### Name: Patricia Q. West

Title: Manager, Environmental, Energy Supp Company: Progress Energy Florida, Inc. Sign Date: 9/3/2010 Name: Carl Vineyard, P.E. Title: Project Manager Company: Grace Consulting, Inc. Sign Date: 9/3/2010 Permitted Facility Representative / Date Testing Company Representative / Date 

## Crystal River 1 Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Thursday, February 17, 2011 Page 1 of 29

### Crystal River 1

9/3/2010 Facility Information: Crystal River Power Plant Unit 1

15760 West Power Line Road

Crystal River FL 344286708
Contact: Dave Meyer

Phone: 727-820-5295

Fax: 727-820-5229

Email: Dave.Meyer@pgnmail.com Testing Company:
Grace Consulting, Inc.

PO Box 58

510 Dickson St. Wellington OH 44090
Contact: Hal Stiles

Phone: 440-647-6672

Fax: 440-647-6673

Email: halstiles@gcitest.com

Air Permit Number:
0170004-024-AV Permitted Source ID/Name: Crystal River Power Plant 0170004

Permitted Maximum Process Rate:
3750 mmBtu/hr Max. Normal Operation Process Rate:
3750 mmBtu/hr Target Process Test Rate
3375 mmBtu/hr

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: FRS #: 110017431215

SCC / Description 10100202 External Combustion Boilers - Electric Generation - Bituminous/Subbituminous Coal - Pulverized Coal: Dry Bottom (Bituminous Coal)

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width
Stack Unit 1 182 1440 1560 4 0 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location

Carbon Monoxide Method 10 3 180 0 3 points Stack Unit 1 Formaldehyde Method 0011 3 120 0 12 points Stack Unit 1 Total organic compounds

(TOC) as Propane Method 25A 3 120 0 3 points Stack Unit 1

Hydrogen Chloride Method 26A 3 180 0 12 points Stack Unit 1 Hydrogen Fluoride Method 26A 3 180 0 12 points Stack Unit 1 Filterable Particulate OTM - 27/28 3 360 0 12 points Stack Unit 1 Filterable PM2.5 OTM - 27/28 3 360 0 12 points Stack Unit 1



### Thursday, February 17, 2011 Page 2 of 29

### Crystal River 1

9/3/2010

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.

Inorganic (Aqueous) Condensible Part. OTM - 27/28 3 360 0 12 points Stack Unit 1

Organic Condensible

Particulate OTM - 27/28 3 360 0 12 points Stack Unit 1

Total Particulate OTM - 27/28 3 360 0 12 points Stack Unit 1 Total PM2.5 OTM - 27/28 3 360 0 12 points Stack Unit 1 Beryllium Method 29 3 240 0 12 points Stack Unit 1 Arsenic Method 29 3 240 0 12 points Stack Unit 1 Zinc Method 29 3 240 0 Stack Unit 1 Phosphorus (yellow or white) Method 29 3 240 0 12 points Stack Unit 1 Chromium Method 29 3 240 0 12 points Stack Unit 1 Cobalt Method 29 3 240 0 12 points Stack Unit 1 Lead Method 29 3 240 0 12 points Stack Unit 1 Manganese Method 29 3 240 0 12 points Stack Unit 1 Nickel Method 29 3 240 0 12 points Stack Unit 1 Cadmium Method 29 3 240 0 12 points Stack Unit 1 Antimony Method 29 3 240 0 12 points Stack Unit 1 Selenium Method 29 3 240 0 12 points Stack Unit 1 Copper Method 29 3 240 0 Stack Unit 1 Barium Method 29 3 240 0 Stack Unit 1 Silver Method 29 3 240 0 Stack Unit 1 Thallium Method 29 3 240 0 Stack Unit 1
Co2 Method 3A CO2 9 240 0 3 points Stack Unit 1 O2 Method 3A O2 9 240 0 3 Points Stack Unit 1 Sulfur Dioxide Method 6C 3 180 0 3 points Stack Unit 1 Nitrogen oxides (NOx) Method 7E 3 180 0 3 points Stack Unit 1



