 526.3 524.0 

1.60 5.00 661.300 665.172 3.872 67.0 66.0 68.0 66,0 63 0.593 18.0 64.0 64.0 64.0 526.0 526.8 524.0 

2.90 5.00 666.000 671.320 5.320 68.0 66.0 71.0 68.0 73 0.824 16.0 64.0 64.0 64.0 527.0 528.3 524.0 

............................................... RESULTS ................................................... 

)RY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER -- --------- ORIFICE ------ 

.UME VOLUME 

ZRECT CORRECTED 

m(std) Vm(std) 

(cu il) (liters) 

1.579 0.1 

2.260 0.1 

3.039 0.'1 

3.899 0.2 

5.359 0.2 

VOLUME VOLUME VOLUME 

CORRECT CORRECT NOMINAL 

Vcr(sld) Vcr(std) Vcr 

(cu fl) (lilers) (cu fl) 

1.585 0.1 1.572 

2.253 0.1 2.233 

3.035 0.1 3.010 

3.882 0.2 ' 3.850 

5.389 0.2 5.345 

Ave ra g e Y ------- > 

CALIBRATION FACTOR 

Y 

Value Varialion 

(number) (number) 

1.004 0.003 

0.997 -0.003 

0:999 -0.002 

0.996 -0.005 

1.006 0.006 

1.000 

CALIBRATION FACTOR 

dH(g? 

Value Variation 

(in H20) (in H20) 

1.352 -0.0635 

1.391 -0.024 

1.427 0.011 

1.500 0.084 

1.408 -0.008 

1.416 <------- Average dH@ 

: For Calibralion Faclor Y, the ralio of the reading of the calibration meter to the dry gas meter, 

rcceptabie tolerance of individual vaiues from ihe average is +-0.02. 

-or Orifice Calibralion Faclor dH@, lhe orifice differential pressure in inches of H201hat equales to 0.75 cfm of air 

it 68 F and 29.92 inches_of Hg, acceptabie olerance of individual yaiues from the average is +-0.2. 

SIGNED: ~/ `-- ' ~-" ti. ` ~J~_~ Date: 

i...s 

~ 
Temperature Meter Calibrations 

Meter Box #: 10, 

Date: 03l15106 

Caiibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 33 32 34 32 32 

Point 2 212 213 212 214 212 212 

Point 3 752 754 752 754 752 752 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxillary 

Point 1 492 ' 493 492 494 492 492 

Point 2 672 673 672 674 672 672 

Point 3 1212 1214 1212 1214 1212 1212 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0.20284 0 0.404858 0 0 

Point 2 0.148588 0 0.296736 0 0 

Point 3 0.164745 0 0.164745 0 0 

2-0 
CALIBRATION FACTOR 

dH arD 

Value Variation 

(in H20) (in H20) 

1.416 0.0013 

1.413 -0.001 

1.415 -0.000 

1.415 <------- Average dH@ 

Armstrong Environmental Inc. CONVERSION FACTORS 

EPA Method 5 

511 Series Meter Box Calibration 1 mm Hg = 0,13330 kPa 

Post-Test Orifice Method 1 cm = 0.39370 inch 

English Meter Box Units, English K' Factor 1 mm = 0.03937 inch 

1 cu ft= 28.32 liters 

er Box 4 10 Date: -----------------------> 05/04106 

ial #: 30272 Barometric Pressure: •----••---> 29.70 (in. Hg) 

Theoretical Critical Vacuum: --- > 14.01 (in. Hg) 

!!! 

'ORTAt\ For valid test results, the Actual Vacuum shouid be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shovan above. 

'ORTAI\ The Critical Orifice Coefficient, K, must be entered In English units, (ft)"3'(deg R)"0.5/((in.Hg)`(min)). 

H! 

------ --------- DRY GAS METER READINGS --------=------- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 14.01 (in. Hg) 

Volume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual - Ambient Temperature - DGM DGM Ambient 

dH Time Initial Final Total Inlet Outlet Inlet Outlet Serial#t Coefficient Vacuum Initial Final Average Outlet Overall Temp 

120) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.91 10.00 435.400 441.533 6.133 75.0 74.0 77.0 76.0 55 0.464 19.5 75.0 77.0 76.0 535.0 535.5 536.0 

0.91 5.00 441.900 444.972 3.072 77.0 77.0 78.0 77.0 55 0.464 19.5 77.0 77.0 77.0 537.0 537.3 537.0 

0.91 5.00 445.200 448.268 3.068 78.0 77.0 79.0 78.0 55 0.464 19.5 78.0 78.0 78.0 537.5 538.0 538.0 

0/4110//t//.f/f////////.//////,/*/f/fR///1////// RESULTS ///A////1//.//.//////////q11///!i//.11/ff/./f►l11.ffR• 

RY GAS METER --- ----- --- ORIFICE ----•---- - DRY GAS METER - -- ORIFICE 

UME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR 

:RECTI CORRECTED CORRECTI CORRECTI NOMINAL Y 

m(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variation 

(cu ft) (liters) (cu ft) (iiters) (cu ft) (number) (number) 

6.014 0.2 5.951 0.2 6.088 0.990 -0.001 

3.002 0.1 2.973 0.1 3.047 0.990 -0.000 

2.994 0.1 2.970 0.1 3.050 0.992 0.001 

Average Y -------> 0.991 

For Calibration Factor Y, the ratio of the reading of the calibration meter to the dry gas meter, 

icceptable tolerance of individual vaiues from the average is +-0.02. 

=or Orifice Calibration Factor dH@, the orifice differential pressure in inches of H20 that equates to 0.75 cfm of air 

it 68 F and 29.92 inches of Hg, acce table lerance of in ' idual values from the average is +-0.2. , 

SIGNED: ~ Date: 

r' 

~"°'t 
Temperature Mefier Cafibrations 

Meter Box #: 10 

Date: 05/04I06 

Catibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxiliary 

Point 1 68 69 68 68 67 68 

Point 2 138 139 138 139 138 138 

Point 3 250 252 250 251 250 250 

Emtech 42312 

Degrees R Calibrator Probe Stack Oven Exit Auxillary 

Point 1 528 529 528 528 527 528 

Point 2 598 599 598 599 598 598 

Point 3 710 712 710 711 710 710 

Percent Difference 

Probe Stack Oven Exit Auxiliary 

Point 1 0,189036 0 0 0.189394 0 

Point 2 0.166945 0 0.166945 0 0 

Point 3 0.280899 0 0.140647 0 0 

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Con. :)an, Nar:e ~ ~J ~ ~'Ir ~4 Da,~~ e Sanpl ed . • l~(czzl? ~~ !_I ~~ c,=r 

Presamoie Inspection 

I hereby certi fy that the ~above ref erenced no•zzle appears to be 

round, shara-ed ~ged, ~IjF rea o -F nicks and dents nd i s' judged acceptabl e 

for use' at this t irne. a:30~1 O•3°`~ 0.30 ~'' 3o ~{3 

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Last Previousiy Measurec 

Nozzl e?.rea o.o00.i~05' i t2 sigraturVr 

Date Measured q g 0~ date y-IZ-elo {. 

Pos tsampl e Measurement 

rMeasure three. dia.-neters as shown; me.asuremen"L is 

i n i nches; record bel otii; - per f orm cai cul at i-ons. ~ 

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