Dry Scrubber Blue Goose Combustion Data Septem ber 2011 Fyrite

Location : Dry

Scrubber Date 9/25/12 Time: 13:09

run O2 CO2

1 18 3 2 18 3 3 18 3
Avg 18 3

Molecular wt

1 29.2 2 29.2 3 29.2

AVG 29.2

diff 0

0 0

All diff must be less that 0.3
Analysts: O'Brien &Gere

Page 1Test ID: 9-25-12-POM-ABF Run#1 

### Value 0.0001 0 0.0001

130.00 200.00 0.0022 0.0001 0.0000 200.00 200.00 0.002135

185.00 360.00 0.0021 0.0020075

1200.00 1000.00 0.0004 0 0.00040



### Value 2.4075 2.2350 4.6425 Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #1** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/25/2012

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml) Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)Test ID: 9-25-12-POM-ABF Run#1



### Value 0.6542 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 3.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.2 28.8092602 0.034887482 543.5 642.4 29.9 58 1.55 1.044 29.9 128 1.18 81.383 63.5 29.91 0.25 0.00034088462



### Value 82.7249647 40.55859 45.4 2.13698 18.1 0.853415 0.034887 0.040170 98.2486 Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #1**  **9/25/2012**

**Method 5 Parameter**  p = Stack gas v elocity pressure (av g. sqrt  p - in. water) Cp = Pitot tube calibration coefficient

Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute average temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg)

I = % Isokinetic variation



### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moistureTest ID: 9-25-12-POM-ABF Run#1 LIMS ID#: 2012010668



### Value 2.4075 0.0024075 2.235 0.002235 82.72496472 29.9 38.48 8.23 Green Carbon Baked tons/hr 0.034887482 74255.78993 4455347.3957 93641.67202 Acfm 76940.03398 Scfm 0.0009 Emission Rate of Total MCEM gr/dscf 0.29 6.85 0.2651 6.36 **0.55**

**0.035 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon Baked**  **0.032 Emission Rate of Particulate MCEM lb/Ton of Green Carbon Baked**  **0.067 Emission Rate of Total MCEM lb/Ton of Green Carbon Baked** 

Start time: 12.30 pm End time: 2.56 pm

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #1**  **9/25/2012**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

## Value 3.8

0.0038 82.72496472 29.9 38.48 8.23 Green Carbon produced tons/hr 0.034887482 74230.9635 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 4453857.811 0.0007 Particulate gr/dscf **0.45 Particulate lb/hr** 

**0.055 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Emission Calculations Test #1 9/25/2012** 

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions