# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\7567060406235108450\[EPA-HQ-OAR-2013-0291-DRAFT-0157.xls]Boral-Kiln-Emission Calcs** Date: 12/1/14

Plant name: Boral Bricks Inc. Location: FACID: Test date: 9/22/2010 UNITID: Equipment: Kiln 6BK Control device: DIFF Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 18.9 173.6 50,241 0.431 3.83E-11 0.0876 0.5977.48E-06 20.26 3.69E-07

2 19.1 175.4 50,706 0.313 2.75E-11 0.0630 0.4735.42E-06 20.26 2.68E-07 3 19.1 182.4 50,867 0.339 2.87E-11 0.0656 0.4931 5.67E-06 20.26 2.80E-07 Average 19.0 177.1 50,605 0.361 3.15E-11 0.0721 0.521 6.19E-06 20.3 3.06E-07 TEQ 1 M23 18.9 173.6 50,241 0.006873 6.11E-13 0.001398 0.009524 1.19E-07 20.26 5.89E-09

2 19.1 175.4 50,706 0.005279 4.64E-13 0.001063 0.0079839.16E-08 20.26 4.52E-09 3 19.1 182.4 50,867 0.006298 5.33E-13 0.001219 0.009162 1.05E-07 20.26 5.20E-09 Average 19.0 177.1 50,605 0.0062 5.36E-13 0.001227 0.008890 1.05E-07 20.3 5.20E-09 Notes: Salisbury, NC

1 of 1DIOXIN-FURAN PARTICLE CATCH

Measured wt, ng Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Compound Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.0248 0.0388 0.048 Total TCDD 24.8 38.8 48 Total TCDD BDLE 24.8ADLE 38.8ADLE 48 Total PeCDD 0.00686 0.019 0.00817 Total PeCDD 6.86 19 8.17 Total PeCDD ADLE 6.86ADLE 19ADLE 8.17 Total HxCDD 0.0138 0.0111 0.0125 Total HxCDD 13.8 11.1 12.5 Total HxCDD ADLE 13.8ADLE 11.1ADLE 12.5 Total HpCDD 0.00763 0.0184 0.015 Total HpCDD 7.63 18.4 15 Total HpCDD ADLE 7.63ADLE 18.4BDLE 15 Total OCDD 0.0823 0.0631 0.0443 Total OCDD 82.3 63.1 44.3 Total OCDD J 82.3 J 63.1 J 44.3

Total dioxins 0.13539 0.1504 0.12797 Total TCDF 0.241 0.139 0.154 Total TCDF 241 139 154 Total TCDF ADLE 241ADLE 139ADLE 154 Total PeCDF 0.04 0.011 0.0316 Total PeCDF 40 11 31.6 Total PeCDF ADLE 40ADLE 11ADLE 31.6 Total HxCDF 0.00763 0.00397 0.014 Total HxCDF 7.63 3.97 14 Total HxCDF ADLE 7.63ADLE 3.97ADLE 14 Total HpCDF 0.00204 0.00474 0.0053 Total HpCDF 2.04 4.74 5.3 Total HpCDF ADLE 2.04BDLE 4.74ADLE 5.3 Total OCDF 0.00454 0.00368 0.00611 Total OCDF 4.54 3.68 6.11 Total OCDF E J 4.54 J 3.68 J 6.11

Total furans 0.29521 0.16239 0.21101 TOTAL CDD/CDF 0.4306 0.31279 0.33898

Measured wt, ng TEQ, ng Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.00154 0.00111 0.00141 0.00154 0.00111 0.00141 1 2,3,7,8-TCDD 1.54 1.11 1.41 2,3,7,8-TCDD BDL 1.54BDL 1.11BDL 1.41 1,2,3,7,8 PeCDD 0.00143 0.00132 0.00131 0.00143 0.00132 0.00131 1 1,2,3,7,8-PeCDD 1.43 1.32 1.31 1,2,3,7,8-PeCDD BDL 1.43E J 1.32BDL 1.31 1,2,3,4,7,8 HxCDD 0.00127 0.00084 0.0012 0.00013 8.4E-05 0.00012 0.1 1,2,3,4,7,8-HxCDD 1.27 0.84 1.2 1,2,3,4,7,8-HxCDD BDL 1.27BDL 0.84BDL 1.2 1,2,3,6,7,8 HxCDD 0.001250.000878 0.00117 0.00013 8.8E-05 0.00012 0.1 1,2,3,6,7,8-HxCDD 1.25 0.878 1.17 1,2,3,6,7,8-HxCDD BDL 1.25BDL 0.878BDL 1.17 1,2,3,7,8,9 HxCDD 0.00134 0.0017 0.00276 0.00013 0.00017 0.00028 0.1 1,2,3,7,8,9-HxCDD 1.34 1.7 2.76 1,2,3,7,8,9-HxCDD BDL 1.34E J 1.7 J 2.76 1,2,3,4,6,7,8 HpCDD 0.00763 0.00764 0.00766 7.6E-05 7.6E-05 7.7E-05 0.01 1,2,3,4,6,7,8-HpCDD 7.63 7.64 7.66 1,2,3,4,6,7,8-HpCDD J 7.63 J 7.64E J 7.66 Total OCDD 0.0823 0.0631 0.0443 2.5E-05 1.9E-05 1.3E-05 0.0003 OCDD 82.3 63.1 44.3 OCDD J 82.3 J 63.1 J 44.3 Total CDD congeners 0.096760.076588 0.05981 0.00346 0.00287 0.00332 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.0141 0.00928 0.00741 0.00141 0.00093 0.00074 0.1 2,3,7,8-TCDF 14.1 9.28 7.41 2,3,7,8-TCDF ADL 14.1 J 9.28 J 7.41 1,2,3,7,8 PeCDF 0.00385 0.00268 0.00312 0.00012 8E-05 9.4E-05 0.03 1,2,3,7,8-PeCDF 3.85 2.68 3.12 1,2,3,7,8-PeCDF J 3.85E J 2.68E J 3.12 2,3,4,7,8 PeCDF 0.00342 0.00258 0.00401 0.00103 0.00077 0.0012 0.3 2,3,4,7,8-PeCDF 3.42 2.58 4.01 2,3,4,7,8-PeCDF E J 3.42 J 2.58 J 4.01 1,2,3,4,7,8 HxCDF 0.00276 0.00204 0.00299 0.00028 0.0002 0.0003 0.1 1,2,3,4,7,8-HxCDF 2.76 2.04 2.99 1,2,3,4,7,8-HxCDF J 2.76 J 2.04 J 2.99 1,2,3,6,7,8 HxCDF 0.0029 0.00192 0.0026 0.00029 0.00019 0.00026 0.1 1,2,3,6,7,8-HxCDF 2.9 1.92 2.6 1,2,3,6,7,8-HxCDF J 2.9 J 1.92 J 2.6 2,3,4,6,7,8 HxCDF 0.001420.000934 0.00189 0.00014 9.3E-05 0.00019 0.1 2,3,4,6,7,8-HxCDF 1.42 0.934 1.89 2,3,4,6,7,8-HxCDF E J 1.42E J 0.934E J 1.89 1,2,3,7,8,9 HxCDF 0.0009570.000892 0.00105 9.6E-05 8.9E-05 0.00011 0.1 1,2,3,7,8,9-HxCDF 0.957 0.892 1.05 1,2,3,7,8,9-HxCDF BDL 0.957BDL 0.892BDL 1.05 1,2,3,4,6,7,8 HpCDF 0.00476 0.00389 0.00523 4.8E-05 3.9E-05 5.2E-05 0.01 1,2,3,4,6,7,8-HpCDF 4.76 3.89 5.23 1,2,3,4,6,7,8-HpCDF E J 4.76E J 3.89E J 5.23 1,2,3,4,7,8,9 HpCDF 0.00123 0.00106 0.00306 1.2E-05 1.1E-05 3.1E-05 0.01 1,2,3,4,7,8,9-HpCDF 1.23 1.06 3.06 1,2,3,4,7,8,9-HpCDF BDL 1.23BDL 1.06 J 3.06 Total OCDF 0.00454 0.00368 0.00611 1.4E-06 1.1E-06 1.8E-06 0.0003 OCDF 4.54 3.68 6.11 OCDF E J 4.54 J 3.68 J 6.11 Total CDF congeners 0.0399370.028956 0.03747 0.00342 0.00241 0.00298 **TOTAL CDD/CDF (TEQ)** 0.1366970.105544 0.09728 0.00687 0.00528 0.0063

