Dolan Chemical Laboratory

4001 Bixby Road

Groveport, OH 43125

T: 614-836-4221, Audinet 210-4221

F: 614-836-4168, Audinet 210-4168

http://aepenv/labs

Water Analysis

Form REP-703

Rev. 0, 4/2012

Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-001 Date Collected: 10/16/2013 Date Received: 10/16/2013

Field Blank 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Mercury, Hg < 0.2 ng/L U 0.5 0.2 JAB 10/18/2013 EPA 1631E

Sample Number: 134243-002 Date Collected: 10/16/2013 Date Received: 10/16/2013

CPS Influent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 9.82 ug/L 0.05 0.01 DPC 10/25/2013 14:28 EPA 200.8

Arsenic, As 74.5 ug/L 0.1 0.03 DPC 10/25/2013 14:28 EPA 200.8

Barium, Ba 797 ug/L 0.1 0.02 DPC 10/25/2013 14:28 EPA 200.8

Beryllium, Be < 20 ug/L U 50 20 DAM 10/24/2013 12:51 EPA 200.7

Cadmium, Cd 259 ug/L 0.05 0.01 DPC 10/25/2013 14:28 EPA 200.8

Chromium, Cr 221 ug/L 0.2 0.04 DPC 10/25/2013 14:28 EPA 200.8

Cobalt, Co 318 ug/L 0.02 0.004 DPC 10/25/2013 14:28 EPA 200.8

Copper, Cu 265 ug/L 0.05 0.01 DPC 10/25/2013 14:28 EPA 200.8

Lead, Pb 116 ug/L 0.01 0.002 DPC 10/25/2013 14:28 EPA 200.8

Mercury, Hg 256000 ng/L 5000 2000 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 313 ug/L 0.05 0.01 DPC 10/25/2013 14:28 EPA 200.8

Nickel, Ni 1930 ug/L 0.2 0.05 DPC 10/25/2013 14:28 EPA 200.8

Selenium, Se 800 ug/L 0.5 0.2 DPC 10/25/2013 14:28 EPA 200.8

Silver, Ag 0.215 ug/L 0.01 0.002 DPC 10/25/2013 14:28 EPA 200.8

Thallium, Tl 14.8 ug/L 0.05 0.002 DPC 10/25/2013 14:28 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 12:51 EPA 200.7

Titanium, Ti 112 ug/L 100 20 DAM 10/24/2013 12:51 EPA 200.7

Zinc, Zn 3070 ug/L 0.5 0.1 DPC 10/25/2013 14:28 EPA 200.8

Aluminum, Al 7.05 mg/L 0.001 0.0003 DPC 10/25/2013 14:28 EPA 200.8

Boron, B 453 mg/L 1 0.2 DAM 10/24/2013 12:51 EPA 200.7

Calcium, Ca 3730 mg/L 1 0.2 DAM 10/24/2013 12:51 EPA 200.7

Iron, Fe 67.4 mg/L 2 0.5 DAM 10/24/2013 12:51 EPA 200.7

Magnesium, Mg 4830 mg/L 0.5 0.1 DAM 10/24/2013 12:51 EPA 200.7

Manganese, Mn 91.0 mg/L 0.02 0.005 DAM 10/24/2013 12:51 EPA 200.7

Potassium, K 79.7 mg/L 2 0.4 DAM 10/24/2013 12:50 EPA 200.7

Sodium, Na 399 mg/L 2 0.4 DAM 10/24/2013 12:50 EPA 200.7

Strontium, Sr 22.2 mg/L 0.05 0.02 DAM 10/24/2013 12:50 EPA 200.7

Ammonia, NH3, as N < 0.02 mg/L U 0.05 0.02 DMM 11/01/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 14.1 mg/L 5 1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 37.1 mg/L 0.1 0.02 DMM 10/24/2013 SM20 4500NO3 H

Mountaineer Plant, 134243 Page 1 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-002A Date Collected: 10/16/2013 Date Received: 10/16/2013

CPS Influent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 3.04 ug/L 0.05 0.01 DPC 10/25/2013 14:33 EPA 200.8

Arsenic, As 3.65 ug/L 0.1 0.03 DPC 10/25/2013 14:33 EPA 200.8

Barium, Ba 47.4 ug/L 0.1 0.02 DPC 10/25/2013 14:33 EPA 200.8

Beryllium, Be < 20 ug/L U 50 20 DAM 10/24/2013 12:55 EPA 200.7

Cadmium, Cd 164 ug/L 0.05 0.01 DPC 10/25/2013 14:33 EPA 200.8

Chromium, Cr 0.6 ug/L 0.2 0.04 DPC 10/25/2013 14:33 EPA 200.8

Cobalt, Co 244 ug/L 0.02 0.004 DPC 10/25/2013 14:33 EPA 200.8

Copper, Cu 6.66 ug/L 0.05 0.01 DPC 10/25/2013 14:33 EPA 200.8

Lead, Pb 0.154 ug/L 0.01 0.002 DPC 10/25/2013 14:33 EPA 200.8

Mercury, Hg 148 ng/L 10 4 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 287 ug/L 0.05 0.01 DPC 10/25/2013 14:33 EPA 200.8

Nickel, Ni 1510 ug/L 0.2 0.05 DPC 10/25/2013 14:33 EPA 200.8

Selenium, Se 424 ug/L 0.5 0.2 DPC 10/25/2013 14:33 EPA 200.8

Selenite, Se+4 (Hydride) 284 ug/L 20 4 TLT 11/01/2013 AEP Method

Silver, Ag 0.011 ug/L 0.01 0.002 DPC 10/25/2013 14:33 EPA 200.8

Thallium, Tl 8.63 ug/L 0.05 0.002 DPC 10/25/2013 14:33 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 12:55 EPA 200.7

Titanium, Ti < 20 ug/L U 100 20 DAM 10/24/2013 12:55 EPA 200.7

Zinc, Zn 653 ug/L 0.5 0.1 DPC 10/25/2013 14:33 EPA 200.8

Aluminum, Al 0.346 mg/L 0.001 0.0003 DPC 10/25/2013 14:33 EPA 200.8

Boron, B 469 mg/L 1 0.2 DAM 10/24/2013 12:55 EPA 200.7

Calcium, Ca 662 mg/L 1 0.2 DAM 10/24/2013 12:55 EPA 200.7

Iron, Fe < 0.5 mg/L U 2 0.5 DAM 10/24/2013 12:55 EPA 200.7

Magnesium, Mg 4680 mg/L 0.5 0.1 DAM 10/24/2013 12:55 EPA 200.7

Manganese, Mn 88.4 mg/L 0.02 0.005 DAM 10/24/2013 12:55 EPA 200.7

Potassium, K 79.6 mg/L 2 0.4 DAM 10/24/2013 12:54 EPA 200.7

Sodium, Na 408 mg/L 2 0.4 DAM 10/24/2013 12:54 EPA 200.7

Strontium, Sr 10.2 mg/L 0.05 0.02 DAM 10/24/2013 12:54 EPA 200.7

Mountaineer Plant, 134243 Page 2 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-003 Date Collected: 10/16/2013 Date Received: 10/16/2013

Primary Clarifier Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.66 ug/L 0.05 0.01 DPC 10/25/2013 16:36 EPA 200.8

Arsenic, As 3.84 ug/L 0.1 0.03 DPC 10/25/2013 16:36 EPA 200.8

Barium, Ba 52.1 ug/L 0.1 0.02 DPC 10/25/2013 16:36 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 12:59 EPA 200.7

Cadmium, Cd 76.5 ug/L 0.05 0.01 DPC 10/25/2013 16:36 EPA 200.8

Chromium, Cr 7.2 ug/L 0.2 0.04 DPC 10/25/2013 16:36 EPA 200.8

Cobalt, Co 156 ug/L 0.02 0.004 DPC 10/25/2013 16:36 EPA 200.8

Copper, Cu 5.30 ug/L 0.05 0.01 DPC 10/25/2013 16:36 EPA 200.8

Lead, Pb 1.33 ug/L 0.01 0.002 DPC 10/25/2013 16:36 EPA 200.8

Mercury, Hg 1150 ng/L 50 20 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 284 ug/L 0.05 0.01 DPC 10/25/2013 16:36 EPA 200.8

Nickel, Ni 975 ug/L 0.2 0.05 DPC 10/25/2013 16:36 EPA 200.8

Selenium, Se 419 ug/L 0.5 0.2 DPC 10/25/2013 16:36 EPA 200.8

Silver, Ag 0.011 ug/L 0.01 0.002 DPC 10/25/2013 16:36 EPA 200.8

Thallium, Tl 7.26 ug/L 0.05 0.002 DPC 10/25/2013 16:36 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 12:59 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 12:59 EPA 200.7

Zinc, Zn 125 ug/L 0.5 0.1 DPC 10/25/2013 16:36 EPA 200.8

Aluminum, Al 0.302 mg/L 0.001 0.0003 DPC 10/25/2013 16:36 EPA 200.8

Boron, B 356 mg/L 0.2 0.04 DAM 10/24/2013 12:59 EPA 200.7

Calcium, Ca 657 mg/L 0.2 0.04 DAM 10/24/2013 12:59 EPA 200.7

Iron, Fe 1.19 mg/L 0.5 0.1 DAM 10/24/2013 12:59 EPA 200.7

Magnesium, Mg 3670 mg/L 0.1 0.02 DAM 10/24/2013 12:59 EPA 200.7

Manganese, Mn 61.9 mg/L 0.005 0.001 DAM 10/24/2013 12:59 EPA 200.7

Potassium, K 60.3 mg/L 0.5 0.07 DAM 10/24/2013 12:58 EPA 200.7

Sodium, Na 325 mg/L 0.3 0.08 DAM 10/24/2013 12:58 EPA 200.7

Strontium, Sr 8.02 mg/L 0.01 0.003 DAM 10/24/2013 12:58 EPA 200.7

Ammonia, NH3, as N 1.90 mg/L 0.05 0.02 DMM 11/01/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 7.84 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 31.4 mg/L 0.1 0.02 DMM 10/24/2013 SM20 4500NO3 H

Mountaineer Plant, 134243 Page 3 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-003A Date Collected: 10/16/2013 Date Received: 10/16/2013

Primary Clarifier Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.35 ug/L 0.05 0.01 DPC 10/25/2013 16:16 EPA 200.8

Arsenic, As 3.06 ug/L 0.1 0.03 DPC 10/25/2013 16:16 EPA 200.8

Barium, Ba 47.1 ug/L 0.1 0.02 DPC 10/25/2013 16:16 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:08 EPA 200.7

Cadmium, Cd 71.3 ug/L 0.05 0.01 DPC 10/25/2013 16:16 EPA 200.8

Chromium, Cr 1.9 ug/L 0.2 0.04 DPC 10/25/2013 16:16 EPA 200.8

Cobalt, Co 145 ug/L 0.02 0.004 DPC 10/25/2013 16:16 EPA 200.8

Copper, Cu 2.71 ug/L 0.05 0.01 DPC 10/25/2013 16:16 EPA 200.8

Lead, Pb 0.018 ug/L 0.01 0.002 DPC 10/25/2013 16:16 EPA 200.8

Mercury, Hg 47.0 ng/L 5 2 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 267 ug/L 0.05 0.01 DPC 10/25/2013 16:16 EPA 200.8

Nickel, Ni 913 ug/L 0.2 0.05 DPC 10/25/2013 16:16 EPA 200.8

Selenium, Se 385 ug/L 0.5 0.2 DPC 10/25/2013 16:16 EPA 200.8

Selenite, Se+4 (Hydride) 309 ug/L 20 4 TLT 11/01/2013 AEP Method

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 10/25/2013 16:16 EPA 200.8

Thallium, Tl 6.79 ug/L 0.05 0.002 DPC 10/25/2013 16:16 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:09 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:09 EPA 200.7

Zinc, Zn 116 ug/L 0.5 0.1 DPC 10/25/2013 16:16 EPA 200.8

Aluminum, Al 0.0288 mg/L 0.001 0.0003 DPC 10/25/2013 16:16 EPA 200.8

Boron, B 359 mg/L 0.2 0.04 DAM 10/24/2013 13:08 EPA 200.7

Calcium, Ca 661 mg/L 0.2 0.04 DAM 10/24/2013 13:08 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 10/24/2013 13:09 EPA 200.7

Magnesium, Mg 3690 mg/L 0.1 0.02 DAM 10/24/2013 13:08 EPA 200.7

Manganese, Mn 62.3 mg/L 0.005 0.001 DAM 10/24/2013 13:08 EPA 200.7

Potassium, K 60.7 mg/L 0.5 0.07 DAM 10/24/2013 13:07 EPA 200.7

Sodium, Na 328 mg/L 0.3 0.08 DAM 10/24/2013 13:07 EPA 200.7

Strontium, Sr 8.02 mg/L 0.01 0.003 DAM 10/24/2013 13:07 EPA 200.7

Mountaineer Plant, 134243 Page 4 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-004 Date Collected: 10/16/2013 Date Received: 10/16/2013

Landfill Leachate 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 12.8 ug/L 0.05 0.01 DPC 10/28/2013 10:59 EPA 200.8

Arsenic, As 44.8 ug/L 0.1 0.03 DPC 10/28/2013 10:59 EPA 200.8

Barium, Ba 24.8 ug/L 0.1 0.02 DPC 10/28/2013 10:59 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:17 EPA 200.7

Cadmium, Cd 0.90 ug/L 0.05 0.01 DPC 10/28/2013 10:59 EPA 200.8

Chromium, Cr 0.4 ug/L 0.2 0.04 DPC 10/28/2013 10:59 EPA 200.8

Cobalt, Co 2.90 ug/L 0.02 0.004 DPC 10/28/2013 10:59 EPA 200.8

Copper, Cu 0.35 ug/L 0.05 0.01 DPC 10/28/2013 10:59 EPA 200.8

Lead, Pb 0.022 ug/L 0.01 0.002 DPC 10/28/2013 10:59 EPA 200.8

Mercury, Hg 50.9 ng/L 10 4 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 8040 ug/L 0.05 0.01 DPC 10/28/2013 10:59 EPA 200.8

Nickel, Ni 8.50 ug/L 0.2 0.05 DPC 10/28/2013 10:59 EPA 200.8

Selenium, Se 280 ug/L 0.5 0.2 DPC 10/28/2013 10:59 EPA 200.8

Silver, Ag 0.004 ug/L J 0.01 0.002 DPC 10/28/2013 10:59 EPA 200.8

Thallium, Tl 3.68 ug/L 0.05 0.002 DPC 10/28/2013 10:59 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:18 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:18 EPA 200.7

Zinc, Zn 2.9 ug/L 0.5 0.1 DPC 10/28/2013 10:59 EPA 200.8

Aluminum, Al 0.0183 mg/L 0.001 0.0003 DPC 10/28/2013 10:59 EPA 200.8

Boron, B 65.0 mg/L 0.2 0.04 DAM 10/24/2013 13:17 EPA 200.7

Calcium, Ca 483 mg/L 0.2 0.04 DAM 10/24/2013 13:17 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 10/24/2013 13:18 EPA 200.7

Magnesium, Mg 477 mg/L 0.1 0.02 DAM 10/24/2013 13:17 EPA 200.7

Manganese, Mn 1.43 mg/L 0.005 0.001 DAM 10/24/2013 13:17 EPA 200.7

Potassium, K 133 mg/L 0.5 0.07 DAM 10/24/2013 13:16 EPA 200.7

Sodium, Na 2210 mg/L 0.3 0.08 DAM 10/24/2013 13:16 EPA 200.7

Strontium, Sr 6.64 mg/L 0.01 0.003 DAM 10/24/2013 13:16 EPA 200.7

Ammonia, NH3, as N 0.09 mg/L 0.05 0.02 DMM 11/01/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 0.96 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 7.40 mg/L 0.1 0.02 DMM 10/24/2013 SM20 4500NO3 H

Mountaineer Plant, 134243 Page 5 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-004A Date Collected: 10/16/2013 Date Received: 10/16/2013

Landfill Leachate Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.2 ug/L 0.05 0.01 DPC 10/28/2013 11:04 EPA 200.8

Arsenic, As 37.5 ug/L 0.1 0.03 DPC 10/28/2013 11:04 EPA 200.8

Barium, Ba 19.6 ug/L 0.1 0.02 DPC 10/28/2013 11:04 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:29 EPA 200.7

Cadmium, Cd 0.78 ug/L 0.05 0.01 DPC 10/28/2013 11:04 EPA 200.8

Chromium, Cr 0.3 ug/L 0.2 0.04 DPC 10/28/2013 11:04 EPA 200.8

Cobalt, Co 1.93 ug/L 0.02 0.004 DPC 10/28/2013 11:04 EPA 200.8

Copper, Cu 0.30 ug/L 0.05 0.01 DPC 10/28/2013 11:04 EPA 200.8

Lead, Pb 0.054 ug/L 0.01 0.002 DPC 10/28/2013 11:04 EPA 200.8

Mercury, Hg 2.6 ng/L 2 0.8 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 7010 ug/L 0.05 0.01 DPC 10/28/2013 11:04 EPA 200.8

Nickel, Ni 7.48 ug/L 0.2 0.05 DPC 10/28/2013 11:04 EPA 200.8

Selenium, Se 247 ug/L 0.5 0.2 DPC 10/28/2013 11:04 EPA 200.8

Selenite, Se+4 (Hydride) 177 ug/L 20 4 TLT 11/08/2013 AEP Method

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 10/28/2013 11:04 EPA 200.8

Thallium, Tl 3.11 ug/L 0.05 0.002 DPC 10/28/2013 11:04 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:30 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:30 EPA 200.7

Zinc, Zn 8.4 ug/L 0.5 0.1 DPC 10/28/2013 11:04 EPA 200.8

Aluminum, Al 0.0059 mg/L 0.001 0.0003 DPC 10/28/2013 11:04 EPA 200.8

Boron, B 62.7 mg/L 0.2 0.04 DAM 10/24/2013 13:29 EPA 200.7

Calcium, Ca 458 mg/L 0.2 0.04 DAM 10/24/2013 13:29 EPA 200.7

Iron, Fe < 0.1 mg/L U 0.5 0.1 DAM 10/24/2013 13:30 EPA 200.7

Magnesium, Mg 453 mg/L 0.1 0.02 DAM 10/24/2013 13:29 EPA 200.7

Manganese, Mn 1.06 mg/L 0.005 0.001 DAM 10/24/2013 13:29 EPA 200.7

Potassium, K 127 mg/L 0.5 0.07 DAM 10/24/2013 13:28 EPA 200.7

Sodium, Na 2110 mg/L 0.3 0.08 DAM 10/24/2013 13:28 EPA 200.7

Strontium, Sr 6.28 mg/L 0.01 0.003 DAM 10/24/2013 13:28 EPA 200.7

Mountaineer Plant, 134243 Page 6 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-005 Date Collected: 10/16/2013 Date Received: 10/16/2013

1st Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 14.8 ug/L 0.05 0.01 DPC 10/28/2013 11:09 EPA 200.8

Arsenic, As 51.2 ug/L 0.1 0.03 DPC 10/28/2013 11:09 EPA 200.8

Barium, Ba 27.1 ug/L 0.1 0.02 DPC 10/28/2013 11:09 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:33 EPA 200.7

