### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1 Wa bash River Wa bash River Combined Cycle Unit 1 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte 

### Wabash River Wabash River Combined Cycle Unit 1 As Received Higher Heating Value 

### Wabash River Wabash River Combined Cycle Unit 1 As Received % Moisture 

### Wabash River Wabash River Combined Cycle Unit 1 As Received % Ash 

### Wabash River Wabash River Combined Cycle Unit 1 As Received % Sulfur 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Higher Heating Value 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis % Ash 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis % Sulfur 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Antim ony 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Arsenic 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Bery llium 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Cadmium 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Chlorine 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Chromium 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Cobalt 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Fluorine 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Lead 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Manganese 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Mercury 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis Nickel 

### Wabash River Wabash River Combined Cycle Unit 1 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 ASTM D3174 ASTM D4239 ASTM D5865 ASTM D3174 ASTM D4239 SW6010B SW6010B SW6010B SW6010B ASTM E776/9253 SW6010B SW6010B ASTM D3761 SW6010B SW6010B ASTM D6722 SW6010B SW6010BEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### Wabash River Wabash River Combined Cycle Unit 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units WR CC-GFS-COMP-R1A-AG



### 5/26/2010 5/26/2010 9290.00 Btu/lb WR CC-GFS-COMP-R2A-AG



### 5/26/2010 5/26/2010 9240.00 Btu/lb WR CC-GFS-COMP-R3A-AG



### 5/26/2010 5/26/2010 107000.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 37.2 2.03 3.17 14790 Btu/lb 3.23 5.05 37.5 1.56 3.06 14780 Btu/lb 2.5 4.9 27.3 2.76 3.69 14720 Btu/lb 3.8 5.08Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### [< 0.0100] BDL

% 0.05 % [< 0.0100] BDL

%Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 10 ppm 37.2 10 ppm 37.5 10 ppm 27.3 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 12.5 3.23 84.2 85 3.31 1.66 5.05 12.1 2.5 85.4 85 3.47 1.65 4.9 16.8 3.8 79.4 84.3 3.51 1.68 5.08 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 1.67 2.43 1.64EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### Wabash River Wabash River Combined Cycle Unit 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units WR CC-GFS-COMP-R1A-ORG



### 5/27/2010 5/27/2010 9340.00 Btu/lb WR CC-GFS-COMP-R2A-ORG



### 5/27/2010 5/27/2010 9310.00 Btu/lb WR CC-GFS-COMP-R3A-ORG



### 5/27/2010 5/27/2010 9350.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 37.3 1.3 3.05 14900 Btu/lb 2.07 4.86 37.7 1.72 2.87 14940 Btu/lb 2.76 4.61 37.4 1.29 2.65 14940 Btu/lb 2.06 4.23Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt UnitsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur



### 37.3 10.4 2.07 87.6 86.8 3.52 1.66 4.86 37.7 14.2 2.76 83 85.6 3.56 1.64 4.61 37.4 10.5 2.06 87.4 84.7 3.29 1.49 4.23 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 1.12 1.88 4.22EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### Wabash River Wabash River Combined Cycle Unit 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units WR CC-GFS-COMP-R1A-MET



### 6/2/2010 6/2/2010 9240.00 Btu/lb WR CC-GFS-COMP-R2A-MET



### 6/3/2010 6/3/2010 9480.00 Btu/lb WR CC-GFS-COMP-R3A-MET



### 6/3/2010 6/3/2010 9300.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 37.6 2.06 3.08 14810 Btu/lb 3.3 4.94 35.9 1.47 3.31 14790 Btu/lb 2.29 5.16 37.5 1.83 3.04 14880 Btu/lb 2.93 4.86Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 0.023 mg/Kg [< 3] BDL mg/Kg [< 2] BDL mg/Kg [< 1] BDL [< 0.0100] BDL

mg/Kg [< 3] BDL mg/Kg [< 2] BDL mg/Kg [< 1] BDL [< 0.0100] BDL

mg/Kg [< 3] BDL mg/Kg [< 2] BDL mg/Kg [< 1] BDLBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/Kg [< 1] BDL mg/Kg 8.82 mg/Kg [< 1] BDL mg/Kg 6.04 mg/Kg mg/Kg [< 1] BDL mg/Kg 6.81 mg/Kg [< 1] BDL mg/Kg 4.94 mg/Kg mg/Kg [< 1] BDL mg/Kg 6.74 mg/Kg [< 1] BDL mg/Kg 4.64 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 82.1 mg/Kg [< 2] BDL mg/Kg 0.347 mg/Kg 37.6 88.7 mg/Kg [< 2] BDL mg/Kg 0.289 mg/Kg 35.9 90.2 mg/Kg [< 2] BDL mg/Kg 0.212 mg/Kg 37.5 Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 15.8 3.3 80.9 85.3 3.41 1.6 4.94 1.54 10.8 2.29 86.9 85.6 3.31 1.61 5.16 1.95 15.7 2.93 81.4 82.2 3.41 1.63 4.86 4.99 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt1 Facility Name Boiler ID HA Ps Test Group 

### Wabash River Wabash River Combined Cycle Unit 1 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units WR CC-ORG-CS-COMP-R1



### 6/28/2010 6/28/2010 9340.00 Btu/lb WR CC-ORG-CS-COMP-R2



### 6/29/2010 6/29/2010 9340.00 Btu/lb WR CC-ORG-CS-COMP-R3



### 6/30/2010 6/30/2010 9280.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 36.8 1.83 3.85 14780 Btu/lb 2.9 6.09 37.8 1.3 3.85 15020 Btu/lb 2.09 6.19 37.6 1.2 3.91 14870 Btu/lb 1.92 6.27Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 0.027 mg/Kg [<3.0], BDL mg/Kg [<2.0], BDL mg/Kg [<1.0], BDL 0.03 mg/Kg 1560 mg/Kg [<2.0], BDL mg/Kg [<1.0], BDL [<0.01], BDL

mg/Kg 3.54 mg/Kg [<2.0], BDL mg/Kg [<1.0], BDLBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### mg/kg 1.5 mg/kg 10.7 mg/kg [<1.0], BDL mg/kg 6.62 mg/kg mg/kg 1.74 mg/kg 70.7 mg/kg 2760 mg/kg 24 mg/kg mg/kg [<1.0], BDL mg/kg 5.86 mg/kg 3.42 mg/kg 5.84 mg/kgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 117 mg/kg [<2.0], BDL mg/kg [<0.10], BDL mg/kg 36.8 9.88 mg/kg [<2.0], BDL mg/kg [<0.10], BDL mg/kg 37.8 132 mg/kg [<2.0], BDL mg/kg [<0.10], BDL mg/kg 37.6 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 

### 14.9 2.9 82.3 85.4 3.77 1.65 6.09 0.22 16.1 2.09 81.8 86.3 3.65 1.64 6.19 0.08 15.1 1.92 83 85.1 3.51 1.68 6.27 1.51 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm