ELECTRONIC CODE OF FEDERAL REGULATIONS

e-CFR data is current as of December 1, 2015

Title 40 → Chapter I → Subchapter E → Part 180

Title 40: Protection of Environment 

PART 180—TOLERANCES AND EXEMPTIONS FOR PESTICIDE CHEMICAL RESIDUES IN FOOD

Contents

Subpart A—Definitions and Interpretative Regulations

§180.1 Definitions and interpretations.

§180.3 Tolerances for related pesticide chemicals.

§180.4 Exceptions.

§180.5 Zero tolerances.

§180.6 Pesticide tolerances regarding milk, eggs, meat, and/or poultry; statement of policy.

Subpart B—Procedural Regulations

§180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on raw agricultural commodities or 

processed foods.

§180.8 Withdrawal of petitions without prejudice.

§180.9 Substantive amendments to petitions.

§180.29 Establishment, modification, and revocation of tolerance on initiative of Administrator.

§180.30 Judicial review.

§180.31 Temporary tolerances.

§180.32 Procedure for modifying and revoking tolerances or exemptions from tolerances.

§180.33 Fees.

§180.34 Tests on the amount of residue remaining.

§180.35 Tests for potentiation.

§180.40 Tolerances for crop groups.

§180.41 Crop group tables.

Subpart C—Specific Tolerances

§180.101 Specific tolerances; general provisions.

§180.103 Captan; tolerances for residues.

§180.106 Diuron; tolerances for residues.

§180.108 Acephate; tolerances for residues.

§180.111 Malathion; tolerances for residues.

§180.114 Ferbam; tolerances for residues.

§180.116 Ziram; tolerances for residues.

§180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.

§180.121 Methyl parathion; tolerances for residues.

§180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.

§180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.

§180.124 Methyl bromide; tolerances for residues.

§180.127 Piperonyl butoxide; tolerances for residues.

§180.128 Pyrethrins; tolerances for residues.

§180.129 o-Phenylphenol and its sodium salt; tolerances for residues.

§180.130 Hydrogen Cyanide; tolerances for residues.

§180.132 Thiram; tolerances for residues.

§180.142 2,4-D; tolerances for residues.

§180.145 Fluorine compounds; tolerances for residues.

§180.151 Ethylene oxide; tolerances for residues.

§180.153 Diazinon; tolerances for residues.

§180.154 Azinphos-methyl; tolerances for residues.

§180.155 1-Naphthaleneacetic acid; tolerances for residues.

§180.163 Dicofol; tolerances for residues.

§180.169 Carbaryl; tolerances for residues.

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§180.172 Dodine; tolerances for residues.

§180.175 Maleic hydrazide; tolerances for residues.

§180.176 Mancozeb; tolerances for residues.

§180.178 Ethoxyquin; tolerances for residues.

§180.181 Chlorpropham; tolerances for residues.

§180.182 Endosulfan; tolerances for residues.

§180.183 Disulfoton; tolerances for residues.

§180.184 Linuron; tolerances for residues.

§180.185 DCPA; tolerances for residues.

§180.189 Coumaphos; tolerances for residues.

§180.190 Diphenylamine; tolerances for residues.

§180.191 Folpet; tolerances for residues.

§180.198 Trichlorfon; tolerances for residues.

§180.200 Dicloran; tolerances for residues.

§180.202 p-Chlorophenoxyacetic acid; tolerances for residues.

§180.204 Dimethoate; tolerances for residues.

§180.205 Paraquat; tolerances for residues.

§180.206 Phorate; tolerances for residues.

§180.207 Trifluralin; tolerances for residues.

§180.208 Benfluralin; tolerances for residues.

§180.209 Terbacil; tolerances for residues.

§180.210 Bromacil; tolerances for residues.

§180.211 Propachlor; tolerances for residues.

§180.212 S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.

§180.213 Simazine; tolerances for residues.

§180.215 Naled; tolerances for residues.

§180.217 Metiram; tolerances for residues.

§180.220 Atrazine; tolerances for residues.

§180.222 Prometryn; tolerances for residues.

§180.225 Phosphine; tolerances for residues.

§180.226 Diquat; tolerances for residues.

§180.227 Dicamba; tolerances for residues.

§180.229 Fluometuron; tolerances for residues.

§180.231 Dichlobenil; tolerances for residues.

§180.232 Butylate; tolerances for residues.

§180.235 Dichlorvos; tolerances for residues.

§180.236 Triphenyltin hydroxide; tolerances for residues.

§180.241 Bensulide; tolerances for residues.

§180.242 Thiabendazole; tolerances for residues.

§180.243 Propazine; tolerances for residues.

§180.245 Streptomycin; tolerances for residues.

§180.249 Alachlor; tolerances for residues.

§180.252 Tetrachlorvinphos; tolerances for residues.

§180.253 Methomyl; tolerances for residues.

§180.254 Carbofuran; tolerances for residues.

§180.257 Chloroneb; tolerances for residues.

§180.258 Ametryn; tolerances for residues.

§180.259 Propargite; tolerances for residues.

§180.261 Phosmet; tolerances for residues.

§180.262 Ethoprop; tolerances for residues.

§180.263 Phosalone; tolerances for residues.

§180.269 Aldicarb; tolerances for residues.

§180.272 Tribuphos; tolerances for residues.

§180.274 Propanil; tolerances for residues.

§180.275 Chlorothalonil; tolerances for residues.

§180.276 Formetanate hydrochloride; tolerances for residues.

§180.278 Phenmedipham; tolerances for residues.

§180.284 Zinc phosphide; tolerances for residues.

§180.287 Amitraz; tolerances for residues.

§180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.

§180.289 Methanearsonic acid; tolerances for residues.

§180.291 Pentachloronitrobenzene; tolerance for residues.

§180.292 Picloram; tolerances for residues.

§180.293 Endothall; tolerances for residues.

§180.297 N-1-Naphthyl phthalamic acid; tolerances for residues.

§180.298 Methidathion; tolerances for residues.

§180.299 Dicrotophos; tolerances for residues.

§180.300 Ethephon; tolerances for residues.

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§180.301 Carboxin; tolerances for residues.

§180.303 Oxamyl; tolerances for residues.

§180.304 Oryzalin; tolerances for residues.

§180.311 Cacodylic acid; tolerances for residues.

§180.314 Triallate; tolerances for residues.

§180.315 Methamidophos; tolerances for residues.

§180.316 Pyrazon; tolerances for residues.

§180.317 Propyzamide; tolerances for residues.

§180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.

§180.319 Interim tolerances.

§180.324 Bromoxynil; tolerances for residues.

§180.328 Napropamide; tolerances for residues.

§180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.

§180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.

§180.332 Metribuzin; tolerances for residues.

§180.337 Oxytetracycline; tolerances for residues.

§180.339 MCPA; tolerances for residues.

§180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.

§180.342 Chlorpyrifos; tolerances for residues.

§180.345 Ethofumesate; tolerances for residues.

§180.349 Fenamiphos; tolerances for residues.

§180.350 Nitrapyrin; tolerances for residues.

§180.352 Terbufos; tolerances for residues.

§180.353 Desmedipham; tolerances for residues.

§180.355 Bentazon; tolerances for residues.

§180.356 Norflurazon; tolerances for residues.

§180.360 Asulam; tolerance for residues.

§180.361 Pendimethalin; tolerances for residues.

§180.362 Fenbutatin-oxide; tolerances for residues.

§180.364 Glyphosate; tolerances for residues.

§180.367 n-Octyl bicycloheptenedicarboximide; tolerances for residues.

§180.368 Metolachlor; tolerances for residues.

§180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.

§180.371 Thiophanate-methyl; tolerances for residues.

§180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.

§180.373 [Reserved]

§180.377 Diflubenzuron; tolerances for residues.

§180.378 Permethrin; tolerances for residues.

§180.380 Vinclozolin; tolerances for residues.

§180.381 Oxyfluorfen; tolerances for residues.

§180.383 Sodium salt of acifluorfen; tolerances for residues.

§180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.

§180.385 Diclofop-methyl; tolerances for residues.

§§180.388-180.389 [Reserved]

§180.390 Tebuthiuron; tolerances for residues.

§180.395 Hydramethylnon; tolerances for residues.

§180.396 Hexazinone; tolerances for residues.

§180.399 Iprodione; tolerances for residues.

§180.401 Thiobencarb; tolerances for residues.

§180.403 Thidiazuron; tolerances for residues.

§180.404 Profenofos; tolerances for residues.

§180.405 Chlorsulfuron; tolerances for residues.

§180.407 Thiodicarb; tolerances for residues.

§180.408 Metalaxyl; tolerances for residues.

§180.409 Pirimiphos-methyl; tolerances for residues.

§180.410 Triadimefon; tolerances for residues.

§180.411 Fluazifop-P-butyl; tolerances for residues.

§180.412 Sethoxydim; tolerances for residues.

§180.413 Imazalil; tolerances for residues.

§180.414 Cyromazine; tolerances for residues.

§180.415 Aluminum tris (O-ethylphosphonate); tolerances for residues.

§180.416 Ethalfluralin; tolerances for residues.

§180.417 Triclopyr; tolerances for residues.

§180.418 Cypermethrin and isomers alpha-cypermethrin and zeta-cypermethrin; tolerances for residues.

§180.419 Chlorpyrifos-methyl; tolerances for residues.

§180.420 Fluridone; tolerances for residues.

§180.421 Fenarimol; tolerances for residues.

§180.422 Tralomethrin; tolerances for residues.

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§180.425 Clomazone; tolerances for residues.

§180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid; tolerance for 

residues.

§180.427 Tau-Fluvalinate; tolerances for residues.

§180.428 Metsulfuron methyl; tolerances for residues.

§180.429 Chlorimuron ethyl; tolerances for residues.

§180.430 Fenoxaprop-ethyl; tolerances for residues.

§180.431 Clopyralid; tolerances for residues.

§180.432 Lactofen; tolerances for residues.

§180.433 Fomesafen; tolerances for residues.

§180.434 Propiconazole; tolerances for residues.

§180.435 Deltamethrin; tolerances for residues.

§180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.

§180.437 Methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl 6-(4-isopropyl-4-methyl-5-oxo-2-

imidazolin-2-yl)-m-toluate; tolerances for residues.

§180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.

§180.439 Thifensulfuron methyl; tolerances for residues.

§180.440 Tefluthrin; tolerances for residues.

§180.441 Quizalofop ethyl; tolerances for residues.

§180.442 Bifenthrin; tolerances for residues.

§180.443 Myclobutanil; tolerances for residues.

§180.444 Sulfur dioxide; tolerances for residues.

§180.445 Bensulfuron methyl; tolerances for residues.

§180.446 Clofentezine; tolerances for residues.

§180.447 Imazethapyr; tolerances for residues.

§180.448 Hexythiazox; tolerance for residues.

§180.449 Avermectin B1 and its delta-8,9-isomer; tolerances for residues.

§180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol; tolerances for residues.

§180.451 Tribenuron methyl; tolerances for residues.

§180.452 Primisulfuron-methyl; tolerances for residues.

§180.454 Nicosulfuron; tolerances for residues.

§180.455 Procymidone; tolerances for residues.

§180.457 Bitertanol; tolerances for residues.

§180.458 Clethodim; tolerances for residues.

§180.459 Triasulfuron; tolerances for residues.

§180.460 Benoxacor; tolerances for residues.

§180.461 Cadusafos; tolerances for residues.

§180.462 Pyridate; tolerances for residues.

§180.463 Quinclorac; tolerances for residues.

§180.464 Dimethenamid; tolerances for residues.

§180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.

§180.466 Fenpropathrin; tolerances for residues.

§180.467 Carbon disulfide; tolerances for residues.

§180.468 Flumetsulam; tolerances for residues.

§180.469 Dichlormid; tolerances for residues.

§180.470 Acetochlor; tolerances for residues.

§180.471 Furilazole; tolerances for residues.

§180.472 Imidacloprid; tolerances for residues.

§180.473 Glufosinate ammonium; tolerances for residues.

§180.474 Tebuconazole; tolerances for residues.

§180.475 Difenoconazole; tolerances for residues.

§180.476 Triflumizole; tolerances for residues.

§180.477 Flumiclorac pentyl; tolerances for residues.

§180.478 Rimsulfuron; tolerances for residues.

§180.479 Halosulfuron-methyl; tolerances for residues.

§180.480 Fenbuconazole; tolerances for residues.

§180.481 Prosulfuron; tolerances for residues.

§180.482 Tebufenozide; tolerances for residues.

§180.484 Flutolanil; tolerances for residues.

§180.485 Cyproconazole; tolerances for residues.

§180.486 Chlorethoxyfos; tolerances for residues.

§180.487 Pyrithiobac sodium; tolerances for residues.

§180.490 Imazapic; tolerances for residues.

§180.491 Propylene oxide; tolerances for residues.

§180.492 Triflusulfuron-methyl; tolerances for residues.

§180.493 Dimethomorph; tolerances for residues.

§180.494 Pyridaben; tolerance for residues.

§180.495 Spinosad; tolerances for residues.

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§180.496 Thiazopyr; tolerances for residues.

§180.497 Clofencet; tolerances for residues.

§180.498 Sulfentrazone; tolerances for residues.

§180.499 Propamocarb; tolerances for residues.

§180.500 Imazapyr; tolerances for residues.

§180.501 Hydroprene; tolerances for residues.

§180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.

§180.503 Cymoxanil, tolerance for residues.

§180.504 [Reserved]

§180.505 Emamectin; tolerances for residues.

§180.506 Cyclanilide; tolerances for residues.

§180.507 Azoxystrobin; tolerances for residues.

§180.509 Mefenpyr-diethyl; tolerance for residues.

§180.510 Pyriproxyfen; tolerances for residues.

§180.511 Buprofezin; tolerances for residues.

§180.512 [Reserved]

§180.513 Chlorfenapyr; tolerances for residues.

§180.514 Cloransulam-methyl; tolerances for residues.

§180.515 Carfentrazone-ethyl; tolerances for residues.

§180.516 Fludioxonil; tolerances for residues.

§180.517 Fipronil; tolerances for residues.

§180.518 Pyrimethanil; tolerances for residues.

§180.519 Bromide ion and residual bromine; tolerances for residues.

§180.521 Fumigants for grain-mill machinery; tolerances for residues.

§180.522 Fumigants for processed grains used in production of fermented malt beverage; tolerances for residues.

§180.523 Metaldehyde; tolerances for residues.

§180.525 Resmethrin; tolerances for residues.

§180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.

§180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide 

and its metabolites containing the 4-fluoro-N-methylethyl benzenamine tolerances for residues.

§180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol methylcarbamate; tolerances for residues.

§180.532 Cyprodinil; tolerances for residues.

§180.533 Esfenvalerate; tolerances for residues.

§180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.

§180.537 Isoxaflutole; tolerances for residues.

§180.539 d-Limonene; tolerances for residues.

§180.540 Fenitrothion; tolerances for residues.

§180.541 Propetamphos; tolerances for residues.

§180.543 Diclosulam; tolerances for residues.

§180.544 Methoxyfenozide; tolerances for residues.

§180.545 Prallethrin; tolerances for residues.

§180.546 Mefenoxam; tolerances for residues.

§180.547 Prohexadione calcium; tolerances for residues.

§180.548 Tralkoxydim; tolerances for residues.

§180.549 Diflufenzopyr; tolerances for residues.

§180.551 Fluthiacet-methyl; tolerances for residues.

§180.552 Sulfosulfuron; tolerances for residues.

§180.553 Fenhexamid; tolerances for residues.

§180.554 Kresoxim-methyl; tolerances for residues.

§180.555 Trifloxystrobin; tolerances for residues.

§180.556 Pymetrozine; tolerances for residues.

§180.557 Tetraconazole; tolerances for residues.

§180.559 Clodinafop-propargyl; tolerances for residues.

§180.560 Cloquintocet-mexyl; tolerances for residues.

§180.561 Acibenzolar-S-methyl; tolerances for residues.

§180.562 Flucarbazone-sodium; tolerances for residues.

§180.563 Ethametsulfuron-methyl; tolerances for residues.

§180.564 Indoxacarb; tolerances for residues.

§180.565 Thiamethoxam; tolerances for residues.

§180.566 Fenpyroximate; tolerances for residues.

§180.567 Zoxamide; tolerances for residues.

§180.568 Flumioxazin; tolerances for residues.

§180.569 Forchlorfenuron; tolerances for residues.

§180.570 Isoxadifen-ethyl; tolerances for residues.

§180.571 Mesotrione; tolerances for residues.

§180.572 Bifenazate; tolerance for residues.

§180.573 Tepraloxydim; tolerances for residues.

§180.574 Fluazinam; tolerances for residues.

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§180.575 Sulfuryl fluoride; tolerances for residues.

§180.576 Cyhalofop-butyl; tolerances for residues.

§180.577 Bispyribac-sodium; tolerances for residues.

§180.578 Acetamiprid; tolerances for residues.

§180.579 Fenamidone; tolerances for residues.

§180.580 Iodosulfuron-Methyl-Sodium; tolerances for residues.

§180.581 Iprovalicarb; tolerances for residues.

§180.582 Pyraclostrobin; tolerances for residues.

§180.583 Triticonazole; tolerances for residues.

§180.584 Tolylfluanid; tolerances for residues.

§180.585 Pyraflufen-ethyl; tolerances for residues.

§180.586 Clothianidin; tolerances for residues.

§180.587 Famoxadone; tolerance for residues.

§180.588 Quinoxyfen; tolerances for residues.

§180.589 Boscalid; tolerances for residues.

§180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.

§180.591 Trifloxysulfuron; tolerances for residues.

§180.592 Butafenacil; tolerances for residues.

§180.593 Etoxazole; tolerances for residues.

§180.594 Thiacloprid; tolerances for residues.

§180.595 Flufenpyr-ethyl; tolerances for residues.

§180.596 Fosthiazate; tolerances for residues.

§180.597 Mesosulfuron-methyl; tolerances for residues.

§180.598 Novaluron; tolerances for residues.

§180.599 Acequinocyl; tolerances for residues.

§180.600 Propoxycarbazone; tolerances for residues.

§180.601 Cyazofamid; tolerances for residues.

§180.602 Spiroxamine; tolerances for residues.

§180.603 Dinotefuran; tolerances for residues.

§180.604 Mepanipyrim; tolerances for residues.

§180.605 Penoxsulam; tolerances for residues.

§180.607 Spiromesifen; tolerances for residues.

§180.608 Spirodiclofen; tolerances for residues.

§180.609 Fluoxastrobin; tolerances for residues.

§180.610 Aminopyralid; tolerances for residues.

§180.611 Pinoxaden; tolerances for residues.

§180.612 Topramezone; tolerances for residues.

§180.613 Flonicamid; tolerances for residues.

§180.614 Kasugamycin; tolerances for residues.

§180.615 Amicarbazone; tolerances for residues.

§180.616 Fenpropimorph; tolerances for residues.

§180.617 Metconazole; tolerances for residues.

§180.618 Benthiavalicarb-isopropyl; tolerance for residues.

§180.619 Epoxiconazole; tolerances for residues.

§180.620 Etofenprox; tolerances for residues.

§180.621 Dithianon; tolerances for residues.

§180.622 Ethaboxam; tolerances for residues.

§180.623 Flufenoxuron; tolerances for residues.

§180.624 Metrafenone; tolerances for residues.

§180.625 Orthosulfamuron; tolerances for residues.

§180.626 Prothioconazole; tolerances for residues.

§180.627 Fluopicolide; tolerances for residues.

§180.628 Chlorantraniliprole; tolerances for residues.

§180.629 Flutriafol; tolerances for residues.

§180.630 Flusilazole; tolerances for residues.

§180.631 Pyrasulfotole; tolerances for residues.

§180.632 Fenazaquin; Tolerances for residues.

§180.633 Florasulam; tolerances for residues.

§180.634 Tembotrione; tolerances for residues.

§180.635 Spinetoram; tolerances for residues.

§180.636 1,3-dichloropropene; tolerances for residues.

§180.637 Mandipropamid; tolerances for residues.

§180.638 Pyroxsulam; tolerances for residues.

§180.639 Flubendiamide; tolerances for residues.

§180.640 Pyridalyl; tolerances for residues.

§180.641 Spirotetramat; tolerances for residues.

§180.642 Gentamicin; tolerances for residues.

§180.643 Uniconazole; tolerances for residues.

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§180.644 Cyprosulfamide; tolerances for residues.

§180.645 Thiencarbazone-methyl; tolerances for residues.

§180.646 Ipconazole; tolerances for residues.

§180.647 d-Phenothrin; tolerances for residues.

§180.648 Meptyldinocap; tolerances for residues.

§180.649 Saflufenacil; tolerances for residues.

§180.650 Isoxaben; tolerances for residues.

§180.651 Imazosulfuron; tolerances for residues.

§180.652 Ethiprole; tolerances for residues.

§180.653 Indaziflam; tolerances for residues.

§180.654 Isopyrazam; tolerances for residues.

§180.655 Flazasulfuron; tolerances for residues.

§180.656 Amisulbrom; tolerances for residues.

§180.657 Metaflumizone; tolerances for residues.

§180.658 Penthiopyrad; tolerances for residues.

§180.659 Pyroxasulfone; tolerances for residues.

§180.660 Pyriofenone; tolerances for residues.

§180.661 Fluopyram; tolerances for residues.

§180.662 Trinexapac-ethyl; tolerances for residues.

§180.663 Ametoctradin; tolerances for residues.

§180.664 Penflufen; tolerances for residues.

§180.665 Sedaxane; tolerances for residues.

§180.666 Fluxapyroxad; tolerances for residues.

§180.667 Cyflufenamid, tolerance for residues.

§180.668 Sulfoxaflor; tolerances for residues.

§180.669 Picoxystrobin; tolerances for residues.

§180.671 Fenpyrazamine; tolerances for residues.

§180.672 Cyantraniliprole; tolerances for residues.

§180.673 Triforine; tolerances for residues.

§180.674 Proquinazid; tolerances for residues.

§180.675 Tolfenpyrad; tolerances for residues.

§180.676 Fenpropidin; tolerances for residues.

§180.677 Cyflumetofen; tolerances for residues.

§180.678 Tricyclazole; tolerances for residues.

§180.679 Flupyradifurone; tolerances for residues.

§180.680 Fluensulfone; tolerances for residues.

§180.681 Isofetamid; tolerances for residues.

§180.682 Bicyclopyrone; tolerances for residues.

§180.684 Benalaxyl-M; tolerances for residues.

§180.685 Oxathiapiprolin; tolerances for residues.

§180.686 Benzovindiflupyr; tolerances for residues.

§180.687 Teflubenzuron; tolerances for residues.

§180.688 Diethofencarb; tolerance for residue.

Subpart D—Exemptions From Tolerances

§180.900 Exemptions from the requirement of a tolerance.

§180.905 Pesticide chemicals; exemptions from the requirement of a tolerance.

§180.910 Inert ingredients used pre- and post-harvest; exemptions from the requirement of a tolerance.

§180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a tolerance.

§180.930 Inert ingredients applied to animals; exemptions from the requirement of a tolerance.

§180.940 Tolerance exemptions for active and inert ingredients for use in antimicrobial formulations (Food-contact 

surface sanitizing solutions).

§180.950 Tolerance exemptions for minimal risk active and inert ingredients.

§180.960 Polymers; exemptions from the requirement of a tolerance.

§180.1011 Viable spores of the microorganism Bacillus thuringiensis Berliner; exemption from the requirement of a 

tolerance.

§180.1016 Ethylene; exemption from the requirement of a tolerance.

§180.1017 Diatomaceous earth; exemption from the requirement of a tolerance.

§180.1019 Sulfuric acid; exemption from the requirement of a tolerance.

§180.1020 Sodium chlorate; exemption from the requirement of a tolerance.

§180.1021 Copper; exemption from the requirement of a tolerance.

§180.1022 Iodine-detergent complex; exemption from the requirement of a tolerance.

§180.1023 Propanoic acid; exemptions from the requirement of a tolerance.

§180.1025 Xylene; exemption from the requirement of a tolerance.

§180.1027 Nuclear polyhedrosis virus of Heliothis zea; exemption from the requirement of a tolerance.

§180.1033 Methoprene; exemption from the requirement of a tolerance.

§180.1037 Polybutenes; exemption from the requirement of a tolerance.

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§180.1040 Ethylene glycol; exemption from the requirement of a tolerance.

§180.1041 Nosema locustae; exemption from the requirement of a tolerance.

§180.1043 Gossyplure; exemption from the requirement of a tolerance.

§180.1049 Carbon dioxide; exemption from the requirement of a tolerance.

§180.1050 Nitrogen; exemption from the requirements of a tolerance.

§180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption from the requirement of a tolerance.

§180.1054 Calcium hypochlorite; exemptions from the requirement of a tolerance.

§180.1056 Boiled linseed oil; exemption from requirement of tolerance.

§180.1057 Phytophthora palmivora; exemption from requirement of tolerance.

§180.1058 Sodium diacetate; exemption from the requirement of a tolerance.

§180.1064 Tomato pinworm insect pheromone; exemption from the requirement of a tolerance.

§180.1065 2-Amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one; exemption from the requirement 

of a tolerance.

§180.1067 Methyl eugenol and malathion combination; exemption from the requirement of a tolerance.

§180.1068 C12-C18 fatty acid potassium salts; exemption from the requirement of a tolerance.

§180.1069 (Z)-11-Hexadecenal; exemption from the requirement of a tolerance.

§180.1070 Sodium chlorite; exemption from the requirement of a tolerance.

§180.1071 Peanuts, Tree Nuts, Milk, Soybeans, Eggs, Fish, Crustacea, and Wheat; exemption from the requirement of a 

tolerance.

§180.1072 Poly-D-glucosamine (chitosan); exemption from the requirement of a tolerance.

§180.1073 Isomate-M; exemption from the requirement of a tolerance.

§180.1074 F.D.&C. Blue No. 1; exemption from the requirement of a tolerance.

§180.1075 Colletotrichum gloeosporioides f. sp. aeschynomene; exemption from the requirement of a tolerance.

§180.1076 Viable spores of the microorganism Bacillus popilliae; exemption from the requirement of a tolerance.

§180.1080 Plant volatiles and pheromone; exemptions from the requirement of a tolerance.

§180.1083 Dimethyl sulfoxide; exemption from the requirement of a tolerance.

§180.1084 Monocarbamide dihydrogen sulfate; exemption from the requirement of a tolerance.

§180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-trimethyl-2,6,10-dodecatriene-3-ol; exemption from the 

requirement of a tolerance.

§180.1087 Sesame stalks; exemption from the requirement of a tolerance.

§180.1089 Poly-N-acetyl-D-glucosamine; exemption from the requirement of tolerance.

§180.1090 Lactic acid; exemption from the requirement of a tolerance.

§180.1091 Aluminum isopropoxide and aluminum secondary butoxide; exemption from the requirement of a tolerance.

§180.1092 Menthol; exemption from the requirement of a tolerance.

§180.1095 Chlorine gas; exemptions from the requirement of a tolerance.

§180.1097 GBM-ROPE; exemption from the requirement of a tolerance.

§180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and Sodium or Potassium Gibberellate]; exemption 

from the requirement of a tolerance.

§180.1100 Gliocladium virens isolate GL-21; exemption from the requirement of a tolerance.

§180.1101 Parasitic (parasitoid) and predatory insects; exemption from the requirement of a tolerance.

§180.1102 Trichoderma harzianum KRL-AG2 (ATCC #20847) strain T-22; exemption from requirement of a tolerance.

§180.1103 Isomate-C; exemption from the requirement of a tolerance.

§180.1107 Delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas fluorescens;

exemption from the requirement of a tolerance.

§180.1108 Delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas 

fluorescens; exemption from the requirement of a tolerance.

§180.1110 3-Carbamyl-2,4,5-trichlorobenzoic acid; exemption from the requirement of a tolerance.

§180.1111 Bacillus subtilis GB03; exemption from the requirement of a tolerance.

§180.1113 Lagenidium giganteum; exemption from the requirement of a tolerance.

§180.1114 Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and Pseudomonas syringae 742RS; 

exemptions from the requirement of a tolerance.

§180.1118 Spodoptera exigua nuclear polyhedrosis virus; exemption from the requirement of a tolerance.

§180.1119 Azadirachtin; exemption from the requirement of a tolerance.

§180.1120 Streptomyces sp. strain K61; exemption from the requirement of a tolerance.

§180.1121 Boric acid and its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric oxide 

(boric anhydride), sodium borate and sodium metaborate; exemptions from the requirement of a tolerance.

§180.1122 Inert ingredients of semiochemical dispensers; exemptions from the requirement of a tolerance.

§180.1124 Arthropod pheromones; exemption from the requirement of a tolerance.

§180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; exemption from the requirement of a tolerance.

§180.1127 Biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde, cinnamyl alcohol, 

4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 1,2,4-trimethoxybenzene; 

exemptions from the requirement of a tolerance.

§180.1128 Bacillus subtilis MBI 600; exemption from the requirement of a tolerance.

§180.1130 N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone; exemptions from the requirement of a tolerance.

§180.1131 Ampelomyces quisqualis isolate M10; exemption from the requirement of a tolerance.

§180.1135 Pasteuria penetrans; exemption from the requirement of a tolerance.

§180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of a tolerance.

§180.1140 Sodium o-nitrophenolate; exemption from the requirement of a tolerance.

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§180.1141 Sodium p-nitrophenolate; exemption from the requirement of a tolerance.

§180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a tolerance.

§180.1143 Methyl anthranilate; exemption from the requirement of a tolerance.

§180.1144 Candida oleophila isolate I-182; exemption from the requirement of a tolerance.

§180.1145 Pseudomonas syringae; exemption from the requirement of a tolerance.

§180.1146 Beauveria bassiana Strain GHA; exemption from the requirement of a tolerance.

§180.1148 Occlusion Bodies of the Granulosis Virus of Cydia pomenella; tolerance exemption.

§180.1149 Inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera; exemption from the 

requirement of a tolerance.

§180.1150 6-Benzyladenine; exemption from the requirement of a tolerance.

§180.1153 Lepidopteran pheromones; exemption from the requirement of a tolerance.

§180.1154 CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in killed 

Pseudomonas fluorescens, and the expression plasmid and cloning vector genetic constructs.

§180.1156 Cinnamaldehyde; exemption from the requirement of a tolerance.

§180.1157 Cytokinins; exemption from the requirement of a tolerance.

§180.1158 Auxins; exemption from the requirement of a tolerance.

§180.1159 Pelargonic acid; exemption from the requirement of tolerances.

§180.1160 Jojoba oil; exemption from the requirement of a tolerance.

§180.1161 Clarified hydrophobic extract of neem oil; exemption from the requirement of a tolerance.

§180.1162 Acrylate polymers and copolymers; exemption from the requirement of a tolerance.

§180.1163 Killed Myrothecium verrucaria; exemption from the requirement of a tolerance.

§180.1165 Capsaicin; exemption from the requirement of a tolerance.

§180.1167 Allyl isothiocyanate as a component of food grade oil of mustard; exemption from the requirement of a 

tolerance.

§180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance.

§180.1177 Potassium bicarbonate; exemption from the requirement of a tolerance.

§180.1178 Formic acid; exemption from the requirement of a tolerance.

§180.1179 Plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and Rhizophoria mangle;

exemption from the requirement of a tolerance.

§180.1180 Kaolin; exemption from the requirement of a tolerance.

§180.1181 Bacillus cereus strain BPO1; exemption from the requirement of a tolerance.

§180.1187 L-glutamic acid; exemption from the requirement of a tolerance.

§180.1188 Gamma aminobutyric acid; exemption from the requirement of a tolerance.

§180.1189 Methyl salicylate; exemption from the requirement of a tolerance.

§180.1191 Ferric phosphate; exemption from the requirement of a tolerance.

§180.1193 Potassium dihydrogen phosphate; exemption from the requirement of a tolerance.

§180.1195 Titanium dioxide.

§180.1196 Peroxyacetic acid; exemption from the requirement of a tolerance.

§180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance.

§180.1198 Gliocladium catenulatum strain J1446; exemption from the requirement of a tolerance.

§180.1199 Lysophosphatidylethanolamine (LPE); exemption from the requirement of a tolerance.

§180.1200 Pseudomonas fluorescens strain PRA-25; temporary exemption from the requirement of a tolerance.

§180.1201 Trichoderma harzianum strain T-39; exemption from the requirement of a tolerance.

§180.1202 Bacillus sphaericus; exemption from the requirement of a tolerance.

§180.1204 Harpin protein; exemption from the requirement of a tolerance.

§180.1205 Beauveria bassiana ATCC #74040; exemption from the requirements of a tolerance.

§180.1206 Aspergillus flavus AF36; exemption from the requirement of a tolerance.

§180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemption from the requirement of a tolerance.

§180.1209 Bacillus subtilis strain QST 713 and strain QST 713 variant soil; exemption from the requirement of a 

tolerance.

§180.1210 Phosphorous acid; exemption from the requirement of a tolerance.

§180.1212 Pseudomonas chlororaphis Strain 63-28; exemption from the requirement of a tolerance.

§180.1213 Coniothyrium minitans strain CON/M/91-08; exemption from the requirement of a tolerance.

§180.1218 Indian Meal Moth Granulosis Virus; exemption from the requirement of a tolerance.

§180.1219 Foramsulfuron; exemption from the requirement of a tolerance.

§180.1220 1-Methylcyclopropene; exemption from the requirement of a tolerance.

§180.1221 Pseudozyma flocculosa strain PF-A22 UL; exemption from the requirement of a tolerance.

§180.1222 Sucrose octanoate esters; exemption from the requirement of a tolerance.

§180.1223 Imazamox; exemption from the requirement of a tolerance.

§180.1224 Bacillus pumilus GB34; exemption from the requirement of a tolerance.

§180.1225 Decanoic acid; exemption from the requirement of a tolerance.

§180.1226 Bacillus pumilus strain QST2808; temporary exemption from the requirement of a tolerance.

§180.1228 Diallyl sulfides; exemption from the requirement of a tolerance.

§180.1230 Ferrous sulfate; exemption from the requirement of a tolerance.

§180.1231 Lime; exemption from the requirement of a tolerance.

§180.1232 Lime-sulfur; exemption from the requirement of a tolerance.

§180.1233 Potassium sorbate; exemption from the requirement of a tolerance.

§180.1234 Sodium carbonate; exemption from the requirement of a tolerance.

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§180.1235 Sodium hypochlorite; exemption from the requirement of a tolerance.

§180.1236 Sulfur; exemption from the requirement of a tolerance.

§180.1237 Sodium metasilicate; exemption from the requirement of a tolerance.

§180.1240 Thymol; exemption from the requirement of a tolerance.

§180.1241 Eucalyptus oil; exemption from the requirement of a tolerance.

§180.1243 Bacillus subtilis var. amyloliquefaciens strain FZB24; exemption from the requirement of a tolerance.

§180.1244 Ammonium bicarbonate; exemption from the requirement of a tolerance.

§180.1245 Rhamnolipid biosurfactant; exemption from the requirement of a tolerance.

§180.1246 Yeast Extract Hydrolysate from Saccharomyces cerevisiae: exemption from the requirement of a tolerance.

§180.1248 Exemption of citronellol from the requirement of a tolerance.

§180.1250 C8, C10, and C12 fatty acid monoesters of glycerol and propylene glycol; exemption from the requirement of 

a tolerance.

§180.1251 Geraniol; exemption from the requirement of a tolerance.

§180.1253 Streptomyces lydicus WYEC 108; exemption from the requirement of a tolerance.

§180.1254 Aspergillus flavus NRRL 21882; exemption from the requirement of a tolerance.

§180.1255 Bacillus pumilus strain QST 2808; exemption from the requirement of a tolerance.

§180.1256 Alternaria destruens strain 059; exemption from the requirement of a tolerance.

§180.1257 Paecilomyces lilacinus strain 251; exemption from the requirement of a tolerance.

§180.1258 Acetic acid; exemption from the requirement of a tolerance.

§180.1259 Reynoutria sachalinensis extract; exemption from the requirement of a tolerance.

§180.1260 Muscodor albus QST 20799 and the volatiles produced on rehydration; exemption from the requirement of a 

tolerance.

§180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas syringae pv. tomato specific Bacteriophages.

§180.1262 Sorbitol octanoate; exemption from the requirement of a tolerance.

§180.1263 Tetrahydrofurfuryl alcohol; exemption from the requirement of a tolerance.

§180.1267 Pantoea agglomerans strain C9-1; exemption from the requirement of a tolerance.

§180.1268 Potassium silicate; exemption from the requirement of a tolerance.

§180.1269 Bacillus mycoides isolate J; exemption from the requirement of a tolerance.

§180.1270 Isophorone; exemption from the requirement of a tolerance.

§180.1271 Eucalyptus oil; exemption from the requirement of a tolerance.

§180.1272 Pantoea agglomerans strain E325; exemption from the requirement of a tolerance.

§180.1273 Beauveria bassiana HF23; exemption from the requirement of a tolerance.

§180.1274 Tris (2-ethylhexyl) phosphate; exemption from the requirement of a tolerance.

§180.1275 Pythium; exception from the requirement of a tolerance.

§180.1276 Tobacco mild green mosaic tobamovirus strain U2; exemption from the requirement of a tolerance.

§180.1277 Dibasic esters; exemption from the requirement of a tolerance.

§180.1278 Quillaja saponaria extract (saponins); exemption from the requirement of a tolerance.

§180.1279 Zucchini yellow mosaic virus—weak strain; exemption from the requirement of a tolerance.

§180.1280 Poly(hexamethylenebiguanide) hydrochloride (PHMB); exemption from the requirement of a tolerance.

§180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)-3-methyl-penta-(2Z,4E)-dienoic 

Acid; exemption from the requirement of a tolerance.

§180.1282 Bacillus firmus I-1582; exemption from the requirement of a tolerance.

§180.1283 (Z)-7,8-epoxy-2-methyloctadecane (Disparlure); exemption from the requirement of a tolerance.

§180.1284 Ammonium salts of higher fatty acids (C8-C18 saturated; C8-C12 unsaturated); exemption from the requirement 

of a tolerance.

§180.1285 Polyoxin D zinc salt; exemption from the requirement of a tolerance.

§180.1287 Extract of Chenopodium ambrosioides near ambrosioides; exemption from the requirement of a tolerance.

§180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a tolerance.

§180.1289 Candida oleophila Strain O; exemption from the requirement of a tolerance.

§180.1290 Pasteuria usgae; exemption from the requirement of a tolerance.

§180.1291 Cold pressed neem oil; exemption from the requirement of a tolerance.

§180.1292 Ulocladium oudemansii (U3 Strain); exemption from the requirement of a tolerance.

§180.1293 Trichoderma gamsii strain ICC 080; exemption from the requirement of a tolerance.

§180.1294 Trichoderma asperellum strain ICC 012; exemption from the requirement of a tolerance.

§180.1295 Laminarin; exemption from the requirement of a tolerance.

§180.1296 Terpene Constituents α-terpinene, d-limonene and p-cymene, of the Extract of Chenopodium ambrosioides

near ambrosioides as Synthetically Manufactured; exemption from the requirement of a tolerance.

§180.1297 Homobrassinolide; exemption from the requirement of a tolerance.

§180.1298 Trichoderma hamatum isolate 382; exemption from the requirement of a tolerance.

§180.1299 Prohydrojasmon; exemption from the requirement of a tolerance.

§180.1300 Potassium hypochlorite; exemption from the requirement of a tolerance.

§180.1301 Escherichia coli O157:H7 specific bacteriophages; temporary exemption from the requirement of a tolerance.

§180.1302 Sodium Ferric Ethylenediaminetetraacetate (EDTA); exemption from the requirement of a tolerance.

§180.1303 Metarhizium anisopliae strain F52; exemption from the requirement of a tolerance.

§180.1304 Pseudomonas fluorescens strain CL145A; exemption from the requirement of a tolerance.

§180.1305 Chromobacterium subtsugae strain PRAA4-1; exemption from the requirement of a tolerance.

§180.1306 Isaria fumosorosea (formerly Paecilomyces fumosoroseus) Apopka strain 97; exemption from the requirement 

of a tolerance.

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§180.1307 Bacteriophage of Clavibacter michiganensis subspecies michiganensis; exemption from the requirement of a 

tolerance.

§180.1308 Bacillus amyloliquefaciens strain D747; exemption from the requirement of a tolerance.

§180.1309 Bacillus subtilis strain CX-9060; exemption from the requirement of a tolerance.

§180.1310 Trichoderma virens strain G-41; exemption from the requirement of a tolerance.

§180.1311 Pasteuria nishizawae—Pn1; exemption from the requirement of a tolerance.

§180.1312 Aureobasidium pullulans strains DSM 14940 and DSM 14941; exemption from the requirement of a tolerance.

§180.1313 Bacillus pumilus strain GHA 180; exemption from the requirement of a tolerance.

§180.1314 Killed, nonviable Streptomyces acidiscabies strain RL-110; exemption from the requirement of a tolerance.

§180.1315 Natamycin; exemption from the requirement of a tolerance.

§180.1316 Pasteuria spp. (Rotylenchulus reniformis nematode)—Pr3; exemption from the requirement of a tolerance.

§180.1317 Pesticide chemicals; exemption from the requirements of a tolerance.

§180.1318 3-decen-2-one; exemption from the requirement of a tolerance.

§180.1319 Banda de Lupinus albus doce (BLAD); exemption from the requirement of a tolerance.

§180.1320 Methyl jasmonate; exemption from the requirement of a tolerance.

§180.1321 Complex Polymeric Polyhydroxy Acids; exemption from the requirement of a tolerance.

§180.1322 Bacillus pumilus strain BU F-33; exemption from the requirement of a tolerance.

§180.1323 Ethyl-2E,4Z-decadienoate (Pear Ester); exemption from the requirement of a tolerance.

§180.1324 GS-omega/kappa-Hxtx-Hv1a; exemption from the requirement of a tolerance.

§180.1325 Heat-killed Burkholderia spp. strain A396 cells and spent fermentation media exemption from the requirement 

of a tolerance.

§180.1326 Pseudomonas fluorescens strain D7; exemption from the requirement of a tolerance.

§180.1327 Tetraacetylethylenediamine (TAED) and its metabolite Diacetylethylenediamine (DAED); exemption from the 

requirement of a tolerance.

§180.1328 Beauveria bassiana strain ANT-03; exemption from the requirement of a tolerance.

§180.1329 Bacillus subtilis strain IAB/BS03, exemption from the requirement of a tolerance.

§180.1330 1-Octanol; exemption from the requirement of a tolerance.

§180.1331 Trichoderma asperelloides strain JM41R; exemption from the requirement of a tolerance.

§180.1332 Lavandulyl senecioate; exemption from the requirement of a tolerance.

§180.1333 Potassium Salts of Hops Beta acids; exemption from the requirement of a tolerance.

Subpart E—Pesticide Chemicals Not Requiring a Tolerance or an Exemption From a Tolerance

§180.2000 Scope.

§180.2003 Definitions.

§180.2010 Threshold of regulation determinations.

§180.2020 Non-food determinations.

AUTHORITY: 21 U.S.C. 321(q), 346a and 371. 

SOURCE: 36 FR 22540, Nov. 25, 1971, unless otherwise noted. 

EDITORIAL NOTE: Nomenclature changes to part 180 appear at 62 FR 66023, Dec. 17, 1997. 

GLOSSARY

NOTE: The items in this glossary were compiled as an aid to the users of the Code of Federal Regulations. Inclusion or 

exclusion from this glossary has no legal significance.

APPLI = APPLICATION

C-I MET = CHOLINESTERASE-INHIBITING METABOLITES

CARB = CARBAMATES

EPWRR = EDIBLE PORTION WITH RIND REMOVED

EXC = EXCEPT

I (IN PPM COLUMN) = INTERIM TOLERANCE

INC = INCLUDING

K = CWHR = KERNEL PLUS COB WITH HUSK REMOVED

MBYP = MEAT BYPRODUCTS

MIN = MINIMUM

N (IN PPM COLUMN) = NEGLIGIBLE RESIDUES

NMT = NOT MORE THAN

NON-PER BAG/PKGD RAC = NON-PERISHABLE PACKAGED OR BAGGED RAW AGRICULTURAL COMMODITY

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PPM = PART(S) PER MILLION

POST-H = POSTHARVEST APPLICATION

PRE-H = PREHARVEST APPLICATION

PRE-S = PRESLAUGHTER APPLICATION

PRODS = PRODUCTS rollert

T (IN PPM COLUMN) = TEMPORARY TOLERANCE

[41 FR 4537, Jan. 30, 1976]

 Back to Top

Subpart A—Definitions and Interpretative Regulations

 Back to Top

§180.1 Definitions and interpretations.

(a) Administrator, without qualification, means the Administrator of the Environmental Protection Agency.

(b) Agency, without qualification, means the Environmental Protection Agency.

(c) FFDCA means the Federal Food, Drug, and Cosmetic Act, as amended, 21 U.S.C. 301-392.

(d) Raw agricultural commodities include, among other things, fresh fruits, whether or not they have been washed and 

colored or otherwise treated in their unpeeled natural form; vegetables in their raw or natural state, whether or not they 

have been stripped of their outer leaves, waxed, prepared into fresh green salads, etc.; grains, nuts, eggs, raw milk, 

meats, and similar agricultural produce. It does not include foods that have been processed, fabricated, or manufactured 

by cooking, freezing, dehydrating, or milling.

(e) Where a raw agricultural commodity bearing a pesticide chemical residue that has been exempted from the 

requirement of a tolerance, or which is within a tolerance permitted under FFDCA section 408, is used in preparing a 

processed food, the processed food will not be considered unsafe within the meaning of FFDCA sections 402 and 408(a), 

despite the lack of a tolerance or exemption for the pesticide chemical residue in the processed food, if:

(1) The pesticide chemical has been used in or on the raw agricultural commodity in conformity with a tolerance under 

this section;

(2) The pesticide chemical residue has been removed to the extent possible in good manufacturing practice; and

(3) The concentration of the pesticide chemical residue in the processed food is not greater than the tolerance 

prescribed for the pesticide chemical residue on the raw agricultural commodity.

(f) For the purpose of computing fees as required by §180.33, each group of related crops listed in §180.34(e) and 

each crop group or subgroup listed in §180.41 is counted as a single raw agricultural commodity in a petition or request for 

tolerances or exemption from the requirement of a tolerance.

(g) Tolerances and exemptions established for pesticide chemicals in or on the general category of raw agricultural 

commodities listed in column A apply to the corresponding specific raw agricultural commodities listed in column B. 

However, a tolerance or exemption for a specific commodity in column B does not apply to the general category in column 

A.

A B

Alfalfa Medicago sativa L. Subsp. sativa, (alfalfa, lucerne); Onobrychis viciifolia Scop. (sainfoin, holy clover, esparcet); and Lotus corniculatus L.

(trefoil); and varieties and/or hybrids of these.

Banana Banana, plantain.

Bean Cicer arietinum (chickpea, garbanzo bean); Lupinus spp. (including sweet lupine, white sweet lupine, white lupine, and grain lupine). 

Phaseolus spp. (including kidney bean, lima bean, mung bean, navy bean, pinto bean, snap bean, and waxbean; Vicia faba (broad bean, fava 

bean); Vigna spp. (including asparagus bean, blackeyed pea and cowpea).

Bean, dry All beans above in dry form only.

Bean, 

succulent

All beans above in succulent form only.

Blackberry Rubus eubatus (including bingleberry, black satin berry, boysenberry Cherokee blackberry, Chesterberry, Cheyenne blackberry, coryberry, 

darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth blackberry, 

marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangerberry, ravenberry, rossberry, Shawnee blackberry, 

and varieties and/or hybrids of these).

Broccoli Broccoli, chinese broccoli (gia lon, white flowering broccoli).

Cabbage Cabbage, Chinese cabbage (tight-heading varieties only).

Caneberry Rubus spp. (including blackberry);

Rubus caesius (youngberry);

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Rubus loganbaccus (loganberry);

Rubus idaeus (red and black raspberry); cultivars, varieties, and/or hybrids of these.

Celery Celery, Florence fennel (sweet anise, sweet fennel, finochio) (fresh leaves and stalks only).

Cherry Cherry, sweet, and cherry, tart.

Endive Endive, escarole.

Fruit, citrus Grapefruit, lemon, lime, orange, tangelo, tangerine, citrus citron, kumquat, and hybrids of these.

Garlic Garlic, great headed; garlic, and serpent garlic.

Lettuce Lettuce, head; and lettuce, leaf

Lettuce, head Lettuce, head; crisphead varieties only

Lettuce, leaf Lettuce, leaf; cos (romaine), butterhead varieties

Marjoram Origanum spp. (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram).

Melon Muskmelon, including hybrids and/or varieties of Cucumis melo (including true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw 

melon, honeydew melon, honey balls, Persian melon, golden pershaw melon, mango melon, pineapple melon, snake melon); and 

watermelon, including hybrids and/or varieties of (Citrullus spp.).

Muskmelon Cucumis melo (includes true cantaloupe, cantaloupe, casaba, Santa Claus melon, crenshaw melon, honeydew melon, honey balls, Persian 

melon, golden pershaw melon, mango melon, pineapple melon, snake melon, and other varieties and/or hybrids of these.)

Onion Bulb onion; green onion; and garlic.

Onion, bulb Bulb onion; garlic; great headed garlic; serpent garlic; Chinese onion; pearl onion; potato onion; and shallot, bulb.

Onion, green Green onion; lady's leek; leek; wild leek; Beltsville bunching onion; fresh onion; tree onion, tops; Welsh onion; and shallot, fresh leaves.

Peach Peach, nectarine

Pea Cajanus cajan (includes pigeon pea); Cicer spp. (includes chickpea and garbanzo bean); Lens culinaris (lentil); Pisum spp. (includes dwarf 

pea, garden pea, green pea, English pea, field pea, and edible pod pea). [Note: A variety of pesticide tolerances have been previously 

established for pea and/or bean. Chickpea/garbanzo bean is now classified in both the bean and the pea categories. For garbanzo

bean/chickpea only, the highest established pea or bean tolerance will apply to pesticide residues found in this commodity.]

Pea, dry All peas in dry form only.

Pea, succulent All peas in succulent form only.

Pepper All varieties of pepper including pimento and bell, hot, and sweet pepper.

Radish, 

oriental, roots

Raphanus sativus var. longipinnatus (roots and tops), including Chinese or Japanese radish (both white and red), winter radish, daikon, lobok, 

lo pak, and other cultivars and/or hybrids of these.

Radish, 

oriental, tops)

Raphanus sativus var. longipinnatus (roots and tops), including Chinese or Japanese radish (both white and red), winter radish, daikon, lobok, 

lo pak, and other cultivars and/or hybrids of these.

Rapeseed Brassica napus, B. campestris, and Crambe abyssinica (oilseed-producing varieties only which include canola and crambe.)

Raspberry Rubus spp. (including bababerry; black raspberry; blackcap; caneberry; framboise; frambueso; himbeere; keriberry; mayberry; red raspberry; 

thimbleberry; tulameen; yellow raspberry; and cultivars, varieties, and/or hybrids of these).

Sorghum, 

grain, grain

Sorghum spp. [sorghum, grain, sudangrass (seed crop), and hybrids of these grown for its seed].

Sorghum, 

forage, stover

Sorghum spp. [sorghum, forage; sorghum, stover; sudangrass, and hybrids of these grown for forage and/or stover.

Squash Pumpkin, summer squash, and winter squash.

Sugar apple Annona squamosa L. (sugar apple, sweetsop, anon), and its hybrid A. squamosa L. x A. cherimoya M. (atemoya). Also A. reticulata L. (true 

custard apple).

Squash, 

summer

Fruits of the gourd (Cucurbitaceae) family that are consumed when immature, 100% of the fruit is edible either cooked or raw, once picked it 

cannot be stored, has a soft rind which is easily penetrated, and if seeds were harvested they would not germinate; e.g., Cucurbita pepo (i.e., 

crookneck squash, straightneck squash, scallop squash, and vegetable marrow); Lagenaria spp. (i.e., spaghetti squash, hyotan, cucuzza); 

Luffa spp. (i.e., hechima, Chinese okra); Momordica spp. (i.e., bitter melon, balsam pear, balsam apple, Chinese cucumber); Sechium edule

(chayote); and other cultivars and/or hybrids of these.

Sweet potato Sweet potato, yam.

Tangerine Tangerine (mandarin or mandarin orange); clementine; Mediterranean mandarin; satsuma mandarin; tangelo; tangor; cultivars, varieties, 

and/or hybrids of these.

Tomato Tomato, tomatillo.

Turnip tops or 

turnip greens

Broccoli raab (raab, raab salad), hanover salad, turnip tops (turnip greens).

Wheat Wheat, triticale.

(h) Unless otherwise specified in this paragraph or in tolerance regulations prescribed in this part for specific pesticide 

chemicals, the raw agricultural commodity or processed food to be examined for pesticide residues, shall consist of the 

whole raw agricultural commodity or processed food.

(1) The raw agricultural commodity bananas, when examined for pesticide residues, shall not include any crown 

tissue or stalk.

(2) Shell shall be removed and discarded from nuts before examination for pesticide residues.

(3) Caps (hulls) shall be removed and discarded from strawberries before examination for pesticide residues.

(4) Stems shall be removed and discarded from melons before examination for pesticide residues.

(5) Roots, stems, and outer sheaths (or husks) shall be removed and discarded from garlic bulbs and dry bulb onions, 

and only the garlic cloves and onion bulbs shall be examined for pesticide residues.

(6) Where a tolerance is established on a root vegetable including tops and/or with tops, and the tops and the roots 

are marketed together, they shall be analyzed separately and neither the pesticide residue on the roots nor the pesticide 

residue on the tops shall exceed the tolerance level, except that in the case of carrots, parsnips, and rutabagas, the tops 

shall be removed and discarded before analyzing roots for pesticide residues.

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(7) The crowns (leaves at the top of the fruit) shall be removed and discarded from pineapples before examination for 

pesticide residues.

(8) The term lima beans means the beans and the pod.

(9) The term peanuts means the peanut meat after removal of the hulls.

(10) For processed foods consisting primarily of one ingredient and sold in a form requiring further preparation prior to 

consumption (e.g., fruit juice concentrates, dehydrated vegetables, and powdered potatoes), the processed food to be 

examined for residues shall be the whole processed commodity after compensating for or reconstituting to the 

commodity's normal moisture content, unless a tolerance for the concentrated or dehydrated food form is included in this 

part. If there exists a tolerance for a specific pesticide on the processed food in its concentrated or dehydrated food form, 

for the purpose of determining whether the food is in compliance with that tolerance, the processed food to be examined 

for residues shall be the whole processed commodity on an “as is” basis.

(i) The term pesticide chemical shall have the meaning specified in FFDCA section 201(q)(1), as amended, except as 

provided in §180.4.

(j) The term negligible residue means any amount of a pesticide chemical remaining in or on a raw agricultural 

commodity or group of raw agricultural commodities that would result in a daily intake regarded as toxicologically 

insignificant on the basis of scientific judgment of adequate safety data. Ordinarily this will add to the diet an amount which

will be less than 1/2,000th of the amount that has been demonstrated to have no effect from feeding studies on the most 

sensitive animal species tested. Such toxicity studies shall usually include at least 90-day feeding studies in two species of 

mammals.

(k) The term nonperishable raw agricultural commodity means any raw agricultural commodity not subject to rapid 

decay or deterioration that would render it unfit for consumption. Examples are cocoa beans, coffee beans, field-dried 

beans, field-dried peas, grains, and nuts. Not included are eggs, milk, meat, poultry, fresh fruits, and vegetables such as 

onions, parsnips, potatoes, and carrots.

(l) The term tolerance with regional registration means any tolerance which is established for pesticide residues 

resulting from the use of the pesticide pursuant to a regional registration. Such a tolerance is supported by residue data 

from specific growing regions for a raw agricultural commodity. Individual tolerances with regional registration are 

designated in separate subsections in 40 CFR 180.101 through 180.999, as appropriate. Additional residue data which are 

representative of the proposed use area are required to expand the geographical area of usage of a pesticide on a raw 

agricultural commodity having an established “tolerance with regional registration.” Persons seeking geographically 

broader registration of a crop having a “tolerance with regional registration” should contact the appropriate EPA product 

manager concerning additional residue data required to expand the use area.

(m) The term pesticide chemical residue shall have the meaning specified in FFDCA section 201(q)(2), as amended, 

except as provided in §180.4.

(n) The term food commodity means: 

(1) Any raw agricultural commodity (food or feed) as defined in section 201(r) of the Federal Food, Drug, and 

Cosmetic Act (FFDCA); and 

(2) Any processed food or feed as defined in section 201(gg) of the FFDCA. 

[36 FR 22540, Nov. 25, 1971]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.1, see the List of CFR Sections Affected, which appears in the 

Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.3 Tolerances for related pesticide chemicals.

(a) Pesticide chemicals that cause related pharmacological effects will be regarded, in the absence of evidence to the 

contrary, as having an additive deleterious action. (For example, many pesticide chemicals within each of the following 

groups have related pharmacological effects: Chlorinated organic pesticides, arsenic-containing chemicals, metallic 

dithiocarbamates, cholinesterase-inhibiting pesticides.)

(b) Tolerances established for such related pesticide chemicals may limit the amount of a common component (such 

as As2O3) that may be present, or may limit the amount of biological activity (such as cholinesterase inhibition) that may 

be present, or may limit the total amount of related pesticide chemicals (such as chlorinated organic pesticides) that may 

be present.

(c)(1) Where tolerances for inorganic bromide in or on the same raw agricultural commodity are set in two or more 

sections in this part (example: §§180.123 and 180.199), the overall quantity of inorganic bromide to be tolerated from use 

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of the same pesticide in different modes of application or from two or more pesticide chemicals for which tolerances are 

established is the highest of the separate applicable tolerances. For example, where the bromide tolerance on asparagus 

from methyl bromide commodity fumigation is 100 parts per million (40 CFR 180.123) and on asparagus from methyl 

bromide soil treatment is 300 parts per million (40 CFR 180.199), the overall inorganic bromide tolerance for asparagus 

grown on methyl bromide-treated soil and also fumigated with methyl bromide after harvest is 300 parts per million.

(2) Where tolerances are established in terms of inorganic bromide residues only from use of organic bromide 

fumigants on raw agricutural commodities, such tolerances are sufficient to protect the public health, and no additional 

concurrent tolerances for the organic pesticide chemicals from such use are necessary. This conclusion is based on 

evidence of the dissipation of the organic pesticide or its conversion to inorganic bromide residues in the food when ready 

to eat.

(d)(1) Where tolerances are established for both calcium cyanide and hydrogen cyanide on the same raw agricultural 

commodity, the total amount of such pesticides shall not yield more residue than that permitted by the larger of the two 

tolerances, calculated as hydrogen cyanide.

(2) Where tolerances are established for residues of both O,O-diethyl S-[2-(ethylthio)ethyl] phosphorodithioate and 

demeton (a mixture of O,O-diethyl O-(and S-) [2-(ethylthio)ethyl] phosphorothioates) on the same raw agricultural 

commodity, the total amount of such pesticides shall not yield more residue than that permitted by the larger of the two 

tolerances, calculated as demeton.

(3) Where tolerances are established for both terpene polychlorinates (chlorinated mixture of camphene, pinene, and 

related terpenes, containing 65-66 percent chlorine) and toxaphene (chlorinated camphene containing 67-69 percent 

chlorine) on the same raw agricultural commodities, the total amount of such pesticides shall not yield more residue than 

that permitted by the larger of the two tolerances, calculated as a chlorinated terpene of molecular weight 396.6 containing 

67 percent chlorine.

(4) Where a tolerance is established for more than one pesticide containing arsenic found in, or on a raw agricultural 

commodity, the total amount of such pesticide shall not exceed the highest established tolerance calculated as As2O3.

(5) Where tolerances are established for more than one member of the class of dithiocarbamates listed in paragraph 

(e)(3) of this section on the same raw agricultural commodity, the total residue of such pesticides shall not exceed that 

permitted by the highest tolerance established for any one member of the class, calculated both as zinc 

ethylenebisdithiocarbamate and carbon disulfide. The tolerance based on zinc ethylenebisdithiocarbamate shall first be 

multiplied by 0.6 to convert it to the equivalent carbon disulfide tolerance, and then the carbon disulfide tolerance levels 

will be compared to determine the highest tolerance level per raw agricultural commodity.

(6) Where tolerances are established for residues of both S,S,S-tributyl phosphorotrithioate and tributyl 

phosphorotrithioite in or on the same raw agricultural commodity, the total amount of such pesticides shall not yield more 

residue than that permitted by the higher of the two tolerances, calculated as S,S,S-tributyl phosphorotrithioate.

(7) Where tolerances are established for residues of O,S-dimethyl phosphoramidothioate, resulting from the use of 

acephate (O,S-dimethyl acetylphos-phoramidothioate) and/or O,S - dimethylphosphoramidothioate on the same 

agricultural commodity, the total amount of O,S-dimethyl-phosphoramidothioate shall not yield more residue than that 

permitted by the higher of the two tolerances.

(8) Where a tolerance is established for more than one pesticide having the metabolites 1-(3,4-dichlorophenyl)-3-

methylurea (DCPMU) and 3,4-dichlorophenylurea (DCPU) found in or on a raw agricultural commodity, the total amount of 

such residues shall not exceed the highest established tolerance for a pesticide having these metabolites.

(9) Where a tolerance is established for more than one pesticide having as metabolites compounds containing the 

benzimidazole moiety found in or on a raw agricultural commodity, the total amount of such residues shall not exceed the 

highest established tolerance for a pesticide having these metabolites.

(10) Where a tolerance is established for triclopyr, chloropyrifos, and chlorpyrifos-methyl having the common 

metabolite 3,5,6-trichloro-2-pyridinol on the same raw agricultural commodity, the total amount of such residues shall not 

exceed the highest established tolerance for any of the pesticides having the metabolites.

(11) Where tolerances are established for more than one pesticide having the metabolite 3,5,6-trichloro-2-pyridinol 

found in or on the raw agricultural commodity, the total amount of such residues shall not exceed the highest established 

tolerance for a pesticide having this metabolite.

(12) Where tolerances are established for residues of methomyl, resulting from the use of thiodicarb and/or methomyl 

on the same raw agricultural commodity, the total amount of methomyl shall not yield more residue than that permitted by 

the higher of the two tolerances.

(e) Except as noted in paragraphs (e)(1) and (2) of this section, where residues from two or more chemicals in the 

same class are present in or on a raw agricultural commodity the tolerance for the total of such residues shall be the same 

as that for the chemical having the lowest numerical tolerance in this class, unless a higher tolerance level is specifically 

provided for the combined residues by a regulation in this part.

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(1) Where residues from two or more chemicals in the same class are present in or on a raw agricultural commodity 

and there are available methods that permit quantitative determination of each residue, the quantity of combined residues 

that are within the tolerance may be determined as follows:

(i) Determine the quantity of each residue present.

(ii) Divide the quantity of each residue by the tolerance that would apply if it occurred alone, and multiply by 100 to 

determine the percentage of the permitted amount of residue present.

(iii) Add the percentages so obtained for all residues present.

(iv) The sum of the percentages shall not exceed 100 percent.

(2) Where residues from two or more chemicals in the same class are present in or on a raw agricultural commodity 

and there are available methods that permit quantitative determinations of one or more, but not all, of the residues, the 

amounts of such residues as may be determinable shall be deducted from the total amount of residues present and the 

remainder shall have the same tolerance as that for the chemical having the lowest numerical tolerance in that class. The 

quantity of combined residues that are within the tolerance may be determined as follows: 

(i) Determine the quantity of each determinable residue present.

(ii) Deduct the amounts of such residues from the total amount of residues present and consider the remainder to 

have the same tolerance as that for the chemical having the lowest numerical tolerance in that class.

(iii) Divide the quantity of each determinable residue by the tolerance that would apply if it occurred alone and the 

quantity of the remaining residue by the tolerance for the chemical having the lowest numerical tolerance in that class and 

multiply by 100 to determine the percentage of the permitted amount of residue present.

(iv) Add the percentages so obtained for all residues present.

(v) The sum of the percentages shall not exceed 100 percent.

(3) The following pesticides are members of the class of dithiocarbamates:

A mixture of 5.2 parts by weight of ammoniates of [ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis 

[dithiocarbamic acid] bimolecular and trimolecular cyclic anhydrosulfides and disulfides.

2-Chloroallyl diethyldithiocarbamate.

Coordination product of zinc ion and maneb containing 20 percent manganese, 2.5 percent zinc, and 77.5 percent 

ethylenebisdithiocarbamate.

Ferbam.

Maneb.

Manganous dimethyldithiocarbamate.

Sodium dimethyldithiocarbamate.

Thiram.

Zineb.

Ziram.

(4) The following are members of the class of chlorinated organic pesticides:

Aldrin.

BHC (benzene hexachloride).

1,1-Bis(p-chlorophenyl)-2,2,2-trichloroethanol.

Chlorbenside (p-chlorobenzyl p-chlorophenyl sulfide).

Chlordane.

Chlorobenzilate (ethyl 4,4′-dichlorobenzilate).

p-Chlorophenoxyacetic acid.

p-Chlorophenyl-2,4,5-trichlorophenyl sulfide.

2,4-D (2,4-dichlorophenoxyacetic acid).

DDD (TDE).

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DDT.

1,1-Dichloro-2,2-bis(p-ethylphenyl) ethane.

2,6-Dichloro-4-nitroaniline.

2,4-Dichlorophenyl p-nitrophenyl ether.

Dieldrin.

Dodecachlorooctahydro-1,3,4-metheno-2H-cyclobuta[cd]pentalene.

Endosulfan (6,7,8,9,10,10-hexachloro-1,5,5a, 6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3-oxide).

Endosulfan sulfate (6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide).

Heptachlor (1,4,5,6,7,8,8-heptachlor-3a,4,7, 7a-tetrahydro-4,7-methanoindene).

Heptachlor epoxide (1,4,5,6,7,8,8-heptachloro-2,3-epoxy-2,3,3a,4,7,7a-hexahydro-4,7-methanoindene).

Hexachlorophene (2,2′-methylenebis(3,4,6-trichlorophenol) and its monosodium salt.

Isopropyl 4,4′-dichlorobenzilate.

Lindane.

Methoxychlor.

Ovex (p-chlorophenyl p-chlorobenzenesulfonate).

Sesone (sodium 2,4-dichlorophenoxyethyl sulfate, SES).

Sodium 2,4-dichlorophenoxyacetate.

Sodium trichloroacetate.

Sulphenone (p-chlorophenyl phenyl sulfone).

Terpene polychlorinates (chlorinated mixture of camphene, pinene, and related terpenes 65-66 percent chlorine).

2,3,5,6-Tetrachloronitrobenzene.

Tetradifon (2,4,5,4′-tetrachlorodiphenyl sulfone).

Toxaphene (chlorinated camphene).

Trichlorobenzoic acid.

Trichlorobenzyl chloride.

(5) The following are members of the class of cholinesterase-inhibiting pesticides:

Acephate (O,S-dimethyl acetyl-phosphoramidothioate) and its cholinesterase-inhibiting metabolite O,S-dimethyl 

phosphoramidothioate.

Aldicarb (2-methyl-2-(methylthio) propionaldehyde O-(methylcarbamoyl)oxime) and its chlorinesterase-inhibiting metabolites 

2-methyl-2-(methylsulfinyl)propionaldehyde O-(methycarbamoyl) oxime and 2-methyl-2-(methylsulfonyl)propionaldehyde 

O-(methylcarbamoyl)oxime.

4-tert-Butyl-2-chlorophenyl methyl methyl phosphoramidate.

S-[(tert-Butylthio)methyl] O,O-diethyl phosphorodithioate and its cholinesterase-inhibiting metabolites.

Carbaryl (1-naphthyl N-methylcarbamate).

Carbofuran (2,3,-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate).

Carbofuran metabolite (2,3-dihydro-2,2-dimethyl-3-hydroxy-7-benofuranyl N-methylcarbamate).

Carbophenothion (S-[(p-chlorophenyl) thiolmethyl] O,O-diethyl phosphorodithioate) and its cholinesterase-inhibiting metabolites. 

Chlorpyrifos (O,O-diethyl O-(3,5,6-trichloro-2-pyridyl)phosphorothioate).

Chlorpyrifos-methyl (O,O-dimethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate.

2-Chloro-1-(2,4,5-trichlorophenyl)vinyl dimethyl phosphate.

2-Chloro-1-(2,4-dichlorophenyl) vinyl diethyl phosphate.

Coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl phosran-7-yl phosphate).

Coumaphos oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyphorothioate).

Dialifor (S-(2-chloro-1-phthalimidoethyl) O,O-diethyl phosphorodithioate).

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Dialifor oxygen analog (S-(2-chloro-1-phthalimidoethyl) O,O-diethyl phosphorothioate).

Demeton (a mixture of O,O-diethyl O-(and S) [2-ethylthio)ethyl] phosphorothioates).

Ethiolate (S-ethyl diethylthiocarbamate).

2,2-Dichlorovinyl dimethyl phosphate.

O,O-Diethyl S-[2-(ethylthio)ethyl] phosphorodithioate and its cholinesterase-inhibiting metabolites.

O,O-Diethyl O-(2-diethylamino-6-methyl-4-pyrimidinyl) phosphorothioate and its oxygen analog diethyl 2-diethylamino-6-methyl-4-

pyrimidinyl phosphate.

O,O-Diethyl O-(2-isoprophyl-4-methyl-6-pyrimidinyl) phosphorothioate.

O,O-Diethyl O-[p-(methylsulfinyl)phenyl] phosphorothioate and its cholinesterase-inhibiting metabolites.

Diethyl 2-pyrazinyl phosphate.

O,O-Diethyl O-2-pyrazinyl phosphorothioate.

S-(O,O-Diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide

S-(O,O-Diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide

2-(Dimethylamino)-5.6-dimethyl-4-pyrimidinyl dimethylcarbamate and its metabolites 5,6-dimethyl-2-(formylmethylamino)-4-

pyrimidinyl dimethylcarbamate and 5,6-dimethyl-2-(methylamino)-4-pyrimidinyl dimethylcarbamate (both calculated as parent).

Dimethoate (O,O-dimethyl S-(N-methyl-carbamoylmethyl) phosphorodithioate).

Dimethoate oxygen analog (O,O-dimethyl S-(N-methylcarbamoylmethyl) phosphorothioate).

O,O-Dimethyl O-p-(dimethylsulfamoyl) phenyl phosphate.

O,O-Dimethyl O-p-(dimethylsulfamoyl) phenyl phosphorothioate.

3,5-Dimethyl-4-(methylthio) phenyl methylcarbamate.

O,O-Dimethyl S-[4-oxo-1,2,3-benzotriazin-3-(4H)-ylmethyl] phosphorodithioate.

Dimethyl phosphate of 3-hydroxy-N,N-dimethyl-cis-crotonamide.

Dimethyl phosphate of 3-hydroxy-N-methyl-cis-crotonamide.

Dimethyl phosphate of α-methylbenzyl 3-hydroxy-cis-crotonate.

O,O-Dimethyl 2,2,2-trichloro-1-hydroxyethyl phosphonate.

O,O-Dimethyl phosphorodithioate, S-ester with 4-(mercaptomethyl)-2-methozy-Δ2-1,3,4-thiadiazolin-5-one.

Dioxathion (2,3-p-dioxanedithiol S,S-bis (O,O-diethylphosphorodithioate)) containing approximately 70 percent cis and trans isomers 

and approximately 30 percent related compounds.

EPN.

Ethephon ((2- - chloroethyl) phosphonic acid).

Ethion.

Ethion oxygen analog (S-[[(diethoxyphosphinothioyl)thio] methyl] O,O-diethyl phosphorothioate).

O- Ethyl O-[4-(methylthio) phenyl] S-propyl phosphorodithioate and its cholinesterase-inhibiting metabolites.

O-Ethyl S,S-dipropylphosphorodithioate.

Ethyl 3-methyl-4-(methylthio)phenyl (1-methylethyl) phosphoramidate and its cholinesterase-inhibiting metabolites.

O-Ethyl S-phenyl ethylphosphonodithioate.

O-Ethyl S-phenyl ethylphosphonothiolate.

m-(1-Ethylpropyl)phenyl methylcarbamate.

S-[2-Ethylsulfinyl)ethyl] O,O-dimethyl phosphorothioate and its cholinesterase-inhibiting metabolites, (primarily S-[2-(ethyl-sulfonyl)

ethyl] O,O-dimethyl phosphorothioate).

Fenthion (O,O-dimethyl O-[3-methyl-4-(methylthio)phenyl]phosphorothioate and its cholinesterase-inhibiting metabolites.

Malathion.

N-(Mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorodithioate).

N-(Mercaptomethyl)phthalimide S-(O,O-dimethyl phosphorothioate).

Methomyl (S-methyl N-[(methylcarbamoyl)oxy]thioacetimidate).

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1-Methoxycarbonyl-1-propen-2-yl dimethyl phosphate and its beta isomer.

m-(1-Methylbutyl)phenyl methylcarbamate.

Methyl parathion.

Naled (1,2-dibromo-2,2-dichloroethyl dimethyl phosphate).

Oxamyl (methyl N′,N′-dimethyl-N-[(methylcarbamoyl)oxy]-1-thiooxamimidate)

Parathion.

Phorate (O,O-diethyl S-(ethylthio)methyl phosphorodithioate) and its cholinesterase-inhibiting metabolites.

Phosalone (S-(6-chloro-3-mercaptomethyl)-2-benzoxazolinone) O,O-diethyl phosphorodithioate).

Phosphamidon (2-chloro-2-diethylcarbamoyl-1-methylvinyl dimethyl phosphate) including all of its related cholinesterase-inhibiting 

compounds. 

Pirimiphos-methyl O-[2-diethylamino-6-methyl-pyrimidinyl) O,O-dimethyl phosphorothioate

Ronnel.

Schradan (octamethylpyrophosphoramide).

Tetraethyl pyrophosphate.

O,O,O′,O′-Tetramethyl O,O′-sulfinyldi-p-phenylene phosphorothioate.

O,O,O′,O′-Tetramethyl O,O′-thiodi-p-phenylene phosphorothioate.

Tributyl phosphorotritlioite.

S,S,S-Tributyl phosphorothrithioate.

3,4,5-Trimethylphenyl methylcarbamate and its isomer 2,3,5-trimethylphenyl methylcarbamate.

(6) The following pesticides are members of the class of dinitrophenols:

2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate, mixture of.

4,6-Dinitro-o-cresol and its sodium salt.

Dinoseb (2-sec-butyl-4,6-dinitrophenol) and its alkanolamine, ammonium, and sodium salts.

[41 FR 8969, Mar. 2, 1976]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.3, see the List of CFR Sections Affected, which appears in the 

Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.4 Exceptions.

The substances listed in this section are excepted from the definitions of “pesticide chemical” and “pesticide chemical 

residue” under FFDCA section 201(q)(3) and are therefore exempt from regulation under FFDCA section 402(a)(2)(B) and 

408. These substances are subject to regulation by the Food and Drug Administration as food additives under FFDCA 

section 409.

(a) Inert ingredients in food packaging treated with a pesticide, when such inert ingredients are the components of the 

food packaging material (e.g. paper and paperboard, coatings, adhesives, and polymers).

(b) [Reserved]

[63 FR 10720, Mar. 4, 1998, as amended at 73 FR 54976, Sept. 24, 2008]

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§180.5 Zero tolerances.

A zero tolerance means that no amount of the pesticide chemical may remain on the raw agricultural commodity when 

it is offered for shipment. A zero tolerance for a pesticide chemical in or on a raw agricultural commodity may be 

established because, among other reasons:

(a) A safe level of the pesticide chemical in the diet of two different species of warm-blooded animals has not been 

reliably determined.

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(b) The chemical is carcinogenic to or has other alarming physiological effects upon one or more of the species of the 

test animals used, when fed in the diet of such animals.

(c) The pesticide chemical is toxic, but is normally used at times when, or in such manner that, fruit, vegetables, or 

other raw agricultural commodities will not bear or contain it.

(d) All residue of the pesticide chemical is normally removed through good agricultural practice such as washing or 

brushing or through weathering or other changes in the chemical itself, prior to introduction of the raw agricultural 

commodity into interstate commerce.

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§180.6 Pesticide tolerances regarding milk, eggs, meat, and/or poultry; statement of policy.

(a) When establishing tolerances for pesticide residues in or on raw agricultural commodities, consideration is always 

given to possible residues of those pesticide chemicals or their conversion products entering the diet of man through the 

ingestion of milk, eggs, meat, and/or poultry produced by animals fed agricultural products bearing such pesticide 

residues. In each instance an evaluation of all available data will result in a conclusion either:

(1) That finite residues will actually be incurred in these foods from feed use of the raw agricultural commodity 

including its byproducts; or

(2) That it is not possible to establish with certainty whether finite residues will be incurred, but there is a reasonable 

expectation of finite residues; or

(3) That it is not possible to establish with certainty whether finite residues will be incurred, but there is no reasonable 

expectation of finite residues.

(b) When the data show that finite residues will actually be incurred in milk, eggs, meat, and/or poultry, a tolerance will 

be established on the raw agricultural commodity used as feed provided that tolerances can be established at the same 

time, on the basis of the toxicological and other data available, for the finite residues incurred in milk, eggs, meat, and/or 

poultry. When it is not possible to determine with certainty whether finite residues will be incurred in milk, eggs, meat, 

and/or poultry but there is a reasonable expectation of finite residues in light of data reflecting exaggerated pesticides 

levels in feeding studies, a tolerance will be established on the raw agricultural commodity provided that appropriate 

tolerances can be established at the same time, on the basis of the toxicological and other data available, for the finite 

residues likely to be incurred in these foods through the feed use of the raw agricultural commodity or its byproducts. 

When it is not possible to determine with certainty whether finite residues will be incurred in milk, eggs, meat, and/or 

poultry but there is no reasonable expectation of finite residues in light of data such as those reflecting exaggerated 

pesticide levels in feeding studies and those elucidating the biochemistry of the pesticide chemical in the animal, a 

tolerance may be established on the raw agricultural commodity without the necessity of a tolerance on food products 

derived from the animal.

(c) The principles outlined in paragraphs (a) and (b) of this section will also be followed with respect to tolerances for 

residues which will actually be incurred or are reasonably to be expected in milk, eggs, meat, and/or poultry by the use of 

pesticides directly on the animal or administered purposely in the feed or drinking water.

(d) Tolerances contemplated by paragraphs (a) and (b) of this section will in addition to toxicological considerations 

be conditioned on the availability of a practicable analytical method to determine the pesticide residue; that is, the method 

must be sensitive and reliable at the tolerance level or in special cases at a higher level where such level is deemed 

satisfactory and safe in light of the toxicity of the pesticide residue and of the unlikelihood of such residue exceeding the 

tolerance. The analytical methods to be used for enforcement purposes will be those set forth in the “Pesticide Analytical 

Manual” (see §180.101(c)). The sensitivities of these methods are expressed in that manual.

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Subpart B—Procedural Regulations

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§180.7 Petitions proposing tolerances or exemptions for pesticide residues in or on raw agricultural 

commodities or processed foods.

(a) Petitions to be filed with the Agency under the provisions of FFDCA section 408(d) shall be submitted in duplicate. 

If any part of the material submitted is in a foreign language, it shall be accompanied by an accurate and complete English 

translation. The petition shall be accompanied by an advance deposit for fees described in §180.33. The petition shall 

state the petitioner's mail address to which notice of objection under FFDCA section 408(g)(2) may be sent. The petition 

must be signed by the petitioner or by his attorney or agent, or (if a corporation) by an authorized official.

(b) Petitions shall include the following information:

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(1) An informative summary of the petition and of the data, information, and arguments submitted or cited in support 

of the petition. Both a paper and electronic copy of the summary should be submitted. The electronic copy should be 

formatted according to the Office of Pesticide Programs' current standard for electronic data submission as specified at 

http://www.epa.gov/pesticides/regulating/registering/submissions/index.htm.

(2) A statement that the petitioner agrees that such summary or any information it contains may be published as a 

part of the notice of filing of the petition to be published under FFDCA section 408(d)(3) and as a part of a proposed or 

final regulation issued under FFDCA section 408.

(3) The name, chemical identity, and composition of the pesticide chemical residue and of the pesticide chemical that 

produces the residue.

(4) Data showing the recommended amount, frequency, method, and time of application of the pesticide chemical.

(5) Full reports of tests and investigations made with respect to the safety of the pesticide chemical, including full 

information as to the methods and controls used in conducting those tests and investigations.

(6) Full reports of tests and investigations made with respect to the nature and amount of the pesticide chemical 

residue that is likely to remain in or on the food, including a description of the analytical methods used. (See §180.34 for 

further information about residue tests.)

(7) Proposed tolerances for the pesticide chemical residue if tolerances are proposed.

(8) Practicable methods for removing any amount of the residue that would exceed any proposed tolerance.

(9) A practical method for detecting and measuring the levels of the pesticide chemical residue in or on the food, or for 

exemptions, a statement why such a method is not needed.

(10) If the petition relates to a tolerance for a processed food, reports of investigations conducted using the 

processing method(s) used to produce that food.

(11) Such information as the Administrator may require to make the determination under FFDCA section 408(b)(2)(C).

(12) Such information as the Administrator may require on whether the pesticide chemical may have an effect in 

humans that is similar to an effect produced by a naturally occurring estrogen or other endocrine effects.

(13) Information regarding exposure to the pesticide chemical residue due to any tolerance or exemption already 

granted for such residue.

(14) Information concerning any maximum residue level established by the Codex Alimentarius Commission for the 

pesticide chemical residue addressed in the petition. If a Codex maximum residue level has been established for the 

pesticide chemical residue and the petitioner does not propose that this level be adopted, a statement explaining the 

reasons for this departure from the Codex level.

(15) Such other data and information as the Administrator requires by regulation to support the petition.

(16) Reasonable grounds in support of the petition.

(c) The data specified under paragraphs (b)(1) through (b)(16) of this section should be on separate sheets or sets of 

sheets, suitably identified. If such data have already been submitted with an earlier application, the present petition may 

incorporate it by reference to the earlier one.

(d) Except as noted in paragraph (e) of this section, a petition shall not be accepted for filing if any of the data 

prescribed by FFDCA section 408(d) are lacking or are not set forth so as to be readily understood. The availability to the 

public of information provided to, or otherwise obtained by, the Agency under this part shall be governed by part 2 of this 

chapter. The Administrator shall make the full text of the summary referenced in paragraph (b)(1) of this section available 

to the public in the public docket at http://www.regulations.gov no later than publication in the FEDERAL REGISTER of the 

notice of the petition filing.

(e) The Administrator shall notify the petitioner within 15 days after its receipt of acceptance or nonacceptance of a 

petition, and if not accepted the reasons therefor. If petitioner desires, the petitioner may supplement a deficient petition 

after notification as to deficiencies. If the petitioner does not wish to supplement or explain the petition and requests in 

writing that it be filed as submitted, the petition shall be filed and the petitioner so notified.

(f) A notice of the filing of a petition for a pesticide chemical residue tolerance that the Administrator determines has 

met the requirements of paragraph (b) of this section shall be published in the FEDERAL REGISTER by the Administrator 

within 30 days after such determination. The notice shall state the name of the pesticide chemical residue and the 

commodities for which a tolerance is sought and announce the availability of a description of the analytical methods 

available to the Administrator for the detection and measurement of the pesticide chemical residue with respect to which 

the petition is filed or shall set forth the petitioner's statement of why such a method is not needed. The notice shall 

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explicitly reference the specific docket identification number in the public docket at http://www.regulations.gov where the 

full text of the summary required in paragraph (b) of this section is located, and refer interested parties to this document for 

further information on the petition. The full text of the summary may be omitted from the notice.

(g) The Administrator may request a sample of the pesticide chemical at any time while a petition is under 

consideration. The Administrator shall specify in its request for a sample of the pesticide chemical, a quantity which it 

deems adequate to permit tests of analytical methods used to determine residues of the pesticide chemical and of 

methods proposed by the petitioner for removing any residues of the chemical that exceed the tolerance proposed.

(h) The Administrator shall determine, in accordance with the Act, whether to issue an order that establishes, 

modifies, or revokes a tolerance regulation (whether or not in accord with the action proposed by the petitioner), whether 

to publish a proposed tolerance regulation and request public comment thereon under §180.29, or whether to deny the 

petition. The Administrator shall publish in the FEDERAL REGISTER such order or proposed regulation. After receiving 

comments on any proposed regulation, the Administrator may issue an order that establishes, modifies, or revokes a 

tolerance regulation. An order published under this section shall describe briefly how to submit objections and requests for 

a hearing under part 178 of this chapter. A regulation issued under this section shall be effective on the date of publication 

in the FEDERAL REGISTER unless otherwise provided in the regulation.

[70 FR 33360, June 8, 2005, as amended at 73 FR 75600, Dec. 12, 2008]

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§180.8 Withdrawal of petitions without prejudice.

In some cases the Administrator will notify the petitioner that the petition, while technically complete, is inadequate to 

justify the establishment of a tolerance or the tolerance requested by petitioner. This may be due to the fact that the data 

are not sufficiently clear or complete. In such cases, the petitioner may withdraw the petition pending its clarification or the 

obtaining of additional data. This withdrawal may be without prejudice to a future filing. A deposit for fees as specified in 

§180.33 shall accompany the resubmission of the petition.

[70 FR 33361, June 8, 2005]

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§180.9 Substantive amendments to petitions.

After a petition has been filed, the petitioner may submit additional information or data in support thereof, but in such 

cases the petition will be given a new filing date.

[70 FR 33361, June 8, 2005]

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§180.29 Establishment, modification, and revocation of tolerance on initiative of Administrator.

(a) Upon the Administrator's own initiative, the Administrator may propose, under FFDCA section 408(e), the issuance 

of a regulation establishing a tolerance for a pesticide chemical or exempting it from the necessity of a tolerance, or a 

regulation modifying or revoking an existing tolerance or exemption.

(b) The Administrator shall provide a period of not less than 60 days for persons to comment on the proposed 

regulation, except that a shorter period for comment may be provided if the Administrator for good cause finds that it would 

be in the public interest to do so and states the reasons for the finding in the notice of proposed rulemaking.

(c) After reviewing any timely comments received, the Administrator may by order establish, modify, or revoke a 

tolerance regulation, which order and regulation shall be published in the FEDERAL REGISTER. An order published under 

this section shall state that persons may submit objections and requests for a hearing in the manner described in part 178 

of this chapter.

(d) Any final regulation issued under this section shall be effective on the date of publication in the FEDERAL REGISTER

unless otherwise provided in the regulation.

[70 FR 33361, June 8, 2005]

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§180.30 Judicial review.

(a) Under FFDCA section 408(h), judicial review is available in the United States Courts of Appeal as to the following 

actions:

(1) Regulations establishing general procedures and requirements under FFDCA section 408(e)(1)(C).

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(2) Orders issued under FFDCA section 408(f)(1)(C) requiring the submission of data.

(3) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to establishment, modification, or revocation 

of a tolerance or exemption under FFDCA section 408(d)(4), or any regulation that is the subject of such an order. The 

underlying action here is Agency disposition of a petition seeking the establishment, modification, or revocation of a 

tolerance or exemption.

(4) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the denial of a petition under FFDCA 

section 408(d)(4).

(5) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the establishment, modification, 

suspension, or revocation of a tolerance or exemption under FFDCA section 408(e)(1)(A) or (e)(1)(B). The underlying 

action here is the establishment, modification, suspension, or revocation of a tolerance or exemption upon the initiative of 

EPA including EPA actions pursuant to FFDCA sections 408(b)(2)(B)(v), 408(b)(2)(E)(ii), 408(d)(4)(C)(ii), 408(l)(4), and 

408(q)(1).

(6) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to the revocation or modification of a 

tolerance or exemption under FFDCA section 408(f)(2) for noncompliance with requirements for the submission of data.

(7) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to rules issued under FFDCA sections 408

(n)(3) and 408(d) or (e) regarding determinations pertaining to State authority to establish regulatory limits on pesticide 

chemical residues.

(8) Orders issued under FFDCA section 408(g)(2)(C) ruling on objections to orders issued under FFDCA section 408

(n)(5)(C) authorizing States to establish regulatory limits not identical to certain tolerances or exemptions.

(b) Any issue as to which review is or was obtainable under paragraph (a) of this section shall not be the subject of 

judicial review under any other provision of law. In part, this means that, for the Agency actions subject to the objection 

procedure in FFDCA section 408(g)(2), judicial review is not available unless an adversely affected party exhausts these 

objection procedures, and any petition procedures preliminary thereto.

[70 FR 33362, June 8, 2005]

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§180.31 Temporary tolerances.

(a) A temporary tolerance (or exemption from a tolerance) established under the authority of FFDCA section 408(r) 

shall be deemed to be a tolerance (or exemption from the requirement of a tolerance) for the purposes of FFDCA section 

408(a)(1) or (a)(2) and for the purposes of §180.30.

(b) A request for a temporary tolerance or a temporary exemption from a tolerance by a person who has obtained or 

is seeking an experimental permit for a pesticide chemical under the Federal Insecticide, Fungicide, and Rodenticide Act 

shall be accompanied by such data as are available on subjects outlined in §180.7(b) and an advance deposit to cover 

fees as provided in §180.33.

(c) To obtain a temporary tolerance, a requestor must comply with the petition procedures specified in FFDCA section 

408(d) and §180.7 except as provided in this section.

(d) A temporary tolerance or exemption from a tolerance may be issued for a period designed to allow the orderly 

marketing of the raw agricultural commodities produced while testing a pesticide chemical under an experimental permit 

issued under authority of the Federal Insecticide, Fungicide, and Rodenticide Act if the Administrator concludes that the 

safety standard in FFDCA section 408(b)(2) or (c), as applicable, is met. Subject to the requirements of FFDCA section 

408(e), a temporary tolerance or exemption from a tolerance may be revoked if the experimental permit is revoked, or may 

be revoked at any time if it develops that the application for a temporary tolerance contains a misstatement of a material 

fact or that new scientific data or experience with the pesticide chemical indicates that it does not meet the safety standard 

in FFDCA section 408(b)(2) or (c), as applicable.

(e) Conditions under which a temporary tolerance is established shall include:

(1) A limitation on the amount of the chemical to be used on the designated crops permitted under the experimental 

permit.

(2) A limitation for the use of the chemical on the designated crops to bona fide experimental use by qualified persons 

as indicated in the experimental permit.

(3) A requirement that the person or firm which obtains the experimental permit for which the temporary tolerance is 

established will immediately inform the Environmental Protection Agency of any reports on findings from the experimental 

use that have a bearing on safety.

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(4) A requirement that the person or firm which obtained the experimental permit for which the temporary tolerance is 

established will keep records of production, distribution, and performance for a period of 2 years and, on request, at any 

reasonable time, make these records available to any authorized officer or employee of the Environmental Protection 

Agency.

[70 FR 33362, June 8, 2005]

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§180.32 Procedure for modifying and revoking tolerances or exemptions from tolerances.

(a) The Administrator on his/her own initiative may propose the issuance of a regulation modifying or revoking a 

tolerance for a pesticide chemical residue on raw agricultural commodities or processed foods or modifying or revoking an 

exemption from tolerance for such residue.

(b) Any person may file with the Administrator a petition proposing the issuance of a regulation modifying or revoking 

a tolerance or exemption from a tolerance for a pesticide chemical residue. The petition shall furnish reasonable grounds 

for the action sought. Reasonable grounds shall include an explanation showing wherein the person has a substantial 

interest in such tolerance or exemption from tolerance and an assertion of facts (supported by data if available) showing 

that new uses for the pesticide chemical have been developed or old uses abandoned, that new data are available as to 

toxicity of the chemical, or that experience with the application of the tolerance or exemption from tolerance may justify its 

modification or revocation. Evidence that a person has registered or has submitted an application for the registration of a 

pesticide under the Federal Insecticide, Fungicide, and Rodenticide Act will be regarded as evidence that the person has a 

substantial interest in a tolerance or exemption from the requirement of a tolerance for a pesticide chemical that consists 

in whole or in part of the pesticide. New data should be furnished in the form specified in §180.7(b) for submitting petitions,

as applicable.

(c) The procedures for completing action on an Administrator initiated proposal or a petition shall be those specified in 

§§180.29 and 180.7, as applicable.

[70 FR 33362, June 8, 2005]

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§180.33 Fees.

(a) Each petition for the establishment of a new tolerance or a tolerance higher than already established, shall be 

accompanied by a fee of $80,950, plus $2,025 for each raw agricultural commodity more than nine on which the 

establishment of a tolerance is requested, except as provided in paragraphs (b), (d), and (h) of this section. 

(b) Each petition for the establishment of a tolerance at a lower numerical level or levels than a tolerance already 

established for the same pesticide chemical, or for the establishment of a tolerance on additional raw agricultural 

commodities at the same numerical level as a tolerance already established for the same pesticide chemical, shall be 

accompanied by a fee of $18,500 plus $1,225 for each raw agricultural commodity on which a tolerance is requested. 

(c) Each petition for an exemption from the requirement of a tolerance or repeal of an exemption shall be 

accompanied by a fee of $14,925. 

(d) Each petition or request for a temporary tolerance or a temporary exemption from the requirement of a tolerance 

shall be accompanied by a fee of $32,325 except as provided in paragraph (e) of this section. A petition or request to 

renew or extend such temporary tolerance or temporary exemption shall be accompanied by a fee of $4,600. 

(e) A petition or request for a temporary tolerance for a pesticide chemical which has a tolerance for other uses at the 

same numerical level or a higher numerical level shall be accompanied by a fee of $16,075, plus $1,225 for each raw 

agricultural commodity on which the temporary tolerance is sought. 

(f) Each petition for revocation of a tolerance shall be accompanied by a fee of $10,125. Such fee is not required 

when, in connection with the change sought under this paragraph, a petition is filed for the establishment of new 

tolerances to take the place of those sought to be revoked and a fee is paid as required by paragraph (a) of this section.

(g) If a petition or a request is not accepted for processing because it is technically incomplete, the fee, less $2,025 

for handling and initial review, shall be returned. If a petition is withdrawn by the petitioner after initial processing, but 

before significant Agency scientific review has begun, the fee, less $2,025 for handling and initial review, shall be returned.

If an unacceptable or withdrawn petition is resubmitted, it shall be accompanied by the fee that would be required if it were 

being submitted for the first time.

(h) Each petition for a crop group tolerance, regardless of the number of raw agricultural commodities involved, shall 

be accompanied by a fee equal to the fee required by the analogous category for a single tolerance that is not a crop 

group tolerance, i.e., paragraphs (a) through (f) of this section, without a charge for each commodity where that would 

otherwise apply. 

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(i) Objections under section 408(d)(5) of the Act shall be accompanied by a filing fee of $4,050.

(j) The person who files a petition for judicial review of an order under section 408(h) of the Act shall pay the costs of 

preparing the record on which the order is based unless the person has no financial interest in the petition for judicial 

review.

(k) No fee under this section will be imposed on the Interregional Research Project Number 4 (IR-4 Program).

(l) The Administrator may waive or refund part or all of any fee imposed by this section if the Administrator determines 

in his or her sole discretion that such a waiver or refund will promote the public interest or that payment of the fee would 

work an unreasonable hardship on the person on whom the fee is imposed. A request for waiver or refund of a fee shall be 

submitted to the Office of Pesticide Programs' Document Processing Desk at the appropriate address as set forth in 40 

CFR 150.17(a) or (b). A fee of $2,025 shall accompany every request for a waiver or refund, as specified in paragraph (m) 

of this section, except that the fee under this paragraph shall not be imposed on any person who has no financial interest 

in any action requested by such person under paragraphs (a) through (j) of this section. The fee for requesting a waiver or 

refund shall be refunded if the request is granted.

(m) All deposits and fees required by the regulations in this part shall be paid by money order, bank draft, or certified 

check drawn to the order of the Environmental Protection Agency. All deposits and fees shall be forwarded to the 

Environmental Protection Agency, Headquarters Accounting Operations Branch, Office of Pesticide Programs (Tolerance 

Fees), P.O. Box 360277M, Pittsburgh, PA 15251. The payments should be specifically labeled “Tolerance Petition Fees” 

and should be accompanied only by a copy of the letter or petition requesting the tolerance. The actual letter or petition, 

along with supporting data, shall be forwarded within 30 days of payment to the Office of Pesticide Programs' Document 

Processing Desk at the appropriate address as set forth in 40 CFR 150.17(a) or (b). A petition will not be accepted for 

processing until the required fees have been submitted. A petition for which a waiver of fees has been requested will not 

be accepted for processing until the fee has been waived or, if the waiver has been denied, the proper fee is submitted 

after notice of denial. A request for waiver or refund will not be accepted after scientific review has begun on a petition.

(n) This fee schedule will be changed annually by the same percentage as the percent change in the Federal General 

Schedule (GS) pay scale. In addition, processing costs and fees will periodically be reviewed and changes will be made to 

the schedule as necessary. When automatic adjustments are made based on the GS pay scale, the new fee schedule will 

be published in the FEDERAL REGISTER as a final rule to become effective 30 days or more after publication, as specified 

in the rule. When changes are made based on periodic reviews, the changes will be subject to public comment.

(o) No fee required by this section shall be levied during the period beginning on October 1, 2003, and ending 

September 30, 2008.

[68 FR 24371, May 7, 2003, as amended at 69 FR 12544, Mar. 17, 2004; 70 FR 33363, June 8, 2005; 71 FR 35547, June 21, 2006]

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§180.34 Tests on the amount of residue remaining.

(a) Data in a petition on the amount of residue remaining in or on a raw agricultural commodity should establish the 

residue that may remain when the pesticide chemical is applied according to directions registered under the Federal 

Insecticide, Fungicide, and Rodenticide Act, or according to directions contained in an application for registration. These 

data should establish the residues that may remain under conditions most likely to result in high residues on the 

commodity.

(b) The petition should establish the reliability of the residue data reported in it. Sufficient information should be 

submitted about the analytical method to permit competent analysts to apply it successfully.

(c) If the pesticide chemical is absorbed into a living plant or animal when applied (is systemic), residue data may be 

needed on each plant or animal on which a tolerance or exemption is requested.

(d) If the pesticide chemical is not absorbed into the living plant or animal when applied (is not systemic), it may be 

possible to make a reliable estimate of the residues to be expected on each commodity in a group of related commodities 

on the basis of less data than would be required for each commodity in the group, considered separately. 

(e) Each of the following groups of crops lists raw agricultural commodities that are considered to be related for the 

purpose of paragraph (d) of this section. Commodities not listed in this paragraph are not considered to be related for the 

purpose of paragraph (d) of this section.

(1) Apples, crabapples, pears, quinces.

(2) Avocados, papayas.

(3) Blackberries, boysenberries, dewberries, loganberries, raspberries.

(4) Blueberries, currants, gooseberries, huckleberries.

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(5) Cherries, plums, prunes.

(6) Oranges, citrus citron, grapefruit, kumquats, lemons, limes, tangelos, tangerines.

(7) Mangoes, persimmons.

(8) Peaches, apricots, nectarines.

(9) Beans, peas, soybeans (each in dry form).

(10) Beans, peas, soybeans (each in succulent form).

(11) Broccoli, brussels sprouts, cauliflower, kohlrabi.

(12) Cantaloups, honeydew melons, muskmelons, pumpkins, watermelons, winter squash.

(13) Carrots, garden beets, sugar beets, horseradish, parsnips, radishes, rutabagas, salsify roots, turnips.

(14) Celery, fennel.

(15) Cucumbers, summer squash.

(16) Lettuce, endive (escarole), Chinese cabbage, salsify tops.

(17) Onions, garlic, leeks, shallots (green, or in dry bulb form).

(18) Potatoes, Jerusalem-artichokes, sweetpotatoes, yams.

(19) Spinach, beet tops, collards, dandelion, kale, mustard greens, parsley, Swiss chard, turnip tops, watercress.

(20) Tomatoes, eggplants, peppers, pimentos.

(21) Pecans, almonds, brazil nuts, bush nuts, butternuts, chestnuts, filberts, hazelnuts, hickory nuts, walnuts.

(22) Field corn, popcorn, sweet corn (each in grain form).

(23) Milo, sorghum (each in grain form).

(24) Wheat, barley, oats, rice, rye (each in grain form).

(25) Alfalfa, Bermuda grass, bluegrass, brome grass, clovers, cowpea hay, fescue, lespedeza, lupines, orchard grass, 

peanut hay, peavine hay, rye grass, soybean hay, sudan grass, timothy, and vetch.

(26) Corn forage, sorghum forage.

(27) Sugarcane, cane sorghum.

[36 FR 22540, Nov. 25, 1971, as amended at 39 FR 28286, Aug. 6, 1974; 39 FR 28977, Aug. 13, 1974; 40 FR 6972, Feb. 18, 1975; 

45 FR 82928, Dec. 17, 1980; 48 FR 29860, June 29, 1983; 60 FR 26635, May 17, 1995; 73 FR 75600, Dec. 12, 2008]

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§180.35 Tests for potentiation.

Experiments have shown that certain cholinesterase-inhibiting pesticides when fed together to test animals are more 

toxic than the sum of their individual toxicities when fed separately. One substance potentiates the toxicity of the other. 

Important toxicological interactions also have been observed between pesticides and other substances. Wherever there is 

reason to believe that a pesticide chemical for which a tolerance is proposed may interact with other pesticide chemicals 

or other substances to which man is exposed, it may be necessary to require special experimental data regarding 

potentiation capacities to evaluate the safety of the proposed tolerance. This necessarily will be determined on a case-bycase basis.

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§180.40 Tolerances for crop groups.

(a) Group or subgroup tolerances may be established as a result of:

(1) A petition from a person who has submitted an application for the registration of a pesticide under the Federal 

Insecticide, Fungicide, and Rodenticide Act.

(2) On the initiative of the Administrator.

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(3) A petition by an interested person.

(b) The tables in §180.41 are to be used in conjunction with this section for the establishment of crop group 

tolerances. Each table in §180.41 lists a group of raw agricultural commodities that are considered to be related for the 

purposes of this section. Refer also to §180.1(g) for a listing of commodities for which established tolerances may be 

applied to certain other related and similar commodities.

(c) When there is an established or proposed tolerance for all of the representative commodities for a specific group 

or subgroup of related commodities, a tolerance may be established for all commodities in the associated group or 

subgroup. Tolerances may be established for a crop group or, alternatively, tolerances may be established for one or more 

of the subgroups of a crop group.

(d) The representative crops are given as an indication of the minimum residue chemistry data base acceptable to the 

Agency for the purposes of establishing a group tolerance. The Agency may, at its discretion, allow group tolerances when 

data on suitable substitutes for the representative crops are available (e.g., limes instead of lemons).

(e) Since a group tolerance reflects maximum residues likely to occur on all individual crops within a group, the 

proposed or registered patterns of use for all crops in the group or subgroup must be similar before a group tolerance is 

established. The pattern of use consists of the amount of pesticide applied, the number of times applied, the timing of the 

first application, the interval between applications, and the interval between the last application and harvest. The pattern of

use will also include the type of application; for example, soil or foliar application, or application by ground or aerial 

equipment.

(f) When the crop grouping contains commodities or byproducts that are utilized for animal feed, any needed 

tolerance or exemption from a tolerance for the pesticide in meat, milk, poultry and/or eggs must be established before a 

tolerance will be granted for the group as a whole. The representative crops include all crops in the group that could be 

processed such that residues may concentrate in processed food and/or feed. Processing data will be required prior to 

establishment of a group tolerance. Tolerances will not be granted on a group basis as to processed foods prepared from 

crops covered by the group tolerance.

(g) If maximum residues (tolerances) for the representative crops vary by more than a factor of 5 from the maximum 

value observed for any crop in the group, a group or subgroup tolerance will ordinarily not be established. In this case 

individual crop tolerances, rather than group tolerances, will normally be established.

(h) Alternatively, a commodity with a residue level significantly higher or lower than the other commodities in a group 

may be excluded from the group tolerance (e.g., cereal grains, except corn). In this case an individual tolerance at the 

appropriate level for the unique commodity would be established, if necessary. The alternative approach of excluding a 

commodity with a significantly higher or lower residue level will not be used to establish a tolerance for a commodity 

subgroup. Most subgroups have only two representative commodities; to exclude one such commodity and its related 

residue data would likely provide insufficient residue information to support the remainder of the subgroup. Residue data 

from crops additional to those representative crops in a grouping may be required for systemic pesticides.

(i) The commodities included in the groups will be updated periodically either at the initiative of the Agency or at the 

request of an interested party. Persons interested in updating this section should contact the Registration Division of the 

Office of Pesticide Programs.

(j) When EPA amends a crop group in a manner that expands or contracts the commodities that are covered by the 

group, EPA will initially retain the pre-existing as well as the revised crop group in the CFR. The revised crop group will 

have the same number as the pre-existing crop group; however, the revised crop group number will be followed by a 

hyphen and the final two digits of the year in which it was established (e.g., if Crop Group 1 is amended in 2007, the 

revised group will be designated as Crop Group 1-07). If the pre-existing crop group had crop subgroups, these subgroups 

will be numbered in a similar fashion in the revised crop group. The name of the revised crop group will not be changed 

from the pre-existing crop group unless the revision so changes the composition of the crop group that the pre-existing 

name is no longer accurate. Once a revised crop group is established, EPA will no longer establish tolerances under the 

pre-existing crop group. At appropriate times, EPA will amend tolerances for crop groups that have been superseded by 

revised crop groups to conform the pre-existing crop group to the revised crop group. Once all of the tolerances for the 

pre-existing crop group have been updated, the pre-existing crop group will be removed from the CFR.

(k) Establishment of a tolerance does not substitute for the additional need to register the pesticide under a 

companion law, the Federal Insecticide, Fungicide, and Rodenticide Act. The Registration Division of the Office of 

Pesticide Programs should be contacted concerning procedures for registration of new uses of a pesticide.

[60 FR 26635, May 17, 1995, as amended at 70 FR 33363, June 8, 2005; 72 FR 69155, Dec. 7, 2007; 75 FR 56014, Sept. 15, 2010]

 Back to Top

§180.41 Crop group tables.

(a) The tables in this section are to be used in conjunction with §180.40 to establish crop group tolerances.

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(b) Commodities not listed are not considered as included in the groups for the purposes of this paragraph, and 

individual tolerances must be established. Miscellaneous commodities intentionally not included in any group include 

asparagus, avocado, banana, fig, globe artichoke, hops, mango, papaya, pawpaw, peanut, persimmon, pineapple, water 

chestnut, and watercress.

(c) Each group is identified by a group name and consists of a list of representative commodities followed by a list of 

all commodity members for the group. If the group includes subgroups, each subgroup lists the subgroup name, the 

representative commodity or commodities, and the member commodities for the subgroup. Subgroups, which are a subset 

of their associated crop group, are established for some but not all crops groups.

(1) Crop Group 1: Root and Tuber Vegetables Group.

(i) Representative commodities. Carrot, potato, radish, and sugar beet.

(ii) Table. The following table 1 lists all the commodities included in Crop Group 1 and identifies the related crop 

subgroups.

TABLE 1—CROP GROUP 1: ROOT AND TUBER VEGETABLES

Commodities Related crop subgroups

Arracacha (Arracacia xanthorrhiza) 1C, 1D

Arrowroot (Maranta arundinacea) 1C, 1D

Artichoke, Chinese (Stachys affinis) 1C, 1D

Artichoke, Jerusalem (Helianthus tuberosus) 1C, 1D

Beet, garden (Beta vulgaris) 1A, 1B

Beet, sugar (Beta vulgaris) 1A

Burdock, edible (Arctium lappa) 1A, 1B

Canna, edible (Queensland arrowroot) (Canna indica) 1C, 1D

Carrot (Daucus carota) 1A, 1B

Cassava, bitter and sweet (Manihot esculenta) 1C, 1D

Celeriac (celery root) (Apium graveolens var. rapaceum) 1A, 1B

Chayote (root) (Sechium edule) 1C, 1D

Chervil, turnip-rooted (Chaerophyllum bulbosum). 1A, 1B

Chicory (Cichorium intybus) 1A, 1B

Chufa (Cyperus esculentus) 1C, 1D

Dasheen (taro) (Colocasia esculenta) 1C, 1D

Ginger (Zingiber officinale) 1C, 1D

Ginseng (Panax quinquefolius) 1A, 1B

Horseradish (Armoracia rusticana) 1A, 1B

Leren (Calathea allouia) 1C, 1D

Parsley, turnip-rooted (Petroselinum crispum var. tuberosum) 1A, 1B

Parsnip (Pastinaca sativa) 1A, 1B

Potato (Solanum tuberosum) 1C

Radish (Raphanus sativus) 1A, 1B

Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus) 1A, 1B

Rutabaga (Brassica campestris var. napobrassica) 1A, 1B

Salsify (oyster plant) (Tragopogon porrifolius). 1A, 1B

Salsify, black (Scorzonera hispanica) 1A, 1B

Salsify, Spanish (Scolymus hispanicus) 1A, 1B

Skirret (Sium sisarum) 1A, 1B

Sweet potato (Ipomoea batatas) 1C, 1D

Tanier (cocoyam) (Xanthosoma sagittifolium) 1C, 1D

Turmeric (Curcuma longa) 1C, 1D

Turnip (Brassica rapa var. rapa) 1A, 1B

Yam bean (jicama, manoic pea) (Pachyrhizus spp.) 1C, 1D

Yam, true (Dioscorea spp.) 1C, 1D

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 1, specifies the representative 

commodity(ies) for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 1 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 1A. Root vegetables 

subgroup.

Carrot, radish, and sugar beet. Beet, garden; beet, sugar; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; 

parsley, turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; 

turnip.

Crop Subgroup 1B. Root vegetables 

(except sugar beet) subgroup.

Carrot and radish. Beet, garden; burdock, edible; carrot; celeriac; chervil, turnip-rooted; chicory; ginseng; horseradish; parsley, 

turnip-rooted; parsnip; radish; radish, oriental; rutabaga; salsify; salsify, black; salsify, Spanish; skirret; turnip.

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Crop Subgroup 1C. Tuberous and corm 

vegetables subgroup.

Potato. Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; 

chayote (root); chufa; dasheen; ginger; leren; potato; sweet potato; tanier; turmeric; yam bean; yam, true.

Crop Subgroup 1D. Tuberous and corm 

vegetables (except potato) subgroup.

Sweet potato. Arracacha; arrowroot; artichoke, Chinese; artichoke, Jerusalem; canna, edible; cassava, bitter and sweet; 

chayote (root); chufa; dasheen; ginger; leren; sweet potato; tanier; turmeric; yam bean; yam, true.

(2) Crop Group 2. Leaves of Root and Tuber Vegetables (Human Food or Animal Feed) Group (Human Food or 

Animal Feed) Group.

(i) Representative commodities. Turnip and garden beet or sugar beet.

(ii) Commodities. The following is a list of all the commodities included in Crop Group 2:

CROP GROUP 2: LEAVES OF ROOT AND TUBER VEGETABLES (HUMAN FOOD OR ANIMAL FEED) GROUP—COMMODITIES

Beet, garden (Beta vulgaris)

Beet, sugar (Beta vulgaris)

Burdock, edible (Arctium lappa)

Carrot (Daucus carota)

Cassava, bitter and sweet (Manihot esculenta)

Celeriac (celery root) (Apium graveolens var. rapaceum)

Chervil, turnip-rooted (Chaerophyllum bulbosum)

Chicory (Cichorium intybus)

Dasheen (taro) (Colocasia esculenta)

Parsnip (Pastinaca sativa)

Radish (Raphanus sativus)

Radish, oriental (daikon) (Raphanus sativus subvar. longipinnatus)

Rutabaga (Brassica campestris var. napobrassica)

Salsify, black (Scorzonera hispanica)

Sweet potato (Ipomoea batatas)

Tanier (cocoyam) (Xanthosoma sagittifolium)

Turnip (Brassica rapa var. rapa)

Yam, true (Dioscorea spp.)

(3) Crop Group 3. Bulb Vegetables (Allium spp.) Group.

(i) Representative commodities. Onion, green; and onion, dry bulb.

(ii) Commodities. The following is a list of all the commodities in Crop Group 3.

CROP GROUP 3: BULB VEGETABLE (ALLIUM SPP.) GROUP—COMMODITIES

Garlic, bulb (Allium sativum)

Garlic, great headed, (elephant) (Allium ampeloprasum var. ampeloprasum)

Leek (Allium ampeloprasum, A. porrum, A. tricoccum)

Onion, dry bulb and green (Allium cepa, A. fistulosum)

Onion, Welsh, (Allium fistulosum)

Shallot (Allium cepa var. cepa)

(4) Crop Group 3-07. Bulb Vegetable Group. 

(i) Representative Commodities. Onion, bulb and onion, green.

(ii) Table. The following Table 1 lists all the commodities listed in Crop Group 3-07 and identifies the related crop 

subgroups.

TABLE 1—CROP GROUP 3-07: BULB VEGETABLE GROUP

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Commodities

Related crop 

subgroups

Chive, fresh leaves (Allium schoenoprasum L.) 3-07B

Chive, Chinese, fresh leaves (Allium tuberosum Rottler ex Spreng) 3-07B

Daylily, bulb (Hemerocallis fulva (L.) L. var. fulva) 3-07A

Elegans hosta (Hosta Sieboldiana (Hook.) Engl) 3-07B

Fritillaria, bulb (Fritillaria L. fritillary) 3-07A

Fritillaria, leaves (Fritillaria L. fritillary) 3-07B

Garlic, bulb (Allium sativum L. var. sativum) (A. sativum Common Garlic Group) 3-07A

Garlic, great headed, bulb (Allium ampeloprasum L. var. ampeloprasum) (A. ampeloprasum Great Headed Garlic Group) 3-07A

Garlic, Serpent, bulb (Allium sativum var. ophioscorodon or A. sativum Ophioscorodon Group) 3-07A

Kurrat (Allium kurrat Schweinf. Ex. K. Krause or A. ampeloprasum Kurrat Group) 3-07B

Lady's leek (Allium cernuum Roth) 3-07B

Leek Allium porrum L. (syn: A. ampeloprasum L. var. porrum (L.) J. Gay) (A.ampeloprasum Leek Group) 3-07B

Leek, wild (Allium tricoccum Aiton) 3-07B

Lily, bulb (Lilium spp. (Lilium Leichtlinii var. maximowiczii, Lilium lancifolium)) 3-07A

Onion, Beltsville bunching (Allium x proliferum (Moench) Schrad.) (syn: Allium fistulosum L. x A. cepa L.) 3-07B

Onion, bulb (Allium cepa L. var. cepa) (A. cepa Common Onion Group) 3-07A

Onion, Chinese, bulb (Allium chinense G. Don.) (syn: A. bakeri Regel) 3-07A

Onion, fresh (Allium fistulosum L. var. caespitosum Makino) 3-07B

Onion, green (Allium cepa L. var. cepa) (A. cepa Common Onion Group) 3-07B

Onion, macrostem (Allium macrostemom Bunge) 3-07B

Onion, pearl (Allium porrum var. sectivum or A. ampeloprasum Pearl Onion Group) 3-07A

Onion, potato, bulb (Allium cepa L. var. aggregatum G. Don.) (A. cepa Aggregatum Group) 3-07A

Onion, tree, tops (Allium x proliferum (Moench) Schrad. ex Willd.) (syn: A. cepa var. proliferum (Moench) Regel; A. cepa L. var. 

bulbiferum L.H. Bailey; A. cepa L. var. viviparum (Metz.) Alef.)

3-07B

Onion, Welsh, tops (Allium fistulosum L.) 3-07B

Shallot, bulb (Allium cepa var. aggregatum G. Don.) 3-07A

Shallot, fresh leaves (Allium cepa var. aggregatum G. Don.) 3-07B

Cultivars, varieties, and/or hybrids of these.

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 3-07, specifies the representative 

commodities for each subgroup and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 3-07: SUBGROUP LISTING

Representative 

commodities Commodities

Crop subgroup 3-07A.

Onion, bulb, subgroup.

Onion, bulb.

Daylily, bulb; fritillaria, bulb; garlic, bulb; garlic, great-headed, bulb; garlic, serpent, bulb; lily, bulb; onion, bulb; onion, Chinese, 

bulb; onion, pearl; onion, potato, bulb; shallot, bulb; cultivars, varieties, and/or hybrids of these.

Crop subgroup 3-07B.

Onion, green, subgroup.

Onion, green.

Chive, fresh leaves; chive, Chinese, fresh leaves; elegans hosta; fritillaria, leaves; kurrat; lady's leek; leek; leek, wild; Onion, 

Beltsville bunching; onion, fresh; onion, green; onion, macrostem; onion, tree, tops; onion, Welsh, tops; shallot, fresh leaves; 

cultivars, varieties, and/or hybrids of these.

(5) Crop Group 4. Leafy Vegetables (Except Brassica Vegetables) Group.

(i) Representative commodities. Celery, head lettuce, leaf lettuce, and spinach (Spinacia oleracea).

(ii) Table. The following table 1 lists all the commodities included in Crop Group 4 and identifies the related crop 

subgroups.

TABLE 1—CROP GROUP 4: LEAFY VEGETABLES (EXCEPT BRASSICA VEGETABLES) GROUP

Commodities Related crop subgroups

Amaranth (leafy amaranth, Chinese spinach, tampala) (Amaranthus spp.) 4A

Arugula (Roquette) (Eruca sativa) 4A

Cardoon (Cynara cardunculus) 4B

Celery (Apium graveolens var. dulce) 4B

Celery, Chinese (Apium graveolens var. secalinum) 4B

Celtuce (Lactuca sativa var. angustana) 4B

Chervil (Anthriscus cerefolium) 4A

Chrysanthemum, edible-leaved (Chrysanthemum coronarium var. coronarium) 4A

Chrysanthemum, garland (Chrysanthemum coronarium var. spatiosum) 4A

Corn salad (Valerianella locusta) 4A

Cress, garden (Lepidium sativum) 4A

Cress, upland (yellow rocket, winter cress) (Barbarea vulgaris) 4A

Dandelion (Taraxacum officinale) 4A

Dock (sorrel) (Rumex spp.) 4A

Endive (escarole) (Cichorium endivia) 4A

Fennel, Florence (finochio) (Foeniculum vulgare Azoricum Group) 4B

Lettuce, head and leaf (Lactuca sativa) 4A

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Orach (Atriplex hortensis) 4A

Parsley (Petroselinum crispum) 4A

Purslane, garden (Portulaca oleracea) 4A

Purslane, winter (Montia perfoliata) 4A

Radicchio (red chicory) (Cichorium intybus) 4A

Rhubarb (Rheum rhabarbarum) 4B

Spinach (Spinacia oleracea) 4A

Spinach, New Zealand (Tetragonia tetragonioides, T. expansa) 4A

Spinach, vine (Malabar spinach, Indian spinach) (Basella alba) 4A

Swiss chard (Beta vulgaris var. cicla) 4B

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 4, specifies the representative 

commodities for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 4 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 4A. Leafy greens 

subgroup.

Head lettuce and leaf lettuce, and 

spinach (Spinacia oleracea)

Amaranth; arugula; chervil; chrysanthemum, edible-leaved; chrysanthemum, garland; corn salad; cress, garden; cress, 

upland; dandelion; dock; endive; lettuce; orach; parsley; purslane, garden; purslane, winter; radicchio (red chicory); 

spinach; spinach, New Zealand; spinach, vine.

Crop Subgroup 4B. Leaf petioles 

subgroup.

Celery. Cardoon; celery; celery, Chinese; celtuce; fennel, Florence; rhubarb; Swiss chard.

(6) Crop Group 5. Brassica (Cole) Leafy Vegetables Group.

(i) Representative commodities. Broccoli or cauliflower; cabbage; and mustard greens.

(ii) Table. The following table 1 lists all the commodities included in Crop Group 5 and identifies the related crop 

subgroups.

TABLE 1—CROP GROUP 5: BRASSICA (COLE) LEAFY VEGETABLES

Commodities Related crop subgroups

Broccoli (Brassica oleracea var. botrytis) 5A

Broccoli, Chinese (gai lon) (Brassica alboglabra) 5A

Broccoli raab (rapini) (Brassica campestris) 5B

Brussels sprouts (Brassica oleracea var. gemmifera) 5A

Cabbage (Brassica oleracea) 5A

Cabbage, Chinese (bok choy) (Brassica chinensis) 5B

Cabbage, Chinese (napa) (Brassica pekinensis) 5A

Cabbage, Chinese mustard (gai choy) (Brassica campestris) 5A

Cauliflower (Brassica oleracea var. botrytis) 5A

Cavalo broccolo (Brassica oleracea var. botrytis) 5A

Collards (Brassica oleracea var. acephala) 5B

Kale (Brassica oleracea var. acephala) 5B

Kohlrabi (Brassica oleracea var. gongylodes) 5A

Mizuna (Brassica rapa Japonica Group) 5B

Mustard greens (Brassica juncea) 5B

Mustard spinach (Brassica rapa Perviridis Group) 5B

Rape greens (Brassica napus) 5B

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 5, specifies the representative 

commodity(ies) for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 5 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 5A. Head and stem 

Brassica subgroup

Broccoli or cauliflower; and cabbage Broccoli; broccoli, Chinese; brussels sprouts; cabbage; cabbage, Chinese (napa); cabbage, Chinese mustard; 

cauliflower; cavalo broccolo; kohlrabi

Crop Subgroup 5B. Leafy Brassica greens 

subgroup.

Mustard greens Broccoli raab; cabbage, Chinese (bok choy); collards; kale; mizuna; mustard greens; mustard spinach; rape 

greens

(7) Crop Group 6. Legume Vegetables (Succulent or Dried) Group.

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(i) Representative commodities. Bean (Phaseolus spp.; one succulent cultivar and one dried cultivar); pea (Pisum

spp.; one succulent cultivar and one dried cultivar); and soybean.

(ii) Table. The following table 1 lists all the commodities included in Crop Group 6 and identifies the related crop 

subgroups.

TABLE 1—CROP GROUP 6: LEGUME VEGETABLES (SUCCULENT OR DRIED)

Commodities

Related crop 

subgroups

Bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin) 6C

Bean (Phaseolus spp.) (includes field bean, kidney bean, lima bean, navy bean, pinto bean, runner bean, snap bean, tepary bean, wax 

bean)

6A, 6B, 6C

Bean (Vigna spp.) (includes adzuki bean, asparagus bean, blackeyed pea, catjang, Chinese longbean, cowpea, Crowder pea, moth 

bean, mung bean, rice bean, southern pea, urd bean, yardlong bean)

6A, 6B, 6C

Broad bean (fava bean) (Vicia faba) 6B, 6C

Chickpea (garbanzo bean) (Cicer arietinum) 6C

Guar (Cyamopsis tetragonoloba) 6C

Jackbean (Canavalia ensiformis) 6A

Lablab bean (hyacinth bean) (Lablab purpureus) 6C

Lentil (Lens esculenta) 6C

Pea (Pisum spp.) (includes dwarf pea, edible-pod pea, En glish pea, field pea, garden pea, green pea, snow pea, sugar snap pea) 6A, 6B, 6C

Pigeon pea (Cajanus cajan) 6A, 6B, 6C

Soybean (Glycine max) N/A

Soybean (immature seed) (Glycine max) 6A

Sword bean (Canavalia gladiata) 6A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 6, specifies the representative 

commodities for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 6 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 6A. Edible-podded 

legume vegetables subgroup.

Any one succulent cultivar of ediblepodded bean (Phaseolus spp.) and any 

one succulent cultivar of edible-podded 

pea (Pisum spp.).

Bean (Phaseolus spp.) (includes runner bean, snap bean, wax bean); bean (Vigna spp.) (includes asparagus 

bean, Chinese longbean, moth bean, yardlong bean); jackbean; pea (Pisum spp.) (includes dwarf pea, edible-pod 

pea, snow pea, sugar snap pea); pigeon pea; soybean (immature seed); sword bean.

Crop Subgroup 6B. Succulent shelled 

pea and bean subgroup.

Any succulent shelled cultivar of bean 

(Phaseolus spp.) and garden pea (Pisum

spp.).

Bean (Phaseolus spp.) (includes lima bean (green)); broad bean (succulent); bean (Vigna spp.) (includes 

blackeyed pea, cowpea, southern pea); pea (Pisum spp.) (includes English pea, garden pea, green pea); pigeon 

pea.

Crop Subgroup 6C. Dried shelled pea 

and bean (except soybean) subgroup

Any one dried cultivar of bean (Phaseolus

spp.); and any one dried cultivar of pea 

(Pisum spp.)

Dried cultivars of bean (Lupinus spp.) (includes grain lupin, sweet lupin, white lupin, and white sweet lupin); 

(Phaseolus spp.) (includes field bean, kidney bean, lima bean (dry), navy bean, pinto bean; tepary bean; bean 

(Vigna spp.) (includes adzuki bean, blackeyed pea, catjang, cowpea, Crowder pea, moth bean, mung bean, rice 

bean, southern pea, urd bean); broad bean (dry); chickpea; guar; lablab bean; lentil; pea (Pisum spp.) (includes 

field pea); pigeon pea.

(8) Crop Group 7. Foliage of Legume Vegetables Group.

(i) Representative commodities. Any cultivar of bean (Phaseolus spp.), field pea (Pisum spp.), and soybean.

(ii) Table. The following table 1 lists the commodities included in Crop Group 7.

TABLE 1—CROP GROUP 7: FOLIAGE OF LEGUME VEGETABLES GROUP

Representative commodities Commodities

Any cultivar of bean (Phaseolus spp.) and field pea (Pisum spp.), and 

soybean (Glycine max)

Plant parts of any legume vegetable included in the legume vegetables that will be 

used as animal feed.

(iii) Table. The following table 2 identifies the crop subgroup for Crop Group 7 and specifies the representative 

commodities for the subgroup, and lists all the commodities included in the subgroup.

TABLE 2—CROP GROUP 7 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 7A. Foliage of legume vegetables (except 

soybeans) subgroup

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Any cultivar of bean (Phaseolus spp.), and field pea (Pisum

spp.)

Plant parts of any legume vegetable (except soybeans) included in the legume vegetables 

group that will be used as animal feed.

(9) Crop Group 8. Fruiting Vegetables Group.

(i) Representative commodities. Tomato, bell pepper, and one cultivar of non-bell pepper.

(ii) Commodities. The following is a list of all the commodities included in Crop Group 8: 

CROP GROUP 8: FRUITING VEGETABLES (EXCEPT CUCURBITS)—COMMODITIES

Eggplant (Solanum melongena)

Groundcherry (Physalis spp.)

Pepino (Solanum muricatum)

Pepper (Capsicum spp.) (includes bell pepper, chili pepper, cooking pepper, pimento, sweet pepper)

Tomatillo (Physalis ixocarpa)

Tomato (Lycopersicon esculentum)

(10) Crop Group 8-10. Fruiting Vegetable Group.

(i) Representative commodities. Tomato, standard size, and one cultivar of small tomato; bell pepper and one cultivar 

of small nonbell pepper.

(ii) Commodities. The following is a list of all commodities included in the Crop group 8-10.

TABLE 1—CROP GROUP 8-10: FRUITING VEGETABLE GROUP

Commodities

Related crop 

subgroups

African eggplant, Solanum macrocarpon L 8-10B, 8-10C

Bush tomato, Solanum centrale J.M. Black 8-10A

Cocona, Solanum sessiliflorum Dunal 8-10A

Currant tomato, Lycopersicon pimpinellifolium L 8-10A

Eggplant, Solanum melongena L 8-10B, 8-10C

Garden huckleberry, Solanum scabrum Mill 8-10A

Goji berry, Lycium barbarum L 8-10A

Groundcherry, Physalis alkekengi L., P. grisea (Waterf.) M. Martinez, P. peruviana L., P. pubescens L 8-10A

Martynia, Proboscidea louisianica (Mill.) Thell 8-10B, 8-10C

Naranjilla, Solanum quitoense Lam 8-10A

Okra, Abelmoschus esculentus (L.) Moench 8-10B, 8-10C

Pea eggplant, Solanum torvum Sw. 8-10B, 8-10C

Pepino, Solanum muricatum Aiton 8-10B, 8-10C

Pepper, bell, Capsicum annuum L. var. annuum, Capsicum spp 8-10B

Pepper, nonbell, Capsicum chinese Jacq., C. annuum L. var. annuum, C. frutescens L., C. baccatum L., C. pubescens Ruiz & Pav., 

Capsicum spp

8-10B, 8-10C

Roselle, Hibiscus sabdariffa L 8-10B, 8-10C

Scarlet eggplant, Solanum aethiopicum L 8-10B, 8-10C

Sunberry, Solanum retroflexum Dunal 8-10A

Tomatillo, Physalis philadelphica Lam 8-10A

Tomato, Solanum lycopersicum L., Solanum lycopersicum L. var. lycopersicum 8-10A

Tree tomato, Solanum betaceum Cav 8-10A

Cultivars, varieties and/or hybrids of these

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 8-10, specifies the representative 

commodities for each subgroup and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 8-10. SUBGROUP LISTING

Representative commodities Commodities

Crop subgroup 8-10A. Tomato subgroup

Tomato, standard size, and one cultivar of 

small tomato

Bush tomato; cocona; currant tomato; garden huckleberry; goji berry; groundcherry; naranjilla; sunberry; 

tomatillo; tomato; tree tomato; cultivars, varieties, and/or hybrids of these.

Crop subgroup 8-10B. Pepper/Eggplant 

subgroup

Bell pepper and one cultivar of small nonbell 

pepper

African eggplant; bell pepper; eggplant; Martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet 

eggplant; cultivars, varieties, and/or hybrids of these.

Crop subgroup 8-10C. Nonbell 

pepper/Eggplant subgroup

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One cultivar of small nonbell pepper or one 

cultivar of small eggplant

African eggplant; eggplant; martynia; nonbell pepper; okra; pea eggplant; pepino; roselle; scarlet eggplant; 

cultivars, varieties, and/or hybrids of these.

(11) Crop Group 9. Cucurbit Vegetables Group.

(i) Representative commodities. Cucumber, muskmelon, and summer squash.

(ii) Table. The following table 1 lists all the commodities included in Crop Group 9 and identifies the related 

subgroups.

TABLE 1—CROP GROUP 9: CUCURBIT VEGETABLES

Commodities

Related crop 

subgroups

Chayote (fruit) (Sechium edule) 9B

Chinese waxgourd (Chinese preserving melon) (Benincasa hispida) 9B

Citron melon (Citrullus lanatus var. citroides) 9A

Cucumber (Cucumis sativus) 9B

Gherkin (Cucumis anguria) 9B

Gourd, edible (Lagenaria spp.) (includes hyotan, cucuzza); (Luffa acutangula, L. cylindrica) (includes hechima, Chinese okra) 9B

Momordica spp. (includes balsam apple, balsam pear, bitter melon, Chinese cucumber) 9B

Muskmelon (hybrids and/or cultivars of Cucumis melo) (includes true cantaloupe, cantaloupe, casaba, crenshaw melon, golden pershaw 

melon, honeydew melon, honey balls, mango melon, Persian melon, pineapple melon, Santa Claus melon, and snake melon)

9A

Pumpkin (Cucurbita spp.) 9B

Squash, summer (Cucurbita pepo var. melopepo) (includes crookneck squash, scallop squash, straightneck squash, vegetable marrow, 

zucchini)

9B

Squash, winter (Cucurbita maxima; C. moschata) (includes butternut squash, calabaza, hubbard squash); (C. mixta; C. pepo) (includes 

acorn squash, spaghetti squash)

9B

Watermelon (includes hybrids and/or varieties of Citrullus lanatus) 9A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 9, specifies the representative 

commodities for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 9 SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 9A. Melon subgroup

Cantaloupes Citron melon; muskmelon; watermelon

Crop Subgroup 9B. Squash/cucumber 

subgroup

One cultivar of summer squash and 

cucumber.

Chayote (fruit); Chinese waxgourd; cucumber; gherkin; gourd, edible; Momordica spp.; pumpkin; squash, 

summer; squash, winter.

(12) Crop Group 10. Citrus Fruit Group. 

(i) Representative commodities. Sweet orange; lemon and grapefruit.

(ii) Commodities. The following is a list of all the commodities in Crop Group 10:

CROP GROUP 10: CITRUS FRUITS (CITRUS SPP., FORTUNELLA SPP.) GROUP—COMMODITIES

Calamondin (Citrus mitis × Citrofortunella mitis)

Citrus citron (Citrus medica)

Citrus hybrids (Citrus spp.) (includes chironja, tangelo, tangor)

Grapefruit (Citrus paradisi)

Kumquat (Fortunella spp.)

Lemon (Citrus jambhiri, Citrus limon)

Lime (Citrus aurantiifolia)

Mandarin (tangerine) (Citrus reticulata)

Orange, sour (Citrus aurantium)

Orange, sweet (Citrus sinensis)

Pummelo (Citrus grandis, Citrus maxima)

Satsuma mandarin (Citrus unshiu)

(13) Crop Group 10-10. Citrus Fruit Group.

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(i) Representative commodities. Orange or Tangerine/Mandarin, Lemon or Lime, and Grapefruit.

(ii) Commodities. The following is a list of all the commodities in Crop Group 10-10.

TABLE 1—CROP GROUP 10-10: CITRUS FRUIT GROUP

Commodities Related crop subgroups

Australian desert lime, Eremocitrus glauca (Lindl.) Swingle 10-10B

Australian finger lime, Microcitrus australasica (F. Muell.) Swingle 10-10B

Australian round lime, Microcitrus australis (A. Cunn. Ex Mudie) Swingle 10-10B

Brown River finger lime, Microcitrus papuana Winters 10-10B

Calamondin, Citrofortunella microcarpa (Bunge) Wijnands 10-10A

Citron, Citrus medica L 10-10A

Citrus hybrids, Citrus spp. Eremocitrus spp., Fortunella spp., Microcitrus spp., and Poncirus spp 10-10A

Grapefruit, Citrus paradisi Macfad 10-10C

Japanese summer grapefruit, Citrus natsudaidai Hayata 10-10C

Kumquat, Fortunella spp 10-10B

Lemon, Citrus limon (L.) Burm. f 10-10B

Lime, Citrus aurantiifolia (Christm.) Swingle 10-10B

Mediterranean mandarin, Citrus deliciosa Ten 10-10A

Mount White lime, Microcitrus garrowayae (F.M. Bailey) Swingle 10-10B

New Guinea wild lime, Microcitrus warburgiana (F.M. Bailey) Tanaka 10-10B

Orange, sour, Citrus aurantium L 10-10A

Orange, sweet, Citrus sinensis (L.) Osbeck 10-10A

Pummelo, Citrus maxima (Burm.) Merr 10-10C

Russell River lime, Microcitrus inodora (F.M. Bailey) Swingle 10-10B

Satsuma mandarin, Citrus unshiu Marcow 10-10A

Sweet lime, Citrus limetta Risso 10-10B

Tachibana orange, Citrus tachibana (Makino) Tanaka 10-10A

Tahiti lime, Citrus latifolia (Yu. Tanaka) Tanaka 10-10B

Tangelo, Citrus xtangelo J.W. Ingram & H.E. Moore 10-10A, 10-10C

Tangerine (Mandarin), Citrus reticulata Blanco 10-10A

Tangor, Citrus nobilis Lour 10-10A

Trifoliate orange, Poncirus trifoliata (L.) Raf 10-10A

Uniq fruit, Citrus aurantium Tangelo group 10-10C

Cultivars, varieties and/or hybrids of these

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 10-10, specifies the representative 

commodities for each subgroup and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 10-10: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 10-10A. Orange 

subgroup

Orange or tangerine/mandarin Calamondin; citron; citrus hybrids; mediterranean mandarin; orange, sour; orange, sweet; satsuma mandarin; tachibana 

orange; tangerine (mandarin); tangelo; tangor; trifoliate orange; cultivars, varieties, and/or hybrids of these.

Crop Subgroup 10-10B. 

Lemon/Lime subgroup

Lemon or lime Australian desert lime; Australian finger lime; Australian round lime; brown river finger lime; kumquat; lemon; lime; mount 

white lime; New Guinea wild lime; Russell River lime; sweet lime; Tahiti lime; cultivars , varieties, and/or hybrids of these.

Crop Subgroup 10-10C. 

Grapefruit subgroup

Grapefruit Grapefruit; Japanese summer grapefruit; pummelo; tangelo; uniq fruit; cultivars, varieties, and/or hybrids of these.

(14) Crop Group 11: Pome Fruits Group.

(i) Representative commodities. Apple and pear.

(ii) Commodities. The following is a list of all the commodities included in Crop Group 11:

CROP GROUP 11: POME FRUITS GROUP—COMMODITIES

Apple (Malus domestica)

Crabapple (Malus spp.)

Loquat (Eriobotrya japonica)

Mayhaw (Crataegus aestivalis, C. opaca, and C. rufula)

Pear (Pyrus communis)

Pear, oriental (Pyrus pyrifolia)

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Quince (Cydonia oblonga)

(15) Crop group 11-10. Pome Fruit Group.

(i) Representative commodities. Apple and Pear

(ii) Commodities. The following is a list of all the commodities in Crop Group 11-10.

CROP GROUP 11-10: POME FRUIT GROUP—COMMODITIES

Apple, Malus domestica Borkh.

Azarole, Crataegus azarolus L.

Crabapple, Malus sylvestris (L.) Mill., M. prunifolia (Willd.) Borkh.

Loquat, Eriobotrya japonica (Thunb.) Lindl.

Mayhaw, Crataegus aestivalis (Walter) Torr. & A. Gray, C. opaca

Hook. & Arn., and C. rufula Sarg.

Medlar, Mespilus germanica L.

Pear, Pyrus communis L.

Pear, Asian, Pyrus pyrifolia (Burm. f.) Nakai var. culta (Makino) Nakai

Pseudocydonia sinensis (Thouin) C.K. Schneid.

Quince, Cydonia oblonga Mill.

Quince, Chinese, Chaenomeles speciosa (Sweet) Nakai,

Quince, Japanese, Chaenomeles japonica (Thunb.) Lindl. ex Spach

Tejocote, Crataegus mexicana DC.

Cultivars, varieties and/or hybrids of these.

(16) Crop Group 12. Stone Fruits Group.

(i) Representative commodities. Sweet cherry or tart cherry; peach; and plum or fresh prune (Prunus domestica, 

Prunus spp.)

(ii) Commodities. The following is a list of all the commodities included in Crop Group 12:

CROP GROUP 12: STONE FRUITS GROUP—COMMODITIES

Apricot (Prunus armeniaca)

Cherry, sweet (Prunus avium),

Cherry, tart (Prunus cerasus)

Nectarine (Prunus persica)

Peach (Prunus persica)

Plum (Prunus domestica, Prunus spp.)

Plum, Chickasaw (Prunus angustifolia)

Plum, Damson (Prunus domestica spp. insititia)

Plum, Japanese (Prunus salicina)

Plumcot (Prunus. armeniaca × P. domestica)

Prune (fresh) (Prunus domestica, Prunus spp.)

(17) Crop Group 12-12: Stone Fruit Group.

(i) Representative commodities. Sweet cherry or Tart cherry; Peach; and Plum or Prune plum.

(ii) Commodities. The following Table 1 is a list of all commodities included in Crop Group 12-12.

TABLE 1—CROP GROUP 12-12: STONE FRUIT GROUP

Commodities Related crop subgroup

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Apricot (Prunus armeniaca L.) 12-12C

Apricot, Japanese (Prunus mume Siebold & Zucc.) 12-12C

Capulin (Prunus serotina Ehrh. var. salicifolia (Kunth) Koehne) 12-12A

Cherry, black (Prunus serotina Ehrh.) 12-12A

Cherry, Nanking (Prunus tomentosa Thunb.) 12-12A

Cherry, sweet (Prunus avium (L.) L.) 12-12A

Cherry, tart (Prunus cerasus L.) 12-12A

Jujube, Chinese (Ziziphus jujuba Mill.) 12-12C

Nectarine (Prunuspersica (L.) Batsch var. nucipersica (Suckow) C.K. Schneid) 12-12B

Peach (Prunus persica (L.) Batsch var. persica) 12-12B

Plum (Prunus domestica L. subsp. domestica) 12-12C

Plum, American (Prunus americana Marshall) 12-12C

Plum, beach (Prunus maritima Marshall) 12-12C

Plum, Canada (Prunus nigra Aiton) 12-12C

Plum, cherry (Prunus cerasifera Ehrh.) 12-12C

Plum, Chickasaw (Prunus angustifolia Marshall) 12-12C

Plum, Damson (Prunus domestica L. subsp. insititia (L.) C.K. Schneid.) 12-12C

Plum, Japanese (Prunus salicina Lindl.; P. salicina Lindl. var. salicina) 12-12C

Plum, Klamath (Prunus subcordata Benth.) 12-12C

Plum, prune (Prunus domestica L. subsp. domestica) 12-12C

Plumcot (Prunus hybr.) 12-12C

Sloe (Prunus spinosa L.) 12-12C

Cultivars, varieties, and/or hybrids of these

(iii) Crop subgroups. The following Table 2 identifies the crop subgroups for Crop Group 12-12, specifies the 

representative commodities for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 12-12: SUBGROUP LISTING

Representative 

commodities Commodities

Crop subgroup 12-12A. Cherry subgroup

Cherry, sweet or 

Cherry, tart

Capulin; Cherry, black; Cherry, Nanking; Cherry, sweet; Cherry, tart; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12-12B. Peach subgroup

Peach Peach; Nectarine; cultivars, varieties, and/or hybrids of these.

Crop subgroup 12-12C. Plum subgroup

Plum or Prune plum Apricot; Apricot, Japanese; Jujube, Chinese; Plum; Plum, American; Plum, beach; Plum, Canada; Plum, cherry; Plum, Chickasaw; 

Plum, Damson; Plum, Japanese; Plum, Klamath; Plumcot; Plum, prune; Sloe; cultivars, varieties, and/or hybrids of these.

(18) Crop Group 13. Berries Group.

(i) Representative commodities. Any one blackberry or any one raspberry; and blueberry.

(ii) Table. The following table 1 lists all the commodities included in Crop Group 13 and identifies the related 

subgroups.

TABLE 1—CROP GROUP 13: BERRIES GROUP

Commodities

Related crop 

subgroups

Blackberry (Rubus eubatus) (including bingleberry, black satin berry, boysenberry, Cherokee blackberry, Chesterberry, Cheyenne blackberry, 

coryberry, darrowberry, dewberry, Dirksen thornless berry, Himalayaberry, hullberry, Lavacaberry, lowberry, Lucretiaberry, mammoth 

blackberry, marionberry, nectarberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, ravenberry, rossberry, Shawnee 

blackberry, youngberry, and varieties and/or hybrids of these)

13A

Blueberry (Vaccinium spp.) 13B

Currant (Ribes spp.) 13B

Elderberry (Sambucus spp.) 13B

Gooseberry (Ribes spp.) 13B

Huckleberry (Gaylussacia spp.) 13B

Loganberry (Rubus loganobaccus) 13A

Raspberry, black and red (Rubus occidentalis, Rubus strigosus, Rubus idaeus) 13A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 13, specifies the representative 

commodities for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 13 SUBGROUPS LISTING

Representative commodities Commodities

Crop Subgroup 13A. Caneberry (blackberry and raspberry) subgroup.

Any one blackberry or any one raspberry. Blackberry; loganberry; red and black raspberry; cultivars and/or hybrids of these.

Crop Subgroup 13B. Bushberry subgroup.

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Blueberry, highbush. Blueberry, highbush and lowbush; currant; elderberry; gooseberry; huckleberry.

(19) Crop Group 13-07. Berry and Small Fruit Crop Group

(i) Representative commodities. Any one blackberry or any one raspberry; highbush blueberry; elderberry or mulberry; 

grape; fuzzy kiwifruit, and strawberry.

(ii) Table. The following Table 1 lists all the commodities listed in Crop Group 13-07 and identifies the related crop 

subgroups.

TABLE 1—CROP GROUP 13-07: BERRY AND SMALL FRUIT CROP GROUP

Commodities

Related crop 

subgroups

Amur river grape (Vitis amurensis Rupr) 13-07D, 13-

07E, 13-07F

Aronia berry (Aronia spp.) 13-07B

Bayberry (Myrica spp.) 13-07C

Bearberry (Arctostaphylos uva-ursi) 13-07G, 13-

07H

Bilberry (Vaccinium myrtillus L.) 13-07G, 13-

07H

Blackberry (Rubus spp.) (including Andean blackberry, arctic blackberry, bingleberry, black satin berry, boysenberry, brombeere, California 

blackberry, Chesterberry, Cherokee blackberry, Cheyenne blackberry, common blackberry, coryberry, darrowberry, dewberry, Dirksen 

thornless berry, evergreen blackberry, Himalayaberry, hullberry, lavacaberry, loganberry, lowberry, Lucretiaberry, mammoth blackberry, 

marionberry, mora, mures deronce, nectarberry, Northern dewberry, olallieberry, Oregon evergreen berry, phenomenalberry, rangeberry, 

ravenberry, rossberry, Shawnee blackberry, Southern dewberry, tayberry, youngberry, zarzamora, and cultivars, varieties and/or hybrids of 

these.)

13-07A

Blueberry, highbush (Vaccinium spp.) 13-07B

Blueberry, lowbush (Vaccinium angustifolium Aiton) 13-07B

Buffalo currant (Ribes aureum Pursh) 13-07B

Buffaloberry (Shepherdia argentea (Pursh) Nutt.) 13-07C

Che (Cudrania tricuspidata Bur. Ex Lavallee) 13-07C

Chilean guava (Myrtus ugni Mol.) 13-07B

Chokecherry (Prunus virginiana L.) 13-07C

Cloudberry (Rubus chamaemorus L.) 13-07G, 13-

07H

Cranberry (Vaccinium macrocarpon Aiton) 13-07G, 13-

07H

Currant, black (Ribes nigrum L.) 13-07B

Currant, red (Ribes rubrum L.) 13-07B

Elderberry (Sambucus spp.) 13-07B, 13-

07C

European barberry (Berberis vulgaris L.) 13-07B

Gooseberry (Ribes spp.) 13-07B, 13-

07D, 13-07E, 

13-07F

Grape (Vitis spp.) 13-07D, 13-

07F

Highbush cranberry (Viburnum opulus L. var. Americanum Aiton) 13-07B

Honeysuckle, edible (Lonicera caerula L. var. emphyllocalyx Nakai, Lonicera caerula L var . edulis Turcz. ex herder) 13-07B

Huckleberry (Gaylussacia spp.) 13-07B

Jostaberry (Ribes x nidigrolaria Rud. Bauer and A. Bauer) 13-07B

Juneberry (Saskatoon berry) (Amelanchier spp.) 13-07B, 13-

07C

Kiwifruit, fuzzy (Actinidia deliciosa A. Chev.) (C.F. Liang and A.R. Fergusons, Actinida chinensis Planch.) 13-07D, 13-

07E

Kiwifruit, hardy (Actinidia arguta (Siebold and Zucc.) Planch. ex Miq) 13-07D, 13-

07E, 13-07F

Lingonberry (Vaccinium vitis-idaea L.) 13-07B, 13-

07G 13-07H

Maypop (Passiflora incarnata L.) 13-07E, 13-

07F

Mountain pepper berries (Tasmannia lanceolata)(Poir.) A.C.Sm. 13-07C

Mulberry (Morus spp.) 13-07C

Muntries (Kunzea pomifera F. Muell.) 13-07G, 13-

07H

Native currant (Acrotriche depressa R. BR.) 13-07B

Partridgeberry (Mitchella repens L.) 13-07G, 13-

07H

Phalsa (Grewia subinaequalis DC.) 13-07C

Pincherry (Prunus pensylvanica L.f.) 13-07C

Raspberry, black and red (Rubus spp.) 13-07A

Riberry (Syzygium luehmannii) 13-07C

Salal (Gaultheria shallon Pursh.) 13-07B, 13-

07C

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Schisandra berry (Schisandra chinensis (Turcz.) Baill.) 13-07D, 13-

07E, 13-07F

Sea buckthorn (Hippophae rhamnoides L.) 13-07B

Serviceberry (Sorbus spp.) 13-07C

Strawberry (Fragaria x ananassa Duchesne) 13-07G

Wild raspberry (Rubus muelleri Lefevre ex P.J. Mull) 13-07A

Cultivars, varieties, and/or hybrids of these.

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 13-07, specifies the representative 

commodities for each subgroup and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 13-07: SUBGROUP LISTING

Representative commodities Commodities

Crop Subgroup 13-07A. Caneberry 

subgroup

Any one blackberry or any one 

raspberry.

Blackberry; loganberry; raspberry, red and black; wild raspberry; cultivars, varieties, and/or hybrids of these.

Crop Subgroup 13-07B. Bushberry 

subgroup.

Blueberry, highbush. Aronia berry; blueberry, highbush; blueberry, lowbush; buffalo currant; Chilean guava; currant, black; currant, red; 

elderberry; European, barberry; gooseberry; cranberry, highbush; honeysuckle, edible; huckleberry; jostaberry; 

Juneberry; lingonberry; native currant; salal; sea buckthorn; cultivars, varieties, and/or hybrids of these.

Crop Subgroup 13-07C. Large 

shrub/tree berry subgroup.

Elderberry or mulberry. Bayberry; buffaloberry; che; chokecherry; elderberry; Juneberry; mountain pepper berries; mulberry; phalsa; 

pincherry; riberry; salal; serviceberry; cultivars, varieties, and/or hybrids of these.

Crop Subgroup 13-07D. Small fruit 

vine climbing subgroup.

Grape and fuzzy kiwifruit. Amur river grape; gooseberry; grape; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, 

and /or hybrids of these.

Crop Subgroup 13-07E. Small fruit 

vine climbing subgroup, except grape.

Fuzzy kiwifruit. Amur river grape; gooseberry; kiwifruit, fuzzy; kiwifruit, hardy; Maypop; schisandra berry; cultivars, varieties, and/or 

hybrids of these.

Crop Subgroup 13-07F. Small fruit 

vine climbing subgroup except fuzzy 

kiwifruit.

Grape. Amur river grape; gooseberry; grape; kiwifruit, hardy; Maypop; schisandra berry; cultivars varieties, and/or hybrids of 

these.

Crop Subgroup 13-07G. Low growing 

berry subgroup.

Strawberry. Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; strawberry; 

cultivars, varieties, and/or hybrids of these.

Crop Subgroup 13-07H. Low growing 

berry subgroup, except strawberry.

Cranberry Bearberry; bilberry; blueberry, lowbush; cloudberry; cranberry; lingonberry; muntries; partridgeberry; cultivars, 

varieties, and/or cultivars of these.

(20) Crop Group 14. Tree Nuts Group.

(i) Representative commodities. Almond and pecan.

(ii) Commodities. The following is a list of all the commodities included in Crop Group 14: 

CROP GROUP 14: TREE NUTS—COMMODITIES

Almond (Prunus dulcis)

Beech nut (Fagus spp.)

Brazil nut (Bertholletia excelsa)

Butternut (Juglans cinerea)

Cashew (Anacardium occidentale)

Chestnut (Castanea spp.)

Chinquapin (Castanea pumila)

Filbert (hazelnut) (Corylus spp.)

Hickory nut (Carya spp.)

Macadamia nut (bush nut) (Macadamia spp.)

Pecan (Carya illinoensis)

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Walnut, black and English (Persian) (Juglans spp.)

(21) Crop Group 14-12. Tree Nut Group.

(i) Representative commodities. Almond and Pecan.

(ii) Commodities. The following is a list of all commodities included in Crop Group 14-12.

CROP GROUP 14-12: TREE NUT GROUP

African nut-tree (Ricinodendron heudelotii (Baill.) Heckel)

Almond (Prunus dulcis (Mill.) D.A. Webb)

Beechnut (Fagus grandifolia Ehrh.; F. sylvatica L.)

Brazil nut (Bertholletia excelsa Humb. & Bonpl.)

Brazilian pine (Araucaria angustifolia (Bertol.) Kuntze)

Bunya (Araucaria bidwillii Hook.)

Bur oak (Quercus macrocarpa Michx.)

Butternut (Juglans cinerea L.)

Cajou nut (Anacardium giganteum Hance ex Engl.)

Candlenut (Aleurites moluccanus (L.) Willd.)

Cashew (Anacardium occidentale L.)

Chestnut (Castanea crenata Siebold & Zucc.; C. dentata (Marshall) Borkh.; C. mollissima Blume; C. sativa Mill.)

Chinquapin (Castaneapumila (L.) Mill.)

Coconut (Cocos nucifera L.)

Coquito nut (Jubaea chilensis (Molina) Baill.)

Dika nut (Irvingia gabonensis (Aubry-Lecomte ex O'Rorke) Baill.)

Ginkgo (Ginkgo biloba L.)

Guiana chestnut (Pachira aquatica Aubl.)

Hazelnut (Filbert) (Corylus americana Marshall; C. avellana L.; C. californica (A. DC.) Rose; C. chinensis Franch.)

Heartnut (Juglans ailantifolia Carrière var. cordiformis (Makino) Rehder)

Hickory nut (Carya cathayensis Sarg.; C. glabra (Mill.) Sweet; C. laciniosa (F. Michx.) W. P. C. Barton; C. myristiciformis (F. Michx.) 

Elliott; C. ovata (Mill.) K. Koch; C. tomentosa (Lam.) Nutt.)

Japanese horse-chestnut (Aesculus turbinate Blume)

Macadamia nut (Macadamia integrifolia Maiden & Betche; M. tetraphylla L.A.S. Johnson)

Mongongo nut (Schinziophyton rautanenii (Schinz) Radcl.-Sm.)

Monkey-pot (Lecythis pisonis Cambess.)

Monkey puzzle nut (Araucaria araucana (Molina) K. Koch)

Okari nut (Terminalia kaernbachii Warb.)

Pachira nut (Pachira insignis (Sw.) Savigny)

Peach palm nut (Bactris gasipaes Kunth var. gasipaes)

Pecan (Carya illinoinensis (Wangenh.) K. Koch)

Pequi (Caryocar brasiliense Cambess.; C. villosum (Aubl.) Pers; C. nuciferum L.)

Pili nut (Canarium ovatum Engl.; C. vulgare Leenh.)

Pine nut (Pinus edulis Engelm.; P. koraiensis Siebold & Zucc.; P. sibirica Du Tour; P. pumila (Pall.) Regel; P. gerardiana Wall. ex D. 

Don; P. monophylla Torr. & Frém.; P. quadrifolia Parl. ex Sudw.; P. pinea L.)

Pistachio (Pistacia vera L.)

Sapucaia nut (Lecythis zabucaja Aubl.)

Tropical almond (Terminalia catappa L.)

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Walnut, black (Juglans nigra L.; J. hindsii Jeps. ex R. E. Sm.; J. microcarpa Berland.)

Walnut, English (Juglans regia L.)

Yellowhorn (Xanthoceras sorbifolium Bunge)

Cultivars, varieties, and/or hybrids of these

(22) Crop Group 15. Cereal Grains Group.

(i) Representative commodities. Corn (fresh sweet corn and dried field corn), rice, sorghum, and wheat.

(ii) Commodities. The following is a list of all the commodities included in Crop Group 15:

CROP GROUP 15: CEREAL GRAINS—COMMODITIES

Barley (Hordeum spp.)

Buckwheat (Fagopyrum esculentum)

Corn (Zea mays)

Millet, pearl (Pennisetum glaucum)

Millet, proso (Panicum milliaceum)

Oats (Avena spp.)

Popcorn (Zea mays var. everta)

Rice (Oryza sativa)

Rye (Secale cereale)

Sorghum (milo) (Sorghum spp.)

Teosinte (Euchlaena mexicana)

Triticale (Triticum-Secale hybrids)

Wheat (Triticum spp.)

Wild rice (Zizania aquatica)

(23) Crop Group 16. Forage, Fodder and Straw of Cereal Grains Group.

(i) Representative commodities. Corn, wheat, and any other cereal grain crop.

(ii) Commodities. The commodities included in Crop Group 16 are: Forage, fodder, and straw of all commodities 

included in the group cereal grains group.

(24) Crop Group 17. Grass Forage, Fodder, and Hay Group.

(i) Representative commodities. Bermuda grass; bluegrass; and bromegrass or fescue.

(ii) Commodities. The commodities included in Crop Group 17 are: Any grass, Gramineae family (either green or 

cured) except sugarcane and those included in the cereal grains group, that will be fed to or grazed by livestock, all 

pasture and range grasses and grasses grown for hay or silage.

(25) Crop Group 18. Nongrass Animal Feeds (Forage, Fodder, Straw, and Hay) Group.

(i) Representative commodities. Alfalfa and clover (Trifolium spp.)

(ii) Commodities. The following is a list of all the commodities included in Crop Group 18:

CROP GROUP 18: NONGRASS ANIMAL FEEDS (FORAGE, FODDER, STRAW, AND HAY) GROUP—COMMODITIES

Alfalfa (Medicago sativa subsp. sativa)

Bean, velvet (Mucuna pruriens var. utilis)

Clover (Trifolium spp., Melilotus spp.)

Kudzu (Pueraria lobata)

Lespedeza (Lespedeza spp.)

Lupin (Lupinus spp.)

Sainfoin (Onobrychis viciifolia);

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Trefoil (Lotus spp.)

Vetch (Vicia spp.)

Vetch, crown (Coronilla varia)

Vetch, milk (Astragalus spp).

(26) Crop Group 19. Herbs and Spices Group.

(i) Representative commodities. Basil (fresh and dried); black pepper; chive; and celery seed or dill seed.

(ii) Table. The following table 1 lists all the commodities included in Crop Group 19 and identifies the related 

subgroups.

TABLE 1—CROP GROUP 19: HERBS AND SPICES GROUP

Commodities Related crop subgroups

Allspice (Pimenta dioica) 19B

Angelica (Angelica archangelica) 19A

Anise (anise seed) (Pimpinella anisum) 19B

Anise, star (Illicium verum) 19B

Annatto (seed) 19B

Balm (lemon balm) (Melissa officinalis) 19A

Basil (Ocimum basilicum) 19A

Borage (Borago officinalis) 19A

Burnet (Sanguisorba minor) 19A

Camomile (Anthemis nobilis) 19A

Caper buds (Capparis spinosa) 19B

Caraway (Carum carvi) 19B

Caraway, black (Nigella sativa) 19B

Cardamom (Elettaria cardamomum) 19B

Cassia bark (Cinnamomum aromaticum) 19B

Cassia buds (Cinnamomum aromaticum) 19B

Catnip (Nepeta cataria) 19A

Celery seed (Apicum graveolens) 19B

Chervil (dried) (Anthriscus cerefolium) 19A

Chive (Allium schoenoprasum) 19A

Chive, Chinese (Allium tuberosum) 19A

Cinnamon (Cinnamomum verum) 19B

Clary (Salvia sclarea) 19A

Clove buds (Eugenia caryophyllata) 19B

Coriander (cilantro or Chinese parsley) (leaf) (Coriandrum sativum) 19A

Coriander (cilantro) (seed) (Coriandrum sativum) 19B

Costmary (Chrysanthemum balsamita) 19A

Culantro (leaf) (Eryngium foetidum) 19A

Culantro (seed) (Eryngium foetidum) 19B

Cumin (Cuminum cyminum) 19B

Curry (leaf) (Murraya koenigii) 19A

Dill (dillweed) (Anethum graveolens) 19A

Dill (seed) (Anethum graveolens) 19B

Fennel (common) (Foeniculum vulgare) 19B

Fennel, Florence (seed) (Foeniculum vulgare Azoricum Group) 19B

Fenugreek (Trigonella foenumgraecum) 19B

Grains of paradise (Aframomum melegueta) 19B

Horehound (Marrubium vulgare) 19A

Hyssop (Hyssopus officinalis) 19A

Juniper berry (Juniperus communis) 19B

Lavender (Lavandula officinalis) 19A

Lemongrass (Cymbopogon citratus) 19A

Lovage (leaf) (Levisticum officinale) 19A

Lovage (seed) (Levisticum officinale) 19B

Mace (Myristica fragrans) 19B

Marigold (Calendula officinalis) 19A

Marjoram (Origanum spp.) (includes sweet or annual marjoram, wild marjoram or oregano, and pot marjoram) 19A

Mustard (seed) (Brassica juncea, B. hirta, B. nigra) 19B

Nasturtium (Tropaeolum majus) 19A

Nutmeg (Myristica fragrans) 19B

Parsley (dried) (Petroselinum crispum) 19A

Pennyroyal (Mentha pulegium) 19A

Pepper, black (Piper nigrum) 19B

Pepper, white 19B

Poppy (seed) (Papaver somniferum) 19B

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Rosemary (Rosemarinus officinalis) 19A

Rue (Ruta graveolens) 19A

Saffron (Crocus sativus) 19B

Sage (Salvia officinalis) 19A

Savory, summer and winter (Satureja spp.) 19A

Sweet bay (bay leaf) (Laurus nobilis) 19A

Tansy (Tanacetum vulgare) 19A

Tarragon (Artemisia dracunculus) 19A

Thyme (Thymus spp.) 19A

Vanilla (Vanilla planifolia) 19B

Wintergreen (Gaultheria procumbens) 19A

Woodruff (Galium odorata) 19A

Wormwood (Artemisia absinthium) 19A

(iii) Table. The following table 2 identifies the crop subgroups for Crop Group 19, specifies the representative 

commodities for each subgroup, and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 19 SUBGROUPS

Representative 

commodities Commodities

Crop Subgroup 19A.

Herb subgroup.

Basil (fresh and dried) 

and chive.

Angelica; balm; basil; borage; burnet; camomile; catnip; chervil (dried); chive; chive, Chinese, clary; coriander (leaf); costmary; 

culantro (leaf); curry (leaf); dillweed; horehound; hyssop; lavender; lemongrass; lovage (leaf); marigold; marjoram (Origanum spp.); 

nasturtium; parsley (dried); pennyroyal; rosemary; rue; sage; savory, summer and winter; sweet bay; tansy; tarragon; thyme; 

wintergreen; woodruff; and wormwood.

Crop Subgroup 19B.

Spice subgroup.

Black pepper; and 

celery seed or dill seed.

Allspice; anise (seed); anise, star; annatto (seed); caper (buds); caraway; caraway, black; cardamom; cassia (buds); celery (seed); 

cinnamon; clove (buds); coriander (seed); culantro (seed); cumin; dill (seed); fennel, common; fennel, Florence (seed); fenugreek; 

grains of paradise; juniper (berry); lovage (seed); mace; mustard (seed); nutmeg; pepper, black; pepper, white; poppy (seed); saffron; 

and vanilla.

(27) Crop Group 20. Oilseed Group.

(i) Representative commodities. Rapeseed (canola varieties only); sunflower, seed and cottonseed.

(ii) Table. The following Table 1 lists all the commodities listed in Crop Group 20 and identifies the related crop 

subgroups and includes cultivars and/or varieties of these commodities.

TABLE 1—CROP GROUP 20: OILSEED GROUP

Commodities Related crop subgroups

Borage, Borago officinalis L 20A

Calendula, Calendula officinalis L 20B

Castor oil plant, Ricinus communis L 20B

Chinese tallowtree, Triadica sebifera (L.) Small 20B

Cottonseed, Gossypium hirsutum L. Gossypium spp 20C

Crambe, Crambe hispanica L.; C. abyssinica Hochst. ex R.E. Fr 20A

Cuphea, Cuphea hyssopifolia Kunth 20A

Echium, Echium plantagineum L 20A

Euphorbia, Euphorbia esula L 20B

Evening primrose, Oenothera biennis L 20B

Flax seed, Linum usitatissimum L 20A

Gold of pleasure, Camelina sativa (L.) Crantz 20A

Hare's ear mustard, Conringia orientalis (L.) Dumort 20A

Jojoba, Simmondsia chinensis (Link) C.K. Schneid 20B

Lesquerella, Lesquerella recurvata (Engelm. ex A. Gray) S. Watson 20A

Lunaria, Lunaria annua L 20A

Meadowfoam, Limnanthes alba Hartw. ex Benth 20A

Milkweed, Asclepias spp 20A

Mustard seed, Brassica hirta Moench, Sinapis alba L. subsp. Alba.. 20A

Niger seed, Guizotia abyssinica (L.f.) Cass 20B

Oil radish, Raphanus sativus L. var. oleiformis Pers 20A

Poppy seed, Papaver somniferum L. subsp. Somniferum 20A

Rapeseed, Brassica spp.; B. napus L 20A

Rose hip, Rosa rubiginosa L 20B

Safflower, Carthamus tinctorious L 20B

Sesame, Sesamum indicum L., S. radiatum Schumach. & honn 20A

Stokes aster, Stokesia laevis (Hill) Greene 20B

Sunflower, Helianthus annuus L 20B

Sweet rocket, Hesperis matronalis L 20A

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Tallowwood, Ximenia americana L 20B

Tea oil plant, Camellia oleifera C. Abel 20B

Vernonia, Vernonia galamensis (Cass.) Less 20B

Cultivars, varieties, and/or hybrids of these

(iii) Table. The following Table 2 identifies the crop subgroups for Crop Group 20, specifies the representative 

commodities for each subgroup and lists all the commodities included in each subgroup.

TABLE 2—CROP GROUP 20: SUBGROUP LISTING

Representative 

commodities Commodities

Crop subgroup 20A. 

Rapeseed subgroup

Rapeseed, canola varieties 

only

Borage; crambe; cuphea; echium; flax seed; gold of pleasure; hare's ear mustard; lesquerella; lunaria; meadowfoam; milkweed; 

mustard seed; oil radish; poppy seed; rapeseed; sesame; sweet rocket cultivars, varieties, and/or hybrids of these.

Crop subgroup 20B. 

Sunflower subgroup

Sunflower, seed Calendula; castor oil plant; chinese tallowtree; euphorbia; evening primrose; jojoba; niger seed; rose hip; safflower; stokes 

aster; sunflower; tallowwood; tea oil plant; vernonia; cultivars, varieties, and/or hybrids of these.

Crop subgroup 20C. 

Cottonseed subgroup

Cottonseed Cottonseed; cultivars, varieties, and/or hybrids of these.

(28) Crop Group 21. Edible fungi Group.

(i) Representative commodities. White button mushroom and any one oyster mushroom or any Shiitake mushroom.

(ii) Table. The following is a list of all the commodities in Crop Group 21. There are no related subgroups.

CROP GROUP 21—EDIBLE FUNGI GROUP—COMMODITIES

Blewitt (Lepista nuda)

Bunashimeji (Hypsizygus marrmoreus)

Chinese mushroom (Volvariella volvacea) (Bull.) Singer

Enoki (Flammulina velutipes) (Curt.) Singer

Hime-Matsutake (Agaricus blazei) Murill

Hirmeola (Auricularia auricular)

Maitake (Grifola frondosa)

Morel (Morchella spp.)

Nameko (Pholiota nameko)

Net Bearing (Dictyophora)

Oyster mushroom (Pleurotus spp.)

Pom Pom (Hericium erinaceus)

Reishi mushroom (Ganoderma lucidum (Leyss. Fr.) Karst.)

Rodman's agaricus (Agaricus bitorquis) (Quel.) Saccardo

Shiitake mushroom (Lentinula edodes (Berk.) Pegl.)

Shimeji (Tricholoma conglobatum)

Stropharia (Stropharia spp.)

Truffle (Tuber spp.)

White button mushroom (Agaricus bisporous (Lange) Imbach)

White Jelly Fungi (Tremella fuciformis)

[60 FR 26635, May 17, 1995, as amended at 72 FR 69156, 69157, Dec. 7, 2007; 73 FR 52, Jan. 2, 2008; 75 FR 76289, Dec. 8, 

2010; 77 FR 50620, Aug. 22, 2012]

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Subpart C—Specific Tolerances

EDITORIAL NOTE: Nomenclature changes to subpart C of part 180 appear at 67 FR 41803, June 19, 2002; 67 FR 42393, June 

21, 2002; 68 FR 39430, July 1, 2003; 71 FR 74804, Dec. 13, 2006; 72 FR 53137, Sept. 18, 2007; 72 FR 61536, Oct. 31, 2007; 73 

FR 60155, Oct. 10, 2008; 75 FR 56014, Sept. 15, 2010; and 76 FR 34885, June 15, 2011. 

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§180.101 Specific tolerances; general provisions.

(a) The tolerances established for pesticide chemicals in this subpart C apply to residues resulting from their 

application prior to harvest or slaughter, unless otherwise stated. Tolerances are expressed in terms of parts by weight of 

the pesticide chemical per one million parts by weight of the raw agricultural commodity.

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(b) The poisonous and deleterious substances for which tolerances are established by the regulations in this subpart 

C are named by their common names wherever practicable, otherwise by their chemical names.

(c) The analytical methods to be used for determining whether pesticide residues, including negligible residues, in or 

on raw agricultural commodities are in compliance with the tolerances established in this part 180 are identified among the 

methods contained or referenced in the Food and Drug Administration's “Pesticide Analytical Manual” which is available 

from the Food and Drug Administration, Department of Health, Education, and Welfare, 200 C Street SW., Washington, 

DC 20204.

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§180.103 Captan; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the fungicide, captan (N-trichloromethylthio-4-

cyclohexene-1,2-dicarboximide) in or on the following commodities:

Commodity Parts per million

Almond 0.25

Almond, hulls 75.0

Animal feed, nongrass, group 18 0.05

Apple 25.0

Apricot 10.0

Blueberry 20.0

Caneberry, subgroup 13A 25.0

Cherry, sweet 50.0

Cherry, tart 50.0

Cotton, undelinted seed 0.05

Dill, seed 0.05

Flax, seed 0.05

Grape 25.0

Grain, cereal, forage, fodder and straw, group 16 0.05

Grain, cereal, group 15 0.05

Grass, forage 0.05

Grass, hay 0.05

Nectarine 25.0

Okra 0.05

Peach 15.0

Peanut 0.05

Peanut, hay 0.05

Pear 25.0

Plum, prune, fresh 10.0

Rapeseed, forage 0.05

Rapeseed, seed 0.05

Safflower, seed 0.05

Sesame, seed 0.05

Strawberry 20.0

Sunflower, seed 0.05

Vegetable, brassica leafy, group 5 0.05

Vegetable, bulb, group 3 0.05

Vegetable, cucurbit, group 9 0.05

Vegetable, foliage of legume, group 7 0.05

Vegetable, fruiting, group 8 0.05

Vegetable, leafy, except brassica, group 4 0.05

Vegetable, leaves of root and tuber, group 2 0.05

Vegetable, legume, group 6 0.05

Vegetable, root and tuber, group 1 0.05

(2) Tolerances are established for the combined residues of the fungicide, captan (N-trichloromethylthio-4-

cyclohexene-1,2-dicarboximide) and its metabolite 1,2,3,6-tetrahydrophthalimide (THPI), measured at THPI, in or on the 

following commodities:

Commodity Parts per million

Cattle, fat 0.15

Cattle, meat 0.20

Cattle, meat byproducts 0.30

Goat, fat 0.15

Goat, meat 0.20

Goat, meat byproducts 0.30

Hog, fat 0.15

Hog, meat 0.20

Hog, meat byproducts 0.30

Horse, fat 0.15

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Horse, meat 0.20

Horse, meat byproducts 0.30

Milk 0.10

Sheep, fat 0.15

Sheep, meat 0.20

Sheep, meat byproducts 0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52016, Sept. 12, 2007]

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§180.106 Diuron; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diuron, 3-(3,4-dichlorophenyl)

-1,1-dimethylurea and its metabolites convertible to 3,4-dichloroaniline in or on food commodities, as follows:

Commodity Parts per million 

Alfalfa, forage 3.0 

Alfalfa, hay 2.0 

Apple 0.1 

Artichoke, globe 1 

Asparagus 7 

Banana 0.1 

Berry group 13 0.1 

Cattle, fat 1 

Cattle, meat 1 

Cattle, meat byproducts 1 

Citrus, oil 3.0 

Corn, field, grain 0.1 

Corn, pop, grain 0.1 

Cotton, undelinted seed 0.2 

Fish - freshwater finfish, farm raised 2.0 

Fruit, citrus, group 10, except lemon 0.05 

Goat, fat 1 

Goat, meat 1 

Goat, meat byproducts 1 

Grain, aspirated fractions 5.0 

Grape 0.05 

Grass, forage, except bermudagrass 2 

Grass, hay, except bermudagrass 2 

Hazelnut 0.1 

Hog, fat 1 

Hog, meat 1 

Hog, meat byproducts 1 

Horse, fat 1 

Horse, meat 1 

Horse, meat byproducts 1 

Lemon 0.5 

Nut, macadamia 0.05 

Olive 1 

Papaya 0.5 

Peach 0.1 

Pear 1 

Pea, field, seed 0.1 

Pea, field, vines 2 

Pea, field, hay 2 

Pecan 0.05 

Peppermint, tops 1.5 

Pineapple 0.1 

Pineapple, process residue 0.4 

Sheep, fat 1 

Sheep, meat 1 

Sheep, meat byproducts 1 

Sorghum, grain, forage 2 

Sorghum, grain, grain 0.5 

Sorghum, grain, stover 2 

Spearmint, tops 1.5 

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Sugarcane, cane 0.2 

Sugarcane, molasses 0.7 

Walnut 0.05 

Wheat, bran 0.7 

Wheat, forage 2 

Wheat, grain 0.5 

Wheat, hay 2 

Wheat, straw 1.5

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in §180.1(l) are 

established for the combined residues of the herbicide diuron (3-(3,4-dichlorophenyl)-1,1-dimethylurea and its metabolites 

convertible to 3,4-dichloroaniline) in or on the raw agricultural commodities:

Commodity Parts per million 

Barley, bran 0.7 

Barley, grain 0.2 

Barley, hay 2 

Barley, straw 1.5 

Cactus 0.05 

Clover, forage 0.1 

Clover, hay 1.0 

Oat, forage 2 

Oat, grain 0.1 

Oat, hay 2 

Oat, straw 1.5 

Trefoil, forage 0.1 

Trefoil, hay 1.5 

Vetch, forage 0.1 

Vetch, hay 1.5 

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2164, Jan. 14, 1998, as amended at 63 FR 57072, Oct. 26, 1998; 64 FR 41305, July 30, 1999; 66 FR 28671, May 24, 2001; 

67 FR 46883, July 17, 2002; 69 FR 71717, Dec. 10, 2004; 72 FR 32540, June 13, 2007; 72 FR 35666, June 29, 2007; 73 FR 54958, 

Sept. 24, 2008; 76 FR 34885, June 15, 2011]

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§180.108 Acephate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, 

including its metabolites and degradates other than methamidophos, in or on the commodities in the following table. 

Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, 

O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

Commodity1 Parts per million

Bean, dry, seed 3.0

Bean, succulent 3.0

Brussels sprouts 3.0

Cattle, fat 0.1

Cattle, meat 0.1

Cattle, meat byproducts 0.1

Cauliflower 2.0

Celery 10

Cotton, hulls 1.0

Cotton, meal 1.0

Cotton, undelinted seed 0.5

Cranberry 0.5

Egg 0.1

Goat, fat 0.1

Goat, meat 0.1

Goat, meat byproducts 0.1

Hog, fat 0.1

Hog, meat 0.1

Hog, meat byproducts 0.1

Horse, fat 0.1

Horse, meat 0.1

Horse, meat byproducts 0.1

Lettuce, head 10

Milk 0.1

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Peanut 0.2

Pepper 4.0

Peppermint, tops 27

Poultry, fat 0.1

Poultry, meat 0.1

Poultry, meat byproducts 0.1

Sheep, fat 0.1

Sheep, meat 0.1

Sheep, meat byproducts 0.1

Spearmint, tops 27

Soybean, seed 1.0

1

Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from 

methamidophos application are regulated under 40 CFR 180.315.

(2) A tolerance of 0.02 ppm is established for residues of acephate, O,S-dimethyl acetyl phosphoramidothioate, 

including its metabolites and degradates other than methamidophos, in or on all food items (other than those already 

covered by a higher tolerance as a result of use on growing crops) in food handling establishments where food and food 

products are held, processed, prepared and served, including food service, manufacturing and processing establishments, 

such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and 

canneries, where application of acephate shall be limited solely to spot and/or crack and crevice treatment (a coarse, lowpressure spray shall be used to avoid atomization or splashing of the spray for spot treatments; equipment capable of 

delivering a pin-stream of insecticide shall be used for crack and crevice treatments). Spray concentration shall be limited 

to a maximum of 1.0 percent active ingredient. Contamination of food or food-contact surfaces shall be avoided. 

Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only acephate, 

O,S-dimethyl acetyl phosphoramidothioate, in or on the commodity.

(3) Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate, including its 

metabolites and degradates, in or on the commodities in the following table as a result of the application of acephate. 

Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only methamidophos, 

O,S-dimethyl phosphoramidothioate, in or on the commodity.

Commodity Parts per million

Bean, dry, seed 1

Bean, succulent 1

Brussels sprouts 0.5

Cauliflower 0.5

Celery 1

Cranberry 0.1

Lettuce, head 1

Pepper 1

Peppermint, tops 1

Spearmint, tops 1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of 

acephate, O,S-dimethyl acetyl phosphoramidothioate, including its metabolites and degradates other than 

methamidophos, in or on the commodity in the following table. Compliance with the tolerance level specified in this 

paragraph is to be determined by measuring only acephate, O,S-dimethyl acetyl phosphoramidothioate, in or on the 

commodity.

Commodity1 Parts per million

Nut, macadamia 0.05

1

Where there is a direct use of methamidophos on the commodity, residues of methamidophos resulting from 

methamidophos application are regulated under 40 CFR 180.315.

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 13542, Mar. 20, 1998, as amended at 67 FR 49615, July 31, 2002; 73 FR 5108, Jan. 29, 2008; 75 FR 60237, Sept. 29, 2010]

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§180.111 Malathion; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of 

diethyl mercaptosuccinate) in or on the following food commodities: 

Commodity Parts per million 

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Alfalfa, forage 135

Alfalfa, hay 135

Almond, hulls 50

Almond, postharvest 8

Apple 8

Apricot 8

Asparagus 8

Avocado 8

Barley, grain, postharvest 8

Bean, dry, seed 8

Bean, succulent 8

Beet, garden, roots 8

Beet, garden, tops 8

Beet, sugar, roots 1

Beet, sugar, tops 8

Blackberry 8

Blueberry 8

Boysenberry 8

Carrot, roots 8

Chayote, fruit 8

Chayote, roots 8

Cherry 8

Chestnut 1

Clover, forage 135

Clover, hay 135

Corn, field, forage 8

Corn, field, grain, postharvest 8

Corn, pop, grain, postharvest 8

Corn, sweet, forage 8

Corn, sweet, kernel plus cob with husks removed 2

Cowpea, forage 135

Cowpea, hay 135

Cranberry 8

Cucumber 8

Currant 8

Date, dried fruit 8

Dewberry 8

Eggplant 8

Fig 8

Flax, seed 0.1

Garlic, bulb 8

Gooseberry 8

Grape 8

Grapefruit 8

Guava 8

Hazelnut 1

Hop, dried cones 1

Horseradish 8

Kumquat 8

Leek 8

Lemon 8

Lentil, seed 8

Lespedeza, hay 135

Lime 8

Loganberry 8

Lupin, seed 8

Mango 8

Melon 8

Mushroom 8

Nectarine 8

Nut, macadamia 1

Oat, grain, postharvest 8

Okra 8

Onion, bulb 8

Onion, green 8

Orange 8

Papaya 1

Parsnip 8

Passionfruit 8

Pea 8

Pea, field, hay 8

Pea, field, vines 8

Peach 8

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Peanut, hay 135

Peanut, postharvest 8

Pear 8

Pecan 8

Pepper 8

Peppermint, tops 8

Pineapple 8

Plum 8

Plum, prune 8

Potato 8

Pumpkin 8

Quince 8

Radish 8

Raspberry 8

Rice, grain, postharvest 8

Rice, wild 8

Rutabaga 8

Rye, grain, postharvest 8

Safflower, seed 0.2

Salsify, roots 8

Salsify, tops 8

Shallot, bulb 8

Sorghum, grain, forage 8

Sorghum, grain, grain, postharvest 8

Soybean, forage 135

Soybean, hay 135

Soybean, seed 8

Soybean, vegetable, succulent 8

Spearmint, tops 8

Squash, summer 8

Squash, winter 8

Strawberry 8

Sunflower, seed, postharvest 8

Sweet potato, roots 1

Tangerine 8

Tomato 8

Trefoil, forage 135

Trefoil, hay 135

Turnip, greens 8

Turnip, roots 8

Vegetable, brassica, leafy, group 5 8

Vegetable, leafy, except brassica, group 4 8

Vetch, hay 135

Walnut 8

Wheat, grain, postharvest 8

(2) Tolerances are established for the combined residues of the insecticide malathion (O,O-dimethyl dithiophosphate 

of diethyl mercaptosuccinate) and its metabolite, malaoxon (O,O-dimethyl thiophosphate of diethyl mercaptosuccinate), in 

or on the following food commodities:

Commodity Parts per million

Barley, straw 50

Corn, field, stover 30.0

Cotton, undelinted seed 20.0

Grass, forage 200

Grass, hay 270

Oat, forage 4.0

Oat, straw 50

Rye, forage 4.0

Rye, straw 50

Watercress 0.2

Wheat, forage 4.0

Wheat, straw 50

(3) Tolerances are established for residues of the insecticide malathion (O,O-dimethyl dithiophosphate of diethyl 

mercaptosuccinate), in or on the following food commodities:

Commodity Parts per million

Cattle, fat 4

Cattle, meat1 4

Cattle, meat byproducts1 4

Egg 0.1

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Goat, fat 4

Goat, meat1 4

Goat, meat byproducts1 4

Hog, fat 4

Hog, meat1 4

Hog, meat byproducts1 4

Horse, fat 4

Horse, meat1 4

Horse, meat byproducts1 4

Milk, fat 0.5

Poultry, fat 4

Poultry, meat1 4

Poultry, meat byproducts1 4

Sheep, fat 4

Sheep, meat1 4

Sheep, meat byproducts1 4

1

The tolerance level shall not be exceeded in any cut of meat or in any meat byproducts from cattle, goat, hog, horse, 

poultry, or sheep.

(4) Malathion may be safely used in accordance with the following conditions: 

(i) It is incorporated into paper trays in amounts not exceeding 100 milligrams per square foot. 

(ii) Treated paper trays are intended for use only in the drying of grape (raisins). 

(iii) Total residues of malathion resulting from drying of grape on treated trays and from application to grape before 

harvest shall not exceed 12 parts per million on processed ready-to-eat raisins. 

(5) Residues of malathion in safflower, refined oil from application to the growing safflower plant shall not exceed 0.6 

parts per million. 

(6) Malathion may be safely used for the control of insects during the drying of grape (raisins) in compliance with 

paragraph (a)(4) of this section by incorporation into paper trays in amounts not exceeding 100 milligrams per square foot.

(7) Malathion (O,O-dimethyl dithiophosphate of diethyl mercaptosuccinate) may be safely used in feed in accordance 

with the following conditions. 

(i) A tolerance of 50 parts per million is established for residues of malathion in citrus, dried pulp for cattle feed, when 

present as the result of the application of the pesticide to bagged citrus pulp during storage. Whether or not tolerances for 

residues of malathion on the fresh fruit have been established under section 408 of the Act, the total residue of malathion 

in the citrus, dried pulp shall not exceed 50 parts per million. 

(ii) A tolerance of 10 parts per million is established for malathion in nonmedicated cattle feed concentrate blocks 

resulting from its application as a pesticide to paper used in packaging the nonmedicated cattle feed concentrate blocks. 

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 22974, May 30, 1978, as amended at 43 FR 45584, Oct. 3, 1978; 44 FR 38844, July 3, 1979; 45 FR 76145, Nov. 18, 1980; 

47 FR 42738, Sept. 29, 1982; 47 FR 55226, Dec. 8, 1982; 52 FR 45183, Nov. 25, 1987; 62 FR 66023, 66025, Dec. 17, 1997; 65 FR 

33694, May 24, 2000; 72 FR 35665, June 29, 2007; 73 FR 54959, Sept. 24, 2008; 74 FR 47455, Sept. 16, 2009; 75 FR 60238, Sept. 

29, 2010] 

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§180.114 Ferbam; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), 

calculated as carbon disulfide, in or on the following food commodities:

Commodity Parts per million Expiration/Revocation Date

Apple 4.01 None

Bean 7.01 10/27/07

Cabbage 7.01 10/27/07

Cherry 4.01 None

Cranberry 4.01 None

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Fruit, citrus, group 10 4.01 None

Grape 4.01 None

Lettuce 7.01 10/27/07

Nectarine 4.01 None

Peach 4.01 None

Pear 4.01 None

Raspberry 7.01 10/27/07

1

Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 

(formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure 

specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are 

established for residues of the fungicide ferbam (ferric dimethyldithiocarbamate), calculated as carbon disulfide, in or on 

the following food commodities:

Commodity Parts per million

Mango 4.01

1

This tolerance was established on the basis of data acquired at the public hearings held in 1950 (formerly §180.101) 

and the remainder was established on the basis of pesticide petitions presented under the procedure specified in the 

amendment to the Federal Food, Drug, and Cosmetic Act by Pub. L. 518, 83d Congress (68 Stat. 511)

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57072, Oct. 26, 1998, as amended at 72 FR 53453, Sept. 19, 2007]

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§180.116 Ziram; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ziram (zinc dimethyldithiocarbamate), calculated 

as zinc ethylenebisdithiocarbamate, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date

Almond 1

0.1 None

Apple 1

7.0 None

Apricot 1

7.0 None

Blackberry 1

7.0 5/11/13

Blueberry 1

7.0 None

Cherry, sweet 1

7.0 None

Cherry, tart 1

7.0 None

Grape 7.0 None

Huckleberry 7.0 None

Peach 7.0 None

Pear 1

7.0 None

Pecan 0.1 None

Quince 1

7.0 None

Strawberry 7.0 None

Tomato 1

7.0 None

1

Some of these tolerances were established on the basis of data acquired at the public hearings held in 1950 

(formerly §180.101) and the remainder were established on the basis of pesticide petitions presented under the procedure 

specified in the amendment to the Federal Food, Drug, and Cosmetic Act by Public Law 518, 83d Congress (68 Stat. 511).

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39437, July 1, 2003, as amended at 71 FR 54432, Sept. 15, 2006; 73 FR 54959, Sept. 24, 2008; 77 FR 59123, Sept. 26, 

2012]

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§180.117 S-Ethyl dipropylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl dipropylthiocarbamate, including its 

metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified 

in this paragraph is to be determined by measuring only the sum of S-ethyl dipropylthiocarbamate, S-ethyl 

(2-hydroxypropyl)propylcarbamothioate, S-(2-hydroxyethyl)dipropylcarbamothioate, and S-ethyl (3-hydroxypropyl)

propylcarbamothioate, calculated as the stoichiometric equivalent of S-ethyl dipropylthiocarbamate, in or on the 

commodity.

Commodity Parts per million

Alfalfa, forage 0.2

Alfalfa, hay 0.6

Almond 0.08

Almond, hulls 0.08

Bean, dry, seed 0.08

Bean, succulent 0.08

Beet, garden, tops 0.5

Beet, sugar, molasses 0.4

Beet, sugar, tops 0.5

Clover, forage 0.1

Clover, hay 0.1

Corn, field, forage 0.08

Corn, field, grain 0.08

Corn, field, stover 0.08

Corn, pop, grain 0.08

Corn, pop, stover 0.08

Corn, sweet, forage 0.08

Corn, sweet, kernel plus cob with husks removed 0.08

Corn, sweet, stover 0.08

Cotton, gin byproducts 0.20

Cotton, undelinted seed 0.08

Fruit, citrus, group 10 0.1

Lespedeza, forage 0.1

Lespedeza, hay 0.1

Pea, succulent 0.08

Safflower, seed 0.08

Sunflower, seed 0.08

Tomato 0.08

Trefoil, forage 0.1

Trefoil, hay 0.1

Vegetable, root 0.1

Walnut 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60239, Sept. 29, 2010]

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§180.121 Methyl parathion; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methyl parathion, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only methyl parathion, O,O-dimethyl O-(4-nitrophenyl) phosphorothioate, in 

or on the commodity.

Commodity

Parts per

million

Expiration/

Revocation

date

Alfalfa, forage 1.25 12/31/13

Alfalfa, hay 5.0 12/31/13

Almond 0.1 12/31/13

Almond, hulls 3.0 12/31/13

Barley 1.0 12/31/13

Corn, field, forage 1.0 12/31/13

Corn, field, grain 1.0 12/31/13

Corn, pop, grain 1.0 12/31/13

Corn, sweet, forage 1.0 12/31/13

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Corn, sweet, kernel plus cob with husks removed 1.0 12/31/13

Cotton, undelinted seed 0.75 12/31/13

Grass, forage 1.0 12/31/13

Oat 1.0 12/31/13

Onion 1.0 12/31/13

Pea, field, vines 1.0 12/31/13

Potato 0.1 12/31/13

Rapeseed, seed 0.2 12/31/13

Rice, grain 1.0 12/31/13

Soybean, hay 1.0 12/31/13

Soybean, seed 0.1 12/31/13

Sunflower, seed 0.2 12/31/13

Sweet potato, roots 0.1 12/31/13

Walnut 0.1 12/31/13

Wheat 1.0 12/31/13

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 1245, Jan. 5, 2001, as amended at 66 FR 38955, July 26, 2001; 67 FR 38603, June 5, 2002; 72 FR 35666, June 29, 2007; 

73 FR 54959, Sept. 24, 2008; 74 FR 46372, Sept. 9, 2009; 76 FR 56652, Sept. 14, 2011; 78 FR 60721, Oct. 2, 2013]

 Back to Top

§180.123 Inorganic bromide residues resulting from fumigation with methyl bromide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of inorganic bromides (calculated as Br) in or on the following 

food commodities which have been fumigated with the antimicrobial agent and insecticide methyl bromide after harvest 

(with the exception of strawberry):

Commodity Parts per million Expiration/Revocation Date 

Alfalfa, hay, postharvest 50.0 10/31/11

Almond, postharvest 200.0 None

Apple, postharvest 5.0 None

Apricot, postharvest 20.0 None

Artichoke, jerusalem, postharvest 30.0 None

Asparagus, postharvest 100.0 None

Avocado, postharvest 75.0 None

Barley, grain, postharvest 50.0 None

Bean, lima, postharvest 50.0 None

Bean, postharvest 50.0 None

Bean, snap, succulent, postharvest 50.0 None

Bean, succulent, postharvest 50.0 None

Beet, garden, roots, postharvest 30.0 None

Beet, sugar, roots, postharvest 30.0 None

Blueberry, postharvest 20.0 None

Butternut, postharvest 200.0 None

Cabbage, postharvest 50.0 None

Cacao bean, roasted bean, postharvest 50.0 None

Cantaloupe, postharvest 20.0 None

Carrot, roots, postharvest 30.0 None

Cashew, postharvest 200.0 None

Cherry, sweet, postharvest 20.0 None

Cherry, tart, postharvest 20 None

Chestnut, postharvest 200.0 None

Cippolini, bulb, postharvest 50.0 None

Citron, citrus, postharvest 30.0 None

Coconut, copra, postharvest 100.0 None

Coffee, bean, green, postharvest 75.0 None

Corn, field, grain, postharvest 50.0 None

Corn, pop, postharvest 240.0 None

Corn, sweet, kernel plus cob with husks removed, postharvest 50.0 None

Cotton, undelinted seed, postharvest 200.0 10/31/11

Cucumber, postharvest 30.0 None

Cumin, seed, postharvest 100.0 None

Eggplant, postharvest 20.0 None

Garlic, postharvest 50.0 None

Ginger, postharvest 100.0 None

Grape, postharvest 20.0 None

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Grapefruit, postharvest 30.0 None

Hazelnut, postharvest 200.0 None

Horseradish, postharvest 30.0 None

Kumquat, postharvest 30.0 None

Lemon, postharvest 30.0 None

Lime, postharvest 30.0 None

Melon, honeydew, postharvest 20.0 None

Muskmelon, postharvest 20.0 None

Nectarine, postharvest 20.0 None

Nut, brazil, postharvest 200.0 None

Nut, hickory, postharvest 200.0 None

Nut, macadamia, postharvest 200.0 None

Oat, postharvest 50.0 None

Okra, postharvest 30.0 None

Onion, bulb, postharvest 20.0 None

Onion, green, postharvest 20.0 None

Orange, postharvest 30.0 None

Parsnip, roots, postharvest 30.0 None

Peach, postharvest 20.0 None

Peanut, postharvest 200.0 None

Pear, postharvest 5.0 None

Pea, blackeyed, postharvest 50.0 None

Pea, postharvest 50.0 None

Pecan, postharvest 200.0 None

Pepper, postharvest 30.0 None

Pimento, postharvest 30.0 None

Pineapple, postharvest 20.0 None

Pistachio, postharvest 200.0 None

Plum, postharvest 20.0 None

Pomegranate, postharvest 100.0 None

Potato, postharvest 75.0 None

Pumpkin, postharvest 20.0 None

Quince, postharvest 5.0 None

Radish, postharvest 30.0 None

Rice, grain, postharvest 50.0 None

Rutabaga, roots, postharvest 30.0 None

Rutabaga, tops, postharvest 30.0 None

Rye, grain, postharvest 50.0 None

Salsify, roots, postharvest 30.0 None

Sorghum, grain, grain, postharvest 50.0 None

Soybean, postharvest 200.0 None

Squash, summer, postharvest 30.0 None

Squash, winter, postharvest 20.0 None

Squash, zucchini, postharvest 20.0 None

Strawberry, postharvest 60.0 None

Sweet potato, postharvest 75.0 None

Tangerine, postharvest 30.0 None

Timothy, hay, postharvest 50.0 10/19/10

Tomato, postharvest 20.0 None

Turnip, roots, postharvest 30.0 None

Walnut, postharvest 200.0 None

Watermelon, postharvest 20.0 None

Wheat 50.0 None

(2) Inorganic bromide may be present as a residue in certain processed food in accordance with the following 

conditions:

(i) When inorganic bromide residues are present as a result of fumigation of the processed food with methyl bromide 

or from such fumigation in addition to the authorized use of methyl bromide on the source raw agricultural commodity, as 

provided for in this part, the total residues of inorganic bromides (calculated as Br) shall not exceed the following levels:

(A) 400 parts per million in or on egg, dried and herb, processed and spice.

(B) 325 parts per million in or on cheese, parmesan and cheese, roquefort cheese.

(C) 250 parts per million in or on tomato, concentrated products and fig, dried fruit.

(D) 125 parts per million in or on processed food other than those listed above.

(ii) When inorganic bromide residues are present in malt beverage, fermented in accordance with 21 CFR 172.730(a)

(2), the amount shall not exceed 25 parts per million (calculated as Br).

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(iii) Where tolerances are established on both the raw agricultural commodities and processed food made therefrom, 

the total residues of inorganic bromides in or on the processed food shall not be greater than those designated in 

paragraph (a)(2) of this section, unless a higher level is established elsewhere in this part.

(3) Tolerances are established for residues of inorganic bromides (calculated as Br) as follows:

(i) 400 parts per million for residues in or on dog food, resulting from fumigation with methyl bromide.

(ii) 125 parts per million for residues in or on processed commodities for animal feedstuffs from barley, corn, grain 

sorghum, oat, rice, rye and wheat, resulting directly from fumigation with methyl bromide or from carryover and 

concentration of residues of inorganic bromides from fumigation of the grains with methyl bromide.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established 

for residues of inorganic bromides (calculated as Br) in or on the following food commodity grown in soil fumigated with 

methyl bromide.

Commodity Parts per million

Ginger, postharvest 100

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74812, Dec. 13, 2006, as amended at 75 FR 60239, Sept. 29, 2010]

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§180.123a Inorganic bromide residues in peanut hay and peanut hulls; statement of policy.

(a) Investigations by the Food and Drug Administration show that peanut hay and peanut shells have been used as 

feed for meat and dairy animals. While many growers now harvest peanuts with combines and leave the hay on the 

ground to be incorporated into the soil, some growers follow the practice of curing peanuts on the vines in a stack and 

save the hay for animal feed. Peanut shells or hulls have been used to a minor extent as roughage for cattle feed. It has 

been established that the feeding to cattle of peanut hay and peanut hulls containing residues of inorganic bromides will 

contribute considerable residues of inorganic bromides to the meat and milk.

(b) There are no tolerances for inorganic bromides in meat and milk to cover residues from use of such peanut hulls 

as animal feed. Peanut hulls containing residues of inorganic bromides from the use of methyl bromide are unsuitable as 

an ingredient in the feed of meat and dairy animals and should not be represented, sold, or used for that purpose.

[58 FR 65555, Dec. 15, 1993]

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§180.124 Methyl bromide; tolerances for residues.

(a) General. A tolerance is established for residues of the fumigant methyl bromide, including metabolites and 

degradates, in or on the commodity in the table below. Compliance with the tolerance level specified below is to be 

determined by measuring only methyl bromide.

Commodity

Parts per

million

Cotton, undelinted seed 150

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 35298, June 13, 2012]

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§180.127 Piperonyl butoxide; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide piperonyl butoxide [(butyl carbityl)(6-propyl piperonyl)ether] 

are established in or on the following food commodities:

Commodity Parts per million

Almond, postharvest 8

Apple, postharvest 8

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Barley, postharvest 20

Bean, postharvest 8

Birdseed, mixtures, postharvest 20 

Blackberry, postharvest 8 

Blueberry, postharvest 8 

Boysenberry, postharvest 8 

Buckwheat, grain, postharvest 20 

Cattle, fat 0.1 

Cattle, meat 0.1 

Cattle, meat byproducts 0.1 

Cherry, sweet, postharvest 8 

Cherry, tart, postharvest 8

Cacoa bean, roasted bean, postharvest 8 

Coconut, copra, postharvest 8 

Corn, field, grain, postharvest 20 

Corn, pop, postharvest 20

Cotton, undelinted seed, postharvest 8 

Crabapple, postharvest 8 

Currant, postharvest 8 

Dewberry, postharvest 8 

Egg 1 

Fig, postharvest 8 

Flax, seed, postharvest 8 

Goat, fat 0.1 

Goat, meat 0.1 

Goat, meat byproducts 0.1 

Gooseberry, postharvest 8 

Grape, postharvest 8 

Guava, postharvest 8 

Hog, fat 0.1 

Hog, meat 0.1 

Hog, meat byproducts 0.1 

Horse, fat 0.1 

Horse, meat 0.1 

Horse, meat byproducts 0.1 

Loganberry, postharvest 8 

Mango, postharvest 8 

Milk, fat 0.25 

Muskmelon, postharvest 8 

Oat, postharvest 8 

Orange, postharvest 8 

Peach, postharvest 8 

Peanut, postharvest 8 

Pea, postharvest 8 

Pear, postharvest 8 

Pineapple, postharvest 8 

Plum, prune, fresh, postharvest 8 

Potato, postharvest 0.25 

Poultry, fat 3 

Poultry, meat 3 

Poultry, meat byproducts 3 

Raspberry, postharvest 8 

Rice, postharvest 20 

Rye, postharvest 20 

Sheep, fat 0.1 

Sheep, meat 0.1 

Sheep, meat byproducts 0.1 

Sorghum, grain, postharvest 8 

Sweet potato, postharvest 0.25 

Tomato, postharvest 8 

Walnut, postharvest 8 

Wheat, postharvest 20

(2) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) In cereal grain mills and in storage areas for milled cereal grain products, whereby the amount of piperonyl 

butoxide is at least equal to but not more than 10 times the amount of pyrethrins in the formulation.

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(B) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams 

per square foot, whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. 

Such treated bags are to be used only for food, dried.

(C) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth, 

whereby the amount of piperonyl butoxide is equal to 10 times the amount of pyrethrins in the formulation. Such treated 

bags are constructed with waxed paper liners and are to be used only for food, dried that contain 4 percent fat or less.

(D) In two-ply bags consisting of cellophane/polyolefin sheets bound together by an adhesive layer when it is 

incorporated in the adhesive. The treated sheets shall contain not more than 50 milligrams of piperonyl butoxide per 

square foot (538 milligrams per square meter). Such treated bags are to be used only for packaging plum, prune, dried; 

grape, raisin; and other fruit, dried and are to have a maximum ratio of 3.12 milligrams of piperonyl butoxide per ounce of 

fruit (0.10 milligram of piperonyl butoxide per gram of product).

(E) In food processing and food storage areas: Provided, That the food is removed or covered prior to such use.

(ii) It is used or intended for use in combination with pyrethrins and N-octylbicycloheptene dicarboximide for insect 

control in accordance with 21 CFR 178.3730.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide in or on:

(A) Grain, cereal, milled fractions when present therein as a result of its use in cereal grain mills and in storage areas 

for milled cereal grain products.

(B) Food, dried when present as a result of migration from its use on the outer ply of multiwall paper bags of 50 

pounds or more capacity.

(C) Food treated in accordance with 21 CFR 178.3730.

(D) Food, dried that contain 4 percent fat, or less, when present as a result of migration from its use on the cloth of 

cotton bags of 50 pounds or more capacity constructed with waxed paper liners.

(E) Food treated in accordance with paragraph (a)(2)(i)(D) and (E) of this section.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. 

Environmental Protection Agency, and it shall be used in accordance with such label and labeling.

(v) Where tolerances are established on both raw agricultural commodities and processed food made therefrom, the 

total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of the 

two tolerances.

(3) Piperonyl butoxide may be safely used in accordance with the following prescribed conditions:

(i) It is used or intended for use in combination with pyrethrins for control of insects:

(A) On the outer ply of multiwall paper bags of 50 pounds or more capacity in amounts not exceeding 60 milligrams 

per square foot.

(B) On cotton bags of 50 pounds or more capacity in amounts not exceeding 55 milligrams per square foot of cloth. 

Such treated bags are constructed with waxed paper liners and are to be used only for feed, dried that contain 4 percent 

fat or less.

(ii) It is used in combination with pyrethrins, whereby the amount of piperonyl butoxide is equal to 10 times the amount 

of pyrethrins in the formulation. Such treated bags are to be used only for feed, dried.

(iii) A tolerance of 10 parts per million is established for residues of piperonyl butoxide when present as the result of 

migration:

(A) In or on feed, dried from its use on the outer ply of multiwall paper bags of 50 pounds or more capacity.

(B) In or on feed, dried that contain 4 percent fat, or less, from its use on cotton bags of 50 pounds or more capacity 

constructed with waxed paper liners.

(iv) To assure safe use of the pesticide, its label and labeling shall conform to that registered with the U.S. 

Environmental Protection Agency.

(v) Where tolerances are established on both the raw agricultural commodities and food, processed made therefrom, 

the total residues of piperonyl butoxide in or on the processed food shall not be greater than that permitted by the larger of 

the two tolerances.

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74813, Dec. 13, 2006]

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§180.128 Pyrethrins; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide pyrethrins ((1S)-2-methyl-4-oxo-3-(2Z)

-2,4-pentadienylcyclopenten-1-yl (1R,3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (pyrethrin 1), (1S)

-2-methyl-4-oxo-3-(2Z)-2,4-pentadienyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]

-2,2-dimethylcyclopropane-carboxylate (pyrethrin 2), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-cyclopenten-1-yl (1R,3R)

-2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate (cinerin 1), (1S)-3-(2Z)-2-butenyl-2-methyl-4-oxo-2-

cyclopenten-1-yl (1R,3R)-3-[(1E)-3-methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (cinerin 2), 

(1S)-2-methyl-4-oxo-3-(2Z)-2-pentenyl-2-cyclopenten-1-yl (1R, 3R)-2,2-dimethyl-3-(2-methyl-1-propenyl)

cyclopropanecarboxylate (jasmolin 1), and (1S)-2-methyl-4-oxo-3-(2Z)-pentenyl-2-cyclopenten-1-yl (1R,3R)-3-[(1E)-3-

methoxy-2-methyl-3-oxo-1-propenyl]-2,2-dimethylcyclopropanecarboxylate (jasmolin 2)), the insecticidally active principles 

of Chrysanthemum cinerariaefolium, which are measured as cumulative residues of pyrethrin 1, cinerin 1, and jasmolin 1 

are not to exceed the following:

Commodity Parts per million

Almond, postharvest 1.0

Apple, postharvest 1.0

Barley, grain, postharvest 3.0

Bean, succulent, postharvest 1.0

Birdseed, mixtures, postharvest 3.0

Blackberry, postharvest 1.0

Blueberry, postharvest 1.0

Boysenberry, postharvest 1.0

Buckwheat, grain, postharvest 3.0

Cacao bean, roasted bean, postharvest 1.0

Cattle, fat 1.0

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Cherry, sweet, postharvest 1.0

Cherry, tart, postharvest 1.0

Coconut, copra, postharvest 1.0

Corn, field, grain, postharvest 3.0

Corn, pop, grain, postharvest 3.0

Cotton, undelinted seed, postharvest 1.0

Crabapple, postharvest 1.0

Currant, postharvest 1.0

Dewberry, postharvest 1.0

Fig, postharvest 1.0

Flax, seed, postharvest 1.0

Goat, fat 1.0

Goat, meat 0.05

Goat, meat byproducts 0.05

Gooseberry, postharvest 1.0

Grape, postharvest 1.0

Guava, postharvest 1.0

Hog, fat 1.0

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 1.0

Horse, meat 0.05

Horse, meat byproducts 0.05

Loganberry, postharvest 1.0

Mango, postharvest 1.0

Milk, fat (reflecting negligible residues in milk) 0.05

Muskmelon, postharvest 1.0

Oat, grain, postharvest 1.0

Orange, postharvest 1.0

Pea, dry, seed, postharvest 1.0

Peach, postharvest 1.0

Peanut, postharvest 1.0

Pear, postharvest 1.0

Pineapple, postharvest 1.0

Plum, prune, fresh, postharvest 1.0

Potato, postharvest 0.05

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Raspberry, postharvest 1.0

Rice, grain, postharvest 3.0

Rye, grain, postharvest 3.0

Sheep, fat 1.0

Sheep, meat 0.05

Sheep, meat byproducts 0.05

Sorghum, grain, grain, postharvest 1.0

Sweet potato, postharvest 0.05

Tomato, postharvest 1.0

Walnut, postharvest 1.0

Wheat, grain, postharvest 3.0

(2) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on milled fractions derived 

from grain, cereal when present as a result of its use in cereal grain mills and in storage areas for milled cereal grain 

products.

(3) A tolerance of 1.0 ppm is established for residues of the insecticide pyrethrins in or on all food items in food 

handling establishments where food and food products are held, processed, prepared and/or served. Food must be 

removed or covered prior to use.

(4) Where tolerances are established on both the raw agricultural commodities and processed foods made there-from, 

the total residues of pyrethrins in or on the processed food shall not be greater than that permitted by the larger of the two 

tolerances.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74814, Dec. 13, 2006, as amended at 73 FR 5108, Jan. 29, 2008]

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§180.129 o-Phenylphenol and its sodium salt; tolerances for residues.

(a) General. Tolerances are established for combined residues of the fungicide o-phenylphenol and sodium 

o-phenylphenate, each expressed as o-phenylphenol, from postharvest application of either in or on the following food 

commodities:

Commodity Parts per million 

Apple 25 

Cantaloupe (NMT 10 ppm in edible portion) 125 

Carrot, roots 20 

Cherry 5 

Citrus fruits 10 

Cucumber 10 

Lemon 10 

Nectarine 5 

Orange 10 

Pepper, bell 10 

Peach 20 

Pear 25.0 

Pineapple 10 

Plum, prune, fresh 20 

Sweet potato, roots 15 

Tomato 10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54960, Sept. 24, 2008]

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§180.130 Hydrogen Cyanide; tolerances for residues.

(a) General. A tolerance for residues of the insecticide hydrogen cyanide from postharvest fumigation as a result of 

application of sodium cyanide is established as follows: 50 parts per million in or on Fruit, citrus. 

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(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999]

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§180.132 Thiram; tolerances for residues.

Link to an amendment published at 80 FR 72597, November 20, 2015.

(a) General. Tolerances for residues of the fungicide thiram (tetramethyl thiuram disulfide), including its metabolites 

and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified is to be 

determined by measuring only thiram.

Commodity Parts per million

Apple 7.0

Avocado1 15

Banana1 0.80

Peach 7.0

Strawberry 20

1

No U.S. registrations as of September 23, 2009. 

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 49615, July 31, 2002, as amended at 74 FR 48391, Sept. 23, 2009; 79 FR 8301, Feb. 12, 2014; 79 FR 18822, Apr. 4, 2014; 

80 FR 16306, Mar. 27, 2015; 80 FR 35252, June 19, 2015]

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§180.142 2,4-D; tolerances for residues.

Link to an amendment published at 80 FR 72597, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including 

its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be 

determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the 

acid, in or on the following commodities:

Commodity Parts per million

Almond hulls 0.1

Asparagus 5.0

Barley, bran 4.0

Barley, grain 2.0

Barley, straw 50

Berry, group 13 0.2

Cattle, fat 0.3

Cattle, kidney 4.0

Cattle, meat 0.3

Cattle, meat byproducts, except kidney 0.3

Corn, field, forage 6.0

Corn, field, grain 0.05

Corn, field, stover 50

Corn, pop, grain 0.05

Corn, pop, stover 50

Corn, sweet, forage 6.0

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 50

Cranberry 0.5

Fish 0.1

Fruit, citrus, group 10 3.0

Fruit, pome, group 11 0.05

Fruit, stone, group 12 0.05

Goat, fat 0.3

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Goat, kidney 4.0

Goat, meat 0.3

Goat, meat byproducts, except kidney 0.3

Grain, aspirated fractions 40

Grape 0.05

Grass, forage 360

Grass, hay 300

Hop, dried cones 0.2

Horse, fat 0.3

Horse, kidney 4.0

Horse, meat 0.3

Horse, meat byproducts, except kidney 0.3

Millet, forage 25

Millet, grain 2.0

Millet, straw 50

Milk 0.05

Nut, tree, group 14 0.2

Oat, forage 25

Oat, grain 2.0

Oat, straw 50

Pistachio 0.05

Potato 0.4

Rice, grain 0.5

Rice, hulls 2.0

Rice, straw 10

Rye, bran 4.0

Rye, forage 25

Rye, grain 2.0

Rye, straw 50

Sheep, fat 0.3

Sheep, kidney 4.0

Sheep, meat 0.3

Sheep, meat byproducts, except kidney 0.3

Shellfish 1.0

Sorghum, grain, forage 0.2

Sorghum, grain, grain 0.2

Sorghum, grain, stover 0.2

Soybean, forage 0.02

Soybean, hay 2.0

Soybean, seed 0.02

Strawberry 0.05

Sugarcane, cane 0.05

Sugarcane, molasses 0.2

Teff, bran 4.0

Teff, forage 25.0

Teff, grain 2.0

Teff, straw 50.0

Vegetable, leaves of root and tuber, group 2 0.1

Vegetable, root and tuber, except potato, group 1 0.1

Wheat, bran 4.0

Wheat, forage 25

Wheat, grain 2.0

Wheat, straw 50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the herbicide, plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels is to be determined by measuring residues 

of 2,4-D (2,4-dichlorophenoxyacetic acid), both free and conjugated, determined as the acid, in or on the follow 

commodities:

Commodity Parts per million

Rice, wild, grain 0.05

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide, 

plant regulator, and fungicide 2,4-D, including its metabolites and degradates, in or on the commodities in the table below. 

Compliance with the tolerances levels is to be determined by measuring residues of 2,4-D (2,4-dichlorophenoxyacetic 

acid), both free and conjugated, determined as the acid, in or on the following commodities:

Commodity Parts per million

Animal feed, nongrass, group 18 0.2

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Avocado 0.05

Cotton, undelinted seed 0.05

Dill, seed 0.05

Okra 0.05

Vegetable, brassica leafy, group 5 0.4

Vegetable, bulb, group 3 0.05

Vegetable, cucurbit, group 9 0.05

Vegetable, foliage of legume, group 7 0.2

Vegetable, fruiting, group 8 0.05

Vegetable, leafy, except brassica, group 4 0.4

Vegetable, legume, group 6 0.05

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 74 FR 48411, Sept. 23, 2009; 76 FR 55817, Sept. 9, 

2011]

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§180.145 Fluorine compounds; tolerances for residues.

(a) General. (1) Tolerances are established for combined residues of the insecticidal fluorine compounds cryolite and 

synthetic cryolite (sodium aluminum fluoride) in or on the following agricultural commodities:

Commodity Parts per million

Apricot 7

Blackberry 7

Blueberry 7

Boysenberry 7

Broccoli 7

Brussels sprouts 7

Cabbage 7

Cauliflower 7

Collards 7

Cranberry 7

Cucumber 7

Dewberry 7

Eggplant 7

Fruit, citrus 7

Grape 7

Kale 7

Kohlrabi 7

Lettuce, head 7

Lettuce, leaf 7

Loganberry 7

Melon 7

Nectarine 7

Peach 7

Pepper 7

Plum, prune, fresh 7

Pumpkin 7

Raspberry 7

Squash, summer 7

Squash, winter 7

Strawberry 7

Tomato 7

Youngberry 7

(2) Tolerances are established for residues of fluoride in or on the following commodities from the postharvest 

fumigation with sulfuryl fluoride for the control of insects:

Commodity Parts per million

All processed food commodities not otherwise listed 70

Barley, bran, postharvest 45.0

Barley, flour, postharvest 45.0

Barley, grain, postharvest 15.0

Barley, pearled barley, postharvest 45.0

Cattle, meat, dried 40

Cheese 5.0

Cacao bean, roasted bean, postharvest 20

Coconut, postharvest 40

Coffee, bean, green, postharvest 15

Corn, field, flour, postharvest 35.0

Corn, field, grain, postharvest 10.0

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Corn, field, grits, postharvest 10.0

Corn, field, meal, postharvest 30.0

Corn, pop, grain, postharvest 10.0

Cotton, undelinted seed, postharvest 70

Egg, dried 900

Fruit, dried, except grape, raisin, postharvest 3.0

Ginger, postharvest 70

Grain, aspirated fractions, postharvest 55.0

Grape, raisin, postharvest 7.0

Hog, meat 20

Herbs and spices group 19, postharvest 70

Milk, powdered 5.0

Millet, grain, postharvest 40.0

Nut, pine, postharvest 20

Nut, tree, Group 14, postharvest 10.0

Oat, flour, postharvest 75.0

Oat, grain, postharvest 25.0

Oat, groats/rolled oats 75.0

Peanut, postharvest 15

Pistachio, postharvest 10.0

Rice, bran, postharvest 31.0

Rice, flour, postharvest 45

Rice, grain, postharvest 12.0

Rice, hulls, postharvest 35.0

Rice, polished rice, postharvest 25.0

Rice, wild, grain, postharvest 25.0

Sorghum, grain, postharvest 40.0

Triticale, grain, postharvest 40.0

Vegetable, legume, group 6, postharvest 70

Wheat, bran, postharvest 40.0

Wheat, flour, postharvest 125.0

Wheat, germ, postharvest 130.0

Wheat, grain, postharvest 40.0

Wheat, milled byproducts, postharvest 130.0

Wheat, shorts, postharvest 40.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined by §180.1(l), are 

established for the combined residues of the insecticidal fluorine compounds, cryolite and synthetic cryolite (sodium 

aluminum fluoride), in or on the following raw agricultural commodities:

Commodity Parts per million

Kiwifruit 15

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74815, Dec. 13, 2006, as amended at 76 FR 34885, June 15, 2011]

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§180.151 Ethylene oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the antimicrobial agent and insecticide ethylene oxide, 

when used as a postharvest fumigant in or on the following food commodities: 

Commodity Parts per million

Herb and spice, group 19, dried, except basil 7

Licorice, roots 7

Peppermint, tops, dried 7

Sesame, seed 7

Spearmint, tops, dried 7

Vegetable, dried 7

Walnut 50

(2) Tolerances are established for residues of the ethylene oxide reaction product, 2-chloroethanol, commonly 

referred to as ethylene chlorohydrin, when ethylene oxide is used as a postharvest fumigant in or on food commodities as 

follows:

Commodity Parts per million

Herb and spice, group 19, dried, except basil 940

Licorice, roots 940

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Peppermint, tops, dried 940

Sesame, seed 940

Spearmint, tops, dried 940

Vegetable, dried 940

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33695, May 24, 2000, as amended at 74 FR 46696, Sept. 11, 2009]

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§180.153 Diazinon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide diazinon, O,O-diethyl O-[6-methyl2-(1-methylethyl)-4-pyrimidinyl]phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

Commodity Parts per million

Almond, hulls 3.0

Apple 0.50

Apricot 0.20

Bean, lima 0.50

Bean, snap, succulent 0.50

Beet, garden, roots 0.75

Beet, garden, tops 0.70

Blueberry 0.50

Caneberry subgroup 13-07A 0.75

Carrot, roots 0.75

Cattle, fat 0.50

Cherry, sweet 0.20

Cherry, tart 0.20

Cranberry 0.50

Endive 0.70

Fig 0.50

Ginseng 0.75

Grape 0.752

Hazelnut 0.50

Kiwifruit1 0.75

Lettuce 0.70

Melon 0.75

Mushroom 0.752

Nectarine 0.20

Onion, bulb 0.75

Onion, green 0.75

Pea, succulent 0.50

Peach 0.20

Pear 0.50

Pineapple 0.50

Plum, prune, fresh 0.20

Radish 0.50

Rutabaga 0.75

Spinach 0.70

Strawberry 0.50

Tomato 0.75

Vegetable, brassica, leafy, group 5 0.70

Watercress 0.05

1

There are no domestic registrations for kiwifruit as of March 6, 2002.

2

The expiration/revocation date for this tolerance is 9/10/2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the insecticide diazinon, O, O-diethyl O-[6-methyl-2-(1-methylethyl)-4-pyrimidinyl]

-phosphorothioate (CAS No. 333-41-5), in or on the following food commodities:

Commodity Parts per million

Almond 0.50

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Banana 0.20

Celery 0.70

Cucumber 0.75

Parsley, leaves 0.75

Parsnip 0.50

Pepper 0.5

Potato 0.10

Squash, summer 0.50

Squash, winter 0.75

Sweet potato, roots 0.10

Swiss chard 0.70

Turnip, roots 0.50

Turnip, tops 0.75

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 42738, Sept. 29, 1982]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.153, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.154 Azinphos-methyl; tolerances for residues.

(a) General. Tolerances for residues of the insecticide O,O-dimethyl S-[(4-oxo-1,2,3-benzotriazin-3(4H)-yl)methyl]

phosphorodithioate in or on the following raw agricultural commodities: 

Commodity Parts per million Expiration/Revocation Date 

Almond1 0.2 None

Almond, hulls1 5.0 None

Apple2 1.5 None

Blackberry3 2.0 None

Blueberry2 5.0 None

Boysenberry3 2.0 None

Brussels sprouts4 2.0 None

Cherry2 2.0 None

Crabapple2 1.5 None

Cranberry3 0.5 12/31/12

Loganberry3 2.0 None

Parsley, leaves2 5.0 None

Parsley, turnip rooted, roots2 2.0 None

Peach3 2.0 None

Pear2 1.5 None

Pistachio1 0.3 None

Plum, prune5 2.0 None

Quince5 1.5 None

Raspberry3 2.0 None

Walnut1 0.3 None

1

There are no U.S. registrations as of October 30, 2009.

2

There are no U.S. registrations as of September 30, 2012.

3

There are no U.S. registrations since September 30, 2006.

4

There are no U.S. registrations since September 30, 2008.

5

There are no U.S. registrations since December 28, 2005.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 38752, June 22, 2000, as amended at 74 FR 46697, Sept. 11, 2009]

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§180.155 1-Naphthaleneacetic acid; tolerances for residues.

(a) General. Tolerances are established for the residues of 1-naphthaleneacetic acid, including its metabolites and 

degradates in or on the commodities in the following table. Compliance with the tolerance levels specified is to be 

determined by measuring only 1-naphthaleneacetic acid and its conjugates, calculated as the Stoichiometric equivalent of 

1-naphthaleneacetic acid, in or on the commodity.

Commodity 

Parts per

million

Avocado 0.05

Cherry, sweet 0.1

Fruit, pome, group 11-10 0.15

Mango 0.05

Olive 0.7

Orange 0.1

Pineapple1 0.05

Potato 0.01

Rambutan 2.0

Sapote, mamey 0.05

Tangerine 0.1

1

There are no U.S. registrations since 1988.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 30218, May 22, 2013]

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§180.163 Dicofol; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide dicofol, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only dicofol as the sum of its p,p-dicofol and o,p-dicofol isomers: 4-chloroα-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)

benzenemethanol, in or on the commodity.

Commodity Parts per million Expiration/revocation date

Apple, wet pomace 38.0 10/31/16

Bean, dry, seed 0.5 10/31/16

Bean, succulent 3.0 10/31/16

Butternut 0.1 10/31/16

Caneberry subgroup 13A 5.0 10/31/16

Chestnut 0.1 10/31/16

Citrus, dried pulp 12.0 10/31/16

Citrus oil 200.0 10/31/16

Cotton, refined oil 0.5 10/31/16

Cotton, undelinted seed 0.1 10/31/16

Fruit, citrus, group 10 6.0 10/31/16

Fruit, pome, group 11 10.0 10/31/16

Fruit, stone, group 12 5.0 10/31/16

Grape 5.0 10/31/16

Grape, raisin 20.0 10/31/16

Hazelnut 0.1 10/31/16

Hop, dried cones 65.0 10/31/16

Nut, hickory 0.1 10/31/16

Nut, macadamia 0.1 10/31/16

Pecan 0.1 10/31/16

Peppermint, oil 30.0 10/31/16

Peppermint, tops 25.0 10/31/16

Spearmint, oil 30.0 10/31/16

Spearmint, tops 25.0 10/31/16

Strawberry 10.0 10/31/16

Tea, dried 50.0 None

Tea, plucked leaves 30.0 None

Vegetable, cucurbit, group 9 2.0 10/31/16

Vegetable, fruiting, group 8 2.0 10/31/16

Walnut 0.1 10/31/16

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(2) Tolerances are established for residues of the insecticide dicofol, including its metabolites and degradates, in or 

on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be 

determined by measuring only the sum of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, its 

isomer o,p-dicofol, 2-chloro-α-(4-chlorophenyl)-α-(trichloromethyl)benzenemethanol, and its metabolites 4-chloroα-(4-chlorophenyl)-α-(dichloromethyl)benzenemethanol and 2-chloro-α-(4-chlorophenyl)-α-(dichloromethyl)

benzenemethanol, calculated as the stoichiometric equivalent of p,p-dicofol, 4-chloro-α-(4-chlorophenyl)

-α-(trichloromethyl)benzenemethanol, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date

Cattle, fat 50.0 10/31/16

Cattle, liver 5.0 10/31/16

Cattle, meat 3.0 10/31/16

Cattle, meat byproducts, except liver 3.0 10/31/16

Egg 0.05 10/31/16

Goat, fat 50.0 10/31/16

Goat, liver 5.0 10/31/16

Goat, meat 3.0 10/31/16

Goat, meat byproducts, except liver 3.0 10/31/16

Hog, fat 50.0 10/31/16

Hog, liver 5.0 10/31/16

Hog, meat 3.0 10/31/16

Hog, meat byproducts, except liver 3.0 10/31/16

Horse, fat 50.0 10/31/16

Horse, liver 5.0 10/31/16

Horse, meat 3.0 10/31/16

Horse, meat byproducts, except liver 3.0 10/31/16

Milk, fat (reflecting 0.75 ppm in whole milk) 22.0 10/31/16

Poultry, fat 0.1 10/31/16

Poultry, meat 0.1 10/31/16

Poultry, meat byproducts 0.1 10/31/16

Sheep, fat 50.0 10/31/16

Sheep, liver 5.0 10/31/16

Sheep, meat 3.0 10/31/16

Sheep, meat byproducts, except liver 3.0 10/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34826, June 26, 1998, as amended at 72 FR 35665, June 29, 2007; 72 FR 41928, Aug. 1, 2007; 77 FR 59124, Sept. 26, 

2012]

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§180.169 Carbaryl; tolerances for residues.

Link to an amendment published at 80 FR 72597, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per 

se, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date

Alfalfa, forage 50 None

Alfalfa, hay 75 None

Almond, hulls 50 None

Apple, wet pomace 15 None

Asparagus 15 None

Banana 5.0 None

Beet, sugar, roots 0.5 None

Beet, sugar, tops 25 None

Bushberry subgroup 13-07B 3.0 None

Cabbage 21 None

Cactus, fruit 5.0 None

Cactus, pads 12 None

Caneberry subgroup 13-07A 12.0 None

Citrus, oil 20 None

Clover, forage 50 None

Clover, hay 70 None

Corn, field, forage 30 None

Corn, field, grain 0.02 None

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Corn, field, stover 20 None

Corn, pop, grain 0.02 None

Corn, pop, stover 20 None

Corn, sweet, forage 185 None

Corn, sweet, kernel plus cob with husks removed 0.1 None

Corn, sweet, stover 215 None

Cotton, undelinted seed 5.0 10/31/09

Cranberry 3.0 None

Dandelion, leaves 22 None

Endive 10 None

Flax, seed 0.5 None

Fruit, citrus, group 10 10 None

Fruit, pome, group 11 12 None

Fruit, stone, group 12 10 None

Grain, aspirated fractions 70 None

Grape 10 None

Grape, raisin 12 None

Grass, forage 100 None

Grass, hay 15 None

Leaf petiole subgroup 4B 3.0 None

Lettuce 10 None

Millet, proso, grain 1.0 None

Millet, proso, straw 20 None

Nut, tree group 14, except walnut 0.1 None

Okra 4.0 None

Olive 10 None

Oyster 0.25 None

Parsley, leaves 22 None

Pea and bean, dried shelled, except soybean, subgroup 6C 1.0 None

Peanut 0.05 None

Peanut, hay 20 None

Pineapple 2.0 None

Pistachio 0.1 None

Rice, grain 15 None

Rice, hulls 30 None

Rice, straw 60 None

Sorghum grain, forage 30 None

Sorghum grain, grain 10 None

Sorghum grain, stover 30 None

Soybean, forage 15 None

Soybean, hay 15 None

Soybean, seed 0.5 None

Spinach 22 None

Strawberry 4.0 None

Sunflower, seed 0.5 None

Sweet potato, roots 0.2 None

Trefoil, forage 15 None

Trefoil, hay 25 None

Vegetable, brassica, leafy, group 5, except cabbage 10 None

Vegetable, cucurbit, group 9 3.0 None

Vegetable, foliage of legume, subgroup 7A, except soybean 60 None

Vegetable, fruiting, group 8 5.0 None

Vegetable, leaves of root and tuber, group 2, except sugar beet tops 75 None

Vegetable, legume, edible podded, subgroup 6A 10 None

Vegetable, root and tuber, group 1, except sugar beet and sweet potato 2.0 None

Walnut 1.0 None

Wheat, forage 30 None

Wheat, grain 1.0 None

Wheat, hay 30 None

Wheat, straw 20 None

(2) Tolerances are established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate, including its 

metabolites: 1-naphthol (naphthyl-sulfate); 5,6-dihydrodihydroxycarbaryl; and 5,6-dihydrodihydroxy naphthol, calculated as 

1-naphthyl N-methylcarbamate and the free and conjugated residues of carbaryl: 5,6-dihydro-5,6-dihydroxy carbaryl and 

5-methoxy-6-hydroxy carbaryl, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date

Cattle, fat 0.5 None

Cattle, meat 1.0 None

Cattle, meat byproducts 3.0 None

Egg 0.5 10/31/09

Goat, fat 0.5 None

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Goat, meat 1.0 None

Goat, meat byproducts 3.0 None

Hog, fat 0.5 None

Hog, meat 1.0 None

Hog, meat byproducts 3.0 None

Horse, fat 0.5 None

Horse, meat 1.0 None

Horse, meat byproducts 3.0 None

Milk 1.0 None

Poultry, fat 5.0 10/31/09

Poultry, meat 5.0 10/31/09

Sheep, fat 0.5 None

Sheep, meat 1.0 None

Sheep, meat byproducts 3.0 None

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are 

established for residues of the insecticide carbaryl, 1-naphthyl N-methylcarbamate per se, in or on the following food 

commodities:

Commodity Parts per million

Dillweed, fresh leaves 0.2

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33695, May 24, 2000, as amended at 66 FR 38955, July 26, 2001; 67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 

73 FR 52611, Sept. 10, 2008; 74 FR 10490, Mar. 11, 2009]

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§180.172 Dodine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dodine, including its metabolites and degradates, 

in or on the commodities listed in the table below. Compliance with the tolerance levels specified in the table is to be 

determined by measuring only dodine, N-dodecylguanidine acetate; in or on the following commodities.

Commodity Parts per million

Almond, hull 30.0

Apple 5.0

Apple, wet pomace 15.0

Banana 0.50

Fruit, stone, crop group 12 5.0

Nuts, tree, crop group 14 0.3

Peanut 0.013

Pear 5.0

Strawberry 5.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52017, Sept. 12, 2007, as amended at 73 FR 45634, Aug. 6, 2008; 77 FR 72237, Dec. 5, 2012]

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§180.175 Maleic hydrazide; tolerances for residues.

(a) General. (1) Tolerances for residues of the herbicide and plant regulator maleic hydrazide 

(1,2-dihydro-3,6-pyridazinedione) are established in or on the following raw agricultural commodities:

Commodity Parts per million

Onion, bulb 15.0

Potato 50.0

(2) A food additive known as maleic hydrazide (1,2-dihydro-3,6-pyridazinedione) may be present in potato, chips 

when used in accordance with the following conditions:

(i) The food additive is present as a result of the application of a pesticide formulation containing maleic hydrazide to 

the growing potato plant in accordance with directions registered by the U.S. Environmental Protection Agency.

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(ii) The label of the pesticide formulation containing the food additive conforms to labeling registered by the U.S. 

Environmental Protection Agency.

(iii) The food additive is present in an amount not to exceed 160 parts per million by weight of the finished food.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 64293, Dec. 5, 1997, as amended at 64 FR 11792, Mar. 10, 1999; 67 FR 35048, May 17, 2002]

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§180.176 Mancozeb; tolerances for residues.

Link to an amendment published at 80 FR 72597, November 20, 2015.

(a) General. Tolerances are established for residues of mancozeb (a coordination product of zinc ion and maneb 

(manganese ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodities in the 

following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only 

those mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity Parts per million

Almond 0.1

Almond, hulls 4

Apple 0.6

Asparagus 0.1

Atemoya 3.0

Banana 2

Barley, bran 20

Barley, flour 20

Barley, grain 5

Barley, pearled barley 20

Barley, straw 25

Beet, sugar, dried pulp 3.0

Beet, sugar, roots 1.2

Beet, sugar, tops 60

Broccoli 7

Cabbage 9

Canistel 15.0

Cattle, kidney 0.5

Cattle, liver 0.5

Cherimoya 3.0

Corn, field, forage 40

Corn, field, grain 0.1

Corn, field, stover 15

Corn, pop, grain 0.1

Corn, pop, stover 40

Corn, sweet, forage 70

Corn, sweet, kernel plus cob with husks removed 0.1

Corn, sweet, stover 40

Cotton, undelinted seed 0.5

Crabapple 0.6

Cranberry 5

Custard apple 3.0

Fennel 2.5

Flax, seed 0.15

Ginseng 1.2

Goat, kidney 0.5

Goat, liver 0.5

Grape 1.5

Hog, kidney 0.5

Hog, liver 0.5

Horse, kidney 0.5

Horse, liver 0.5

Lettuce, head 3.5

Lettuce, leaf 18

Mango 15.0

Oat, flour 20

Oat, grain 5

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Oat, groats/rolled oats 20

Oat, straw 25

Onion, bulb 1.5

Papaya 10

Peanut 0.1

Peanut, hay 65

Pear 0.6

Pepper 12

Potato 0.2

Poultry, kidney 0.5

Poultry, liver 0.5

Quince 0.6

Rice, grain 0.06

Rye, bran 20

Rye, grain 5

Rye, straw 25

Sapodilla 15.0

Sapote, mamey 15.0

Sapote, white 15.0

Sheep, kidney 0.5

Sheep, liver 0.5

Sorghum, grain, forage 0.15

Sorghum, grain, grain 0.25

Sorghum, grain, stover 0.15

Star apple 15.0

Sugar apple 3.0

Tangerine1 10

Tomato 2.5

Vegetable, cucurbit, group 9 2.0

Walnut 0.70

Wheat, bran 20

Wheat, flour 20

Wheat, germ 20

Wheat, grain 5

Wheat, middlings 20

Wheat, shorts 20

Wheat, straw 25

1

There are no U.S. registrations for use of mancozeb on tangerine.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registrations, as defined in §180.1(l), is 

established for residues of the fungicide mancozeb, (a coordination product of zinc ion and maneb (manganese 

ethylenebisdithiocarbamate)), including its metabolites and degradates, in or on the commodity in the following table in this 

paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those 

mancozeb residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity Parts per million

Carrot, roots 1

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33708, May 24, 2000, as amended at 65 FR 49924, Aug. 16, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, Jan. 16, 2003; 

69 FR 29458, May 24, 2004; 71 FR 76199, Dec. 20, 2006; 74 FR 46372, Sept. 9, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 50913, Aug. 

18, 2010; 76 FR 18915, Apr. 6, 2011; 78 FR 44455, July 24, 2013; 79 FR 27501, May 14, 2014]

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§180.178 Ethoxyquin; tolerances for residues.

(a) General. A tolerance is established for residues of the plant regulator ethoxyquin (1,2-dihydro-6-

ethoxy-2,2,4-trimethylquinoline) from preharvest or postharvest use in or on the following commodity:

Commodity Parts per million

Pear 3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

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[63 FR 57073, Oct. 26, 1998]

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§180.181 Chlorpropham; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the plant regulator and herbicide chlorpropham (isopropyl 

m-chlorocarbanilate (CIPC) in or on the following food commodities:

Commodity Parts per million

Potato 30

Potato, wet peel 40

(2) Tolerances are established for the combined residues of the plant regulator and herbicide chlorpropham (isopropyl 

m-chlorocarbanilate (CIPC) and its metabolite 4-hydroxychlorpropham-O-sulfonic acid (4-HSA) in or on the following food 

commodities:

Commodity Parts per million

Cattle, fat 0.20

Cattle, kidney 0.30

Cattle, meat 0.06

Cattle, meat byproducts except kidney 0.06

Goat, fat 0.20

Goat, kidney 0.30

Goat, meat 0.06

Goat, meat byproducts except kidney 0.06

Hog, fat 0.20

Hog, kidney 0.30

Hog, meat 0.06

Hog, meat byproducts except kidney 0.06

Horse, fat 0.20

Horse, kidney 0.30

Horse, meat 0.06

Horse, meat byproducts except kidney 0.06

Milk 0.30

Sheep, fat 0.20

Sheep, kidney 0.30

Sheep, meat 0.06

Sheep, meat byproducts except kidney 0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 52487, Nov. 13, 1978, as amended at 63 FR 57073, Oct. 26, 1998; 72 FR 37653, July 11, 2007]

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§180.182 Endosulfan; tolerances for residues.

(a)(1) General. Tolerances are established for residues of the insecticide endosulfan, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its metabolite endosulfan sulfate, 

6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the 

stoichiometric equivalent of endosulfan, in or on the commodity.

Commodity Parts per million

Expiration/

revocation

date

Almond 0.3 7/31/12

Almond, hulls 1.0 7/31/12

Apricot 2.0 7/31/12

Bean 2.0 7/31/12

Broccoli 3.0 7/31/12

Brussels sprouts 2.0 7/31/12

Cabbage 4.0 7/31/12

Cantaloupe 1.0 7/31/12

Carrot, roots 0.2 7/31/12

Cattle, fat 13.0 7/31/16

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Cattle, liver 5.0 7/31/16

Cattle, meat 2.0 7/31/16

Cattle, meat byproducts, except liver 1.0 7/31/16

Cauliflower 2.0 7/31/12

Celery 8.0 7/31/12

Cherry, sweet 2.0 7/31/12

Cherry, tart 2.0 7/31/12

Collards 2.0 7/31/12

Cotton, gin byproducts 30.0 7/31/12

Cotton, undelinted seed 1.0 7/31/12

Cucumber 1.0 7/31/12

Eggplant 1.0 7/31/12

Goat, fat 13.0 7/31/16

Goat, liver 5.0 7/31/16

Goat, meat 2.0 7/31/16

Goat, meat byproducts, except liver 1.0 7/31/16

Hazelnut 0.2 7/31/12

Hog, fat 13.0 7/31/16

Hog, liver 5.0 7/31/16

Hog, meat 2.0 7/31/16

Hog, meat byproducts, except liver 1.0 7/31/16

Horse, fat 13.0 7/31/16

Horse, liver 5.0 7/31/16

Horse, meat 2.0 7/31/16

Horse, meat byproducts, except liver 1.0 7/31/16

Kale 2.0 7/31/12

Lettuce, head 11.0 7/31/12

Lettuce, leaf 6.0 7/31/12

Milk, fat 2.0 7/31/16

Muskmelon 1.0 7/31/12

Mustard greens 2.0 7/31/12

Mustard, seed 0.2 7/31/12

Nectarine 2.0 7/31/12

Nut, macadamia 0.2 7/31/12

Peach 2.0 7/31/12

Pear 2.0 7/31/13

Pineapple 1.0 7/31/16

Pineapple, process residue 20.0 7/31/16

Plum 2.0 7/31/12

Plum, prune 2.0 7/31/12

Sheep, fat 13.0 7/31/16

Sheep, liver 5.0 7/31/16

Sheep, meat 2.0 7/31/16

Sheep, meat byproducts, except liver 1.0 7/31/16

Squash, summer 1.0 7/31/12

Strawberry 2.0 7/31/16

Sweet potato, roots 0.15 7/31/12

Walnut 0.2 7/31/12

Watermelon 1.0 7/31/12

(2) A tolerance is established for the combined residues of the insecticide endosulfan, 6,7,8,9,10,10-

hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 4,3-benzodioxathiepin-3-oxide (alpha and beta isomers), and its 

metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2, 

4,3-benzodioxathiepin-3,3-dioxide in or on the commodity in the following table:

Commodity Parts per million

Expiration/

revocation date

Tea, dried 24 (reflecting less than 0.1 ppm in beverage tea) resulting from application of the insecticide to growing tea 7/31/16

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. (1) Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities 

in the table in this paragraph, when endosulfan is used in the state of Florida. Compliance with the tolerance levels 

specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-

hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its 

metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in 

or on the commodity.

Commodity Parts per million

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Expiration/

revocation

date

Apple 1.0 12/31/14

Apple, wet pomace 5.0 12/31/14

Blueberry 0.3 12/31/14

Corn, sweet, forage 12.0 12/31/14

Corn, sweet, kernel plus cob with husks removed 0.2 12/31/14

Corn, sweet, stover 14.0 12/31/14

Pepper 2.0 12/31/14

Potato 0.2 12/31/14

Pumpkin 1.0 12/31/14

Squash, winter 1.0 12/31/14

Tomato 1.0 12/31/14

(2) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the insecticide endosulfan, including its metabolites and degradates, in or on the commodities 

in the table in this paragraph, when endosulfan is used in the United States (except Florida). Compliance with the 

tolerance levels specified in this paragraph is to be determined by measuring only the sum of endosulfan, 6,7,8,9,10,10-

hexachloro-1,5,5a,6,9,9a-hexahydro-6,9-methano-2,4,3-benzodioxathiepin 3-oxide (alpha and beta isomers), and its 

metabolite endosulfan sulfate, 6,7,8,9,10,10-hexachloro-1,5,5a,6,9,9ahexahydro-6,9-methano-2,4,3-benzodioxathiepin-3,3-dioxide, calculated as the stoichiometric equivalent of endosulfan, in 

or on the commodity.

Commodity Parts per million

Expiration/

revocation

date

Apple 1.0 7/31/15

Apple, wet pomace 5.0 7/31/15

Blueberry 0.3 7/31/15

Corn, sweet, forage 12.0 7/31/15

Corn, sweet, kernel plus cob with husks removed 0.2 7/31/15

Corn, sweet, stover 14.0 7/31/15

Pepper 2.0 7/31/15

Potato 0.2 7/31/15

Pumpkin 1.0 7/31/15

Squash, winter 1.0 7/31/15

Tomato 1.0 7/31/15

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33696, May 24, 2000, as amended at 71 FR 54433, Sept. 15, 2006; 76 FR 56653, Sept. 14, 2011; 78 FR 8409, Feb. 6, 2013]

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§180.183 Disulfoton; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) 

phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance 

with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of disulfoton, 

O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) 

phosphorothioate; disulfoton sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog 

sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) 

phosphorodithioate; and disulfoton oxygen analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; 

calculated as the stoichiometric equivalent of disulfoton, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date 

Bean, lima 0.75 12/31/13

Bean, snap, succulent 0.75 12/31/13

Broccoli 0.75 12/31/13

Brussels sprouts 0.75 12/31/13

Cabbage 0.75 12/31/13

Cauliflower 0.75 12/31/13

Coffee, green bean 0.2 6/30/14

Cotton, undelinted seed 0.75 12/31/13

Lettuce, head 0.75 12/31/14

Lettuce, leaf 2 12/31/14

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration is established for residues of the 

insecticide disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, including its metabolites and degradates, in or 

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on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be 

determined by measuring only the sum of disulfoton, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorodithioate, and its 

metabolites demeton-S, O,O-diethyl S-(2-(ethylthio)ethyl) phosphorothioate; disulfoton sulfoxide, O,O-diethyl 

S-(2-(ethylsulfinyl)ethyl) phosphorodithioate; disulfoton oxygen analog sulfoxide, O,O-diethyl S-(2-(ethylsulfinyl)ethyl) 

phosphorothioate, disulfoton sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorodithioate; and disulfoton oxygen 

analog sulfone, O,O-diethyl S-(2-(ethylsulfonyl)ethyl) phosphorothioate; calculated as the stoichiometric equivalent of 

disulfoton, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date 

Asparagus 0.1 12/31/13

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57073, Oct. 26, 1998; 66 FR 38955, July 26, 2001; 67 FR 41806, June 19, 2002; 

67 FR 49615, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 73 FR 54960, Sept. 24, 2008; 74 FR 46697, Sept. 11, 2009; 75 FR 60240, 

Sept. 29, 2010]

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§180.184 Linuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-

methylurea), including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 

3,4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity:

Commodity Parts per million

Asparagus 7.0

Carrot, roots 1.0

Cattle, fat 0.2

Cattle, kidney 2.0

Cattle, liver 2.0

Cattle, meat 0.1

Cattle, meat byproducts except kidney and liver 0.1

Celeriac 1.0

Cilantro, dried leaves 10

Cilantro, fresh leaves 3.0

Coriander, seed 0.01

Corn, field, forage 1.0

Corn, field, grain 0.1

Corn, field, stover 6.0

Corn, sweet, forage 1.0

Corn, sweet, kernel plus cob with husks removed 0.25

Corn, sweet, stover 6.0

Cotton, gin byproducts 5.0

Cotton, undelinted seed 0.25

Dill, oil 2.0

Dill, seed 0.5

Dillweed, dried leaves 5.0

Dillweed, fresh leaves 1.5

Goat, fat 0.2

Goat, kidney 2.0

Goat, liver 2.0

Goat, meat 0.1

Goat, meat byproducts except kidney and liver 0.1

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.1

Horse, fat 0.2

Horse, kidney 2.0

Horse, liver 2.0

Horse, meat 0.1

Horse, meat byproducts except kidney and liver 0.1

Horseradish 0.05

Milk 0.05

Parsley, dried leaves 9.0

Parsley, leaves 4.0

Parsnip, roots 0.05

Parsnip, tops 0.05

Pea, dry, seed 0.09

Rhubarb 0.5

Sheep, fat 0.2

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Sheep, kidney 2.0

Sheep, liver 2.0

Sheep, meat 0.1

Sheep, meat byproducts except kidney and liver 0.1

Sorghum, grain, forage 1.0

Sorghum, grain, grain 0.25

Sorghum, grain, stover 1.0

Soybean, seed 1.0

Soybean, vegetable 1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide linuron 

[3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea], including its metabolites and degradates, in or on the commodities in the 

table below, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the 

tolerance levels specified below is to be determined by measuring only those linuron residues convertible to 

3.4-dichloroaniline, calculated as the stoichiometric equivalent of linuron, in or on the commodity. The tolerance expires 

and is revoked on the date specified in the table.

Commodity

Parts per

million Expiration/revocation date

Lentil 0.1 12/31/14

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are 

established for residues of the herbicide linuron (3-(3,4-dichlorophenyl)-1-methoxy-1-methylurea), including its metabolites 

and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only those linuron residues convertible to 3,4-dichloroaniline, calculated as the stoichiometric 

equivalent of linuron, in or on the commodity.

Commodity Parts per million

Celery 0.5

Potato 0.2

Wheat, forage 0.5

Wheat, grain 0.05

Wheat, hay 0.5

Wheat, straw 2.0

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 41822, Aug. 2, 1999, as amended at 72 FR 37653, July 11, 2007; 73 FR 51727, Sept. 5, 2008; 76 FR 81396, Dec. 28, 2011; 

79 FR 8307, Feb. 12, 2014]

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§180.185 DCPA; tolerances for residues.

(a) General. Tolerances for the combined residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its 

metabolites monomethyltetrachloroterephthalate (MTP) and tetrachloroterephthalic acid (TCP) (calculated as dimethyl 

tetrachloroterephthalate) are established in or on the following food commodities:

Commodity Parts per million

Cantaloupe 1.0

Garlic 1.0

Ginseng 2.0

Horseradish 2.0

Muskmelon 1.0

Onion, bulb 1.0

Onion, green 1.0

Strawberry 2.0

Tomato 1.0

Vegetable, brassica, leafy, group 5 5.0

Watermelon 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for the combined inadvertent residues of the herbicide dimethyl tetrachloroterephthalate (DCPA) and its 

metabolites monomethyl tetrachloroterephthalate acid (MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or 

on the following food commodities:

Commodity Parts per million

Radish, roots 2.0

Radish, tops 15.0

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(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of 

the herbicide dimethyl tetrachloroterephthalate (DCPA) and its metabolites monomethyl tetrachloroterephthalate acid 

(MTP) and terachlorophthalic acid (TCP) (calculated as DCPA) in or on the following food commodities:

Commodity Parts per million

Basil, dried leaves 20.0

Basil, fresh leaves 5.0

Bean, dry 2.0

Bean, mung, seed 2.0

Bean, snap, succulent 2.0

Celeriac 2.0

Chicory, roots 2.0

Chicory, tops 5.0

Chive 5.0

Coriander, leaves 5.0

Corn, field, forage 0.4

Corn, field, grain 0.05

Corn, field, stover 0.4

Corn, pop, forage 0.4

Corn, pop, grain 0.05

Corn, pop, stover 0.4

Corn, sweet, forage 0.4

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 0.4

Cotton, undelinted seed 0.2

Cucumber 1.0

Dill 5.0

Eggplant 1.0

Lettuce 2.0

Marjoram 5.0

Parsley, dried leaves 20.0

Parsley, leaves 5.0

Pea, blackeyed, seed 2.0

Pepper 2.0

Pimento 2.0

Potato 2.0

Radicchio 5.0

Radish, oriental, roots 2.0

Radish, oriental, tops 2.0

Rutabaga 2.0

Soybean 2.0

Squash, summer 1.0

Squash, winter 1.0

Sweet potato 2.0

Turnip, roots 2.0

Turnip, tops 5.0

Yam, true, tuber 2.0

[72 FR 52018, Sept. 12, 2007, as amended at 73 FR 53737, Sept. 17, 2008; 73 FR 80302, Dec. 31, 2008; 74 FR 14744, Apr. 1, 

2009]

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§180.189 Coumaphos; tolerances for residues.

(a) General. Tolerances for residues of the insecticide coumaphos (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-

benzopyran-7-yl phosphorothioate and its oxygen analog (O,O-diethyl O-3-chloro-4-methyl-2-oxo-2H-1-benzopyran-7-yl 

phosphate) in or on food commodities as follows: 

Commodity Parts per million

Cattle, fat 1.0

Cattle, meat 1.0

Cattle, meat byproducts 1.0

Goat, fat 1.0

Goat, meat 1.0

Goat, meat byproducts 1.0

Hog, fat 1.0

Hog, meat 1.0

Hog, meat byproducts 1.0

Honey 0.15

Honeycomb 45.0

Horse, fat 1.0

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Horse, meat 1.0

Horse, meat byproducts 1.0

Milk, fat ( = n in whole milk) 0.5

Sheep, fat 1.0

Sheep, meat 1.0

Sheep, meat byproducts 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 39077, July 21, 1999, as amended at 65 FR 49936, Aug. 16, 2000; 67 FR 46883, July 17, 2002; 69 FR 29458, May 24, 2004; 

72 FR 28876, May 23, 2007]

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§180.190 Diphenylamine; tolerances for residues.

(a) General. Tolerances for residues of the plant regulator diphenylamine are established in or on the following 

commodities: 

Commodity Parts per million 

Apple, wet pomace 30.0 

Apple from preharvest or postharvest use, including use of impregnated wraps 10.0 

Cattle, fat 0.01 

Cattle, liver 0.1 

Cattle, meat byproducts, except liver 0.01 

Cattle, meat 0.01 

Goat, fat 0.01 

Goat, liver 0.1 

Goat, meat byproducts, except liver 0.01 

Goat, meat 0.01 

Horse, fat 0.01 

Horse, liver 0.1 

Horse, meat byproducts, except liver 0.01 

Horse, meat 0.01 

Milk 0.01 

Pear (post harvest) 5.0

Sheep, fat 0.01 

Sheep, liver 0.1 

Sheep, meat byproducts, except liver 0.01 

Sheep, meat 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 25848, May 13, 1999, as amended at 66 FR 63198, Dec. 5, 2001; 72 FR 16283, Apr. 4, 2007; 76 FR 34885, June 15, 2011]

 Back to Top

§180.191 Folpet; tolerances for residues.

(a) General. Tolerances are established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on raw 

agricultural commodities as follows:

Commodity Parts per million

Apple1 5.0

Cranberry1 15.0

Cucumber1 2.0

Grape1 50.0

Grape, raisin1 80.0

Hop, dried cones 120.0

Lettuce1 50.0

Melon1 3.0

Onion,bulb1 2.0

Strawberry1 5.0

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Tomato1 25.0

1

 No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined in §180.1(l) are 

established for the fungicide folpet (N-(trichloromethylthio)phthalimide) in or on the following raw agricultural commodity:

Commodity Parts per million

Avocado 25.0

(d) Indirect or inadvertent residues. [Reserved]

[61 FR 37222, July 17, 1996, as amended at 68 FR 10388, Mar. 5, 2003; 69 FR 52192, Aug. 25, 2004; 72 FR 41928, Aug. 1, 2007]

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§180.198 Trichlorfon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide trichlorfon (dimethyl (2,2,2-trichloro-1-

hydroxyethyl) phosphonate) in or on the following food commodities:

Commodity Parts per million

Cattle, fat1 0.5

Cattle, meat1 0.2

Cattle, meat byproducts1 0.1

1

There are no U.S. registrations for cattle commodities as of June 24, 1999.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

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§180.200 Dicloran; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dicloran, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only dicloran, 2,6-dichloro-4-nitroaniline, in or on the commodity.

Commodity

Parts per

million Expiration/revocation date

Apricot 20 None

Bean, snap, succulent 20 None

Carrot, roots 10 11/2/11

Celery 15 None

Cherry, sweet 20 None

Cucumber 5 None

Endive 10 None

Garlic 5 None

Grape 10 None

Lettuce 10 None

Nectarine 20 None

Onion 10 None

Peach 20 None

Plum, prune, fresh 15 None

Potato 0.25 12/31/14

Rhubarb 10 None

Sweet potato, roots 10 None

Tomato 5 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

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§180.202 p-Chlorophenoxyacetic acid; tolerances for residues.

(a) General. A tolerance is established for the combined residues of the plant regulator p-chlorophenoxyacetic acid 

and its metabolite p-chlorophenol to inhibit embryonic root development in or on the following food commodity:

Commodity Parts per million

Bean, mung, sprouts 0.2

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 71 FR 56398, Sept. 27, 2006]

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§180.204 Dimethoate; tolerances for residues.

(a) General. Tolerances are established for total residues of the insecticide dimethoate (O,O-dimethyl S-(Nmethylcarbamoylmethyl) phosphorodithioate) including its oxygen analog (O,O-dimethyl S-(N- methylcarbamoylmethyl) 

phosphorothioate) in or on the following food commodities: 

Commodity Parts per million

Alfalfa, forage 2.0

Alfalfa, hay 2.0

Bean, dry, seed 2.0

Bean, lima 2.0

Bean, snap, succulent 2.0

Blueberry1 1.0

Broccoli 2.0

Cattle, meat byproducts 0.02

Cauliflower 2.0

Celery 2.0

Citrus, dried pulp 5.0

Corn, field, forage 1.0

Corn, field, grain 0.1

Corn, field, stover 1.0

Corn, pop, grain 0.1

Corn, pop, stover 1.0

Corn, sweet, forage 1.0

Cotton, undelinted seed 0.1

Egg 0.02

Endive 2.0

Goat, meat byproducts 0.02

Grapefruit 2.0

Hog, meat byproducts 0.02

Horse, meat byproducts 0.02

Kale 2.0

Lemon 2.0

Lettuce, leaf 2.0

Melon 1.0

Milk 0.002

Mustard greens 2.0

Orange 2.0

Pea 2.0

Pear 2.0

Pecan 0.1

Pepper 2.0

Potato 0.2

Poultry, meat byproducts 0.02

Safflower, seed 0.1

Sheep, meat byproducts 0.02

Sorghum, grain, forage 0.1

Sorghum, grain, grain 0.1

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Sorghum, grain, stover 0.1

Soybean, forage 2.0

Soybean, hay 2.0

Soybean, seed 0.05

Swiss chard 2.0

Tangerine 2.0

Tomato 2.0

Turnip, roots 0.2

Turnip, tops 2.0

Wheat, forage 2.0

Wheat, grain 0.04

Wheat, hay 2.0

Wheat, straw 2.0

1

 There are U.S. registrations as of August 16, 1996.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for total residues of dimethoate including its oxygen analog in or on the following food commodities:

Commodity Parts per million

Asparagus 0.15

Brussels sprouts 5.0

Cherry, sweet 2.0

Cherry, tart 2.0

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33697, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 53737, Sept. 17, 2008]

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§180.205 Paraquat; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for residues of the desiccant, defoliant, and herbicide paraquat (1,1′

-dimethyl-4,4′-bipyridinium-ion) derived from application of either the bis(methyl sulfate) or the dichloride salt (both 

calculated as the cation) in or on the following food commodities:

Commodity Parts per million

Acerola 0.05

Almond, hulls 0.5

Animal feed, nongrass, group 18, forage 75.0

Animal feed, nongrass, group 18, hay 210.0

Artichoke, globe 0.05

Asparagus 0.5

Atemoya 0.05

Avocado 0.05

Banana 0.05

Barley, grain 0.05

Barley, hay 3.5

Barley, straw 1.0

Beet, sugar, roots 0.5

Beet, sugar, tops 0.05

Berry group 13 0.05

Biriba 0.05

Cacao bean, bean 0.05

Canistel 0.05

Carrot, roots 0.05

Cattle, fat 0.05

Cattle, kidney 0.5

Cattle, meat 0.05

Cattle, meat byproducts, except kidney 0.05

Cherimoya 0.05

Coffee, bean, green 0.05

Corn, field, forage 3.0

Corn, field, grain 0.1

Corn, field, stover 10.0

Corn, pop, grain 0.1

Corn, pop, stover 10.0

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Corn, sweet, kernel plus cob with husks removed 0.05

Cotton, gin byproducts 110.0

Cotton, undelinted seed 3.5

Cowpea, forage 0.1

Cowpea, hay 0.4

Cranberry 0.05

Custard apple 0.05

Egg 0.01

Endive 0.05

Feijoa 0.05

Fig 0.05

Fruit, citrus, group 10 0.05

Fruit, pome, group 11 0.05

Fruit, stone, group 12 0.05

Goat, fat 0.05

Goat, kidney 0.5

Goat, meat 0.05

Goat, meat byproducts, except kidney 0.05

Grain, aspirated fractions 65.0

Grape 0.05

Grass, forage 90.0

Grass, hay 40.0

Guar, seed 0.5

Guava 0.05

Hog, fat 0.05

Hog, kidney 0.5

Hog, meat 0.05

Hog, meat byproducts, except kidney 0.05

Hop, dried cones 0.5

Horse, fat 0.05

Horse, kidney 0.5

Horse, meat 0.05

Horse, meat byproducts, except kidney 0.05

Ilama 0.05

Jaboticaba 0.05

Kiwifruit 0.05

Lentil, seed 0.3

Lettuce 0.05

Longan 0.05

Lychee 0.05

Mango 0.05

Milk 0.01

Nut, tree, group 14 0.05

Okra 0.05

Olive 0.05

Onion, bulb 0.1

Onion, green 0.05

Papaya 0.05

Passionfruit 0.2

Pawpaw 0.05

Pea and bean, dried shelled, except soybean, subgroup 6C, except guar bean 0.3

Pea and bean, succulent shelled, subgroup 6B 0.05

Pea, field, hay 0.8

Pea, field, vines 0.2

Peanut 0.05

Peanut, hay 0.5

Peppermint, tops 0.5 

Persimmon 0.05

Pineapple 0.05

Pineapple, process residue 0.25

Pistachio 0.05

Pomegranate 0.05

Pulasan 0.05

Rambutan 0.05

Rhubarb 0.05

Rice, grain 0.05

Rice, straw 0.06

Safflower, seed 0.05

Sapodilla 0.05

Sapote, black 0.05

Sapote, mamey 0.05

Sapote, white 0.05

Sheep, fat 0.05

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Sheep, kidney 0.5

Sheep, meat 0.05

Sheep, meat byproducts, except kidney 0.05

Sorghum, forage, forage 0.1

Sorghum, grain, forage 0.1

Sorghum, grain, grain 0.05

Soursop 0.05

Soybean, forage 0.4

Soybean, hay 10.0

Soybean, hulls 4.5

Soybean, seed 0.7

Spanish lime 0.05

Spearmint, tops 0.5 

Star apple 0.05

Starfruit 0.05

Strawberry 0.25

Sugar apple 0.05

Sugarcane, cane 0.5

Sugarcane, molasses 3.0

Sunflower, seed 2.0

Turnip, greens 0.05

Turnip, roots 0.05

Vegetable, brassica, leafy, group 5 0.05

Vegetable, cucurbit, group 9 0.05

Vegetable, fruiting, group 8 0.05

Vegetable, legume, edible podded, subgroup 6A 0.05

Vegetable, tuberous and corm, subgroup 1C 0.50

Wax jambu 0.05

Wheat, forage 0.5

Wheat, grain 1.1

Wheat, hay 3.5

Wheat, straw 50.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(l), are established 

for residues of the pesticide paraquat (1,1′-dimethyl-4,4′ bipyridinium ion) derived from application of either the bis(methyl 

sulfate) or the dichloride salt (both calculated as the cation) in or on the following food commodities:

Commodity Parts per million

Pea, pigeon, seed 0.05

Taro, corm 0.1

Tyfon 0.05

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 51614, Oct. 21, 1981]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.205, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.206 Phorate; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide phorate (O,O-diethyl S (ethylthio) 

methyl]phosphorodithioate), phorate sulfoxide, phorate sulfone, phorate oxygen analog, phorate oxygen analog sulfoxide, 

and phorate oxygen analog sulfone in or on the following food commodities:

Commodity Parts per million

Bean, dry, seed 0.05

Bean, succulent 0.05

Beet, sugar, roots 0.3

Beet, sugar, tops 3.0

Coffee, green bean1 0.02

Corn, field, forage 0.5

Corn, field, grain 0.05

Corn, sweet, forage 0.5

Corn, sweet, kernel plus cob with husks removed 0.05

Cotton, undelinted seed 0.05

Hop, dried cones 2.0

Peanut 0.1

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Potato 0.2

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.1

Soybean, seed 0.05

Sugarcane, cane 0.05

Wheat, forage 1.5

Wheat, grain 0.05

Wheat, hay 1.5

Wheat, straw 0.05

1

 There are no U.S. registrations as of September 1, 1993 for the use of phorate on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[58 FR 62038, Nov. 24, 1993, as amended at 63 FR 2165, Jan. 14, 1998; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 

67 FR 49616, July 31, 2002; 71 FR 74816, Dec. 13, 2006; 73 FR 53738, Sept. 17, 2008]

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§180.207 Trifluralin; tolerances for residues.

(a) General. Tolerances are established for residues of trifluralin, including its metabolites and degradates, in or on 

the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by only trifluralin α,α,α-trifluoro-2,6-dinitro-N,N-dipropyl-p-toluidine, in or on the commodity.

Commodity Parts per million

Alfalfa, forage 3.0

Alfalfa, hay 2.0

Almond, hulls 0.05

Asparagus 0.05

Barley, grain 0.05

Barley, hay 0.05

Barley, straw 0.05

Bean, mung, sprouts 2.0

Carrot, roots 1.0

Celery 0.05

Corn, field, forage 0.05

Corn, field, grain 0.05

Corn, field, stover 0.05

Cotton, gin byproducts 0.05

Endive 0.05

Fruit, citrus, group 10 0.05

Fruit, stone, group 12 0.05

Grape 0.05

Hop, dried cones 0.05

Nut, tree, group 14 0.05

Oilseed, crop group 20 0.05

Okra 0.05

Peanut 0.05

Peanut, hay 0.05

Peppermint, oil 2.0

Peppermint, tops 0.05

Sorghum, grain, forage 0.05

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.05

Spearmint, oil 2.0

Spearmint, tops 0.05

Sugarcane, cane 0.05

Vegetable, brassica, leafy group 5 0.05

Vegetable, bulb, group 3 0.05

Vegetable, cucurbit, group 9 0.05

Vegetable, foliage of legume, group 7 0.05

Vegetable, fruiting, group 8 0.05

Vegetable, leaves of root and tuber, group 2 0.05

Vegetable, legume, group 6 0.05

Vegetable, root and tuber, group 1, except carrot 0.05

Wheat, grain 0.05

Wheat, straw 0.05

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(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 42619, June 25, 1980, as amended at 45 FR 56346, Aug. 25, 1980; 45 FR 86493, Dec. 31, 1980; 46 FR 37250, July 20, 

1981; 47 FR 13524, Mar. 31, 1982; 47 FR 20309, May 12, 1982; 63 FR 57074, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 70 FR 

21643, Apr. 27, 2005; 71 FR 54433, Sept. 15, 2006; 78 FR 46274, July 31, 2013]

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§180.208 Benfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide benfluralin, N-butyl-N-ethyl-αααtrifluoro-2,6-dinitro-p-toluidine, in or on the following food commodities:

Commodity Parts per million

Alfalfa, forage 0.05

Alfalfa, hay 0.05

Clover, forage 0.05

Clover, hay 0.05

Lettuce 0.05

Trefoil, forage 0.05

Trefoil, hay 0.05

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 73 FR 52613, Sept. 10, 2008]

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§180.209 Terbacil; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide terbacil, (3-tert-butyl-5-chloro-6-

methyluracil) and its metabolites [3-tert-butyl-5-chloro-6-hydroxymethyluracil], [6-chloro-2,3-dihydro-7-hydroxymethyl 

3,3-dimethyl-5H-oxazolo(3,2-a) pyrimidin-5-one], and [6-chloro-2,3-dihydro-3,3,7-trimethyl-5H-oxazolo(3,2-a) pyrimidin-5-

one], calculated as terbacil, in or on the following raw agricultural commodities:

Commodity Parts per million

Alfalfa, forage 1.0

Alfalfa, hay 2.0

Apple 0.3

Asparagus 0.4

Blueberry 0.2

Caneberry subgroup 13A 0.2

Peach 0.2

Peppermint, tops 2.0

Spearmint, tops 2.0

Strawberry 0.1

Sugarcane, cane 0.4

Watermelon 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 30818, May 31, 2006]

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§180.210 Bromacil; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide bromacil (5-bromo-3-sec-butyl-6-methyluracil) in 

or on the following food commodities:

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Commodity Parts per million

Fruit, citrus 0.1

Pineapple 0.1

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

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§180.211 Propachlor; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide propachlor (2-chloro-Nisopropylacetanilide) and its metabolites containing the N-isopropylaniline moiety, calculated as 2-chloro-Nisopropylacetanilide, in or on the following raw agricultural commodities:

Commodity Parts per million

Cattle, fat 0.05

Cattle, kidney 0.2

Cattle, meat 0.02

Cattle, meat byproducts, except kidney 0.05

Corn, field, forage 3.0

Corn, field, grain 0.2

Corn, field, stover 1.0

Corn, sweet, forage 3.0

Goat, fat 0.05

Goat, kidney 0.2

Goat, meat 0.02

Goat, meat byproducts, except kidney 0.05

Hog, fat 0.02

Hog, meat 0.02

Hog, meat byproducts 0.02

Horse, fat 0.05

Horse, kidney 0.2

Horse, meat 0.02

Horse, meat byproducts, except kidney 0.05

Milk 0.02

Sheep, fat 0.05

Sheep, kidney 0.2

Sheep, meat 0.02

Sheep, meat byproducts, except kidney 0.05

Sorghum, forage, forage 8.0

Sorghum, grain, forage 8.0

Sorghum, grain, grain 0.25

Sorghum, grain, stover 12.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 25959, June 16, 1982, as amended at 47 FR 28381, June 30, 1982; 47 FR 28626, July 1, 1982; 47 FR 46701, Oct. 20, 1982; 

63 FR 57074, Oct. 26, 1998; 72 FR 53454, Sept. 19, 2007]

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§180.212 S-Ethyl cyclohexylethylthiocarbamate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide S-ethyl cyclohexylethylthiocarbamate in or on 

the following food commodities:

Commodity Parts per million

Beet, garden, roots 0.05(N)

Beet, garden, tops 0.05(N)

Beet, sugar, roots 0.05(N)

Beet, sugar, tops 0.05(N)

Spinach 0.05(N)

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(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003]

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§180.213 Simazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide simazine (2-chloro-4,6-bis

(ethylamino)-s-triazine) and its two chlorinated degradates (2-amino-4-chloro-6-ethylamino-s-triazine and 2,4-diamino-6-

chloro-s-triazine), the total residue to be measured in or on the following food commodities:

Commodity Parts per million

Almond 0.25

Almond, hulls 0.25

Apple 0.20

Avocado 0.20

Blackberry 0.20

Blueberry 0.20

Cattle, meat 0.03

Cattle, meat byproducts 0.03

Cherry 0.25

Corn, field, forage 0.20

Corn, field, grain 0.20

Corn, field, stover 0.25

Corn, pop, grain 0.20

Corn, pop, stover 0.25

Corn, sweet, forage 0.20

Corn, sweet, kernel plus cob with husks removed 0.25

Corn, sweet, stover 0.25

Cranberry 0.25

Currant 0.25

Egg 0.03

Goat, meat 0.03

Goat, meat byproducts 0.03

Grape 0.20

Grapefruit 0.25

Hazelnut 0.20

Horse, meat 0.03

Horse, meat byproducts 0.03

Lemon 0.25

Loganberry 0.20

Milk 0.03

Nut, macadamia 0.25

Olive 0.20

Orange 0.25

Peach 0.20

Pear 0.25

Pecan 0.20

Plum 0.20

Raspberry 0.20

Sheep, meat 0.03

Sheep, meat byproducts 0.03

Strawberry 0.25

Walnut 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 2165, Jan. 14, 1998, as amended at 63 FR 57074, Oct. 26, 1998; 72 FR 35665, June 29, 2007; 72 FR 53454, Sept. 19, 

2007]

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§180.215 Naled; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide naled (1,2-dibromo-2,2-dichloro-ethyl 

dimethyl phosphate) and its conversion product 2,2-dichlorovinyl dimethyl phosphate, expressed as naled, resulting from 

the application of the pesticide to growing crops or from direct application to livestock and poultry, in or on the following 

raw agricultural commodities:

Commodity Parts per million

Almond, hulls 0.5

Almond 0.5

Bean, dry, seed 0.5

Bean, succulent 0.5

Beet, sugar, roots 0.5

Beet, sugar, tops 0.5

Broccoli 1

Brussels sprouts 1

Cabbage 1

Cauliflower 1

Celery 3

Collards 3

Cotton, undelinted seed 0.5

Cucumber 0.5

Eggplant 0.5

Grape 0.5

Grapefruit 3

Grass, forage 10

Hop, dried cones 0.5

Kale 3

Legume, forage 10

Lemon 3

Melon 0.5

Orange, sweet 3

Peach 0.5

Pea, succulent 0.5

Pepper 0.5

Pumpkin 0.5

Safflower, seed 0.5

Spinach 3

Squash, summer 0.5

Squash, winter 0.5

Strawberry 1

Swiss chard 3

Tangerine 3

Tomato 0.5

Turnip, greens 3

Walnut 0.5

(2) A tolerance of 0.5 part per million is established for the pesticide naled in or on all raw agricultural commodities, 

except those otherwise listed in this section, from use of the pesticide for area pest (mosquito and fly) control.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 46304, Sept. 15, 1977, as amended at 54 FR 20125, May 10, 1989; 63 FR 57074, Oct. 26, 1998; 66 FR 50833, Oct. 5, 2001; 

77 FR 59124, Sept. 26, 2012]

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§180.217 Metiram; tolerances for residues.