Cadmium, Cd 0.98 ug/L 0.05 0.01 DPC 10/28/2013 11:09 EPA 200.8

Chromium, Cr 0.9 ug/L 0.2 0.04 DPC 10/28/2013 11:09 EPA 200.8

Cobalt, Co 3.04 ug/L 0.02 0.004 DPC 10/28/2013 11:09 EPA 200.8

Copper, Cu 0.50 ug/L 0.05 0.01 DPC 10/28/2013 11:09 EPA 200.8

Lead, Pb 0.024 ug/L 0.01 0.002 DPC 10/28/2013 11:09 EPA 200.8

Mercury, Hg 51.6 ng/L 10 4 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 9070 ug/L 0.05 0.01 DPC 10/28/2013 11:09 EPA 200.8

Nickel, Ni 9.82 ug/L 0.2 0.05 DPC 10/28/2013 11:09 EPA 200.8

Selenium, Se 317 ug/L 0.5 0.2 DPC 10/28/2013 11:09 EPA 200.8

Silver, Ag 0.004 ug/L J 0.01 0.002 DPC 10/28/2013 11:09 EPA 200.8

Thallium, Tl 4.07 ug/L 0.05 0.002 DPC 10/28/2013 11:09 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:34 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:34 EPA 200.7

Zinc, Zn 3.2 ug/L 0.5 0.1 DPC 10/28/2013 11:09 EPA 200.8

Aluminum, Al 0.0204 mg/L 0.001 0.0003 DPC 10/28/2013 11:09 EPA 200.8

Boron, B 66.1 mg/L 0.2 0.04 DAM 10/24/2013 13:33 EPA 200.7

Calcium, Ca 490 mg/L 0.2 0.04 DAM 10/24/2013 13:33 EPA 200.7

Iron, Fe 0.668 mg/L 0.5 0.1 DAM 10/24/2013 13:34 EPA 200.7

Magnesium, Mg 484 mg/L 0.1 0.02 DAM 10/24/2013 13:33 EPA 200.7

Manganese, Mn 1.41 mg/L 0.005 0.001 DAM 10/24/2013 13:33 EPA 200.7

Potassium, K 134 mg/L 0.5 0.07 DAM 10/24/2013 13:32 EPA 200.7

Sodium, Na 2230 mg/L 0.3 0.08 DAM 10/24/2013 13:32 EPA 200.7

Strontium, Sr 6.68 mg/L 0.01 0.003 DAM 10/24/2013 13:32 EPA 200.7

Ammonia, NH3, as N 0.11 mg/L 0.05 0.02 DMM 11/01/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 1.56 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 6.37 mg/L 0.1 0.02 DMM 10/24/2013 SM20 4500NO3 H

Mountaineer Plant, 134243 Page 7 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-005A Date Collected: 10/16/2013 Date Received: 10/16/2013

1st Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 11.3 ug/L 0.05 0.01 DPC 10/28/2013 11:14 EPA 200.8

Arsenic, As 23.7 ug/L 0.1 0.03 DPC 10/28/2013 11:14 EPA 200.8

Barium, Ba 20.5 ug/L 0.1 0.02 DPC 10/28/2013 11:14 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:38 EPA 200.7

Cadmium, Cd 1.04 ug/L 0.05 0.01 DPC 10/28/2013 11:14 EPA 200.8

Chromium, Cr 0.2 ug/L 0.2 0.04 DPC 10/28/2013 11:14 EPA 200.8

Cobalt, Co 2.34 ug/L 0.02 0.004 DPC 10/28/2013 11:14 EPA 200.8

Copper, Cu 0.18 ug/L 0.05 0.01 DPC 10/28/2013 11:14 EPA 200.8

Lead, Pb 0.016 ug/L 0.01 0.002 DPC 10/28/2013 11:14 EPA 200.8

Mercury, Hg 3.0 ng/L 2 0.8 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 7150 ug/L 0.05 0.01 DPC 10/28/2013 11:14 EPA 200.8

Nickel, Ni 7.57 ug/L 0.2 0.05 DPC 10/28/2013 11:14 EPA 200.8

Selenium, Se 242 ug/L 0.5 0.2 DPC 10/28/2013 11:14 EPA 200.8

Selenite, Se+4 (Hydride) 169 ug/L 20 4 TLT 11/08/2013 AEP Method

Silver, Ag 0.004 ug/L J 0.01 0.002 DPC 10/28/2013 11:14 EPA 200.8

Thallium, Tl 3.20 ug/L 0.05 0.002 DPC 10/28/2013 11:14 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:38 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:38 EPA 200.7

Zinc, Zn 2.9 ug/L 0.5 0.1 DPC 10/28/2013 11:14 EPA 200.8

Aluminum, Al 0.0065 mg/L 0.001 0.0003 DPC 10/28/2013 11:14 EPA 200.8

Boron, B 65.5 mg/L 0.2 0.04 DAM 10/24/2013 13:38 EPA 200.7

Calcium, Ca 484 mg/L 0.2 0.04 DAM 10/24/2013 13:38 EPA 200.7

Iron, Fe 0.1 mg/L J 0.5 0.1 DAM 10/24/2013 13:38 EPA 200.7

Magnesium, Mg 478 mg/L 0.1 0.02 DAM 10/24/2013 13:38 EPA 200.7

Manganese, Mn 1.36 mg/L 0.005 0.001 DAM 10/24/2013 13:38 EPA 200.7

Potassium, K 134 mg/L 0.5 0.07 DAM 10/24/2013 13:36 EPA 200.7

Sodium, Na 2230 mg/L 0.3 0.08 DAM 10/24/2013 13:36 EPA 200.7

Strontium, Sr 6.68 mg/L 0.01 0.003 DAM 10/24/2013 13:36 EPA 200.7

Mountaineer Plant, 134243 Page 8 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-006 Date Collected: 10/16/2013 Date Received: 10/16/2013

2nd Stage Feed 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.43 ug/L 0.05 0.01 DPC 10/28/2013 11:19 EPA 200.8

Arsenic, As 11.4 ug/L 0.1 0.03 DPC 10/28/2013 11:19 EPA 200.8

Barium, Ba 24.2 ug/L 0.1 0.02 DPC 10/28/2013 11:19 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:42 EPA 200.7

Cadmium, Cd 0.77 ug/L 0.05 0.01 DPC 10/28/2013 11:19 EPA 200.8

Chromium, Cr 0.7 ug/L 0.2 0.04 DPC 10/28/2013 11:19 EPA 200.8

Cobalt, Co 3.03 ug/L 0.02 0.004 DPC 10/28/2013 11:19 EPA 200.8

Copper, Cu 0.11 ug/L 0.05 0.01 DPC 10/28/2013 11:19 EPA 200.8

Lead, Pb 0.014 ug/L 0.01 0.002 DPC 10/28/2013 11:19 EPA 200.8

Mercury, Hg 12.8 ng/L 2 0.8 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 7150 ug/L 0.05 0.01 DPC 10/28/2013 11:19 EPA 200.8

Nickel, Ni 32.7 ug/L 0.2 0.05 DPC 10/28/2013 11:19 EPA 200.8

Selenium, Se 9.4 ug/L 0.5 0.2 DPC 10/28/2013 11:19 EPA 200.8

Silver, Ag < 0.002 ug/L U 0.01 0.002 DPC 10/28/2013 11:19 EPA 200.8

Thallium, Tl 0.25 ug/L 0.05 0.002 DPC 10/28/2013 11:19 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:42 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:42 EPA 200.7

Zinc, Zn 1.8 ug/L 0.5 0.1 DPC 10/28/2013 11:19 EPA 200.8

Aluminum, Al 0.157 mg/L 0.001 0.0003 DPC 10/28/2013 11:19 EPA 200.8

Boron, B 64.0 mg/L 0.2 0.04 DAM 10/24/2013 13:42 EPA 200.7

Calcium, Ca 444 mg/L 0.2 0.04 DAM 10/24/2013 13:42 EPA 200.7

Iron, Fe 0.798 mg/L 0.5 0.1 DAM 10/24/2013 13:42 EPA 200.7

Magnesium, Mg 450 mg/L 0.1 0.02 DAM 10/24/2013 13:42 EPA 200.7

Manganese, Mn 2.07 mg/L 0.005 0.001 DAM 10/24/2013 13:42 EPA 200.7

Potassium, K 125 mg/L 0.5 0.07 DAM 10/24/2013 13:40 EPA 200.7

Sodium, Na 2080 mg/L 0.3 0.08 DAM 10/24/2013 13:40 EPA 200.7

Strontium, Sr 6.08 mg/L 0.01 0.003 DAM 10/24/2013 13:40 EPA 200.7

Ammonia, NH3, as N 0.64 mg/L 0.05 0.02 DMM 11/01/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 3.30 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N < 0.02 mg/L U 0.1 0.02 DMM 10/24/2013 SM20 4500NO3 H

Mountaineer Plant, 134243 Page 9 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-006A Date Collected: 10/16/2013 Date Received: 10/16/2013

2nd Stage Feed Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 2.36 ug/L 0.05 0.01 DPC 10/28/2013 11:24 EPA 200.8

Arsenic, As 10.5 ug/L 0.1 0.03 DPC 10/28/2013 11:24 EPA 200.8

Barium, Ba 24.2 ug/L 0.1 0.02 DPC 10/28/2013 11:24 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 13:46 EPA 200.7

Cadmium, Cd 0.71 ug/L 0.05 0.01 DPC 10/28/2013 11:24 EPA 200.8

Chromium, Cr 0.6 ug/L 0.2 0.04 DPC 10/28/2013 11:24 EPA 200.8

Cobalt, Co 2.91 ug/L 0.02 0.004 DPC 10/28/2013 11:24 EPA 200.8

Copper, Cu 0.14 ug/L 0.05 0.01 DPC 10/28/2013 11:24 EPA 200.8

Lead, Pb 0.029 ug/L 0.01 0.002 DPC 10/28/2013 11:24 EPA 200.8

Mercury, Hg 2.9 ng/L 1 0.4 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 7080 ug/L 0.05 0.01 DPC 10/28/2013 11:24 EPA 200.8

Nickel, Ni 33.0 ug/L 0.2 0.05 DPC 10/28/2013 11:24 EPA 200.8

Selenium, Se 4.3 ug/L 0.5 0.2 DPC 10/28/2013 11:24 EPA 200.8

Selenite, Se+4 (Hydride) 2.5 ug/L 2 0.4 TLT 11/08/2013 AEP Method

Silver, Ag 0.002 ug/L J 0.01 0.002 DPC 10/28/2013 11:24 EPA 200.8

Thallium, Tl 0.26 ug/L 0.05 0.002 DPC 10/28/2013 11:24 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 13:46 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 13:46 EPA 200.7

Zinc, Zn 7.5 ug/L 0.5 0.1 DPC 10/28/2013 11:24 EPA 200.8

Aluminum, Al 0.150 mg/L 0.001 0.0003 DPC 10/28/2013 11:24 EPA 200.8

Boron, B 66.9 mg/L 0.2 0.04 DAM 10/24/2013 13:46 EPA 200.7

Calcium, Ca 466 mg/L 0.2 0.04 DAM 10/24/2013 13:46 EPA 200.7

Iron, Fe 0.721 mg/L 0.5 0.1 DAM 10/24/2013 13:46 EPA 200.7

Magnesium, Mg 474 mg/L 0.1 0.02 DAM 10/24/2013 13:46 EPA 200.7

Manganese, Mn 2.17 mg/L 0.005 0.001 DAM 10/24/2013 13:46 EPA 200.7

Potassium, K 132 mg/L 0.5 0.07 DAM 10/24/2013 13:44 EPA 200.7

Sodium, Na 2180 mg/L 0.3 0.08 DAM 10/24/2013 13:44 EPA 200.7

Strontium, Sr 6.36 mg/L 0.01 0.003 DAM 10/24/2013 13:44 EPA 200.7

Mountaineer Plant, 134243 Page 10 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-007 Date Collected: 10/16/2013 Date Received: 10/16/2013

Bioreactor Effluent 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.09 ug/L 0.05 0.01 DPC 10/28/2013 11:29 EPA 200.8

Arsenic, As 0.36 ug/L 0.1 0.03 DPC 10/28/2013 11:29 EPA 200.8

Barium, Ba 33.6 ug/L 0.1 0.02 DPC 10/28/2013 11:29 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 14:03 EPA 200.7

Cadmium, Cd 0.07 ug/L 0.05 0.01 DPC 10/28/2013 11:29 EPA 200.8

Chromium, Cr 0.4 ug/L 0.2 0.04 DPC 10/28/2013 11:29 EPA 200.8

Cobalt, Co 0.080 ug/L 0.02 0.004 DPC 10/28/2013 11:29 EPA 200.8

Copper, Cu 0.11 ug/L 0.05 0.01 DPC 10/28/2013 11:29 EPA 200.8

Lead, Pb 0.012 ug/L 0.01 0.002 DPC 10/28/2013 11:29 EPA 200.8

Mercury, Hg 2.7 ng/L 1 0.4 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 954 ug/L 0.05 0.01 DPC 10/28/2013 11:29 EPA 200.8

Nickel, Ni 1.91 ug/L 0.2 0.05 DPC 10/28/2013 11:29 EPA 200.8

Selenium, Se 1.0 ug/L 0.5 0.2 DPC 10/28/2013 11:29 EPA 200.8

Silver, Ag < 0.002 ug/L U 0.01 0.002 DPC 10/28/2013 11:29 EPA 200.8

Thallium, Tl 0.006 ug/L J 0.05 0.002 DPC 10/28/2013 11:29 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 14:03 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 14:03 EPA 200.7

Zinc, Zn 2.2 ug/L 0.5 0.1 DPC 10/28/2013 11:29 EPA 200.8

Aluminum, Al 0.283 mg/L 0.001 0.0003 DPC 10/28/2013 11:29 EPA 200.8

Boron, B 68.2 mg/L 0.2 0.04 DAM 10/24/2013 14:03 EPA 200.7

Calcium, Ca 422 mg/L 0.2 0.04 DAM 10/24/2013 14:03 EPA 200.7

Iron, Fe 0.4 mg/L J 0.5 0.1 DAM 10/24/2013 14:03 EPA 200.7

Magnesium, Mg 451 mg/L 0.1 0.02 DAM 10/24/2013 14:03 EPA 200.7

Manganese, Mn 4.91 mg/L 0.005 0.001 DAM 10/24/2013 14:03 EPA 200.7

Potassium, K 122 mg/L 0.5 0.07 DAM 10/24/2013 14:01 EPA 200.7

Sodium, Na 2020 mg/L 0.3 0.08 DAM 10/24/2013 14:01 EPA 200.7

Strontium, Sr 5.68 mg/L 0.01 0.003 DAM 10/24/2013 14:01 EPA 200.7

Ammonia, NH3, as N 2.12 mg/L 0.05 0.02 DMM 11/01/2013 EPA 350.1

Total Kjeldahl Nitrogen, TKN as N 2.99 mg/L 0.5 0.1 DMM 10/29/2013 EPA 351.2

Nitrate-Nitrite, NO3-NO2, as N 0.58 mg/L 0.1 0.02 DMM 10/24/2013 SM20 4500NO3 H

Mountaineer Plant, 134243 Page 11 of 12
Location: Mountaineer Plant Report Date: 11/11/2013

Sample Number: 134243-007A Date Collected: 10/16/2013 Date Received: 10/16/2013

Bioreactor Effluent Dissolved 

Parameter Result Units RL MDL Analysis By Analysis Date/Time Method

Data 

Qual

Antimony, Sb 0.07 ug/L 0.05 0.01 DPC 10/28/2013 11:34 EPA 200.8

Arsenic, As 0.36 ug/L 0.1 0.03 DPC 10/28/2013 11:34 EPA 200.8

Barium, Ba 31.5 ug/L 0.1 0.02 DPC 10/28/2013 11:34 EPA 200.8

Beryllium, Be < 3 ug/L U 10 3 DAM 10/24/2013 14:07 EPA 200.7

Cadmium, Cd 0.04 ug/L J 0.05 0.01 DPC 10/28/2013 11:34 EPA 200.8

Chromium, Cr 0.4 ug/L 0.2 0.04 DPC 10/28/2013 11:34 EPA 200.8

Cobalt, Co 0.042 ug/L 0.02 0.004 DPC 10/28/2013 11:34 EPA 200.8

Copper, Cu 0.03 ug/L J 0.05 0.01 DPC 10/28/2013 11:34 EPA 200.8

Lead, Pb 0.005 ug/L J 0.01 0.002 DPC 10/28/2013 11:34 EPA 200.8

Mercury, Hg 1.3 ng/L 0.5 0.2 JAB 10/18/2013 EPA 1631E

Molybdenum, Mo 897 ug/L 0.05 0.01 DPC 10/28/2013 11:34 EPA 200.8

Nickel, Ni 1.85 ug/L 0.2 0.05 DPC 10/28/2013 11:34 EPA 200.8

Selenium, Se 0.8 ug/L 0.5 0.2 DPC 10/28/2013 11:34 EPA 200.8

Selenite, Se+4 (Hydride) < 0.08 ug/L U 0.4 0.08 TLT 11/08/2013 AEP Method

Silver, Ag < 0.002 ug/L U 0.01 0.002 DPC 10/28/2013 11:34 EPA 200.8

Thallium, Tl 0.003 ug/L J 0.05 0.002 DPC 10/28/2013 11:34 EPA 200.8

Tin, Sn < 30 ug/L U 100 30 DAM 10/24/2013 14:07 EPA 200.7

Titanium, Ti < 3 ug/L U 20 3 DAM 10/24/2013 14:07 EPA 200.7

Zinc, Zn 3.1 ug/L 0.5 0.1 DPC 10/28/2013 11:34 EPA 200.8

Aluminum, Al 0.270 mg/L 0.001 0.0003 DPC 10/28/2013 11:34 EPA 200.8

Boron, B 71.0 mg/L 0.2 0.04 DAM 10/24/2013 14:07 EPA 200.7

Calcium, Ca 443 mg/L 0.2 0.04 DAM 10/24/2013 14:07 EPA 200.7

Iron, Fe 0.4 mg/L J 0.5 0.1 DAM 10/24/2013 14:07 EPA 200.7

Magnesium, Mg 474 mg/L 0.1 0.02 DAM 10/24/2013 14:07 EPA 200.7

Manganese, Mn 5.11 mg/L 0.005 0.001 DAM 10/24/2013 14:07 EPA 200.7

Potassium, K 126 mg/L 0.5 0.07 DAM 10/24/2013 14:05 EPA 200.7

Sodium, Na 2090 mg/L 0.3 0.08 DAM 10/24/2013 14:05 EPA 200.7

Strontium, Sr 5.92 mg/L 0.01 0.003 DAM 10/24/2013 14:05 EPA 200.7

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN 

APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, 

UNLESS OTHERWISE NOTED.

U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit

J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II

Email bssnyder@aep.com Tel. 614-836-4224

Fax 614-836-4168 Audinet 210-4224

Mountaineer Plant, 134243 Page 12 of 12