### Thursday, February 17, 2011 Page 3 of 29

### Crystal River 1

9/3/2010 Sampling / Stack Data Results Summary



### Location Stack Unit 1 - Method 0011 Average
Run Number 1 2 3

Test Date 3/26/2010 3/26/2010 3/26/2010

Run Start Time 1:55:00 PM 4:25:00 PM 6:55:00 PM

Run Finish Time 4:00:00 PM 6:30:00 PM 9:00:00 PM
Net Run Time, minutes 120 120 120 Dry Gas Meter Volume Sampled, dscf 92.829 93.318 93.185 93.111
Moisture Content of Stack Gas, % 6.29 4.87 4.82 5.327 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000
Carbon Dioxide, % 12.7 12.7 12.9 12.767 Oxygen, % 6.4 6.3 6.2 6.300 Average Stack Gas Temperature, °F 341.83 343.33 343.08 342.747 Dry Volumetric Flow Rate, dry scfm 834,868.8 847,333.0 845,738.6 842,646.800
Actual Wet Volumetric Flue Gas Flow Rate, acfm 1,363,427.5 1,366,137.5 1,362,885.5 1,364,150.16 7 Percent Isokinetic of Sampling Rate, % 100.2 99.3 99.3 99.600
F-Factor, dscfm/MMBtu @ %O2 9599 9481 9512 9,530.667

Fw 0 0 0 0.000

Fc 0 0 0 0.000



### Location Stack Unit 1 - Method 10 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Thursday, February 17, 2011 Page 4 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 25A Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Unit 1 - Method 26A Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Thursday, February 17, 2011 Page 5 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 29 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Stack Unit 1 - Method 3A CO2 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Thursday, February 17, 2011 Page 6 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A CO2 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Unit 1 - Method 3A CO2 3 6 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Thursday, February 17, 2011 Page 7 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A O2 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Unit 1 - Method 3A O2 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Thursday, February 17, 2011 Page 8 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A O2 3 6 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Unit 1 - Method 6C Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Thursday, February 17, 2011 Page 9 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 7E Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Unit 1 - OTM - 27/28 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Thursday, February 17, 2011 Page 10 of 29

### Crystal River 1

9/3/2010 Emissions Summary



### Location: Stack Unit 1 - Method 0011 Compound: Formaldehyde Average RunNumber 1 2 3 Mass_mg 0.0049 0.00228 0.00075 0.003 lb/mmBtuO2 1.61E-06 7.31E-07 2.40E-07 0.000
ppm 1.49E-03 6.91E-04 2.28E-04 0.001 ppm@7%O2 1.43E-03 6.58E-04 2.16E-04 0.001



### Location: Stack Unit 1 - Method 10 Compound: Carbon Monoxide Average
Run 1 2 3 lb/mmBtuO2 3.44E-03 1.18E-03 2.90E-03 0.003
ppm 3.42E+00 1.19E+00 2.95E+00 2.520 ppm@7%O2 3.28E+00 1.13E+00 2.79E+00 2.400



### Location: Stack Unit 1 - Method 25A Compound: Total organic compounds (TOC) as Average
Run 1 2 3 lb/mmBtuO2 1.61E-03 2.83E-03 1.79E-03 0.002
ppm 1.02E+00 1.82E+00 1.16E+00 1.333 ppm@7%O2 9.78E-01 1.73E+00 1.10E+00 1.269



### Location: Stack Unit 1 - Method 26A Compound: Hydrogen Chloride Average RunNumber M26A-1 M26A-2 M26A-3 Mass_mg 241.147 416.811 409.396 355.785 lb/mmBtuO2 5.05E-02 8.74E-02 8.52E-02 0.074



### Compound: Hydrogen Fluoride Average RunNumber M26A-1 M26A-2 M26A-3 Mass_mg 38.432 37.938 30.828 35.733 lb/mmBtuO2 8.04E-03 7.95E-03 6.42E-03 0.007



### Location: Stack Unit 1 - Method 29 Compound: Antimony Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.00449 0.01074 0.00908 0.008 lb/mmBtuO2 6.13E-07 1.46E-06 1.24E-06 0.000



### Compound: Arsenic Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.05607 0.09097 0.08137 0.076



### Thursday, February 17, 2011 Page 11 of 29

### Crystal River 1

9/3/2010

lb/mmBtuO2 7.66E-06 1.24E-05 1.12E-05 0.000


### Compound: Barium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.3265 0.5887 1.1892 0.701 lb/mmBtuO2 4.46E-05 8.01E-05 1.63E-04 0.000



### Compound: Beryllium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.005329 0.010042 0.010326 0.009 lb/mmBtuO2 7.28E-07 1.37E-06 1.42E-06 0.000



### Compound: Cadmium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.000767 0.00322 0.00493 0.003 lb/mmBtuO2 1.05E-07 4.38E-07 6.76E-07 0.000


### Compound: Chromium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.3253 0.1103 0.0834 0.173 lb/mmBtuO2 4.44E-05 1.50E-05 1.14E-05 0.000



### Compound: Cobalt Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.02639 0.03791 0.04061 0.035 lb/mmBtuO2 3.60E-06 5.16E-06 5.57E-06 0.000



### Compound: Copper Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.11733 0.16133 0.15093 0.143 lb/mmBtuO2 1.60E-05 2.20E-05 2.07E-05 0.000



### Compound: Lead Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.0479 0.0825 0.0812 0.071 lb/mmBtuO2 6.54E-06 1.12E-05 1.11E-05 0.000



### Compound: Manganese Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.08464 0.09114 0.08874 0.088 lb/mmBtuO2 1.16E-05 1.24E-05 1.22E-05 0.000


### Compound: Nickel Average RunNumber M29-1 M29-2 M29-3 Mass_mg 1.46133 0.12263 0.09153 0.558



### Thursday, February 17, 2011 Page 12 of 29

### Crystal River 1

9/3/2010

lb/mmBtuO2 2.00E-04 1.67E-05 1.25E-05 0.000


### Compound: Phosphorus (yellow or white) Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.3688 0.9372 0.8631 0.723 lb/mmBtuO2 5.04E-05 1.28E-04 1.18E-04 0.000



### Compound: Selenium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.535 0.956 1.102 0.864 lb/mmBtuO2 7.31E-05 1.30E-04 1.51E-04 0.000



### Compound: Silver Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.000829 0.001139 0.000919 0.001 lb/mmBtuO2 1.13E-07 1.55E-07 1.26E-07 0.000


### Compound: Thallium Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.002151 0.003251 0.003251 0.003 lb/mmBtuO2 2.94E-07 4.43E-07 4.46E-07 0.000



### Compound: Zinc Average RunNumber M29-1 M29-2 M29-3 Mass_mg 0.1148 0.177 0.1117 0.135 lb/mmBtuO2 1.57E-05 2.41E-05 1.53E-05 0.000



### Location: Stack Unit 1 - Method 6C Compound: Sulfur Dioxide Average
Run 1 2 3 lb/mmBtuO2 1.31E+00 1.36E+00 1.43E+00 1.367
ppm 5.58E+02 5.82E+02 6.08E+02 582.667 ppm@7%O2 5.50E+02 5.70E+02 5.95E+02 571.667



### Location: Stack Unit 1 - Method 7E Compound: Nitrogen oxides (NOx) Average
Run 1 2 3 lb/mmBtuO2 3.12E-01 3.09E-01 3.21E-01 0.314
ppm 1.85E+02 1.84E+02 1.91E+02 186.667 ppm@7%O2 1.82E+02 1.80E+02 1.87E+02 183.000



### Location: Stack Unit 1 - OTM - 27/28 Compound: Filterable Particulate Average RunNumber M027-1 m027-2 M027-3



### Thursday, February 17, 2011 Page 13 of 29

### Crystal River 1

9/3/2010

Process Run Data Mass_mg 1573.9 199.6 89.7 621.067 lb/mmBtuO2 3.48E-01 6.35E-02 2.98E-02 0.147



### Compound: Filterable PM2.5 Average RunNumber M027-1 m027-2 M027-3 Mass_mg 225.4 63.1 35.1 107.867 lb/mmBtuO2 4.98E-02 2.01E-02 1.17E-02 0.027



### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber M027-1 m027-2 M027-3 Mass_mg 57.4 57.8 48 54.400 lb/mmBtuO2 1.27E-02 1.84E-02 1.59E-02 0.016



### Compound: Organic Condensible Particulate Average RunNumber M027-1 m027-2 M027-3 Mass_mg 39.7 34.7 18.1 30.833 lb/mmBtuO2 8.77E-03 1.10E-02 6.01E-03 0.009



### Compound: Total Particulate Average RunNumber M027-1 m027-2 M027-3 Mass_mg 1671 292.1 155.8 706.300 lb/mmBtuO2 3.69E-01 9.29E-02 5.17E-02 0.171



### Compound: Total PM2.5 Average RunNumber M027-1 m027-2 M027-3 Mass_mg 322.5 155.6 101.2 193.100 lb/mmBtuO2 7.13E-02 4.95E-02 3.36E-02 0.051



### Thursday, February 17, 2011 Page 14 of 29

### Crystal River 1

9/3/2010
Process Run Data

APCD Run Data

Process Lab Run Data 

### Run Name Value UOM Comments Target Value
1 Coal Burned 148 tons/hr 140



### 1 Average Heat Input 3619 lbs/mmBtu 3500

1 Steam Output 2010 1000 lbs/hr 2010

1 Flue Gas Sampling Point Temperature 330 Deg F 280



### 1 Unit Gross Electrical Output 386 Mwe 375

1 Unit Net Electric Generation 360 MW 360

2 Coal Burned 144 tons/hr 140



### 2 Average Heat Input 3515 lbs/mmBtu 3500

2 Steam Output 2009 1000 lbs/hr 2010

2 Flue Gas Sampling Point Temperature 335 Deg F 280



### 2 Unit Gross Electrical Output 386 Mwe 375

2 Unit Net Electric Generation 361 MW 360

3 Coal Burned 149 tons/hr 140



### 3 Average Heat Input 3701 lbs/mmBtu 3500

3 Steam Output 2050 1000 lbs/hr 2010

3 Flue Gas Sampling Point Temperature 335 Deg F 280



### 3 Unit Gross Electrical Output 390 Mwe 375

3 Unit Net Electric Generation 370 MW 360

1 Heat Input 0 Million Btus/million BTU using O2 0

Run Name Value UOM Comments Target Value


### ELECTROSTATIC PRECIPITATOR 0

Run Name Value UOM Comments
1 Acid Gas HAP , Chlorine, Fluroine sulfur, HHV, Proximate & Ultimate 0



### 1 NON-Dioxin/furan Organic HAP analysis 0
1 Mercury & Non Mercury Metallic Hap (metals analysis) 0



### Thursday, February 17, 2011 Page 15 of 29

### Crystal River 1

9/3/2010
Sampling / Stack Data Results Detail



### Location Stack Unit 1 - Method 0011 Average Run Number 1 2 3
Test Date 3/26/2010 3/26/2010 3/26/2010 Run Start Time 1:55:00 PM 4:25:00 PM 6:55:00 PM Run Finish Time 4:00:00 PM 6:30:00 PM 9:00:00 PM Net Traversing Points 12 12 12 Net Run Time, minutes 120 120 120 Nozzle Diameter, inches 0.175 0.175 0.175 0.175 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.018 1.018 1.018 1.018 Barometric Pressure, inches of Mercury 29.85 29.85 29.85 29.850 Average Orifice Meter Differential, inches H2O 2.10 2.10 2.10 2.100 Dry Gas Meter Volume Sampled, cubic feet 91.348 91.727 91.582 91.552 Average Dry Gas Meter Temperature, °F 70.42 69.83 69.75 70.000 Dry Gas Meter Volume Sampled, dscf 92.829 93.318 93.185 93.111 Total Moisture Liquid collected, g 132.4 101.5 100.3 111.400 Volume of Water Vapor, standard cubic feet 6.23 4.78 4.72 5.243 Moisture Content of Stack Gas, % 6.29 4.87 4.82 5.327 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9371 0.9513 0.9518 0.947 Carbon Dioxide, % 12.7 12.7 12.9 12.767 Oxygen, % 6.4 6.3 6.2 6.300 Carbon Monoxide & Nitrogen, % 80.9 81 80.9 80.933 Fuel Factor 1.14 1.15 1.14 Dry Molecular Weight, lb/lb-Mole 30.29 30.28 30.31 30.293 Wet Molecular weight, lb/lb-Mole 29.52 29.68 29.72 29.640 Flue Gas Static Pressure, inches of H2O -2.2 -2.3 -2.5 -2.333 Absolute Flue Gas Pressure, inches of Mercury 29.69 29.68 29.67 29.680 Average Stack Gas Temperature, °F 341.83 343.33 343.08 342.747 Average Velocity Head, inches of H2O 3.3535234384 2617 3.377354937

2345 3.365924828

19975 3.366

Average Stack Gas Velocity, feet/second 125.78 126.03 125.73 125.847 Stack Cross-Sectional Area, square feet 180.663 180.663 180.663 180.663 Dry Volumetric Flow Rate, dry scfm 834,868.8 847,333.0 845,738.6 842,646.800 Actual Wet Volumetric Flue Gas Flow Rate, acfm 1,363,427.5 1,366,137.5 1,362,885.5 1,364,150.1 67 Percent Isokinetic of Sampling Rate, % 100.2 99.3 99.3 99.600 Percent Excess Air, % 42.8 41.8 40.9 41.833 F-Factor, dscfm/MMBtu @ %O2 9599 9481 9512 9,530.667 Round Duct Diameter, inches 182 182 182 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0
Fw 0 0 0 0.000
Fc 0 0 0 0.000



### Thursday, February 17, 2011 Page 16 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 10 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 17 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 25A Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 18 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 26A Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Thursday, February 17, 2011 Page 19 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 29 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Thursday, February 17, 2011 Page 20 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A CO2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 21 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A CO2 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 22 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A CO2 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 23 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A O2 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 24 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A O2 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 25 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 3A O2 3 6 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 26 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 6C Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 27 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - Method 7E Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Thursday, February 17, 2011 Page 28 of 29

### Crystal River 1

9/3/2010

Location Stack Unit 1 - OTM - 27/28 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Thursday, February 17, 2011 Page 29 of 29