(a) General. Tolerances are established for residues of a metiram (a mixture of 5.2 parts by weight of ammoniates of 

[ethylenebis (dithiocarbamato)] zinc with 1 part by weight ethylenebis [dithiocarbamic acid] bimolecular and trimolecular 

cyclic anhydrosulfides and disulfides), including its metabolites and degradates, in or on the commodities in the following 

table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those 

metiram residues convertible to and expressed in terms of the degradate carbon disulfide.

Commodity Parts per million

Apple 0.5

Apple, pomace, wet 2

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Banana1 3

Grape, wine1 5

Potato 0.2

1

There are no U.S. registrations on bananas and grape, wine as of April 29, 2011.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 57074, Oct. 26, 1998, as amended at 76 FR 23891, Apr. 29, 2011]

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§180.220 Atrazine; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide atrazine (2-chloro-4-ethylamino-6-

isopropylamino-s-triazine) and its chlorinated metabolites 2-amino-4-chloro-6-isopropylamino-s-triazine, 2-amino-4-chloro6-ethylamino-s-triazine, and 2,4-diamino-6-chloro-s-triazine, in or on the following food commodities:

Commodity

Parts per

million

Cattle, fat 0.02

Cattle, meat 0.02

Cattle, meat byproducts 0.02

Corn, field, forage 1.5

Corn, field, grain 0.20

Corn, field, stover 0.5

Corn, pop, forage 1.5

Corn, pop, grain 0.20

Corn, pop, stover 0.5

Corn, sweet, forage 15

Corn, sweet, kernel plus cob with husks removed 0.20

Corn, sweet, stover 2.0

Goat, fat 0.02

Goat, meat 0.02

Goat, meat byproducts 0.02

Grass, forage 4.0

Grass, hay 4.0

Guava 0.05

Horse, fat 0.02

Horse, meat 0.02

Horse, meat byproducts 0.02

Milk 0.02

Nut, macadamia 0.20

Sheep, fat 0.02

Sheep, meat 0.02

Sheep, meat byproducts 0.02

Sorghum, forage, forage 0.25

Sorghum, grain, forage 0.25

Sorghum, grain, grain 0.20

Sorghum, grain, stover 0.50

Sugarcane, cane 0.20

Wheat, forage 1.5

Wheat, grain 0.10

Wheat, hay 5.0

Wheat, straw 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertant residues of atrazine, 

2-chloro-4-ethylamino-6-isopropylamino-s-triazine, in or on the following raw agricultural commodity when present therein 

as a result of application of atrazine to the growing crops in paragraph (a) of this section:

Commodity Parts per million

Vegetable, leafy, except brassica, group 4 0.25

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[43 FR 29121, July 6, 1978, as amended at 44 FR 67116, Nov. 23, 1979; 47 FR 3771, Jan. 27, 1982; 47 FR 8012, Feb. 24, 1982; 63 

FR 57075, Oct. 26, 1998; 67 FR 46893, July 17, 2002; 69 FR 6567, Feb. 11, 2004; 72 FR 35666, June 29, 2007; 72 FR 53454, 

Sept. 19, 2007; 73 FR 37852, July 2, 2008; 76 FR 56654, Sept. 14, 2011]

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§180.222 Prometryn; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide prometryn, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)-6-methylthio-s-triazine, in or on the 

following raw agricultural commodities:

Commodity Parts per million

Bean, snap, succulent 0.05

Carrot, roots 0.45

Celeriac, roots 0.05

Celeriac, tops 0.20

Cilantro, leaves 3.5

Coriander, dried leaves 9.0

Cotton, gin byproducts 1.0

Cotton, undelinted seed 0.25

Dill, oil 1.3

Dillweed, dried leaves 1.1

Dillweed, fresh leaves 0.30

Leaf petioles subgroup 4B 0.50

Okra 0.05

Parsley, dried leaves 1.5

Parsley, leaves 0.60

Pea, pigeon, seed 0.25

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional exemptions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide 

prometryn, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the 

tolerance levels specified in the following table is to be determined by measuring only prometryn, 2,4-bis(isopropylamino)

-6-methylthio-s-triazine, in or on the following raw agricultural commodities.

Commodity Parts per million

Barley, forage 0.3

Barley, hay 1.0

Barley, straw 0.3

Oat, forage 0.3

Oat, hay 1.0

Oat, straw 0.3

Rye, forage 0.3

Rye, hay 1.0

Rye, straw 0.3

Triticale, forage 0.3

Triticale, hay 1.0

Triticale, straw 0.3

Wheat, forage 0.3

Wheat, hay 1.0

Wheat, straw 0.3

[43 FR 29121, July 6, 1978, as amended at 45 FR 51782, Aug. 5, 1980; 54 FR 6918, Feb. 15, 1989; 60 FR 20434, Apr. 26, 1995; 63 

FR 17692, Apr. 10, 1998; 63 FR 57075, Oct. 26, 1998; 64 FR 39082, July 21, 1999; 74 FR 47456, Sept. 16, 2009; 74 FR 67108, 

Dec. 18, 2009; 76 FR 34885, June 15, 2011; 78 FR 55640, Sept. 11, 2013]

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§180.225 Phosphine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of phosphine in or on the following raw agricultural 

commodities (RACs) resulting from post-harvest fumigation for the control of insects with phosphine gas or phosphide 

compounds that produce phosphine gas. 

Commodity Parts per million 

Almond 0.1 

Avocado 0.01 

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Banana 0.01 

Barley, grain 0.1 

Cabbage, Chinese, bok choy 0.01 

Cabbage, Chinese, napa 0.01 

Cacao bean, dried bean 0.1 

Cashew 0.1 

Citron, citrus 0.01 

Coffee, bean, green 0.1 

Corn, field, grain 0.1 

Corn, pop, grain 0.1 

Cotton, undelinted seed 0.1 

Date, dried fruit 0.1 

Dill, seed 0.01 

Eggplant 0.01 

Endive 0.01 

Grapefruit 0.01 

Hazelnut 0.1 

Kumquat 0.01 

Lemon 0.01 

Lettuce 0.01 

Lime 0.01 

Mango 0.01 

Millet, grain 0.1 

Mushroom 0.01 

Nut, brazil 0.1

Oat, grain 0.1 

Okra 0.01 

Orange, sweet 0.01 

Papaya 0.01 

Peanut 0.1 

Pecan 0.1 

Pepper 0.01 

Persimmon 0.01 

Pistachio 0.1 

Rice, grain 0.1 

Rye, grain 0.1 

Safflower, seed 0.1 

Salsify, tops 0.01 

Sesame, seed 0.1 

Sorghum, grain 0.1 

Soybean, seed 0.1 

Sunflower, seed 0.1 

Sweet potato, roots 0.01 

Tangelo 0.01 

Tangerine 0.01 

Tomato 0.01 

Vegetable, legume, group 6, except soybean 0.01 

Walnut 0.1 

Wheat, grain 0.1

(2) Tolerances are established for residues of the fumigant in or on all RACs resulting from preharvest treatment of 

pest burrows in agricultural and non-crop land areas. 

Commodity Parts per million 

All raw agricultural commodities resulting from preharvest treatment of pest burrows 0.01

(3) Residues resulting from fumigation of processed food:

Commodity Parts per million

Processed food 0.01

(4) Residues resulting from fumigation of animal feed: 

Commodity Parts per million 

Animal feed 0.1

(5) To assure safe use of this pesticide, it must be used in compliance with the labeling conforming to that registered 

by the U.S. Environmental Protection Agency (EPA) under FIFRA. Labeling shall bear a restriction to aerate the finished 

food/feed for 48 hours before it is offered to the consumer, unless EPA specifically determines that a different time period 

is appropriate. Where appropriate, a warning shall state that under no condition should any formulation containing 

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aluminum or magnesium phosphide be used so that it will come in contact with any processed food, except processed 

brewer's rice, malt, and corn grits stored in breweries for use in the manufacture of beer. 

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertant residues. [Reserved] 

[64 FR 72950, Dec. 29, 1999, as amended at 71 FR 74816, Dec. 13, 2006; 72 FR 41929, Aug. 1, 2007; 74 FR 46372, Sept. 9, 2009]

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§180.226 Diquat; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the plant growth regulator and herbicide diquat, 

(6,7-dihydrodipyrido (1,2-a:2′1′-c)pyrazinediium) derived from application of the dibromide salt and calculated as the cation 

in or on the following food commodities:

Commodity Parts per million

Alfalfa, seed 3.0

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Canola, meal 6.0

Canola, seed 2.0

Egg 0.05

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 0.05

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.05

Horse, meat 0.05

Horse, meat byproducts 0.05

Milk 0.02

Potato 0.1

Poultry, fat 0.05

Poultry, meat 0.05

Poultry, meat byproducts 0.05

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.05

(2)(i) Tolerances are established for residues of the herbicide diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) 

(calculated as the cation) derived from the application of the dibromide salt to ponds, lakes, reservoirs, marshes, drainage 

ditches, canals, streams, and rivers which are slow-moving or quiescent in programs of the Corp of Engineers or other 

Federal or State public agencies and to ponds, lakes and drainage ditches only where there is little or no outflow of water 

and which are totally under the control of the user, in or on the following food commodities:

Commodity Parts per million

Avocado 0.2

Berry group 13 0.05

Cotton, undelinted seed 0.2

Cranberry 0.05

Fish 2.0

Fruit, citrus, group 10 0.05

Fruit, pome, group 11 0.02

Fruit, stone, group 12 0.02

Grain, cereal, forage, fodder and straw, group 16 0.02

Grain, cereal, group 15 0.02

Grape 0.05

Grass, forage, fodder and hay, group 17 0.2

Hop, dried cones 0.2

Nut, tree, group 14 0.02

Shellfish 20.0

Strawberry 0.05

Sugarcane, cane 0.2

Vegetable, brassica, leafy, group 5 0.05

Vegetable, cucurbit, group 9 0.02

Vegetable, foliage of legume, group 7 0.2

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Vegetable, fruiting, group 8 0.05

Vegetable, leafy, except brassica, group 4 0.05

Vegetable, root and tuber, group 1 0.02

Vegetable, seed and pod 0.05

(ii) Where tolerances are established at higher levels from other uses of diquat on the subject crops, the higher 

tolerances applies also to residues of the aquatic uses cited in this paragraph. 

(3) Tolerances are established for the plant growth regulator diquat (6,7 dihydrodipyrido(1,2-a:2'1'-c)pyrazinediium) 

derived from application of the dibromide salt and calculated as the cation in or on the following food commodites:

Commodity Parts per million

Banana1 0.05

Coffee, bean, green1 0.05

Soybean, hulls 0.6

1

There are no U.S. registrations as of May 26, 2010.

(4) A tolerance of 0.5 part per million is established for residues of diquat in potato, granules/flakes and potato, chips. 

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33709, May 24, 2000, as amended at 72 FR 41929, Aug. 1, 2007; 75 FR 29441, May 26, 2010; 75 FR 60241, Sept. 29, 

2010]

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§180.227 Dicamba; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of the herbicide dicamba (3,6-dichloro-o-anisic acid), 

including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels 

is to be determined by measuring only the sum of the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 

3,6-dichloro-5-hydroxy-o-anisic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following 

commodities:

Commodity Parts per million

Barley, grain 6.0

Barley, hay 2.0

Barley, straw 15.0

Corn, field, forage 3.0

Corn, field, grain 0.1

Corn, field, stover 3.0

Corn, pop, grain 0.1

Corn, pop, stover 3.0

Corn, sweet, forage 0.50

Corn, sweet, kernel plus cob with husks removed 0.04

Corn, sweet, stover 0.50

Cotton, undelinted seed 0.2

Grass, forage, fodder and hay, group 17, forage 125.0

Grass, forage, fodder and hay, group 17, hay 200.0

Millet, proso, forage 90.0

Millet, proso, grain 2.0

Millet, proso, hay 40.0

Millet, proso, straw 30.0

Oat, forage 90.0

Oat, grain 2.0

Oat, hay 40.0

Oat, straw 30.0

Rye, forage 90.0

Rye, grain 2.0

Rye, straw 30.0

Sorghum, grain, forage 3.0

Sorghum, grain, grain 4.0

Sorghum, grain, stover 10.0

Sugarcane, cane 0.3

Sugarcane, molasses 5.0

Teff, forage 90.0

Teff, grain 6.0

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Teff, hay 40.0

Teff, straw 30.0

Wheat, forage 90.0

Wheat, grain 2.0

Wheat, hay 40.0

Wheat, straw 30.0

(2) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its 

metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be 

determined by measuring only the residues of dicamba (3,6-dichloro-o-anisic acid) and its metabolite, 3,6-dichloro-2-

hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in or on the following commodities:

Commodity Parts per million 

Asparagus 4.0 

Cattle, fat 0.3 

Cattle, kidney 25.0 

Cattle, meat 0.25 

Cattle, meat byproducts, except kidney 3.0 

Goat, fat 0.3 

Goat, kidney 25.0 

Goat, meat 0.25 

Goat, meat byproducts, except kidney 3.0 

Hog, fat 0.3 

Hog, kidney 25.0 

Hog, meat 0.25 

Hog, meat byproducts, except kidney 3.0 

Horse, fat 0.3 

Horse, kidney 25.0 

Horse, meat 0.25 

Horse, meat byproducts, except kidney 3.0 

Milk 0.2 

Sheep, fat 0.3 

Sheep, kidney 25.0 

Sheep, meat 0.25 

Sheep, meat byproducts, except kidney 3.0

(3) Tolerances are established for residues of the herbicide dicamba, 3,6-dichloro-o-anisic acid, including its 

metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be 

determined by measuring only the residues of dicamba, 3,6-dichloro-o-anisic acid, and its metabolites, 3,6-dichloro-5-

hydroxy-o-anisic acid, and 3,6-dichloro-2-hydroxybenzoic acid, calculated as the stoichiometric equivalent of dicamba, in 

or on the following commodities:

Commodity Parts per million 

Grain, aspirated fractions 1000 

Soybean, hulls 30.0 

Soybean, seed 10.0

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33709, May 24, 2000, as amended at 72 FR 35665, June 29, 2007; 73 FR 17918, Apr. 2, 2008; 73 FR 54960, Sept. 24, 

2008; 75 FR 60241, Sept. 29, 2010; 76 FR 55806, Sept. 9, 2011]

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§180.229 Fluometuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide fluometuron, N, N-dimethylN'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined as TFMA, in or on the 

following food commodities:

Commodity Parts per million

Cotton, gin byproducts 3.5

Cotton, undelinted seed 1.0

(2) Tolerances are established for the combined residues of the herbicide fluometuron, N,N-dimethylN'-[3-(trifluoromethyl)phenyl]urea, and its metabolites determined as TFMA and the hydroxylated metabolites: CGAeCFR — Code of Federal Regulations Page 95 of 441

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236431, 1-(4-hydroxy-3-trifluoromethylphenyl)urea; CGA-236432, 1-methyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea; and 

CGA-13211, 1,1-dimethyl-3-(4-hydroxy-3-trifluoromethylphenyl)urea, in or on the following food commodities:

Commodity Parts per million

Cattle, meat byproducts 0.1

Egg 0.1

Goat, meat byproducts 0.1

Hog, meat byproducts 0.1

Horse, meat byproducts 0.1

Milk 0.02

Poultry, fat 0.1

Poultry, meat 0.1

Poultry, meat byproducts 0.1

Sheep, meat byproducts 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the herbicide 

fluometuron, N, N-dimethyl-N'-[3-(trifluoromethyl)phenyl]urea, and its metabolite, trifluoromethylaniline (TFMA) determined 

as TFMA, in or on the following food commodities.

Commodity Parts per million

Grain, cereal, forage, fodder, and straw group 16, forage 3.0

Grain, cereal, forage, fodder, and straw, group 16, stover 6.0

Grain, cereal, group 15 0.5

Peanut 0.1

Peanut, hay 4.0

Peanut, meal 0.2

Soybean, forage 3.0

Soybean, hay 3.0

Soybean, seed 2.0

Rice, hulls 1.0

Wheat, milled byproducts 1.0

[73 FR 52613, Sept. 10, 2008]

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§180.231 Dichlobenil; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide dichlobenil 

(2,6-dichlorobenzonitrile) and its metabolite 2,6-dichlorobenzamide in or on the following raw agricultural commodities: 

Commodity Parts per million 

Apple 0.5 

Bushberry subgroup 13-07B 0.15

Caneberry subgroup 13-07A 0.10

Cranberry 0.1 

Fruit, stone, group 12 0.15 

Grape 0.15 

Hazelnut 0.1 

Pear 0.5 

Rhubarb 0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[36 FR 22540, Nov. 25, 1971, as amended at 63 FR 57075, Oct. 26, 1998; 66 FR 63198, Dec. 5, 2001; 73 FR 50570, Aug. 27, 2008]

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§180.232 Butylate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide butylate, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only butylate, S-ethyl bis (2-methylpropyl) carbamothioate, in or on the 

commodity.

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Commodity

Parts per

million Expiration/revocation date

Corn, field, forage 0.1 3/23/13

Corn, field, grain 0.1 3/23/13

Corn, field, stover 0.1 3/23/13

Corn, pop, grain 0.1 3/23/13

Corn, pop, stover 0.1 3/23/13

Corn, sweet, forage 0.1 3/23/13

Corn, sweet, kernel plus cob with husks removed 0.1 3/23/13

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39439, July 1, 2003, as amended at 76 FR 23493, Apr. 27, 2011; 77 FR 59125, Sept. 26, 2012]

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§180.235 Dichlorvos; tolerances for residues.

(a) General. (1) Tolerances for residues of the insecticide 2,2-dichlorovinyl dimethyl phosphate are established as 

follows:

Commodity Parts per million

Cattle, fat 0.02(N)

Cattle, meat 0.02(N)

Cattle, meat byproducts 0.02(N)

Egg 0.05(N)

Goat, fat 0.02(N)

Goat, meat 0.02(N)

Goat, meat byproducts 0.02(N)

Horse, fat 0.02(N)

Horse, meat 0.02(N)

Horse, meat byproducts 0.02(N)

Milk 0.02(N)

Mushroom (residues expressed as naled) 0.5

Poultry, fat 0.05(N)

Poultry, meat 0.05(N)

Poultry, meat byproducts 0.05(N)

Raw agricultural commodities, nonperishable, bulk stored regardless of fat content, postharvest 0.5

Raw agricultural commodities nonperishable, packaged or bagged, containing 6 percent fat or less, postharvest 0.5

Raw agricultural commodities, nonperishable, packaged or bagged, containing more than 6 percent fat, postharvest 2

Sheep, fat 0.02(N)

Sheep, meat 0.02(N)

Sheep, meat byproducts 0.02(N)

(2) The tolerance of 0.1 part per million prescribed by 21 CFR 556.180 for negligible residues of 2,2-dichlorovinyl 

dimethyl phosphate in hog, fat; hog, meat; hog, meat byproducts; and hog, skin covers both its use as an anthelmintic in 

swine feed and as an insecticide applied directly to swine.

(3) Dichlorvos may be present as a residue from application as an insecticide on packaged or bagged nonperishable 

processed food (see: 21 CFR 170.3(j)) in an amount in such food not in excess of 0.5 part per million (ppm). To assure 

safe use of the insecticide, its label and labeling shall conform to the label and labeling registered by the U.S. 

Environmental Protection Agency, and the usage employed shall conform with such label or labeling. 

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 55223, Dec. 8, 1982, as amended at 55 FR 26440, June 28, 1990; 56 FR 29183, June 26, 1991; 63 FR 57075, Oct. 26, 

1998; 65 FR 33697, May 24, 2000; 74 FR 46373, Sept. 9, 2009; 77 FR 59125, Sept. 26, 2012]

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§180.236 Triphenyltin hydroxide; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the fungicide triphenyltin hydroxide (TPTH) and 

its monophenyltin (MPTH) and diphenyltin (DPTH) hydroxide and oxide metabolites, expressed in terms of parent TPTH, 

in or on the following raw agricultural commodities:

Commodity Parts per million

Beet, sugar, roots 0.05

Beet, sugar, tops 10.0

Cattle, fat 0.2

Cattle, kidney 2.0

Cattle, liver 4.0

Cattle, meat 0.5

Goat, fat 0.2

Goat, kidney 2.0

Goat, liver 4.0

Goat, meat 0.5

Hog, fat 0.3

Hog, meat 0.06

Hog, meat byproducts 0.3

Horse, fat 0.2

Horse, kidney 2.0

Horse, liver 4.0

Horse, meat 0.5

Milk 0.06

Pecan 0.05

Potato 0.05

Sheep, fat 0.2

Sheep, kidney 2.0

Sheep, liver 4.0

Sheep, meat 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 41929, Aug. 1, 2007]

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§180.241 Bensulide; tolerances for residues.

(a) General. Tolerances are established for the residues of S-(O,O-diisopropyl phosphorodithioate) of 

N-(2-mercaptoethyl) benzenesulfonamide including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of 

N-(2-mercaptoethyl) benzenesulfonamide in or on the following food commodities:

Commodity Parts per million

Onion, bulb 0.10

Vegetable, brassica, leafy group 5 0.15

Vegetable, cucurbits group 9 0.15

Vegetable, fruiting group 8 0.10

Vegetable, leafy except brassica group 4 0.15

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for the residues of S-(O,O-diisopropyl phosphorodithioate) of N-(2-mercaptoethyl) benzenesulfonamide 

including its oxygen analog S-(O,O-diisopropyl phosphorothioate) of N-(2-mercaptoethyl) benzenesulfonamide in or on the 

following food commodities:

Commodity Parts per million

Carrot, roots 0.10

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 73 FR 53738, Sept. 17, 2008]

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§180.242 Thiabendazole; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolite benzimidazole (free and 

conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or on the commodity.

Commodity

Parts per

million

Alfalfa, forage 0.02

Alfalfa, hay 0.02

Apple, wet pomace 12.0

Avocado1 10.0

Banana, postharvest 3.0

Barley, grain 0.05

Barley, hay 0.30

Barley, straw 0.30

Bean, dry, seed 0.1

Brassica, head and stem, subgroup 5A 0.02

Cantaloupe1 15.0

Carrot, roots, postharvest 10.0

Citrus, oil 15.0

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Corn, pop, forage 0.01

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Corn, sweet, forage 0.01

Corn, sweet, kernels plus cop with husks removed 0.01

Corn, sweet, stover 0.01

Fruit, citrus, group 10, postharvest 10.0

Fruit, pome, group 11, postharvest 5.0

Mango 10.0

Mushroom 40.0

Oats, forage 0.30

Oats, grain 0.05

Oats, hay 0.30

Oats, straw 0.30

Onion, bulb, subgroup 3-07A 0.02

Papaya, postharvest 5.0

Potato, postharvest 10.0

Radish, tops 0.02

Rye, forage 0.30

Rye, grain 0.05

Rye, straw 0.30

Soybean 0.1

Spinach 0.02

Strawberry1 5.0

Sweet potato (postharvest to sweet potato intended only for use as seed) 0.05

Triticale, forage 0.30

Triticale, grain 0.05

Triticale, hay 0.30

Triticale, straw 0.30

Vegetable, cucurbit, group 9 0.02

Vegetable, root (except sugarbeet), subgroup 1B 0.02

Wheat, forage 0.30

Wheat, grain 0.05

Wheat, hay 0.30

Wheat, straw 0.30

1

There are no U.S. registrations on the indicated commodity.

(2) Tolerances are established for residues of thiabendazole, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and its metabolites 5-hydroxythiabendazole (free and 

conjugated) and benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole, in or 

on the commodity.

Commodity Parts per million

Cattle, meat 0.1

Cattle, meat byproducts 0.4

Goat, meat byproducts 0.4

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Hog, meat byproducts 0.3

Horse, meat byproducts 0.4

Milk 0.1

Sheep, meat byproducts 0.4

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

residues of the thiabendazole, including its metabolites and degradates, in or on the specified agricultural commodities, 

resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. Compliance with the tolerance 

levels specified below is to be determined by measuring only the sum of thiabendazole (2-(4-thiazolyl)benzimidazole) and 

its metabolite benzimidazole (free and conjugated), calculated as the stoichiometric equivalent of thiabendazole. The 

tolerances expire on the date specified in the table.

Commodity

Parts per

million Expiration date

Pea, succulent shelled 0.02 12/31/18

(c) Tolerances with regional exemptions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 32783, June 28, 1977]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.242, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.243 Propazine; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propazine, 2-chloro-4,6-bis(isopropylamino)

-s-triazine, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the 

tolerance levels specified in this paragraph is to be determined by measuring only the sum of propazine, 2-chloro-4,6-bis

(isopropylamino)-s-triazine, and its two chlorinated degradates, 2-amino-4-chloro-6-isopropylamino-s-triazine and 

2,4-diamino-6-chloro-s-triazine, calculated as the stoichiometric equivalent of propazine, in or on the commodity.

Commodity Parts per million

Sorghum, grain, forage 0.25

Sorghum, grain, grain 0.25

Sorghum, grain, stover 0.25

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60242, Sept. 29, 2010]

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§180.245 Streptomycin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide streptomycin in or on food commodities as 

follows:

Commodity Parts per million 

Bean, dry, seed 0.5 

Bean, succulent 0.5 

Fruit, pome, group 11 0.25

(2) Tolerances are established for residues of the fungicide streptomycin from treatment of seedling plants before 

transplanting in or on the following food commodities: 

Commodity Parts per million

Celery 0.25

Pepper 0.25

Tomato 0.25

(3) Tolerances are established for residues of the fungicide streptomycin from treatment of seed pieces in or on the 

following food commodity: 

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Commodity Parts per million

Potato 0.25

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of streptomycin, in or on 

the agricultural commodities, as specified in the following table, resulting from use of the pesticide pursuant to FIFRA 

section 18 emergency exemptions. Compliance with the tolerance levels listed in the following table is to be determined by 

measuring the levels of streptomycin only, in or on the commodities listed in the table. The tolerances expire on the dates 

specified in the table.

Commodity Parts per million Expiration date

Grapefruit 0.15 12/31/2015

Grapefruit, dried pulp 0.40 12/31/2015

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 73 FR 54960, Sept. 24, 2008; 78 FR 29055, May 17, 2013]

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§180.249 Alachlor; tolerances for residues.

(a) General. Tolerances are established for combined residues of alachlor (2-chloro-2′,6′′-diethyl-N-(methoxymethyl)

acetanilide) and its metabolites which can be converted to 2,6-diethylaniline (DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline 

(1-HEEA) upon basic hydrolysis, calculated as alachlor in or on the following raw agricultural commodities.

Commodity Parts per million

Beans, dry 0.1

Beans, succulent lima 0.1

Cattle, fat 0.02

Cattle, meat byproducts 0.02

Cattle, meat 0.02

Corn, field, forage 2.0

Corn, field, grain 0.2

Corn, field, pop 0.2

Corn, field, stover 2.0

Corn, pop, stover 2.0

Corn, sweet (K + CWHR) 0.05

Corn, sweet, stover 2.0

Cotton, gin byproducts 0.7

Cotton, undelinted seed 0.03

Cowpea, forage 5.0

Cowpea, hay 5.0

Egg 0.02

Goat, fat 0.02

Goat, meat byproducts 0.02

Goat, meat 0.02

Hog, fat 0.02

Hog meat byproducts 0.02

Hog, meat 0.02

Horse, fat 0.02

Horse, meat byproducts 0.02

Horse, meat 0.02

Milk 0.02

Peanut 0.5

Poultry, fat 0.02

Poultry, meat byproducts 0.02

Poultry, meat 0.02

Sheep, fat 0.02

Sheep, meat byproducts 0.02

Sheep, meat 0.02

Sorghum grain, forage 2.0

Sorghum, grain, grain 0.1

Sorghum, grain, stover 1.0

Soybeans, seed 1.0

Sunflower, meal 3.4

Sunflower, seed 2.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of alachlor 

(2-chloro-2′,6′-diethyl-N-(methoxymethyl)acetanilide) and its metabolites which can be converted to 2,6-diethylaniline 

(DEA) or 2-ethyl-6-(1-hydroxyethyl)aniline (1-HEEA) upon basic hydrolysis, calculated as alachlor, in or on the following 

raw agricultural commodities when present therein as a result of the application of alachlor to the growing crops in 

paragraph (a) of this section:

Commodity Parts per million

Animal feed, nongrass, group 18, forage 1.4

Animal feed, nongrass, group 18, hay 1.2

Grain, cereal, forage, and straw, group 16 except corn, sorghum, rice, straw 0.8

Grain, cereal, forage, fodder and straw, group 16 except corn, sorghum, rice, forage 0.6

Grain, cereal, forage, fodder, and straw, group 16 except for corn, sorghum, rice, hay 0.8

Grain, cereal, group 15 except corn, sorghum, rice 0.05

[72 FR 54584, Sept. 26, 2007]

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§180.252 Tetrachlorvinphos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide tetrachlorvinphos [(Z)-2-chloro1-(2,4,5-trichlorophenyl) vinyl dimethyl phosphate], including its metabolites, 1-(2,4,5-trichlorophenyl)-ethanol (free and 

conjugated forms), 2,4,5-trichloroacetophenone, and 1-(2,4,5-trichlorophenyl)-ethanediol, in or on the following 

commodities:

Commodity

Parts per

million

Cattle, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se) 0.2

Cattle, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se) 1.0

Cattle, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.5

Cattle, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se) 2.0

Cattle, meat byproducts, except kidney and liver 1.0

Egg (of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.2

Hog, fat (of which no more than 0.1 ppm is tetrachlorvinphos per se) 0.2

Hog, kidney (of which no more than 0.05 ppm is tetrachlorvinphos per se) 1.0

Hog, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.5

Hog, meat (of which no more than 2.0 ppm is tetrachlorvinphos per se) 2.0

Hog, meat byproducts, except kidney and liver 1.0

Milk, fat (reflecting negligible residues in whole milk and of which no more than 0.05 ppm is tetrachlorvinphos per se) 0.05

Poultry, fat (of which no more than 7.0 ppm is tetrachlorvinphos per se) 7.0

Poultry, liver (of which no more than 0.05 ppm is tetrachlorvinphos per se) 2.0

Poultry, meat (of which no more than 3.0 ppm is tetrachlorvinphos per se) 3.0

Poultry, meat byproducts, except liver 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 57659, Sept. 16, 2011, as amended at 78 FR 15882, Mar. 13, 2013; 78 FR 53684, Aug. 30, 2013]

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§180.253 Methomyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methomyl, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in 

or on the commodity.

Commodity Parts per million Expiration/revocation date

Alfalfa, forage 10 None

Alfalfa, hay 10 None

Apple 1 None

Asparagus 2 None

Avocado 2 None

Barley, grain 1 None

Barley, hay 10 None

Barley, straw 10 None

Bean, dry, seed 0.1 None

Bean, forage 10 None

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Bean, succulent 2 None

Beet, garden, tops 6 None

Bermudagrass, forage 10 None

Bermudagrass, hay 40 None

Blueberry 6 None

Broccoli 3 None

Brussels sprouts 2 None

Cabbage 5 None

Cabbage, Chinese, bok choy 5 None

Cabbage, Chinese, napa 5 None

Cauliflower 2 None

Celery 3 None

Collards 6 None

Corn, field, forage 10 None

Corn, field, grain 0.1 None

Corn, field, stover 10 None

Corn, pop, grain 0.1 None

Corn, pop, stover 10 None

Corn, sweet, forage 10 None

Corn, sweet, kernel plus cob with husks removed 0.1 None

Corn, sweet, stover 10 None

Cotton, undelinted seed 0.1 None

Dandelion, leaves 6 None

Endive 5 None

Grape 5 12/31/16

Grapefruit 2 None

Hop, dried cones1 12 None

Kale 6 None

Lemon 2 None

Lentil, seed 0.1 None

Lettuce 5 None

Mustard greens 6 None

Nectarine 5 None

Oat, forage 10 None

Oat, grain 1 None

Oat, hay 10 None

Oat, straw 10 None

Onion, dry bulb 0.2 None

Onion, green 3 None

Orange 2 None

Parsley, leaves 6 None

Pea 5 None

Pea, field, vines 10 None

Peach 5 None

Peanut 0.1 None

Pecan 0.1 None

Pepper, bell 2 None

Pepper, nonbell 2 None

Peppermint, tops 2 None

Pomegranate 0.2 None

Rye, forage 10 None

Rye, grain 1 None

Rye, straw 10 None

Sorghum, grain, forage 1 None

Sorghum, grain, grain 0.2 None

Soybean, forage 10 None

Soybean, seed 0.2 None

Spearmint, tops 2 None

Spinach 6 None

Swiss chard 6 None

Tangerine 2 None

Tomato 1 None

Turnip, greens 6 None

Vegetable, brassica, leafy, group 5 6.0 None

Vegetable, cucurbit, group 9 0.2 None

Vegetable, fruiting, group 8 0.2 None

Vegetables, leafy2 0.2 None

Vegetable, root and tuber, group 1 0.2 None

Wheat, forage 10 None

Wheat, grain 1 None

Wheat, hay 10 None

Wheat, straw 10 None

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1

There are no U.S. registrations for use of methomyl on hop, dried cone, as of February 14, 1990.

2

Except for Beet (tops), broccoli, Brussels sprouts, cabbage, cabbage, Chinese, cauliflower, celery, collards, 

dandelions, endive (escarole), kale, lettuce, mustard greens, parsley, spinach, Swiss chard, turnip, greens (tops), and 

watercress.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established 

for residues of the insecticide methomyl, including its metabolites and degradates, in or on the commodity in the table in 

this paragraph. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only 

methomyl, methyl N-[[(methylamino)carbonyl]oxy]ethanimidothioate, in or on the commodity.

Commodity

Parts

per million

Pear 4

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33697, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 

2010; 76 FR 34885, June 15, 2011; 77 FR 59125, Sept. 26, 2012; 80 FR 72598, Nov. 20, 2015]

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§180.254 Carbofuran; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide carbofuran 

(2,3-dihydro-2,2-dimethyl-7-benzofuranyl-N-methylcarbamate), its carbamate metabolite-2,3-dihydro-2,2-dimethyl-3-

hydroxy-7-benzofuranyl-N-methylcarbamate, and its phenolic metabolites 2,3-dihydro-2,2-dimethyl-7-benzofuranol, 

2,3-dihydro-2,2-dimethyl-3,-oxo-7-benzofuranol and 2,3-dihydro-2,2-dimethyl-3,7-benzofurandiol in or on the following raw 

agricultural commodities:

Commodity Parts per million

Banana1 0.1

Coffee, bean, green1 0.1

Rice, grain1 0.2

Sugarcane, cane1 0.1

1

There are no U.S. registrations for use of carbofuran on these commodities.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[39 FR 20597, June 12, 1974]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.254, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.257 Chloroneb; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide chloroneb, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of chloroneb, 1,4-dichloro-2,5-dimethoxybenzene, and its 

metabolite 2,5-dichloro-4-methoxyphenol (free and conjugated), calculated as the stoichiometric equivalent of chloroneb, 

in or on the commodity.

Commodity

Parts per

million

Expiration/

revocation

date

Bean, dry, seed 0.2 4/16/12

Bean, succulent 0.2 4/16/12

Beet, sugar, roots 0.2 4/16/12

Beet, sugar, tops 0.2 4/16/12

Cowpea, forage 2.0 4/16/12

Cowpea, hay 2.0 4/16/12

Cattle, fat 0.2 4/16/12

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Cattle, meat 0.2 4/16/12

Cattle, meat byproducts 0.2 4/16/12

Cotton, gin byproducts 1.0 4/16/12

Cotton, undelinted seed 0.2 4/16/12

Goat, fat 0.2 4/16/12

Goat, meat 0.2 4/16/12

Goat, meat byproducts 0.2 4/16/12

Hog, fat 0.2 4/16/12

Hog, meat 0.2 4/16/12

Hog, meat byproducts 0.2 4/16/12

Horse, fat 0.2 4/16/12

Horse, meat 0.2 4/16/12

Horse, meat byproducts 0.2 4/16/12

Milk 0.05 4/16/12

Sheep, fat 0.2 4/16/12

Sheep, meat 0.2 4/16/12

Sheep, meat byproducts 0.2 4/16/12

Soybean, forage 2.0 4/16/12

Soybean, hay 2.0 4/16/12

Soybean, seed 0.2 4/16/12

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 72 FR 53460, Sept. 19, 2007; 76 FR 56654, Sept. 14, 2011]

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§180.258 Ametryn; tolerances for residues.

(a) General. Tolerances are established for residues of the desiccant and herbicide (2-ethylamino)-4-(isopropylamino)

-6-(methylthio)-s-triazine in or on the following raw agricultural commodities:

Commodity Parts per million Expiration/Revocation Date 

Banana 0.25 6/16/10

Corn, field, forage 0.1 None

Corn, field, grain 0.05 None

Corn, field, stover 0.05 None

Corn, pop, grain 0.05 None

Corn, pop, stover 0.05 None

Corn, sweet, forage 0.5 6/16/10

Corn, sweet, kernel plus cob with husks removed 0.25 6/16/10

Corn, sweet, stover 0.5 6/16/10

Pineapple 0.05 None

Sugarcane, cane 0.05 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 29121, July 6, 1978, as amended at 48 FR 13175, Mar. 30, 1983; 48 FR 21132, May 11, 1983; 52 FR 33237, Sept. 2, 1987; 

63 FR 57075, Oct. 26, 1998; 73 FR 54961, Sept. 24, 2008; 74 FR 47456, Sept. 16, 2009]

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§180.259 Propargite; tolerances for residues.

(a) General. Tolerances are established for residues of the pesticide propargite (2-(p-tert-butylphenoxy) cyclohexyl 

2-propynyl sulfite) in or on the following food commodities. 

Commodity Parts per million 

Almond 0.1 

Almond, hulls 55.0 

Bean, dry, seed 0.2 

Cattle, fat 0.1 

Cattle, meat 0.1 

Cattle, meat byproducts 0.1 

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Citrus, oil 30.0 

Corn, field, forage 10.0 

Corn, field, grain 0.1 

Corn, field, stover 10.0 

Corn, pop, grain 0.1 

Corn, pop, stover 10.0 

Corn, sweet, forage 10.0 

Corn, sweet, stover 10.0 

Cotton, undelinted seed 0.1 

Egg 0.1 

Goat, fat 0.1 

Goat, meat 0.1 

Goat, meat byproducts 0.1 

Grain, aspirated fractions 0.4 

Grape 10.0 

Grapefruit 5.0 

Hog, fat 0.1 

Hog, meat 0.1 

Hog, meat byproducts 0.1 

Hop, dried cones 100.0 

Horse, fat 0.1 

Horse, meat 0.1 

Horse, meat byproducts 0.1 

Lemon 5.0 

Milk, fat (0.08 ppm in milk) 2.0 

Nectarine 4.0 

Orange 10.0 

Peanut 0.1 

Peppermint, tops 50.0 

Poultry, fat 0.1 

Potato 0.1 

Sheep, fat 0.1 

Sheep, meat 0.1 

Sheep, meat byproducts 0.1 

Sorghum, grain, forage 10.0 

Sorghum, grain, grain 5.0 

Sorghum, grain, stover 10.0 

Spearmint, tops 50.0 

Tea, dried 10.0 

Walnut 0.1

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of propargite in or on the following raw agricultural commodities: 

Commodity Parts per million 

Corn, sweet, kernel plus cob with husks removed 0.1

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33710, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 54961, Sept. 24, 2008; 76 FR 34885, June 15, 

2011]

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§180.261 Phosmet; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide phosmet, N-(mercaptomethyl) phthalimide 

S-(O,O-dimethyl phosphorodithioate), including its metabolites and degradates, in or on the commodities in the following 

table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of 

phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), and its oxygen analog, 

N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, calculated as the stoichiometric equivalent of 

phosmet, in or on the commodity.

Commodity Parts per million

Alfalfa, forage 20

Alfalfa, hay 40

Almond, hulls 10

Apple 10

Apricot 5

Blueberry 10

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Cattle, fat 0.2

Cattle, meat 0.1

Cattle, meat byproducts 0.1

Cherry 10

Cranberry 10

Fruit, citrus, group 10 5

Goat, fat 0.1

Goat, meat 0.1

Goat, meat byproducts 0.1

Grape 10

Hog, fat 0.2

Hog, meat 0.04

Hog, meat byproducts 0.04

Horse, fat 0.1

Horse, meat 0.1

Horse, meat byproducts 0.1

Kiwifruit 25

Milk 0.1

Nectarine 5

Nut, tree, group 14 0.1

Pea, dry, seed 0.5

Pea, field, hay 20

Pea, field, vines 10

Pea, succulent 1

Peach 10

Pear 10

Plum, prune, fresh 5

Potato 0.1

Sheep, fat 0.1

Sheep, meat 0.1

Sheep, meat byproducts 0.1

Sweet potato, roots 12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the 

insecticide phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorodithioate), including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of phosmet, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl 

phosphorodithioate), and its oxygen analog, N-(mercaptomethyl) phthalimide S-(O,O-dimethyl phosphorothioate, 

calculated as the stoichiometric equivalent of phosmet, in or on the commodity.

Commodity Parts per million

Crabapple 20

Pistachio 0.1

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 46538, Oct. 10, 1978, as amended at 45 FR 8981, Feb. 11, 1980; 48 FR 37213, Aug. 17, 1983; 52 FR 48539, Dec. 23, 1987; 

53 FR 657, Jan. 11, 1988; 53 FR 39090, Oct. 5, 1988; 63 FR 57075, Oct. 26, 1998; 67 FR 49616, July 31, 2002; 74 FR 46698, Sept.

11, 2009; 75 FR 60242, Sept. 29, 2010]

 Back to Top

§180.262 Ethoprop; tolerances for residues.

(a) General. Tolerances are established for residues of the nematocide and insecticide ethoprop, O-ethyl S,S-dipropyl 

phosphorodithioate, including its metabolites and degradates, in or on the commodities in the following table. Compliance 

with the tolerance levels specified in this paragraph is to be determined by measuring only ethoprop, O-ethyl S,S-dipropyl 

phosphorodithioate, in or on the commodity.

Commodity Parts per million 

Banana 0.02

Bean, lima 0.02

Bean, snap, succulent 0.02

Cabbage 0.02

Corn, field, forage 0.02

Corn, field, grain 0.02

Corn, field, stover 0.02

Corn, sweet, forage 0.02

Corn, sweet, kernel plus cob with husks removed 0.02

Corn, sweet, stover 0.02

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Cucumber 0.02

Hop, dried cones 0.02

Peppermint, tops 0.02

Pineapple1 0.02

Potato 0.02

Spearmint, tops 0.02

Sugarcane, cane 0.02

Sweet potato, roots 0.02

1

There are no U.S. registrations as of July 23, 2009, except for existing stocks bearing old labeling whose sale, 

distribution, and use is allowed, provided it is consistent with the terms of the cancellation order of July 9, 2009; i.e., the 

EPA will allow the technical registrant to continue to sell and distribute existing stocks of the amended registered product 

bearing old labeling for use on pineapple for 18 months (until January 9, 2011) and persons other than the registrant may 

continue to sell and/or use existing stocks of product bearing the old labeling until such stocks are exhausted, provided 

that such use is consistent with the terms of the previously approved labeling on, or that accompanied, the modified 

product.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 53004, Nov. 24, 1982, as amended at 48 FR 51485, Nov. 9, 1983; 52 FR 33237, Sept. 2, 1987; 53 FR 30053, Aug. 10, 1988; 

63 FR 57075, Oct. 26, 1998; 64 FR 39078, July 21, 1999; 66 FR 38955, July 26, 2001; 67 FR 49616, July 31, 2002; 73 FR 53731, 

Sept. 17, 2008; 73 FR 54961, Sept. 24, 2008; 74 FR 46373, Sept. 9, 2009; 75 FR 60242, Sept. 29, 2010]

 Back to Top

§180.263 Phosalone; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide phosalone, S-(6-chloro-3-(mercaptomethyl)-2-

benzoxazolinone) O,O-diethyl phosphorodithioate, in or on the following food commodities:

Commodity Parts per million Expiration/Revocation Date 

Apple1 10.0 9/30/13

Cherry1 15.0 9/30/13

Grape1 10.0 9/30/13

Peach1 15.0 9/30/13

Pear1 10.0 9/30/13

Plum, prune, fresh1 15.0 9/30/13

1

There are no U.S. registrations since 1992.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 46698, Sept. 11, 2009]

 Back to Top

§180.269 Aldicarb; tolerances for residues.

(a) General. Tolerances are established for combined residues of the insecticide and nematocide aldicarb (2-methyl2-(methylthio)propionaldehyde O-(methylcarbamoyl) oxime and its cholinesterase-inhibiting metabolites 2-methyl 

2-(methylsulfinyl) propionaldehyde O-(methylcarbamoyl) oxime and 2-methyl-2-(methylsulfonyl) propionaldehyde 

O-(methylcarbamoyl) oxime in or on the following food commodities: 

Commodity Parts per million 

Bean, dry, seed 0.1 

Beet, sugar, roots 0.05 

Beet, sugar, tops 1 

Citrus, dried pulp 0.6 

Coffee, bean, green 0.1 

Cotton, undelinted seed 0.1 

Cotton, hulls 0.3 

Grapefruit 0.3 

Lemon 0.3 

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Lime 0.3 

Orange, sweet 0.3 

Peanut 0.05 

Pecan 0.5 

Potato 1 

Sorghum, grain, bran 0.5 

Sorghum, grain, grain 0.2 

Sorghum, grain, stover 0.5 

Soybean 0.02 

Sugarcane, cane 0.02 

Sweet potato, roots 0.1

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33710, May 24, 2000, as amended at 69 FR 6567, Feb. 11, 2004; 73 FR 54961, Sept. 24, 2008]

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§180.272 Tribuphos; tolerances for residues.

(a) General. Tolerances are established for residues of the defoliant tribuphos (S,S,S-tributyl phosphorotrithioate) in 

or on food commodities as follows: 

Commodity Parts per million

Cattle, fat 0.15

Cattle, meat 0.02

Cattle, meat byproducts 0.02

Cotton, gin byproducts 40.0

Cotton, undelinted seed 4.0

Goat, fat 0.15

Goat, meat 0.02

Goat, meat byproducts 0.02

Hog, fat 0.15

Hog, meat 0.02

Hog, meat byproducts 0.02

Horse, fat 0.15

Horse, meat 0.02

Horse, meat byproducts 0.02

Milk 0.01

Sheep, fat 0.15

Sheep, meat 0.02

Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33698, May 24, 2000, as amended at 67 FR 49616, July 31, 2002; 72 FR 53460, Sept. 19, 2007]

 Back to Top

§180.274 Propanil; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for the combined residues of the herbicide propanil (3′, 4′

-dichloropropionanilide) and its metabolites convertible to 3, 4-dichloroaniline (3, 4-DCA) in or on the following food 

commodities:

Commodity Parts per million

Cattle, fat 0.10

Cattle, meat 0.05

Cattle, meat byproducts 1.0

Crayfish 0.05

Egg 0.30

Goat, fat 0.10

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Goat, meat 0.05

Goat, meat byproducts 1.0

Hog, fat 0.10

Hog, meat 0.05

Hog, meat byproducts 1.0

Horse, fat 0.10

Horse, meat 0.05

Horse, meat byproducts 1.0

Milk 0.05

Poultry, fat 0.05

Poultry, meat 0.10

Poultry, meat byproducts 0.50

Rice, bran 40

Rice, grain 10

Rice, hulls 30

Rice, straw 75

Sheep, fat 0.10

Sheep, meat 0.05

Sheep, meat byproducts 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34827, June 26, 1998, as amended at 72 FR 28888, May 23, 2007]

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§180.275 Chlorothalonil; tolerances for residues.

(a) General. (1) Tolerances are established for the fungicide chlorothalonil (tetrachloroisophthalonitrile) and its 

metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food commodities. 

Commodity Parts per million

Almond 0.05 

Almond, hulls 1.0 

Apricot 0.5

Asparagus 0.1 

Banana (NMT 0.05 ppm in edible pulp) 0.5

Bean, dry, seed 0.1

Bean, snap, succulent 5

Blueberry 1.0

Brassica, head and stem, subgroup 5A 5.0

Carrot, roots 1

Celery 15

Cherry, sweet 0.5

Cherry, tart 0.5

Cocoa bean, dried bean 0.05

Coffee, bean, green 0.20

Corn, sweet, kernel plus cob with husks removed 1

Cranberry 5.0

Ginseng 4.0

Horseradish 4.0

Lentil 0.10

Lychee 15

Mango 1.0 

Mushroom 1.0

Nectarine 0.5

Okra 6.0

Onion, bulb 0.5

Onion, green 5

Papaya 15

Parsnip, roots 1

Passionfruit 3

Pea, edible podded 5

Peach 0.5

Peanut 0.3

Pistachio 0.2 

Plum 0.2

Plum, prune 0.2

Potato 0.1

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Rhubarb 4.0

Soybean 0.2

Starfruit 3.0

Tomato 5

Vegetable, cucurbit, group 9 5.0

Vegetable, fruiting, group 8, except tomato 6.0

Yam, true 0.10

(2) Tolerances are established for the metabolite 4-hydroxy-2,5,6-trichloroisophthalonitrile in or on the following food 

commodities.

Commodity Parts per million 

Cattle, fat 0.1 

Cattle, kidney 0.5 

Cattle, meat byproducts, except kidney 0.05 

Cattle, meat 0.03 

Goat, fat 0.1 

Goat, kidney 0.5 

Goat, meat byproducts, except kidney 0.05 

Goat, meat 0.03 

Hog, fat 0.1 

Hog, kidney 0.5 

Hog, meat byproducts, except kidney 0.05 

Hog, meat 0.03 

Horse, fat 0.1 

Horse, kidney 0.5 

Horse, meat byproducts, except kidney 0.05 

Horse, meat 0.03 

Milk 0.1 

Sheep, fat 0.1 

Sheep, kidney 0.5 

Sheep, meat byproducts, except kidney 0.05 

Sheep, meat 0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for the combined residues of chlorothalonil and its metabolite in or on the following raw agricultural 

commodities:

Commodity Parts per million

Hazelnut 0.1

Peppermint, tops 2 

Persimmon 1.5

Spearmint, tops 2

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 56114, Oct. 21, 1977]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.275, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.276 Formetanate hydrochloride; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide formetanate hydrochloride, including its 

metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels 

specified in this paragraph is to be determined by measuring only formetanate hydrochloride, N,N-dimethylN'-[3-[(methylamino)carbonyl]oxy]phenyl]methanimidamide hydrochloride, in or on the commodity.

Commodity

Parts per

million Expiration/revocation date

Apple 0.50 12/31/13

Apple, wet pomace 1.5 12/31/13

Grapefruit 1.5 None

Lemon 0.60 None

Lime 0.03 None

Nectarine 0.40 None

Orange 1.5 None

Peach 0.40 12/31/13

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Pear 0.50 12/31/13

Tangelo 0.03 None

Tangerine 0.03 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 40815, July 11, 2012]

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§180.278 Phenmedipham; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide phenmedipham 

(3-methoxycarbonylaminophenyl-3′-methylcarbanilate) in or on the following food commodities:

Commodity Parts per million

Beet, garden, roots 0.2

Beet, garden, tops 0.2

Beet, sugar, dried pulp 0.5

Beet, sugar, molasses 0.2

Beet, sugar, roots 0.1

Beet, sugar, tops 0.1

Spinach 4.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007]

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§180.284 Zinc phosphide; tolerances for residues.

(a) General. Tolerances are established for residues of the phosphine resulting from the use of the rodenticide zinc 

phosphide in or on the raw agricultural commodities as follows:

Commodity Parts per million

Alfalfa, forage 0.2

Alfalfa, hay 0.2

Barley, grain 0.05

Barley, hay 0.2

Barley, straw 0.2

Bean, dry, seed 0.05

Beet, sugar, roots 0.05

Beet, sugar, tops 0.2

Grape 0.01

Grass, rangeland, forage 0.1 

Grass, rangeland, hay 0.1 

Potato 0.05

Sugarcane, cane 0.01

Timothy, hay 0.5

Timothy, forage 0.5

Wheat, forage 0.05

Wheat, grain 0.05

Wheat, hay 0.05

Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of phosphine resulting from the use of the rodenticide zinc phosphide in or on the following raw 

agricultural commodities as follows:

Commodity Parts per million

Artichoke, globe 0.01

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Beet, sugar, roots 0.04

Beet, sugar, tops 0.02

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 45182, Aug. 25, 1998, as amended at 63 FR 67799, Dec. 9, 1998; 64 FR 40772, July 28, 1999; 64 FR 61791, Nov. 15, 1999; 

65 FR 8874, Feb. 23, 2000; 65 FR 49941, Aug. 16, 2000; 65 FR 62634, Oct. 19, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 2247, 

Jan. 16, 2003; 68 FR 56195, Sept. 30, 2003; 70 FR 7046, Feb. 10, 2005; 74 FR 46373, Sept. 9, 2009; 76 FR 34885, June 15, 2011]

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§180.287 Amitraz; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for residues of the insecticide amitraz (N'-[2,4-dimethylphenyl]-N-

[[(2,4-dimethylphenyl)imino]methyl]]-N-methylmethanimidamide), including its metabolites and degradates, in or on the 

commodities in the following table. Compliance with the tolerance levels specified is to be determined by measuring 

amitraz residues convertible to 2,4-dimethylaniline, expressed as the stoichiometric equivalent of amitraz, in or on the 

following raw agricultural commodities:

Commodity Parts per million

Cattle, fat 0.1

Cattle, meat 0.02

Cattle, meat byproducts 0.2

Cotton, undelinted seed1 1.0

Hog, fat 0.1

Hog, kidney 0.1

Hog, liver 0.1

Hog, meat 0.05

Hog, meat byproducts 0.3

Honey 0.2 

Honeycomb 9 

Milk 0.03

Milk, fat 0.2

1

There are no U.S. registrations on cottonseed as of May 3, 2006.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[44 FR 70145, Dec. 6, 1979, as amended at 51 FR 16846, May 7, 1986; 52 FR 5767, Feb. 26, 1987; 57 FR 53568, Nov. 12, 1992; 

58 FR 14316, Mar. 17, 1993; 60 FR 12704, Mar. 8, 1995; 67 FR 49616, July 31, 2002; 72 FR 53454, Sept. 19, 2007; 74 FR 47456, 

Sept. 16, 2009; 78 FR 17133, Mar. 20, 2013]

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§180.288 2-(Thiocyanomethylthio)benzothiazole; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for residues of the fungicide 2-(thiocyanomethylthio)benzothiazole in or on 

the following food commodities:

Commodity Parts per million

Barley, grain 0.1(N)

Barley, straw 0.1(N)

Beet, sugar, roots 0.1(N)

Beet, sugar, tops 0.1(N)

Corn, field, forage 0.1(N)

Corn, field, grain 0.1 

Corn, field, stover 0.1 

Corn, pop, grain 0.1 

Corn, pop, stover 0.1 

Cotton, forage 0.1(N)

Cotton, undelinted seed 0.1(N)

Oat, forage 0.1(N)

Oat, grain 0.1(N)

Oat, hay 0.1(N)

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Oat, straw 0.1(N)

Rice, grain 0.1(N)

Rice, straw 0.1(N)

Safflower, seed 0.1(N)

Sorghum, grain, forage 0.1(N)

Sorghum, grain, grain 0.1(N)

Sorghum, grain, stover 0.1(N)

Wheat, forage 0.1(N)

Wheat, grain 0.1(N)

Wheat, hay 0.1(N)

Wheat, straw 0.1(N)

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39440, July 1, 2003, as amended at 74 FR 46374, Sept. 9, 2009]

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§180.289 Methanearsonic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide methanearsonic acid, including its metabolites 

and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in 

this paragraph is to be determined by measuring only methanearsonic acid, from application of the disodium and 

monosodium salts of methanearsonic acid, calculated as the stoichiometric equivalent of As2O3, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date

Cotton, undelinted seed 0.7 None

Cotton, hulls 0.9 None

Fruit, citrus 0.35 12/31/12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 77 FR 59126, Sept. 26, 2012]

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§180.291 Pentachloronitrobenzene; tolerance for residues.

(a) General. Tolerances are established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) 

and its metabolites pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

Commodity Parts per million

Bean 0.1

Brassica, head and stem, subgroup 5A 0.1

Cotton, undelinted seed 0.1

Garlic, bulb 0.1

Peanut 1.0

Potato 0.1

Soybean, forage 0.02

Soybean, hay 0.02

Soybean, seed 0.02

Vegetable, fruiting, group 8 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are 

established for the combined residues of the fungicide pentachloronitrobenzene (PCNB) and its metabolites 

pentachloroaniline (PCA), and pentachlorothioanisole (PCTA), in or on the following food commodities:

Commodity Parts per million

Collards 0.2

Kale 0.2

Mustard, greens 0.2

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(d) Indirect or inadvertent residues. [Reserved]

[74 FR 47456, Sept. 16, 2009]

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§180.292 Picloram; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide picloram, 4-amino-3,5,6-trichloropicolinic acid, 

including its metabolites and degradates, in or on the commodities in the following table from its application in the acid 

form or in the form of its salts. Compliance with the tolerance levels specified in this paragraph is to be determined by 

measuring only picloram, 4-amino-3,5,6-trichloropicolinic acid, in or on the commodity.

Commodity Parts per million

Barley, grain 0.5

Barley, pearled barley 3.0

Barley, straw 1.0

Cattle, fat 0.4

Cattle, meat 0.4

Cattle, meat byproducts 15

Egg 0.05

Goat, fat 0.4

Goat, meat 0.4

Goat, meat byproducts 15

Grain, aspirated fractions 4.0

Grass, forage 400

Grass, hay 225

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.4

Horse, meat 0.4

Horse, meat byproducts 15

Milk 0.25

Oat, forage 1.0

Oat, grain 0.5

Oat, groats/rolled oats 3.0

Oat, straw 1.0

Poultry, fat 0.05

Poultry, meat 0.05

Poultry, meat byproducts 0.05

Sheep, fat 0.4

Sheep, meat 0.4

Sheep, meat byproducts 15

Wheat, bran 3.0

Wheat, forage 1.0

Wheat, germ 3.0

Wheat, grain 0.5

Wheat, middlings 3.0

Wheat, shorts 3.0

Wheat, straw 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[41 FR 19221, May 11, 1976, as amended at 47 FR 53005, Nov. 24, 1982; 64 FR 425, Jan. 5, 1999; 64 FR 39082, July 21, 1999; 72 

FR 41930, Aug. 1, 2007; 75 FR 60243, Sept. 29, 2010]

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§180.293 Endothall; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. (1) Tolerances are established for the residues of endothall, including its metabolites and degradates, in 

or on the commodities in the table, below. Compliance with the tolerance levels specified, below, is to be determined by 

measuring only endothall (7-oxabicylco [2.2.1] heptanes-2,3-dicarboxylic acid) and its mono-methyl ester.

Commodity Parts per million

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Apple 0.05

Apple, wet pomace 0.15

Cotton, undelinted seed 0.1

Fish 0.1

Hop, dried cones 0.1

Potato 0.1

Rice, grain 0.05

Rice, straw 0.05

(2) An interim tolerance of 0.2 parts per million is established for residues of the herbicide endothall (7 - oxabicyclo

[2.2.1] heptane-2,3-dicarboxylic acid) in water, potable from use of its potassium, sodium, di-N, N-dimethylalkylamine, and 

mono-N-N,-dimethylalkylamine salts as algicides or herbicides to control aquatic plants in canals, lakes, ponds, and other 

potential sources of water, potable.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent combined residues of 

the herbicide, endothall (7 - oxabicyclo[2.2.1] heptane-2,3-dicarboxylic acid) in potable water from use of its potassium, 

sodium, di-N, N -dimethylalkylamine, and mono- N-N, -dimethylalkylamine salts as algicides or herbicides to control 

aquatic plants in canals, lakes, ponds, and other potable water sources that may lead to endothall residues in or on the 

following commodities:

Commodity Parts per million

Almond, hulls 15.0

Animal feed, nongrass, group 18, forage 4.0

Animal feed, nongrass, group 18, hay 10

Apple, wet pomace 0.15

Beet, sugar, molasses 1.5

Brassica, head and stem subgroup 5A 0.1

Brassica, leafy, subgroup 5B 2.0

Bushberry subgroup 13-07B 0.6

Caneberry subgroup 13-07A 0.6

Cattle, fat 0.01

Cattle, kidney 0.20

Cattle, liver 0.10

Cattle, meat 0.03

Corn, field, grain 0.07

Corn, pop, grain 0.07

Corn, sweet, kernel plus cob with husks removed 0.3

Citrus, dried pulp 0.1

Egg 0.05

Feed commodities not otherwise listed 10.0

Food commodities not otherwise listed 5.0

Fruit, citrus group 10 0.05

Fruit, pome, group 11 0.05

Fruit, stone, group 12 0.3

Goat, fat 0.005

Goat, kidney 0.15

Goat, liver 0.05

Goat, meat 0.015

Grain, aspirated fractions 35.0

Grain cereal, forage, fodder and straw, group 16 10.0

Grain, cereal, group 15, except corn 4.0

Grape 1.0

Grape, raisin 5.0

Grass, forage, fodder, and hay group 17, forage 3.5

Grass, forage, fodder, and hay group 17, hay 18.0

Herb and spice, group 19 5.0

Hog, fat 0.005

Hog, kidney 0.10

Hog, liver 0.05

Hog, meat 0.01

Milk 0.03

Nut, tree, group 14 0.05

Okra 0.05

Pea and bean, dried shelled, subgroup 6C 0.2

Pea and bean, succulent shelled, subgroup 6B 2.0

Peppermint, tops 5.0

Pistachio 0.05

Poultry, fat 0.015

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Poultry, liver 0.05

Poultry, meat 0.015

Poultry, meat byproducts 0.20

Rice, hulls 8.0

Sheep, fat 0.005

Sheep, kidney 0.15

Sheep, liver 0.05

Sheep, meat 0.015

Soybean, hulls 0.5

Soybean, seed 0.2

Spearmint, tops 5.0

Tomato, paste 0.1

Tomato, puree 0.1

Vegetable, bulb, group 3-07 0.5

Vegetable, cucurbit, group 9 1.5

Vegetable, foliage of legume, group 7 4.0

Vegetable, fruiting, group 8 0.05

Vegetable, leafy, except brassica, group 4 2.0

Vegetable, leaves of root and tuber, group 2 3.0

Vegetable, legume, edible, podded, subgroup 6A 2.0

Vegetable, root and tuber, group 1 1.0

Wheat, milled byproducts 5.0

[41 FR 23717, June 11, 1976, as amended at 51 FR 4498, Feb. 5, 1986; 62 FR 49931, Sept. 24, 1997; 63 FR 42249, Aug. 7, 1998; 

67 FR 35048, May 17, 2002; 71 FR 47106, Aug. 16, 2006; 71 FR 74816, Dec. 13, 2006; 72 FR 52018, Sept. 12, 2007; 74 FR 67097, 

Dec. 18, 2009; 78 FR 76566, Dec. 18, 2013]

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§180.297 N-1-Naphthyl phthalamic acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide N-1-naphthyl phthalamic acid from application of 

its sodium salt in or on the following raw agricultural commodities:

Commodity Parts per million

Cantaloupe 0.1(N)

Cucumber 0.1(N)

Muskmelon 0.1(N)

Watermelon 0.1(N)

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 32306, May 16, 1980, as amended at 63 FR 57075, Oct. 26, 1998]

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§180.298 Methidathion; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide methidathion, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] 

O,O-dimethyl phosphorodithioate, in or on the commodity.

Commodity Parts per million Expiration/revocation date

Almond, hulls 6.0 12/31/16

Artichoke, globe 0.05 12/31/16

Citrus, oil 420.0 12/31/16

Cotton, undelinted seed 0.2 12/31/16

Fruit, citrus, group 10, except tangerine 4.0 12/31/16

Fruit, pome, group 11 0.05 12/31/16

Fruit, stone, group 12 0.05 12/31/16

Mango 0.05 12/31/16

Nut, tree, group 14 0.05 12/31/16

Olive 0.05 12/31/16

Safflower, seed 0.5 12/31/16

Sorghum, forage, forage 2.0 12/31/16

Sorghum, grain, forage 2.0 12/31/16

Sorghum, grain, grain 0.2 12/31/16

Sorghum, grain, stover 2.0 12/31/16

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Sunflower, seed 0.5 12/31/16

Tangerine 6.0 12/31/16

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the insecticide methidathion, including its metabolites and degradates, in or on the commodities 

in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by 

measuring only methidathion, S-[(5-methoxy-2-oxo-1,3,4-thiadiazol-3(2H)-yl)methyl] O,O-dimethyl phosphorodithioate, in 

or on the commodity.

Commodity

Parts per

million

Expiration/

revocation

date

Kiwifruit 0.1 12/31/16

Longan 0.1 12/31/16

Starfruit 0.1 12/31/16

Sugar apple 0.2 12/31/16

(d) Indirect or inadvertent residues. [Reserved]

[43 FR 44845, Sept. 29, 1978]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.298, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.299 Dicrotophos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide dicrotophos, dimethyl phosphate of 

3-hydroxy-N,N-dimethyl-cis-crotonamide, in or on the following food commodities:

Commodity Parts per million

Cotton, gin byproducts 2.0

Cotton, undelinted seed 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52613, Sept. 10, 2008]

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§180.300 Ethephon; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for residues of the plant regulator ethephon [(2-chloroethyl) phosphonic acid] 

in or on food commodities as follows: 

Commodity Parts per million

Apple 5.0

Apple, juice 10.0

Barley, bran 5.0

Barley, grain 2.0

Barley, straw 10.0

Blackberry 30.0

Blueberry 20.0

Cantaloupe 2.0

Cattle, fat 0.02

Cattle, kidney 1.0

Cattle, meat 0.02

Cattle, meat byproducts, except kidney 0.2

Cherry 10.0

Coffee, bean, green 0.5

Cotton, gin byproducts 180.0

Cotton, undelinted seed 6.0

Cucumber 0.1

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Egg 0.002

Goat, fat 0.02

Goat, kidney 1.0

Goat, meat 0.02

Goat, meat byproducts, except kidney 0.2

Grape 2.0

Grape, raisin 12.0

Hazelnut 0.80

Hog, fat 0.02

Hog, kidney 1.0

Hog, meat 0.02

Hog, meat byproducts, except kidney 0.2

Horse, fat 0.02

Horse, kidney 1.0

Horse, meat 0.02

Horse, meat byproducts, except kidney 0.2

Milk 0.01

Nut, macadamia 0.5

Pepper 30.0

Pineapple 2.0

Poultry, fat 0.02

Poultry, liver 0.05

Poultry, meat 0.01

Poultry, meat byproducts, except liver 0.01

Sheep, fat 0.02

Sheep, kidney 1.0

Sheep, meat 0.02

Sheep, meat byproducts, except kidney 0.2

Sugarcane, molasses 1.5

Tomato 2.0

Walnut 0.5

Wheat, bran 5.0

Wheat, germ 5.0

Wheat, grain 2.0

Wheat, middlings 5.0

Wheat, shorts 5.0

Wheat, straw 10.0

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(m), of 0.1 part 

per million is established for residues of the plant regulator ethephon [(2-chloroethyl)phosphonic acid] in or on the food 

commodity sugarcane. 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33710, May 24, 2000, as amended at 72 FR 53455, Sept. 19, 2007; 75 FR 56015, Sept. 15, 2010]

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§180.301 Carboxin; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for the combined residues of the fungicide carboxin (5,6-dihydro-2-

methyl-1,4-oxathiin-3-carboxanilide) and its metabolites determined as aniline and expressed as parent compound, in or 

on food commodities as follows:

Commodity Parts per million

Barley, grain 0.2

Barley, straw 0.2

Bean, dry, seed 0.2

Bean, succulent 0.2

Canola, seed 0.03

Cattle, fat 0.05

Cattle, meat byproducts 0.1

Cattle, meat 0.05

Corn, field, forage 0.2

Corn, field, grain 0.2

Corn, field, stover 0.2

Corn, pop, grain 0.2

Corn, pop, stover 0.2

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Corn, sweet, forage 0.2

Corn, sweet, kernel plus cob with husks removed 0.2

Corn, sweet, stover 0.2

Cotton, undelinted seed 0.2

Egg 0.05

Goat, fat 0.05

Goat, meat byproducts 0.1

Goat, meat 0.05

Hog, fat 0.05

Hog, meat byproducts 0.1

Hog, meat 0.05

Horse, fat 0.05

Horse, meat byproducts 0.1

Horse, meat 0.05

Milk 0.05

Oat, forage 0.5

Oat, grain 0.2

Oat, straw 0.2

Onion, bulb 0.2

Peanut 0.2

Peanut, hay 0.2

Poultry, fat 0.1

Poultry, meat byproducts 0.1

Poultry, meat 0.1

Rice, grain 0.2

Rice, straw 0.2

Safflower, seed 0.2

Sheep, fat 0.05

Sheep, meat byproducts 0.1

Sheep, meat 0.05

Soybean, seed 0.2

Wheat, forage 0.5

Wheat, grain 0.2

Wheat, straw 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[47 FR 55222, Dec. 8, 1982, as amended at 50 FR 81, Jan. 2, 1985; 62 FR 4915, Feb. 3, 1997; 63 FR 4586, Jan. 30, 1998; 64 FR 

11801, Mar. 10, 1999; 66 FR 9773, Feb. 12, 2001; 66 FR 64773, Dec. 14, 2001; 67 FR 40218, June 12, 2002; 67 FR 72853, Dec. 9, 

2002; 71 FR 56383, Sept. 27, 2006]

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§180.303 Oxamyl; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for the combined residues of the insecticide oxamyl, methyl 

N,N-dimethyl-N-[(methylcarbamoyl)-oxy]-1-thiooxamimidate, and its oxime metabolite methyl N,N-dimethyl-N-hydroxy-1-

thiooxamimidate calculated as oxamyl in or on the following food commodities:

Commodity Parts per million 

Apple 2 

Banana 0.3 

Cantaloupe 2.0 

Carrot 0.1 

Celery 10.0 

Cotton, undelinted seed 0.2 

Cucumber 2.0 

Eggplant 2.0 

Fruit, citrus, group 10 3 

Garlic, bulb 0.2 

Melon, honeydew 2.0 

Onion, bulb 0.2 

Peanut 0.05 

Peanut, hay 2.0 

Pear 2.0 

Peppermint, tops 10.0 

Pepper, bell 2.0 

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Pepper, nonbell 5.0 

Pineapple 1 

Pineapple, process residue 2.0 

Pumpkin 2.0 

Soybean, seed 0.1 

Spearmint, tops 10.0 

Squash, summer 2.0 

Squash, winter 2.0 

Tomato 2 

Vegetable, tuberous and corm, subgroup 1C 0.1 

Watermelon 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008]

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§180.304 Oryzalin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, 

in or on the following raw agricultural commodities:

Commodity Parts per million

Almond, hulls 0.05

Avocado 0.05

Berry group 13 0.05

Cranberry 0.05

Fig 0.05

Fruit, citrus, group 10 0.05

Fruit, pome, group 11 0.05

Fruit, stone, group 12 0.05

Grape 0.05

Kiwifruit 0.05

Nut, tree, group 14 0.05

Olive 0.05

Pistachio 0.05

Pomegranate 0.05

Strawberry 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of oryzalin, 3,5-dinitro-N4,N4-dipropylsulfanilamide, in or on the following raw agricultural 

commodities:

Commodity Parts per million

Guava 0.05

Papaya 0.05

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 54434, Sept. 15, 2006, as amended at 76 FR 34885, June 15, 2011]

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§180.311 Cacodylic acid; tolerances for residues.

(a) General. A tolerance is established for residues of the defoliant cacodylic acid, dimethylarsinic acid, including its 

metabolites and degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in 

this paragraph is to be determined by measuring only those cacodylic acid residues convertible to As2O3, expressed as 

the stoichiometric equivalent of cacodylic acid, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date 

Cotton, undelinted seed 2.8 1/1/12

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 6567, Feb. 11, 2004, as amended at 75 FR 60243, Sept. 29, 2010]

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§180.314 Triallate; tolerances for residues.

(a) General. Tolerances are established for residues of triallate, S-2,3,4-trichloroallyl diisopropylthiocarbamate and its 

metabolite 2,3,3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodity:

Commodity Parts per million

Bermudagrass, hay 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration, as defined in 180.1(l),are 

established for residues of the herbicide (S-2, 3, 4-trichloroallyl diisopropylthiocarbamate) and its metabolite 2, 3, 

3-trichloroprop-2-enesulfonic acid (TCPSA) in or on the following food commodities:

Commodity Parts per million

Barley, grain 0.05

Barley, hay 1.0

Barley, straw 0.3

Beet, sugar, dried pulp 0.2

Beet, sugar, roots 0.1

Beet, sugar, tops 0.5

Pea, dry 0.2

Pea, field, hay 1.0

Pea, field, vines 0.5

Pea, succulent 0.2

Wheat, forage 0.5

Wheat, grain 0.05

Wheat, hay 1.0

Wheat, straw 1.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008; 73 FR 53738, Sept. 17, 2008; 74 FR 29963, June 24, 

2009]

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§180.315 Methamidophos; tolerances for residues.

(a) General. Tolerances are established for residues of methamidophos, O,S-dimethyl phosphoramidothioate, 

including its metabolites and degradates, in or on the commodities in the following table as a result of the application of 

methamidophos. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only 

methamidophos, O,S-dimethyl phosphoramidothioate, in or on the commodity.

Commodity Parts per million Expiration/Revocation Date 

Broccoli1 1.0 12/31/12

Cabbage2 1.0 12/31/12

Cotton, undelinted seed 0.1 12/31/13

Potato 0.1 12/31/13

1

There are no U.S. registrations since 1989.

2

There are no U.S. registrations since 2001.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of 

methamidophos, O,S-dimethyl phosphoramidothioate, including its metabolites and degradates, in or on the commodity in 

the following table as a result of the application of methamidophos. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only methamidophos, O,S-dimethyl phosphoramidothioate, in or on the 

commodity.

Commodity Parts per million Expiration/Revocation Date 

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Tomato 2.0 12/31/13

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60243, Sept. 29, 2010]

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§180.316 Pyrazon; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide pyrazon (5-amino-4-chloro-2-phenyl-3

(2H)-pyridazinone) and its metabolites (calculated as pyrazon) in or on the following food commodities:

Commodity Parts per million

Beet, garden, roots 0.9

Beet, garden, tops 7.0

Beet, sugar, molasses 1.5

Beet, sugar, roots 0.2

Beet, sugar, tops 3.0

Cattle, fat 0.10

Cattle, liver 0.15

Cattle, meat 0.10

Cattle, meat byproducts, except liver 0.10

Goat, fat 0.10

Goat, liver 0.15

Goat, meat 0.10

Goat, meat byproducts, except liver 0.10

Horse, fat 0.10

Horse, liver 0.15

Horse, meat 0.10

Horse, meat byproducts, except liver 0.10

Milk 0.02

Sheep, fat 0.10

Sheep, liver 0.15

Sheep, meat 0.10

Sheep, meat byproducts, except liver 0.10

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. Tolerances are established for combined residues of the herbicide pyrazon, 

5-amino-4-chloro-2-phenyl-3(2H)-pyridazinone, and its metabolites (calculated as pyrazon), in or on the following food 

commodities:

Commodity Parts per million

Corn, field, forage 0.5

Corn, field, stover 0.5

Soybean, forage 0.5

Soybean, hay 0.5

Wheat, forage 0.3

Wheat, hay 0.2

Wheat, straw 0.1

[68 FR 39441, July 1, 2003, as amended at 73 FR 52614, Sept. 10, 2008]

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§180.317 Propyzamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide propyzamide, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, 

expressed as the stoichiometric equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on 

the commodity.

Commodity Parts per million

Alfalfa, seed 10.0

Animal feed, nongrass, group 18 10.0

Apple 0.1

Artichoke, globe 0.01

Blackberry 0.05

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Blueberry 0.05

Boysenberry 0.05

Cattle, fat 0.2

Cattle, kidney 0.4

Cattle, liver 0.4

Cattle, meat 0.02

Cattle, meat byproducts, except kidney and liver 0.02

Egg 0.02

Endive 1.0

Fruit, stone, group 12 0.1

Goat, fat 0.2

Goat, kidney 0.4

Goat, liver 0.4

Goat, meat 0.02

Goat, meat byproducts, except kidney and liver 0.02

Grape 0.1

Hog, fat 0.2

Hog, kidney 0.4

Hog, liver 0.4

Hog, meat 0.02

Hog, meat byproducts, except kidney and liver 0.02

Horse, fat 0.2

Horse, kidney 0.4

Horse, liver 0.4

Horse, meat 0.02

Horse, meat byproducts, except kidney and liver 0.02

Lettuce, head 1.0

Milk 0.02

Pear 0.1

Poultry, fat 0.02

Poultry, liver 0.2

Poultry, meat 0.02

Poultry, meat byproducts, except liver 0.02

Radicchio 2.0

Raspberry 0.05

Sheep, fat 0.2

Sheep, kidney 0.4

Sheep, liver 0.4

Sheep, meat 0.02

Sheep, meat byproducts, except kidney and liver 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the herbicide propyzamide, including its metabolites and degradates, in or on the commodities 

in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by 

measuring only those propyzamide residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric 

equivalent of propyzamide, 3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity Parts per million

Pea, field, seed 0.05

Rhubarb 0.1

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide 

propyzamide, including its metabolites and degradates, in or on the commodities in the table in this paragraph. 

Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only those propyzamide 

residues convertible to methyl 3,5-dichlorobenzoate, expressed as the stoichiometric equivalent of propyzamide, 

3,5-dichloro-N-(1,1-dimethyl-2-propynyl)benzamide, in or on the commodity.

Commodity Parts per million

Grain, cereal, forage, group 16 0.6

Grain, cereal, hay, group 16 0.2

Grain, cereal, straw, group 16 0.3

[72 FR 52018, Sept. 12, 2007, as amended at 76 FR 23493, Apr. 27, 2011]

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§180.318 4-(2-Methyl-4-chlorophenoxy) butyric acid; tolerance for residues.

(a) General. (1) A tolerance is established for the herbicide 4-(2-methyl-4-chlorophenoxy) butyric acid in or on the 

following food commodity:

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Commodity Parts per million

Pea 0.1(N)

(2) Tolerances are established for the combined residues, free and conjugated, of the herbicide MCPB, 4-(4-chloro-2-

methylphenoxy)butanoic acid, and its metabolite MCPA, (4-chloro-2-methylphenoxy)acetic acid, in or on the following food 

commodities:

Commodity Parts per million

Peppermint, tops 0.20

Spearmint, tops 0.20

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 73 FR 66785, Nov. 12, 2008]

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§180.319 Interim tolerances.

(a) General. While petitions for tolerances for negligible residues are pending and until action is completed on these 

petitions, interim tolerances are established for residues of the listed pesticide chemicals in or on the following raw 

agricultural commodities:

Substances Uses Tolerance in parts per million

Raw

agricultural

commodity

Expiration/

revocation

date

Endothall (7-oxabicyclo-(2,2,1)heptane 2,3-dicarboxylic acid Herbicide 0.2 Beet, sugar None

Methyl parathion Herbicide 0.5 Rye 12/31/13

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 59126, Sept. 26, 2012, as amended at 79 FR 27502, May 14, 2014]

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§180.324 Bromoxynil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide bromoxynil, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be determined by 

measuring only bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, resulting from application of its octanoic and/or heptanoic 

acid ester, in or on the commodities.

Commodity Parts per million

Alfalfa, forage 0.1

Alfalfa, hay 0.5

Barley, grain 0.05

Barley, hay 9.0

Barley, straw 4.0

Corn, field, forage 0.3

Corn, field, grain 0.05

Corn, field, stover 0.2

Corn, pop, grain 0.05

Corn, pop, stover 0.2

Flax, seed 0.1

Garlic 0.1

Grain, aspirated fractions 1.2

Grass, forage 18

Grass, hay 5.0

Oat, forage 0.3

Oat, grain 0.05

Oat, hay 9.0

Oat, straw 4.0

Onion, bulb 0.1

Peppermint, hay 0.1

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Rye, forage 1.0

Rye, grain 0.05

Rye, straw 2.0

Sorghum, grain, forage 0.8

Sorghum, grain, grain 0.2

Sorghum, grain, stover 0.2

Spearmint, hay 0.1

Wheat, forage 1.0

Wheat, grain 0.05

Wheat, hay 4.0

Wheat, straw 2.0

(2) Tolerances are established for residues of the herbicide bromoxynil, 3,5-dibromo-4-hydroxybenzonitrile, including 

its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels is to be 

determined by measuring only bromoxynil and its metabolite, 3,5-dibromo-4-hydroxybenzoic acid (DBHA), resulting from 

application of its octanoic and/or heptanoic acid ester, in or on the commodities.

Commodity Parts per million

Cattle, fat 1 

Cattle, meat byproducts 3.5 

Cattle, meat 0.5 

Cotton, gin byproducts 7.0 

Cotton, hulls 5.0 

Cotton, undelinted seed 1.5 

Egg 0.05 

Goat, fat 1 

Goat, meat byproducts 3.5 

Goat, meat 0.5 

Hog, fat 1 

Hog, meat byproducts 3.5 

Hog, meat 0.5 

Horse, fat 1 

Horse, meat byproducts 3.5 

Horse, meat 0.5 

Milk 0.4

Poultry, fat 0.05 

Poultry, meat byproducts 0.3 

Poultry, meat 0.05 

Sheep, fat 1 

Sheep, meat byproducts 3.5 

Sheep, meat 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 33023, June 18, 1997, as amended at 63 FR 26480, May 13, 1998; 66 FR 47402, Sept. 12, 2001; 70 FR 7046, Feb. 10, 

2005; 72 FR 35666, June 29, 2007; 72 FR 41930, Aug. 1, 2007; 76 FR 31491, June 1, 2011]

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§180.328 Napropamide; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide napropamide, N,N-diethyl-2-(1-napthalenyloxy) 

propionamide, in or on the following food commodities:

Commodity Parts per million Expiration/revocation date

Almond, hulls 0.1 None

Asparagus 0.1 None

Basil 0.1 None

Berry group 13 0.1 None

Coffee, green bean 0.1 None

Cranberry 0.1 None

Grape 0.1 None

Kiwifruit 0.1 None

Marjoram 0.1 None

Nut, tree, group 14 0.1 None

Peppermint, tops 0.1 None

Persimmon 0.1 None

Rhubarb 0.1 None

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Rosemary 0.1 None

Savory, summer 0.1 None

Savory, winter 0.1 None

Spearmint, tops 0.1 None

Strawberry 0.1 None

Sweet potato, roots 0.1 None

Vegetable, brassica, leafy, group 5 0.1 None

Vegetable, fruiting, group 8 0.1 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 52614, Sept. 10, 2008, as amended at 76 FR 34885, June 15, 2011]

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§180.330 S-(2-(Ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl 

(S-(2-(ethylsulfinyl)ethyl) O,O-dimethyl phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the 

following food commodities:

Commodity Parts per million

Alfalfa, forage 5.0

Alfalfa, hay 11.0

Bean, lima 0.2

Beet, sugar, roots 0.3

Beet, sugar, tops 0.5

Broccoli 1.0

Brussels sprouts 1.0

Cabbage 2.0

Cauliflower 1.0

Clover, forage 5.0

Clover, hay 10.0

Corn, sweet, forage 1.0

Corn, sweet, kernel plus cob with husks removed 0.5

Corn, sweet, stover 3.0

Cotton, undelinted seed 0.02

Cucumber 1.0

Eggplant 1.0

Grapefruit 1.0

Hazelnut 0.05

Lemon 1.0

Lettuce, head 2.0

Melon 0.2

Onion, bulb 0.05

Orange 1.0

Pepper 0.75

Peppermint, tops 12.5

Pumpkin 0.2

Safflower, seed 1.0

Sorghum, forage, forage 2.0

Sorghum, grain, forage 2.0

Sorghum, grain, grain 0.75

Spearmint, tops 12.5

Squash, summer 1.0

Squash, winter 0.3

Strawberry 2.0

Walnut 0.05

(2) Tolerances are established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)

ethyl) O,O-dimethyl phosphorothioate) and its cholinesterase-inhibiting metabolites in or on the following food 

commodities:

Commodity Parts per million

Cattle, fat 0.01

Cattle, meat 0.01

Cattle, meat byproducts 0.01

Egg 0.01

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Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.01

Hog, fat 0.01

Hog, meat 0.01

Hog, meat byproducts 0.01

Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.01

Milk 0.01

Poultry, fat 0.01

Poultry, meat 0.01

Poultry, meat byproducts 0.01

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations, as defined in §180.1(l), are 

established for the combined residues of the insecticide oxydemeton-methyl (S-(2-(ethylsulfinyl)-ethyl) O,O-dimethyl 

phosphorothioate) and its metabolite oxydemeton-methyl sulfone in or on the following food commodities:

Commodity Parts per million

Broccoli raab 2.0

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 54578, Sept. 26, 2007]

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§180.331 4-(2,4-Dichlorophenoxy) butyric acid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide 4-(2,4-dichlorophenoxy) butyric acid (2,4-DB), 

both free and conjugated, determined as the acid, in or on food commodities, as follows:

Commodity Parts per million 

Alfalfa, forage 0.7 

Alfalfa, hay 2.0 

Cattle, meat byproducts 0.05 

Clover, forage 0.2 

Clover, hay 0.2 

Goat, meat byproducts 0.05 

Hog, meat byproducts 0.05 

Horse, meat byproducts 0.05 

Peanut 0.2 

Peppermint, tops 0.2 

Sheep, meat byproducts 0.05 

Soybean, forage 0.7 

Soybean, hay 2.0 

Soybean, seed 0.5 

Spearmint, tops 0.2 

Trefoil, forage 0.7 

Trefoil, hay 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008, as amended at 74 FR 46374, Sept. 9, 2009]

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§180.332 Metribuzin; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide metribuzin (4-amino-6-(1,1-dimethylethyl)-3-(methylthio)-;1,2,4-triazin-5(4H)-one) and its triazinone metabolites in or on food commodities: 

Commodity Parts per million 

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Alfalfa, forage 2.0 

Alfalfa, hay 7.0 

Asparagus 0.1 

Barley, grain 0.75 

Barley, hay 7.0 

Barley, pearled barley 3.0 

Barley, straw 1.0 

Carrot, roots 0.3 

Cattle, fat 0.7 

Cattle, meat 0.7 

Cattle, meat byproducts 0.7 

Corn, field, forage 0.1 

Corn, field, grain 0.05 

Corn, field, stover 0.1 

Corn, pop, grain 0.05 

Corn, sweet, forage 0.1 

Corn, sweet, kernel plus cob with husks removed 0.05 

Corn, sweet, stover 0.1 

Egg 0.01 

Goat, fat 0.7 

Goat, meat 0.7 

Goat, meat byproducts 0.7 

Grass, forage 2.0 

Grass, hay 7.0 

Hog, fat 0.7 

Hog, meat 0.7 

Hog, meat byproducts 0.7 

Horse, fat 0.7 

Horse, meat 0.7 

Horse, meat byproducts 0.7 

Lentil 0.05 

Milk 0.05 

Pea, dry, seed 0.05 

Pea, field, hay 4.0 

Pea, field, vines 0.5 

Pea, succulent 0.1 

Potato 0.6 

Potato, chips 3.0 

Potato, processed potato waste 3.0 

Poultry, fat 0.7 

Poultry, meat 0.7 

Poultry, meat byproducts 0.7 

Sainfoin, forage 2.0 

Sainfoin, hay 7.0 

Sheep, fat 0.7 

Sheep, meat 0.7 

Sheep, meat byproducts 0.7 

Soybean, seed 0.3 

Soybean, forage 4.0 

Soybean, hay 4.0 

Sugarcane, cane 0.1 

Sugarcane, molasses 2.0 

Tomato 0.1 

Wheat, bran 3.0 

Wheat, forage 2.0 

Wheat, germ 3.0 

Wheat, grain 0.75 

Wheat, hay 7.0 

Wheat, middlings 3.0 

Wheat, shorts 3.0 

Wheat, straw 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 62913, Dec. 14, 1977, as amended at 43 FR 41396, Sept. 18, 1978; 44 FR 26744, May 7, 1979; 44 FR 45387, Aug. 2, 1979; 

52 FR 23654, June 24, 1987; 55 FR 26440, June 28, 1990; 62 FR 66024, 66025, Dec. 17, 1997; 65 FR 33698, May 24, 2000; 66 FR 

63198, Dec. 5, 2001; 67 FR 49617, July 31, 2002]

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§180.337 Oxytetracycline; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide/bactericide oxytetracycline, including its 

metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels 

specified in this paragraph is to be determined by measuring only oxytetracycline, (4S,4aR,5S,5aR,6S,12aS)

-4-(dimethylamino)-1,4,4a,5,5a,6,11,12a-octahydro-3,5,6,10,12,12a-hexahydroxy-6-methyl-1,11-dioxo-2-

naphthacenecarboxamide, in or on the commodity.