Total Dioxins 0.096760.076588 0.05981 Total Dioxins 96.76 76.588 59.81 Total Dioxins 96.76 76.588 59.81 Total Furans 0.0399370.028956 0.03747 Total Furans 39.937 28.956 37.47 Total Furans 39.937 28.956 37.47 Total CDD/CDF 0.1366970.105544 0.09728 Measured wt, pg Measured wt, pg Measured wt, pg

Measured wt, pg

EPA-HQ-OAR-2013-0291-DRAFT-0157 Boral-Kiln D-F Data 12/1/2014

# Filename: **C:\PROGRA~2\Documentum\CTS\docbases\ProDocbase\config\temp_sessions\7567060406235108450\[EPA-HQ-OAR-2013-0291-DRAFT-0157.xls]Boral-Kiln-Emission Calcs** Date: 12/1/14

Plant name: Boral Bricks Location: FACID: Test date: 9/23/2010 UNITID: Equipment: Dryer Control device: Gas Volum. Emission Process

Run Test O2

# conc.,volume, flow rate, Mass, Concentration, rate, rate, Emission factor, Pollutant No. Method % DSCF DSCFM ng BDL MW gr/dscf ng/dscm @7%O2 

# g/hr ton/hr g/ton g/lb CDD/CDF 1 M23 20.9 161.7 30,136 0.077 7.39E-12 0.0169 #DIV/0! 8.65E-07 20.26 4.27E-08

2 20.9 159.1 30,367 0.125 1.22E-11 0.0278 #DIV/0! 1.43E-06 20.26 7.08E-08 3 20.9 158.6 30,299 0.128 1.25E-11 0.0285 #DIV/0! 1.47E-06 20.26 7.25E-08 Average 20.9 159.8 30,267 0.11 1.07E-11 0.0244 #DIV/0! 1.26E-06 20.3 6.20E-08 TEQ 1 M23 20.9 161.7 30,136 0.005912 5.64E-13 0.0012906 #DIV/0! 6.61E-08 20.26 3.26E-09

2 20.9 159.1 30,367 0.006114 5.93E-13 0.0013571 #DIV/0! 7.00E-08 20.26 3.46E-09 3 20.9 158.6 30,299 0.007232 7.04E-13 0.0016102 #DIV/0! 8.29E-08 20.26 4.09E-09 Average 20.9 159.8 30,267 0.0064 6.20E-13 0.0014193 #DIV/0! 7.30E-08 20.3 3.60E-09 Notes: Salisbury, NC

1 of 1DIOXIN-FURAN PARTICLE CATCH

Measured wt, ng Congener Run 1 Run 2 Run 3 Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 Total TCDD 0.00676 0.00961 0.0158 Total TCDD 6.76 9.61 15.8 Total TCDD ADLE 6.76BDLE 9.61ADLE 15.8 Total PeCDD 0.00591 0.003 0.0104 Total PeCDD 5.91 3 10.4 Total PeCDD ADLE 5.91ADLE 3ADLE 10.4 Total HxCDD 0.0146 0.0147 0.0157 Total HxCDD 14.6 14.7 15.7 Total HxCDD ADLE 14.6ADLE 14.7ADLE 15.7 Total HpCDD 0.00553 0.02050.00945 Total HpCDD 5.53 20.5 9.45 Total HpCDD ADLE 5.53BDLE 20.5ADLE 9.45 Total OCDD 0.0346 0.0492 0.0449 Total OCDD 34.6 49.2 44.9 Total OCDD J 34.6 J 49.2E J 44.9

Total dioxins 0.0674 0.09701 0.09625 Total TCDF 0.00149 0.0128 0.0181 Total TCDF 1.49 12.8 18.1 Total TCDF ADLE 1.49ADLE 12.8ADLE 18.1 Total PeCDF 0.00147 0.00222 0.00583 Total PeCDF 1.47 2.22 5.83 Total PeCDF BDL 1.47BDLE 2.22ADLE 5.83 Total HxCDF 0.0014 0.00626 0.00181 Total HxCDF 1.4 6.26 1.81 Total HxCDF BDL 1.4ADLE 6.26BDLE 1.81 Total HpCDF 0.001750.004390.00353 Total HpCDF 1.75 4.39 3.53 Total HpCDF BDL 1.75BDLE 4.39ADLE 3.53 Total OCDF 0.00390.00257 0.00254 Total OCDF 3.9 2.57 2.54 Total OCDF BDL 3.9BDL 2.57BDL 2.54

Total furans0.01001 0.02824 0.03181 TOTAL CDD/CDF 0.07741 0.125250.12806

Measured wt, ng TEQ, ng Congener Run 1 Run 2 Run 3 Run 1 Run 2 Run 3 TEF Congener Run 1 Run 2 Run 3 Congener Flag Run 1 Flag Run 2 Flag Run 3 2,3,7,8 TCDD 0.00204 0.00186 0.00246 0.00204 0.00186 0.00246 1 2,3,7,8-TCDD 2.04 1.86 2.46 2,3,7,8-TCDD BDL 2.04BDL 1.86E J 2.46 1,2,3,7,8 PeCDD 0.00195 0.0024 0.002780.00195 0.0024 0.00278 1 1,2,3,7,8-PeCDD 1.95 2.4 2.78 1,2,3,7,8-PeCDD BDL 1.95BDL 2.4BDL 2.78 1,2,3,4,7,8 HxCDD 0.00212 0.001780.002180.00021 0.000180.00022 0.1 1,2,3,4,7,8-HxCDD 2.12 1.78 2.18 1,2,3,4,7,8-HxCDD BDL 2.12BDL 1.78BDL 2.18 1,2,3,6,7,8 HxCDD 0.00213 0.00181 0.00207 0.00021 0.000180.00021 0.1 1,2,3,6,7,8-HxCDD 2.13 1.81 2.07 1,2,3,6,7,8-HxCDD BDL 2.13BDL 1.81BDL 2.07 1,2,3,7,8,9 HxCDD 0.00221 0.001950.00227 0.00022 0.0002 0.00023 0.1 1,2,3,7,8,9-HxCDD 2.21 1.95 2.27 1,2,3,7,8,9-HxCDD BDL 2.21BDL 1.95BDL 2.27 1,2,3,4,6,7,8 HpCDD 0.00553 0.009680.00945 5.5E-05 9.7E-05 9.5E-05 0.01 1,2,3,4,6,7,8-HpCDD 5.53 9.68 9.45 1,2,3,4,6,7,8-HpCDD J 5.53E J 9.68 J 9.45 Total OCDD 0.0346 0.0492 0.0449 1E-05 1.5E-05 1.3E-05 0.0003 OCDD 34.6 49.2 44.9 OCDD J 34.6 J 49.2E J 44.9 Total CDD congeners 0.05058 0.068680.06611 0.0047 0.00493 0.006 Measured wt, ng TEQ, ng 2,3,7,8 TCDF 0.00136 0.00147 0.001480.00014 0.000150.00015 0.1 2,3,7,8-TCDF 1.36 1.47 1.48 2,3,7,8-TCDF BDL 1.36E J 1.47E J 1.48 1,2,3,7,8 PeCDF 0.00153 0.00142 0.00146 4.6E-05 4.3E-05 4.4E-05 0.03 1,2,3,7,8-PeCDF 1.53 1.42 1.46 1,2,3,7,8-PeCDF BDL 1.53BDL 1.42 J 1.46 2,3,4,7,8 PeCDF 0.00141 0.00131 0.00131 0.00042 0.000390.00039 0.3 2,3,4,7,8-PeCDF 1.41 1.31 1.31 2,3,4,7,8-PeCDF BDL 1.41BDL 1.31E J 1.31 1,2,3,4,7,8 HxCDF 0.00136 0.00163 0.00136 0.00014 0.00016 0.00014 0.1 1,2,3,4,7,8-HxCDF 1.36 1.63 1.36 1,2,3,4,7,8-HxCDF BDL 1.36E J 1.63BDL 1.36 1,2,3,6,7,8 HxCDF 0.00128 0.001650.00132 0.00013 0.00017 0.00013 0.1 1,2,3,6,7,8-HxCDF 1.28 1.65 1.32 1,2,3,6,7,8-HxCDF BDL 1.28E J 1.65BDL 1.32 2,3,4,6,7,8 HxCDF 0.0012 0.00093 0.00137 0.00012 9.3E-050.00014 0.1 2,3,4,6,7,8-HxCDF 1.2 0.933 1.37 2,3,4,6,7,8-HxCDF BDL 1.2BDL 0.933BDL 1.37 1,2,3,7,8,9 HxCDF 0.00184 0.00123 0.00184 0.00018 0.00012 0.00018 0.1 1,2,3,7,8,9-HxCDF 1.84 1.23 1.84 1,2,3,7,8,9-HxCDF BDL 1.84BDL 1.23BDL 1.84 1,2,3,4,6,7,8 HpCDF 0.001450.004390.00353 1.5E-05 4.4E-05 3.5E-05 0.01 1,2,3,4,6,7,8-HpCDF 1.45 4.39 3.53 1,2,3,4,6,7,8-HpCDFBDL 1.45E J 4.39 J 3.53 1,2,3,4,7,8,9 HpCDF 0.00214 0.00166 0.00218 2.1E-05 1.7E-05 2.2E-05 0.01 1,2,3,4,7,8,9-HpCDF 2.14 1.66 2.18 1,2,3,4,7,8,9-HpCDFBDL 2.14BDL 1.66BDL 2.18 Total OCDF 0.00390.00257 0.00254 1.2E-06 7.7E-07 7.6E-07 0.0003 OCDF 3.9 2.57 2.54 OCDF BDL 3.9BDL 2.57BDL 2.54 Total CDF congeners 0.01747 0.01826 0.018390.00121 0.001190.00123 **TOTA L CDD/CDF (TEQ)**  0.068050.08694 0.08450.00591 0.00611 0.00723

Total Dioxins 0.05058 0.068680.06611 Total Dioxins 50.58 68.68 66.11 Total Dioxins 50.58 68.68 66.11 Total Furans 0.01747 0.01826 0.01839 Total Furans 17.47 18.263 18.39 Total Furans 17.47 18.263 18.39 Total CDD/CDF 0.068050.08694 0.0845 Measured wt, pg Measured wt, pg Measured wt, pg

Measured wt, pg

EPA-HQ-OAR-2013-0291-DRAFT-0157 Boral Dryer D-F Data 12/1/2014

## Boral - Salisbury, NC

**Location Method**  **Compound Run 1**  **Mass Run 1**  **Flag Run 1 Comments**  **Run 2 Mass** **Run 2 Flag**  **Run 2 Comments Run 3**  **Mass Run 3**  **Flag Run 3 Comments**  **Units** Kiln 6BK Method 23 1,2,3,4,6,7,8-HpCDD 7.63 ADL 7.64 ADL 7.66 ADL EMPC AS REPORTED BY ALTA pg Kiln 6BK Method 23 1,2,3,4,6,7,8-HpCDF 4.76 ADL EMPC AS REPORTED BY ALTA 3.89 ADL EMPC AS REPORTED BY ALTA 5.23 ADL EMPC AS REPORTED BY ALTA pg Kiln 6BK Method 23 1,2,3,4,7,8,9-HpCDF 1.23 BDL DL AS REPORTED BY ALTA 1.06 BDL DL AS REPORTED BY ALTA 3.06 ADL pg Kiln 6BK Method 23 1,2,3,4,7,8-HxCDD 1.27 BDL DL AS REPORTED BY ALTA 0.84 BDL DL AS REPORTED BY ALTA 1.2 BDL DL AS REPORTED BY ALTA pg Kiln 6BK Method 23 1,2,3,4,7,8-HxCDF 2.76 ADL 2.04 ADL 2.99 ADL pg Kiln 6BK Method 23 1,2,3,6,7,8-HxCDD 1.25 BDL DL AS REPORTED BY ALTA 0.878BDL DL AS REPORTED BY ALTA 1.17 BDL DL AS REPORTED BY ALTA pg Kiln 6BK Method 23 1,2,3,6,7,8-HxCDF 2.9 ADL 1.92 ADL 2.6 ADL pg Kiln 6BK Method 23 1,2,3,7,8,9-HxCDD 1.34 BDL DL AS REPORTED BY ALTA 1.7 ADL EMPC AS REPORTED BY ALTA 2.76 ADL pg Kiln 6BK Method 23 1,2,3,7,8,9-HxCDF 0.957BDL DL AS REPORTED BY ALTA 0.892BDL DL AS REPORTED BY ALTA 1.05 BDL DL AS REPORTED BY ALTA pg Kiln 6BK Method 23 1,2,3,7,8-PeCDD 1.43 BDL DL AS REPORTED BY ALTA 1.32 ADL EMPC AS REPORTED BY ALTA 1.31 BDL DL AS REPORTED BY ALTA pg Kiln 6BK Method 23 1,2,3,7,8-PeCDF 3.85 ADL 2.68 ADL EMPC AS REPORTED BY ALTA 3.12 ADL EMPC AS REPORTED BY ALTA pg Kiln 6BK Method 23 2,3,4,6,7,8-HxCDF 1.42 ADL EMPC AS REPORTED BY ALTA 0.934ADL EMPC AS REPORTED BY ALTA 1.89 ADL EMPC AS REPORTED BY ALTA pg Kiln 6BK Method 23 2,3,4,7,8-PeCDF 3.42 ADL EMPC AS REPORTED BY ALTA 2.58 ADL 4.01 ADL pg Kiln 6BK Method 23 2,3,7,8-TCDD 1.54 BDL DL AS REPORTED BY ALTA 1.11 BDL DL AS REPORTED BY ALTA 1.41 BDL DL AS REPORTED BY ALTA pg Kiln 6BK Method 23 2,3,7,8-TCDF 14.1 ADL 9.28 ADL 7.41 ADL pg Kiln 6BK Method 23 OCDD 82.3 ADL 63.1 ADL 44.3 ADL pg Kiln 6BK Method 23 OCDF 4.54 ADL EMPC AS REPORTED BY ALTA 3.68 ADL 6.11 ADL pg Kiln 6BK Method 26AChlorine 0.135ADL 0 BDL ND AS REPORTED BY ENTHALPY 0.006ADL gm Kiln 6BK Method 26AHydrogen Chloride 3E-04ADL 3E-04ADL 2E-04ADL gm Kiln 6BK Method 26AHydrogen Fluoride 28.7 BDL ND AS REPORTED BY ENTHALPY 0 BDL ND AS ENTHALPY BY ENTHALPY 0 BDL ND AS REPORTED BY ENTHALPY gm Kiln 6BK Method 29 Antimony 2.4 BDL 2.5 BDL 2.4 BDL ug Kiln 6BK Method 29 Arsenic 0.1 BDL 1.3 BDL 1.2 BDL ug Kiln 6BK Method 29 Barium 15.9 ADL 6.4 DLL 8.9 ADL ug Kiln 6BK Method 29 Beryllium 0.12 BDL 0.13 BDL 0.12 BDL ug Kiln 6BK Method 29 Cadmium 0.73 BDL 0.75 BDL 0.71 BDL ug Kiln 6BK Method 29 Chromium 4.7 ADL 2.1 DLL 2.1 DLL ug Kiln 6BK Method 29 Cobalt 0.7 BDL 0.8 BDL 0.7 BDL ug Kiln 6BK Method 29 Copper 1.4 DLL 1.8 DLL 2 DLL ug

Kiln 6BK Method 29 Filterable Particulate Conducted in conjunction with EPA M26A Conducted in conjunction w/ EPA M26a 0 Performed in conjunction w EPA M26a ug Kiln 6BK Method 29 Lead 1.2 BDL 1.3 BDL 1.2 BDL ug Kiln 6BK Method 29 Magnesium 16.1 ADL 18.8 ADL 18.1 ADL ug Kiln 6BK Method 29 Manganese 3 ADL 3.5 ADL 12.9 ADL ug Kiln 6BK Method 29 Mercury 3.4 BDL 3.3 BDL 3.6 ADL ug Kiln 6BK Method 29 Nickel 17 ADL 2.7 ADL 2.2 ADL ug

Kiln 6BK Method 29 Phosphorus (yellow or white) 36.9 ADL 34.8 ADL 38.8 ADL ug Kiln 6BK Method 29 Selenium 2.9 DLL 2.5 BDL 2.4 BDL ug Kiln 6BK Method 29 Silver 1.2 BDL 1.3 BDL 1.2 BDL ug Kiln 6BK Method 29 Thallium 1.2 BDL 1.3 BDL 1.2 BDL ug Kiln 6BK Method 29 Zinc 5 ADL 6.4 ADL 6.8 ADL ug Kiln 6BK Method 5 Filterable Particulate 0.002ADL 0 BDL ND = Non Detect 0.001ADL gm Dryer Method 23 1,2,3,4,6,7,8-HpCDD 5.53 ADL 9.68 ADL EMPC AS REPORTED BY ALTA 9.45 ADL pg Dryer Method 23 1,2,3,4,6,7,8-HpCDF 1.45 BDL DL AS REPORTED BY ALTA 4.39 ADL EMPC AS REPORTED BY ALTA 3.53 ADL pg Dryer Method 23 1,2,3,4,7,8,9-HpCDF 2.14 BDL DL AS REPORTED BY ALTA 1.66 BDL DL AS REPORTED BY ALTA 2.18 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,4,7,8-HxCDD 2.12 BDL DL AS REPORTED BY ALTA 1.78 BDL DL AS REPORTED BY ALTA 2.18 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,4,7,8-HxCDF 1.36 BDL DL AS REPORTED BY ALTA 1.63 ADL EMPC AS REPORTED BY ALTA 1.36 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,6,7,8-HxCDD 2.13 BDL DL AS REPORTED BY ALTA 1.81 BDL DL AS REPORTED BY ALTA 2.07 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,6,7,8-HxCDF 1.28 BDL DL AS REPORTED BY ALTA 1.65 ADL EMPC AS REPORTED BY ALTA 1.32 BDL DL AS REPORTED BY ALTA pg

## Location **Method Compound**  **Run 1 Mass** **Run 1 Flag**  **Run 1 Comments Run 2**  **Mass Run 2**  **Flag Run 2 Comments**  **Run 3 Mass** **Run 3 Flag**  **Run 3 Comments Units**  Dryer Method 23 1,2,3,7,8,9-HxCDD 2.21 BDL DL AS REPORTED BY ALTA 1.95 BDL DL AS REPORTED BY ALTA 2.27 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,7,8,9-HxCDF 1.84 BDL DL AS REPORTED BY ALTA 1.23 BDL DL AS REPORTED BY ALTA 1.84 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,7,8-PeCDD 1.95 BDL DL AS REPORTED BY ALTA 2.4 BDL DL AS REPORTED BY ALTA 2.78 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 1,2,3,7,8-PeCDF 1.53 BDL DL AS REPORTED BY ALTA 1.42 BDL DL AS REPORTED BY ALTA 1.46 ADL pg Dryer Method 23 2,3,4,6,7,8-HxCDF 1.2 BDL DL AS REPORTED BY ALTA 0.933BDL DL AS REPORTED BY ALTA 1.37 BDL DL AS REPORTED BY ALTA pg Dryer Method 23 2,3,4,7,8-PeCDF 1.41 BDL DL AS REPORTED BY ALTA 1.31 BDL DL AS REPORTED BY ALTA 1.31 ADL EMPC AS REPORTED BY ALTA pg Dryer Method 23 2,3,7,8-TCDD 2.04 BDL DL AS REPORTED BY ALTA 1.86 BDL DL AS REPORTED BY ALTA 2.46 ADL EMPC AS REPORTED BY ALTA pg Dryer Method 23 2,3,7,8-TCDF 1.36 BDL DL AS REPORTED BY ALTA 1.47 ADL EMPC AS REPORTED BY ALTA 1.48 ADL EMPC AS REPORTED BY ALTA pg Dryer Method 23 OCDD 34.6 ADL 49.2 ADL 44.9 ADL EMPC AS REPORTED BY ALTA pg Dryer Method 23 OCDF 3.9 BDL DL AS REPORTED BY ALTA 2.57 BDL DL AS REPORTED BY ALTA 2.54 BDL DL AS REPORTED BY ALTA pg