Commodity Parts per million

Apple 0.35

Peach 0.35

Pear 0.35

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23493, Apr. 27, 2011]

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§180.339 MCPA; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic 

acid), both free and conjugated, resulting from the direct application of MCPA or its sodium or dimethylamine salts, or its 

2-ethylhexyl ester in or on the following food commodities:

Commodity Parts per million

Alfalfa, forage 0.5

Alfalfa, hay 2.0

Barley, grain 1.0

Barley, hay 40

Barley, straw 25

Clover, forage 0.5

Clover, hay 2.0

Flax, seed 0.1

Grain, aspirated fractions 3.0

Grass, forage 300

Grass, hay 20

Lespedeza, forage 0.5

Lespedeza, hay 2.0

Oat, forage 20

Oat, grain 1.0

Oat, hay 115

Oat, straw 25

Pea, dry 0.1

Pea, field, hay 0.1

Pea, succulent 0.1

Pea, field, vines 0.1

Rye, forage 20

Rye, grain 1.0

Rye, straw 25

Trefoil, forage 0.5

Trefoil, hay 2.0

Vetch, forage 0.5

Vetch, hay 2.0

Wheat, forage 20

Wheat, grain 1.0

Wheat, hay 115

Wheat, straw 25

(2) Tolerances are established for residues of the herbicide MCPA ((4-chloro-2-methylphenoxy)acetic acid) resulting 

from the direct application of MCPA or its sodium or dimethylamine salts, or its 2-ethylhexyl ester in or on the following 

food commodities:

Commodity Parts per million

Cattle, fat 0.1

Cattle, meat 0.1

Cattle, meat byproducts 0.1

Goat, fat 0.1

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Goat, meat 0.1

Goat, meat byproducts 0.1

Hog, fat 0.1

Hog, meat 0.1

Hog, meat byproducts 0.1

Horse, fat 0.1

Horse, meat 0.1

Horse, meat byproducts 0.1

Milk 0.1

Sheep, fat 0.1

Sheep meat 0.1

Sheep meat byproducts 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 28888, May 23, 2007, as amended at 73 FR 5109, Jan. 29, 2008]

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§180.341 2,4-Dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate; tolerances for residues.

(a) General. Tolerances are established for combined negligible residues of a fungicide and insecticide that is a 

mixture of 2,4-dinitro-6-octylphenyl crotonate and 2,6-dinitro-4-octylphenyl crotonate in or on raw agricultural commodities 

as follows: 

Commodity Parts per million

Apple1 0.1

Grape1 0.1

1

There are no U.S. registrations on apple and grape as of October 24, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 29715, July 15, 1975, as amended at 63 FR 57076, Oct. 26, 1998; 69 FR 43924, July 23, 2004]

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§180.342 Chlorpyrifos; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the pesticide chlorpyrifos per se

(O,O-diethyl-O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the following food commodities:

Commodity Parts per million

Alfalfa, forage 3.0

Alfalfa, hay 13

Almond 0.2

Almond, hulls 12

Apple 0.01

Apple, wet pomace 0.02

Banana 0.1

Beet, sugar, dried pulp 5.0

Beet, sugar, molasses 15

Beet, sugar, roots 1.0

Beet, sugar, tops 8.0

Cattle, fat 0.3

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Cherry, sweet 1.0

Cherry, tart 1.0

Citrus, dried pulp 5.0

Citrus, oil 20

Corn, field, forage 8.0

Corn, field, grain 0.05

Corn, field, refined oil 0.25

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Corn, field, stover 8.0

Corn, sweet, forage 8.0

Corn, sweet, kernel plus cob with husk removed 0.05

Corn, sweet, stover 8.0

Cotton, undelinted seed 0.2

Cranberry 1.0

Cucumber 0.05

Egg 0.01

Fig 0.01

Fruit, citrus, group 10 1.0

Goat, fat 0.2

Goat, meat 0.05

Goat, meat byproducts 0.05

Hazelnut 0.2

Hog, fat 0.2

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.25

Horse, meat 0.25

Horse, meat byproducts 0.25

Kiwifruit 2.0

Milk, fat (Reflecting 0.01 ppm in whole milk) 0.25

Nectarine 0.05

Onion, bulb 0.5

Peach 0.05

Peanut 0.2

Peanut, refined oil 0.2

Pear 0.05

Pecan 0.2

Pepper 1.0

Peppermint, tops 0.8

Peppermint, oil 8.0

Plum, prune, fresh 0.05

Poultry, fat 0.1

Poultry, meat 0.1

Poultry, meat byproducts 0.1

Pumpkin 0.05

Radish 2.0

Rutabaga 0.5

Sheep, fat 0.2

Sheep, meat 0.05

Sheep, meat byproducts 0.05

Spearmint, tops 0.8

Spearmint, oil 8.0

Sorghum, grain, forage 0.5

Sorghum, grain, grain 0.5

Sorghum, grain, stover 2.0

Soybean, seed 0.3

Strawberry 0.2

Sunflower, seed 0.1

Sweet potato, roots 0.05

Turnip, roots 1.0

Turnip, tops 0.3

Vegetable, brassica, leafy, group 5 1.0

Vegetable, legume, group 6. except soybean 0.05

Walnut 0.2

Wheat, forage 3.0

Wheat, grain 0.5

Wheat, straw 6.0

(2) Chlorpyrifos [O,O-diethyl O-(3,5,6-trichloro-2-pyridyl) phosphorothioate] may be safely used in accordance with the 

following prescribed conditions. 

(i) Application shall be limited solely to spot and/or crack and crevice treatment in food handling establishments where 

food and food products are held, processed, prepared or served. Contamination of food or food contact surfaces shall be 

avoided. Food must be removed or covered during treatment. 

(ii) Spray concentration for spot treatment shall be limited to a maximum of 0.5 percent of the active ingredient by 

weight. A course, low-pressure spray shall be used to avoid atomization or splashing of the spray. 

(iii) Paint-on application for spot treatment shall be limited to a maximum of 2 percent of the active ingredient by 

weight. 

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(iv) Crack and crevice treatment shall be limited to a maximum of 2 percent of the active ingredient by weight. 

Equipment capable of delivering a pin-stream of insecticide shall be used. 

(v) Application via adhesive strips shall contain a maximum of 10% by weight of the controlled-release product in 

food-handling establishments where food and food products are held, processed, prepared, or served. A maximum of 36 

strips (or 5.15 grams of chlorpyrifos) is to be used per 100 square feet of floor space. The strips are not to be placed in 

exposed areas where direct contact with food, utensils, and food-contact surfaces would be likely to occur. 

(vi) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. 

Environmental Protection Agency, and it shall be used in accordance with such label and labeling. 

(3) A tolerance of 0.1 part per million is established for residues of chlorpyrifos, per se, in or on food commodities 

(other than those already covered by a higher tolerance as a result of use on growing crops) in food service 

establishments where food and food products are prepared and served, as a result of the application of chlorpyrifos in 

microencapsulated form.

(i) Application of a microencapsulated product shall be limited solely to spot and/or crack and crevice treatment in 

food handling establishments where food and food products are prepared and served. All treatments shall be applied in 

such a manner as to avoid contamination of food or food contact surfaces. 

(ii) Spray concentrations shall be limited to a maximum of 0.5 percent of the active ingredient by weight. 

(iii) For crack and crevice treatment, equipment capable of delivering a pin stream of spray directly into cracks and 

crevices or capable of applying small amounts of insecticide into cracks and crevices shall be used. 

(iv) For spot treatment, an individual spot shall not exceed 2 square feet. 

(v) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. 

Environmental Protection Agency, and it shall be used in accordance with such label and labeling. 

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in 180.1(l), are established 

for residues of the pesticide chlorpyrifos per se (O,O-diethyl- O-(3,5,6-trichloro-2-pyridyl) phosphorothioate) in or on the 

following food commodities:

Commodity Parts per million

Asparagus 5.0

Grape 0.01

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33711, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 71 FR 74817, Dec. 13, 2006; 73 FR 53739, Sept. 17, 

2008; 76 FR 56656, Sept. 14, 2011]

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§180.345 Ethofumesate; tolerances for residues.

(a) General. Tolerances for the combined residues of the herbicide ethofumesate (2-ethoxy-2,3-dihydro-3,3-dimethyl5-benzofuranyl methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl 

methanesulfonate and 2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranyl methanesulfonate both calculated as parent 

compound in or on the following food commodities:

Commodity Parts per million

Beet, garden, roots 0.5

Beet, garden, tops 5.0

Beet, sugar, molasses 0.5

Beet, sugar, refined sugar 0.2

Beet, sugar, roots 0.3

Beet, sugar, tops 4.0

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Garlic 0.25

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 0.05

Grass, straw 1.0

Horse, fat 0.05

Horse, meat 0.05

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Horse, meat byproducts 0.05

Onion, bulb 0.25

Shallot, bulb 0.25

Shallot, fresh leaves 0.25

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. Tolerances with regional registration as defined in 40 CFR 180.1(l) are 

established for the combined residues of ethofumesate,(2-ethoxy -2, 3-dihydro-3, 3-dimethyl-5-benzofuranyl 

methanesulfonate) and its metabolites 2-hydroxy-2,3-dihydro-3,3-dimethyl-5-benzofuranyl methanesulfonate and 

2,3-dihydro-3,3-dimethyl-2-oxo-5-benzofuranyl methanesulfonate (both calculated as the parent compound) in or on the 

raw agricultural commodities:

Commodity Parts per million

Carrot, roots 7.0

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 71 FR 51516, Aug. 30, 2006; 72 FR 52019, Sept. 12, 2007]

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§180.349 Fenamiphos; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide/insecticide fenamiphos, ethyl 3-methyl4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, including its metabolites and degradates, in or on the commodities 

in the following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring 

only the sum of fenamiphos, ethyl 3-methyl-4-(methylthio)phenyl 1-(methylethyl)phosphoramidate, and its cholinesterase 

inhibiting metabolites ethyl 3-methyl-4-(methylsulfinyl)phenyl 1-(methylethyl)phosphoramidate and ethyl 3-methyl4-(methylsulfonyl)phenyl 1-(methylethyl)phosphoramidate, calculated as the stoichiometric equivalent of fenamiphos, in or 

on the commodity.

Commodity Parts per million

Banana1 0.1

Grape1 0.1

Grape, raisin1 0.3

Pineapple1 0.3

1

There are no U.S. registrations as of May 31, 2007.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33712, May 24, 2000, as amended at 73 FR 53739, Sept. 17, 2008; 75 FR 60243, Sept. 29, 2010]

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§180.350 Nitrapyrin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the soil microbiocide nitrapyrin [2-chloro6-(trichloromethyl) pyridine] and its metabolite, 6-chloropicolinic acid in or on the following raw agricultural commodities:

Commodity Parts per million

Corn, field, forage 1.0

Corn, field, grain 0.1

Corn, field, milled byproducts 0.2

Corn, field, stover 1.0

Corn, pop, grain 0.1

Corn, pop, stover 1.0

Corn, sweet, forage 1.0

Corn, sweet, kernel plus cob with husks removed 0.1

Corn, sweet, stover 1.0

Sorghum, forage, forage 0.5

Sorghum, grain, forage 0.5

Sorghum, grain, grain 0.1

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Sorghum, grain, stover 0.5

Wheat, bran 3.0

Wheat, forage 2.0

Wheat, grain 0.5

Wheat, milled byproducts, except flour 2.0

Wheat, straw 6.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[46 FR 58315, Dec. 1, 1981, as amended at 47 FR 22957, May 26, 1982; 52 FR 33238, Sept. 2, 1987; 58 FR 32304, June 9, 1993; 

63 FR 57076, Oct. 26, 1998; 72 FR 53461, Sept. 19, 2007]

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§180.352 Terbufos; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide terbufos (phosphorodithioic acid, 

S-(t-butylthio)methyl O,O-diethyl ester) and its phosphorylated (cholinesterase-inhibiting) metabolites (phosphorothioic 

acid, S-(t-butylthio)methyl O,O-diethyl ester; phosphorothioic acid, S-(t-butylsulfinyl)methyl O,O-diethyl ester; 

phosphorothioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester; phosphorodithioic acid, S-(t-butylsulfinyl)methyl 

O,O-diethyl ester; and phosphorodithioic acid, S-(t-butylsulfonyl)methyl O,O-diethyl ester) in or on food commodities:

Commodity Parts per million

Banana 0.025

Beet, sugar, roots 0.05

Beet, sugar, tops 0.1

Coffee, green bean1 0.05

Corn, field, forage 0.5

Corn, field, grain 0.5

Corn, field, stover 0.5

Corn, pop, grain 0.5

Corn, pop, stover 0.5

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, forage 0.5

Corn, sweet, stover 0.5

Sorghum, grain, forage 0.5

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.5

1

 There are no U. S. registrations as of August 2, 1995, for the use of terbufos on the growing crop, coffee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 53740, Sept. 17, 2008]

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§180.353 Desmedipham; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide desmedipham, (ethyl-m-hydroxycarbanilate 

carbanilate) in or on the following raw agricultural commodities in the table that follows:

Commodity Parts per million

Beet, garden, roots 0.05

Beet, garden, tops 1.0

Beet, sugar, roots 0.1

Beet, sugar, tops 5.0

Spinach 6.0

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

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[40 FR 4658, Jan. 31, 1975, as amended at 62 FR 45747, Aug. 29, 1997; 63 FR 49472, Sept. 16, 1998; 64 FR 46292, Aug. 25, 

1999; 65 FR 82293, Dec. 28, 2000; 66 FR 64773, Dec. 14, 2001; 68 FR 37764, June 25, 2003; 69 FR 71717, Dec. 10, 2004; 72 FR 

53449, Sept. 19, 2007; 73 FR 53740, Sept. 17, 2008]

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§180.355 Bentazon; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. (1) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food 

commodities: 

Commodity Parts per million

Bean, dry, seed 0.05

Bean, succulent 0.5

Corn, field, forage 3.0

Corn, field, grain 0.05

Corn, field, stover 3.0

Corn, pop, grain 0.05

Corn, sweet, kernel plus cob with husks removed 0.05

Cowpea, forage 10.0

Cowpea, hay 3.0

Flax, seed 1.0

Pea, dry, seed 1.0

Pea, field, hay 8.0

Pea, field, vines 3.0

Pea, succulent 3.0

Peanut 0.05

Peanut, hay 3.0

Pepper, nonbell 0.05

Peppermint, tops 1.0

Rice, grain 0.05

Rice, hulls 0.25

Rice, straw 3.0

Sorghum, forage 0.20

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.05

Soybean, forage 8.0

Soybean, hay 8.0

Soybean, seed 0.05

Spearmint, tops 1.0

(2) Tolerances are established for the combined residues of the herbicide bentazon (3-isopropyl1H-2,1,3-benzothiadiazin-4(3H)-one-2,2-dioxide) and its metabolite 2-amino-N-isopropyl benzamide (AIBA) in or on the 

following food commodities: 

Commodity Parts per million 

Cattle, fat 0.05 

Cattle, meat byproducts 0.05 

Cattle, meat 0.05 

Egg 0.05 

Goat, fat 0.05 

Goat, meat byproducts 0.05 

Goat, meat 0.05 

Hog, fat 0.05 

Hog, meat byproducts 0.05 

Hog, meat 0.05 

Milk 0.02 

Poultry, fat 0.05 

Poultry, meat byproducts 0.05 

Poultry, meat 0.05 

Sheep, fat 0.05 

Sheep, meat byproducts 0.05 

Sheep, meat 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration as defined in §180.1(m), are 

established for combined residues of the herbicide, bentazon (3-isopropyl-1H-2, 1,3-benzothiadiazin-4(3H)

-one-2,2-dioxide) and its 6- and 8-hydroxy metabolites in or on the following food commodities:

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Commodity Parts per million

Clover, forage 1.0

Clover, hay 2.0

(d) Indirect or inadvertent residues. [Reserved]

[42 FR 26979, May 26, 1977]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.355, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.356 Norflurazon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide norflurazon (4-chloro5-(methylamino)-2-(alpha, alpha, alpha-trifluoro-m-tolyl)-3-(2H)-pyridazinone) and its desmethyl metabolite 4-chloro5-(amino)-2-alpha, alpha, alpha-trifluoro-m-tolyl)-3(2H)-pyridazinone in or on the following raw agricultural commodities:

Commodity Parts per million

Alfalfa, forage 3.0

Alfalfa, hay 5.0

Alfalfa, seed 0.1

Almond, hulls 1.0

Almond 0.1

Apple 0.1

Apricot 0.1

Asparagus 0.05

Avocado 0.20

Blackberry 0.1

Blueberry 0.2

Cattle, fat 0.1

Cattle, liver 0.50

Cattle, meat 0.1

Cattle, meat byproducts, except liver 0.1

Cherry 0.1

Citrus, dried pulp 0.4

Citrus, molasses 1.0

Cotton, undelinted seed 0.1

Cranberry 0.1

Fruit, citrus 0.2

Goat, fat 0.1

Goat, liver 0.50

Goat, meat 0.1

Goat, meat byproducts, except liver 0.1

Grape 0.1

Hazelnut 0.1

Hog, fat 0.1

Hog, liver 0.50

Hog, meat 0.1

Hog, meat byproducts, except liver 0.1

Hop, dried cones 3.0

Hop, vines 1.0

Horse, fat 0.1

Horse, liver 0.50

Horse, meat 0.1

Horse, meat byproducts, except liver 0.1

Milk 0.1

Nectarine 0.1

Peach 0.1

Peanut 0.05

Peanut, hay 5.50

Peanut, hay 1.5

Pear 0.1

Pecan 0.1

Plum, prune, fresh 0.1

Poultry, fat 0.1

Poultry, meat 0.1

Poultry, meat byproducts 0.1

Raspberry 0.2

Sheep, fat 0.1

Sheep, liver 0.50

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Sheep, meat 0.1

Sheep, meat byproducts, except liver 0.1

Soybean 0.1

Soybean, forage 1.0

Soybean, hay 1.0

Walnut 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 14909, Apr. 7, 1982]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.356, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.360 Asulam; tolerance for residues.

(a) General. Tolerances are established for the combined residues of asulam (methyl sulfanilylcarbamate) and its 

sulfanilamide containing metabolites in or on the following food commodities:

Commodity Parts per million

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.2

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 0.2

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.2

Horse, fat 0.05

Horse, meat 0.05

Horse, meat byproducts 0.2

Milk 0.05

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.2

Sugarcane, cane 1.0

Sugarcane, molasses 30

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 39441, July 1, 2003, as amended at 72 FR 37654, July 11, 2007]

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§180.361 Pendimethalin; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide pendimethalin, including its metabolites and 

degradates, in or on the commodities. Compliance with the tolerance levels specified in the following table below is to be 

determined by measuring only pendimethalin, [N- (1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine], and its metabolite, 

4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, calculated as the stoichiometric equivalent of pendimethalin, in 

or on the following commodities:

Commodity Parts per million 

Alfalfa, forage 3.5

Alfalfa, hay 4.0

Alfalfa, seed 0.10

Almond, hulls 6.0

Apple, wet pomace 0.20

Artichoke, globe 0.1

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Asparagus 0.15

Beans 0.10

Beans, forage 0.10

Beans, hay 0.10

Berry, low growing subgroup 13-07G 0.1

Brassica head and stem, subgroup 5-A 0.1

Brassica, leafy greens, subgroup 5B 0.20

Carrot 0.5

Citrus, oil 0.5

Corn, field, forage 0.1 

Corn, field, grain 0.1

Corn, field, stover 0.1 

Corn, pop, grain 0.1

Corn, sweet, forage 0.1 

Corn, sweet, kernel plus cob with husks removed 0.1 

Corn, sweet, stover 0.1 

Cotton, gin byproducts 3.0 

Cotton, undelinted seed 0.1 

Crayfish 0.05 

Fruit, citrus, group 10-10 0.1

Fruit, pome, group 11-10 0.1

Fruit, small vine climbing, except grape, subgroup 13-07E 0.10

Fruit, stone, group 12-12 0.1

Grape 0.1

Grass forage, fodder, and hay crop group 17, forage 20

Grass forage, fodder, and hay crop group 17, hay 13

Grass forage, fodder, and hay crop group 17, straw 4.0

Hop, dried cones 0.1

Juneberry 0.10

Lettuce, leaf 4.0

Melon subgroup 9A 0.10

Nut, tree, group 14 0.1

Olive 0.1 

Onion, bulb subgroup 3-07A 0.1

Onion, green subgroup 3-07B 0.2

Peanut 0.1 

Peanut, hay 0.1 

Peas (except field peas) 0.10

Peppermint, oil 1.0

Peppermint, tops 0.2

Pistachio 0.1

Pomegranate 0.10

Potato 0.1 

Rice, grain 0.1 

Rice, straw 0.1 

Sorghum, forage 0.1 

Sorghum, grain, grain 0.1 

Sorghum, grain, stover 0.1 

Soybean, forage 0.1 

Soybean, hay 0.1 

Soybean, seed 0.1 

Spearmint, oil 1.0

Spearmint, tops 0.2

Sugarcane, cane 0.1 

Sunflower subgroup 20B 0.1

Turnip greens 0.20

Vegetable, fruiting, group 8-10 0.1

Vegetable, soybean, succulent 0.10

Wheat, grain 0.10

Wheat, forage 3.0

Wheat, hay 0.60

Wheat, straw 0.30

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

combined residues of the herbicide pendimethalin, [N-(1-ethylpropyl)-3,4-dimethyl-2,6-dinitrobenzenamine], and its 

metabolite 4-[(1-ethylpropyl)amino]-2-methyl-3,5-dinitrobenzyl alcohol, in or on the specified agricultural commodities, 

resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerances expire and are 

revoked on the date specified in the table.

Commodity Parts per million Expiration/revocation date

Bermuda grass, forage 25 12/31/10

Bermuda grass, hay 60 12/31/10

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(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[49 FR 15293, Apr. 18, 1984]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.361, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.362 Fenbutatin-oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its 

metabolites and degradates, in or on the plant commodities in the table in this paragraph. Compliance with the tolerance 

levels specified in this paragraph is to be determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-

phenylpropyl) distannoxane, in or on the commodity.

Commodity Parts per million

Almond, hulls 80.0

Apple 15.0

Apple, wet pomace 100.0

Cherry, sweet 6.0

Cherry, tart 6.0

Citrus, dried pulp 100.0

Citrus, oil 140.0

Cucumber 4.0

Eggplant 6.0

Fruit, citrus, group 10 20.0

Grape 5.0

Grape, raisin 20.0

Nut, tree, group 14 0.5

Papaya 2.0

Peach 10.0

Pear 15.0

Pistachio 0.5

Plum, prune, fresh 4.0

Plum, prune, dried 20.0

Strawberry 10.0

(2) Tolerances are established for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and 

degradates, in or on the animal commodities in the table in this paragraph. Compliance with the tolerance levels specified 

in this paragraph is to be determined by measuring only the sum of fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) 

distannoxane, and its organotin metabolites, dihydroxybis(2-methyl-2-phenylpropyl) stannane and 2-methyl-2-

phenylpropylstannoic acid, calculated as the stoichiometric equivalent of fenbutatin-oxide, in or on the commodity.

Commodity Parts per million

Cattle, fat 0.5

Cattle, meat 0.5

Cattle, meat byproducts 0.5

Egg 0.1

Goat, fat 0.5

Goat, meat 0.5

Goat, meat byproducts 0.5

Hog, fat 0.5

Hog, meat 0.5

Hog, meat byproducts 0.5

Horse, fat 0.5

Horse, meat 0.5

Horse, meat byproducts 0.5

Milk, fat 0.1

Poultry, fat 0.1

Poultry, meat 0.1

Poultry, meat byproducts 0.1

Sheep, fat 0.5

Sheep, meat 0.5

Sheep, meat byproducts 0.5

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established 

for residues of the miticide/acaricide fenbutatin-oxide, including its metabolites and degradates, in or on the plant 

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commodity in the table in this paragraph. Compliance with the tolerance level specified in this paragraph is to be 

determined by measuring only fenbutatin-oxide, hexakis (2-methyl-2-phenylpropyl) distannoxane, in or on the commodity.

Commodity Parts per million 

Raspberry 10.0

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33713, May 24, 2000, as amended at 72 FR 41930, Aug. 1, 2007; 73 FR 5109, Jan. 29, 2008; 76 FR 23494, Apr. 27, 2011]

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§180.364 Glyphosate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or 

on the commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the 

ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the 

potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only 

glyphosate (N-(phosphonomethyl)glycine).

Commodity Parts per million

Acerola 0.2

Alfalfa, seed 0.5

Almond, hulls 25

Aloe vera 0.5

Ambarella 0.2

Animal feed, nongrass, group 18 400

Artichoke, globe 0.2

Asparagus 0.5

Atemoya 0.2

Avocado 0.2

Bamboo, shoots 0.2

Banana 0.2

Barley, bran 30

Beet, sugar, dried pulp 25

Beet, sugar, roots 10

Beet, sugar, tops 10

Berry and small fruit, group 13-07 0.20

Betelnut 1.0

Biriba 0.2

Blimbe 0.2

Breadfruit 0.2

Cacao bean, bean 0.2

Cactus, fruit 0.5

Cactus, pads 0.5

Canistel 0.2

Carrot 5.0

Chaya 1.0

Cherimoya 0.2

Citrus, dried pulp 1.5

Coconut 0.1

Coffee, bean, green 1.0

Corn, pop, grain 0.1

Corn, sweet, kernel plus cob with husk removed 3.5

Cotton, gin byproducts 210

Custard apple 0.2

Date, dried fruit 0.2

Dokudami 2.0

Durian 0.2

Epazote 1.3

Feijoa 0.2

Fig 0.2

Fish 0.25

Fruit, citrus, group 10-10 0.50

Fruit, pome, group 11-10 0.20

Fruit, stone, group 12 0.2

Galangal, roots 0.2

Ginger, white, flower 0.2

Gourd, buffalo, seed 0.1

Governor's plum 0.2

Gow kee, leaves 0.2

Grain, cereal, forage, fodder and straw, group 16, except field corn, forage and field corn, stover 100

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Grain, cereal, group 15 except field corn, popcorn, rice, sweet corn, and wild rice 30

Grass, forage, fodder and hay, group 17 300

Guava 0.2

Herbs subgroup 19A 0.2

Hop, dried cones 7.0

Ilama 0.2

Imbe 0.2

Imbu 0.2

Jaboticaba 0.2

Jackfruit 0.2

Kava, roots 0.2

Kenaf, forage 200

Leucaena, forage 200

Longan 0.2

Lychee 0.2

Mamey apple 0.2

Mango 0.2

Mangosteen 0.2

Marmaladebox 0.2

Mioga, flower 0.2

Noni 0.20

Nut, pine 1.0

Nut, tree, group 14 1.0

Oilseeds, group 20, except canola 40

Okra 0.5

Olive 0.2

Oregano, Mexican, leaves 2.0

Palm heart 0.2

Palm heart, leaves 0.2

Palm, oil 0.1

Papaya 0.2

Papaya, mountain 0.2

Passionfruit 0.2

Pawpaw 0.2

Pea, dry 8.0

Peanut 0.1

Peanut, hay 0.5

Pepper leaf, fresh leaves 0.2

Peppermint, tops 200

Perilla, tops 1.8

Persimmon 0.2

Pineapple 0.1

Pistachio 1.0

Pomegranate 0.2

Pulasan 0.2

Quinoa, grain 5.0

Rambutan 0.2

Rice, grain 0.1

Rice, wild, grain 0.1

Rose apple 0.2

Sapodilla 0.2

Sapote, black 0.2

Sapote, mamey 0.2

Sapote, white 0.2

Shellfish 3.0

Soursop 0.2

Spanish lime 0.2

Spearmint, tops 200

Spice subgroup 19B 7.0

Star apple 0.2

Starfruit 0.2

Stevia, dried leaves 1.0

Sugar apple 0.2

Sugarcane, cane 2.0

Sugarcane, molasses 30

Surinam cherry 0.2

Sweet potato 3.0

Tamarind 0.2

Tea, dried 1.0

Tea, instant 7.0

Teff, forage 100

Teff, grain 5.0

Teff, hay 100

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Ti, leaves 0.2

Ti, roots 0.2

Ugli fruit 0.5

Vegetable, bulb, group 3-07 0.20

Vegetable, cucurbit, group 9 0.5

Vegetable, foliage of legume, subgroup 7A, except soybean 0.2

Vegetable, fruiting, group 8-10 (except okra) 0.10

Vegetable, leafy, brassica, group 5 0.2

Vegetable, leafy, except brassica, group 4 0.2

Vegetable, leaves of root and tuber, group 2, except sugar beet tops 0.2

Vegetable, legume, group 6 except soybean and dry pea 5.0

Vegetables, root and tuber, group 1, except carrot, sweet potato, and sugar beet 0.20

Wasabi, roots 0.2

Water spinach, tops 0.2

Watercress, upland 0.2

Wax jambu 0.2

Yacon, tuber 0.2

(2) Tolerances are established for residues of glyphosate, including its metabolites and degradates, in or on the 

commodities listed below resulting from the application of glyphosate, the isopropylamine salt of glyphosate, the 

ethanolamine salt of glyphosate, the dimethylamine salt of glyphosate, the ammonium salt of glyphosate, and the 

potassium salt of glyphosate. Compliance with the following tolerance levels is to be determined by measuring only 

glyphosate (N-(phosphonomethyl)glycine) and its metabolite N-acetyl-glyphosate (N-acetyl-N-(phosphonomethyl)glycine; 

calculated as the stoichiometric equivalent of glyphosate).

Commodity Parts per Million

Canola, seed 20

Cattle, meat byproducts 5.0

Corn, field, forage 13

Corn, field, grain 5.0

Corn, field, stover 100

Egg 0.05

Goat, meat byproducts 5.0

Grain aspirated fractions 310.0

Hog, meat byproducts 5.0

Horse, meat byproducts 5.0

Poultry, meat 0.10

Poultry, meat byproducts 1.0

Sheep, meat byproducts 5.0

Soybean, forage 100.0

Soybean, hay 200.0

Soybean, hulls 120.0

Soybean, seed 20.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 64911, Oct. 1, 1980]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.364, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.367 n-Octyl bicycloheptenedicarboximide; tolerances for residues.

(a) General. A tolerance of 5 parts per million is established for residues of the insecticide synergist N-octyl 

bicycloheptene dicarboximide, including its metabolites and degradates, in or on all food items in food handling 

establishments where food and food products are held, processed, prepared and/or served, provided that the food is 

removed or covered prior to such use, except for bagged food in warehouse storage which need not be removed or 

covered prior to applications of formulations containing N-octyl bicycloheptene dicarboximide. Compliance with the 

tolerance level specified in this paragraph is to be determined by measuring only N-octyl bicycloheptene dicarboximide, in 

or on the commodity.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

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§180.368 Metolachlor; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues (free and bound) of the herbicide metolachlor, 

2-chloro-N-(2- ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, and its metabolites, determined as the 

derivatives, 2- [(2-ethyl-6- methylphenyl)amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-

morpholinone, each expressed as the parent compound in the following raw agricultural commodities:

Commodity Parts per million

Almond, hulls 0.30

Animal feed, nongrass, group 18 1.0

Cattle, fat 0.02

Cattle, kidney 0.20

Cattle, liver 0.05

Cattle, meat 0.02

Cattle, meat byproducts, except kidney and liver 0.04

Corn, field, forage 6.0

Corn, field, grain 0.10

Corn, field, stover 6.0

Corn, pop, grain 0.10

Corn, pop, stover 6.0

Corn, sweet, forage 6.0

Corn, sweet, kernel plus cob with husks removed 0.10

Corn, sweet, stover 6.0

Cotton, gin byproducts 4.0

Cotton, undelinted seed 0.10

Dillweed 0.50

Egg 0.02

Goat, fat 0.02

Goat, kidney 0.20

Goat, liver 0.05

Goat, meat 0.02

Goat, meat byproducts, except kidney and liver 0.04

Grass, forage 10

Grass, hay 0.20

Horse, fat 0.02

Horse, kidney 0.20

Horse, liver 0.05

Horse, meat 0.02

Horse, meat byproducts, except kidney and liver 0.04

Milk 0.02

Nut, tree, group 14 0.10

Okra 0.50

Peanut 0.20

Peanut, hay 20

Peanut, meal 0.40

Potato 0.20

Poultry, fat 0.02

Poultry, meat 0.02

Poultry, meat byproducts 0.05

Safflower, seed 0.10

Sheep, fat 0.02

Sheep, kidney 0.20

Sheep, liver 0.05

Sheep, meat 0.02

Sheep, meat byproducts, except kidney and liver 0.04

Sorghum, grain, forage 1.0

Sorghum, grain, grain 0.30

Sorghum, grain, stover 4.0

Soybean, forage 5.0

Soybean, hay 8.0

Soybean, seed 0.20

Tomato 0.10

Vegetable, foliage of legume, subgroup 7A, except soybean 15.0

Vegetable, legume, group 6 0.30

(2) Tolerances are established for residues of S-metolachlor, including its metabolites and degradates, in or on the 

commodity(s), as defined. Compliance with the tolerance levels specified in the following table below is to be determined 

by measuring only the sum of free and bound S-metolachlor, S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-

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methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as the derivatives, 2-(2-ethyl-6-methylphenyl)

amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, calculated as the stoichiometric 

equivalent of S-metolachlor, in or on the commodity.

Commodity Parts per million

Asparagus 0.10

Beet, garden, leaves 1.8

Beet, sugar, molasses 2.0

Beet, sugar, roots 0.5

Beet, sugar, tops 15.0

Brassica, head and stem, subgroup 5A 0.60

Brassica, leafy greens, subgroup 5B 1.8

Bushberry subgroup 13-07B 0.15

Caneberry subgroup 13-07A 0.10

Carrot, roots 0.40

Cattle, fat 0.02

Cattle, kidney 0.20

Cattle, liver 0.05

Cattle, meat 0.02

Cattle, meat byproducts, except kidney and liver 0.04

Cilantro, leaves 8.0

Coriander, seed 0.13

Corn, field, forage 40

Corn, field, grain 0.10

Corn, field, stover 40

Corn, pop, grain 0.10

Corn, pop, stover 40

Corn, sweet, forage 40

Corn, sweet, kernel plus cob with husks removed 0.10

Corn, sweet, stover 40

Cotton, gin byproducts 4.0

Cotton, undelinted seed 0.10

Egg 0.02

Grain, aspirated fractions 0.70

Goat, fat 0.02

Goat, kidney 0.20

Goat, liver 0.05

Goat, meat 0.02

Goat, meat byproducts, except kidney and liver 0.04

Grass, forage 10.0

Grass, hay 0.20

Horse, fat 0.02

Horse, kidney 0.20

Horse, liver 0.05

Horse, meat 0.02

Horse, meat byproducts, except kidney and liver 0.04

Leaf petioles, subgroup 4B 0.10

Lettuce 1.5

Low growing berry subgroup 13-07G, except cranberry 0.40

Milk 0.02

Onion, bulb, subgroup 3-07A 0.10

Onion, green, subgroup 3-07B 2.0

Peanut 0.20

Peanut, hay 20.0

Peanut, meal 0.40

Poultry, fat 0.02

Poultry, meat 0.02

Poultry, meat byproducts 0.05

Safflower, seed 0.10

Sesame, seed 0.13

Sheep, fat 0.02

Sheep, kidney 0.20

Sheep, liver 0.05

Sheep, meat 0.02

Sheep, meat byproducts, except kidney and liver 0.04

Sorghum, grain, forage 1.0

Sorghum, grain, grain 0.3

Sorghum, grain, stover 4.0

Sorghum, sweet, stalk 4.0

Soybean, forage 5.0

Soybean, hay 8.0

Soybean, seed 0.20

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Spinach 0.50

Sunflower, meal 1.0

Sunflower subgroup 20B 1.0

Tomato, paste 0.30

Turnip, greens 1.8

Vegetable, cucurbit group 9 0.50

Vegetable, foliage of legume, except soybean, subgroup 7A 15.0

Vegetable, fruiting, group 8-10, except tabasco pepper 0.10

Vegetable, legume, group 6 0.30

Vegetable, root, except sugar beet, subgroup 1B, except carrot 0.30

Vegetable, tuberous and corm, subgroup 1C 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. (1) Tolerances with regional registration as defined in 180.1(l) are 

established for the combined residues (free and bound) of the herbicide metolachlor [2-chloro-N-(2-ethyl-6-methylphenyl)

-N-(2-methoxy-1-methylethyl)acetamide] and its metabolites, determined as the derivatives, 2-[2-ethyl-6-methylphenyl)

amino]-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-morpholinone, each expressed as the parent 

compound, in or on the following raw agricultural commodities:

Commodity Parts per million

Pepper, nonbell 0.50

(2) Tolerances with regional registration are established for residues of S-metolachlor, including its metabolites and 

degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels specified 

in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, S-2-chloroN-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, determined as 

the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-methyl-3-

morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Commodity Parts per million

Pepper, tabasco 0.50

(d) Indirect or inadvertent residues. (1) Tolerances are established for the indirect or inadvertent combined residues 

(free and bound) of the herbicide metolachlor, 2-chloro-N-(2-ethyl-6- methylphenyl)-N-(2-methoxy-1-methylethyl)

acetamide, and its metabolites, determined as the derivatives, 2-[(2-ethyl-6-methylphenyl)amino]-1-propanol and 

4-(2-ethyl-6-methylphenyl)-2- hydroxy-5-methyl-3-morpholinone, each expressed as the parent compound in the following 

raw agricultural commodities:

Commodity Parts per million

Animal feed, nongrass, group 18 1.0

Barley, grain 0.10

Barley, hay 0.80

Barley, straw 0.80

Buckwheat, grain 0.10

Millet, forage 0.50

Millet, grain 0.10

Millet, hay 0.80

Millet, straw 0.80

Oat, forage 0.50

Oat, grain 0.10

Oat, hay 0.80

Oat, straw 0.80

Rice, grain 0.10

Rye, forage 0.50

Rye, grain 0.10

Rye, straw 0.80

Wheat, forage 0.50

Wheat, grain 0.10

Wheat, hay 0.80

Wheat, straw 0.80

(2) Tolerances for are established for the indirect or inadvertent residues of S-metolachlor, including its metabolites 

and degradates, in or on the commodities identified in the following table below. Compliance with the tolerance levels 

specified in the following table below is to be determined by measuring only the sum of free and bound S-metolachlor, 

S-2-chloro-N-(2-ethyl-6-methylphenyl)-N-(2-methoxy-1-methylethyl)acetamide, its R-enantiomer, and its metabolites, 

determined as the derivatives, 2-(2-ethyl-6-methylphenyl)amino-1-propanol and 4-(2-ethyl-6-methylphenyl)-2-hydroxy-5-

methyl-3-morpholinone, calculated as the stoichiometric equivalent of S-metolachlor, in or on the commodity.

Commodity Parts per million

Animal feed, nongrass, group 18 1.0

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Barley, grain 0.10

Barley, hay 0.50

Barley, straw 0.50

Buckwheat, grain 0.10

Millet, forage 0.50

Millet, grain 0.10

Millet, hay 0.50

Millet, straw 0.50

Oat, forage 0.50

Oat, grain 0.10

Oat, hay 0.50

Oat, straw 0.50

Rice, grain 0.10

Rye, forage 0.50

Rye, grain 0.10

Rye, straw 0.50

Wheat, forage 0.50

Wheat, grain 0.10

Wheat, hay 0.50

Wheat, straw 0.50

[73 FR 53740, Sept. 17, 2008, as amended at 74 FR 48412, Sept. 23, 2009; 75 FR 56903, Sept. 17, 2010; 77 FR 48906, Aug. 15, 

2012; 77 FR 59127, Sept. 26, 2012; 79 FR 17441, Mar. 28, 2014; 80 FR 38986, July 8, 2015]

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§180.370 5-Ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide 5-ethoxy-3-(trichloromethyl)-1,2,4-thiadiazole 

and its monoacid metabolite 3-carboxy-5-ethoxy-1,2,4-thiadiazole in or on the following raw agricultural commodities:

Commodity Parts per million

Barley, grain 0.1

Barley, hay 0.1

Corn, field, forage 0.1

Corn, field, grain 0.1

Corn, field, stover 0.1

Corn, sweet, forage 0.1

Corn, sweet, stover 0.1

Cotton, gin byproducts 0.1

Cotton, undelinted seed 0.1

Peanut 0.1

Peanut, hay 0.1 

Safflower, seed 0.1

Sorghum, grain, forage 0.1

Sorghum, grain, grain 0.1

Tomato 0.15

Vegetable, foliage of legume, group 7 0.1

Vegetable, legume, group 6 0.1

Wheat, forage 0.1

Wheat, grain 0.1

Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 49845, Nov. 3, 1982, as amended at 48 FR 12088, Mar. 23, 1983; 63 FR 57076, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007; 

73 FR 54961, Sept. 24, 2008]

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§180.371 Thiophanate-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of thiophanate-methyl, dimethyl ((1,2-phenylene) bis 

(iminocarbonothioyl)) bis(carbamate), including its metabolites and degradates, in or on the commodities in the following 

table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of 

thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) bis(carbamate), and its metabolite, methyl 

2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent of thiophanate-methyl, in or on the 

commodity.

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Commodity Parts per million

Almond 0.1

Almond, hulls 0.5

Apple 2.0

Apricot 15.0

Banana 2.0

Bean, dry, seed 0.2

Bean, snap, succulent 2.0

Beet, sugar, roots 0.2

Cherry, sweet 20.0

Cherry, tart 20.0

Grain, aspirated fractions 12

Grape 5.0

Onion, bulb 0.5

Onion, green 3.0

Peach 3.0

Peanut 0.1

Peanut, hay 5.0

Pear 3.0

Pecan 0.1

Pistachio 0.1

Plum 0.5

Potato 0.1

Soybean, hulls 1.5

Soybean, seed 0.2

Strawberry 7.0

Vegetable, cucurbit, group 9 1.0

Wheat, forage 1.1

Wheat, grain 0.1

Wheat, hay 0.1

Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with a regional registration is established for residues of 

thiophanate-methyl, dimethyl ((1,2-phenylene) bis(iminocarbonothioyl)) bis(carbamate), including its metabolites and 

degradates, in or on the commodity in the following table. Compliance with the tolerance level specified in this paragraph 

is to be determined by measuring only the sum of thiophanate-methyl, dimethyl ((1,2-phenylene) bis (iminocarbonothioyl)) 

bis(carbamate), and its metabolite, methyl 2-benzimidazoyl carbamate (MBC), calculated as the stoichiometric equivalent 

of thiophanate-methyl, in or on the commodity.

Commodity Parts per million

Canola, seed 0.1

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 60244, Sept. 29, 2010]

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§180.372 2,6-Dimethyl-4-tridecylmorpholine; tolerances for residues.

(a) General. A tolerance is established for residues of the fungicide 2,6-dimethyl-4-tridecylmorpholine in or on the 

following food commodity:

Commodity Parts per million 

Banana1 1.0 

1

There are no U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54961, Sept. 24, 2008]

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§180.373 [Reserved]

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§180.377 Diflubenzuron; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. (1) Tolerances are established for residues of diflubenzuron, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

Commodity Parts per million 

Artichoke, globe 6.0 

Cattle, fat 0.05 

Cattle, meat 0.05 

Cotton, undelinted seed 0.2 

Egg 0.05 

Goat, fat 0.05 

Goat, meat 0.05 

Hog, fat 0.05 

Hog, meat 0.05 

Horse, fat 0.05 

Horse, meat 0.05 

Milk 0.05 

Mushroom 0.2 

Poultry, fat 0.05 

Poultry, meat byproducts 0.05 

Poultry, meat 0.05 

Sheep, fat 0.05 

Sheep, meat 0.05 

Soybean 0.05 

Soybean, hulls 0.5

(2) Tolerances are established for residues of the insecticide diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]

-2,6-difluorobenzamide), in or on the commodities in the table below. Compliance with the tolerance levels specified below 

is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]

-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of 

diflubenzuron, in or on the commodity.

Commodity Parts per million

Almond, hulls 6.0 

Barley, grain 0.06

Barley, hay 3.0

Barley, straw 1.8

Brassica, leafy greens, subgroup 5B 9.0

Cattle, meat byproducts 0.15

Citrus, oil 32

Fruit, citrus, group 10-10 3.0

Fruit, stone, group 12, except cherry 0.07

Goat, meat byproducts 0.15

Grain, aspirated fractions 11

Grass, forage, fodder, and hay, group 17 6.0

Hog, meat byproducts 0.15

Horse, meat byproducts 0.15

Nut, tree, group 14 0.06 

Oat, forage 7.0

Oat, grain 0.06

Oat, hay 6.0

Oat, straw 3.5

Peanut 0.10

Peanut, hay 55

Peanut, refined oil 0.20

Pear 0.50

Pepper 1.0 

Pistachio 0.06

Rice, grain 0.02

Rice, straw 0.8

Sheep, meat byproducts 0.15

Turnip greens 9.0

Wheat, forage 7.0

Wheat, grain 0.06

Wheat, hay 6.0

Wheat, straw 3.5

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(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide 

diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]-2,6- difluorobenzamide) and its metabolites, in connection with use of 

the pesticide under section 18 emergency exemptions granted by EPA. Compliance with the tolerance levels specified 

below is to be determined by measuring only the sum of diflubenzuron (N-[[(4-chlorophenyl)amino]carbonyl]

-2,6-difluorobenzamide), 4-chlorophenylyurea and 4-chloroaniline, calculated as the stoichiometric equivalent of 

diflubenzuron, in or on the commodity. The tolerances are specified in the following table, and will expire and are revoked 

on the dates specified.

Commodity Parts per million Expiration/revocation date

Alfalfa, forage 6.0 12/31/17

Alfalfa, hay 6.0 12/31/17

Lemon 0.8 12/31/10

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33699, May 24, 2000]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.377, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.378 Permethrin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide cis- and trans-permethrin 

isomers [cis-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] and 

[trans-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] in/on the following food 

commodities:

Commodity Parts per million

Alfalfa, forage 20

Alfalfa, hay 45

Almond 0.05

Almond, hulls 20

Artichoke, globe 5.0

Asparagus 2.0

Avocado 1.0

Broccoli 2.0

Brussels sprouts 1.0

Cabbage 6.0

Cattle, fat 1.5

Cattle, meat 0.10

Cattle, meat byproducts 0.10

Cauliflower 0.5

Cherry, sweet 4.0

Cherry, tart 4.0

Corn, field, forage 50

Corn, field, grain 0.05

Corn, field, stover 30

Corn, pop, grain 0.05

Corn, pop, stover 30

Corn, sweet, forage 50

Corn, sweet, kernel plus cob with husks removed 0.10

Corn, sweet, stover 30

Egg 0.10

Eggplant 0.50

Fruit, pome, group 11 0.05

Garlic, bulb 0.10

Grain, aspirated fractions 0.50

Goat, fat 1.5

Goat, meat 0.10

Goat, meat byproducts 0.10

Hazelnut 0.05

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 1.5

Horse, meat 0.10

Horse, meat byproducts 0.10

Horseradish 0.50

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Kiwifruit 2.0

Leaf petioles subgroup 4B 5.0

Leafy greens subgroup 4A 20

Lettuce, head 20

Milk, fat (reflecting 0.88 ppm in whole milk) 3.0

Mushroom 5.0

Onion, bulb 0.10

Peach 1.0

Pepper, bell 0.50

Pistachio 0.10

Potato 0.05

Poultry, fat 0.15

Poultry, meat 0.05

Poultry, meat byproducts 0.05

Sheep, fat 1.5

Sheep, meat 0.10

Sheep, meat byproducts 0.10

Soybean, seed 0.05

Spinach 20

Tomato 2.0

Vegetable, cucurbit, group 9 1.5

Walnut 0.05

Watercress 5.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l) are established 

for the combined residues of the insecticide cis- and trans-permethrin isomers [cis-(3-phenoxyphenyl)methyl 

3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate] and [trans-(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)

-2,2-dimethylcyclopropane carboxylate] in/on the following food commodities:

Commodity Parts per million

Collards 15

Grass, forage 15

Grass, hay 15

Papaya 1.0

Turnip, tops 10

Turnip, roots 0.20

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 52019, Sept. 12, 2007]

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§180.380 Vinclozolin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide vinclozolin (3-(3,5-dichlorophenyl)

-5-ethenyl-5-methyl-2,4-oxazolidinedione) and its metabolites containing the 3,5-dichloroaniline moiety in or on the food 

commodities in the table below. There are no U.S. registrations for grape (wine) as of July 30, 1997.

Commodity Parts per million Expiration/Revocation Date

Bean, succulent 2.0 11/30/05

Canola, seed 1.0 11/30/08

Cattle, fat 0.05 11/30/08

Cattle, meat 0.05 11/30/08

Cattle, meat byproducts 0.05 11/30/08

Egg 0.05 11/30/08

Goat, fat 0.05 11/30/08

Goat, meat 0.05 11/30/08

Goat, meat byproducts 0.05 11/30/08

Grape, wine 6. 0 None

Hog, fat 0.05 11/30/08

Hog, meat 0.05 11/30/08

Hog, meat byproducts 0.05 11/30/08

Horse, fat 0.05 11/30/08

Horse, meat 0.05 11/30/08

Horse, meat byproducts 0.05 11/30/08

Lettuce, head 10.0 11/30/05

Lettuce, leaf 10.0 11/30/05

Milk 0.05 11/30/08

Poultry, fat 0.1 11/30/08

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Poultry, meat 0.1 11/30/08

Poultry, meat byproducts 0.1 11/30/08

Sheep, fat 0.05 11/30/08

Sheep, meat 0.05 11/30/08

Sheep, meat byproducts 0.05 11/30/08

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

(e) Revoked tolerances subject to the channel of trade provisions. The following table lists commodities with residues 

of vinclozolin resulting from lawful use are subject to the channels of trade provisions of section 408(l)(5) of the FFDCA: 

Commodity Parts per million 

Cucumber 1.0 

Fruit, stone, except plum, prune, fresh 25.0 

Pepper, bell 3.0 

Strawberry 10.0

[62 FR 38474, July 18, 1997, as amended at 63 FR 7308, Feb. 13, 1998; 65 FR 44468, July 18, 2000; 67 FR 40189, June 12, 2002; 

68 FR 56189, Sept. 30, 2003; 68 FR 69323, Dec. 12, 2003; 70 FR 55268, Sept. 21, 2005]

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§180.381 Oxyfluorfen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-

nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food commodities:

Commodity Parts per million

Almond, hulls 0.1

Artichoke, globe 0.05

Avocado 0.05

Banana 0.05

Broccoli 0.05

Cabbage 0.05

Cacao bean, dried bean 0.05

Cattle, fat 0.01

Cattle, meat 0.01

Cattle, meat byproducts 0.01

Cauliflower 0.05

Coffee, bean, green 0.05

Corn, field, grain 0.05

Cotton, undelinted seed 0.05

Date, dried fruit 0.05

Egg 0.03

Feijoa 0.05

Fig 0.05

Fruit, pome, group 11 0.05

Fruit, stone, group 12 0.05

Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.01

Grape 0.05

Hog, fat 0.01

Hog, meat 0.01

Hog, meat byproducts 0.01

Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.01

Horseradish 0.05

Kiwifruit 0.05

Milk 0.01

Nut, tree, group 14 0.05

Olive 0.05

Onion, bulb 0.05

Peppermint, tops 0.05

Persimmon 0.05

Pistachio 0.05

Pomegranate 0.05

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Poultry, fat 0.2

Poultry, meat 0.01

Poultry, meat byproducts 0.01

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.01

Soybean 0.05

Spearmint, tops 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the 

herbicide oxyfluorfen [2-chloro-1-(3-ethoxy-4-nitrophenoxy)-4-(trifluoromethyl)benzene] in or on the following food 

commodities:

Commodity Parts per million

Blackberry 0.05

Chickpea, seed 0.05

Grass, forage 0.05

Grass, hay 0.05

Grass, seed screenings 0.05

Guava 0.05

Papaya 0.05

Raspberry 0.05

Taro, corm 0.05

Taro, leaves 0.05

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 85022, Dec. 24, 1980]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.381, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.383 Sodium salt of acifluorfen; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. Tolerances are established for combined residues of the herbicide sodium salt of acifluorfen, sodium 

5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, and its metabolites (the corresponding acid, methyl ester, and 

amino analogues) in or on the following raw agricultural commodities:

Commodity Parts per million

Peanut 0.1

Rice, grain 0.1

Rice, straw 0.2

Soybean, seed 0.1

Strawberry 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 24877, Apr. 11, 1980, as amended at 46 FR 61272, Dec. 16, 1981; 47 FR 39490, Sept. 8, 1982; 61 FR 30165, June 14, 

1996; 62 FR 39974, July 25, 1997; 67 FR 35048, May 17, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 54434, Sept. 15, 2006]

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§180.384 Mepiquat (N,N-dimethylpiperidinium); tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the plant growth regulator mepiquat 

(N,N-dimethylpiperidinium) in or on the following commodities: 

Commodity Parts per million 

Cattle, meat byproducts 0.1 

Cotton, gin byproducts 6.0 

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Cotton, undelinted seed 2.0 

Goat, meat byproducts 0.1 

Hog, meat byproducts 0.1 

Horse, meat byproducts 0.1 

Sheep, meat byproducts 0.1

(2) Tolerances are established for residues of the plant growth regulator mepiquat chloride (N,N-dimethylpiperidinium 

chloride) in or on the following commodities: 

Commodity Parts per million 

Cattle, fat 0.1 

Cattle, meat 0.1 

Goat, fat 0.1 

Goat, meat 0.1 

Grape 1.0 

Grape, raisin 5.0 

Hog, fat 0.1 

Hog, meat 0.1 

Horse, fat 0.1 

Horse, meat 0.1 

Sheep, fat 0.1 

Sheep, meat 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 3118, Jan. 23, 2002]

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§180.385 Diclofop-methyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide diclofop-methyl (methyl 

2-[4-(2,4-dichlorophenoxy)phenoxy]propanoate) and its metabolites, 2-[4-(2,4-dichlorophenoxy)phenoxy]propanoic acid 

and 2-[4-(2,4-dichloro-5-hydroxyphenoxy)phenoxy]propanoic acid, in or on the following raw agricultural commodities:

Commodity Parts per million

Barley, grain 0.1

Barley, straw 0.1

Wheat, grain 0.1

Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 23425, Apr. 7, 1980, as amended at 50 FR 20211, May 15, 1985; 51 FR 3599, Jan. 29, 1986; 51 FR 19176, May 28, 1986; 

63 FR 57077, Oct. 26, 1998; 72 FR 41931, Aug. 1, 2007]

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§§180.388-180.389 [Reserved]

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§180.390 Tebuthiuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide tebuthiuron 

(N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(2-hydroxy-1,1-dimethylethyl)

-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, and 

N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural 

commodities:

Commodity Parts per million

Grass, forage 10.0

Grass, hay 10.0

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(2) Tolerances are established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)

-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, 

N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 2-dimethylethyl-5-amino-1,3,4-thiadiazole, and N-(5-(1,1-dimethylethyl)

-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity Parts per million

Cattle, fat 1.0

Cattle, meat 1.0

Cattle, meat byproducts 5.0

Goat, fat 1.0

Goat, meat 1.0

Goat, meat byproducts 5.0

Horse, fat 1.0

Horse, meat 1.0

Horse, meat byproducts 5.0

Sheep, fat 1.0

Sheep, meat 1.0

Sheep, meat byproducts 5.0

(3) A tolerance is established for the combined residues of the herbicide tebuthiuron (N-(5-(1,1-dimethylethyl)

-1,3,4-thiadiazol-2-yl)-N,N'-dimethylurea) and its metabolites N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, 

N-(5-(2-hydroxy-1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N-methylurea, N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)urea, 

N-(5-(1,1-dimethylethyl)-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea, and N-(5-(2-hydroxy-1,1-dimethylethyl)

-1,3,4-thiadiazol-2-yl)-N'-hydroxymethyl-N-methylurea in or on the following raw agricultural commodities:

Commodity Parts per million

Milk 0.8

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 53461, Sept. 19, 2007]

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§180.395 Hydramethylnon; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide tetrahydro-5,5-dimethyl-2(1H)-pyrimidinone

(3-(4-(trifluoromethyl)phenyl)-1-(2-(4-(trifluoromethyl)phenyl)ethenyl)-2-propenylidene)hydrazone in or on the following raw 

agricultural commodities:

Commodity Parts per million

Grass, forage 2.0

Grass, hay 2.0

Pineapple 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[45 FR 55198, Aug. 19, 1980, as amended at 63 FR 10543, Mar. 4, 1998; 63 FR 65073, Nov. 25, 1998; 66 FR 28672, May 24, 2001; 

68 FR 37764, June 25, 2003; 68 FR 48312, Aug. 13, 2003; 72 FR 41931, Aug. 1, 2007]

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§180.396 Hexazinone; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)

-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the 

following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the 

sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its plant metabolites: 

metabolite A, 3-(4-hydroxycyclohexyl)-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite B, 

3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)

-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite D, 3-cyclohexyl-1-methyl-1,3,5-triazine-2,4,6-(1H, 

3H, 5H)-trione, and metabolite E, 3-(4-hydroxycyclohexyl)-1-methyl-1,3,5-triazine-2,4,6-(1H, 3H, 5H)-trione, calculated as 

the stoichiometric equivalent of hexazinone, in or on the commodity.

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Commodity Parts per million

Alfalfa, forage 2.0

Alfalfa, hay 4.0

Alfalfa, seed 2.0

Blueberry 0.6

Grass, forage 250

Grass, hay 230

Pineapple 0.6

Sugarcane, cane 0.6

Sugarcane, molasses 4.0

(2) Tolerances are established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-

methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodities in the 

following table. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the 

sum of hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its animal tissue 

metabolites: metabolite B, 3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 

3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, calculated as the stoichiometric equivalent of 

hexazinone, in or on the commodity.

Commodity Parts per million

Cattle, fat 0.1

Cattle, meat 0.5

Cattle, meat byproducts 4.0

Goat, fat 0.1

Goat, meat 0.5

Goat, meat byproducts 4.0

Hog, fat 0.1

Hog, meat 0.5

Hog, meat byproducts 4.0

Horse, fat 0.1

Horse, meat 0.5

Horse, meat byproducts 4.0

Sheep, fat 0.1

Sheep, meat 0.5

Sheep, meat byproducts 4.0

(3) A tolerance is established for residues of the herbicide hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-

methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, including its metabolites and degradates, in or on the commodity in the following 

table. Compliance with the tolerance level specified in this paragraph is to be determined by measuring only the sum of 

hexazinone, 3-cyclohexyl-6-(dimethylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and its metabolites: metabolite B, 

3-cyclohexyl-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C, 3-(4-hydroxycyclohexyl)

-6-(methylamino)-1-methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, metabolite C-2, 3-(3-hydroxycyclohexyl)-6-(methylamino)-1-

methyl-1,3,5-triazine-2,4-(1H, 3H)-dione, and metabolite F, 3-cyclohexyl-6-amino-1-methyl-1,3,5-triazine-2,4-(1H, 3H)

-dione, calculated as the stoichiometric equivalent of hexazinone, in or on the commodity.

Commodity Parts per million

Milk 11

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33713, May 24, 2000, as amended at 71 FR 56399, Sept. 27, 2006; 75 FR 60244, Sept. 29, 2010]

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§180.399 Iprodione; tolerances for residues.

Link to an amendment published at 80 FR 72598, November 20, 2015.

(a) General. (1) Tolerances are established for the combined residues of the fungicide iprodione 

[3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-imidazolidinecarboxamide], its isomer 3-(1-methylethyl)

-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide, and its metabolite 3-(3,5-dichlorophenyl)-2,4-dioxo-1-

imidazolidine-carboxamide in or on the following food commodities:

Commodity Parts per million

Almond, hulls 2.0

Almond 0.3

Apricot 20.0

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Bean, dry, seed 2.0

Bean, forage 90.0

Bean, succulent 2.0

Blueberry 15.0

Boysenberry 15.0

Broccoli 25.0

Caneberry subgroup 13A 25.0

Carrot, roots 5.0

Cherry, sweet, postharvest 20.0

Cherry, tart 20.0

Cotton, undelinted seed 0.10

Cowpea, hay 90.0

Currant 15.0

Garlic 0.1

Ginseng 2.0

Ginseng, dried root 4.0

Grape 60.0

Grape, raisin 300

Kiwifruit 10.0

Lettuce 25.0

Nectarine, postharvest 20.0

Onion, bulb 0.5

Peach, postharvest 20.0

Peanut 0.5

Peanut, hay 150.0

Plum, postharvest 20.0

Plum, prune 20.0

Potato 0.5

Raspberry 15.0

Rice, bran 30.0

Rice, grain 10.0

Rice, hulls 50.0

Rice, straw 20.0

Strawberry 15.0

(2) Tolerances are established for the combined residues of iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)

-2,4-dioxo-1-imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-

imidazolidinecarboxamide, and its metabolites [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidine-carboxamide] and 

[N-(3,5-dichloro-4-hydroxyphenyl)-ureido-carboxamide], all expressed as iprodione equivalents in or on the following food 

commodities of animal origin:

Commodity Parts per million

Cattle, fat 0.5

Cattle, kidney 3.0

Cattle, liver 3.0

Cattle, meat 0.5

Cattle, meat byproducts, except kidney and liver 0.5

Egg 1.5

Goat, fat 0.5

Goat, kidney 3.0

Goat, liver 3.0

Goat, meat 0.5

Goat, meat byproducts, except kidney and liver 0.5

Hog, fat 0.5

Hog, kidney 3.0

Hog, liver 3.0

Hog, meat 0.5

Hog, meat byproducts, except kidney and liver 0.5

Horse, fat 0.5

Horse, kidney 3.0

Horse, liver 3.0

Horse, meat 0.5

Horse, meat byproducts, except kidney and liver 0.5

Milk 0.5

Poultry, fat 3.5

Poultry, liver 5.0

Poultry, meat 1.0

Poultry, meat byproducts, except liver 1.0

Sheep, fat 0.5

Sheep, kidney 3.0

Sheep, liver 3.0

Sheep, meat 0.5

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Sheep, meat byproducts, except kidney and liver 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for the combined residues of the fungicide iprodione [3-(3,5-dichlorophenyl)-N-(1-methylethyl)-2,4-dioxo-1-

imidazolidinecarboxamide], its isomer [3-(1-methylethyl)-N-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide], 

and its metabolite [3-(3,5-dichlorophenyl)-2,4-dioxo-1-imidazolidinecarboxamide] in or on the following food commodity:

Commodity Parts per million

Mustard greens 15.0

(d) Indirect or inadvertent residues. [Reserved]

[48 FR 40385, Sept. 7, 1983]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.399, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.401 Thiobencarb; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for the combined residues of the herbicide thiobencarb (S-[(4-chlorophenyl)

methyl]diethyl-carbamothioate) and its chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following 

raw agricultural commodities:

Commodity Part per million

Cattle, fat 0.2

Cattle, meat byproducts 0.2

Cattle, meat 0.2

Egg 0.2

Goat, fat 0.2

Goat, meat byproducts 0.2

Goat, meat 0.2

Hog, fat 0.2

Hog, meat byproducts 0.2

Hog, meat 0.2

Horse, fat 0.2

Horse, meat byproducts 0.2

Horse, meat 0.2

Milk 0.05

Poultry, fat 0.2

Poultry, meat byproducts 0.2

Poultry, meat 0.2

Rice, grain 0.2

Rice, straw 1.0

Sheep, fat 0.2

Sheep, meat byproducts 0.2

Sheep, meat 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the herbicide thiobencarb (S-[(4-chloro-phenyl)methyl]diethylcarbamothioate) and its 

chlorobenzyl and chlorophenyl moiety-containing metabolites in or on the following raw agricultural commodities:

Commodity Parts per million

Celery 0.2

Endive 0.2

Lettuce 0.2

(d) Indirect or inadvertent residues. [Reserved]

[47 FR 6833, Feb. 17, 1982, as amended at 56 FR 2440, Jan. 23, 1991; 76 FR 34885, June 15, 2011]

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§180.403 Thidiazuron; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the defoliant thidiazuron (N-phenylN-1,2,3-thiadiazol-5-ylurea) and its aniline containing metabolites in or on the following food commodities: 

Commodity Parts per million

Cattle, fat 0.4

Cattle, meat 0.4

Cattle, meat byproducts 0.4

Cotton, gin byproducts 24.0

Cotton, undelinted seed 0.3

Goat, fat 0.4

Goat, meat 0.4

Goat, meat byproducts 0.4

Hog, fat 0.4

Hog, meat 0.4

Hog, meat byproducts 0.4

Horse, fat 0.4

Horse, meat 0.4

Horse, meat byproducts 0.4

Milk 0.05

Sheep, fat 0.4

Sheep, meat 0.4

Sheep, meat byproducts 0.4

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33700, May 24, 2000, as amended at 72 FR 53462, Sept. 19, 2007]

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§180.404 Profenofos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide profenofos (O-(4-bromo-2-chlorophenyl)-Oethyl-S-propyl phosphorothioate) in or on the following food commodities:

Commodity Parts per million

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Cotton, gin byproducts 55.0

Cotton, undelinted seed 2.0

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 0.05

Horse, fat 0.05

Horse, meat 0.05

Horse, meat byproducts 0.05

Milk 0.01

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33700, May 24, 2000, as amended at 66 FR 50833, Oct. 5, 2001; 67 FR 49617, July 31, 2002; 72 FR 54579, Sept. 26, 2007]

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§180.405 Chlorsulfuron; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-

methyl-1,3,5-triazin-2-yl)aminocarbonyl]benzenesulfonamide) and its metabolite, 2-chloro-5-hydroxy-N-[(4-methoxy-6-

methyl-1,3,5-triazin-2-yl)aminocarbonyl] benzenesulfonamide in or on the following raw agricultural commodities: 

Commodity Parts per million 

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Barley, grain 0.1

Barley, straw 0.5

Oat, forage 20.0

Oat, grain 0.1

Oat, straw 0.5

Wheat, forage 20.0

Wheat, grain 0.1

Wheat, straw 0.5

(2) Tolerances are established for residues of chlorsulfuron (2-chloro-N-[(4-methoxy-6-methyl-1,3,5-triazin-2- yl)

aminocarbonyl] benzenesulfonamide) in or on the following raw agricultural commodities. 

Commodity Parts per million 

Cattle, fat 0.3

Cattle, meat 0.3

Cattle, meat byproducts 0.3

Goat, fat 0.3

Goat, meat 0.3

Goat, meat byproducts 0.3

Grass, forage 11.0

Grass, hay 19.0

Hog, fat 0.3

Hog, meat 0.3

Hog, meat byproducts 0.3

Horse, fat 0.3

Horse, meat 0.3

Horse, meat byproducts 0.3

Milk 0.1

Sheep, fat 0.3

Sheep, meat 0.3

Sheep, meat byproducts 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 52873, Aug. 14, 2002]

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§180.407 Thiodicarb; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide thiodicarb (dimethyl N,N′-[thiobis

[[(methylimino)carbonyloxy]] bis[ethanimidothioate]) and its metabolite methomyl (S-methyl 

N-[(methylcarbamoyl) oxy]thioacetimidate) in or on the following food commodities or groups. The time-limited 

tolerances expire and are revoked on the dates listed in the following table: 

Commodity Parts per million Expiration/revocation date 

Broccoli 7.0 None 

Cabbage 7.0 None 

Cauliflower 7.0 None 

Corn, sweet, kernel plus cob with husks removed 2.0 None 

Cotton, undelinted seed 0.4 None 

Soybean, hulls 0.8 None 

Soybean 0.2 None

Vegetable, leafy, except brassica, group 4 35 None

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[62 FR 44595, Aug. 22, 1997, as amended at 75 FR 60245, Sept. 29, 2010]

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§180.408 Metalaxyl; tolerances for residues.

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(a) General. Tolerances are established for the combined residues of the fungicide metalaxyl [N-(2,6-dmethylphyenyl)

-N-(methoxyacetyl) alanine methylester] and its metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy 

methyl-6-methylphenyl)-N-(methoxyacetyl)-alanine methyl ester, each expressed as metalaxyl equivalents, in or on the 

following food commodities: 

Commodity Parts per million 

Alfalfa, forage 6.0 

Alfalfa, hay 20.0 

Almond 0.5 

Almond, hulls 10.0 

Apple 0.2 

Apple, wet pomace 0.4 

Apricot, dried 4.0 

Asparagus 7.0 

Avocado 4.0 

Beet, garden, roots 0.1 

Beet, garden, tops 0.1 

Beet, sugar 0.1 

Beet, sugar, molasses 1.0 

Beet, sugar, roots 0.5 

Beet, sugar, tops 10.0 

Blueberry 2.0 

Broccoli 2.0 

Brussels sprouts 2.0 

Cabbage 1.0 

Cattle, fat 0.4 

Cattle, kidney 0.4 

Cattle, liver 0.4 

Cattle, meat 0.05 

Cattle, meat byproducts, except kidney and liver 0.05 

Cauliflower 1.0 

Citrus, oil 7.0 

Citrus, dried pulp 7.0 

Clover, forage 1.0 

Clover, hay 2.5 

Cotton, undelinted seed 0.1 

Cranberry 4.0 

Egg 0.05 

Fruit, citrus 1.0 

Fruit, stone, group 12 1.0 

Ginseng 3.0 

Goat, fat 0.4 

Goat, kidney 0.4 

Goat, liver 0.4 

Goat, meat 0.05 

Goat, meat byproducts, except kidney and liver 0.05 

Grain, cereal, group 15, except barley, oat and wheat 0.1

Grain, crop 0.1 

Grape 2.0 

Grape, raisin 6.0 

Grass, forage 10.0 

Grass, hay 25.0 

Hog, fat 0.4 

Hog, kidney 0.4 

Hog, liver 0.4 

Hog, meat 0.05 

Hog, meat byproducts, except kidney and liver 0.05 

Hop, dried cones 20 

Hop, vines 2.0 

Horse, fat 0.4 

Horse, kidney 0.4 

Horse, liver 0.4 

Horse, meat 0.05 

Horse, meat byproducts, except kidney and liver 0.05 

Lettuce, head 5.0 

Milk 0.02 

Mustard greens 5.0 

Onion, bulb 3.0 

Onion, green 10.0 

Peanut 0.2 

Peanut, hay 20.0 

Peanut, meal 1.0 

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Peanut, hulls 2.0 

Pineapple 0.1 

Pineapple, fodder 0.1 

Pineapple, forage 0.1 

Plum, prune, dried 4.0 

Potato, chips 4.0 

Potato, granules, flakes 4.0 

Potato, processed potato waste 4.0 

Potato, wet peel 4.0 

Poultry, fat 0.4 

Poultry, kidney 0.4 

Poultry, liver 0.4 

Poultry, meat 0.05 

Poultry, meat byproducts, except kidney and liver 0.05 

Potato 0.5 

Raspberry 0.5 

Sheep, fat 0.4 

Sheep, kidney 0.4 

Sheep, liver 0.4 

Sheep, meat 0.05 

Sheep, meat byproducts, except kidney and liver 0.05 

Soybean, hulls 2.0 

Soybean, meal 2.0 

Soybean, seed 1.0 

Spinach 10.0 

Strawberry 10.0 

Sunflower, seed 0.1 

Sunflower, forage 0.1 

Tomato, paste 3.0

Tomato, puree 3.0

Vegetable, brassica, leafy, group 5, except broccoli, cabbage, cauliflower, brussels sprouts, and mustard greens 0.1 

Vegetable, cucurbit, group 9 1.0 

Vegetable, foilage of legume, group 7 8.0 

Vegetable, fruiting, group 8 1.0 

Vegetable, leafy, except brassica, group 4, except spinach 5.0 

Vegetable, leaves of root and tuber, group 2 15.0 

Vegetable, legume, cannery waste 5.0 

Vegetable, legume, group 6 0.2 

Vegetable, root and tuber, group 1 0.5 

Walnut 0.5

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration (refer to §180.1(m)) are established for 

the combined residues of the fungicide metalaxyl [N-(2,6-dimethylphenyl)-N-(methoxyacetyl) alanine methyl ester] and its 

metabolites containing the 2,6-dimethylaniline moiety, and N-(2-hydroxy methyl-6-methyl)-N-(methoxyacetyl)-alanine 

methylester, each expressed as metalaxyl, in or on the following raw agricultural commodity: 

Commodity Parts per million 

Papaya 0.1

(d) Indirect or inadvertent tolerances. Tolerances are established for indirect or inadvertent residues of metalaxyl in or 

on the food commodities when present therein as a result of the application of metalaxyl to growing crops listed in 

paragraph (a) of this section and other non-food crops to read as follows: 

Commodity Part per million 

Barley, bran 1.0 

Barley, flour 1.0 

Barley, grain 0.2 

Barley, pearled barley 1.0 

Barley, straw 2.0 

Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; forage 1.0 

Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; stover 1.0 

Grain, cereal, forage, fodder and straw, group 16, except barley, oat, and wheat; straw 1.0 

Oat, flour 1.0 

Oat, forage 2.0 

Oat, grain 0.2 

Oat, groats, rolled oats 1.0 

Oat, straw 2.0 

Wheat, bran 1.0 

Wheat, flour 1.0 

Wheat, forage 2.0 

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Wheat, germ 1.0 

Wheat, grain 0.2 

Wheat, middlings 1.0 

Wheat, shorts 1.0 

Wheat, straw 2.0

[65 FR 33700, May 24, 2000, as amended at 72 FR 35666, June 29, 2007; 74 FR 46374, Sept. 9, 2009; 75 FR 56015, Sept. 15, 

2010]

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§180.409 Pirimiphos-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide pirimiphos-methyl (O-(2-diethylamino-6-methyl4-pyrimidinyl) O,O-dimethyl phosphorothioate) in or on the following raw agricultural commodities:

Commodity Parts per million

Cattle, fat 0.02

Cattle, meat byproducts 0.02

Corn, field, grain 8.0

Corn, pop, grain 8.0

Goat, fat 0.02

Goat, meat byproducts 0.02

Grain, aspirated fractions 20.0

Hog, fat 0.02

Hog, meat byproducts 0.02

Horse, fat 0.02

Horse, meat byproducts 0.02

Poultry, fat 0.02

Sheep, fat 0.02

Sheep, meat byproducts 0.02

Sorghum, grain, grain 8.0

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33714, May 24, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 49617, July 31, 2002; 70 FR 44492, Aug. 3, 2005; 

72 FR 53462, Sept. 19, 2007]

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§180.410 Triadimefon; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide triadimefon, 1-(4-chlorophenoxy)

-3,3-dimethyl-1-(1H-1,2,4-triazol-1-yl)-2-butanone, and triadimenol, β-(4-chlorophenoxy)-α-(1,1-dimethylethyl)

-1H-1,2,4-triazole-1-ethanol, expressed as triadimefon, in or on the following food commodities:

Commodity Parts per million Expiration/Revocation Date 

Pineapple 2.0 None

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54962, Sept. 24, 2008, as amended at 76 FR 34885, June 15, 2011]

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§180.411 Fluazifop-P-butyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fluazifop-P-butyl, including its metabolites and 

degradates, in or on the following commodities in the table. Compliance with the tolerance levels specified in the table 

below is to be determined by measuring only the sum of fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]

phenoxy]propanoate, and the free and conjugated forms of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-

pyridinyl]oxy]phenoxy]propanoic acid, calculated as the stoichiometric equivalent of fluazifop, in or on the commodity.

Commodity Parts per million

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Banana 0.01

Beans, dry, seed 50

Beet, sugar, dried pulp 1.0

Beet, sugar, molasses 3.5

Beet, sugar, roots 0.25

Carrot, roots 2.0

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Citrus, dried pulp 0.40

Citrus, juice 0.06

Citrus, oil 30.0

Cotton, gin byproducts 1.5

Cotton, refined oil 1.3

Cotton, undelinted seed 1.0

Egg 0.05

Endive 6.0

Fruit, citrus, group 10 0.03

Fruit, stone 0.05

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 0.05

Grape 0.01

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.05

Horse, meat 0.05

Horse, meat byproducts 0.05

Milk 0.05

Nut, macadamia 0.1

Onion, bulb 0.5

Peanut 1.5

Peanut, meal 2.2

Pecans 0.05

Poultry, fat 0.05

Poultry, meat 0.05

Poultry, meat byproducts 0.05

Potato1 1.0

Potato, chips1 2.0

Potato, granules/flakes1 4.0

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.05

Soybean, seed 2.5

Sweet potato, roots 1.5

1

No U.S. registrations.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

herbicide fluazifop-P-butyl, including its metabolites and degradates, in or on the following commodities in the table. 

Compliance with the tolerance levels specified in the table below is to be determined by measuring only the sum of 

fluazifop-P-butyl, butyl(R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoate, and the free and conjugated forms 

of the resolved isomer of fluazifop, (R)-2-[4-[[5-(trifluoromethyl)-2-pyridinyl]oxy]phenoxy]propanoic acid, calculated as the 

stoichiometric equivalent of fluazifop, in or on the commodity.

Commodity Parts per million

Asparagus 3.0

Coffee, bean 0.1

Pepper, tabasco 1.0

Rhubarb 0.5

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33714, May 24, 2000, as amended at 74 FR 9372, Mar. 4, 2009; 74 FR 46374, Sept. 9, 2009; 74 FR 47457, Sept. 16, 2009; 

76 FR 5703, Feb. 2, 2011; 76 FR 59908, Sept. 28, 2011; 80 FR 46822, Aug. 6, 2015]

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§180.412 Sethoxydim; tolerances for residues.

(a) Tolerances are established for the herbicide sethoxydim, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one (CAS Reg. No. 

74051-80-2) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the stoichiometric equivalent of 

sethoxydim, in or on the commodity.

Commodity

Parts per

million

Alfalfa, forage 40

Alfalfa, hay 40

Almond, hulls 2.0

Apricot 0.2

Apple, wet pomace 0.8

Asparagus 4.0

Bean, succulent 15

Beet, sugar, molasses 10

Beet, sugar, tops 3.0

Berry, low growing, subgroup 13-07H, except strawberry 2.5

Borage, meal 40

Buckwheat, flour 25

Buckwheat, grain 19

Bushberry subgroup 13-07B 4.0

Calendula, meal 20

Caneberry subgroup 13-07A 5.0

Canola, meal 40

Castor oil plant, meal 20

Cattle, fat 0.2

Cattle, meat 0.2

Cattle, meat byproducts 1.0

Cherry, sweet 0.2

Cherry, tart 0.2

Chinese tallowtree, meal 20

Citrus, dried pulp 1.5

Clover, forage 35

Clover, hay 55

Coriander, leaves 4.0

Corn, field, forage 2.0

Corn, field, grain 0.5

Corn, field, stover 2.5

Corn, sweet, forage 3.0

Corn, sweet, kernel plus cob with husk removed 0.4

Corn, sweet, stover 3.5

Cottonseed subgroup 20C 5.0

Cowpea, forage 15

Cowpea, hay 50

Crambe, meal 40

Cuphea, meal 40

Dillweed, fresh leaves 10

Echium, meal 40

Egg 2.0

Euphorbia, meal 20

Evening primrose, meal 20

Flax seed, meal 40

Fruit, citrus, group 10-10 0.5

Fruit, pome, group 11-10 0.2

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0

Goat, fat 0.2

Goat, meat 0.2

Goat, meat byproducts 1.0

Gold of pleasure, meal 40

Grape, raisin 2.0

Hare's ear mustard, meal 40

Hog, fat 0.2

Hog, meat 0.2

Hog, meat byproducts 1.0

Horse, fat 0.2

Horse, meat 0.2

Horse, meat byproducts 1.0

Jojoba, meal 20

Juneberry1 5.0

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Lesquerella, meal 40

Lingonberry1 5.0

Lunaria, meal 40

Meadowfoam, meal 40

Milk 0.5

Milkweed, meal 40

Mustard, meal 40

Nectarine 0.2

Niger seed, meal 20

Nut, tree, group 14 0.2

Oil radish, meal 40

Pea and bean, dried shelled, except soybean, subgroup 6C 25

Pea, field, hay 40

Pea, field, vines 20

Pea, succulent 10

Peach 0.2

Peanut 25

Peppermint, tops 30

Pistachio 0.2

Poppy seed, meal 40

Potato granules/flakes 8.0

Potato waste, processed 8.0

Poultry, fat 0.2

Poultry, meat 0.2

Poultry, meat byproducts 2.0

Radish, tops 4.5

Rapeseed, meal 40

Rapeseed subgroup 20A 35

Rose hip, meal 20

Safflower, seed 15

Salal1 5.0

Sesame, meal 40

Sheep, fat 0.2

Sheep, meat 0.2

Sheep, meat byproducts 1.0

Soybean, hay 10

Soybean, seed 16

Spearmint, tops 30

Strawberry 10

Stokes aster, meal 20

Sunflower, meal 20

Sunflower subgroup 20B, except safflower 7.0

Sweet rocket, meal 40

Tallowwood, meal 20

Tea oil plant, meal 20

Turnip, tops 5.0

Vegetable, brassica, leafy, group 5 5.0

Vegetable, bulb, group 3-07 1.0

Vegetable, cucurbit, group 9 4.0

Vegetable, fruiting, group 8-10 4.0

Vegetable, leafy, except brassica, group 4 4.0

Vegetable, root and tuber, group 1 4.0

Vernonia, meal 20

1

The individual tolerances for Juneberry, Lingonberry, and Salal expire on December 15, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. Tolerances are established for the herbicide sethoxydim, including its 

metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring only the sum of the herbicide 2-[1-(ethoxyimino)butyl]-5-[2-(ethylthio)propyl]-3-

hydroxy-2-cyclohexen-1-one) and its metabolites containing the 2-cyclohexen-1-one moiety, calculated as the 

stoichiometric equivalent of sethoxydim, in or on the commodity.

Commodity

Parts per

million

Artichoke, globe 5.0

Fescue, forage 7.0

Fescue, hay 4.0

Rhubarb 0.3

(d) Indirect and inadvertent residues. [Reserved]

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[80 FR 34077, June 15, 2015]

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§180.413 Imazalil; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the fungicide imazalil, 

1-[2-(2,4-dichlorophenyl)-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolite, 1-(2,4-dichlorophenyl)-2-(1H-imidazole1-yl)-1-ethanol, in or on the following food commodities:

Commodity Parts per million

Banana 3.0

Barley, grain 0.1

Barley, hay 0.5

Barley, straw 0.5

Citrus, dried pulp 25.0

Citrus, oil 200.0

Fruit, citrus, postharvest 10.0

Wheat, forage 0.5

Wheat, grain 0.1

Wheat, hay 0.5

Wheat, straw 0.5

(2) Tolerances are established for the combined residues of the fungicide imazalil, 1-[2-(2,4-dichlorophenyl)

-2-(2-propenyloxy)ethyl]-1H-imidazole, and its metabolites, 3-[2-(2,4-dichlorophenyl)-2-(2,3-dihydroxypropoxy)ethyl]

-2,4-imidazolidinedione (FK772) and 3-[2-(2,4-dichlorophenyl)-2-(hydroxy)]-2,4-imidazolidinedione (FK284), in or on the 

following food commodities:

Commodity Parts per million

Cattle, fat 0.01

Cattle, meat 0.01

Cattle, meat byproducts 0.2

Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.2

Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.2

Milk 0.02

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.2

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33715, May 24, 2000, as amended at 67 FR 46893, July 17, 2002; 71 FR 54434, Sept. 15, 2006]

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§180.414 Cyromazine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide cyromazine, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only cyromazine, N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the 

commodity.

Commodity Parts per million 

Bean, dry, except cowpea 3.0

Bean, lima 1.0

Bean, succulent 2.0

Broccoli 1.0

Cabbage, abyssinian 10.0

Cabbage, seakale 10.0

Cattle, fat 0.05 

Cattle, kidney 0.2

Cattle, meat 0.05 

Cattle, meat byproducts, except kidney 0.05

Egg 0.25 

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Garlic 0.2

Garlic, great-headed, bulb 0.2

Goat, fat 0.05 

Goat, kidney 0.2

Goat, meat 0.05 

Goat, meat byproducts, except kidney 0.05

Hanover salad, leaves 10.0

Hog, fat 0.05 

Hog, kidney 0.2

Hog, meat 0.05 

Hog, meat byproducts, except kidney 0.05

Horse, fat 0.05 

Horse, kidney 0.2

Horse, meat 0.05

Horse, meat byproducts, except kidney 0.05

Leek 3.0

Mango1 0.3 

Milk 0.05 

Mushroom 1.0 

Onion, bulb 0.2

Onion, green 3.0

Onion, potato 3.0

Onion, tree 3.0

Onion, welsh 3.0

Pepper 1.0 

Potato 0.8 

Poultry, fat (from chicken layer hens and chicken breeder hens only) 0.05 

Poultry, meat (from chicken layer hens and chicken breeder hens only) 0.05 

Poultry, meat byproducts (from chicken layer hens and chicken breeder hens only) 0.05 

Rakkyo, bulb 0.2

Shallot, bulb 0.2

Shallot, fresh leaves 3.0

Sheep, fat 0.05 

Sheep, kidney 0.2

Sheep, meat 0.05 

Sheep, meat byproducts, except kidney 0.05

Tomato 0.5 

Turnip, greens 10.0

Vegetable, brassica, leafy, group 5, except broccoli 10.0

Vegetable, leafy, except brassica, group 4 7.0 

Vegetable, cucurbit, group 9 1.0 

1

There are no U.S. registrations on mango as of May 4, 2000.

(2) A tolerance of 5.0 parts per million is established for residues of the insecticide cyromazine, including its 

metabolites and degradates, in or on poultry feed when used as a feed additive only in feed for chicken layer hens and 

chicken breeder hens at the rate of not more than 0.01 pound of cyromazine per ton of poultry feed for control of flies in 

manure of treated chicken layer hens and chicken breeder hens, provided the feeding of cyromazine-treated feed must 

stop at least 3 days (72 hours) before slaughter. If the feed is formulated by any person other than the end user, the 

formulator must inform the end user, in writing, of the 3-day (72 hours) pre-slaughter interval. Compliance with the 

tolerance level specified in this paragraph is to be determined by measuring only cyromazine, 

N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide 

cyromazine, including its metabolites and degradates, in or on the commodities in the table in this paragraph when present 

therein as a result of the application of cyromazine to growing crops listed in paragraph (a)(1) of this section. Compliance 

with the tolerance levels specified in this paragraph is to be determined by measuring only cyromazine, 

N-cyclopropyl-1,3,5-triazine-2,4,6-triamine, in or on the commodity.

Commodity Parts per million 

Cotton, undelinted seed 0.1 

Corn, sweet, kernel plus cob with husks removed 0.5 

Corn, sweet, forage 0.5 

Corn, sweet, stover 0.5 

Radish, roots 0.5 

Radish, tops 0.5

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[65 FR 25860, May 4, 2000, as amended at 67 FR 72593, Dec. 6, 2002; 68 FR 55269, Sept. 24, 2003; 75 FR 22256, Apr. 28, 2010; 

76 FR 23494, Apr. 27, 2011]

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§180.415 Aluminum tris (O-ethylphosphonate); tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its 

metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels 

specified in this paragraph is to be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the 

commodity.

Commodity Parts per million

Avocado 25

Banana 3.0

Bushberry subgroup 13B 40

Caneberry subgroup 13A 0.1

Cranberry 0.5

Fruit, citrus, group 10 5.0

Fruit, pome, group 11 10

Ginseng 0.1

Hop, dried cones 45

Juneberry 40

Lingonberry 40

Nut, macadamia 0.20

Onion, bulb 0.5

Onion, green 10.0

Pea, succulent 0.3

Pepper/eggplant, subgroup 8-10B1 0.01

Pineapple 0.1

Salal 40

Strawberry 75

Tomato 3

Turnip, greens 40

Turnip, roots 15

Vegetable, brassica, leafy, group 5 60

Vegetable, cucurbit, group 9 15

Vegetable, leafy, except brassica, group 4 100

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the fungicide aluminum tris (O-ethylphosphonate), including its metabolites and degradates, in 

or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to 

be determined by measuring only aluminum tris (O-ethylphosphonate), in or on the commodity.

Commodity Parts per million

Asparagus 0.1

Grape 10

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 36801, July 8, 1999, as amended at 64 FR 37875, July 14, 1999; 65 FR 50438, Aug. 18, 2000; 67 FR 55346, Aug. 29, 2002; 

68 FR 11335, Mar. 10, 2003; 70 FR 7047, Feb. 10, 2005; 76 FR 23494, Apr. 27, 2011; 80 FR 2320, Jan. 16, 2015]

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§180.416 Ethalfluralin; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide ethalfluralin, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only the residues of ethalfluralin, N-ethyl-N-(2-methyl-2-propenyl)-2,6-dinitro4-(trifluoromethyl)benzenamine.

Commodity Parts per million

Bean, dry, seed 0.05

Dill, dried leaves 0.05

Dill, fresh leaves 0.05

Peanut 0.05

Pea, dry, seed 0.05

Potato 0.05

Rapeseed subgroup 20A 0.05

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Soybean 0.05

Sunflower subgroup 20B 0.05

Vegetable, cucurbit, group 9 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[49 FR 391, Jan. 4, 1984, as amended at 50 FR 4976, Feb. 5, 1985; 52 FR 11262, Apr. 8, 1987; 62 FR 66014, Dec. 17, 1997; 64 FR 

5191, Feb. 3, 1999; 64 FR 54782, Oct. 8, 1999; 66 FR 37598, July 19, 2001; 66 FR 41454, Aug. 8, 2001; 67 FR 2342, Jan. 17, 

2002; 67 FR 49617, July 31, 2002; 72 FR 68534, Dec. 5, 2007; 78 FR 40020, July 3, 2013]

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§180.417 Triclopyr; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances for residues of the herbicide triclopyr per se, as a result of the application/use of 

butoxyethyl ester of triclopyr and triethyylamine salt of triclopyr, are established in or on the following raw agricultural 

commodities:

Commodity Parts per million

Egg 0.05

Fish 3.0

Grass, forage 700.0

Grass, hay 200.0

Milk 0.01

Poultry, fat 0.1

Poultry, meat 0.1

Poultry, meat byproducts, except kidney 0.1

Rice, grain 0.3

Rice, straw 10.0

Shellfish 3.5

(2) Tolerances for the combined residues of the herbicide triclopyr ((3,5,6-trichloro-2-pyridinyl)oxy) acetic acid and its 

metabolite 3,5,6-trichloro-2-pyridinol (TCP), as a result of the application/use of butoxyethyl ester of triclopyr or the 

triethylamine salt of triclopyr, are established in or on the following raw agricultural commodities:

Commodity Parts per million

Cattle, fat 0.05

Cattle, kidney 0.5

Cattle, liver 0.5

Cattle, meat 0.05

Cattle, meat byproducts, except kidney and liver 0.05

Goat, fat 0.05

Goat, kidney 0.5

Goat, liver 0.5

Goat, meat 0.05

Goat, meat byproducts, except kidney and liver 0.05

Hog, fat 0.05

Hog, kidney 0.5

Hog, liver 0.5

Hog, meat 0.05

Hog, meat byproducts, except kidney and liver 0.05

Horse, fat 0.05

Horse, kidney 0.5

Horse, liver 0.5

Horse, meat 0.05

Horse, meat byproducts, except kidney and liver 0.05

Sheep, fat 0.05

Sheep, kidney 0.5

Sheep, liver 0.5

Sheep, meat 0.05

Sheep, meat byproducts, except kidney and liver 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

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(d) Indirect or inadvertent residues. [Reserved] 

[50 FR 18486, May 1, 1985, as amended at 55 FR 26440, June 28, 1990; 60 FR 4095, Jan. 20, 1995; 62 FR 46894, Sept. 5, 1997; 

63 FR 45406, Aug. 26, 1998; 67 FR 35048, May 17, 2002; 67 FR 58725, Sept. 18, 2002; 72 FR 41931, Aug. 1, 2007]

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§180.418 Cypermethrin and isomers alpha-cypermethrin and zeta-cypermethrin; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the insecticide cypermethrin (±)alpha 

cyano-(3-phenoxyphenyl)methyl(±)cis,trans-3(2,2-dichloroethenyl-2,2-dimethylcyclopropanecarboxylate in or on the 

following commodities:

Commodity Parts per million

Brassica, head and stem, subgroup 5A 2.0

Brassica, leafy greens, subgroup 5B 14.0

Cattle, fat 1.0

Cattle, meat 0.2

Cattle, meat byproducts 0.05

Cotton, gin byproducts 11.0

Cotton, undelinted seed 0.5

Egg 0.05

Goat, fat 1.0

Goat, meat 0.2

Goat, meat byproducts 0.05

Hog, fat 0.1

Hog, meat 0.05

Horse, fat 1.0

Horse, meat 0.2

Horse, meat byproducts 0.05

Lettuce, head 4.0

Milk, fat (reflecting 0.10 in whole milk) 2.5

Onion, bulb 0.1

Onion, green 6.0

Pecan 0.05

Poultry, fat 0.05

Poultry, meat 0.05

Sheep, fat 1.0

Sheep, meat 0.2

Sheep, meat byproducts 0.05

(2) Tolerances are established for residues of zeta-cypermethrin, (S-cyano(3-phenoxyphenyl) methyl (±))(cis-trans 

3-(2,2-dichloroethenyl)-2,2 dimethylcyclopropanecarboxylate), including its metabolites and degradates, in or on the 

commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined 

by measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane 

carboxylate, in or on the commodity.

Commodity

Parts per 

million

Alfalfa, forage 15

Alfalfa, hay 30

Alfalfa, seed 0.50

Almond, hulls 6

Animal feed, nongrass, group 18, forage 8

Animal feed, nongrass, group 18, hay 40

Artichoke, globe 0.60

Avocado 0.50

Barley, grain 3.0

Barley, hay 6.0

Barley, straw 20.0

Beet, sugar, roots 0.05

Beet, sugar, tops 0.20

Berry group 13 0.8

Borage, seed 0.2

Brassica, head and stem, subgroup 5A 2.00

Brassica, leafy greens, subgroup 5B 14.00

Buckwheat, grain 3.0

Buckwheat, hay 6.0

Buckwheat, straw 20.0

Cabbage 2.00

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Canistel 0.50

Castor oil plant, refined oil 0.4

Castor oil plant, seed 0.2

Cattle, fat 1.00

Cattle, meat 0.2

Cattle, meat byproducts 0.05

Chinese tallowtree, refined oil 0.4

Chinese tallowtree, seed 0.2

Cilantro, leaves 10

Citrus, dried pulp 1.8

Citrus, oil 4.0

Corn, field, forage 9.0

Corn, field, grain 0.05

Corn, field, stover 30

Corn, pop, grain 0.05

Corn, pop, stover 30

Corn, sweet, forage 15.00

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 15.00

Cotton, undelinted seed 0.5

Crambe, seed 0.2

Cuphea, seed 0.2

Echium, seed 0.2

Egg 0.05

Euphorbia, refined oil 0.4

Euphorbia, seed 0.2

Evening primrose, refined oil 0.4

Evening primrose, seed 0.2

Flax, seed 0.2

Food commodities/feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed 

handling establishments

0.05

Fruit, citrus, group 10 0.35

Fruit, pome, group 11 2

Fruit, stone, group 12 1

Goat, fat 1.00

Goat, meat 0.2

Goat, meat byproducts 0.05

Gold of pleasure, seed 0.2

Grain, aspirated fractions 10.0

Grape 2

Grass, forage, fodder, and hay, group 17, forage 10

Grass, forage, fodder and hay, group 17, hay 35

Hare's-ear mustard, seed 0.2

Hog, fat 0.1

Hog, meat 0.05

Horse, fat 1.00

Horse, meat 0.2

Horse, meat byproducts 0.05

Jojoba, refined oil 0.4

Jojoba, seed 0.2

Lesquerella, seed 0.2

Lunaria, seed 0.2

Mango 0.70

Meadowfoam, seed 0.2

Milk, fat (reflecting 0.10 in whole milk) 2.50

Milkweed, seed 0.2

Mustard, seed 0.2

Niger seed, refined oil 0.4

Niger seed, seed 0.2

Nut, tree, group 14 0.05

Oat, grain 3.0

Oat, hay 6.0

Oat, straw 20.0

Oil radish, seed 0.2

Okra 0.2

Onion, bulb 0.10

Onion, green 3.00

Papaya 0.50

Pea and bean, dried shelled, except soybean, subgroup 6C 0.05

Pea and bean, succulent shelled, subgroup 6B 0.1

Peanut 0.05

Pecan 0.05

Pistachio 0.05

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Poppy, seed 0.2

Poultry, fat 0.05

Poultry, meat 0.05

Rapeseed 0.2

Rice, grain 1.50

Rice, hulls 6.00

Rice, straw 2.00

Rice, wild, grain 1.5

Rose hip, refined oil 0.4

Rose hip, seed 0.2

Rye, grain 3.0

Rye, hay 6.0

Rye, straw 20.0

Safflower, seed 0.2

Sapodilla 0.50

Sapote, black 0.50

Sapote, mamey 0.50

Sesame, seed 0.2

Sheep, fat 1.00

Sheep, meat 0.2

Sheep, meat byproducts 0.05

Sorghum, grain, forage 0.1

Sorghum, grain, grain 0.5

Sorghum, grain, stover 5.0

Soybean, seed 0.05

Star apple 0.50

Stokes aster, refined oil 0.4

Stokes aster, seed 0.2

Sugarcane, cane 0.60

Sunflower, refined oil 0.5

Sunflower, seed 0.2

Sweet rocket, seed 0.2

Tallowwood, refined oil 0.4

Tallowwood, seed 0.2

Tea oil plant, refined oil 0.4

Tea oil plant, seed 0.2

Turnip, greens 14

Vegetable, cucurbit, group 9 0.2

Vegetable, fruiting, group 8 0.2

Vegetable, leafy, except brassica, group 4 10.00

Vegetable, legume, edible podded, subgroup 6A 0.5

Vegetable, root and tuber, group 1, except sugar beet 0.1

Vernonia, refined oil 0.4

Vernonia, seed 0.2

Wheat, forage 3.0

Wheat, grain 0.2

Wheat, hay 6.0

Wheat, straw 7.0

(3) Tolerances are established for residues of the insecticide, alpha-cypermethrin, (R)-cyano(3-phenoxyphenyl)methyl 

(1S,3S)-rel-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane carboxylate, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only total cypermethrin, cyano(3-phenoxyphenyl)methyl 3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropane 

carboxylate, in or on the commodity.

Commodity

Parts per 

million

Alfalfa, hay 15

Beet, sugar, roots 0.05

Beet, sugar, tops 0.20

Brassica, head and stem, subgroup 5A 2.0

Cattle, fat 1.0

Cattle, meat 0.20

Cattle, meat byproducts 0.05

Citrus, dried pulp 1.8

Citrus, oil 4.0

Corn, field, grain 0.05

Corn, pop, grain 0.05

Corn, sweet, kernel plus cob with husks removed 0.05

Cotton, undelinted seed 0.50

Egg 0.05

Food commodities/feed commodities (other than those covered by a higher tolerance as a results of use on growing crops) in food/feed 

handling establishments

0.05

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Fruit, citrus, group 10-10 10

Goat, fat 1.0

Goat, meat 0.20

Goat, meat byproducts 0.05

Hog, fat 1.0

Hog, meat 0.05

Horse, fat 1.0

Horse, meat 0.20

Horse, meat byproducts 0.05

Milk, fat, reflecting 0.10 ppm in whole milk 2.5

Nut, tree, group 14-12 0.05

Pea and bean, dried shelled, except soybean, subgroup 6C 0.05

Pea and bean, succulent shelled, subgroup 6B 0.10

Poultry, fat 0.05

Poultry, meat 0.05

Rice, grain 1.5

Sheep, fat 1.0

Sheep, meat 0.20

Sheep, meat byproducts 0.05

Sorghum, grain, grain 0.50

Soybean, seed 0.05

Vegetable, cucurbit, group 9 0.20

Vegetable, fruiting, group 8-10 0.20

Vegetable, leafy, group 4 10

Vegetable, legume, edible podded, subgroup 6A 0.50

Vegetable, root and tuber, group 1, except sugar beet 0.10

Wheat, grain 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63235, 63243, Nov. 26, 1997, as amended at 63 FR 48586, Sept. 11, 1998; 66 FR 47993, Sept. 17, 2001; 67 FR 6430, Feb. 

12, 2002; 67 FR 56495, Sept. 4, 2002; 69 FR 71717, Dec. 10, 2004; 71 FR 78382, Dec. 29, 2006; 72 FR 53462, Sept. 19, 2007; 72 

FR 71801, Dec. 19, 2007; 73 FR 1525, Jan. 9, 2008; 77 FR 72984, Dec. 7, 2012; 78 FR 7275, Feb. 1, 2013; 79 FR 73213, Dec. 10, 

2014; 79 FR 77394, Dec. 24, 2014; 80 FR 45438, July 30, 2015]

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§180.419 Chlorpyrifos-methyl; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl 

[O,-O,-dimethyl O-(3,5,6-trichloro-2-pyridyl)] phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the 

following food commodities: 

Commodity Parts per million 

Barley, grain 6.0 

Cattle, fat 0.5 

Cattle, meat 0.5 

Cattle, meat byproducts 0.5 

Egg 0.1 

Goat, fat 0.5 

Goat, meat 0.5 

Goat, meat byproducts 0.5 

Hog, fat 0.5 

Hog, meat 0.5 

Hog, meat byproducts 0.5 

Horse, fat 0.5 

Horse, meat 0.5 

Horse, meat byproducts 0.5 

Milk, fat (0.05 ppm (N) in whole milk 1.25 

Oat, grain 6.0 

Poultry, fat 0.5 

Poultry, meat .5 

Poultry, meat byproducts .5 

Rice, grain 6.0 

Sheep, fat 0.5 

Sheep, meat 0.5 

Sheep, meat byproducts 0.5 

Sorghum, grain 6.0 

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Wheat, grain 6.0

(2) Tolerances are established for the combined residues of the insecticide chlorpyrifos-methyl (O,-O- dimethylO-(3,5,6-trichloro-2-pyridyl) phosphorothioate and its metabolite (3,5,6-trichloro-2-pyridinol) in or on the following food 

commodities when present therein as a result of application to stored grains: 

Commodity Parts per million 

Barley, bran 90 

Barley, pearled barley 90 

Rice, bran 30 

Rice, hulls 30 

Rice, polished rice 30 

Sorghum, grain, bran 90 

Wheat, bran 30 

Wheat, germ 30 

Wheat, middlings 30 

Wheat, shorts 30

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33715, May 24, 2000, as amended at 74 FR 46374, Sept. 9, 2009]

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§180.420 Fluridone; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide fluridone, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4

(1H)-pyridinone, and its bound residues, calculated as the stoichiometric equivalent of fluridone, in or on the commodity.

Commodity Parts per million

Crayfish 0.5

Fish 0.5

(2) Tolerances are established for residues of the herbicide fluridone, including its metabolites and degradates, in or 

on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be 

determined by measuring only fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, in or on the 

commodity.

Commodity Parts per million

Cattle, fat 0.05

Cattle, kidney 0.1

Cattle, liver 0.1

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Egg 0.05

Goat, fat 0.05

Goat, kidney 0.1

Goat, liver 0.1

Goat, meat 0.05

Goat, meat byproducts 0.05

Hog, fat 0.05

Hog, kidney 0.1

Hog, liver 0.1

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.05

Horse, kidney 0.1

Horse, liver 0.1

Horse, meat 0.05

Horse, meat byproducts 0.05

Milk 0.05

Poultry, fat 0.05

Poultry, kidney 0.01

Poultry, liver 0.01

Poultry, meat 0.05

Poultry, meat byproducts 0.05

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Sheep, fat 0.05

Sheep, kidney 0.1

Sheep, liver 0.1

Sheep, meat 0.05

Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

residues of the herbicide fluridone, 1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, including its 

metabolites and degradates in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to 

the Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA) section 18 emergency exemptions. Compliance with the 

tolerance levels specified below is to be determined by measuring only fluridone. The tolerances expire on the date 

specified in the table.

Commodity Parts per million Expiration/revocation date

Cotton, undelinted seed 0.1 12/31/17

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide 

fluridone, including its metabolites and degradates, in or on the irrigated crop commodities and crop groupings in the table 

in this paragraph, resulting from use of irrigation water containing residues of 0.15 parts per million following applications 

of fluridone on or around aquatic sites. Where tolerances are established at higher levels from other uses of fluridone on 

the crops in the table in this paragraph, the higher tolerance also applies to residues in or on the irrigated commodity. 

Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only fluridone, 

1-methyl-3-phenyl-5-(3-(trifluoromethyl)phenyl)-4(1H)-pyridinone, in or on the commodity.

Commodity Parts per million

Animal feed, nongrass, group 18 0.15

Avocado 0.1

Berry, group 13 0.1

Cotton, undelinted seed 0.1

Cranberry 0.1

Fruit, citrus, group 10 0.1

Fruit, pome, group 11 0.1

Fruit, stone, group 12 0.1

Grain, cereal, forage, fodder and straw, group 16 0.1

Grain, cereal, group 15 0.1

Grape 0.1

Grass, forage 0.15

Hop, dried cones 0.1

Nut, tree, group 14 0.1

Okra 0.1

Strawberry 0.1

Vegetable, brassica, leafy, group 5 0.1

Vegetable, cucurbit, group 9 0.1

Vegetable, fruiting, group 8 0.1

Vegetable, leafy, except brassica, group 4 0.1

Vegetable, leaves of root and tuber, group 2 0.1

Vegetable, legume, group 6 0.1

Vegetable, root and tuber, group 1 0.1

[76 FR 23495, Apr. 27, 2011, as amended at 77 FR 66720, Nov. 7, 2012; 80 FR 18143, Apr. 3, 2015]

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§180.421 Fenarimol; tolerances for residues.

(a) General. Tolerances are established for residues of fenarimol, including its metabolites and degradates, in or on 

the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only fenarimol alpha-(2 chlorophenyl)-alpha-(4-chlorophenyl)-5-pyrimidinemethanol.

Commodity Parts per million

Apple 0.3

Apple, wet pomace 0.3

Banana 0.25

Cattle, fat 0.01

Cattle, kidney 0.01

Cattle, meat 0.01

Cattle, meat byproducts, except kidney 0.05

Cherry, sweet 1.0

Cherry, tart 1.0

Goat, fat 0.01

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Goat, kidney 0.01

Goat, meat 0.01

Goat, meat byproducts, except kidney 0.05

Grape 0.1.

Hazelnut 0.02

Hop, dried cones 5.0

Horse, fat 0.01

Horse, kidney 0.01

Horse, meat 0.01

Horse, meat byproducts, except kidney 0.05

Pear 0.1

Pecan 0.02

Sheep, fat 0.01

Sheep, kidney 0.01

Sheep, meat 0.01

Sheep, meat byproducts, except kidney 0.05

Vegetable, cucurbit, group 9* 0.20

*There are no U.S. registrations as of August 27, 2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[51 FR 39662, Oct. 30, 1986, as amended at 53 FR 27349, July 20, 1988; 53 FR 44403, Nov. 3, 1988; 54 FR 45734, Oct. 31, 1989; 

60 FR 33354, June 28, 1995; 62 FR 49937, Sept. 24, 1997; 62 FR 61447, Nov. 18, 1997; 67 FR 35048, May 17, 2002; 67 FR 

41807, June 19, 2002; 69 FR 6567, Feb. 11, 2004; 71 FR 32846, June 7, 2006; 71 FR 54434, Sept. 15, 2006; 74 FR 68173, Dec. 

23, 2009; 75 FR 56897, Sept. 17, 2010]

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§180.422 Tralomethrin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide tralomethrin, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano(3-phenoxyphenyl)methyl (1R,3S)

-2,2-dimethyl-3-(1,2,2,2-tetrabromoethyl)cyclopropanecarboxylate, and its metabolites (S)-cyano(3-phenoxyphenyl)methyl 

(1R,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate and (S)-cyano(3-phenoxyphenyl)methyl (1S,3R)

-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate, calculated as the stoichiometric equivalent of tralomethrin, 

in or on the commodity.

Commodity Parts per million Expiration/revocation date

Broccoli 0.5 7/9/13

Cotton, undelinted seed 0.02 7/9/13

Cotton, oil 0.20 7/9/13

Lettuce, head 1.00 7/9/13

Lettuce, leaf 3.00 7/9/13

Soybean, seed 0.05 7/9/13

Sunflower, seed 0.05 7/9/13

(2) A tolerance of 0.02 part per million with an expiration/revocation date of July 9, 2013 is established for residues of 

the insecticide tralomethrin, including its metabolites and degradates, in or on food commodities (other than those covered 

by a higher tolerance as a result of use on growing crops) in food-handling establishments. Compliance with the tolerance 

level specified in this paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano

(3-phenoxyphenyl)methyl (1R,3S)-2,2-dimethyl-3-(1,2,2,2-tetrabromoethyl)cyclopropanecarboxylate, and its metabolites 

(S)-cyano(3-phenoxyphenyl)methyl (1R,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate and (S)-cyano

(3-phenoxyphenyl)methyl (1S,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate, calculated as the 

stoichiometric equivalent of tralomethrin, in or on the commodity.

(i) The insecticide may be present as a residue from application of tralomethrin in food-handling establishments, 

including food service, manufacturing, and processing establishments, such as restaurants, cafeterias, supermarkets, 

bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries.

(ii) The application shall be made in accordance with the following prescribed conditions: Application shall be limited 

to a general surface and spot and/or crack and crevice treatment in food-handling establishments where food and food 

products are held, processed, prepared, and served. General surface application may be used only when the facility is not 

in operation provided exposed food has been covered or removed from the area being treated. All food-contact surfaces 

and equipment must be thoroughly cleaned after general surface applications. Spot and/or crack and crevice application 

may be used while the facility is in operation provided exposed food is covered or removed from the area being treated 

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prior to application. Spray concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of 

food and food-contact surfaces shall be avoided.

(3) A tolerance of 0.02 part per million with an expiration/revocation date of July 9, 2013 is established for residues of 

the insecticide tralomethrin, including its metabolites and degradates, in or on feed commodities (other than those covered 

by a higher tolerance as a result of use on growing crops) in feed-handling establishments. Compliance with the tolerance 

level specified in this paragraph is to be determined by measuring only the sum of tralomethrin, (S)-cyano

(3-phenoxyphenyl)methyl (1R,3S)-2,2-dimethyl-3-(1,2,2,2-tetrabromoethyl)cyclopropanecarboxylate, and its metabolites 

(S)-cyano(3-phenoxyphenyl)methyl (1R,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate and (S)-cyano

(3-phenoxyphenyl)methyl (1S,3R)-3-(2,2-dibromoethenyl)-2,2-dimethylcyclopropanecarboxylate, calculated as the 

stoichiometric equivalent of tralomethrin, in or on the commodity.

(i) The insecticide may be present as a residue from application of tralomethrin in feed-handling establishments, 

including feed manufacturing and processing establishments.

(ii) The application shall be made in accordance with the following prescribed conditions: Application shall be limited 

to a general surface and spot and/or crack and crevice treatment in feed-handling establishments where feed and feed 

products are held or processed. General surface application may be used only when the facility is not in operation 

provided exposed feed has been covered or removed from the area being treated. All feed-contact surfaces and 

equipment must be thoroughly cleaned after general surface applications. Spot and/or crack and crevice application may 

be used while the facility is in operation provided exposed feed is covered or removed from the area being treated prior to 

application. Spray concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of feed 

and feed-contact surfaces shall be avoided.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63001, Nov. 26, 1997, as amended at 62 FR 66025, Dec. 17, 1997; 65 FR 33701, May 24, 2000; 71 FR 74817, Dec. 13, 

2006; 77 FR 59127, Sept. 26, 2012]

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§180.425 Clomazone; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide clomazone, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only clomazone, 2-[(2-chlorophenyl)methyl]-4,4-dimethyl-3-isoxazolidinone, 

in or on the commodity.

Commodity Parts per million

Bean, snap, succulent 0.05

Brassica, head and stem, subgroup 5A 0.10

Cotton, undelinted seed 0.05

Cowpea, forage 0.05

Cowpea, hay 0.05

Cucumber 0.1

Pea, southern, dry seed 0.05

Pea, southern, succulent seed 0.05

Pea, succulent 0.05

Pepper 0.05

Peppermint, tops 0.05

Pumpkin 0.1

Rhubarb 0.30

Rice, grain 0.02

Rice, straw 0.02

Soybean 0.05

Spearmint, tops 0.05

Squash, summer 0.1

Squash, winter 0.1

Sugarcane, cane 0.05

Sweet potato, roots 0.05

Vegetable, cucurbit, group 9 0.05 

Vegetable, tuberous and corm, except potato, subgroup 1D 0.05

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[51 FR 9446, Mar. 19, 1986]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.425, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.426 2-[4,5-Dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-quinoline carboxylic acid; tolerance 

for residues.

A tolerance is established for residues of the herbicide 2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-

yl]-3-quinoline carboxylic acid, in or on the raw agricultural commodity soybean at 0.05 part per million.

[51 FR 13309, Apr. 2, 1986]

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§180.427 Tau-Fluvalinate; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide tau-fluvalinate, cyano-(3-phenoxyphenyl)methyl 

N-[2-chloro-4-(trifluoromethyl)phenyl]-D-valinate, in or on the following food commodities:

Commodity Parts per million

Honey 0.02

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect and inadvertent residues. [Reserved] 

[65 FR 33701, May 24, 2000, as amended at 67 FR 49617, July 31, 2002; 73 FR 52616, Sept. 10, 2008]

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§180.428 Metsulfuron methyl; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the herbicide metsulfuron methyl (methyl 

2-[[[[(4-methoxy-6-methyl-1,3,5- triazin- 2-yl)amino]carbonyl]amino] sulfonyl] benzoate) and its metabolite methyl 

2-[[[[(4-methoxy-6-methyl-1-,3,5- triazin-2-yl)amino]carbonyl]amino] sulfonyl]-4-hydroxybenzoate in or on the following raw 

material agricultural commodities:

Commodity Parts per million

Barley, grain 0.1

Barley, hay 20.0

Barley, straw 0.3

Grass, forage 15.0

Grass, hay 15.0

Grass, straw 15.0

Sorghum, grain, forage 0.2

Sorghum, grain, grain 0.1

Sorghum, grain, stover 0.2

Sugarcane, cane 0.05

Wheat, forage 5.0

Wheat, grain 0.1

Wheat, hay 20.0

Wheat, straw 0.3

(2) Tolerances are established for residues of metsulfuron methyl (methyl-2[[[[(4-methoxy- 6-methyl-1,3,5-triazin-2- yl)

amino]carbonyl]amino] sulfonyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million

Cattle, fat 0.1

Cattle, kidney 0.5

Cattle, meat 0.1

Cattle, meat byproducts 0.1

Goat, fat 0.1

Goat, kidney 0.5

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Goat, meat 0.1

Goat, meat byproducts 0.1

Hog, fat 0.1

Hog, kidney 0.5

Hog, meat 0.1

Hog, meat byproducts 0.1

Horse, fat 0.1

Horse, kidney 0.5

Horse, meat 0.1

Horse, meat byproducts 0.1

Milk 0.05

Sheep, fat 0.1

Sheep, kidney 0.5

Sheep, meat 0.1

Sheep, meat byproducts 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 70191, Dec. 16, 1999, as amended at 66 FR 64773, Dec. 14, 2001; 67 FR 51097, Aug. 7, 2002]

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§180.429 Chlorimuron ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide chlorimuron ethyl, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only chlorimuron ethyl, ethyl 2-[[[[(4-chloro-6-methoxypyrimidin-2yl)amino]carbonyl]

sulfonyl]benzoate] in or on the following commodities:

Commodity Parts per million

Berry, low growing, except strawberry, subgroup 13-07H 0.02

Corn, field, forage 0.5

Corn, field, grain 0.01

Corn, field, stover 2.0

Grain, aspirated fractions 3.0

Peanut 0.02

Soybean, forage 0.45

Soybean, hay 1.8

Soybean, seed 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 10494, Mar. 11, 2009, as amended at 74 FR 67087, Dec. 18, 2009]

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§180.430 Fenoxaprop-ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fenoxaprop-ethyl, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of fenoxaprop-ethyl, (±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)

oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoic acid and 

6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of fenoxaprop-ethyl, in or on the 

commodity.

Commodity Parts per million

Barley, grain 0.05

Barley, straw 0.1

Cattle, fat 0.05

Cattle, meat byproducts 0.05

Cattle, meat 0.05

Cotton, undelinted seed 0.05

Goat, fat 0.05

Goat, meat byproducts 0.05

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Goat, meat 0.05

Hog, fat 0.05

Hog, meat byproducts 0.05

Hog, meat 0.05

Horse, fat 0.05

Horse, meat byproducts 0.05

Horse, meat 0.05

Milk 0.02

Peanut 0.05

Peanut, hulls 0.05

Rice, grain 0.05

Sheep, fat 0.05

Sheep, meat byproducts 0.05

Sheep, meat 0.05

Soybean 0.05

Wheat, grain 0.05

Wheat, straw 0.50

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide 

fenoxaprop-ethyl, including its metabolites and degradates, in or on the commodities in the table in this paragraph in 

connection with use of fenoxaprop-ethyl under section 18 emergency exemptions granted by EPA. Compliance with the 

tolerance levels specified in this paragraph is to be determined by measuring only the sum of fenoxaprop-ethyl, (±)-ethyl 

2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]

propanoic acid and 6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric equivalent of fenoxaprop-ethyl, 

in or on the commodity. The tolerances expire and are revoked on the dates specified in the table in this paragraph.

Commodity Parts per million

Expiration/

revocation date

Grass, forage 0.05 12/31/16

Grass, hay 0.05 12/31/16

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the herbicide fenoxaprop-ethyl, including its metabolites and degradates, in or on the 

commodities in the table in this paragraph when fenoxaprop-ethyl is used in the states of Oregon, Washington, and Utah. 

Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of 

fenoxaprop-ethyl, (±)-ethyl 2-[4-[(6-chloro-2-benzoxazolyl)oxy]phenoxy]propanoate, and its metabolites, 2-[4-[(6-chloro-2-

benzoxazolyl)oxy]phenoxy]propanoic acid and 6-chloro-2,3-dihydrobenzoxazol-2-one, calculated as the stoichiometric 

equivalent of fenoxaprop-ethyl, in or on the commodity

Commodity

Parts per

million

Grass, hay 0.09

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 1377, Jan. 9, 1998, as amended at 63 FR 19837, Apr. 22, 1998; 73 FR 33718, June 13, 2008; 75 FR 80346, Dec. 22, 2010; 

76 FR 23495, Apr. 27, 2011; 78 FR 78748, Dec. 27, 2013; 79 FR 26164, May 7, 2014]

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§180.431 Clopyralid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide clopyralid, including its metabolites and 

degradates, in or on the commodities in the table below from its application in the acid form or in the form of its salts. 

Compliance with the tolerance levels specified below is to be determined by measuring only clopyralid, (3,6-dichloro-2-

pyridinecarboxylic acid), in or on the following commodities:

Commodity Parts per million

Apple 0.05

Asparagus 1.0

Barley, bran 12 

Barley, grain 3.0

Barley, hay 9.0 

Barley, pearled barley 12 

Barley, straw 9.0

Beet, garden, tops 3.0 

Beet, garden, roots 4.0 

Beet, sugar, molasses 10 

Beet, sugar, roots 2.0 

Beet, sugar, tops 3.0 

Brassica, head and stem, subgroup 5A 2.0 

Brassica, leafy greens, subgroup 5B 5.0

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Bushberry subgroup 13-07B 0.50

Canola, meal 6.0 

Canola, seed 3.0 

Cattle, fat 1.0

Cattle, liver 3.0 

Cattle, meat 1.0

Cattle, meat byproducts, except liver 36.0 

Corn, field, forage 3.0

Corn, field, grain 1.0

Corn, field, milled byproducts 1.5

Corn, field, stover 10.0

Corn, pop, grain 1.0 

Corn, pop, stover 10.0 

Corn, sweet, forage 7.0 

Corn, sweet, kernel plus cob with husks removed 1.0 

Corn, sweet, stover 10.0 

Cranberry 4.0 

Egg 0.1

Flax, meal 6.0 

Fruit, stone, group 12 0.5 

Goat, fat 1.0

Goat, liver 3.0 

Goat, meat 1.0

Goat, meat byproducts, except liver 36.0 

Grass, forage 500.0 

Grass, hay 500.0 

Hog, fat 0.2

Hog, meat 0.2

Hog, meat byproducts 0.2

Hop, dried cones 5.0 

Horse, fat 1.0

Horse, liver 3.0 

Horse, meat 1.0

Horse, meat byproducts, except liver 36.0 

Milk 0.2 

Oat, forage 9.0

Oat, grain 3.0

Oat, groats/rolled oats 12 

Oat, straw 9.0

Peppermint, tops 3.0 

Plum, prune, dried 1.5 

Poultry, fat 0.2

Poultry, meat 0.2

Poultry, meat byproducts 0.2

Rapeseed, forage 3.0 

Rapeseed, meal 6.0

Rapeseed, subgroup 20A, except gold of pleasure 3.0

Sheep, fat 1.0

Sheep, liver 3.0 

Sheep, meat 1.0

Sheep, meat byproducts, except liver 36.0 

Spearmint, tops 3.0 

Spinach 5.0 

Strawberry 4.0

Swiss chard 3.0

Teff, forage 9.0

Teff, grain 3.0

Teff, hay 9.0

Teff, straw 9.0

Turnip, greens 4.0 

Turnip, roots 1.0 

Wheat, bran 12 

Wheat, forage 9.0

Wheat, germ 12 

Wheat, grain 3.0

Wheat, middling 12 

Wheat, shorts 12 

Wheat, straw 9.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]

[52 FR 10566, Apr. 2, 1987]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.431, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.432 Lactofen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide lactofen, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only lactofen, 2-ethoxy-1-methyl-2-oxoethyl 5-[2-chloro-4-(trifluoromethyl)

phenoxy]-2-nitrobenzoate, in or on the commodity.

Commodity Parts per million

Beans, snap, succulent, except lima bean 0.01

Cotton, gin byproducts 0.02

Cotton, undelinted seed 0.01

Peanut 0.01

Soybean, seed 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of the herbicide lactofen, including its metabolites and degradates, in or on the commodities in the 

table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring 

only lactofen, 2-ethoxy-1-methyl-2-oxoethyl 5-[2-chloro-4-(trifluoromethyl)phenoxy]-2-nitrobenzoate, in or on the 

commodity.

Commodity Parts per million

Okra 0.02

Vegetables, fruiting, group 08 0.02

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 57216, Sept. 24, 2004, as amended at 72 FR 33906, June 20, 2007; 76 FR 23496, Apr. 27, 2011]

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§180.433 Fomesafen; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide fomesafen, including its metabolites and 

degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table below 

is to be determined by measuring only fomesafen, 5-[2-chloro-4-(trifluoromethyl)phenoxy]-N-(methylsulfonyl)-2-

nitrobenzamide, in or on the commodity.

Commodity Parts per million

Bean, dry 0.05

Bean, lima, succulent 0.05

Bean, snap, succulent 0.05

Cantaloupe 0.025

Cotton, gin byproducts 0.025

Cotton, undelinted seed 0.025

Cucumber 0.025

Pea, succulent 0.025

Pepper, bell 0.025

Pepper, non-bell 0.025

Potato 0.025

Pumpkin 0.025

Soybean 0.05

Soybean, vegetable, succulent 0.05

Squash, summer 0.025

Squash, winter 0.025

Tomato 0.025

Watermelon 0.025

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]

[71 FR 25951, May 3, 2006, as amended at 72 FR 52020, Sept. 12, 2007; 76 FR 12882, Mar. 9, 2011; 78 FR 65570, Nov. 1, 2013; 

80 FR 9391, Feb. 23, 2015]

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§180.434 Propiconazole; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of propiconazole, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only those propiconazole residues convertible to 2,4-dichlorobenzoic acid (2,4-DCBA), expressed as the 

stoichiometric equivalent of propiconazole, in or on the commodity in the table below:

Commodity Parts per million

Almond, hulls 7.0

Banana 0.2

Barley, bran 6.0

Barley, grain 3.0

Barley, hay 30

Barley, straw 20

Bean, dry seed 0.40 

Bean, snap 0.70 

Bean, succulent shelled 0.10 

Beet, garden, roots 0.30 

Beet, garden, tops 5.5 

Beet, sugar, dried pulp 1.0

Beet, sugar, molasses 1.5

Beet, sugar, roots 0.3

Beet, sugar, tops 10

Bushberry, subgroup 13-07B 1.0

Caneberry, subgroup 13-07A 1.0

Carrot, roots 0.25

Cattle, fat 0.05

Cattle, kidney 2.0

Cattle, liver 2.0

Cattle, meat 0.05

Cattle, meat byproducts, except liver and kidney 0.05

Cilantro, leaves 13 

Citrus, oil 1000 

Corn, field, forage 12

Corn, field, grain 0.2

Corn, field, stover 30

Corn, pop, grain 0.2

Corn, pop, stover 30

Corn, sweet, forage 6.0

Corn, sweet, kernel plus cob with husks removed 0.1

Corn, sweet, stover 30

Fruit, citrus, group 10-10 8.0 

Fruit, stone, group 12, except plum 4.0 

Goat, fat 0.05

Goat, kidney 2.0

Goat, liver 2.0

Goat, meat 0.05

Goat, meat byproducts, except liver and kidney 0.05

Grain, aspirated fractions 110

Grass, forage 0.5

Grass, hay 0.5

Grass, straw 40

Hog, kidney 0.2

Hog, liver 0.2

Horse, fat 0.05

Horse, kidney 2.0

Horse, liver 2.0

Horse, meat 0.05

Horse, meat byproducts, except liver and kidney 0.05

Leaf petioles subgroup 4B 5.0

Low growing berry subgroup 13-07G, except cranberry 1.3

Milk 0.05

Mushroom 0.1

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Nut, tree, group 14 0.1

Oat, forage 4.0

Oat, grain 3.0

Oat, hay 15

Oat, straw 10

Onion, bulb subgroup 3-07A 0.2

Onion, green, subgroup 3-07B 9.0

Parsley, fresh leaves 13 

Parsley, dried leaves 35 

Peanut 0.2

Peanut, hay 20

Peppermint, tops 10.0

Pineapple 4.5

Pineapple, process residue 7.0

Pistachio 0.1

Plum 0.60 

Rapeseed subgroup 20A 0.30

Rice, bran 15

Rice, grain 7.0

Rice, hulls 20

Rice, straw 18

Rye, bran 0.6

Rye, forage 9.0

Rye, grain 0.3

Rye, straw 10

Sheep, fat 0.05

Sheep, kidney 2.0

Sheep, liver 2.0

Sheep, meat 0.05

Sheep, meat byproducts, except liver and kidney 0.05

Sorghum, grain, forage 12

Sorghum, grain, grain 3.5

Sorghum, grain, stover 15

Soybean, forage 11

Soybean, hay 30

Soybean, seed 2.0

Spearmint, tops 10.0

Sugarcane, cane 0.4

Tomato 3.0 

Vegetable, foliage of legume, group 7 30 

Wheat, bran 0.6

Wheat, forage 15

Wheat, grain 0.3

Wheat, hay 30

Wheat, straw 20

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of propiconazole 

(1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole) and its metabolites determined as 

2,4-dichlorobenzoic acid and expressed as parent compound, in connection with use of the pesticide under section 18 

emergency exemptions granted by EPA. The tolerances will expire and are revoked on the dates specified in the following 

table:

Commodity Parts per million Expiration/revocation date

Avocado 10 12/31/16

Nectarine 2.0 12/31/13

Peach 2.0 12/31/13

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established 

for residues of 1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl]methyl]-1H-1,2,4-triazole and its metabolites 

determined as 2,4-dichlorobenzoic acid and expressed as parent compound, in or on the following commodities:

Commodity Parts per million

Cranberry 1.0

Rice, wild, grain 0.5

(d) Indirect or inadvertent residues. Tolerances are established for the combined residues of the fungicide 

1-[[2-(2,4-dichlorophenyl)-4-propyl-1,3-dioxolan-2-yl] methyl]-1H-1,2,4-triazole and its metabolites determined as 

2,4-dichlorobenzoic acid and expressed as parent compound in or on the following commodities when present therein as a 

result of application of propiconazole to growing crops in paragraphs (a) and (c) of this section:

Commodity Parts per million

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Alfalfa, forage 0.1

Alfalfa, hay 0.1

[71 FR 55306, Sept. 22, 2006, as amended at 72 FR 20439, Apr. 25, 2007; 74 FR 12613, Mar. 25, 2009; 75 FR 80346, Dec. 22, 

2010; 76 FR 27268, May 11, 2011; 77 FR 38204, June 27, 2012; 77 FR 75044, Dec. 19, 2012; 78 FR 23503, Apr. 19, 2013; 78 FR 

78748, Dec. 27, 2013; 79 FR 18467, Apr. 2, 2014]

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§180.435 Deltamethrin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of deltamethrin, including its metabolites and degradates, in 

or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by 

measuring only deltamethrin, (1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylic acid (S)-alpha-cyano-3-

phenoxybenzyl ester, and its major metabolites, trans-deltamethrin, (S)-alpha-cyano-m-phenoxybenzyl(1R,3S)

-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, and alpha-R-deltamethrin, (R)

-alpha-cyano-m-phenoxybenzyl-(1R,3R)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, in or on the 

commodity.

Commodity Parts per million

Almond, hulls 2.5

Apple, wet pomace 1.0

Artichoke, globe 0.5

Barley, bran 5.0

Cattle, fat 0.05

Cattle, meat 0.02

Cattle, meat byproducts 0.05

Corn, field, forage 0.7

Corn, field, refined oil 2.5

Corn, field, stover 5.0

Corn, pop, stover 5.0

Corn, sweet, forage 10

Corn, sweet, kernel plus cob with husks removed 0.03

Corn, sweet, stover 15

Cotton, refined oil 0.2

Cotton, undelinted seed 0.04

Egg 0.02

Fish—freshwater finfish 0.01

Fish—freshwater finfish, farm raised 0.01

Fish—saltwater finfish, other 0.01

Fish—saltwater finfish, tuna 0.01

Fruit, pome, Group 11 0.2

Goat, fat 0.05

Goat, meat 0.02

Goat, meat byproducts 0.05

Grain, aspirated fractions 65

Grain, cereal, Group 15, except sweet corn 1.0

Hog, fat 0.05

Horse, fat 0.05

Horse, meat 0.02

Horse, meat byproducts 0.05

Lychee* 0.2

Milk, fat (reflecting 0.02 ppm in whole milk) 0.1

Nut, tree, Group 14 0.1

Onion, bulb 0.1

Onion, green 1.5

Poultry, fat 0.05

Poultry, meat 0.02

Poultry, meat byproducts 0.02

Radish, tops 4.0

Rapeseed 0.2

Rice, hulls 2.5

Rye, bran 5.0

Sheep, fat 0.05

Sheep, meat 0.02

Sheep, meat byproducts 0.05

Sorghum, grain, forage 0.5

Sorghum, grain, stover 1.0

Soybean, seed 0.1

Soybean, hulls 0.2

Starfruit* 0.2

Sunflower, seed 0.1

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Tomato 0.2

Tomato, paste 1.0 

Tomato, puree 1.0 

Vegetable, cucurbit, Group 9 0.2

Vegetable, fruiting, Group 8 0.3

Vegetable, root, except sugar beet, Subgroup IB 0.2

Vegetable, tuberous and corm, Subgroup IC 0.04

Wheat, bran 5.0

*There are no U.S. registrations for use of deltamethrin on starfruit and lychee.

(2) A tolerance of 0.05 ppm is established for residues of the insecticide deltamethrin, including its metabolites and 

degradates, in or on all food/feed items (other than those covered by a higher tolerance as a result of use on growing 

crops) when deltamethrin is used in food/feed handling establishments or as a wide-area mosquito adulticide. Compliance 

with the tolerance levels specified is to be determined by measuring only deltamethrin, (1R,3R)-3-(2,2-dibromovinyl)

-2,2-dimethylcyclopropanecarboxylic acid (S)-alpha-cyano-3-phenoxybenzyl ester, and its major metabolites, 

trans-deltamethrin, (S)-alpha-cyano-m-phenoxybenzyl(1R,3S)-3-(2,2-dibromovinyl)-2,2-dimethylcyclopropanecarboxylate, 

and alpha-R-deltamethrin, (R)-alpha-cyano-m-phenoxybenzyl-(1R,3R)-3-(2,2-dibromovinyl)

-2,2-dimethylcyclopropanecarboxylate, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63001, Nov. 26, 1997, as amended at 63 FR 45414, Aug. 26, 1998; 69 FR 62614, Oct. 27, 2004; 74 FR 46375, Sept. 9, 

2009; 76 FR 34885, June 15, 2011; 79 FR 66301, Nov. 7, 2014; 80 FR 16302, Mar. 27, 2015]

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§180.436 Cyfluthrin and the isomer beta-cyfluthrin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3-phenoxyphenyl)

methyl-3-(2,2-dichloroethenyl)-2,2dimethyl-cyclopropane-carboxylate; CAS No. 68359-37-5) in or on the following raw 

agricultural commodities:

Commodity Parts per million 

Alfalfa 5.0 

Alfalfa, forage 5.0 

Alfalfa, hay 13 

Almond, hulls 0.5 

Barley, bran 0.5 

Barley, grain 0.15 

Beet, sugar, dried pulp 1.0 

Beet, sugar, roots 0.10 

Brassica, head and stem, subgroup 5A 2.5 

Brassica, leafy greens, subgroup 5B 7.0 

Buckwheat, grain 0.15 

Carrot, roots 0.20 

Cattle, fat 2.0 

Cattle, meat 0.10 

Cattle, meat byproducts 0.10 

Citrus, dried pulp 0.3 

Citrus, oil 0.3 

Corn, field, grain 0.05 

Corn, pop, grain 0.05 

Corn, sweet, kernel plus cob with husks removed 0.05 

Cotton, hulls 2.0 

Cotton, refined oil 2.0 

Cotton, undelinted seed 1.0 

Egg 0.01 

Fruit, citrus, group 10 0.2 

Fruit, pome, group 11 0.5 

Fruit, stone, group 12 0.3 

Goat, fat 2.0 

Goat, meat 0.05 

Goat, meat byproducts 0.05 

Grain, aspirated fractions 150 

Grain, cereal, forage, fodder and hay, group 16, forage, except rice 25 

Grain, cereal, forage, fodder and hay, group 16, hay, except rice 6.0 

Grain, cereal, forage, fodder and hay, group 16, stover, except rice 30 

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Grain, cereal, forage, fodder and hay, group 16, straw, except rice 7.0 

Grape 1.0 

Grape, raisin 3.5 

Grass, forage, fodder and hay, group 17, forage 12 

Grass, forage, fodder and hay, group 17, hay 50 

Hog, fat 0.5 

Hog, meat 0.01 

Hog, meat byproducts 0.01 

Hop, dried cones 20.0 

Hop, vines 4.0 

Horse, fat 2.0 

Horse, meat 0.05 

Horse, meat byproducts 0.05 

Lettuce, head 2.0 

Lettuce, leaf 3.0 

Milk 0.2 

Milk, fat 5.0 

Millet, grain 0.15 

Mustard greens 7.0 

Nut, tree, group 14 0.01 

Oat, bran 0.5 

Oat, grain 0.15 

Pea and bean, dried shelled, except soybean, subgroup 6C 0.15 

Pea, dry, seed 0.15 

Pea, southern, succulent 0.25 

Peanut 0.01 

Peanut, hay 6.0 

Pepper 0.50 

Pistachio 0.01 

Poultry, fat 0.01 

Poultry, meat 0.01 

Poultry, meat byproducts 0.01 

Radish, roots 1.0 

Rye, bran 0.5 

Rye, grain 0.15 

Sheep, fat 2.0 

Sheep, meat 0.05 

Sheep, meat byproducts 0.05 

Sorghum, grain, grain 3.5 

Soybean, forage 8.0 

Soybean, hay 4.0 

Soybean, seed 0.03 

Sugarcane, cane 0.05 

Sugarcane, molasses 0.20 

Sunflower, forage 5.0 

Sunflower, seed 0.02 

Teosinte, grain 0.05 

Tomato 0.20 

Tomato, dry pomace 5.0 

Tomato, paste 0.5 

Tomato, wet pomace 5.0 

Triticale, grain 0.15 

Turnip, greens 7.0 

Vegetable, cucurbit, group 9 0.1 

Vegetable, fruiting, group 8 0.5 

Vegetable, leafy, except brassica, group 4 6.0 

Vegetable, tuberous and corm, subgroup 1C 0.01 

Wheat, bran 0.5 

Wheat, grain 0.15 

Wheat, shorts 0.5

(2) A tolerance of 0.05 ppm is established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3-phenoxyphenyl)

methyl-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate; CAS Reg. No. 69359-37-5) in food commodities 

exposed to the insecticide during treatment of food-handling establishments where food and food products are held, 

processed, prepared, or served. Treatments may be made by general surface, spot, and/or crack and crevice applications.

(i) General surface treatments shall be limited to a maximum of 3.8 grams of active ingredient per 1,000 square feet, 

applying to walls, floors, and ceilings with a low-pressure system. Cover or remove all food processing and/or handling 

equipment during application. Do not apply directly to food products. Reapplications may be made at 10-day intervals.

(ii) Crack and crevice or spot treatments shall be limited to a maximum of 0.1 percent of the active ingredient weight, 

applied with a low-pressure system with a pinpoint or variable-pattern nozzle. Dust formulation shall be limited to a 

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maximum of 0.1 percent of the active ingredient by weight, applied using a hand duster, power duster, or other equipment 

capable of applying dust insecticide directly into voids and cracks and crevices. Dust applications should be made in a 

manner to avoid deposits on exposed surfaces or introducing the material into the air. Cover exposed food or remove food 

from premises. Do not apply directly to food. Reapplications may be made at 10-day intervals.

(iii) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by the Environmental 

Protection Agency, and it shall be used in accordance with such label and labeling.

(3) A tolerance of 0.05 part per million is established for residues of the insecticide cyfluthrin (cyano(4-fluoro-3-

phenoxyphenyl)methyl-3-(2,2-dichloroethenyl)-2,2-dimethylcyclopropanecarboxylate; CAS Reg. No. 68359-37-5) in feed 

commodities exposed to the insecticide during treatment of feed-handling establishments where feed and feed products 

are held, processed, prepared, or served. Treatments may be made by general surface, spot, and/or crack and crevice 

applications.

(i) General surface tratments shall be limited to a maximum of 3.8 grams of active ingredient per 1,000 square feet, 

applying to walls, floors, and ceilings with a low-pressure system. Cover or remove all feed processing and/or handling 

equipment during application. Do not apply directly to feed products. Reapplications may be made at 10-day intervals.

(ii) Crack and crevice or spot treatments shall be limited to a maximum of 0.1 percent of the active ingredient by 

weight, applied with a low-pressure system with a pinpoint or variable-pattern nozzle. Dust formulation shall be limited to a 

maximum of 0.1 percent of the active ingredient by weight, applied using a hand duster, power duster, or other equipment 

capable of applying dust insecticide directly into voids and cracks and crevices. Dust applications should be made in a 

manner to avoid deposits on exposed surfaces or introducing the material into the air. Cover exposed feed or remove feed 

from premises. Do not apply directly to feed. Reapplications may be made at 10-day intervals.

(iii) To ensure safe use of the insecticide, its label and labeling shall conform to that registered by EPA, and it shall be 

used in accordance with such label and labeling.

(4) Tolerances are established for residues of the isomer, beta-cyfluthrin, cyano(4-fluoro-3-phenoxyphenyl)methyl3-(2,2-dichloroethenyl)-2,2-dimethyl-cyclopropanecarboxylate [mixture comprising the enantiomeric pair (R)-α-cyano-4-

fluoro-3-phenoxybenzyl (1S,3S)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3-

phenoxybenzyl (1R,3R)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate with the enantiomeric pair (R)-α-cyano4-fluoro-3-phenoxybenzyl (1S,3R)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate and (S)-α-cyano-4-fluoro-3-

phenoxybenzyl (1R,3S)-3-(2,2-dichlorovinyl)-2,2-dimethylcyclopropanecarboxylate], in or on the following raw agricultural 

commodities:

Commodity Parts per million 

Alfalfa 5.0 

Alfalfa, forage 5.0 

Alfalfa, hay 13 

Almond, hulls 0.5 

Barley, bran 0.5 

Barley, grain 0.15 

Beet, sugar, dried pulp 1.0 

Beet, sugar, roots 0.10 

Brassica, head and stem, subgroup 5A 2.5 

Brassica, leafy greens, subgroup 5B 7.0 

Buckwheat, grain 0.15 

Carrot, roots 0.20 

Cattle, fat 2.0 

Cattle, meat 0.10 

Cattle, meat byproducts 0.10 

Citrus, dried pulp 0.3 

Citrus, oil 0.3 

Corn, field, grain 0.05 

Corn, pop, grain 0.05 

Corn, sweet, kernel plus cob with husks removed 0.05 

Cotton, hulls 2.0 

Cotton, refined oil 2.0 

Cotton, undelinted seed 1.0 

Egg 0.01 

Fruit, citrus, group 10 0.2 

Fruit, pome, group 11 0.5 

Fruit, stone, group 12 0.3 

Goat, fat 2.0 

Goat, meat 0.05 

Goat, meat byproducts 0.05 

Grain, aspirated fractions 150 

Grain, cereal, forage, fodder and hay, group 16, forage, except rice 25 

Grain, cereal, forage, fodder and hay, group 16, hay, except rice 6.0 

Grain, cereal, forage, fodder and hay, group 16, stover, except rice 30 

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Grain, cereal, forage, fodder and hay, group 16, straw, except rice 7.0 

Grape 1.0 

Grape, raisin 3.5 

Grass, forage, fodder and hay, group 17, forage 12 

Grass, forage, fodder and hay, group 17, hay 50 

Hog, fat 0.5 

Hog, meat 0.01 

Hog, meat byproducts 0.01 

Hop, dried cones 20.0 

Hop, vines 4.0 

Horse, fat 2.0 

Horse, meat 0.05 

Horse, meat byproducts 0.05 

Lettuce, head 2.0 

Lettuce, leaf 3.0 

Milk 0.2 

Milk, fat 5.0 

Millet, grain 0.15 

Mustard greens 7.0 

Nut, tree, group 14 0.01 

Oat, bran 0.5 

Oat, grain 0.15 

Pea and bean, dried shelled, except soybean, subgroup 6C 0.15 

Pea, dry, seed 0.15 

Pea, southern, succulent 0.25 

Peanut 0.01 

Peanut, hay 6.0 

Pepper 0.50 

Pistachio 0.01 

Poultry, fat 0.01 

Poultry, meat 0.01 

Poultry, meat byproducts 0.01 

Radish, roots 1.0 

Rye, bran 0.5 

Rye, grain 0.15 

Sheep, fat 2.0 

Sheep, meat 0.05 

Sheep, meat byproducts 0.05 

Sorghum, grain, grain 3.5 

Soybean, forage 8.0 

Soybean, hay 4.0 

Soybean, seed 0.03 

Sugarcane, cane 0.05 

Sugarcane, molasses 0.20 

Sunflower, forage 5.0 

Sunflower, seed 0.02 

Teosinte, grain 0.05 

Tomato 0.20 

Tomato, paste 0.5 

Tomato, pomace 5.0 

Triticale, grain 0.15 

Turnip, greens 7.0 

Vegetable, cucurbit, group 9 0.1 

Vegetable, fruiting, group 8 0.5 

Vegetable, leafy greens, except Brassica, group 4 6.0 

Vegetable, tuberous and corm, subgroup 1C 0.01 

Wheat, bran 0.5 

Wheat, grain 0.15 

Wheat, shorts 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[53 FR 1924, Jan. 25, 1988]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.436, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.437 Methyl 2-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-p-toluate and methyl 6-(4-isopropyl-4-methyl-5-

oxo-2-imidazolin-2-yl)-m-toluate; tolerances for residues.

Tolerances are established for the combined residues of the herbicide methyl 2-(4-isopropyl-4-methyl-5-oxo-2-

imidazolin-2-yl)-p-toluate and methyl 6-(4-isopropyl-4-methyl-5-oxo-2-imidazolin-2-yl)-m-toluate in or on the following raw 

agricultural commodities:

Commodity Parts per million

Barley, grain 0.10

Barley, straw 2.00

Sunflower, seed 0.10

Wheat, grain 0.10

Wheat, straw 2.00

[53 FR 24069, June 27, 1988]

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§180.438 Lambda-cyhalothrin and an isomer gamma-cyhalothrin; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for the combined residues of the pyrethroid lambda-cyhalothrin, 1:1 

mixture of (S)-α-cyano-3-phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)

-2,2-dimethylcyclopropanecarboxylate and (R)-α-cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1-

enyl)-2,2-dimethylcyclopropanecarboxylate and its epimer expressed as epimer of lambda-cyhalothrin, a 1:1 mixture of (S)

-α-cyano-3-phenoxybenzyl-(Z)-(1S,3S)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate and 

(R)-α-cyano-3-phenoxybenzyl-(Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate, on 

plants and livestocks, as indicated in the following table.

Commodity Parts per million

Alfalfa, forage 5.0

Alfalfa, hay 6.0

Almond, hulls 1.5

Apple, wet pomace 2.50

Avocado, imported 0.20

Barley, bran 0.2

Barley, grain 0.05

Barley, hay 2.0

Barley, straw 2.0

Brassica, head and stem, subgroup 5A 0.4

Buckwheat, grain 0.05

Canola, refined oil 2.0

Canola, seed 1.0

Cattle, fat 3.0

Cattle, meat 0.2

Cattle, meat byproducts 0.2

Corn, field, flour 0.15

Corn, field, forage 6.0

Corn, field, grain 0.05

Corn, field, stover 1.0

Corn, pop, grain 0.05

Corn, pop, grain, flour 0.05

Corn, pop, stover 1.0

Corn, sweet, forage 6.0

Corn, sweet, stover 1.0

Corn, sweet, kernel plus cob with husks removed 0.05

Cotton, undelinted seed 0.05

Egg 0.01

Fruit, pome, group 11 0.30

Fruit, stone, group 12 0.50

Garlic 0.1

Goat, fat 3.0

Goat, meat 0.2

Goat, meat byproducts 0.2

Grain, aspirated fractions 2.0

Grass, forage, fodder and hay, group 17 7.0

Hog, fat 0.2

Hog, meat 0.01

Hog, meat byproducts 0.02

Hop, dried cones 10.0

Horse, fat 3.0

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Horse, meat 0.2

Horse, meat byproducts 0.2

Lettuce, head 2.0

Lettuce, leaf 2.0

Milk, fat (reflecting 0.4 ppm in whole milk) 10.0

Nut, tree, group 14 0.05

Oat, grain 0.05

Oat, forage 2.0

Oat, hay 2.0

Oat, straw 2.0

Onion, bulb 0.1

Pea and bean, dried shelled, except soybean, subgroup 6C 0.10

Pea and bean, succulent shelled, subgroup 6B 0.01

Peanut 0.05

Peanut, hay 3.0

Pistachio 0.05

Poultry, fat 0.03

Poultry, meat 0.01

Poultry, meat byproducts 0.01

Rice, grain 1.0

Rice, hulls 5.0

Rice, straw 1.8

Rice, wild, grain 1.0

Rye, bran 0.2

Rye, grain 0.05

Rye, forage 2.0

Rye, straw 2.0

Sheep, fat 3.0

Sheep, meat 0.2

Sheep, meat byproducts 0.2

Soybean 0.01

Sorghum, grain, grain 0.2

Sorghum, grain, forage 0.30

Sorghum, grain, stover 0.50

Sugarcane, cane 0.05

Sunflower, forage 0.2

Sunflower, seed, hulls 0.50

Sunflower, refined oil 0.30

Sunflower, seed 0.2

Tomato 0.1

Tomato, dry pomace 6.0

Tomato, wet pomace 6.0

Vegetable, cucurbit, group 9 0.05

Vegetable, fruiting, group 8 0.20

Vegetable, legume, edible podded, subgroup 6A 0.20

Vegetable, tuberous and corm, subgroup 1C 0.02

Wheat, grain 0.05

Wheat, forage 2.0

Wheat, hay 2.0

Wheat, straw 2.0

Wheat, bran 0.2

(2) Tolerances1 are established for the combined residues of the pyrethroid [gamma-cyhalothrin (the isolated active 

isomer of lambda-cyhalothrin) (S)-′-cyano-3-phenoxybenzyl (Z)-(1R,3R)-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)

-2,2-dimethylcyclopropanecarboxylate)) and its epimer (R)-′-cyano-3-phenoxybenzyl (Z)-(1R,3R)

-3-(2-chloro-3,3,3-trifluoroprop-1-enyl)-2,2-dimethylcyclopropanecarboxylate in/on the following commodities:

Commodity Parts per million

Alfalfa, forage 5

Alfalfa, hay 6

Almond, hulls 1.5

Apple, pomace, wet 2.50

Avocado, imported 0.20

Brassica, head and stem, subgroup 5A 0.4

Canola, seed 0.15

Cattle, fat 3

Cattle, meat 0.2

Cattle, meat byproducts 0.2

Corn, field, flour 0.15

Corn, field, forage 6.0

Corn, field, grain 0.05

Corn, field, stover 1.0

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Corn, pop, grain 0.05

Corn, pop, stover 1.0

Corn, sweet, forage 6.0

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 1.0

Cotton, undelinted seed 0.05

Egg 0.01

Fruit, pome, group 11 0.30

Fruit, stone, group 12 0.50

Garlic 0.10

Goat, fat 3.0

Goat, meat 0.2

Goat, meat byproducts 0.2

Grain, aspirated fractions 2.0

Hog, fat 3.0

Hog, meat 0.2

Hog, meat byproducts 0.2

Horse, fat 3.0

Horse, meat 0.2

Horse, meat byproducts 0.2

Lettuce, head 2.0

Lettuce, leaf 2.0

Milk, fat (reflecting 0.20 ppm in whole milk) 5.0

Nut, tree, group 14 0.05

Okra 0.20

Onion, bulb 0.1

Pea and bean, dried shelled, except soybean, subgroup 6C 0.10

Pea and bean, succulent shelled, subgroup 6B 0.01

Peanut 0.05

Peanut, hay 3.0

Pistachio 0.05

Poultry, fat 0.03

Poultry, meat 0.01

Poultry, meat byproducts 0.01

Rice, grain 1.0

Rice, hulls 5.0

Rice, straw 1.8

Sheep, fat 3.0

Sheep, meat 0.2

Sheep, meat byproducts 0.2

Sorghum, grain, forage 0.30

Sorghum, grain, grain 0.20

Sorghum, grain, stover 0.50

Soybean 0.01

Sugarcane 0.05

Sunflower, forage 0.20

Sunflower, refined oil 0.30

Sunflower, seed 0.20

Sunflower, seed, hulls 0.50

Tomato 0.10

Tomato, dry pomace 6.0

Tomato, wet pomace 6.0

Vegetables, fruiting, group 8 0.20

Vegetable, legume, edible podded, subgroup 6A 0.20

Wheat, bran 2.0

Wheat, forage 2.0

Wheat, grain 0.05

Wheat, hay 2.0

Wheat, straw 2.0

1

 The analytical enforcement methods for lambda-cyhalothrin are applicable for determination of gamma-cyhalothrin 

residues in plant and animal commodities.

(3) A tolerance of 0.01 part per million is established for residues of the insecticide lamba-cyhalothrin and an isomer 

gamma-cyhalothrin in or on all food commodities (other than those already covered by a higher tolerance as a result of 

use on growing crops) in food-handling establishments where food products are held, processed, or prepared.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

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[71 FR 74817, Dec. 13, 2006, as amended at 72 FR 45663, Aug. 15, 2007; 73 FR 39264, July 9, 2008; 76 FR 34885, June 15, 2011]

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§180.439 Thifensulfuron methyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of thifensulfuron methyl, including its metabolites and 

degradates, in or on the commodities listed in the following table [below]. Compliance with the tolerance levels specified in 

the following table [below] is to be determined by measuring only thifensulfuron methyl (methyl 3-[[[[(4-methoxy-6-

methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino] sulfonyl]-2-thiophenecarboxylate).

Commodity Parts per million

Barley, grain 0.05

Barley, hay 0.8

Barley, straw 0.10

Canola, seed 0.02

Chicory, roots 0.01

Chicory, tops 0.01

Corn, field, forage 0.10

Corn, field, grain 0.05

Corn, field, stover 0.10

Cotton, gin byproducts 0.02

Cotton, undelinted seed 0.02

Flax, seed 0.02

Oat, forage 0.2

Oat, grain 0.05

Oat, hay 0.05

Oat, straw 0.10

Rice, grain 0.05

Rice, straw 0.05

Sorghum, grain, forage. 0.05

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.05

Soybean 0.10

Wheat, forage 2.5

Wheat, grain 0.05

Wheat, hay 0.7

Wheat, straw 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of thifensulfuron methyl, including 

its metabolites and degradates, in or on the commodities listed in the following table [below]. Compliance with the 

tolerance levels specified in the following table [below] is to be determined by measuring only thifensulfuron methyl 

(methyl 3-[[[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino] sulfonyl]-2-thiophenecarboxylate).

Commodity Parts per million

Safflower, seed 0.05

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 55982, Sept. 17, 2004, as amended at 69 FR 63957, Nov. 3, 2004; 72 FR 13184, Mar. 21, 2007; 73 FR 47075, Aug. 13, 

2008; 75 FR 19277, Apr. 14, 2010; 77 FR 52240, Aug. 29, 2012]

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§180.440 Tefluthrin; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide tefluthrin (2,3,5,6 tetrafluroro-4-

methylphenyl)methyl-(1 alpha, 3 alpha)-(Z)-(±)-3(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-diemthylcyclopropanecarboxylate) 

and its metabolite (Z)-3-(2-chloro-3,3,3-trifluroro-1-propenyl)-2,2-dimethylcyclopropanecarboxylic acid in or on the 

following commodities:

Commodity Parts per million

Corn, field, forage 0.06 

Corn, field, grain 0.06 

Corn, field, stover 0.06 

Corn, pop, grain 0.06 

Corn, pop, stover 0.06 

Corn, sweet, forage 0.06 

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Corn, sweet, kernel plus cob with husks removed 0.06

Corn, sweet, stover 0.06

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 62961, Nov. 26, 1997, as amended at 74 FR 46375, Sept. 9, 2009]

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§180.441 Quizalofop ethyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the herbicide quizalofop ethyl, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only those quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline, 

expressed as the stoichiometric equivalent of quizalofop ethyl, in or on the commodity.

Commodity

Parts per

million

Barley, grain 0.05

Barley, hay 0.05

Barley, straw 0.05

Bean, dry, seed 0.4

Bean, succulent 0.25

Beet, sugar, molasses 0.2

Beet, sugar, roots 0.1

Beet, sugar, tops 0.5

Cotton, undelinted seed 0.1

Cowpea, forage 3.0

Cowpea, hay 3.0

Crambe, meal 2.0

Flax, seed 0.05

Gold of pleasure, meal 2.0

Lentil, seed 0.05

Pea, dry 0.25

Pea, field, hay 3.0

Pea, field, vines 3.0

Pea, succulent 0.3

Peppermint, tops 2.0

Rapeseed, meal 2.0

Rapeseed subgroup 20A, except flax, seed 1.5

Sorghum, grain, aspirated grain fractions 1.0

Sorghum, grain, forage 0.20

Sorghum, grain, grain 0.20

Sorghum, grain, stover 0.30

Soybean, flour 0.5

Soybean, hulls 0.02

Soybean, meal 0.5

Soybean, seed 0.05

Soybean, soapstock 1.0

Spearmint, tops 2.0

Sunflower, seed 1.9

Wheat, forage 0.05

Wheat, grain 0.05

Wheat, hay 0.05

Wheat, straw 0.05

(2) Tolerances are established for residues of the herbicide quizalofop ethyl, including its metabolites and degradates, 

in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be

determined by measuring only those quizalofop ethyl residues convertible to quizalofop (2-[4-(6-chloroquinoxalin-2-yl-oxy)

phenoxy]propanoic acid), expressed as quizalofop, in or on the commodity.

Commodity Parts per million

Cattle, fat 0.05

Cattle, meat 0.02

Cattle, meat byproducts 0.05

Egg 0.02

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Goat, fat 0.05

Goat, meat 0.02

Goat, meat byproducts 0.05

Hog, fat 0.05

Hog, meat 0.02

Hog, meat byproducts 0.05

Horse, fat 0.05

Horse, meat 0.02

Horse, meat byproducts 0.05

Milk 0.01

Milk, fat 0.25

Poultry, fat 0.05

Poultry, meat 0.02

Poultry, meat byproducts 0.05

Sheep, fat 0.05

Sheep, meat 0.02

Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of the 

herbicide quizalofop ethyl, including its metabolites and degradates, in or on the commodities in the following table. 

Compliance with the tolerance levels specified in the following table is to be determined by measuring only those 

quizalofop ethyl residues convertible to 2-methoxy-6-chloroquinoxaline, expressed as the stoichiometric equivalent of 

quizalofop ethyl, in or on the commodity.

Commodity Parts per million

Pineapple 0.1

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 32759, June 16, 1998, as amended at 70 FR 7870, Feb. 16, 2005; 71 FR 56378, Sept. 27, 2006; 76 FR 56045, Sept. 15, 

2010; 77 FR 23630, Apr. 20, 2012]

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§180.442 Bifenthrin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide bifenthrin, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)

-2,2-dimethylcyclopropanecarboxylate.

Commodity Parts per million

Almond, hulls 2.0 

Artichoke, globe 1.0

Banana1 0.1 

Beet, garden, roots 0.45

Beet, garden, tops 15

Brassica, head and stem, subgroup 5A, except cabbage 0.6

Brassica, leafy greens, subgroup 5B 3.5

Bushberry subgroup 13-07B 1.8

Cabbage 4.0

Caneberry subgroup 13A 1.0

Cattle, fat 1.0

Cattle, meat byproducts 0.10

Cattle, meat 0.5

Coriander, dried leaves 25

Coriander, leaves 6.0

Coriander, seed 5.0

Corn, field, forage 3.0 

Corn, field, grain 0.05 

Corn, field, stover 5.0 

Corn, pop, grain 0.05 

Corn, pop, stover 5.0 

Corn, sweet, forage 3.0 

Corn, sweet, kernel plus cob with husk removed 0.05

Corn, sweet, stover 5.0 

Cotton, undelinted seed 0.5

Eggplant 0.05

Egg 0.05

Fruit, citrus, group 10 0.05 

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Goat, fat 1.0

Goat, meat byproducts 0.10

Goat, meat 0.5

Grain, aspirated fractions 70

Grape 0.2

Groundcherry 0.5

Herb subgroup 19A 0.05 

Hog, fat 1.0

Hog, meat byproducts 0.10

Hog, meat 0.5

Hop, dried cones 10.0

Horse, fat 1.0

Horse, meat byproducts 0.10

Horse, meat 0.5

Leafy petioles subgroup 4B 3.0

Lettuce, head 3.0

Mayhaw 1.4

Milk, fat (reflecting 0.1 ppm in whole milk) 1.0

Nut, tree, group 14 0.05 

Okra 0.50

Pea and bean, dried shelled, expect soybean, subgroup 6C 0.15

Pea and bean, succulent shelled, subgroup 6B 0.05

Peanut 0.05

Pear 0.5 

Pepino 0.5

Pepper, bell 0.5 

Pepper, nonbell 0.5

Pistachio 0.05

Poultry, fat 0.05

Poultry, meat byproducts 0.05

Poultry, meat 0.05

Radish, tops 4.5

Rapeseed, seed 0.05

Sheep, fat 1.0

Sheep, meat byproducts 0.1

Sheep, meat 0.5

Soybean, hulls 0.50

Soybean, refined oil 0.30

Soybean, seed 0.2

Spinach 0.2 

Strawberry 3.0

Tea, dried1 30

Tomato 0.15

Turnip, greens 3.5

Vegetable, cucurbit, group 9 0.4

Vegetable, legume, edible podded, subgroup 6A 0.6

Vegetable, root, subgroup 1B except sugar beet and garden beet 0.10

Vegetable, tuberous and corm, subgroup 1C 0.05

1

There are no U.S. registrations.

(2) A tolerance of 0.05 ppm is established for residues of the insecticide bifenthrin, (2-methyl[1,1′-biphenyl]-3-yl)

methyl-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethylcyclopropane-carboxylate, as follows:

(i) In or on all food/feed items (other than those covered by a higher tolerance as a result of use on growing crops) in 

food/feed handling establishments.

(ii) The insecticide may be present as a residue from application of bifenthrin in food handling establishments, 

including food service, manufacturing and processing establishments, such as restaurants, cafeterias, supermarkets, 

bakeries, breweries, dairies, meat slaughtering and packing plants, and canneries, feed handling establishments including 

feed manufacturing and processing establishments, in accordance with the following prescribed conditions:

(A) Application shall be limited to general surface and spot and/or crack and crevice treatment in food/feed handling 

establishments where food/feed and food/feed products are held, processed, prepared and served. General surface 

application may be used only when the facility is not in operation provided exposed food/feed has been covered or 

removed from the area being treated. Spot and/or crack and crevice application may be used while the facility is in 

operation provided exposed food/feed is covered or removed from the area being treated prior to application. Spray 

concentration shall be limited to a maximum of 0.06 percent active ingredient. Contamination of food/feed or food/feed 

contact surfaces shall be avoided.

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(B) To assure safe use of the insecticide, its label and labeling shall conform to that registered with the U.S. 

Environmental Protection Agency and shall be used in accordance with such label and labeling. 

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide 

bifenthrin, including its metabolites and degradates, in connection with use of the pesticide under a Section 18 emergency 

exemption granted by EPA. Compliance with the tolerance levels specified below is to be determined by measuring only 

bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)

-2,2-dimethylcyclopropanecarboxylate. These tolerances will expire and are revoked on the dates specified in the following 

table:

Commodity Parts per million Expiration/revocation date

Apple 0.5 12/31/15

Nectarine 0.5 12/31/15

Peach 0.5 12/31/15

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

insecticide bifenthrin, including its metabolites and degradates, in or on the commodities in the table below. Compliance 

with the tolerance levels specified below is to be determined by measuring only bifenthrin, (2-methyl [1,1′-biphenyl]-3-yl) 

methyl-3-(2-chloro-3,3,3,-trifluoro-1-propenyl)-2,2-dimethylcyclopropanecarboxylate.

Commodity Parts per million

Grass, forage 4.0

Grass, hay 15

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 31002, June 6, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.442, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.443 Myclobutanil; tolerances for residues.

(a) General. Tolerances are established for combined residues of the fungicide myclobutanil alpha-butylalpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile and its alcohol metabolite (alpha-(3-hydroxybutyl)

-alpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile (free and bound), in or on the following food commodities: 

Commodity Parts per million

Almond 0.1

Almond, hulls 2.0

Apple 0.5

Apple, dry pomace 5.0

Apple, wet pomace 5.0

Artichoke, globe 0.90

Asparagus 0.02 

Banana, postharvest 4.0

Bean, snap, succulent 1.0 

Caneberry subgroup 13A 2.0 

Canistel 3.0

Cattle, fat 0.05

Cattle, liver 1.0

Cattle, meat 0.1

Cattle, meat byproducts, except liver 0.2

Cherry, sweet 5.0

Cherry, tart 5.0

Cilantro, leaves 9.0

Cotton, undelinted seed 0.02

Currant 3.0 

Egg 0.02

Fruit, stone, except cherry 2.0

Goat, fat 0.05

Goat, liver 1.0

Goat, meat 0.1

Goat, meat byproducts, except liver 0.2

Gooseberry 2.0 

Grain, aspirated fractions 35

Grape 1.0

Grape, dried pomace 10.0 

Grape, raisin 10.0

Grape, raisin, waste 25.0

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Grape, wet pomace 10.0 

Hog, fat 0.05

Hog, liver 1.0

Hog, meat 0.1

Hog, meat byproducts, except liver 0.2

Hop, dried cones 10

Horse, fat 0.05

Horse, liver 1.0

Horse, meat 0.1

Horse, meat byproducts, except liver 0.2

Leafy greens, subgroup 4A, except spinach 9.0

Mango 3.0

Mayhaw 0.70 

Milk 0.2

Okra 4.0

Papaya 3.0

Peppermint, tops 3.0 

Plum, prune, dried 8.0

Poultry, fat 0.02

Poultry, meat 0.02

Poultry, meat byproducts 0.02

Sapodilla 3.0

Sapote, black 3.0

Sapote, mamey 3.0

Sheep, fat 0.05

Sheep, liver 1.0

Sheep, meat 0.1

Sheep, meat byproducts, except liver 0.2

Soybean, forage 3.5

Soybean, hay 15

Soybean, refined oil 0.40

Soybean, seed 0.25

Spearmint, tops 3.0 

Star apple 3.0

Strawberry 0.50 

Tomato 0.30 

Tomato, puree 0.50 

Tomato, paste 1.0 

Vegetable, cucurbit, group 9 0.20

Vegetable, fruiting, group 8, except tomato 4.0

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide myclobutanil alpha-butylalpha-(4-chlorophenyl)-1H-1,2,4-triazole-1-propanenitrile in or on the following food commodities: 

Commodity Parts per million 

Animal feed, nongrass, group 18 0.03 

Grain, cereal, forage, fodder and straw, group 16 0.03 

Grain, cereal, group 15 0.03 

Vegetable, brassica, leafy, group 5 0.03 

Vegetable, foliage of legume, group 7 0.03 

Vegetable, fruiting, group 8 0.03 

Vegetable, leafy, except brassica, group 4 0.03 

Vegetable, leaves of root and tuber, group 2 0.03 

Vegetable, legume, group 6 0.03 

Vegetable, root and tuber, group 1 0.03

[54 FR 6131, Feb. 8, 1989]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.443, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.444 Sulfur dioxide; tolerances for residues.

(a) General. A tolerance is established as follows for sulfite residues of the fungicide sulfur dioxide (determined as 

(SO2)) in or on the following raw agricultural commodity(ies):

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Commodity Parts per million

Grape, postharvest 10.0

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

residues of sulfur dioxide, including its metabolites and degradates in or on the specified agricultural commodities, 

resulting from use of the pesticide pursuant to FFIFRA section 18 emergency exemptions. Compliance with the tolerance 

levels specified below is to be determined by measuring only sulfur dioxide (SO2). The tolerances expire on the date 

specified in the table.

Commodity

Parts per

million Expiration/revocation date

Fig 10 12/31/14

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[54 FR 20126, May 10, 1989, as amended at 76 FR 56648, Sept. 14, 2011]

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§180.445 Bensulfuron methyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide bensulfuron methyl (methyl-2[[[[[(4,6-dimethoxypyrimidin-2-yl) amino] carbonyl] amino] sulfonyl] methyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million

Crayfish 0.05

Rice, grain 0.02

Rice, straw 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 9435, Feb. 25, 1998]

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§180.446 Clofentezine; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide clofentezine, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only clofentezine, 3,6-bis(2-chlorophenyl)-1,2,4,5-tetrazine, in or on the 

commodity.

Commodity Parts per million

Almond, hulls 5.0

Almond 0.5

Apple 0.5 

Apple, dry pomace 3.0 

Apple, wet pomace 3.0 

Apricot 1.0

Cherry 1.0

Grape 1.0

Nectarine 1.0

Peach 1.0

Pear 0.5

Persimmon 0.05

Walnut 0.02

(2) Tolerances are established for residues of the insecticide clofentezine, including its metabolites and degradates, in 

or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is to 

be determined by measuring only the sum of clofentezine, 3,6-bis(2-chlorophenyl)-1,2,4,5-tetrazine, and its metabolite, 

3-(2-chloro-4-hydroxyphenyl)-6-(2-chlorophenyl)-1,2,4,5-tetrazine, calculated as the stoichiometric equivalent of 

clofentezine, in or on commodity.

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Commodity Parts per million

Cattle, fat 0.05

Cattle, liver 0.4

Cattle, meat 0.05

Cattle, meat byproducts, except liver 0.05

Goat, fat 0.05

Goat, liver 0.4

Goat, meat 0.05

Goat, meat byproducts, except liver 0.05

Hog, fat 0.05

Hog, liver 0.4

Hog, meat 0.05

Hog, meat byproducts, except liver 0.05

Horse, fat 0.05

Horse, liver 0.4

Horse, meat 0.05

Horse, meat byproducts, except liver 0.05

Milk 0.01

Sheep, fat 0.05

Sheep, liver 0.4

Sheep, meat 0.05

Sheep, meat byproducts, except liver 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[56 FR 15503, Apr. 17, 1991, as amended at 56 FR 22335, May 15, 1991; 59 FR 26947, May 25, 1994; 60 FR 12709, Mar. 8, 1995; 

64 FR 19050, Apr. 19, 1999; 70 FR 11572, Mar. 9, 2005; 74 FR 46375, Sept. 9, 2009; 76 FR 23496, Apr. 27, 2011]

 Back to Top

§180.447 Imazethapyr; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, applied as its acid or ammonium salt, in or on 

the following raw agricultural commodities: 

Commodity Parts per million 

Canola, seed1 0.10

Soybean 0.1

Vegetable, legume, group 6 0.1

1 There are no U.S. registrations for canola as of March 21, 2003.

(2) Tolerances are established for the sum of the residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid; its metabolite CL 288511, 2-[4,5-dihydro-4-

methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine carboxylic acid; and its metabolite CL 

182704, 5-[1-(beta-D-glucopyranosyloxy)ethyl]-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-3-

pyridinecarboxylic acid, applied as its acid or ammonium salt, in or on the following commodities: 

Commodity Parts per million 

Alfalfa, seed 0.15

Alfalfa, seed screenings 0.15

Animal feed, nongrass, group 18, forage 3.0

Animal feed, nongrass, group 18, hay 5.5

Peanut 0.1

Rice, bran 1.2

Rice, grain 0.3

Rice, straw 0.4

(3) A tolerance is established for the sum of residues of the herbicide imazethapyr, 2-[4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo- 1H-imidazol-2-yl]-5-ethyl-3-pyridine carboxylic acid, and its metabolite CL 288511, 2-[4,5-dihydro4-methyl-4-(1-methylethyl)-5- oxo-1H-imidazol-2-yl]-5-(1-hydroxyethyl)-3-pyridine carboxylic acid, applied as its acid or 

ammonium salt, in or on the following commodities: 

Commodity Parts per million 

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Cattle, meat byproducts 0.10 

Corn, field, forage 0.1

Corn, field, grain 0.1

Corn, field, stover 0.1

Crayfish 0.15

Goat, meat byproducts 0.10

Hog, meat byproducts 0.10

Horse, meat byproducts 0.10

Sheep, meat byproducts 0.10

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l) of this chapter, 

are established for the sum of residues of the herbicide imazethapyr, 2- [4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1Himidazol-2-yl]-5-ethyl- 3-pyridine carboxylic acid, as its ammonium salt, and its metabolite, 2- [4,5-dihydro-4-methyl4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(1- hydroxyethyl)-3-pyridine carboxylic acid, both free and conjugated, applied 

as its acid or ammonium salt, in or on the following raw agricultural commodities: 

Commodity Parts per million

Endive 0.1

Lettuce, head 0.1

Lettuce, leaf 0.1

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 55331, Aug. 29, 2002, as amended at 68 FR 13849, Mar. 21, 2003; 71 FR 6359, Feb. 8, 2006; 76 FR 34885, June 15, 2011]

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§180.448 Hexythiazox; tolerance for residues.

(a) General. Tolerances are established for residues of hexythiazox, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety, 

calculated as the stoichiometric equivalent of hexythiazox.

Commodity Parts per million

Almond, hulls 10 

Apple, wet pomace 0.40

Berry, low growing, subgroup 13-07G 6

Caneberry subgroup 13-07A 1

Cattle, fat 0.05

Cattle, meat byproducts 0.5

Citrus, dried pulp 0.60

Citrus, oil 24

Corn, field, forage 3.0

Corn, field, grain 0.02

Corn, field, stover 7.0

Date, dried fruit 1.0

Egg 0.05

Fruit, pome, group 11-10 0.4

Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 1

Fruit, stone, group 12 1.0

Goat, fat 0.05

Goat, meat byproducts 0.5

Grain, aspirated fractions 5

Hog, fat 0.02

Hog, meat byproducts 0.05

Hop, dried cones 2.0

Horse, fat 0.05

Horse, meat byproducts 0.5

Milk 0.05

Nut, tree, group 14 0.30

Pepper/eggplant subgroup 8-10B 1.5

Peppermint, tops 2.0

Pistachio 0.30

Plum, prune, dried 1.3

Poultry, fat 0.05

Poultry, meat byproducts 0.05

Sheep, fat 0.05

Sheep, meat byproducts 0.5

Spearmint, tops 2.0

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Tomato 0.50

(b) Section 18 emergency exemptions. A time-limited tolerance specified in the following table is established for 

residues of hexythiazox and its metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety, 

calculated as the stoichiometric equivalent of hexythiazox, in or on the specified agricultural commodity, resulting from use 

of the pesticide pursuant to FIFRA section 18 emergency exemptions. The tolerance expires on the date specified in the 

table.

Commodity

Parts per

million

Expiration

date

Beet, sugar, root 0.15 12/31/19

(c) Tolerances with regional registrations. Tolerances with regional registrations as defined by §180.1(l), are 

established for residues of hexythiazox, including its metabolites and degradates, in or on the commodities in the table 

below. Compliance with the tolerance levels specified below is to be determined by measuring only hexythiazox and its 

metabolites containing the (4-chlorophenyl)-4-methyl-2-oxo-3-thiazolidine moiety, calculated as the stoichiometric 

equivalent of hexythiazox.

Commodity Parts per million

Alfalfa, forage (EPA Regions 9-11 only) 15

Alfalfa, hay (EPA Regions 9-11 only) 30

Bean, dried, seed (EPA Regions 7-12 only) 0.4

Bean, succulent (EPA Regions 7-12 only) 0.3

Corn, field, forage 6.0

Corn, field, grain 0.02

Corn, field, stover 2.5

Corn, sweet, forage (EPA Regions 7-12 only) 4.0

Corn, sweet, kernel plus cob with husks removed (EPA Regions 7-12 only) 0.1

Cotton, gin byproducts, CA and AZ only 3.0

Cotton, undelinted seed, CA and AZ only 0.20

Fruit, citrus group 10 (CA, AZ, TX only) 0.35

Potato 0.02

Sorghum, grain, forage (EPA Regions 6-8 only) 5

Sorghum, grain, grain (EPA Regions 6-8 only) 3

Sorghum, grain, stover (EPA Regions 6-8 only) 6

Timothy, forage (EPA Regions 9-11 only) 40

Timothy, hay (EPA Regions 9-11 only) 40

Wheat, forage (EPA Region 11 only) 6.0

Wheat, grain (EPA Region 11 only) 0.02

Wheat, hay (EPA Region 11 only) 30

Wheat, straw (EPA Region 11 only) 8.0

(d) Indirect or inadvertent residues. [Reserved]

[54 FR 17948, Apr. 26, 1989]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.448, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.449 Avermectin B1 and its delta-8,9-isomer; tolerances for residues.

(a) General. Tolerances are established for residues of abamectin, including its metabolites and degradates, in or on 

the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only avermectin B1 a mixture of avermectins containing greater than or equal to 80% 

avermectin B1 a (5-O-demethyl avermectin A1) and less than or equal to 20% avermectin B1b (5-O-demethyl-25-de

(1-methylpropyl)-25-(1-methylethyl) avermectin A1) and its delta-8,9-isomer in or on the following commodities:

Commodity

Parts per 

million

Almond, hulls 0.10

Apple 0.020

Apple, wet pomace 0.10

Avocado 0.020

Bean, dry, seed 0.01

Cattle, fat 0.03

Cattle, meat 0.02

Cattle, meat byproducts 0.06

Celeriac, roots 0.05

Celeriac, tops 0.05

Chive, dried leaves 0.02

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Chive, fresh leaves 0.01

Citrus, dried pulp 0.10

Citrus, oil 0.10

Citrus 0.02

Cotton, gin byproducts 1.0

Cotton, undelinted seed 0.02

Food products in food handling establishments (other than those already covered by higher tolerances as a result of use on growing crops, and 

other than those already covered by tolerances on milk, meat, and meat byproducts)

0.01

Fruit, stone, group 12 0.09 

Goat, fat 0.01 

Goat, meat 0.02

Goat, meat byproducts 0.02

Grape 0.02

Herb subgroup 19A, except chive 0.030

Hog, fat 0.01 

Hog, meat 0.02

Hog, meat byproducts 0.02

Hop, dried cones 0.20

Horse, fat 0.01 

Horse, meat 0.02

Horse, meat byproducts 0.02

Milk 0.005

Nut, tree, group 14 0.01 

Onion, bulb, subgroup 3-07A 0.01

Pear 0.02

Peppermint, tops 0.010 

Pistachio 0.01 

Plum, prune, dried 0.025

Poultry, meat 0.02

Poultry, meat byproducts 0.02

Sheep, fat 0.01

Sheep, meat 0.02

Sheep, meat byproducts 0.02

Spearmint, tops 0.010 

Strawberry 0.05

Vegetable, cucurbit, group 9 0.005

Vegetable, fruiting, group 8 0.020

Vegetable, leafy, except brassica, group 4 0.10

Vegetable, tuberous and corm, subgroup 01C 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 44095, Aug. 19, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.449, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.450 Beta-(4-Chlorophenoxy)-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide β-(4-chlorophenoxy)

-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol (triadimenol) and its butanediol metabolite, 4-(4-chlorophenoxy)

-2,2-dimethyl-4-(1H-1,2,4-triazol-l-yl)-1,3-butanediol, calculated as triadimenol, in or on the following commodities:

Commodity Parts per million Expiration/Revocation Date 

Banana1 0.2 None

Barley, grain 0.05 None

Barley, straw 0.2 None

Corn, field, forage 0.05 None

Corn, field, grain 0.05 None

Corn, field, stover 0.05 None

Corn, pop, grain 0.05 None

Corn, pop, stover 0.05 None

Corn, sweet, forage 0.05 None

Corn, sweet, kernel plus cob with husks removed 0.05 None

Corn, sweet, stover 0.05 None

Cotton, undelinted seed 0.02 None

Oat, forage 2.5 None

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Oat, grain 0.05 None

Oat, straw 0.2 None

Rye, forage 2.5 None

Rye, grain 0.05 None

Rye, straw 0.1 None

Wheat, forage 2.5 None

Wheat, grain 0.05 None

Wheat, straw 0.2 None

1

There are no U.S. registrations for banana (whole) as of September 22, 1993.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54962, Sept. 24, 2008, as amended at 74 FR 47457, Sept. 16, 2009; 76 FR 34885, June 15, 2011]

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§180.451 Tribenuron methyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide tribenuron methyl and its metabolites and 

degradates in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be 

determined by measuring only tribenuron methyl, methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino] 

carbonyl] amino] sulfonyl] benzoate, in or on the following commodities:

Commodity Parts per million

Barley, grain 0.05

Barley, hay 0.4

Barley, straw 0.10

Canola, seed 0.02

Corn, field, forage 0.15

Corn, field, grain 0.01

Corn, field, stover 1.1

Cotton, gin byproducts 0.02

Cotton, undelinted seed 0.02

Flax, seed 0.02

Grain, aspirated fractions 1.5

Oat, forage 0.05

Oat, grain 0.05

Oat, hay 0.05

Oat, straw 0.10

Rice, grain 0.05

Rice, straw 0.05

Sorghum, grain, forage 0.05

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.05

Soybean, forage 0.07

Soybean, hay 0.35

Soybean, hulls 0.04

Soybean, seed 0.01

Sunflower, seed 0.05

Wheat, forage 0.3

Wheat, grain 0.05

Wheat, hay 0.5

Wheat, straw 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l) are established 

for residues of the herbicide tribenuron methyl (methyl-2-[[[[N-(4-methoxy-6-methyl-1,3,5-triazin-2-yl) methylamino] 

carbonyl]amino]sulfonyl] benzoate) in or on the following raw agricultural commodities:

Commodity Parts per million

Grass, forage, fodder and hay, group 17, except bermudagrass; forage 0.10

Grass, forage, fodder and hay, group 17, except bermudagrass; hay 0.10

(d) Indirect or inadvertent residues. [Reserved]

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[69 FR 56718, Sept. 22, 2004, as amended at 72 FR 11789, Mar. 14, 2007; 73 FR 47065, Aug. 13, 2008; 74 FR 67128, Dec. 18, 

2009; 76 FR 34885, June 15, 2011]

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§180.452 Primisulfuron-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of primisulfuron-methyl (3-[4,6-bis-(difluoromethoxy)-pyrimidin-2-

yl]-1-(2-methoxycarbonylphenylsulfonyl) urea) in or on the following raw agricultural commodities.

Commodity Parts per million

Cattle, fat 0.10

Cattle, meat 0.10

Cattle, meat byproducts 0.10

Corn, field, forage 0.10 

Corn, field, grain 0.02 

Corn, field, stover 0.10 

Corn, pop, grain 0.02 

Corn, pop, stover 0.10 

Egg 0.10

Goat, fat 0.10

Goat, meat 0.10

Goat, meat byproducts 0.10

Hog, fat 0.10

Hog, meat 0.10

Hog, meat byproducts 0.10

Horse, fat 0.10

Horse, meat 0.10

Horse, meat byproducts 0.10

Milk 0.02

Poultry, fat 0.10

Poultry, meat 0.10

Poultry, meat byproducts 0.10

Sheep, fat 0.10

Sheep, meat 0.10

Sheep, meat byproducts 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved] 

[55 FR 21548, May 25, 1990, as amended at 62 FR 66020, Dec. 17, 1997; 63 FR 66458, Dec. 2, 1998; 67 FR 35049, May 17, 2002; 

74 FR 46375, Sept. 9, 2009; 74 FR 46699, Sept. 11, 2009; 77 FR 59128, Sept. 26, 2012]

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§180.454 Nicosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide nicosulfuron, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only nicosulfuron, 2-[[[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]amino]

sulfonyl]-N,N-dimethyl-3-pyridinecarboxamide.

Commodity Parts per million

Cattle, fat 0.01

Cattle, meat 0.01

Cattle, meat byproducts 0.05

Corn, field, forage 0.1

Corn, field, grain 0.1

Corn, field, stover 0.1

Corn, pop, grain 0.1

Corn, pop, stover 0.1

Corn, sweet, forage 0.1

Corn, sweet, kernel plus cob with husks removed 0.1

Corn, sweet, stover 0.1

Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.05

Grass, forage 9.0

Grass, hay 25.0

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Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.05

Milk 0.01

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.05

Sorghum, grain, forage 0.3

Sorghum, grain, grain 0.8

Sorghum, grain, stover 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 17578, Apr. 7, 2010, as amended at 80 FR 68265, Nov. 4, 2015]

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§180.455 Procymidone; tolerances for residues.

A tolerance is established for the residues of the fungicide procymidone, N-(3,5-dichlorophenyl)

-1,2-dimethylcyclopropane-1,2 dicarboximide, in or on the following raw agricultural commodity:

Commodity Parts per million

Grape, wine 5.0

[59 FR 42514, Aug. 18, 1994]

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§180.457 Bitertanol; tolerances for residues.

(a) General. A tolerance is established for the residues of the fungicide bitertanol, β-([1,1′-biphenyl]-4-yloxy)

-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, in or on the following raw agricultural commodity:

Commodity Parts per million

Banana1 0.5

1

There are no U.S. registrations as of April 1, 1992.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 47457, Sept. 16, 2009]

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§180.458 Clethodim; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide clethodim, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of clethodim, 2-[(1E)-1-[[[(2E)-3-chloro-2-propenyl]oxy]imino]

propyl]-5-[2-(ethylthio)propyl]-3-hydroxy-2-cyclohexen-1-one, and its metabolites containing the 5-(2-ethylthiopropyl)

cyclohexene-3-one and 5-(2-ethylthiopropyl)-5-hydroxycyclohexene-3-one moieties and their sulphoxides and sulphones, 

calculated as the stoichiometric equivalent of clethodim, in or on the commodity.

Commodity Parts per million

Alfalfa, forage 6.0

Alfalfa, hay 10

Artichoke, globe 1.2

Asparagus 1.7

Bean, dry, seed 2.5

Beet, sugar, molasses 1.0

Beet, sugar, roots 0.20

Beet, sugar, tops 1.0

Brassica, head and stem, subgroup 5A 3.0

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Brassica, leafy greens, subgroup 5B 3.0

Bushberry subgroup 13-07B 0.20

Caneberry subgroup 13-07A 0.30

Canola, meal 1.0

Canola, seed 0.50

Cattle, fat 0.2

Cattle, meat 0.2

Cattle, meat byproducts 0.2

Clover, forage 10.0

Clover, hay 20.0

Corn, field, forage 0.2

Corn, field, grain 0.2

Corn, field, stover 0.2

Cotton, meal 2.0

Cotton, undelinted seed 1.0

Cranberry 0.50

Egg 0.2

Flax, meal 1.0

Flax, seed 0.6

Goat, fat 0.2

Goat, meat 0.2

Goat, meat byproducts 0.2

Herb subgroup 19A 12.0

Hog, fat 0.2

Hog, meat 0.2

Hog, meat byproducts 0.2

Hop, dried cones 0.5

Horse, fat 0.2

Horse, meat 0.2

Horse, meat byproducts 0.2

Leaf petioles subgroup 4B 0.60

Leafy greens subgroup 4A 2.0

Melon subgroup 9A 2.0

Milk 0.05

Mustard, seed 0.50

Onion, bulb 0.20

Onion, green 2.0

Peach 0.20

Peanut 3.0

Peanut, hay 3.0

Peanut, meal 5.0

Peppermint, tops 5.0

Potato 0.5

Potato, granules/flakes 2.0

Poultry, fat 0.2

Poultry, meat 0.2

Poultry, meat byproducts 0.2

Radish, tops 0.70

Safflower, meal 10.0

Safflower, seed 5.0

Sesame, seed 0.35

Sheep, fat 0.2

Sheep, meat 0.2

Sheep, meat byproducts 0.2

Soybean 10.0

Spearmint, tops 5.0

Squash/cucumber subgroup 9B 0.50

Strawberry 3.0

Sunflower, meal 10.0

Sunflower, seed 5.0

Turnip, greens 3.0

Vegetable, fruiting group 8 1.0

Vegetable, legume, group 6, except soybean 3.5

Vegetable, root, except sugar beet, subgroup 1B 1.0

Vegetable, tuberous and corm, subgroup 1C 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23496, Apr. 27, 2011, as amended at 77 FR 59128, Sept. 26, 2012]

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§180.459 Triasulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide triasulfuron [3-(6-methoxy-4-methyl-1,3,5-triazin2-yl)-1-(2-(2-chloroethoxy)phenylsulfonyl)urea] in or on the following raw agricultural commodities:

Commodity Parts per million

Barley, grain 0.02

Barley, straw 2.0

Cattle, fat 0.1

Cattle, kidney 0.5

Cattle, meat byproducts, except kidney 0.1

Cattle, meat 0.1

Goat, fat 0.1

Goat, kidney 0.5

Goat, meat byproducts, except kidney 0.1

Goat, meat 0.1

Grass, forage 7.0

Grass, hay 2.0

Hog, fat 0.1

Hog, kidney 0.5

Hog, meat byproducts 0.1

Hog, meat 0.1

Horse, fat 0.1

Horse, kidney 0.5

Horse, meat byproducts, except kidney 0.1

Horse, meat 0.1

Milk 0.02

Sheep, fat 0.1

Sheep, kidney 0.5

Sheep, meat byproducts, except kidney 0.1

Sheep, meat 0.1

Wheat, forage 5.0

Wheat, grain 0.02

Wheat, straw 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[60 FR 36731, July 18, 1995, as amended at 63 FR 44152, Aug. 18, 1998; 63 FR 66449, Dec. 2, 1998]

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§180.460 Benoxacor; tolerances for residues.

(a) General. Tolerances are established for residues of the inert ingredient (safener) benoxacor (4-(dichloroacetyl)

-3,4-dihydro-3-methyl-2H-1, 4-benzoxazine) at 0.01 parts per million (ppm) when used in pesticide formulations containing 

metolachlor or S-metolachlor in or on raw agricultural commodities for which tolerances have been established for 

metolachlor or S-metolachlor.

(b) Section 18 energency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 7305, Feb. 13, 1998, as amended at 70 FR 21631, Apr. 27, 2005]

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§180.461 Cadusafos; tolerances for residues.

A tolerance is established for the residues of the nematicide/insecticide cadusafos, O-ethyl S,S-di-sec-butyl 

phosphorodithioate, in or on the following raw agricultural commodity:

Commodity Parts per million

Banana 0.01

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There are no U.S. registrations as of May 10, 1994, for the nematicide/insecticid cadusafos.

[59 FR 39467, Aug. 3, 1994]

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§180.462 Pyridate; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide pyridate, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only the sum of pyridate, O-(6-chloro-3-phenyl-4-pyridazinyl)-S-octylcarbonothioate, and its metabolites, 6-chloro-3-phenyl-pyridazine-4-ol and conjugates of 6-chloro-3-phenyl-pyridazine-4-ol, 

calculated as the stoichiometric equivalent of pyridate, in or on the commodity.

Commodity Parts per million

Brassica, head and stem, subgroup 5A 0.03

Cabbage 0.03

Chickpea, seed 0.1

Collards 0.03

Corn, field, forage 0.03

Corn, field, grain 0.03 

Corn, field, stover 0.03 

Corn, pop, grain 0.03 

Corn, pop, stover 0.03 

Peanut 0.03

Peppermint, tops 0.20

Spearmint, tops 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[57 FR 54303, Nov. 18, 1992, as amended at 62 FR 44558, Aug. 22, 1997; 63 FR 53844, Oct. 7, 1998; 64 FR 46298, Aug. 25, 1999; 

65 FR 25652, May 3, 2000; 67 FR 35049, May 17, 2002; 72 FR 35665, June 29, 2007; 74 FR 46376, Sept. 9, 2009; 76 FR 23496, 

Apr. 27, 2011]

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§180.463 Quinclorac; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a)(1) General. Tolerances are established for residues of the herbicide quinclorac, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only quinclorac, 3,7-dichloro-8-quinolinecarboxylic acid, in or on the 

commodity.

Commodity Parts per million

Barley, grain 2.0

Berry, low growing, except strawberry, subgroup 13-07H 1.5

Cattle, fat 0.7 

Cattle, meat byproducts 1.5 

Cattle, meat 0.05 

Egg 0.05 

Goat, fat 0.7 

Goat, meat byproducts 1.5 

Goat, meat 0.05 

Grain, aspirated fractions 1200

Grass, forage 150

Grass, hay 130

Hog, fat 0.7 

Hog, meat byproducts 1.5 

Hog, meat 0.05 

Horse, fat 0.7 

Horse, meat byproducts 1.5 

Horse, meat 0.05 

Milk 0.05 

Poultry, fat 0.05 

Poultry, meat byproducts 0.1 

Poultry, meat 0.05 

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Rhubarb 0.5

Rice, bran 15.0 

Rice, grain 5.0 

Rice, straw 12.0 

Sheep, fat 0.7 

Sheep, meat byproducts 1.5 

Sheep, meat 0.05 

Sorghum, grain, forage 3.0 

Sorghum, grain, grain 6.0 

Sorghum, grain, stover 1.0 

Wheat, forage 1.0 

Wheat, germ 0.75 

Wheat, grain 0.5 

Wheat, hay 0.5 

Wheat, straw 0.1

(2) Tolerances are established for residues of the herbicide quinclorac, including its metabolites and degradates, in or 

on the commodity in the following table. Compliance with the tolerance levels specified in this paragraph is to be 

determined by measuring only quinclorac, 3,7-dichloro-8-quinolinecarboxylic acid, and its methyl ester, 

methyl-3,7-dichloro-8-quinolinecarboxylate, calculated as the stoichiometric equivalent of quinclorac, in or on the 

commodity.

Commodity Parts per million

Rapeseed, subgroup 20A1 1.5

1

There are no U.S. Registrations.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the herbicide 

quinclorac, including its metabolites and degradates, in or on the commodity in the table in this paragraph. Compliance 

with the tolerance level specified in this paragraph is to be determined by measuring only quinclorac, 3,7-dichloro-8-

quinolinecarboxylic acid, in or on the commodity. The tolerance expires and is revoked on the date specified in the table in 

this paragraph.

Commodity Parts per million Expiration/revocation date

Cranberry 15.0 12/31/12

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[57 FR 47996, Oct. 21, 1992, as amended at 64 FR 6548, 6549, Feb. 10, 1999; 64 FR 14632, Mar. 26, 1999; 65 FR 33701, May 24, 

2000; 67 FR 35049, May 17, 2002; 72 FR 55073, Sept. 28, 2007; 74 FR 51490, Oct. 7, 2009; 74 FR 67090, Dec. 18, 2009; 76 FR 

23497, Apr. 27, 2011; 77 FR 75566, Dec. 21, 2012; 78 FR 71528, Nov. 29, 2013]

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§180.464 Dimethenamid; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide dimethenamid, 1(R,S)-2-chloro-N-[(1-methyl-2-

methoxy)ethyl]-N-(2,4-dimethylthien-3-yl)-acetamide, applied as either the 90:10 or 50:50 S:R isomers, in or on the 

following food commodities:

Commodity Parts per million

Bean, dry, seed 0.01

Beet, garden, roots 0.01

Beet, garden, tops 0.01

Beet, sugar, dried pulp 0.01

Beet, sugar, molasses 0.01

Beet, sugar, roots 0.01

Beet, sugar, tops 0.01

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Corn, pop, forage 0.01

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Corn, sweet, forage 0.01

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.01

Cotton, gin byproducts 1.5

Cottonseed subgroup 20C 0.01

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Garlic 0.01

Grass, forage 0.15

Grass, hay 2.5

Grass, seed screenings 0.01

Grass, straw 0.01

Hop, dried cones 0.05

Horseradish 0.01

Leek 0.01

Onion, bulb 0.01

Onion, green 0.01

Onion, Welsh 0.01

Peanut 0.01

Peanut, hay 0.01

Radish, roots 0.01

Radish, tops 0.01

Rutabaga, roots 0.01

Rutabaga, tops 0.1

Shallot, bulb 0.01

Shallot, fresh leaves 0.01

Sorghum, grain, forage 0.01

Sorghum, grain, grain 0.01

Sorghum, grain, stover 0.01

Soybean, seed 0.01

Turnip, greens 0.1

Turnip, roots 0.01

Turnip, tops 0.1

Vegetable, tuberous and corm, subgroup 1C 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for residues of 

dimethenamid, 1 (R,S)-2-chloro-N-[(1-methyl-2-methoxy) ethyl]-N-(2,4-dimethylthien-3-yl)-acetamide) in or on the following 

raw agricultural commodities:

Commodity Parts per million

Pumpkin 0.01

Squash, winter 0.01

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 51551, Aug. 24, 2000, as amended at 67 FR 46884, July 17, 2002; 69 FR 29459, May 24, 2004; 69 FR 57207, Sept. 24, 

2004; 70 FR 24712, May 11, 2005; 71 FR 25942, May 3, 2006; 71 FR 49354, Aug. 23, 2006; 72 FR 44388, Aug. 8, 2007; 72 FR 

73630, Dec. 28, 2007; 80 FR 9215, Feb. 20, 2015]

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§180.465 4-(Dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane.

(a) General. Tolerances are established for the residues of 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane, (CAS No. 

71526-07-3) when used as an inert ingredient (safener) in or on the following raw agricultural commodities: 

Commodity1 Parts per million 

Corn, field, forage 0.005 

Corn, field, grain 0.005 

Corn, field, stover 0.005 

Corn, pop, grain 0.005 

Corn, pop, stover 0.005 

1

There are no U.S. registered products containing 4-(dichloroacetyl)-1-oxa-4-azaspiro[4.5]decane as of June 17, 

2002.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 4392, Jan. 29, 2003]

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§180.466 Fenpropathrin; tolerances for residues.

(a) General. Tolerances are established for residues of fenpropathrin, including its metabolites and degradates, in or 

on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by 

measuring only fenpropathrin (alpha-cyano-3-phenoxy-benzyl 2,2,3,3 tetramethylcyclopropanecarboxylate).

Commodity Parts per million

Acerola 3.0

Almond, hulls 4.5

Atemoya 1.5

Avocado 1.0

Barley, grain 0.04

Barley, hay 3.0

Barley, straw 2.0

Berry, low growing, subgroup 13-07G 2.0

Biriba 1.5

Brassica, head and stem, subgroup 5A 3.0 

Bushberry subgroup 13-07B 3.0

Caneberry subgroup 13-07A 12

Canistel 1.0

Cattle, fat 1.0

Cattle, meat byproducts 0.1

Cattle, meat 0.1

Cherimoya 1.5

Cherry, sweet 5.0

Cherry, tart 5.0 

Citrus, dried pulp 4.0 

Citrus, oil 75 

Cotton, refined oil 3.0

Cotton, undelinted seed 1.0

Custard apple 1.5

Egg 0.05

Feijoa 3.0

Fruit, citrus, group 10-10 2.0

Fruit, pome, group 11-10 5.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 5.0

Fruit, stone, crop group 12, except cherry 1.4 

Goat, fat 1.0

Goat, meat byproducts 0.1

Goat, meat 0.1

Grape, raisin 10.0 

Guava 3.0

Hog, fat 1.0

Hog, meat byproducts 0.1

Hog, meat 0.1

Horse, fat 1.0

Horse, meat byproducts 0.1

Horse, meat 0.1

Ilama 1.5

Jaboticaba 3.0

Longan 7.0

Lychee 7.0

Mango 1.0

Melon subgroup 9A 0.5

Milk, fat (reflecting 0.08 ppm in whole milk) 2.0

Nut, tree, crop group 14 0.10

Olive 5.0 

Papaya 1.0 

Passionfruit 3.0

Pea, succulent 0.02

Peanut, hay 20.0

Peanut 0.01

Pistachio 0.10

Poultry, fat 0.05

Poultry, meat byproducts 0.05

Poultry, meat 0.05

Pulasan 7.0

Rambutan 7.0

Sapodilla 1.0

Sapote, black 1.0

Sapote, mamey 1.0

Sheep, fat 1.0

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Sheep, meat byproducts 0.1

Sheep, meat 0.1

Soursop 1.5

Spanish lime 7.0

Squash/Cucumber subgroup 9B 0.5

Star apple 1.0

Starfruit 3.0

Sugar apple 1.5

Tea, dried1 2.0

Vegetable, fruiting, group 8-10 1.0

Wax jambu 3.0

1

There are no U.S. registrations as of November 28, 2012, for the use of fenpropathrin on tea, dried.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63034, Nov. 26, 1997, as amended at 63 FR 48116, Sept. 9, 1998; 64 FR 3009, Jan. 20, 1999; 65 FR 11242, Mar. 2, 2000; 

65 FR 24397, Apr. 26, 2000; 65 FR 48620, Aug. 9, 2000; 66 FR 64774, Dec. 14, 2001; 67 FR 35049, May 17, 2002; 70 FR 38789, 

July 6, 2005; 70 FR 55747, Sept. 23, 2005; 74 FR 12606, Mar. 25, 2009; 77 FR 70908, Nov. 28, 2012; 78 FR 69569, Nov. 20, 2013]

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§180.467 Carbon disulfide; tolerances for residues.

Tolerances are established for the nematicide, insecticide, and fungicide carbon disulfide, from the application of 

sodium tetrathiocarbonate, in or on the following raw agricultural commodities:

Commodity Parts per million

Almond 0.1

Almond, hulls 0.1

Grape 0.1

Grapefruit 0.1

Lemon 0.1

Orange, sweet 0.1

Peach 0.1

Plum, prune, fresh 0.1

[58 FR 33771, June 21, 1993, as amended at 62 FR 26949, May 16, 1997]

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§180.468 Flumetsulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide flumetsulam, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only flumetsulam, N-(2,6-difluorophenyl)-5-methyl-(1,2,4)-triazolo-(1,5a)

-pyrimidine-2-sulfonamide, in or on the commodity.

Commodity Parts per million

Bean, dry, seed 0.05

Corn, field, forage 0.05

Corn, field, grain 0.05

Corn, field, stover 0.05

Soybean, seed 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23497, Apr. 27, 2011]

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§180.469 Dichlormid; tolerances for residues.

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(a) General. Tolerances are established for residues of dichlormid, including its metabolites and degradates, when 

used as an inert ingredient (herbicide safener) in pesticide formulations, in or on the commodities in the following table. 

Compliance with the tolerances is to be determined by measuring only dichlormid (2,2-dichloro-N,N-di-2-

propenylacetamide).

Commodity Parts per million 

Corn, field, forage 0.05 

Corn, field, grain 0.05 

Corn, field, stover 0.05 

Corn, pop, grain 0.05 

Corn, pop, stover 0.05 

Corn, sweet, forage 0.05 

Corn, sweet, kernel plus cob with husks removed 0.05 

Corn, sweet, stover 0.05

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 16149, Mar. 27, 2000, as amended at 67 FR 51105, Aug. 7, 2002; 69 FR 58290, Sept. 30, 2004; 70 FR 76699, Dec. 28, 

2005; 74 FR 37623, July 29, 2009; 76 FR 16310, Mar. 23, 2011]

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§180.470 Acetochlor; tolerances for residues.

(a) General. Tolerances are established for residues of acetochlor, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only acetochlor, 2-chloro-2'-methyl-6-ethyl-N-ethoxymethylacetanilide, and its metabolites containing the ethyl 

methyl aniline (EMA) moiety and the hydroxyethyl methyl aniline (HEMA) moiety. Both parent and the named metabolites 

shall be determined as ethyl methyl aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and calculated as the 

stoichiometric equivalents of acetochlor, in or on the following commodities:

Commodity Parts per million

Beet, sugar, dried pulp 0.50

Beet, sugar, molasses 0.80

Beet, sugar, roots 0.30

Beet, sugar, tops 0.70

Corn, field, forage 4.5

Corn, field, grain 0.05

Corn, field, stover 2.5

Corn, pop, grain 0.05

Corn, pop, stover 2.5

Corn, sweet, forage 1.5

Corn, sweet, kernels plus cob with husks removed 0.05

Corn, sweet, stover 1.0

Cotton, gin byproducts 4.0

Cotton, undelinted seed 0.6

Peanut 0.20

Peanut, hay 7.0

Peanut, meal 0.25

Sorghum, grain, forage 1.6

Sorghum, grain, grain 0.05

Sorghum, grain, stover 1.7

Soybean, meal 1.2

Soybean, seed 1.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of acetochlor, 

including its metabolites and degradates, in or on the raw agricultural commodities in the table to this paragraph when 

present therein as a result of application of acetochlor to the growing crops in the table to paragraph (a) of this section. 

Compliance with the tolerance levels specified below is to be determined by measuring only acetochlor, 2-chloro-2'-

methyl-6-ethyl-N-ethoxymethylacetanilide, and its metabolites containing the ethyl methyl aniline (EMA) moiety and the 

hydroxyethyl methyl aniline (HEMA) moiety. Both parent and the named metabolites shall be determined as ethyl methyl 

aniline (EMA) and hydroxyethyl methyl aniline (HEMA), and calculated as the stoichiometric equivalents of acetochlor, in 

or on the following commodities.

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Commodity Parts per million

Animal feed, nongrass, group 18, forage 1.3

Animal feed, nongrass, group 18, hay 3.5

Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, forage 0.5

Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, hay 2.0

Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, rice and wheat, stover 0.1

Grain, cereal, forage, fodder and straw, group 16, except corn, grain sorghum, and wheat, straw 0.3

Grain, cereal, group 15, except corn, grain sorghum, and wheat, grain 0.05

Pea and bean, dried shelled, except soybean, subgroup 6C 0.05

Potato 0.05

Soybean, forage 0.7

Soybean, hay 1.0

Sunflower, seed 0.05

Wheat, forage 0.5

Wheat, grain 0.02

Wheat, hay 2.0

Wheat, straw 0.1

[72 FR 27468, May 16, 2007, as amended at 74 FR 29969, June 24, 2009; 74 FR 47450, Sept. 16, 2009; 78 FR 13268, Feb. 27, 

2013; 79 FR 3517, Jan. 22, 2014]

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§180.471 Furilazole; tolerances for residues.

(a) General. Tolerances are established for residues of furilazole; 3-dichloroacetyl-5-(2-furanyl)-2, 

2-dimethyloxazolidine (CAS Reg. No. 121776-33-8) when used as an inert ingredient (safener) in pesticide formulations in 

or on the following raw agricultural commodities:

Commodity Parts per million

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Sorghum, forage 0.01

Sorghum, grain 0.01

Sorghum, stover 0.01

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 8867, Feb. 23, 2000, as amended at 67 FR 15735, Apr. 3, 2002; 72 FR 57492, Oct. 10, 2007]

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§180.472 Imidacloprid; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide imidacloprid, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl) methyl]-N-nitro-2-imidazolidinimine) and its 

metabolites containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid, in or on the 

following commodities:

Commodity Parts per million

Acerola 1.0

Almond, hulls 4.0

Apple 0.5

Apple, wet pomace 3.0

Artichoke, globe 2.5

Aspirated grain fractions 240

Atemoya 0.30

Avocado 1.0

Banana 0.50

Beet, sugar, molasses 0.30

Beet, sugar, roots 0.05

Beet, sugar, tops 0.50

Biriba 0.30

Blueberry 3.5

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Borage, seed 0.05

Caneberry, subgroup 13-A 2.5

Canistel 1.0

Canola, seed 0.05

Cattle, fat 0.30

Cattle, meat 0.30

Cattle, meat byproducts 0.30

Cherimoya 0.30

Citrus, dried pulp 5.0

Coffee, bean, green 0.80

Cotton, gin byproducts 4.0

Cotton, meal 8.0

Cotton, undelinted seed 6.0

Crambe, seed 0.05

Cranberry 0.05

Currant 3.5

Custard apple 0.30

Egg 0.02

Elderberry 3.5

Feijoa 1.0

Fish 0.05

Fish-shellfish, mollusc 0.05

Flax, seed 0.05

Fruit, citrus, group 10 0.70

Fruit, pome, group 11 0.6

Fruit, stone, group 12 3.0

Goat, fat 0.30

Goat, meat 0.30

Goat, meat byproducts 0.30

Gooseberry 3.5

Grain, cereal, forage, fodder and straw, group 16, forage, except rice 7.0

Grain, cereal, forage, fodder and straw, group 16, hay, except rice 6.0

Grain, cereal, forage, fodder and straw, group 16, stover, except rice 0.30

Grain, cereal, forage, fodder and straw, group 16, straw, except rice 3.0

Grain, cereal, group 15, except rice 0.05

Grape 1.0

Grape, juice 1.5

Grape, raisin 1.5

Guava 1.0

Herbs subgroup 19A, dried herbs 48

Herbs subgroup 19-A, fresh herbs 8.0

Hog, fat 0.30

Hog, meat 0.30

Hog, meat byproducts 0.30

Hop, dried cones 6.0

Horse, fat 0.30

Horse, meat 0.30

Horse, meat byproducts 0.30

Huckleberry 3.5

Ilama 0.30

Jaboticaba 1.0

Juneberry 3.5

Kava, leaves 4.0

Kava, roots 0.40

Leaf petioles subgroup 4B 6.0

Leafy greens subgroup 4A 3.5

Lettuce, head 3.5

Lettuce, leaf 3.5

Lingonberry 3.5

Longan 3.0

Lychee 3.0

Mango 1.0

Milk 0.10

Mustard, black, seed 0.05

Mustard, field, seed 0.05

Mustard, Indian, seed 0.05

Mustard, rapeseed, seed 0.05

Mustard, seed 0.05

Nut, tree, group 14 0.05

Okra 1.0

Onion, dry bulbs, subgroup 3-07A 0.15

Onion, green, subgroup 3-07B 2.5

Papaya 1.0

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Passionfruit 1.0

Peanut 0.45

Peanut, hay 35

Peanut, meal 0.75

Pecan 0.05

Persimmon 3.0

Pistachio 0.05

Pomegranate 0.90

Potato, chip 0.40

Potato, processed potato waste 0.90

Poultry, fat 0.05

Poultry, meat 0.05

Poultry, meat byproducts 0.05

Pulasan 3.0

Rambutan 3.0

Rapeseed, seed 0.05

Raspberry, wild 2.5

Safflower, seed 0.05

Salal 3.5

Sapodilla 1.0

Sapote, black 1.0

Sapote, mamey 1.0

Sheep, fat 0.30

Sheep, meat 0.30

Sheep, meat byproducts 0.30

Soursop 0.30

Soybean, forage 8.0

Soybean, hay 35

Soybean, meal 4.0

Soybean, seed 3.5

Spanish lime 3.0

Star apple 1.0

Starfruit 1.0

Strawberry 0.50

Sugar apple 0.30

Sunflower, seed 0.05

Tomato, paste 6.0

Tomato, puree 3.0

Vegetable, brassica leafy, group 5 3.5

Vegetable, cucurbit, group 9 0.5

Vegetable, fruiting, group 8 1.0

Vegetable, leaves of root and tuber, group 2 4.0

Vegetable, legume, group 6, except soybean 4.0

Vegetable, root and tuber, group 1, except sugar beet 0.40

Watercress 3.5

Watercress, upland 3.5

Wax jambu 1.0

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide 

imidacloprid, including its metabolites and degradates in connection with use of the pesticide under a Section 18 

emergency exemption granted by EPA. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl)methyl]-N-nitro-2-imidazolidinimine) and its metabolites 

containing the 6-chloropyridinyl moiety, calculated as the stoichiometric equivalent of imidacloprid. These tolerances will 

expire and are revoked on the dates specified in the following table:

Commodity Parts per million Expiration/revocation date

Sugarcane, cane 6.0 12/31/15

Sugarcane, molasses 50 12/31/15

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide 

imidacloprid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

tolerance levels specified below is to be determined by measuring only the sum of imidacloprid (1-[6-chloro-3-pyridinyl) 

methyl]-N-nitro-2-imidazolidinimine) and its metabolites containing the 6-chloropyridinyl moiety, calculated as the 

stoichiometric equivalent of imidacloprid, in or on the following commodities, when present therein as a result of the 

application of the pesticide to growing crops listed in this section and other non-food crops as follows:

Commodity Parts per million

Rice, grain 0.05

Vegetable, foliage of legume, group 7 2.5

Vegetable, legume, group 6 0.3

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[75 FR 22251, Apr. 28, 2010, as amended at 78 FR 33743, June 5, 2013]

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§180.473 Glufosinate ammonium; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide glufosinate ammonium, including its metabolites 

and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring the sum of glufosinate ammonium, butanoic acid, 2-amino-4-(hydroxymethylphosphinyl) 

monoammonium salt, and its metabolites, 2-(acetylamino)-4-(hydroxymethyl phosphinyl)butanoic acid, and 

3-(hydroxymethylphosphinyl)propanoic acid, expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid 

equivalents:

Commodity Parts per million

Almond, hulls 0.50

Apple 0.05

Banana 0.30

Banana, pulp 0.20

Beet, sugar, molasses 5.0

Beet, sugar, roots 0.9

Beet, sugar, tops (leaves) 1.5

Bushberry subgroup 13B 0.15

Canola, meal 1.1

Canola, seed 0.40

Cattle, fat 0.40

Cattle, meat 0.15

Cattle, meat byproducts 6.0

Corn, field forage 4.0

Corn, field, grain 0.20

Corn, field, stover 6.0

Corn, sweet, forage 1.5

Corn, sweet, kernels plus cob with husks removed 0.30

Corn, sweet, stover 6.0

Cotton, gin byproducts 15

Cotton, undelinted seed 4.0

Egg 0.15

Fruit, citrus, group 10-10 0.15

Fruit, pome, group 11-10 0.25

Fruit, stone, group 12-12 0.25

Goat, fat 0.40

Goat, meat 0.15

Goat, meat byproducts 6.0

Grain aspirated fractions 25

Grape 0.05

Hog, fat 0.40

Hog, meat 0.15

Hog, meat byproducts 6.0

Horse, fat 0.40

Horse, meat 0.15

Horse, meat byproducts 6.0

Juneberry 0.10

Lingonberry 0.10

Milk 0.15

Nut, tree, group 14 0.10

Olive 0.15

Pistachio 0.10

Potato 0.80

Potato, chips 1.6

Potato granules/flakes 2.0

Poultry, fat 0.15

Poultry, meat 0.15

Poultry, meat byproducts 0.60

Rice, grain 1.0

Rice, hull 2.0

Rice, straw 2.0

Salal 0.10

Sheep, fat 0.40

Sheep, meat 0.15

Sheep, meat byproducts 6.0

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Soybean 2.0

Soybean, hulls 5.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of glufosinate 

ammonium, including its metabolites and degradates, in or on the commodities in the table below, as a result of the 

application of glufosinate ammonium to crops listed in paragraph (a) of this section. Compliance with the tolerance levels 

specified below is to be determined by measuring the sum of glufosinate ammonium, butanoic acid, 2-amino4-(hydroxymethylphosphinyl) monoammonium salt, and its metabolite, 3-(hydroxymethylphosphinyl) propanoic acid, 

expressed as 2-amino-4-(hydroxymethylphosphinyl)butanoic acid equivalents.

Commodity Parts per million

Barley, hay 0.40

Barley, straw 0.40

Buckwheat, fodder 0.40

Buckwheat, forage 0.40

Oat, forage 0.40

Oat, hay 0.40

Oat, straw 0.40

Rye, forage 0.40

Rye, straw 0.40

Teosinte 0.40

Triticale 0.40

Wheat, forage 0.40

Wheat, hay 0.40

Wheat, straw 0.40

[68 FR 55849, Sept. 29, 2003, as amended at 71 FR 25945, May 3, 2006; 72 FR 72625, Dec. 21, 2007; 76 FR 23497, Apr. 27, 2011; 

77 FR 59113, Sept. 26, 2012]

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§180.474 Tebuconazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of tebuconazole, alpha-[2-(4-chlorophenyl)ethyl]

-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, including its metabolites and degradates, in or on the commodities 

in the table below. Compliance with the tolerance levels specified below is to be determined by measuring only 

tebuconazole [α-[2-(4-chlorophenyl) ethyl]-α-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol], in or on the commodity.

Commodity Parts per million

Almond, hulls 6.0

Apple, wet pomace 0.1

Asparagus 0.05

Banana 0.05

Barley, grain 0.3

Barley, hay 7.0

Barley, straw 3.5

Bean, dry seed 0.1

Bean, succulent 0.1

Beet, garden, roots 0.70

Beet, garden, tops 7.0

Brassica, leafy greens, subgroup 5B 2.5

Cherry, sweet, pre- and post-harvest 5.0

Cherry, tart, pre- and post-harvest 5.0

Coffee, green bean1 0.15

Coffee, roasted bean1 0.3

Corn, field, forage 4.0

Corn, field, grain 0.05

Corn, field, stover 3.5

Corn, pop, grain 0.05

Corn, pop, stover 3.5

Corn, sweet, forage 7.0

Corn, sweet, kernel plus cob with husks removed 0.5

Corn, sweet, stover 6.0

Cotton, gin byproducts 25.0

Cotton, undelinted seed 2.0

Fruit, pome, group 11 0.05

Fruit, stone, group 12, except cherry 1.0

Grain, aspirated fractions 16.0

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Grape 5.0

Grass, forage 8.0

Grass, hay 25.0

Grass, seed screenings 55.0

Grass, straw 30.0

Hop, dried cones 35.0

Lychee 1.6

Mango, postharvest 0.15

Nut, tree, group 14 0.05

Oat, forage 0.10

Oat, grain 0.15

Oat, hay 0.10

Oat, straw 0.10

Onion, bulb, subgroup 3-07A 0.2

Onion, green, subgroup 3-07B 1.3

Orange1 1.0

Orange, oil1 10

Peach 1.0

Peanut 0.1

Pistachio 0.05

Plum, pre- and post-harvest 1.0

Soybean, forage 25

Soybean, hay 50

Soybean, seed 0.08

Sunflower, seed 0.05

Sunflower, meal 0.2

Sunflower, refined oil 0.2

Vegetable, cucurbit, group 9 0.4

Vegetable, fruiting, group 8-10 1.3

Wheat, forage 3.0

Wheat, germ 0.20

Wheat, grain 0.15

Wheat, hay 7.0

Wheat, shorts 0.20

Wheat, straw 1.5

1

There are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide tebuconazole, including its metabolites and degradates, in 

or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only the sum of tebuconazole (alpha-[2-(4-chlorophenyl)ethyl]-alpha-(1,1-dimethylethyl)

-1H-1,2,4-triazole-1-ethanol) and its diol metabolite (1-(4-chlorophenyl)-4,4-dimethyl-3-(1H -1,2,4-triazole-1-yl-methyl)

-pentane-3,5-diol), calculated as the stoichiometric equivalent of tebuconzole, in or on the commodity.

Commodity Parts per million

Cattle, meat byproducts 0.2

Goat, meat byproducts 0.2

Horse, meat byproducts 0.2

Milk 0.1

Sheep, meat byproducts 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for residues of the fungicide tebuconazole, 

including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance 

levels specified below is to be determined by measuring only tebuconazole, alpha-[2-(4-chlorophenyl)ethyl]

-alpha-(1,1-dimethylethyl)-1H-1,2,4-triazole-1-ethanol, in or on the commodity.

Commodity Parts per million

Turnip, roots 0.5

Turnip, tops 7.0

(d) Indirect or inadvertent residues. [Reserved]

[59 FR 39464, Aug. 3, 1994]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.474, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

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§180.475 Difenoconazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of difenoconazole, including its metabolites and degradates, 

in or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined 

by measuring only difenoconazole, 1-[2-[2-chloro-4-(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]

-1H-1,2,4-triazole, in or on the following raw agricultural commodities:

Commodity Parts per million

Almond, hulls 7.0

Apple, wet pomace 25

Artichoke, globe 1.5

Aspirated grain fractions 95

Banana1 0.2

Barley, grain 0.1

Barley, hay 0.05

Barley, straw 0.05

Beet, sugar 0.3

Beet, sugar, dried pulp 1.9

Berry, low growing, subgroup 13-07G, except cranberry 2.5

Brassica, head and stem, subgroup 5A 1.9

Brassica, leafy green, subgroup 5B 35

Bushberry subgroup 13-07B 4.0

Carrot 0.50

Citrus, dried pulp 2.0

Citrus, oil 25

Corn, sweet, forage 0.01

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.01

Cotton, gin byproducts 0.05

Cotton, undelinted seed 0.05

Dragonfruit1 1.5

Fruit, citrus, group 10-10 0.60

Fruit, pome, group 11-10 5.0

Fruit, stone, group 12-12 2.5

Ginseng 1.0

Grape 4.0

Grape, raisin 6.0

Mango1 0.07

Nut, tree, group 14-12 0.03

Oat, forage 0.15

Oat, grain 0.01

Oat, hay 0.05

Oat, straw 0.05

Onion, bulb, subgroup 3-07A 0.20

Onion, green, subgroup 3-07B 6.0

Papaya1 0.30

Pea and bean, dried shelled, except soybean, subgroup 6C 0.20

Pea, field, hay 40

Pea, field, vines 10

Potato, wet peel 7.3

Rapeseed subgroup 20A 0.10

Rye, forage 0.15

Rye, grain 0.01

Rye, straw 0.05

Soybean, hulls 0.20

Soybean, seed 0.15

Turnip, greens 35

Vegetable, cucurbit, group 9 0.70

Vegetable, fruiting, group 8-10 0.60

Vegetable, tuberous and corm, subgroup 1C 4.0

Wax jambu1 1.5

Wheat, forage 0.1

Wheat, grain 0.1

Wheat, hay 0.05

Wheat, straw 0.1

1

There are no U.S. registrations.

(2) Tolerances are established for residues of difenoconazole, including its metabolites and degradates, in the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

the sum of difenoconazole, 1-[2-[2-chloro-4-(4-chlorophenoxy)phenyl]-4-methyl-1,3-dioxolan-2-ylmethyl]-1H-1,2,4-triazole, 

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and its metabolite, CGA-205375, 1-[2-chloro-4-(4-chloro-phenoxy)phenyl]-2-[1,2,4]triazol-1-yl-ethanol, calculated as the 

stoichiometric equivalent of difenoconazole, in the following commodities:

Commodity Parts per million

Cattle, fat 0.10

Cattle, liver 0.40

Cattle, meat 0.05

Cattle, meat byproduct (except liver) 0.10

Egg 0.02

Goat, fat 0.10

Goat, liver 0.40

Goat, meat 0.05

Goat, meat byproduct (except liver) 0.10

Hog, fat 0.10

Hog, liver 0.40

Hog, meat 0.05

Hog, meat byproduct (except liver) 0.10

Horse, fat 0.10

Horse, liver 0.40

Horse, meat 0.05

Horse, meat byproduct (except liver) 0.10

Milk 0.02

Sheep, fat 0.10

Sheep, liver 0.40

Sheep, meat 0.05

Sheep, meat byproduct (except liver) 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 36254, July 6, 1999]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.475, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.476 Triflumizole; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and 

degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to 

be determined by measuring only the parent compound triflumizole, 1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-

propoxyethyl)-1 H -imidazole, and its metabolites containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as 

stoichiometric equivalent of the parent compound.

Commodity Parts per million 

Apple, dry pomace 2.0 

Apple, wet pomace 2.0 

Berry, low growing, subgroup 13-07G, except cranberry 2.0

Brassica, head and stem, subgroup 5A 8.0

Brassica, leafy greens, subgroup 5B 40

Canistel 2.5

Cherry, sweet 1.5

Cherry, tart 1.5

Cilantro, leaves 35

Fruit, pome, group 11-10 0.50

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.5

Grape, dried pomace 15.0 

Grape, raisin, waste 10.0

Grape, wet pomace 15.0 

Hazelnut 0.05

Hop, dried cones 50

Leafy greens subgroup 4A, except spinach 35

Mango 2.5

Papaya 2.5

Pineapple 4.0

Sapodilla 2.5

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Sapote, black 2.5

Sapote, mamey 2.5

Star apple 2.5

Swiss chard 18

Tomato 1.5

Turnip, greens 40

Vegetable, cucurbit, Group 9 0.5

(2) Tolerances are established for residues of the fungicide triflumizole, including its metabolites and degradates, in or 

on the commodities of animal origin listed in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the parent compound triflumizole, 1-(1-((4-chloro-2-(trifluoromethyl)phenyl)imino)-2-

propoxyethyl)-1 H -imidazole, the metabolite 4-chloro-2-hydroxy-6-trifluoromethylaniline sulfate, and other metabolites 

containing the 4-chloro-2-trifluoromethylaniline moiety, calculated as the parent compound.

Commodity Parts per million 

Cattle, fat 0.5 

Cattle, meat 0.05 

Cattle, meat byproducts 0.5 

Egg 0.05 

Goat, fat 0.5 

Goat, meat 0.05 

Goat, meat byproducts 0.5 

Hog, fat 0.5 

Hog, meat 0.05 

Hog, meat byproducts 0.5 

Horse, fat 0.5 

Horse, meat 0.05 

Horse, meat byproducts 0.5 

Milk 0.05 

Poultry, fat 0.05 

Poultry, meat 0.05 

Poultry, meat byproducts 0.1 

Sheep, fat 0.5 

Sheep, meat 0.05 

Sheep, meat byproducts 0.5

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33702, May 24, 2000, as amended at 67 FR 40228, June 12, 2002; 67 FR 54587, Aug. 23, 2002; 70 FR 7047, Feb. 10, 2005; 

70 FR 17915, Apr. 8, 2005; 71 FR 13279, Mar. 15, 2006; 71 FR 49358, Aug. 23, 2006; 74 FR 26543, June 3, 2009; 74 FR 46376, 

Sept. 9, 2009; 76 FR 34885, June 15, 2011; 79 FR 12408, Mar. 5, 2014]

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§180.477 Flumiclorac pentyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide flumiclorac pentyl, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only flumiclorac pentyl, pentyl(2-chloro-4-fluoro5-(1,3,4,5,6,7-hexahydro-1,3-dioxo-2H-isoindol-2-yl)phenoxy)acetate, in or on the commodity.

Commodity Parts per million

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Cotton, gin byproducts 3.0

Cotton, undelinted seed 0.2

Soybean, hulls 0.02

Soybean, seed 0.01

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33702, May 24, 2000, as amended at 71 FR 11533, Mar. 8, 2006; 76 FR 23497, Apr. 27, 2011]

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§180.478 Rimsulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide rimsulfuron, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only rimsulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)amino] carbonyl]

-3-(ethylsulfonyl)-2-pyridinesulfonamide.

Commodity Parts per million

Almond, hulls 0.09

Bushberry, subgroup 13-07B 0.01

Caneberry, subgroup 13-07A 0.01

Chicory, roots 0.01

Chicory, tops 0.01

Corn, field, forage 0.4

Corn, field, grain 0.1

Corn, field, stover 2.5

Fruit, citrus, group 10 0.01

Fruit, pome, group 11 0.01

Fruit, stone, group 12 0.01

Grain, aspirated fractions 4.5

Grape 0.01

Nut, tree, group 14 0.01

Pistachio 0.01

Potato 0.1

Sorghum, grain, forage 0.01

Sorghum, grain, grain 0.01

Sorghum, grain, stover 0.01

Soybean, forage 0.25

Soybean, hay 1.2

Soybean, hulls 0.04

Soybean, seed 0.01

Tomato 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 16696, Apr. 6, 1998, as amended at 72 FR 41913, Aug. 1, 2007; 74 FR 67137, Dec. 18, 2009; 77 FR 3625, Jan. 25, 2012; 77 

FR 46306, Aug. 3, 2012; 80 FR 66805, Oct. 30, 2015]

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§180.479 Halosulfuron-methyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 

5-[(4,6-dimethoxy-2-pyrimidiny)amino] carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its 

metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified 

in the following table is to be determined by measuring only those halosulfuron-methyl residues containing the 

3-chlorosulfonamide (3-CSA) moiety, expressed as the stoichiometric equivalent of halosulfuron-methyl, in or on the 

commodity.

Commodity Parts per million

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 1.0

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 1.0

Hog, meat byproducts 0.1

Horse, fat 0.05

Horse, meat 0.05

Horse, meat byproducts 1.0

Milk 0.05

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 1.0

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(2) Tolerances are established for residues of the herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2-

pyrimidiny)amino]carbonylaminosulfonyl]-3-chloro-1-methyl-1H-pyrazole-4-carboxylate, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only halosulfuron-methyl.

Commodity Parts per million

Alfalfa, forage 1.0

Alfalfa, hay 2.0

Almond, hulls 0.2

Artichoke 0.05

Asparagus 0.8

Bean, dry, seed 0.05

Bushberry, subgroup 13-07B 0.05

Caneberry subgroup 13-07A 0.05

Corn, field, forage 0.2

Corn, field, grain 0.05

Corn, field, stover 0.8

Corn, pop, grain 0.05

Corn, pop, stover 0.8

Corn, sweet, forage 0.2

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 0.8

Cotton, gin byproducts 0.05

Cotton, undelinted seed 0.05

Fruit, pome, group 11-10 0.05

Grass, forage, fodder, and hay, group 17, forage 20

Grass, forage, fodder, and hay, group 17, hay 0.5

Melon subgroup 9A 0.1 

Millet, proso, forage 10

Millet, proso, grain 0.01

Millet, proso, hay 0.01

Millet, proso, straw 0.01

Nut, tree, group 14 0.05

Okra 0.05

Pea and bean, succulent shelled, subgroup 6 0.05

Pea and bean, succulent shelled, subgroup 6B 0.05

Pistachio 0.05

Rhubarb 0.05

Rice, grain 0.05

Rice, straw 0.2

Sorghum, grain, forage 0.05

Sorghum, grain, grain 0.05

Sorghum, grain, stover 0.1

Soybean, seed 0.05

Squash/Cucumber subgroup 9B 0.5

Sugarcane, cane 0.05

Vegetable, fruiting, group 8 0.05

Vegetable, tuberous and corm, subgroup 1C 0.05

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

herbicide halosulfuron-methyl, methyl 5-[(4,6-dimethoxy-2-pyrimidiny)amino]carbonylaminosulfonyl]-3-chloro-1-methyl-1Hpyrazole-4-carboxylate, including its metabolites and degradates, in or on the commodities in the following table. 

Compliance with the tolerance levels specified in the following table is to be determined by measuring only halosulfuronmethyl.

Commodity Parts per million

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.05

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 25448, May 12, 1999, as amended at 65 FR 58433, Sept. 29, 2000; 66 FR 66340, Dec. 26, 2001; 66 FR 66786, Dec. 27, 

2001; 67 FR 45649, July 10, 2002; 67 FR 59192, Sept. 20, 2002; 70 FR 51622, Aug. 31, 2005; 72 FR 8927, Feb. 28, 2007; 74 FR 

48401, Sept. 23, 2009; 75 FR 46853, Aug. 4, 2010; 76 FR 34886, June 15, 2011; 77 FR 71561, Dec. 3, 2012; 78 FR 53051, Aug. 

28, 2013; 80 FR 55773, Sept. 17, 2015]

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§180.480 Fenbuconazole; tolerances for residues.

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(a) Tolerances are established for residues of the fungicide fenbuconazole, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of fenbuconazole, alpha-[2-(4-chlorophenyl)-ethyl]-alpha-phenyl-3-(1H-1,2,4-triazole)-1-

propanenitrile, and its metabolites RH-9129, cis-5-(4-chlorophenyl)-dihydro-3-phenyl-3-(1H-1,2,4-triazole-1-ylmethyl)-2-3 

H-furanone, and RH-9130, trans-5-(4-chlorophenyl)-dihydro-3-phenyl-3-(1H-1,2,4-triazole-1-ylmethyl)-2-3 H-furanone, 

calculated as the stoichiometric equivalent of fenbuconazole, in or on the following agricultural commodities.

Commodity Parts per million

Almond 0.05

Almond, hulls 1.0

Apple 0.4

Apple, wet pomace 1.0

Banana 0.3

Beet, sugar, dried pulp 1.0

Beet, sugar, molasses 0.4

Beet, sugar, roots 0.3

Beet, sugar, tops 9.0

Bushberry subgroup 13B 0.3

Cattle, meat byproducts 0.05

Citrus, dried pulp 5.0

Citrus, oil 40.0

Cranberry 0.5

Fruit, citrus, group 10 1.0

Fruit, stone, group 12 1.0

Goat, meat byproducts 0.05

Grain, aspirated fractions 6.0

Grape1 1.0

Horse, meat byproducts 0.05

Peanut 0.1

Pecan 0.05

Pepper 1.0

Sheep, meat byproducts 0.05

Wheat, forage 4.0

Wheat, grain 0.1

Wheat, hay 8.0

Wheat, straw 8.0

1

There are no United States registrations for grape as of August 2006.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[60 FR 11032, Mar. 1, 1995]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.480, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.481 Prosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide prosulfuron and its metabolites and degradates 

in or on the commodities in the table below. Compliance with the tolerance levels specified in the table below is to be 

determined by measuring only prosulfuron, 1-(4-methoxy-6-methyl-triazin-2-yl)-3-[2-(3,3,3-trifluoropropyl)-phenylsulfonyl]

-urea, in or on the commodity.

Commodity Parts per million

Grain, cereal, forage, fodder, and straw, group 16, except rice, fodder 0.01

Grain, cereal, forage, fodder, and straw, group 16, except rice, forage 0.10

Grain, cereal, forage, fodder, and straw, group 16, except rice, hay 0.20

Grain, cereal, forage, fodder, and straw, group 16, except rice, straw 0.02

Grain, cereal, group 15, except rice 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

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[74 FR 67118, Dec. 18, 2009]

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§180.482 Tebufenozide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide tebufenozide, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)

-2-(4-ethylbenzoyl)hydrazide, in or on the commodity.

Commodity Parts per million

Almond, hulls 25

Apple 1.0

Apple, dry pomace 3.0 

Apple, wet pomace 3.0 

Berry group 13 3.0

Brassica, head and stem, subgroup 5A 5.0

Brassica, leafy greens, subgroup 5B 10.0

Canola, refined oil 4.0

Canola, seed 2.0

Citrus, oil 15.0

Cotton 1.5

Cotton, gin byproducts 30

Cranberry 1.0

Fruit, citrus, group 10 0.80

Fruit, pome 1.5

Grape 3.0

Kiwifruit1 0.5

Leaf petioles subgroup 4B 2.0

Leafy greens subgroup 4A 10.0

Nut, tree, group 14 0.1

Peppermint, tops 10.0

Pistachio 0.1 

Spearmint, tops 10.0

Turnip, greens 9.0

Turnip, roots 0.3

Vegetable, fruiting, group 8 1.0

Vegetable, tuberous and corm, except potato, subgroup 1D 0.015

Walnut 0.1

1

There are no U.S. registrations on kiwifruit as of June 15, 1999.

(2) Tolerances are established for residues of the insecticide tebufenozide, including its metabolites and degradates, 

in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this paragraph is 

to be determined by measuring only the sum of tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)

-2-(4-ethylbenzoyl)hydrazide, and its metabolites, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-((4-carboxymethyl)

benzoyl)hydrazide, 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, stearic acid 

conjugate of 3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and 

3-hydroxymethyl-5-methylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as the 

stoichiometric equivalent of tebufenozide, in or on the commodity.

Commodity Parts per million

Cattle, fat 0.1 

Cattle, meat 0.08 

Cattle, meat byproducts 0.08 

Goat, fat 0.1

Goat, meat 0.08

Goat, meat byproducts 0.08 

Hog, fat 0.1 

Hog, meat 0.08 

Hog, meat byproducts 0.08 

Horse, fat 0.1 

Horse, meat 0.08

Horse, meat byproducts 0.08

Milk 0.04

Sheep, fat 0.1 

Sheep, meat 0.08

Sheep, meat byproducts 0.08

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the insecticide 

tebufenozide, including its metabolites and degradates, in or on the commodities in the table in this paragraph when 

present therein as a result of the application of tebufenozide to growing crops listed in the table to paragraph (a)(1) of this

section. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only the sum of 

tebufenozide, 3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-ethylbenzoyl)hydrazide, and its metabolite, 

3,5-dimethylbenzoic acid 1-(1,1-dimethylethyl)-2-(4-(1-hydroxyethyl)benzoyl)hydrazide, calculated as the stoichiometric 

equivalent of tebufenozide, in or on the commodity.

Commodity Parts per million

Animal feed, nongrass, group 18 1.0

Grain, cereal, forage, fodder and straw, group 16 1.0

Grass, forage, fodder and hay, group 17 1.0

Vegetable, foliage of legume, group 7 0.20

[60 FR 29347, May 31, 1995]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.482, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.484 Flutolanil; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of flutolanil, N-(3-(1-methylethoxy) phenyl)-2-(trifluoromethyl)

benzamide, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

tolerance levels specified below is to be determined by measuring only flutolanil and its metabolites converted to 

2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the following commodities:

Commodity Parts per million

Cattle, fat 0.10

Cattle, kidney 1.00

Cattle, liver 2.00

Cattle, meat byproducts 0.05

Cattle, meat 0.05

Cotton, gin byproducts 0.20

Cotton, undelinted seed 0.20

Egg 0.05

Goat, fat 0.10

Goat, kidney 1.00

Goat, liver 2.00

Goat, meat byproducts 0.05

Goat, meat 0.05

Hog, fat 0.10

Hog, kidney 1.00

Hog, liver 2.00

Hog, meat byproducts 0.05

Hog, meat 0.05

Horse, fat 0.10

Horse, kidney 1.00

Horse, liver 2.00

Horse, meat byproducts 0.05

Horse, meat 0.05

Milk 0.05

Peanut 0.5

Peanut, hay 15.0

Peanut, meal 1.0

Potato 0.20 

Potato, wet peel 0.30 

Poultry, fat 0.05

Poultry, meat 0.05

Poultry, meat byproducts 0.05

Rice, bran 10.0 

Rice, grain 7.0 

Rice, hulls 25.0 

Rice, straw 10.0 

Sheep, fat 0.10

Sheep, kidney 1.00

Sheep, liver 2.00

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Sheep, meat 0.05

Sheep, meat byproducts 0.05

Soybean, forage 8.0

Soybean, hay 2.5

Soybean, seed 0.20

Turnip, greens 0.1

Vegetable, brassica, leafy, group 5 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of flutolanil, 

N-(3-(1-methylethoxy)phenyl)-2-(trifluoromethyl)benzamide, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only flutolanil and its metabolites converted to 2-(trifluoromethyl) benzoic acid and calculated as flutolanil, in or on the 

following commodities.

Commodity Parts per million

Wheat, bran 0.20

Wheat, forage 2.5

Wheat, grain 0.05

Wheat, hay 1.2

Wheat, straw 0.20

[60 FR 42458, Aug. 16, 1995, as amended at 61 FR 33044, June 26, 1996; 63 FR 42256, 42257, Aug. 7, 1998; 66 FR 10825, Feb. 

20, 2001; 71 FR 74818, Dec. 13, 2006; 72 FR 35665, June 29, 2007; 73 FR 33017, June 11, 2008; 75 FR 17570, Apr. 7, 2010; 75 

FR 80350, Dec. 22, 2010]

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§180.485 Cyproconazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the free and conjugated forms of the fungicide 

cyproconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

proposed tolerance levels specified below is to be determined by measuring only cyproconazole (α-(4-chlorophenyl)

-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) in or on the following commodities:

Commodity Parts per million

Aspirated grain fractions 2.5

Cattle, fat 0.01

Cattle, meat byproducts (except liver) 0.01

Coffee bean, green (Imported)1 0.1

Corn, field, forage 0.60

Corn, field, grain 0.01

Corn, field, stover 1.2

Goat, fat 0.01

Goat, meat byproducts (except liver) 0.01

Horse, fat 0.01

Horse, meat byproducts (except liver) 0.01

Peanut 0.01

Peanut, hay 6.0

Sheep, fat 0.01

Sheep, meat byproducts (except liver) 0.01

Soybean, forage 1.0

Soybean, hay 3.0

Soybean, oil 0.10

Soybean, seed 0.05

Wheat, forage 0.80

Wheat, grain 0.05

Wheat, grain, milled byproducts 0.10

Wheat, hay 1.3

Wheat, straw 0.90

1

There are no U.S. registrations as of February 15, 2008 for use on coffee bean.

(2) A tolerance is established for the combined residues of the free and conjugated forms of the fungicide 

cyproconazole, including its metabolites and degradates, in or on the commodity in the table below. Compliance with the 

tolerance level specified below is to be determined by measuring only the sum of cyproconazole (α-(4-chlorophenyl)

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1H-1,2,4-triazole-1-hexenoic acid, calculated as the stoichiometric equivalent of cyproconazole, in or on the following 

commodity:

Commodity Parts per million

Milk 0.02

(3) Tolerances are established for the combined residues of the free and conjugated forms of the fungicide 

cyproconazole, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

tolerance level specified below is to be determined by measuring only the sum of cyproconazole (α-(4-chlorophenyl)

-α-(1-cyclopropylethyl)-1H-1,2,4-triazole-1-ethanol) and its metabolite 2-(4-chlorophenyl)-3-cyclopropyl-1-[1,2,4]triazol-1-ylbutane-2,3-diol, calculated as the stoichiometric equivalent of cyproconazole, in or on the following commodities:

Commodity Parts per million

Cattle, liver 0.50

Goat, liver 0.50

Hog, liver 0.01

Horse, liver 0.50

Sheep, liver 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 53835, Oct. 7, 1998, as amended at 71 FR 71058, Dec. 8, 2006; 73 FR 27760, May 14, 2008; 78 FR 37473, June 21, 2013]

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§180.486 Chlorethoxyfos; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide chlorethoxyfos, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only chlorethoxyfos, O,O-diethyl O-(1,2,2,2-tetrachloroethyl) 

phosphorothioate, in or on the commodity.

Commodity Parts per million

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Corn, sweet, forage 0.01

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23498, Apr. 27, 2011]

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§180.487 Pyrithiobac sodium; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, pyrithiobac sodium, (sodium 2-chloro-6-

[(4,6-dimethoxypyrimidin-2-yl)thio]benzoate), resulting from the application of the pesticide chemical in or on the following 

foods/feeds:

Commodity Parts per million

Cotton, gin byproducts 0.15

Cotton, undelinted seed 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

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[62 FR 54783, Oct. 22, 1997, as amended at 64 FR 56469, Oct. 20, 1999; 67 FR 72110, Dec. 4, 2002]

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§180.490 Imazapic; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide imazapic, including its metabolites and 

degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified is to be 

determined by measuring the sum of imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-

methyl-3-pyridinecarboxylic acid) and its metabolites (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]

-5-hydroxymethyl-3-pyridinecarboxylic acid and (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]

-5-(β-D-glucopyranosyloxy)methyl-3-pyridinecarboxylic acid, calculated as the stoichiometric equivalent of imazapic.

Commodity Parts per million 

Grass, forage 15 

Grass, hay 30 

Peanut 0.1

Soybean, seed1 0.40

Sugarcane, cane2 0.03

1

There are no US registrations as of April 4, 2014.

2

There are no U.S. registrations as of June 4, 2014.

(2) Tolerances are established for residues of the herbicide imazapic, including its metabolites and degradates, in or 

on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by 

measuring the sum of imazapic (2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-methyl-3-

pyridinecarboxylic acid) and its metabolite (±)-2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-

hydroxymethyl-3-pyridinecarboxylic acid, calculated as the stoichiometric equivalent of imazapic.

Commodity Parts per million 

Cattle, fat 0.10 

Cattle, kidney 1.0 

Cattle, meat byproducts, except kidney 0.1 

Cattle, meat 0.1 

Goat, fat 0.1 

Goat, kidney 1.0 

Goat, meat byproducts, except kidney 0.1 

Goat, meat 0.1 

Horse, fat 0.1 

Horse, kidney 1.0 

Horse, meat byproducts, except kidney 0.1 

Horse, meat 0.1 

Milk 0.1 

Sheep, fat 0.1 

Sheep, kidney 1.0 

Sheep, meat byproducts, except kidney 0.1 

Sheep, meat 0.1

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 54224, Oct. 6, 1999, as amended at 66 FR 64774, Dec. 14, 2001; 66 FR 66332, Dec. 26, 2001; 78 FR 49932, Aug. 16, 2013; 

79 FR 18818, Apr. 4, 2014; 79 FR 32170, June 4, 2014]

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§180.491 Propylene oxide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fumigant propylene oxide, including its metabolites and 

degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in this 

paragraph is to be determined by measuring only propylene oxide, when used as a postharvest fumigant, in or on the 

commodity.

Commodity

Parts per

million

Cacao bean, cocoa powder 200

Cacao bean, dried bean 200

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Fig 3.0

Garlic, dried 300

Grape, raisin 1.0

Herbs and spices, group 19, dried 300

Nut, pine 300

Nut, tree, group 14 300

Nutmeat, processed, except peanuts 300

Onion, dried 300

Pistachio 300

Plum, prune, dried 2.0

(2) Tolerances are established for residues of the reaction product, propylene chlorohydrin, including its metabolites 

and degradates, in or on the commodities in the table in this paragraph. Compliance with the tolerance levels specified in 

this paragraph is to be determined by measuring only the sum of propylene chlorohydrin (1-chloro-2-propanol), and its 

isomer 2-chloro-1-propanol, calculated as the stoichiometric equivalent of propylene chlorohydrin (1-chloro-2-propanol), 

that results from the use of propylene oxide as a postharvest fumigant, in or on the commodity.

Commodity

Parts per

million

Basil, dried leaves 6000

Cacao bean, cocoa powder 20.0

Cacao bean, dried bean 20.0

Fig 3.0

Garlic, dried 6000

Grape, raisin 4.0

Herbs and spices, group 19, dried, except basil 1500

Nut, pine 10.0

Nut, tree, group 14 10.0

Nutmeat, processed, except peanuts 10.0

Onion, dried 6000

Pistachio 10.0

Plum, prune, dried 2.0

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33702, May 24, 2000, as amended at 68 FR 39430, July 1, 2003; 72 FR 49651, Aug. 29, 2007; 73 FR 54963, Sept. 24, 2008; 

76 FR 38037, June 29, 2011; 77 FR 28495, May 15, 2012]

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§180.492 Triflusulfuron-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of triflusulfuron-methyl, including its metabolites and degradates, 

in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only triflusulfuron-methyl (methyl 2-[[[[[4-(dimethylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-

yl]amino]carbonyl]amino]sulfonyl]-3-methylbenzoate) in or on the following commodities:

Commodity Parts per million

Beet, garden, roots 0.01

Beet, garden, tops 0.02

Beet, sugar, roots 0.05

Beet, sugar, tops 0.05

Chicory, roots 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 40196, June 12, 2002, as amended at 76 FR 22625, Apr. 22, 2011]

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§180.493 Dimethomorph; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide dimethomorph, 4-[3-(4-chlorophenyl)

-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites and degradates, in or on the 

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commodities in the following table. Compliance with the tolerance levels specified in the following table is to be determined 

by measuring only dimethomorph in or on the commodities.

Commodity Parts per million

Brassica, head and stem, subgroup 5A 6.0

Brassica, leafy greens, subgroup 5B 30.0

Ginseng 0.90

Grape 3.0

Grape, raisin 7.0

Hop, dried cones 60

Onion, bulb, subgroup 3-07A 0.6

Onion, green, subgroup 3-07B 15.0

Papaya1 1.5

Potato 0.05

Potato, wet peel 0.20

Strawberry 0.90

Taro, corm 0.5 

Taro, leaves 6.0 

Turnip, greens 20.0

Vegetable, cucurbit, group 9 0.5

Vegetable, fruiting, group 8 1.5

Vegetable, leafy (except Brassica) group 4 30.0

1

There are no U.S. registrations as of January 20, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

fungicide dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its 

metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified 

in the following table is to be determined by measuring only dimethomorph in or on the commodity.

Commodity Parts per million

Bean, lima, succulent 0.60

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide 

dimethomorph, 4-[3-(4-chlorophenyl)-3-(3,4-dimethoxyphenyl)-1-oxo-2-propen-1-yl]morpholine, including its metabolites 

and degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the 

following table is to be determined by measuring only dimethomorph in or on the commodity.

Commodity Parts per million

Wheat, forage 0.15

Wheat, hay 0.15

Wheat, straw 0.4

[62 FR 26416, May 14, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.493, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.494 Pyridaben; tolerance for residues.

(a) General. Tolerances are established for residues of the insecticide pyridaben [2-tert-butyl-5-(4-tert-butylbenzylthio)

-4-chloropyridazin-3(2H)-one] on the following plants, and of the insecticide pyridaben and its metabolites (2-tert-butyl5-(4-(1-carboxy-1-methylethyl)benzylthio)-4-chloropyridazin-3(2H)-one] and (2-tert-butyl-5-[4(-1,1-dimethyl-2-

hypdroxyethyl)benzylthio-4-chloropyridazinn-3(2H)-one) on animals, as indicated in the following table. 

Commodity Parts per million Revocation/expiration date 

Almond, hulls 4.0 None 

Apple 0.5 None 

Apple, wet pomace 0.75 None 

Canistel 0.10 None

Cattle, fat 0.05 None 

Cattle, meat 0.05 None 

Cattle, meat byproducts 0.05 None 

Citrus 0.5 None 

Citrus, dried pulp 1.5 None 

Citrus, oil 10.0 None

Fruit, stone, group 12 2.5 None

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Goat, fat 0.0 None 

Goat, meat 0.05 None 

Goat, meat byproducts 0.05 None 

Grape 1.5 None 

Hog, fat 0.05 None 

Hog, meat 0.05 None 

Hog, meat byproducts 0.05 None 

Hop, dried cones 10.0 None

Horse, fat 0.05 None 

Horse, meat 0.05 None 

Horse, meat byproducts 0.05 None 

Mango 0.10 None

Milk 0.01 None 

Nut, tree, group 14 0.05 None 

Papaya 0.10 None

Pear 0.75 None 

Pistachio 0.05 None 

Sapodilla 0.10 None

Sapote, black 0.10 None

Sapote, mamey 0.10 None

Sheep, fat 0.05 None 

Sheep, meat 0.05 None 

Sheep, meat byproduct 0.05 None

Star apple 0.10 None

Strawberry 2.5 None

Tomato 0.15 None

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(m) are 

established for residues of the insecticide pyridaben [2-tert-butyl-5(4-tert-butylbenzylthio)-4-chloropyridazin-3(2H)-one] in 

or on the following raw agricultural commodity: 

Commodity Parts per million Expiration Date 

Cranberry 0.5 None

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 43712, July 14, 2000, as amended at 66 FR 33199, June 21, 2001; 70 FR 55769, Sept. 23, 2005; 76 FR 56015, Sept. 15, 

2010]

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§180.495 Spinosad; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the insecticide spinosad in or on the food commodities in the 

table to this paragraph. Spinosad is a fermentation product of Saccharopolyspora spinosa. The product consists of two 

related active ingredients: Spinosyn A (Factor A: CAS # 131929-60-7) or 2-[(6-deoxy-2,3,4-tri-O -methyl-α-L-mannopyranosyl)oxy]-13-[[5-(dimethylamino)-tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-

ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16b-tetradecahydro-14-methyl-1H-as-Indaceno[3,2-d]oxacyclododecin-7,15-

dione; and Spinosyn D (Factor D; CAS # 131929-63-0) or 2-[(6-deoxy-2,3,4-tri-O-methyl-α-L-manno-pyranosyl)oxy]-13-

[[5-(dimethyl-amino)-tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-ethyl-2,3,3a,5a,5b,6,9,10,11,12,13,14,16a,16btetradecahydro-4,14-methyl-1H-as-Indaceno[3,2-d]oxacyclododecin-7,15-dione.

Commodity Parts per million

Acerola 1.5

Alfalfa, seed 0.15

Alfalfa, seed screenings 2.0

Almond, hulls 19

Amaranth, grain, grain 1.0

Amaranth, grain, stover 10

Animal feed, nongrass, group, 18 0.02

Animal feed, nongrass, group, 18, forage 35.0

Animal feed, nongrass, group, 18, hay 30.0

Apple, dry pomace 0.5

Apple, wet pomace 0.5

Artichoke, globe 0.3

Asparagus 0.2

Atemoya 0.3

Avocado 0.3

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Banana 0.25

Beet, sugar, molasses 0.75

Biriba 0.3

Brassica, head and stem, subgroup 5A 2.0

Brassica, leafy greens, subgroup 5B 10.0

Bushberry subgroup 13B 0.250

Caneberry subgroup 13A 0.7

Canistel 0.3

Cattle, fat 50

Cattle, liver 10

Cattle, meat 2.0

Cattle, meat byproducts, except liver 5.0

Cherimoya 0.3

Citrus, oil 3.0

Citrus, dried pulp 0.5

Coriander, leaves 8.0

Corn, sweet, kernel plus cob with husks removed 0.02

Cotton, gin byproducts 1.5

Cotton, undelinted seed 0.02

Cranberry 0.01

Custard apple 0.3

Date 0.10

Egg 0.30

Feijoa .05

Fig 0.10

Fish 4.0

Fish-shellfish, crustacean 4.0

Fish-shellfish, mollusc 4.0

Food commodities 0.02

Fruit, citrus, group 10 0.3

Fruit, pome, group 11 0.20

Fruit, stone, group 12 0.20

Goat, fat 50

Goat, liver 10

Goat, meat 2.0

Goat, meat byproducts, except liver 5.0

Grain, aspirated fractions 200

Grain, cereal, group 15 1.5

Grain, cereal, group 16, forage, except rice 2.5

Grain, cereal, group 16, hay, except rice 10.0

Grain, cereal, group, 16, stover, except rice 10.0

Grain, cereal, group, 16, straw, except rice 1.0

Grape 0.50

Grape, raisin 0.70

Grass, forage, fodder and hay, group 17, forage 10.0

Grass, forage, fodder and hay, group 17, hay 5.0

Guava 0.3

Herb subgroup 19A, dried 22

Herb subgroup 19A, fresh 3.0

Hog, fat 5.0

Hog, meat 0.50

Hog, meat byproducts 2.0

Hop, dried cones 22

Horse, fat 50

Horse, liver 10

Horse, meat 2.0

Horse, meat byproducts, except liver 5.0

Ilama 0.3

Jaboticaba 0.3

Juneberry 0.25

Lingonberry 0.250

Longan 0.3

Lychee 0.3

Mango 0.3

Milk 7.0

Milk, fat 85

Nut, tree, group 14 0.10

Okra 0.40

Onion, green 2.0

Papaya 0.3

Passionfruit 0.3

Pea and bean, dried shelled, except soybean, subgroup 6C 0.02

Pea and bean, succulent shelled, subgroup 6B 0.02

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Peanut 0.02

Peanut, hay 11.0

Peppermint, tops 3.5

Pineapple 0.02

Pineapple, process residue 0.08

Pistachio 0.10

Pomegranate 0.30

Poultry, fat 1.3

Poultry, meat 0.10

Poultry, meat byproducts 0.20

Pulasan 0.3

Rambutan 0.3

Rice, hulls 4.0

Salal 0.250

Sapodilla 0.3

Sapote, black 0.3

Sapote, mamey 0.3

Sapote, white 0.3

Sheep, fat 50

Sheep, liver 10

Sheep, meat 2.0

Sheep, meat byproducts, except liver 5.0

Soursop 0.3

Soybean 0.02

Spanish lime 0.3

Spearmint, tops 3.5

Spice, subgroup 19B, except black pepper 1.7

Star apple 0.3

Starfruit 0.3

Strawberry 1.0

Sugar apple 0.3

Ti, leaves 10.0

Vegetable, bulb, group 3, except green onion 0.10

Vegetable, cucurbit, group 9 0.3

Vegetable, foliage of legume, group 7 8.0

Vegetable, fruiting, group 8 0.4

Vegetable, leafy, except brassica, group 4 8.0

Vegetable, leaves of root and tuber, group 2 10.0

Vegetable, legume, edible podded, subgroup 6A 0.30

Vegetable, root and tuber, group 1 0.10

Watercress 8.0

Wax jambu 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[72 FR 68540, Dec. 5, 2007, as amended at 74 FR 46376, Sept. 9, 2009; 74 FR 48408, Sept. 23, 2009; 75 FR 60327, Sept. 30, 

2010]

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§180.496 Thiazopyr; tolerances for residues.

Tolerances are established for combined residues of the herbicide thiazopyr (3-pyridinecaroxylic acid, 

2-(difluoromethyl)-5-(4,5-dihydro-2-thiazolyl)-4-(2-methylpropyl)-6-(trifluoromethyl)-, methyl ester) and its metabolites 

determined as 2-(difluoromethyl)-6-(trifluoromethyl)-3,4,5-pyridinetricarboxylic acid, all expressed as the parent 

equivalents in or on the following raw agricultural commodities:

Commodities Parts per million

Grapefruit 0.05

Orange, sweet 0.05

[62 FR 9978, Mar. 5, 1997]

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§180.497 Clofencet; tolerances for residues.

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(a) General. Tolerances are established for residues of the plant growth regulator (hybridizing agent) clofencet, 

including its metabolites and degradates, in or on the commodities in the table in this paragraph. Compliance with the 

tolerance levels specified in this paragraph is to be determined by measuring only clofencet, potassium 2-(4-chlorophenyl)

-3-ethyl-2,5-dihydro-5-oxo-4-pyridazinecarboxylate, expressed as the free acid, in or on the commodity.

Commodity

Parts per

million

Expiration/

revocation

date

Cattle, fat 0.04 7/14/12

Cattle, kidney 10.0 7/14/12

Cattle, meat 0.15 7/14/12

Cattle, meat byproducts, except kidney 0.5 7/14/12

Egg 1.0 7/14/12

Goat, fat 0.04 7/14/12

Goat, kidney 10.0 7/14/12

Goat, meat 0.15 7/14/12

Goat, meat byproducts, except kidney 0.5 7/14/12

Hog, fat 0.04 7/14/12

Hog, kidney 10.0 7/14/12

Hog, meat 0.15 7/14/12

Hog, meat byproducts, except kidney 0.5 7/14/12

Horse, fat 0.04 7/14/12

Horse, kidney 10.0 7/14/12

Horse, meat 0.15 7/14/12

Horse, meat byproducts, except kidney 0.5 7/14/12

Milk 0.02 7/14/12

Poultry, fat 0.04 7/14/12

Poultry, meat 0.15 7/14/12

Poultry, meat byproducts 0.20 7/14/12

Sheep, fat 0.04 7/14/12

Sheep, kidney 10.0 7/14/12

Sheep, meat 0.15 7/14/12

Sheep, meat byproducts, except kidney 0.5 7/14/12

Wheat, forage 10.0 7/14/12

Wheat, grain 250.0 7/14/12

Wheat, hay 40.0 7/14/12

Wheat, straw 50.0 7/14/12

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the plant growth 

regulator (hybridizing agent) clofencet, including its metabolites and degradates, in or on the commodities in the table in 

this paragraph. Compliance with the tolerance levels specified in this paragraph is to be determined by measuring only 

clofencet, potassium 2-(4-chlorophenyl)-3-ethyl-2,5-dihydro-5-oxo-4-pyridazinecarboxylate, expressed as the free acid, in 

or on the commodity when present therein as a result of the application of clofencet to the growing crops in paragraph (a) 

of this section.

Commodity

Parts per

million

Expiration/

revocation

date

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; forage 4.0 7/14/12

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; hay 15.0 7/14/12

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; stover 1.0 7/14/12

Grain, cereal, forage, fodder and straw, group 16, except rice, sweet corn, wheat, and wild rice; straw 4.0 7/14/12

Grain, cereal group 15, except rice, sweet corn, wheat, and wild rice 20.0 7/14/12

Soybean 30.0 7/14/12

Soybean, forage 10.0 7/14/12

Soybean, hay 10.0 7/14/12

[76 FR 56656, Sept. 14, 2011]

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§180.498 Sulfentrazone; tolerances for residues.

(a)(1) General. Tolerances are established for the combined residues of the free and conjugated forms of 

sulfentrazone, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

tolerance levels specified below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolite HMS 

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(N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)

methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the following commodities.

Commodity Parts per million

Soybean, seed 0.05

(2) Tolerances are established for the combined residues of the free and conjugated forms of sulfentrazone, including 

its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-

methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS 

(N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as 

the stoichiometric equivalent of sulfentrazone in or on the following commodities.

Commodity Parts per million

Apple 0.15

Asparagus 0.15

Berry and small fruit, group 13-07 0.15

Brassica, head and stem, subgroup 5A 0.20

Brassica, leafy greens, subgroup 5B 0.40

Corn, field, forage 0.20

Corn, field, grain 0.15

Corn, field, stover 0.30

Flax 0.15

Fruit, citrus, group 10-10 0.15

Horseradish 0.20

Melon, subgroup 9A 0.15

Nut, tree, group 14 0.15

Pea and bean, dried shelled, except soybean, subgroup 6C 0.15

Pea, succulent 0.15

Peanut 0.20

Peanut, meal 0.40

Peppermint, tops 0.30

Pistachio 0.15

Rhubarb 0.15

Spearmint, tops 0.30

Sugarcane, cane 0.15

Sugarcane, molasses 0.20

Sunflower subgroup 20B 0.20

Turnip, roots 0.15

Turnip, tops 0.60

Vegetable, fruiting, group 8-10 0.15

Vegetable, soybean, succulent 0.15

Vegetable, tuberous and corm, subgroup 1C 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for the combined 

residues of the free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]

phenyl]methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl5-oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-

oxo-1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on 

the following commodities.

Commodity

Parts per

million

Bean, lima, succulent 0.15

Cowpea, succulent 0.15

Wheat, forage 0.50

Wheat, grain 0.15

Wheat, hay 0.30

Wheat, straw 1.5

(d) Indirect or inadvertent residues. Tolerances are established for inadvertent and indirect combined residues of the 

free and conjugated forms of sulfentrazone, including its metabolites and degradates, in or on the commodities in the table 

below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of 

sulfentrazone (N-[2,4-dichloro-5-[4-(difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]phenyl]

methanesulfonamide) and its metabolites HMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-3-hydroxymethyl-5-oxo1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide) and DMS (N-(2,4-dichloro-5-(4-(difluoromethyl)-4,5-dihydro-5-oxoeCFR — Code of Federal Regulations Page 239 of 441

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1H-1,2,4-triazol-1-yl)phenyl)methanesulfonamide, calculated as the stoichiometric equivalent of sulfentrazone in or on the 

following commodities when present therein as a result of the application of sulfentrazone to growing crops.

Commodity Parts per million

Grain, cereal (excluding sweet corn), Hulls 0.30

Grain, cereal, forage, fodder and straw, group 16, except sweet corn; forage 0.2

Grain, cereal, forage, fodder and straw, group 16, except sweet corn; hay 0.2

Grain, cereal, forage, fodder and straw, group 16, except sweet corn; stover 0.1

Grain, cereal, forage, fodder and straw, group 16, except sweet corn; straw 0.6

Grain, cereal, group 15, except sweet corn 0.1

Grain, cereal, group 15, except sweet corn; bran 0.15

[62 FR 10708, Mar. 10, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.498, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.499 Propamocarb; tolerances for residues.

(a) General. Tolerances are established for the residues of propamocarb, including its metabolites and degradates, in 

or on the commodities specified in the following table resulting from the application of the hydrochloride salt of 

propamocarb. Compliance with the following tolerance levels is to be determined by measuring only propamocarb (propyl 

N-[3-(dimethylamino)propyl]carbamate):

Commodity Parts per million

Lettuce, head 50

Lettuce, leaf 90

Potato 0.06

Tomato, paste 5.0

Vegetable, cucurbit, group 9 1.5

Vegetable, fruiting, group 8 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerance with regional registrations. Tolerances with regional registrations are established for the residues of 

propamocarb, including its metabolites and degradates, in or on the commodities specified in the following table resulting 

from the application of the hydrochloride salt of propamocarb. Compliance with the following tolerance levels is to be 

determined by measuring only propamocarb (propyl N-[3-(dimethylamino)propyl]carbamate):

Commodity 

Parts per

million

Bean, lima, succulent 2.0

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 15620, Apr. 2, 1997, as amended at 62 FR 26966, May 16, 1997; 63 FR 32136, June 12, 1998; 64 FR 16843, Apr. 7, 1999; 

65 FR 58399, Sept. 29, 2000; 66 FR 37598, July 19, 2001; 66 FR 48585, Sept. 21, 2001; 67 FR 35049, May 17, 2002; 69 FR 47022, 

Aug. 4, 2004; 70 FR 7047, Feb. 10, 2005; 78 FR 33736, June 5, 2013]

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§180.500 Imazapyr; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, imazapyr, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only the residues of imazapyr [2-[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo1H-imidazol-2-yl]-3-pyridinecarboxylic acid].

Commodity Parts per million

Cattle, fat 0.05

Cattle, kidney 0.20

Cattle, meat 0.05

Cattle, meat byproducts, except kidney 0.05

Corn, field, forage 0.05

Corn, field, grain 0.05

Corn, field, stover 0.05

Fish 1.0

Goat, fat 0.05

Goat, kidney 0.20

Goat, meat 0.05

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Goats, meat byproducts, except kidney 0.05

Grass, forage 100

Grass, hay 30

Horse, fat 0.05

Horse, kidney 0.20

Horse, meat 0.05

Horse, meat byproducts, except kidney 0.05

Lentil1 0.2

Milk 0.01

Rapeseed subgroup 20A1 0.05

Sheep, fat 0.05

Sheep, kidney 0.20

Sheep, meat 0.05

Sheep, meat byproducts, except kidney 0.05

Shellfish 0.10

Soybean, meal1 4.5

Soybean, seed1 4.0

Sunflower subgroup 20B1 0.05

1

There are no U.S. Registrations.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55484, Sept. 26, 2003, as amended at 78 FR 66653, Nov. 6, 2013; 79 FR 19487, Apr. 9, 2014]

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§180.501 Hydroprene; tolerances for residues.

(a) General. A tolerance of 0.2 part per million is established for residues of hydroprene [(S)-(Ethyl (2E,4E,7S)-3,7,11-

trimrthyl-2,4-dodecadienoate)], (CAS Reg. No. 65733-18-8) on food commodities in food-handling establishments in 

accordance with the following prescribed conditions:

(1) Application shall be limited to spot, crack and crevice, perimeter and ultra low volume (ULV) fogging treatment in 

food storage or food-handling establishments, including warehouses, food service, manufacturing, and processing 

establishments such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing 

plants, and canneries where food and food products are held, processed, and served: Provided that the food is removed 

or covered prior to such use, and food-processing surfaces are covered during treatment or thoroughly cleaned before 

using, or in the case of point-source device treatments, devices must not come into direct contact with food preparation 

surfaces and must be in a minimum distance of 3 feet from exposed foods.

(2) To assure safe use of the insect growth regulator, the label and labeling shall conform to that registered by the 

U.S. Environmental Protection Agency, and it shall be used in accordance with such label and labeling. 

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 61647, Nov. 19, 1997, as amended at 71 FR 74818, Dec. 13, 2006]

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§180.502 Aminoethoxyvinylglycine hydrochloride (aviglycine HCl); tolerances for residues.

(a) General. Tolerances are established for residues of aminoethoxyvinylglycine hydrochloride (aviglycine HCl) in or 

on the following food commodities:

Commodity Parts per million

Apple 0.08

Fruit, stone, group 12, except cherry 0.170

Pear 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]

[62 FR 24838, May 7, 1997, as amended at 64 FR 31129, June 10, 1999; 66 FR 36481, 36484, July 12, 2001; 69 FR 7606, Feb. 18, 

2004]

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§180.503 Cymoxanil, tolerance for residues.

(a) General. Tolerances are established for residues of the fungicide, cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]

-2-(methoxyimino) acetamide, in or on the following food commodities:

Commodity Parts per million

Caneberry, subgroup 13A-07 4.0

Cilantro, leaves 19

Hop, dried cones 7.0

Leafy greens, subgroup 4A 19

Leaf petioles, subgroup 4B 6.0

Lychee1 1.0

Onion, bulb, subgroup 3-07A 0.05

Onion, green, subgroup 3-07B 1.1

Potato 0.05

Vegetable, cucurbit, group 9 0.05

Vegetable, fruiting, group 8 0.2

1

 There is no U.S. registration for lychee.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with a regional registration. Tolerances with a regional registration as defined in §180.1(l) are 

established for the residues of the fungicide cymoxanil, 2-cyano -N- [(ethylamino)carbonyl]-2-(methoxyimino) acetamide) 

in or on the raw agricultural commodities:

Commodity Parts per million

Grape 0.10

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 26411, May 14, 1997, as amended at 62 FR 39956, July 25, 1997; 63 FR 24949, May 6, 1998; 63 FR 66464, Dec. 2, 1998; 

64 FR 6539, Feb. 10, 1999; 64 FR 47689, Sept. 1, 1999; 66 FR 37598, July 19, 2001; 67 FR 35049, May 17, 2002; 68 FR 41936, 

July 16, 2003; 70 FR 7047, Feb. 10, 2005; 72 FR 37646, July 11, 2007; 73 FR 58885, Oct. 8, 2008; 76 FR 34885, June 15, 2011]

 Back to Top

§180.504 [Reserved]

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§180.505 Emamectin; tolerances for residues.

(a) General. (1) Tolerances are established for emamectin, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of emamectin (a mixture of a minimum of 90% 4′-epi-methylamino-4′-deoxyavermectin B1a and maximum of 

10% 4′-epi-methylamino-4′-deoxyavermectin B1b) and its metabolites 8,9-isomer of the B1a and B1b component of the 

parent (8,9-ZMA), or 4′-deoxy-4′-epi-amino-avermectin B1a and 4'-deoxy-4′-epi-amino-avermectin B1b; 4′-deoxy-4′-epiamino avermectin B1a (AB1a); 4′-deoxy-4′-epi-(N-formyl-N-methyl)amino-avermectin (MFB1a); and 4′-deoxy-4′

-epi-(N-formyl)amino-avermectin B1a (FAB1a), calculated as the stoichiometric equivalent of emamectin.

Commodity Parts per million

Almond, hulls 0.20

Apple, wet pomace 0.075

Cotton, gin byproducts 0.050

Cotton, undelinted seed 0.025

Fruit, pome, group 11 0.025

Grape, wine1 0.03

Nut, tree, group 14 0.02

Pistachio 0.02

Tomato, paste 0.150

Turnip, greens 0.050

Vegetable, Brassica, leafy, group 5 0.050

Vegetable, cucurbit, group 9 0.02

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Vegetable, fruiting, group 8 0.020

Vegetable, leafy, except Brassica, group 4 0.100

1

There are no U.S. registrations for use of emamectin on grape, wine.

(2) Tolerances are established for emamectin, including its metabolites and degradates, in or on the commodities in 

the following table. Compliance with the tolerance levels specified in the following table is to be determined by measuring 

only the sum of emamectin (MAB1a + MAB1b isomers) and the associated 8,9-Z isomers (8,9-ZB1a and 8,9-ZB1b).

Commodity Parts per million

Cattle, fat 0.010

Cattle, liver 0.050

Cattle, meat 0.003

Cattle, meat byproducts, except liver 0.020

Goat, fat 0.010

Goat, liver 0.050

Goat, meat 0.003

Goat, meat byproducts, except liver 0.020

Hog, fat 0.003

Hog, liver 0.020

Hog, meat 0.002

Hog, meat byproducts (except liver) 0.005

Horse, fat 0.010

Horse, liver 0.050

Horse, meat 0.003

Horse, meat byproducts, except liver 0.020

Milk 0.003

Sheep, fat 0.010

Sheep, liver 0.050

Sheep, meat 0.003

Sheep, meat byproducts, except liver 0.020

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[71 FR 18649, Apr. 12, 2006, as amended at 74 FR 2873, Jan. 16, 2009; 78 FR 18511, Mar. 27, 2013; 78 FR 49939, Aug. 16, 2013]

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§180.506 Cyclanilide; tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth regulator, cyclanilide, 

[1-(2,4-dichlorophenylaminocarbonyl)-cyclopropane carboxylic acid] determined as 2,4-dichloroaniline (calculated as 

cyclanilide) in or on the following food commodities and processed feed:

Commodity Parts Per Million

Cattle, fat 0.10

Cattle, meat 0.02

Cattle, meat byproducts, except kidney 0.2

Cattle, kidney 2.0

Cotton, undelinted seed 0.60

Cotton, gin byproducts 25.0

Goat, fat 0.10

Goat, meat 0.02

Goat, meat byproducts, except kidney 0.20

Goat, kidney 2.0

Horse, fat 0.10

Horse, meat 0.02

Horse, meat byproducts, except kidney 0.20

Horse, kidney 2.0

Hog, fat 0.10

Hog, meat 0.02

Hog, meat byproducts, except kidney 0.20

Hog, kidney 2.0

Milk 0.04

Sheep, fat 0.10

Sheep, meat 0.20

Sheep, meat byproducts, except kidney 0.20

Sheep, kidney 2.0

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(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 28355, May 23, 1997; 62 FR 34182, June 25, 1997]

 Back to Top

§180.507 Azoxystrobin; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of the fungicide, azoxystrobin, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the table is to 

be determined by measuring only the sum of azoxystrobin, [methyl(E)-2-(2-(6-(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)

-3-methoxyacrylate], and the Z-isomer of azoxystrobin [methyl(Z)-2-(2-(6-(2-cyanophenoxy)pyrimidin-4-yloxy)phenyl)-3 

methoxyacrylate] in or on the commodity.

Commodity Parts per million

Acerola 2.0

Almond, hulls 4.0

Animal feed, nongrass, group 18, forage 45

Animal feed, nongrass, group 18, hay 120

Artichoke, globe 4.0

Asparagus 0.04

Atemoya 2.0

Avocado 2.0

Banana *

Barley, bran 6.0

Barley, forage 25

Barley, grain 3.0

Barley, hay 10.0

Barley, straw 15.0

Berry, low growing, subgroup 13-07G, except cranberry 10.0

Biriba 2.0

Brassica, head and stem, subgroup 5A 3.0

Brassica, leafy greens, subgroup 5B 25

Bushberry subgroup 13-07B 5.0

Caneberry subgroup 13-07A 5.0

Canistel 2.0

Cherimoya 2.0

Cilantro, leaves 30.0

Citrus, dried pulp 20.0

Citrus, oil 40.0

Coffee, green bean1 0.03

Corn, field, forage 12.0

Corn, field, grain 0.05

Corn, field, refined oil 0.3

Corn, field, stover 25.0

Corn, pop, grain 0.05

Corn, pop, stover 25.0

Corn, sweet, forage 12.0

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 25.0

Cotton, gin byproducts 45

Cottonseed subgroup 20C 0.7

Cranberry 0.50

Custard apple 2.0

Dragon fruit 2.0

Feijoa 2.0

Fruit, citrus, group 10-10 15.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0

Fruit, stone, group 12 1.5

Ginseng1 0.5

Grain, aspirated fractions 420

Grass, forage 15

Grass, hay 20

Guava 2.0

Herb Subgroup 19A, dried leaves 260

Herb Subgroup 19A, fresh leaves 50

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Hop, dried cones 20.0

Ilama 2.0

Jaboticaba 2.0

Jackfruit 2.0

Longan 2.0

Loquat 2.0

Lychee 2.0

Mango 2.0

Nut, tree, group 14 0.02

Oats, forage 5.0

Oats, grain 1.5

Oats, hay 10.0

Oats, straw 3.0

Onion, bulb, subgroup 3-07A 1.0

Onion, green, subgroup 3-07B 7.5

Papaya 2.0

Passionfruit 2.0

Pawpaw 2.0

Pea and bean, dried shelled, except soybean, subgroup 6C 0.5

Pea and bean, succulent shelled, subgroup 6B 0.5

Peanut 0.2

Peanut, hay 15.0

Peanut, refined oil 0.6

Pear, Asian1 0.07

Pepper/eggplant subgroup 8-10B 3.0

Peppermint, tops 30

Persimmon 2.0

Pistachio 0.50

Pulasan 2.0

Rambutan 2.0

Rapeseed subgroup 20A 1.0

Rice, grain 5.0

Rice, hulls 20

Rice, straw 12

Rice, wild, grain 5.0

Rye, forage 7.0

Rye, grain 0.2

Rye, straw 1.5

Sapodilla 2.0

Sapote, black 2.0

Sapote, mamey 2.0

Sapote, white 2.0

Sorghum, grain, forage 25

Sorghum, grain, grain 11

Sorghum, grain, stover 40

Soursop 2.0

Soybean, hay 55.0

Soybean, hulls 1.0

Soybean, seed 0.5

Spanish lime 2.0

Spearmint, tops 30

Spice Subgroup 19B, except black pepper 38

Star apple 2.0

Starfruit 2.0

Sugar apple 2.0

Sugarcane, cane 0.2

Sunflower subgroup 20B 0.5

Tamarind 2.0

Tea, dried1 20.0

Tomato, paste 0.6

Tomato subgroup 8-10A 0.2

Turnip, greens 25

Vegetable, cucurbit, group 9 0.3

Vegetable, foliage of legume, group 7 30.0

Vegetable, leafy, except brassica, group 4 30.0

Vegetable, leaves of root and tuber, group 2 50.0

Vegetable, legume, edible podded, subgroup 6A, except soybean 3.0

Vegetable, root, subgroup 1A 0.5

Vegetable, tuberous and corm, subgroup 1C 8.0

Wasabi, dry 260

Wasabi, fresh 50

Watercress 3.0

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Wax jambu 2.0

Wheat, forage 15.0

Wheat, grain 0.2

Wheat, hay 30.0

Wheat, straw 10.0

*2.0 (of which not more than 0.1 is contained in the pulp)

1

There are no United States registrations for use of azoxystrobin on coffee, green bean; ginseng; pear, Asian and tea, 

dried.

(2) Tolerances are established for residues of the fungicide, azoxystrobin, including its metabolites and degradates, in 

or on the commodities in the following table. Compliance with the tolerance levels specified in the table is to be determined 

by measuring only azoxystrobin, [methyl(E)-2-(2-(6-(2-cyanophenoxy) pyrimidin-4-yloxy)phenyl)-3-methoxyacrylate] in or 

on the commodity.

Commodity Parts per million

Cattle, fat 0.03

Cattle, meat 0.01

Cattle, meat byproducts 0.07

Goat, fat 0.03

Goat, meat 0.01

Goat, meat byproducts 0.07

Hog, fat 0.010

Hog, meat 0.01

Hog, meat byproducts 0.010

Horse, fat 0.03

Horse, meat 0.01

Horse, meat byproducts 0.07

Milk. 0.006

Sheep, fat 0.03

Sheep, meat 0.01

Sheep, meat byproducts 0.07

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 32235, June 13, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.507, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.509 Mefenpyr-diethyl; tolerance for residues.

(a) General. Tolerances are established for residues of the safener, mefenpyr-diethyl, including its metabolites and 

degradates, when applied at a rate no greater than 0.053 pound safener per acre per growing season in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of mefenpyr-diethyl (1-(2,4-dichlorophenyl)-4,5-dihydro-5-methyl-1H-pyrazole-3,5-dicarboxylic acid, diethyl 

ester) and its 2,4-dichlorophenyl-pyrazoline metabolites, calculated as the stoichiometric equivalent of mefenpyr-diethyl, in 

or on the commodity.

Commodity

Parts per

million

Barley, grain 0.05

Barley, hay 0.2

Barley, straw 0.5

Cattle, meat byproducts 0.1

Goat, meat byproducts 0.1

Grass, forage 1.6

Grass, hay 0.2

Hog, meat byproducts 0.1

Horse, meat byproducts 0.1

Sheep, meat byproducts 0.1

Sorghum, grain, forage 0.4

Sorghum, grain, grain 0.04

Sorghum, grain, stover 0.2

Wheat, forage 0.2

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Wheat, grain 0.05

Wheat, hay 0.2

Wheat, straw 0.5

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of mefenpyrdiethyl, including its metabolites and degradates, when applied at a rate no greater than 0.053 pound safener per acre per 

growing season in or on the commodities identified in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring only the sum of mefenpyr-diethyl (1-(2,4-dichlorophenyl)-4,5-dihydro-5-methyl1H-pyrazole-3,5-dicarboxylic acid, diethyl ester) and its 2,4-dichlorophenyl-pyrazoline metabolites, calculated as the 

stoichiometric equivalent of mefenpyr-diethyl, in or on the commodity.

Commodity

Parts per

million

Canola, seed 0.02

Soybean, forage 0.1

Soybean, hay 0.1

Soybean, seed 0.02

[73 FR 74977, Dec. 10, 2008, as amended at 76 FR 23903, Apr. 29, 2011]

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§180.510 Pyriproxyfen; tolerances for residues.

(a) General. (1) Tolerances are established for residues of pyriproxyfen, including its metabolites and degradates, in 

or on the commodities in the following table. Compliance with the tolerance levels specified is determined by measuring 

only pyriproxyfen, 2-[1-methyl-2-(4-phenoxyphenoxy) ethoxy]pyridine, in or on the commodity.

Commodity Parts per million

Acerola 0.10

Almond, hulls 2.0

Animal feed, nongrass, group 18, forage 0.70

Animal feed, nongrass, group 18, hay 1.1

Animal feed, nongrass, group 18, seed 2.0

Apple, wet pomace 0.8

Artichoke, globe 2.0

Asparagus 2.0

Atemoya 0.20

Avocado 1.0

Banana 0.20

Beet, sugar, dried pulp 3.0 

Berry, low growing, except strawberry, subgroup 13-07H 1.0

Biriba 0.20

Brassica, head and stem, subgroup 5A 0.70

Brassica, leafy greens, subgroup 5B 2.0

Bushberry subgroup 13-07B 1.0

Cacao bean, dried 0.02

Caneberry subgroup 13-07A 1.0

Canistel 1.0

Canola, seed 0.20

Cherimoya 0.20

Citrus, oil 20

Citrus, dried pulp 2.0

Coffee, instant 0.10

Coffee, green bean 0.02 

Cotton, gin byproducts 2.0

Cotton, undelinted seed 0.05

Custard apple 0.20

Date 0.30

Feijoa 0.10

Fig 0.30

Fig, dried fruit 1.0

Fruit, citrus, group 10-10 0.50

Fruit, pome, group 11-10 0.20

Fruit, small, vine climbing, except grape, subgroup 13-07E 0.35

Fruit, stone, group 12 1.0

Grain, cereal, group 15 1.1

Grain, cereal, forage, fodder and straw, group 16 1.1

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Grape 2.5

Grass, forage, fodder, and hay, group 17, forage 0.70

Grass, forage, fodder, and hay, group 17, hay 1.1

Guava 0.10

Herb subgroup 19A 100

Ilama 0.20

Jaboticaba 0.10

Lychee 0.30

Mango 1.0

Nut, tree, group 14 0.02

Olive 1.0

Olive, oil 2.0

Papaya 1.0

Passionfruit 0.10

Pawpaw 1.0

Peanut 0.20

Pineapple 0.30

Pineapple, process residue 1.1

Pistachio 0.02

Pomegranate 0.20

Potato, chips 0.75

Potato, granules/flakes 0.75

Potato, wet peel 0.75

Pulasan 0.30

Rambutan 0.30

Rice, hulls 5.5

Safflower, seed 0.20

Sapodilla 1.0

Sapote, black 1.0

Sapote, mamey 1.0

Sapote, white 0.30

Sesame, seed 0.02

Soursop 0.20

Spanish lime 0.30

Star apple 1.0

Starfruit 0.10

Strawberry 0.30

Sugar apple 0.20

Sugarcane 1.1

Tea 0.02

Vegetable, bulb, group 3-07 0.70

Vegetable, cucurbit, group 9 0.10

Vegetable, foliage of legume, group 7 2.0

Vegetable, fruiting, group 8-10 0.80

Vegetable, leafy, except Brassica, group 4 3.0

Vegetable, leaves of root and tuber, group 2 2.0

Vegetable, legume, group 6 0.20

Vegetable, root and tuber, group 1 0.15

Walnut 0.02

Watercress 2.0

Wax jambu 0.10

(2) A tolerance of 0.10 parts per million is established for all food commodities as a result of the proposed use of 

NYLAR in food handling establishments where food and food products are held, prepared, processed or served. 

Application is limited to space, general surface, spot, and/or crack and crevice treatment in food handling establishments 

where food and food products are held, processed, prepared and served. Space and general surface application may be 

used only when the facility is not in operation provided exposed food is covered or removed from the area being treated 

prior to application. Spot, and/or crack and crevice treatment may be used while the facility is in operation provided 

exposed food is covered or removed from the area being treated prior to application. Food contact surfaces should be 

thoroughly washed with an effective cleaning compound and rinced with potable water after use of the product. To assure 

safe use of this additive, its label and labeling shall conform to that registered with the U.S. Environmental Protection 

Agency, and shall be used in accordance with such label and labeling. 

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 10233, Mar. 3, 1999]

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EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.510, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.511 Buprofezin; tolerances for residues.

(a) General. Tolerances are established for residues of buprofezin, including its metabolites and degradates in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the buprofezin, 2-[(1,1-dimethylethyl)imino]tetrahydro-3(1-methylethyl)-5-phenyl-4H-1,3,5-thiadiazin-4-one, 

in the commodity.

Commodity Parts per million

Acerola 0.30

Almond, hulls 2.0

Apricot 9.0

Atemoya 0.30

Avocado 0.30

Banana 0.20

Bean, snap, succulent 0.02

Bean, succulent 0.02

Berry, low growing, subgroup 13-07G 2.5

Birida 0.30

Brassica, head and stem, subgroup 5A 12.0

Brassica, leafy greens, subgroup 5B 60

Canistel 0.90

Cattle, fat 0.05

Cattle, kidney 0.05

Cattle, liver 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.05

Cherimoya 0.30

Citrus, dried pulp 7.5

Citrus, oil 80

Coffee, green bean 0.35

Cotton, gin byproducts 20.0

Cotton, undelinted seed 0.35

Custard apple 0.30

Feijoa 0.30

Fruit, citrus, group 10 2.5

Fruit, pome, group 11-10, except pear and pear, Asian 3.0

Fruit, stone, group 12, except apricot and peach 1.9

Goat, fat 0.05

Goat, kidney 0.05

Goat, liver 0.05

Goat, meat 0.05

Goat, meat byproducts 0.05

Grape 2.5

Guava 0.3

Hog, fat 0.05

Hog, kidney 0.05

Hog, liver 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.05

Horse, kidney 0.05

Horse, liver 0.05

Horse, meat 0.05

Horse, meat byproducts 0.05

Ilama 0.30

Jaboticaba 0.30

Lettuce, head 6.0

Longan 0.30

Lychee 0.30

Mango 0.90

Milk 0.01

Nut, tree group 14 0.05

Olive 3.5

Olive, oil 4.8

Papaya 0.90

Passionfruit 0.30

Peach 9.0

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Pear 6.0

Pear, Asian 6.0

Persimmon 1.9

Pistachio 0.05

Pomegranate 1.9

Pulasan 0.30

Radicchio 6.0

Rambutan 0.30

Sapodilla 0.90

Sapote, black 0.90

Sapote, mamey 0.90

Sheep, fat 0.05

Sheep, kidney 0.05

Sheep, liver 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.05

Soursop 0.30

Spanish lime 0.30

Star apple 0.90

Starfruit 0.30

Sugar apple 0.30

Tea1 20

Turnip, greens 60

Vegetable, cucurbit, group 9 0.50

Vegetable, fruiting, group 8-10 2.0

Vegetable, leafy, except Brassica, group 4, except head lettuce and radicchio 35

Wax jambu 0.30

1

There are no U.S. registrations at this time.

(b) Section 18 emergency exemption. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[62 FR 40741, July 30, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.511, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.512 [Reserved]

 Back to Top

§180.513 Chlorfenapyr; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide chlorfenapyr [4-bromo-2-(4-chlorophenyl)

-1-(ethoxymethyl)-5-(trifluoromethyl)-1H-pyrrole-3-carbonitrile] in or on the following raw agricultural commodities:

Commodity Parts per million

Vegetable, fruiting, group 8 1.0

(2) A tolerance of 0.01 parts per million is established for residues of chlorfenapyr in or on all food commodities (other 

than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling areas where food/feed 

products are prepared, held, processed, or served and in accordance with the following prescribed conditions:

(i) Application shall be no greater than a 0.5% active ingredient solution for spot crack and crevice use in food/feed 

handling establishments, where food and food products are held, processed, prepared and/or served.

(ii) Application may only be undertaken when the facility is not in operation, and provided exposed food has been 

covered, or removed from the area being treated prior to application.

(iii) Food contact surfaces and equipment should be throughly washed with an effective cleaning compound, and 

rinsed with potable water after each use of the product.

(iv) Contamination of food or food contact surfaces shall be avoided. Application excludes any direct application to 

any food, food packaging, or any food contact surfaces.

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(v) To assure safe use, the label and labeling shall conform to that registered by the U.S. Environmental Protection 

Agency, and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55527, Sept. 26, 2003, as amended at 70 FR 3654, Jan. 26, 2005]

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§180.514 Cloransulam-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, cloransulam-methyl, N-(2-carboxymethyl-6-

chlorophenyl)-5-ethoxy-7-fluoro-(1,2,4)-triazolo[1,5c]-pyrimidine-2-sulfonamide, plus its acid, cloransulam, calculated as 

parent ester in or on the following raw agricultural commodities: 

Commodity Parts per million

Soybean, forage 0.1

Soybean, hay 0.2

Soybean, seed 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 49163, Sept. 19, 1997]

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§180.515 Carfentrazone-ethyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide carfentrazone-ethyl, including its metabolites 

and degradates, in or on the commodities listed in the following table. Compliance with the following tolerance levels is to 

be determined by measuring only the sum of carfentrazone-ethyl (ethyl-alpha-2-dichloro-5-[-4-(difluoromethyl)-4,5-dihydro3-methyl-5-oxo-1H -1,2,4-triazol-1-yl]-4-fluorobenzenepropanoate) and its metabolite carfentrazone-chloropropionic acid 

(alpha, 2-dichloro-5-[-4-difluoromethyl)-4,5-dihydro-3-methyl-5-oxo-1H-1,2,4-triazol-1-yl]-4-fluorobenzenepropanoic acid), 

calculated as the stoichiometric equivalent of carfentrazone-ethyl, in or on the following commodities:

Commodity Parts per million

Acerola 0.10

Almond, hulls 0.20 

Animal feed, nongrass, crop group 18, forage 2.0

Animal feed, nongrass, crop group 18, hay 5.0

Animal feed, nongrass, crop group 18, seed 15.0

Atemoya 0.10 

Avocado 0.10 

Banana 0.20 

Barley, bran 0.80

Barley, flour 0.80

Berry group 13 0.10 

Birida 0.10 

Borage 0.10 

Cacao bean, bean 0.10 

Cactus 0.10

Caneberry subgroup 13A 0.1 

Canistel 0.10 

Canola 0.10 

Cattle, fat 0.10 

Cattle, meat 0.10 

Cattle, meat byproducts 0.10 

Cherimoya 0.10 

Coconut 0.10

Coffee, bean, green 0.10 

Corn, field, forage 0.20 

Corn, sweet, forage 0.20 

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Corn, sweet, kernel plus cob with husk removed 0.10 

Cotton, gin byproducts 10 

Cotton, undelinted seed 0.20 

Cotton, hulls 0.60 

Cotton, meal 0.35 

Cotton, refined oil 1.0 

Crambe, seed 0.10 

Custard apple 0.10 

Date, dried fruit 0.10 

Feijoa 0.10 

Fig 0.10 

Fish 0.30 

Flax, seed 0.10 

Fruit, citrus, group 10 0.10 

Fruit, pome, group 11 0.10 

Fruit, stone, group 12 0.10

Goat, fat 0.10 

Goat, meat 0.10 

Goat, meat byproducts 0.10 

Grain, aspirated grain fractions 1.8

Grain, cereal, forage, fodder and straw group 16, except corn and sorghum; forage 1.0 

Grain, cereal, forage, fodder and straw, group 16, hay 0.30 

Grain, cereal, forage, fodder and straw, group 16, stover 0.30 

Grain, cereal, forage, fodder and straw, group 16, except rice; straw 0.10 

Grain, cereal, group 15 0.10 

Grain, cereal, group 15 (except rice grain and sorghum grain) 0.10

Grain, cereal, stover 0.80

Grain, cereal, straw 3.0

Grape 0.10 

Grass, forage 5.0 

Grass, hay 8.0 

Guava 0.10 

Herbs and spices group 19 2.0 

Hog, fat 0.10

Hog, meat 0.10

Hog, meat byproducts 0.10

Hop, dried cones 0.10 

Horse, fat 0.10 

Horse, meat 0.10 

Horse, meat byproducts 0.10 

Horseradish 0.10 

Ilama 0.10 

Jaboticaba 0.10 

Juneberry 0.10 

Kava, roots 0.10 

Kiwifruit 0.10 

Lingonberry 0.10 

Longan 0.10 

Lychee 0.10 

Mango 0.10 

Milk 0.05 

Millet, flour 0.80

Mustard, seed 0.10 

Noni 0.10 

Nut, tree, group 14 0.10 

Oat, flour 0.80

Okra 0.10 

Olive 0.10 

Palm heart 0.10 

Palm heart, leaves 0.10 

Papaya 0.10 

Passionfruit 0.10 

Pawpaw 0.10 

Peanut 0.10 

Peanut, hay 0.10 

Persimmon 0.10 

Pistachio 0.10 

Pomegranate 0.10 

Poultry, meat byproducts 0.10

Pulasan 0.10 

Pummelo 0.10 

Rambutan 0.10 

Rapeseed, forage 0.10 

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Rapeseed, seed 0.10

Rice, grain 1.3

Rice, hulls 3.5

Rice, straw 1.0 

Rye, bran 0.80

Rye, flour 0.80

Safflower, seed 0.10 

Salal 0.10 

Sapodilla 0.10 

Sapote, black 0.10 

Sapote, mamey 0.10 

Sheep, fat 0.10 

Sheep, meat 0.10 

Sheep, meat byproducts 0.10 

Shellfish 0.30 

Sorghum, forage 0.20

Sorghum, grain 0.25

Sorghum, sweet 0.10 

Soursop 0.10

Soybean, seed 0.10

Spanish lime 0.10 

Star apple 0.10 

Starfruit 0.10 

Stevia 0.10 

Strawberry 0.10 

Strawberrypear 0.10 

Sugar apple 0.10 

Sugarcane 0.15

Sunflower, seed 0.10 

Tea, dried 0.10 

Ti, leaves 0.10 

Ti, roots 0.10 

Vanilla 0.10 

Vegetable, brassica, leafy, group 5 0.10 

Vegetable, bulb, group 3 0.10 

Vegetable, cucurbit, group 9 0.10 

Vegetable, foliage of legume, except soybean, subgroup 7A 0.10 

Vegetable, fruiting, group 8 0.10 

Vegetable, leafy, except brassica, group 4 0.10 

Vegetable, leaves of root and tuber, group 2 0.10 

Vegetable, legume, group 6 0.10 

Vegetable, root and tuber, group 1 0.10 

Wasaba, roots 0.10 

Wax jambu 0.10

Wheat, bran 0.80

Wheat, flour 0.80

Wheat, germ 0.80

Wheat, middlings 0.80

Wheat, shorts 0.80

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 52180, Sept. 30, 1998]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.515, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.516 Fludioxonil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide fludioxonil, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only fludioxonil, 4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1-H-pyrrole-3-carbonitrile).

Commodity Parts per million

Acerola 5.0

Animal feed, nongrass, group 18 0.01

Atemoya 20

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Avocado 5.0

Bean, dry 0.4

Bean, succulent 0.4

Beet, sugar, roots 0.02

Berry, low growing, subgroup 13-07G, except cranberry 3.0

Biriba 20

Brassica, head and stem, subgroup 5A 2.0

Brassica, leafy greens, subgroup 5B 10

Bushberry subgroup 13-07B 2.0

Caneberry subgroup 13-07A 5.0

Canistel 5.0

Carrots 7.0

Cherimoya 20

Citrus, oil 500

Cotton, gin byproducts 0.05

Cotton, undelinted seed 0.05

Custard apple 20

Dragon fruit 1.0

Feijoa 5.0

Flax, seed 0.05

Fruit, citrus, group 10-10 10

Fruit, pome, group 11-10 5.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0

Fruit, stone, group 12-12 5.0

Ginseng 4.0

Grain, cereal, group 15 0.02

Grain, cereal, forage, fodder, and straw, group 16 0.01

Grass, forage, fodder and hay, group 17 0.01

Guava 5.0

Herb subgroup 19A, dried leaves 65

Herb subgroup 19A, fresh leaves 10

Ilama 20

Jaboticaba 5.0

Kiwifruit, fuzzy 20

Leaf petioles subgroup 4B 15

Leafy greens subgroup 4A 30

Longan 20

Lychee 20

Mango 5.0

Melon subgroup 9A 0.03

Onion, bulb, subgroup 3-07A 0.50

Onion, green, subgroup 3-07B 7.0

Papaya 5.0

Passionfruit 5.0

Peanut 0.01

Peanut, hay 0.01

Pineapple 20

Pistachio 0.10

Pomegranate 5.0

Pulasan 20

Rambutan 20

Rapeseed, forage 0.01

Rapeseed subgroup 20A, except flax seed 0.01

Safflower, seed 0.01

Sapodilla 5.0

Sapote, black 5.0

Sapote, mamey 5.0

Soursop 20

Spanish lime 20

Spice subgroup 19B 0.02

Star apple 5.0

Starfruit 5.0

Sugar apple 20

Sunflower, seed 0.01

Tomato 5.0

Turnip, greens 10

Vegetable, cucurbit, group 9 0.45

Vegetable, foliage of legume, group 7 0.01

Vegetable, fruiting, group 8-10, except tomato 0.50

Vegetable, leaves of root and tuber, group 2 30

Vegetable, legume, group 6 0.01

Vegetable, root, except sugar beet, subgroup 1B 0.75

Vegetable, tuberous and corm, subgroup 1C 6.0

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Watercress 7.0

Wax jambu 5.0

Yam, true, tuber 8.0

(2) Tolerances are established for residues of the fungicide fludioxonil, including its metabolites and degradates, in or 

on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only the sum of fludioxonil, 4-(2,2-difluoro-1,3-benzodioxol-4-yl)-1-H-pyrrole-3-carbonitrile), and 

its metabolites converted to 2,2-difluoro-l,3-benzodioxole-4-carboxylic acid, calculated as the stoichiometric equivalent of 

fludioxonil.

Commodity Parts per million

Cattle, fat 0.05

Cattle, meat 0.01

Cattle, meat byproducts 0.05

Goat, fat 0.05

Goat, meat 0.01

Goat, meat byproducts 0.05

Horse, fat 0.05

Horse, meat 0.01

Horse, meat byproducts 0.05

Milk 0.01

Sheep, fat 0.05

Sheep, meat 0.01

Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 56082, Oct. 29, 1997]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.516, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.517 Fipronil; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Therefore, tolerances are established for combined residues of the insecticide fipronil (5-amino1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile) and its metabolites

5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl) sulfonyl]-1H-pyrazole-3-carbonitrile and 5-amino1-[2,6-dichloro-4-(trifluoromethyl) phenyl]-4-[(trifluoromethyl)thio]-1H-pyrazole-3-carbonitrile and its photodegradate 

5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile in or on the 

following items at the levels specified:

Commodity Parts per million

Cattle, fat 0.40 

Cattle, liver 0.10 

Cattle, meat 0.04 

Cattle, meat byproducts, except liver 0.04 

Corn, field, grain 0.02

Corn, field, stover 0.30

Corn, field, forage 0.15

Egg 0.03

Goat, fat 0.40 

Goat, liver 0.10 

Goat, meat 0.04 

Goat, meat byproducts, except liver 0.04 

Hog, fat 0.04

Hog, liver 0.02

Hog, meat 0.01

Hog, meat byproducts, except liver 0.01

Horse, fat 0.40 

Horse, liver 0.10 

Horse, meat 0.04 

Horse, meat byproducts, except liver 0.04 

Milk, fat (reflecting 0.05 ppm in whole milk) 1.50

Potato 0.03

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Potato, wet peel 0.10

Poultry, fat 0.05

Poultry, meat 0.02

Poultry, meat byproducts 0.02

Rice, grain 0.04

Rice, straw 0.10

Sheep, fat 0.40 

Sheep, liver 0.10 

Sheep, meat 0.04 

Sheep, meat byproducts, except liver 0.04

(b) Section 18 emergency exemptions.. Time-limited tolerances are established for combined residues of the 

insecticide, fipronil, 5-amino-1-(2,6-dichloro-4-(trifluoromethyl) phenyl)-4-((1,R,S)-trifluoromethyl)sulfinyl)-1-H-pyrazole-3-

carbonitrile and its 2 metabolites MB45950 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)thio]-1Hpyrazole-3-carbonitrile) and MB46136 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl)-4-[(trifluoromethyl)sulfonyl]-1Hpyrazole-3-carbonitrile) and its photodegradate MB46513 (5-amino-1-(2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(1R,S)

-(trifluoromethyl)]-1H-pyrazole-3-carbonitrile), in connection with use of the pesticide under Section 18 emergency 

exemptions granted by EPA. The tolerances expire and are revoked on the dates specified in the table for this paragraph.

Commodity Parts per million Expiration/revocation date

Rutabaga 1.0 12/31/16

Turnip 1.0 12/31/16

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for combined indirect or inadvertent residues of the 

insecticide fipronil and its metabolites and photodegradate in or on food commodities when present therein as a result of 

the application of fipronil to growing crops listed in paragraphs (a) and (b) of this section and other nonfood crops to read 

as follows:

Commodity Parts per million

Wheat, forage 0.02

Wheat, grain 0.005

Wheat, hay 0.03

Wheat, straw 0.03

[62 FR 62979, Nov. 26, 1997, as amended at 63 FR 38495, July 17, 1998; 72 FR 46913, Aug. 22, 2007; 74 FR 46377, Sept. 9, 

2009; 75 FR 80346, Dec. 22, 2010; 78 FR 78748, Dec. 27, 2013]

 Back to Top

§180.518 Pyrimethanil; tolerances for residues.

Link to an amendment published at 80 FR 63691, October 21, 2015.

(a) General. (1) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and 

degradates, in or on the commodities in the following table Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only pyrimethanil (4,6-dimethyl-N-phenyl-2-pyrimidinamine).

Commodity Parts per million

Almond 0.20

Almond, hulls 12

Apple, wet pomace 40

Banana 0.10

Berry, low growing, subgroup 13-07G 3.0

Bushberry subgroup 13-07B 8.0

Caneberry subgroup 13-07A 15

Citrus, oil 150

Cucumber 1.5

Fruit, citrus, group 10-10 10

Fruit, pome, group 11-10 15

Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 5.0

Fruit, stone, group 12-12 10

Ginseng 1.5

Grape, raisin 8.0

Onion, bulb, subgroup 3-07A 2.0

Onion, green, subgroup 3-07B 3.0

Pistachio 0.20

Pomegranate 5.0

Tomato subgroup 8-10A 0.50

Vegetable, tuberous and corm, subgroup 1C 0.05

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(2) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in 

or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only the sum of pyrimethanil and its metabolite 4-[4,6-dimethyl-2-pyrimidinyl)amino]phenol, 

calculated as the stoichiometric equivalent of pyrimethanil.

Commodity Parts per million

Cattle, fat 0.01

Cattle, kidney 2.5

Cattle, meat 0.01

Cattle, meat byproducts, except kidney 0.01

Goat, fat 0.01

Goat, kidney 2.5

Goat, meat 0.01

Goat, meat byproducts, except kidney 0.01

Horse, fat 0.01

Horse, kidney 2.5

Horse, meat 0.01

Horse, meat byproducts, except kidney 0.01

Sheep, fat 0.01

Sheep, kidney 2.5

Sheep, meat 0.01

Sheep, meat byproducts, except kidney 0.01

(3) Tolerances are established for residues of the fungicide pyrimethanil, including its metabolites and degradates, in 

or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only the sum of pyrimethanil and its metabolite 4,6-dimethyl-2-(phenylamino)-5-pyrimidinol, 

calculated as the stoichiometric equivalent of pyrimethanil.

Commodity Parts per million

Milk 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[62 FR 63669, Dec. 2, 1997, as amended at 69 FR 52443, Aug. 26, 2004; 73 FR 64251, Oct. 29, 2008; 74 FR 32448, July 8, 2009; 

77 FR 45503, Aug. 1, 2012; 80 FR 7975, Feb. 13, 2015; 80 FR 63691, Oct. 21, 2015]

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§180.519 Bromide ion and residual bromine; tolerances for residues.

(a) General. The food additives, bromide ion and residual bromine, may be present in water, potable in accordance 

with the following conditions:

(1) The food additives are present as a result of treating water aboard ships with a polybrominated ion-exchange resin 

(as a source of bromine) under the supervision of trained personnel.

(2) Residual bromine levels are controlled to not exceed 1.0 part per million (ppm) in the final treated water. Control is 

effected using calibrated recirculating or proportioning bromine feeder equipment and periodic checks of residual bromine 

using a bromine test kit. To assure safe use of the additives, the label and labeling of the disinfectant formulation 

containing the food additives shall conform to the label and labeling registered by the U.S. Environmental Protection 

Agency.

(3) No tolerance is established for bromide ion levels.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[41 FR 17893, Apr. 29, 1976. Redesignated at 41 FR 26568, June 28, 1976, and at 53 FR 24667, June 29, 1988. Redesignated and 

amended at 63 FR 34319, June 24, 1998; 71 FR 74818, Dec. 13, 2006]

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§180.521 Fumigants for grain-mill machinery; tolerances for residues.

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(a) General. Fumigants may be safely used in or on grain-mill machinery in accordance with the following prescribed 

conditions:

(1) The fumigants consist of methyl bromide.

(2) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling registered by the 

U.S. Environmental Protection Agency.

(3) Residues of inorganic bromides (calculated as Br) in milled fractions derived from cereal grain from all fumigation 

sources, including fumigation of grain-mill machinery, shall not exceed 125 parts per million.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 14156, Mar. 28, 1975. Redesignated at 41 FR 26568, June 28, 1976, as amended at 49 FR 44459, Nov. 7, 1984. Further 

redesignated at 53 FR 24667, June 29, 1988, as amended at 54 FR 6130, Feb. 8, 1989. Further redesignated and amended at 63 

FR 34319, June 24, 1998]

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§180.522 Fumigants for processed grains used in production of fermented malt beverage; tolerances for 

residues.

(a) General. Fumigants for processed grain may be safely used, in accordance with the following conditions.

(1) Methyl bromide. Total residues of inorganic bromides (calculated as Br) from the use of this fumigant shall not 

exceed 125 parts per milion.

(2) Methyl bromide is used to fumigate corn grits and cracked rice in the production of fermented malt beverage.

(3) To assure safe use of the fumigant, its label and labeling shall conform to the label and labeling registered by the 

U.S. Environmental Protection Agency, and the usage employed should conform with such label or labeling.

(4) The total residue of inorganic bromides in fermented malt beverage, resulting from the use of corn grits and 

cracked rice fumigated with the fumigant described in paragraph (a)(2) of this section plus additional residues of inorganic 

bromides that may be present from uses in accordance with other regulations in this chapter promulgated under section 

408 and/or 409 of the Act, does not exceed 25 parts per million bromide (calculated as Br).

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74818, Dec. 13, 2006]

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§180.523 Metaldehyde; tolerances for residues.

(a) General. Tolerances are established for residues of the molluscicide metaldehyde, including its metabolites and 

degradates, in or on the commodities listed in the following table. Compliance with the specified tolerance levels is to be 

determined by measuring only metaldehyde, 2,4,6,8-tetramethyl-1,3,5,7-tetroxocane, in or on the commodity.

Commodity Parts per million

Artichoke, globe 0.07

Berry, low growing, subgroup 13-07G 6.25

Bushberry subgroup 13-07B 0.15

Cactus 0.07

Caneberry subgroup 13-07A 0.15

Corn, field, forage 0.30

Corn, field, grain 0.05

Corn, field, stover 0.10

Corn, sweet, forage 0.30

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 0.10

Fruit, citrus, group 10-10 0.26

Ginseng 0.05

Grass, forage 2.0

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Grass, hay 2.0

Leaf petioles subgroup 4B 0.50

Lettuce 1.73

Pea and bean, succulent shelled, subgroup 6B 0.20

Peppermint, oil 12

Peppermint, tops 4.0

Spearmint, oil 12

Spearmint, tops 4.0

Taro, corm 0.15

Taro, leaves 1.0

Tomato subgroup 8-10A 0.24

Vegetable, brassica, leafy, group 5 2.5

Vegetable, foliage of legume, except soybean, subgroup 7A 1.5

Vegetable, legume, edible podded subgroup 6A 0.80

Watercress 3.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with a regional registration as defined in §180.1(l) are 

established for residues of the molluscicide metaldehyde, including its metabolites and degradates, in or on the following 

commodities. Compliance with the specified tolerance level is to be determined by measuring only metaldehyde, 

2,4,6,8-tetramethyl-1,3,5,7-tetroxocane, in or on the commodity.

Commodity Parts per million

Clover, forage 0.60

Clover, hay 0.60

Soybean, seed 0.05

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54963, Sept. 24, 2008, as amended at 78 FR 70869, Nov. 27, 2013; 80 FR 11588, Mar. 4, 2015]

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§180.525 Resmethrin; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide resmethrin [5-(phenylmethyl)-3-furanyl] methyl 

2,2-dimethyl-3-(2-methyl-1-propenyl) cyclopropanecarboxylate in or on food commodities at 3.0 ppm resulting from use of 

the insecticide in food handling and storage areas as a space concentration for spot/or crack and crevice treatment and 

shall be limited to a maximum of 3.00 percent of the active ingredient by weight, and as a space treatment shall be limited 

to a maximum of 0.5 fluid ounce of 3.0 percent active ingredient by weight per 1000 cubic feet of space provided that the 

food is removed or covered prior to such use. To assure safe use of the additive, its label and labeling shall conform to 

that registered with the U.S. Environmental Protection Agency, and shall be used in accordance with such label and 

labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 74819, Dec. 13, 2006]

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§180.526 Synthetic isoparaffinic petroleum hydrocarbons; tolerances for residues.

(a) General. Synthetic isoparaffinic petroleum hydrocarbons complying with 21 CFR 172.882 (a) and (b) may be 

safely used as a component of insecticide formulations for use on animal feed in an amount no greater than reasonably 

required to accomplish its intended effect as an adjuvant in the insecticide formulation and shall not be intended to 

accomplish any effect in animal feed. It is used or intended for use as a component of insecticide formulations used in 

compliance with regulations issued in 40 CFR part 180 and in this part.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[40 FR 14161, Mar. 28, 1975, as amended at 50 FR 2959, Jan. 23, 1985, and amended at 53 FR 24668, 24669, June 29, 1988. 

Redesignated and amended at 63 FR 34319, June 24, 1998]

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§180.527 Flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]

acetamide and its metabolites containing the 4-fluoro-N-methylethyl benzenamine tolerances for residues.

(a) General. Tolerances are established for the combined residues of the herbicide flufenacet, N-(4-fluorophenyl)

-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide and its metabolites containing the 

4-fluoro-N-methylethyl benzenamine moiety in or on the following commodities.

Commodity Parts per million

Cattle, kidney 0.05

Corn, field, forage 0.4

Corn, field, grain 0.05

Corn, field, stover 0.4

Corn, sweet, forage 0.45

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 0.30

Goat, kidney 0.05

Hog, kidney 0.05

Horse, kidney 0.05

Sheep, kidney 0.05

Soybean, seed 0.1

Wheat, bran 0.80

Wheat, forage 6.0

Wheat, grain 0.60

Wheat, hay 1.2

Wheat, straw 0.35

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances are established for combined residues of flufenacet, 

N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1, 3, 4-thiadiazol-2-yl] oxy]acetamide, and its metabolites 

containing the 4-fluoro-N-methylethyl benzenamine moiety, with regional registration.

Commodity Parts per million

Grass, forage 7.0

Grass, hay 0.4

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent residues of the herbicide 

flufenacet, N-(4-fluorophenyl)-N-(1-methylethyl)-2-[[5-(trifluoromethyl)-1,3,4-thiadiazol-2-yl]oxy]acetamide and its 

metabolites containing the 4-fluoro-N-methylethyl benzenamine moiety in or on the following raw agricultural commodities 

when present therein as a result of application of flufenacet to the growing crops in paragraph (a) of this section.

Commodity Parts per million

Alfalfa, forage 0.1

Alfalfa, hay 0.1

Alfalfa, seed 0.1

Clover, forage 0.1

Clover, hay 0.1

Grain, cereal, group 15, except rice 0.1

Grain, cereal, forage, fodder, and straw, group 16, except rice 0.1

Grass, forage, fodder, and hay, group 17 0.1

[63 FR 26473, May 13, 1998, as amended at 63 FR 50791, Sept. 23, 1998; 64 FR 42846, Aug. 6, 1999; 65 FR 64366, Oct. 27, 2000; 

68 FR 2247, Jan. 16, 2003; 68 FR 37759, June 25, 2003; 70 FR 37696, June 30, 2005; 71 FR 76200, Dec. 20, 2006; 72 FR 26310, 

May 9, 2007]

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§180.530 2,2-Dimethyl-1,3-benzodioxol-4-ol methylcarbamate; tolerances for residues.

(a) General. (1) The insecticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate may be safely used in spot and/or 

crack and crevice treatments in animal feed handling establishments, including feed manufacturing and processing 

establishments, such as stores, supermarkets, dairies, meat slaughtering and packing plants, and canneries until the 

tolerance expiration/revocation date of April 26, 2005.

(2) The insecticide 2,2-dimethyl-1,3-benzodioxol-4-yl methylcarbamate may be safely used in spot and/or crack and 

crevice treatments in food handling establishments, including food service, manufacturing and processing establishments, 

such as restaurants, cafeterias, supermarkets, bakeries, breweries, dairies, meat slaughtering and packing plants, and 

canneries until the tolerance expiration/revocation date of April 26, 2005.

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(3) To ensure safe use of the additive, its label and labeling shall conform to that registered with the U.S. 

Environmental Protection Agency and it shall be used in accordance with such label and labeling.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 34828, June 26, 1998, as amended at 69 FR 58083, Sept. 29, 2004]

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§180.532 Cyprodinil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide cyprodinil, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine.

Commodity

Parts per

million

Acerola 1.5

Almond 0.02

Almond, hulls 8.0

Apple, wet pomace 4.6

Artichoke, globe 4.0

Avocado 1.2

Bean, dry 0.6

Bean, succulent 0.6

Berry, low growing, subgroup 13-07G, except cranberry 5.0

Brassica, head and stem, subgroup 5A 1.0

Brassica, leafy greens, subgroup 5B 10.0

Bushberry subgroup 13-07B 3.0

Caneberry subgroup 13-07A 10

Canistel 1.2

Canola, seed1 0.03

Citrus, dried pulp 8.0

Citrus, oil 60

Dragon fruit 2.0

Feijoa 1.5

Fruit, pome, group 11-10 1.7

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0

Fruit, stone, group 12-12 2.0

Grape, raisin 5.0

Guava 1.5

Herb subgroup 19A, dried, except parsley 15.0

Herb subgroup 19A, fresh, except parsley 3.0

Jaboticaba 1.5

Kiwifruit 1.8

Leaf petioles subgroup 4B 30

Leafy greens subgroup 4A 50

Lemon 0.60

Lime 0.60

Longan 2.0

Lychee 2.0

Mango 1.2

Onion, bulb, subgroup 3-07A 0.6

Onion, green, subgroup 3-07B 4.0

Papaya 1.2

Parsley, dried leaves 170

Parsley, leaves 35

Passionfruit 1.5

Pistachio 0.10

Pomegranate 10

Pulasan 2.0

Rambutan 2.0

Sapodilla 1.2

Sapote, black 1.2

Sapote, mamey 1.2

Spanish lime 2.0

Star apple 1.2

Starfruit 1.5

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Turnip, greens 10.0

Vegetable, cucurbit, group 9 0.70

Vegetable, fruiting, group 8-10 1.5

Vegetable, leaves of root and tuber, group 2 10

Vegetable, root, except sugarbeet, subgroup 1B 0.75

Watercress 20

Wax jambu 1.5

1

Import only.

(2) Tolerances are established for residues of the fungicide cyprodinil, including its metabolites and degradates, in the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of cyprodinil 4-cyclopropyl-6-methyl-N-phenyl-2-pyrimidinamine and free and conjugated CGA-304075 

4-(4-cyclopropyl-6-methyl-pyrimidin-2-ylamino)-phenol, calculated as the stoichiometric equivalent of cyprodinil.

Commodity

Parts per

million

Cattle, meat byproducts 0.02

Goat, meat byproducts 0.02

Horse, meat byproducts 0.02

Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 17706, Apr. 10, 1998]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.532, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.533 Esfenvalerate; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the insecticide esfenvalerate, (S)-cyano

(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer, (R)-cyano

(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano

(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-

chloro-α-(1-methylethyl)benzeneacetate, in or on food commodities as follows:

Commodity Parts per million

Almond 0.2

Almond, hulls 5.0

Apple 1.0

Artichoke, globe 1.0

Bean, dry, seed 0.25

Bean, snap, succulent 1.0

Beet, sugar, roots 0.05

Beet, sugar, tops 5.0

Blueberry 1.0

Broccoli 1.0

Cabbage, except Chinese cabbage 3.0

Caneberry subgroup 13A 1.0

Cantaloupe 0.5

Carrot, roots 0.5

Cattle, fat 1.5

Cattle, meat 1.5

Cattle, meat byproducts 1.5

Cauliflower 0.5

Collards 3.0

Corn, field, forage 15.0

Corn, field, grain 0.02

Corn, field, stover 15.0

Corn, pop, grain 0.02

Corn, pop, stover 15.0

Corn, sweet, forage 15.0

Corn, sweet, kernel plus cob with husks removed 0.1

Corn, sweet, stover 15.0

Cotton, undelinted seed 0.2

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Cucumber 0.5

Egg 0.03

Eggplant 0.5

Elderberry 1.0

Fruit, stone, group 12 3.0

Goat, fat 1.5

Goat, meat 1.5

Goat, meat byproducts 1.5

Gooseberry 1.0

Hazelnut 0.2

Hog, fat 1.5

Hog, meat 1.5

Hog, meat byproducts 1.5

Horse, fat 1.5

Horse, meat 1.5

Horse, meat byproducts 1.5

Kiwifruit 0.5

Lentil, seed 0.25

Melon, honeydew 0.5

Milk 0.3

Milk, fat 7.0

Muskmelon 0.5

Mustard greens 5.0

Okra 0.5

Pea, dry, seed 0.25

Pea, succulent 0.5

Peanut 0.02

Pear 1.0

Pecan 0.2

Pepper 0.5

Potato 0.02

Poultry, fat 0.3

Poultry, liver 0.03

Poultry, meat 0.03

Poultry, meat byproducts, except liver 0.3

Pumpkin 0.5

Radish, roots 0.3

Radish, tops 3.0

Sheep, fat 1.5

Sheep, meat 1.5

Sheep, meat byproducts 1.5

Sorghum, grain, forage 10.0

Sorghum, grain, grain 5.0

Sorghum, grain, stover 10.0

Soybean, hulls 0.5

Soybean, seed 0.05

Squash, summer 0.5

Squash, winter 0.5

Sugarcane, cane 1.0

Sunflower, seed 0.5

Sweet potato, roots 0.05

Tomato 0.5

Turnip, greens 7.0

Turnip, roots 0.5

Walnut 0.2

Watermelon 0.5

(2) A tolerance of 0.05 ppm on raw agricultural food commodities (other than those food commodities already covered 

by a higher tolerance as a result of use on growing crops) is established for the combined residues of the insecticide 

esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, its non-racemic isomer, 

(R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and its diastereomers (S)-cyano

(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-

chloro-α-(1-methylethyl)benzeneacetate as a result of the use of esfenvalerate in food-handling establishments.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registration are established for the combined 

residues of the insecticide esfenvalerate, (S)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)

benzeneacetate, its non-racemic isomer, (R)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)

benzeneacetate and its diastereomers (S)-cyano(3-phenoxyphenyl)methyl-(R)-4-chloro-α-(1-methylethyl)benzeneacetate 

and (R)-cyano(3-phenoxyphenyl)methyl-(S)-4-chloro-α-(1-methylethyl)benzeneacetate, in or on food commodities as 

follows:

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Commodity Parts per million

Cabbage, chinese, bok choy 1.0

Kohlrabi 2.0

Lettuce, head 5.0

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 23401, Apr. 29, 1998, as amended at 63 FR 48615, Sept. 11, 1998; 74 FR 46699, Sept. 11, 2009]

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§180.535 Fluroxypyr 1-methylheptyl ester; tolerances for residues.

(a) General. Tolerances are established for combined residues of fluroxypyr 1-methylheptyl ester [1-methylheptyl 

((4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)acetate] and its metabolite fluroxypyr [((4-amino-3,5-dichloro-6-fluoro-2-

pyridinyl)oxy)acetic acid] in or on the following raw agricultural commodities. Compliance with the established tolerance 

levels is determined by measuring only the sum of fluroxypyr 1-methylheptyl ester [1-methylheptyl ((4-amino-3, 5-dichloro6-fluoro-2-pyridinyl)oxy)acetate] and its metabolite fluroxypyr [((4-amino-3,5-dichloro-6-fluoro-2-pyridinyl)oxy)acetic acid] 

calculated as the stoichiometric equivalent of fluroxypyr.

Commodity Parts per million

Barley, grain 0.5

Barley, hay 12.0

Barley, hay 20.0 

Barley, straw 12.0

Cattle, fat 0.1

Cattle, kidney 1.5

Cattle, meat 0.1

Cattle, meat byproducts 0.1

Corn, field, forage 1.0

Corn, field, grain 0.02

Corn, field, stover 0.5

Corn, sweet, forage 1.0

Corn, sweet, kernel plus cob with husks removed 0.02

Corn, sweet, stover 2.0

Fruit, pome, group 11 0.02

Garlic, bulb 0.03 

Goat, fat 0.1

Goat, kidney 1.5

Goat, meat 0.1

Goat, meat byproducts 0.1

Grain, aspirated fractions 0.6

Grass, forage 120

Grass, hay 160

Hog, fat 0.1

Hog, kidney 1.5

Hog, meat 0.1

Hog, meat byproducts 0.1

Horse, fat 0.1

Horse, kidney 1.5

Horse, meat 0.1

Horse, meat byproducts 0.1

Milk 0.3

Millet, forage 12.0

Millet, grain 0.5

Millet, hay 20.0

Millet, proso, straw 12.0

Oat, forage 12.0

Oat, grain 0.5

Oat, hay 20.0

Oat, straw 12.0

Onion, bulb 0.03 

Rice, bran 3.0

Rice, grain 1.5

Shallot, bulb 0.03 

Sheep, fat 0.1 

Sheep, kidney 1.5

Sheep, meat 0.1

Sheep, meat byproducts 0.1

Sorghum, grain, forage 2.0

Sorghum, grain, grain 0.02

Sorghum, grain, stover 4.0

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Wheat, forage 12.0 

Wheat, grain 0.5 

Wheat, hay 20.0

Wheat, straw 12.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 52169, Sept. 30, 1998, as amended at 64 FR 22799, Apr. 28, 1999; 66 FR 37598, July 19, 2001; 66 FR 47971, Sept. 17, 

2001; 67 FR 46884, July 17, 2002; 67 FR 60146, Sept. 25, 2002; 68 FR 75438, Dec. 31, 2003; 69 FR 2074, Jan. 14, 2004; 70 FR 

3649, Jan. 26, 2005; 70 FR 7047, Feb. 10, 2005; 71 FR 76204, Dec. 20, 2006; 72 FR 73635, Dec. 28, 2007; 78 FR 3333, Jan. 16, 

2013]

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§180.537 Isoxaflutole; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, isoxaflutole, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of isoxaflutole ((5-cyclopropyl-4-isoxazolyl) [2-(methylsulfonyl)-4-(trifluoromethyl)

phenyl] methanone) and its metabolite 1-(2-methylsulfonyl-4-trifluoromethylphenyl)-2-cyano-3-cyclopropyl 

propan-1,3-dione (RPA 202248), calculated as the stoichiometric equivalent of isoxaflutole, in or on the commodity:

Commodity Parts per million

Corn, field, forage 0.04

Corn, field, grain 0.02

Corn, field, stover 0.02

Grain, aspirated fractions 0.30

Soybean, seed 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 50784, Sept. 23, 1998, as amended at 73 FR 75608, Dec. 12, 2008; 76 FR 76314, Dec. 7, 2011]

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§180.539 d-Limonene; tolerances for residues.

(a) General. (1) The insecticide d-limonene may be safely used in insect-repellent tablecloths and in insect-repellent 

strips used in food- or feed-handling establishments.

(2) To assure safe use of the insect repellent, its label and labeling shall conform to that registered by the U.S. 

Environmental Protection Agency, and it shall be used in accordance with such label and labeling. 

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33715, May 24, 2000, as amended at 70 FR 55268, Sept. 21, 2005]

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§180.540 Fenitrothion; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide fenitrothion, O,O-dimethyl O-(4-nitro-m-tolyl) 

phosphorothioate, from the postharvest application of the insecticide to stored wheat in Australia, in or on the following 

food commodity:

Commodity Parts per million 

Wheat, gluten1 3.0 

1

There are no U.S. registrations on food commodities since 1987.

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(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 54963, Sept. 24, 2008]

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§180.541 Propetamphos; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. A tolerance of 0.1 part per million is established for residues of the insecticide propetamphos, including 

its metabolites and degradates, in or on food or feed commodities when present therein as a result of the treatment of 

food- or feed-handling establishments with propetamphos. Direct application shall be limited solely to spot and/or crack 

and crevice treatment in food- or feed-handling establishments where food or feed and food or feed products are held, 

processed, prepared, served, or sold. Spray and dust concentrations shall be limited to a maximum of 1 percent active 

ingredient. For crack and crevice treatment, equipment capable of delivering a dust or a pin-stream of spray directly into 

cracks and crevices shall be used. For spot treatment, a coarse, low-pressure spray shall be used to avoid contamination 

of food, feed, or food-contact/feed-contact surfaces. Compliance with the tolerance level specified in this paragraph is to 

be determined by measuring only propetamphos, 1-methylethyl-(2E)-3-((ethylamino)methoxyphosphinothioyl)oxy)-2-

butenoate, in or on the commodity.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 33716, May 24, 2000, as amended at 76 FR 23498, Apr. 27, 2011]

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§180.543 Diclosulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide diclosulam [N-(2,6-dichlorophenyl)-5-ethoxy-7-

fluoro[1,2,4] triazolo[1,5-c]pyrimidine-2-sulfonamide] in or on the following raw agricultural commodities as follows: 

Commodity 

Parts per

million 

Peanut 0.020 

Soybean, seed 0.020

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 12134, Mar. 8, 2000]

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§180.544 Methoxyfenozide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide methoxyfenozide, including its metabolites 

and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the 

following table is to be determined by measuring only methoxyfenozide (3-methoxy-2-methylbenzoic acid 

2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide) in or on the commodity.

Commodity Parts per million 

Acerola 0.4

Almond, hulls 25

Animal feed, nongrass, group 18, forage 50.0

Animal feed, nongrass, group 18, hay 150.0

Apple, wet pomace 7.0

Artichoke, globe 3.0

Atemoya 0.60

Avocado 0.6

Beet, sugar, roots 0.50

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Berry, low growing, subgroup 13-07G, except cranberry 2.0

Biriba 0.60

Brassica, head and stem, subgroup 5A 7.0

Brassica, leafy greens, subgroup 5B 30

Bushberry subgroup 13-07B 3.0

Caneberry subgroup 13-07A 6.0

Canistel 0.6

Cattle, fat 0.50

Cattle, meat 0.02

Cherimoya 0.60

Chive, fresh leaves 30

Citrus, oil 100

Corn, field, forage 15

Corn, field, grain 0.05

Corn, field, refined oil 0.20

Corn, field, stover 125

Corn, pop, grain 0.05

Corn, pop, stover 125

Corn, sweet, forage 30

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 60

Cotton, gin byproducts 35

Cotton, undelinted seed 2.0

Cranberry 0.5

Custard apple 0.60

Date 8.0

Feijoa 0.4

Fruit, citrus, group 10-10 3.0

Fruit, pome, group 11-10 2.0

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0

Fruit, stone, group 12-12, except plum, prune, fresh 3.0

Goat, fat 0.50

Goat, meat 0.02

Grain, aspirated grain fractions 120

Grape, raisin 1.5

Grass, forage, fodder and hay, group 17, forage 18.0

Grass, forage, fodder and hay, group 17, hay 30.0

Guava 0.4

Herb subgroup 19A, except chive, fresh leaves 400

Hog, fat 0.1

Hog, meat 0.02

Horse, fat 0.50

Horse, meat 0.02

Ilama 0.60

Jaboticaba 0.4

Leaf petioles subgroup 4B 25

Leafy greens subgroup 4A 30

Longan 2.0

Lychee 2.0

Mango 0.6

Milk 0.10

Nut, tree, group 14-12 0.10

Onion, green, subgroup 3-07B, except chive, fresh leaves 5.0

Papaya 0.6

Passionfruit 0.4

Pea and bean, dried shelled, except soybean, subgroup 6C, except pea, blackeyed, seed and pea, southern, seed 0.50

Pea and bean, succulent shelled, subgroup 6B 0.2

Pea, blackeyed, seed 4.0

Pea, southern, seed 4.0

Peanut 0.02

Peanut, hay 55.0

Peanut, oil 0.04

Peppermint, tops 7.0

Pineapple 0.70

Plum, prune, fresh 0.30

Pomegranate 0.6

Poultry, fat 0.02

Poultry, meat 0.02

Pulasan 2.0

Rambutan 2.0

Sapodilla 0.6

Sapote, black 0.6

Sapote, mamey 0.6

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Sheep, fat 0.50

Sheep, meat 0.02

Sorghum, grain, forage 15

Sorghum, grain, grain 6.0

Sorghum, grain, stover 20

Sorghum, sweet, forage 15

Sorghum, sweet, grain 6.0

Sorghum, sweet, stalk 15

Sorghum, sweet, stover 20

Soursop 0.60

Soybean, aspirated grain fractions 160

Soybean, forage 30

Soybean, hay 80

Soybean, hulls 2.0

Soybean, seed 1.0

Spanish lime 2.0

Spearmint, tops 7.0

Star apple 0.6

Starfruit 0.4

Sugar apple 0.60

Turnip, greens 30

Vegetable, cucurbit, group 9 0.3

Vegetable, foliage of legume, except soybean, subgroup 7A 35

Vegetable, fruiting, group 8-10 2.0

Vegetable, leaves of root and tuber, group 2 30

Vegetable, legume, edible podded, subgroup 6A 1.5

Vegetable, root, except sugar beet, Subgroup 1B 0.90

Vegetable, tuberous and corm, except potato, subgroup 1D 0.02

Wax jambu 0.4

(2) Tolerances are established for residues of the insecticide methoxyfenozide, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only the sum of methoxyfenozide [3-methoxy-2-methylbenzoic acid 

2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and its glucuronide metabolite (β-D-Glucopyranuronic acid, 

3-[[2-(1,1-dimethylethyl)-2-(3,5-dimethylbenzoyl)-hydrazino]carbonyl]-2-methylphenyl-), calculated as the stoichiometric 

equivalent of methoxyfenozide.

Commodity Parts per million

Cattle, liver 0.40

Cattle, meat byproducts, except liver 0.10

Egg 0.02

Goat, liver 0.40

Goat, meat byproducts, except liver 0.10

Hog, liver 0.1

Hog, meat byproducts, except liver 0.02

Horse, liver 0.40

Horse, meat byproducts, except liver 0.10

Poultry, liver 0.10

Poultry, meat byproducts, except liver 0.02

Sheep, liver 0.40

Sheep, meat byproducts, except liver 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent tolerances. (1) Tolerances are established for the indirect or inadvertent residues of the 

insecticide methoxyfenozide, including its metabolites and degradates, in or on the raw agricultural commodities in the 

following table, when present therein as a result of the application of methoxyfenozide to growing crops as listed in 

paragraph (a) of this section. Compliance with the tolerance levels specified in the following table is to be determined by 

measuring only methoxyfenozide [3-methoxy-2-methylbenzoic acid 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) 

hydrazide].

Commodity

Parts per

million

Onion, bulb, subgroup 3-07A 0.10

Potato 0.02

(2) Tolerances are established for the indirect or inadvertent residues of the insecticide methoxyfenozide, including its 

metabolites and degradates, in or on the raw agricultural commodities in the following table, when present therein as a 

result of the application of methoxyfenozide to growing crops as listed in paragraph (a) of this section. Compliance with the 

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tolerance levels specified in the following table is to be determined by measuring only the sum of methoxyfenozide 

[3-methoxy-2-methylbenzoic acid, 2-(3,5-dimethylbenzoyl)-2-(1,1-dimethylethyl) hydrazide] and the following metabolites 

(all calculated as the stoichiometric equivalent of methoxyfenozide): free phenol of methoxyfenozide [3,5-dimethylbenzoic 

acid N-tert-butyl-N′-(3-hydroxy-2-methylbenzoyl) hydrazide], the glucose conjugate of the phenol [3,5-dimethyl benzoic 

acid N-tert-butyl-N′-[3 (β-D-glucopyranosyloxy)-2-methylbenzoyl]-hydrazide] and the malonylglycosyl conjugate of the 

phenol [3,5-dimethyl benzoic acid N-tert-butyl-N′-[3 (β-D-6-malonyl-glucopyranosyl-1-oxy)-2-methylbenzoyl]-hydrazide].

Commodity

Parts per

million

Animal feed, nongrass, group 18, straw 8.0

Grain, cereal, forage, fodder and straw group 16, except corn 6.0

Rapeseed subgroup 20A 1.0

Spice subgroup 19B 4.5

Sunflower subgroup 20B 1.0

[67 FR 59203, Sept. 20, 2002, as amended at 68 FR 32389, May 30, 2003; 68 FR 37765, June 25, 2003; 69 FR 58097, Sept. 29, 

2004; 70 FR 7047, Feb. 10, 2005; 70 FR 51604, Aug. 31, 2005; 70 FR 75739, Dec. 21, 2005; 71 FR 32853, June 7, 2006; 73 FR 

11826, Mar. 5, 2008; 74 FR 22468, May 13, 2009; 74 FR 45335, Sept. 2, 2009; 76 FR 34886, June 15, 2011; 77 FR 40812, July 11, 

2012; 78 FR 60714, Oct. 2, 2013; 79 FR 51106, Aug. 27, 2014; 80 FR 65968, Oct. 28, 2015]

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§180.545 Prallethrin; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide prallethrin, including its metabolites and 

degradates, in or on all raw agricultural commodities and processed food from use of prallethrin in food handling 

establishments where food and food products are held, processed, prepared and/or served, or as a wide-area mosquito 

adulticide at 1.0 part per million (ppm). Compliance with the tolerance level specified is to be determined by measuring 

only prallethrin, 2-methyl-4-oxo-3-(2-propyn-1-yl)-2-cyclopenten-1-yl-2,2-dimethyl-3-(2-methyl-1-propen-1-yl)

cyclopropanecarboxylate.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 64330, Oct. 29, 2014]

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§180.546 Mefenoxam; tolerances for residues.

(a) General. Tolerances are established for residues of mefenoxam, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only metalaxyl (methyl N-(2,6-dimethylphenyl)-N-(methoxyacetyl)-DL-alaninate).

Commodity Parts per million

Artichoke, globe 0.05

Atemoya 0.20 

Bean, snap, succulent 0.20

Bushberry subgroup 13-07B 2.0

Caneberry subgroup 13-07A 0.70

Canistel 0.40

Custard apple 0.20

Herbs, dried 55 

Herbs, fresh 8.0 

Kiwifruit 0.10 

Mango 0.40

Onion, bulb, subgroup 3-07A 3.0

Onion, green, subgroup 3-07B 10

Papaya 0.40

Sapodilla 0.40

Sapote, black 0.40

Sapote, mamey 0.40

Spinach 10

Star apple 0.40

Starfruit 0.20

Sugar apple 0.20

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertant residues. [Reserved]

[65 FR 57556, Sept. 25, 2000, as amended at 66 FR 48003, Sept. 17, 2001; 67 FR 35050, May 17, 2002; 76 FR 4548, Jan. 26, 

2011]

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§180.547 Prohexadione calcium; tolerances for residues.

(a) General. Tolerances are established for residues of the growth regulator, prohexadione calcium, including its 

metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring only prohexadione calcium (calcium 3-oxido-5-oxo-4-propionylcyclohex-3-

enecarboxylate)” in or on the following commodities.

Commodity 

Parts per

million 

Cattle, kidney 0.10 

Cattle, meat byproducts, except kidney 0.05 

Cherry, sweet 0.40

Fruit, pome, group 11 3.0 

Goat, kidney 0.10 

Goat, meat byproducts, except kidney 0.05 

Grass, forage1 0.10

Grass, hay1 0.10

Grass, seed screenings1 3.5 

Grass, straw1 1.2

Hog, kidney 0.10 

Hog, meat byproducts, except kidney 0.05 

Horse, kidney 0.10 

Horse, meat byproducts, except kidney 0.05 

Peanut 1.0 

Peanut, hay 0.60 

Sheep, kidney 0.10 

Sheep, meat byproducts, except kidney 0.05 

Strawberry 0.30

Watercress 4.0

1

Registration is limited to grass grown for seed.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 25660, May 3, 2000, as amended at 66 FR 29712, June 1, 2001; 76 FR 71464, Nov. 18, 2011; 80 FR 38980, July 8, 2015]

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§180.548 Tralkoxydim; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, tralkoxydim, 2-Cyclohexen-1-one, 

2-[1-(ethoxyimino)propyl]-3-hydroxy-5-(2,4,6-trimethylphenyl)-(9Cl) in or on the raw agricultural commodities:

Commodity Parts per million

Barley, grain 0.02

Barley, hay 0.02

Barley, straw 0.05

Wheat, forage 0.05

Wheat, grain 0.02

Wheat, hay 0.02

Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[63 FR 69199, Dec. 16, 1998, as amended at 68 FR 48302, Aug. 13, 2003; 70 FR 70739, Nov. 23, 2005]

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§180.549 Diflufenzopyr; tolerances for residues.

(a) General. Tolerances are established for combined residues of diflufenzopyr, 2-(1-[([3,5-difluorophenylamino] 

carbonyl)hydrazono]ethyl)-3- pyridinecarboxylic acid, and its metabolites convertible to 8- methylpyrido[2,3-d]pyridazin-5

(6H)-one, expressed as diflufenzopyr, in or on the following raw agricultural commodities:

Commodity Parts per million

Corn, field, forage 0.05

Corn, field, grain 0.05

Corn, field, stover 0.05

Corn, pop, grain 0.05

Corn, pop, stover 0.05

Corn, sweet, forage 0.05

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 0.05

Grass, forage 22.0

Grass, hay 7.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 4308, Jan. 28, 1999, as amended at 67 FR 55338, Aug. 29, 2002; 76 FR 34886, June 15, 2011]

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§180.551 Fluthiacet-methyl; tolerances for residues.

(a) General. (1) A tolerance is established for residues of the herbicide, fluthiacet-methyl, acetic acid [[2-chloro-4-

fluoro-5-[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]-methyl ester, in or on the 

food commodity:

Commodity Parts per million

Corn, field, forage 0.050

Corn, field, grain 0.010

Corn, field, stover 0.050

Corn, pop, grain 0.010

Corn, pop, stover 0.050

Corn, sweet, forage 0.050

Corn, sweet, kernel plus cob with husks removed 0.010

Corn, sweet, stover 0.050

Soybean, seed 0.01

(2) A tolerance is established for the combined residues of the herbicide fluthiacet-methyland its acid metabolite: 

acetic acid, [[2-chloro-4-fluoro-5-[tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]pyridazin-1-ylidene)amino]phenyl]thio]

-methyl ester, and its acid metabolite, acetic acid, [[2-chloro-4-fluoro-5-[(tetrahydro-3-oxo-1H,3H-[1,3,4]thiadiazolo[3,4-α]

pyridazin-1-ylidene)amino]phenyl]thio]- , in or on the following food commodities:

Commodity Parts per million

Cotton, gin byproducts 0.20

Cotton, undelinted seed 0.020

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 18357, Apr. 14, 1999, as amended at 66 FR 65850, Dec. 21, 2001; 71 FR 77625, Dec. 27, 2006]

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§180.552 Sulfosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide sulfosulfuron, 1-(4,6-dimethoxypyrimidin-2-yl)-3-

[(2-ethanesulfonyl-imidazo[1,2-a]pyridine-3-yl) sulfonyl]urea and its metabolites converted to 2-(ethylsulfonyl)-imidazo

[1,2-a]pyridine and calculated as sulfosulfuron in or on the raw agricultural commodities.

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Commodity Parts per million

Cattle, fat 0.02

Cattle, meat 0.01

Cattle, meat byproducts 0.3

Goat, fat 0.02

Goat, meat 0.01

Goat, meat byproducts 0.3

Grass, forage, fodder and hay, group 17, forage 14

Grass, forage, fodder and hay, group 17, hay 25

Hog, fat 0.005

Hog, meat 0.005

Hog, meat byproducts 0.05

Horse, fat 0.02

Horse, meat 0.01

Horse, meat byproducts 0.3

Milk 0.02

Sheep, fat 0.02

Sheep, meat 0.01

Sheep, meat byproducts 0.3

Wheat, forage 4.0

Wheat, grain 0.02

Wheat, hay 0.3

Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 27192, May 19, 1999, as amended at 70 FR 69464, Nov. 16, 2005; 72 FR 54574, Sept. 26, 2007]

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§180.553 Fenhexamid; tolerances for residues.

(a) General. Tolerances are established for the residues of the fungicide fenhexamid (N-2,3-dichloro-4-

hydroxyphenyl)-1-methyl cyclohexanecarboxamide) in or on the following commodities:

Commodity Parts per million

Almond, hulls 2.0

Almond 0.02

Asparagus 0.02

Bushberry subgroup 13B 5.0

Caneberry subgroup 13A 20.0

Cilantro, leaves 30.0

Cucumber 2.0

Fruit, stone, group 12, except plum, prune, fresh, postharvest 10.0

Ginseng 0.3

Grape 4.0

Grape, raisin 6.0

Juneberry 5.0 

Kiwifruit, postharvest 15.0

Leafy greens subgroup 4A, except spinach 30.0

Lingonberry 5.0 

Pear 10

Pepper, nonbell 0.02

Pistachio 0.02 

Plum, prune, dried 2.5

Plum, prune, fresh 1.5

Pomegranate 2.0

Salal 5.0 

Strawberry 3.0

Vegetable, fruiting, group 8, except nonbell pepper 2.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

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[64 FR 28924, May 28, 1999, as amended at 65 FR 19849, Apr. 13, 2000; 65 FR 69883, Nov. 21, 2000; 67 FR 19120, Apr. 18, 

2002; 68 FR 2247, Jan. 16, 2003; 68 FR 55519, Sept. 26, 2003; 71 FR 15617, Mar. 29, 2006; 71 FR 43664, Aug. 2, 2006; 73 FR 

19154, Apr. 9, 2008]

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§180.554 Kresoxim-methyl; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of the fungicide kresoxim-methyl (methyl (E)

-2-[2-(2-methylphenoxy)-methyl]phenyl-2-(methoxyimido)acetate) and its metabolites as follows: (E)

-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid; (E)-2-[2-(2-hydroxymethylphenoxy)methyl]-phenyl2-(methoxyimido)acetic acid (free and glucose conjugated); and (E)-2-[2-(4-hydroxy-2-methylphenoxy)-methyl]phenyl2-(methoxyimido)acetic acid (free and glucose conjugated) in or on the following commodities:

Commodity Parts per million

Apple, dry pomace 1.0

Apple, wet pomace 1.0

Fruit, pome 0.5

Grape 1.0

Grape, raisin 1.5

Pecan 0.15

Vegetable, cucurbit, group 9 0.40

(2) Tolerances are established in or on the following commodities for the residues of the metabolite (E)

-2-[2-(2-methylphenoxy)methyl]-phenyl-2-(methoxyimido)acetic acid resulting from the use of the fungicide kresoximmethyl:

Commodity Parts per million

Cattle, meat byproducts 0.01

Goat, meat byproducts 0.01

Sheep, meat byproducts 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[64 FR 31136, June 10, 1999, as amended at 71 FR 50359, Aug. 25, 2006; 74 FR 46377, Sept. 9, 2009]

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§180.555 Trifloxystrobin; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of trifloxystrobin, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of trifloxystrobin, benzeneacetic acid, (E,E)-α-(methoxyimino)-2-[[[[1-[3-(trifluoromethyl) phenyl]

ethylidene] amino]oxy]methyl]-, methyl ester, and the free form of its acid metabolite CGA-321113, (E,E)

-methoxyimino-[2-[1-(3-trifluoromethyl-phenyl)-ethylideneaminooxymethyl]-phenyl]acetic acid, calculated as the 

stoichiometric equivalent of trifloxystrobin, in or on the commodity.

Commodity Parts per million

Alfalfa, forage 0.01

Alfalfa, hay 0.01

Almond, hulls 9.0

Apple, wet pomace 5.0

Artichoke, globe 1.0

Asparagus 0.07

Banana1 0.10

Barley, grain 0.05

Barley, hay 0.3

Barley, straw 5.0

Beet, sugar, dried pulp 0.4 

Beet, sugar, molasses 0.2 

Beet, sugar, roots 0.1 

Beet, sugar, tops 4.0 

Canistel 0.7

Cattle, fat 0.1 

Cattle, meat 0.1 

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Cattle, meat byproducts 0.1 

Citrus, dried pulp 1.0

Citrus, oil 38

Coffee, green bean2 0.02

Corn, field, forage 6.0 

Corn, field, grain 0.05

Corn, field, stover 7

Corn, field, refined oil 0.1

Corn, pop, grain 0.05

Corn, pop, stover 7

Corn, sweet, cannery waste 0.6

Corn, sweet, forage 7.0 

Corn, sweet, kernel plus cob with husks removed 0.04

Corn, sweet, stover 4.0 

Egg 0.04

Fruit, citrus, group 10 0.6

Fruit, pome 0.5

Fruit, stone, group 12 2

Goat, fat 0.1 

Goat, meat 0.1 

Goat, meat byproducts 0.1 

Grain, aspirated fractions 5.0

Grape 2.0

Grape, raisin 5.0

Grass, forage 12

Grass, hay 17

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Hop, dried cones 11.0

Horse, fat 0.1 

Horse, meat 0.1 

Horse, meat byproducts 0.1 

Leaf petioles subgroup 4B 3.5

Mango 0.7

Milk 0.02

Nut, tree, group 14 0.04

Oat, forage 0.3

Oat, grain 0.05

Oat, hay 0.3

Oat, straw 5.0

Papaya 0.7

Pea, dry, seed 0.06

Pea, field, hay 15

Pea, field, vines 4

Peanut, hay 4.0

Peanut 0.05

Pistachio 0.04

Potato 0.04

Poultry, fat 0.04

Poultry, meat 0.04

Poultry, meat byproducts 0.04

Radish, tops 10

Rice, grain 3.5

Rice, hulls 8

Rice, straw 7.5

Sapodilla 0.7

Sapote, black 0.7

Sapote, mamey 0.7

Sheep, fat 0.1 

Sheep, meat 0.1 

Sheep, meat byproducts 0.1 

Soybean, forage 10.0

Soybean, hay 25.0

Soybean, seed 0.08

Star apple 0.7

Strawberry 1.1

Vegetable, cucurbit, group 9 0.50

Vegetable, fruiting 0.5

Vegetable, root, except sugar beet, subgroup 1B 0.1

Wheat, bran 0.15 

Wheat, forage 0.3 

Wheat, grain 0.05 

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Wheat, hay 0.2 

Wheat, straw 5.0

1

 There are no U.S. registrations as of September 27, 1999 for use on banana.

2

There are no U.S. registrations as of January 18, 2012 for use on coffee, green bean.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved] 

[64 FR 51907, Sept. 27, 1999]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.555, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.556 Pymetrozine; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide pymetrozine 1,2,4-triazin-3(2H)

-one,4,5-dihydro-6-methyl-4-[(3-pyridinylmethylene) amino] in or on the following raw agricultural commodities. The 

tolerance level for each commodity is expressed in terms of the parent insecticide only, which serves as an indicator of the 

use of pymetrozine on these raw agricultural commodities. 

Commodity Parts per million

Asparagus 0.04

Brassica, head and stem, subgroup 5A 0.5

Brassica, leafy greens, subgroup 5B 0.25

Cotton, gin byproducts 2.0

Cotton, undelinted seed 0.3

Hop, dried cones 6.0

Pecan 0.02

Turnip, greens 0.25

Vegetable, fruiting, group 8 0.2

Vegetable, cucurbit, group 9 0.1

Vegetable, leafy, execpt brassica, group 4 0.6

Vegetable, tuberous and corm, subgroup 1C 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 48634, Aug. 9, 2000, as amended at 66 FR 14846, Mar. 14, 2001; 66 FR 66794, Dec. 27, 2001; 70 FR 7047, Feb. 10, 2005; 

70 FR 43298, July 27, 2005]

 Back to Top

§180.557 Tetraconazole; tolerances for residues.

(a) General. Tolerances are established for residues of tetraconazole, including its metabolites and degradates, in or 

on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only 

tetraconazole (1-[2-(2,4-dichlorophenyl)-3-(1,1,2,2-tetrafluoroethoxy)propyl]-1H-1,2,4-triazole), in or on the following 

commodities.

Commodity Parts per million

Aspirated grain fractions 1.0

Beet sugar, dried pulp 0.15

Beet sugar, molasses 0.15

Beet sugar, root 0.05

Cattle, fat 0.15

Cattle, liver 1.50

Cattle, meat 0.01

Cattle, meat byproducts (except liver) 0.15

Corn, field, forage 1.1

Corn, field, grain 0.01

Corn, field, stover 1.7

Corn, pop, grain 0.01

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Corn, pop, stover 1.7

Eggs 0.02

Goat, fat 0.15

Goat, liver 1.50

Goat, meat 0.01

Goat, meat byproducts (except liver) 0.15

Hog, fat 0.01

Hog, liver 0.05

Hog, meat 0.01

Hog, meat byproducts (except liver) 0.01

Horse, fat 0.15

Horse, liver 1.50

Horse, meat 0.01

Horse, meat byproducts (except liver) 0.15

Low growing berry subgroup 13-07G, except cranberry 0.25

Milk 0.03

Milk, fat 0.75

Peanut 0.03

Peanut, oil 0.10

Pecan 0.04

Poultry, fat 0.05

Poultry, meat 0.01

Poultry meat byproducts 0.05

Sheep, fat 0.15

Sheep, liver 1.50

Sheep, meat 0.01

Sheep, meat byproducts (except liver) 0.15

Small fruit vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.20

Soybean, refined oil 0.80

Soybean, seed 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 20830, Apr. 22, 2005, as amended at 70 FR 31359, June 1, 2005; 72 FR 18134, Apr. 11, 2007; 73 FR 67406, Nov. 14, 2008; 

76 FR 53648, Aug. 29, 2011]

 Back to Top

§180.559 Clodinafop-propargyl; tolerances for residues.

(a) General. Tolerances are established for clodinafop-propargyl, including its metabolites and degradates, in or on 

the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only clodinafop-propargyl [(2R)-2-[4-[(5-chloro-3-fluoro-2-pyridinyl)oxy]phenoxy]propanoic acid, 

2-propynyl ester] and its metabolite clodinafop [(2R)-2-[4-[(5-chloro-3-fluoro-2- pyridinyl)oxy]phenoxy]propanoic acid].

Commodity Parts per million 

Wheat, forage 0.1 

Wheat, grain 0.02 

Wheat, hay 0.1 

Wheat, straw 0.5

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 38774, June 22, 2000, as amended at 77 FR 72226, Dec. 5, 2012]

 Back to Top

§180.560 Cloquintocet-mexyl; tolerances for residues.

(a) General. Tolerances are established for the combined residues of cloquintocet-mexyl, (acetic acid [(5-chloro-8-

quinolinyl)oxy]-,1-methylhexyl ester; CAS Reg. No. 99607-70-2) and its acid metabolite (5-chloro-8-quinolinoxyacetic 

acid), when used as an inert ingredient (safener) in pesticide formulations containing the active ingredients clodinafoppropargyl (wheat only), dicamba (wheat only), flucarbazone-sodium (wheat only), pinoxaden (wheat or barley), or 

pyroxsulum (wheat only) in or on the following food commodities:

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Commodity Parts per million

Barley, grain 0.1

Barley, hay 0.1

Barley, straw 0.1

Wheat, forage 0.2

Wheat, grain 0.1

Wheat, hay 0.5

Wheat, straw 0.1

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved] 

[65 FR 38764, June 22, 2000, as amended at 70 FR 74688, Dec. 16, 2005; 73 FR 11820, Mar. 5, 2008; 75 FR 16020, Mar. 31, 

2010; 76 FR 38035, June 29, 2011]

 Back to Top

§180.561 Acibenzolar-S-methyl; tolerances for residues.

(a) General. (1) Tolerances are established for residues of acibenzolar-S-methyl, benzo(1,2,3)thiadiazole-7-

carbothioic acid-S-methyl ester, including its metabolites and degradates, in or on the commodities in the table below. 

Compliance with the tolerance levels specified below is to be determined by measuring only those acibenzolar-S-methyl 

residues convertible to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007), expressed as the stoichiometric 

equivalent of acibenzolar-S-methyl, in or on the following raw agricultural commodities.

Commodity Parts per million

Banana1 0.1

Berry, low growing, subgroup 13-07G 0.15

Fruit, citrus, group 10-10 0.02

Fruit, pome, group 11-10 0.03

Onion, bulb, subgroup 3-07A 0.1

Spinach 1.0

Tomato, paste 3.0

Vegetable, brassica, leafy, group 5 1.0

Vegetable, cucurbit, group 9 2.0

Vegetable, fruiting, group 8 1.0

Vegetable, leafy, group 4 0.25

1

There are no United States registrations for banana.

(2) Tolerances are established for residues of acibenzolar- S -methyl, benzo(1,2,3)thiadiazole-7-carbothioic acid- S

-methyl ester, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the 

tolerance levels specified below is to be determined by measuring only those acibenzolar- S -methyl residues convertible 

to benzo(1,2,3)thiadiazole-7-carboxylic acid (CGA-210007), expressed as the Stoichiometric equivalent of acibenzolar- S

-methyl, in or on the following raw agricultural commodities.

Commodity Parts per million Expiration/revocation date

Apple 0.05 12/31/15

Grapefruit 0.05 12/31/15

Pear 0.05 12/31/15

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 50446, Aug. 18, 2000, as amended at 70 FR 7861, Feb. 16, 2005; 71 FR 76200, Dec. 20, 2006; 74 FR 24710, May 26, 2009; 

76 FR 34886, June 15, 2011; 77 FR 21676, Apr. 11, 2012; 77 FR 30406, May 23, 2012; 80 FR 58620, Sept. 30, 2015]

 Back to Top

§180.562 Flucarbazone-sodium; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide flucarbazone-sodium, 4,5-dihydro-3-

methoxy-4-methyl-5-oxo-N-[[2(trifluoromethoxy)phenyl] sulfonyl]-1H-1,2,4-triazole 1-carboxamide, sodium salt) and its 

N-desmethyl metabolite; and its metabolites converted to 2-(trifluoromethoxy)benzene sulfonamide and calculated as 

flucarbazone-sodium in or on the following food commodities:

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Commodity Parts per million

Cattle, liver 1.50

Cattle, meat 0.01

Cattle, meat byproducts, except liver 0.01

Goat, liver 1.50

Goat, meat 0.01

Goat, meat byproducts, except liver 0.01

Hog, liver 1.50

Hog, meat 0.01

Hog, meat byproducts, except liver 0.01

Horse, liver 1.50

Horse, meat 0.01

Horse, meat byproducts, except liver 0.01

Milk 0.005

Sheep, liver 1.50

Sheep, meat 0.01

Sheep, meat byproducts, except liver 0.01

Wheat, forage 0.30

Wheat, grain 0.01

Wheat, hay 0.10

Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[70 FR 67915, Nov. 9, 2005, as amended at 71 FR 76931, Dec. 22, 2006]

 Back to Top

§180.563 Ethametsulfuron-methyl; tolerances for residues.

(a) General. A tolerance is established for residues of ethametsulfuron methyl (methyl 2- ((((4-ethoxy-6- 

(methylamino)-1,3,5- triazin-2-yl) amino) carbonyl) amino) sulfonyl) benzoate) in or on the following raw agricultural 

commodities.

Commodity Parts per million

Canola, seed 0.02

Crambe, seed 0.02

Rapeseed, seed 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect of inadvertent residues. [Reserved]

[65 FR 57972, Sept. 27, 2000, as amended at 66 FR 18207, Apr. 6, 2001; 67 FR 35050, May 17, 2002]

 Back to Top

§180.564 Indoxacarb; tolerances for residues.

(a) General. (1) Tolerances are established for residues of indoxacarb, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only indoxacarb, (S)-methyl 7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]

carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate, and its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2-

[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]indeno[1,2-e][1,3,4][oxadiazine-4a(3H)-carboxylate.

Commodity Parts per million

Apple, wet pomace 3.0

Alfalfa, forage 10

Alfalfa, hay 50

Bean, dry, seed 0.2

Bean, succulent 0.9

Beet, garden, roots 0.30

Beet, garden, tops 6.0

Berry, low growing, except strawberry, subgroup 13-07H 1

Bushberry subgroup 13-07B 1.5

Cattle, fat 1.5

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Cattle, meat 0.05

Cattle, meat byproducts 0.03

Corn, sweet, forage 10

Corn, sweet, kernel plus cob with husk removed 0.02

Corn, sweet, stover 15

Cotton, gin byproducts 15

Cotton, undelinted seed 2.0

Cowpea, forage 50

Cowpea, hay 100

Fruit, pome, except pear, group 11 1.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2

Fruit, stone, group 12 0.90

Goat, fat 1.5

Goat, meat 0.05

Goat, meat byproducts 0.03

Grain, aspirated fractions 45

Grape, raisin 5.0

Hog, fat 1.5

Hog, meat 0.05

Hog, meat byproducts 0.03

Horse, fat 1.5

Horse, meat 0.05

Horse, meat byproducts 0.03

Milk 0.15

Milk, fat 4.0

Okra 0.50

Pea, southern, seed 0.10

Peanut 0.01

Peanut, hay 40

Pear 0.20

Pear, oriental 0.20

Peppermint, tops 11

Sheep, fat 1.5

Sheep, meat 0.05

Sheep, meat byproducts 0.03

Soybean, hulls 4.0

Soybean, seed 0.80

Spearmint, tops 11

Turnip, greens 12

Vegetable, Brassica, leafy, group 5 12

Vegetable, cucurbit, group 9 0.60

Vegetable, fruiting, group 8 0.50

Vegetable, leafy, except Brassica, group 4 14

Vegetable, tuberous and corm, subgroup 1-C 0.01

(2) Tolerances are established for residues of indoxacarb, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of indoxacarb, (S)-methyl-7-chloro-2,5-dihydro-2-[[(methoxycarbonyl)[4-(trifluoromethoxy)-phenyl]amino]

carbonyl]indeno[1,2e] [1,3,4]oxadiazine-4a(3H)-carboxylate, its R-enantiomer, (R)-methyl 7-chloro-2,5-dihydro-2-

[[(methoxycarbonyl)[4-(trifluoromethoxy) phenyl]amino]carbonyl]indeno [1,2-e] [1,3,4] oxadiazine-4a(3H)-carboxylate, and 

the metabolites: IN-JT333, methyl 7-chloro-2,5-dihydro-2-[[[4-(trifluoromethoxy)phenyl]-amino]carbonyl]indeno[1,2-e][1,3,4]

oxadiazine-4a(3H)-carboxylate; IN-KT319, (E)-methyl 5-chloro-2,3,-dihydro-2-hydroxy-1-[[[(methoxycarbonyl)

[4-(trifluoromethoxy)phenyl]amino]-carbonyl]hydrazono]-1H-indene-2-carboxylate; IN-JU873, methyl 5-chloro-2,3-dihydro2-hydroxy-1-[[[[4-(triflurormethoxy)-phenyl]amino]carbonyl]hydrazono]-1H-indene-2-carboxylate; IN-KG433, methyl 

5-chloro-2,3,-dihydro-2-hydroxy-1-[[[(methoxycarbonyl)[4-(trifluoromethoxy)phenyl]amino]carbonyl]-hydrazono]-1H-indene2-carboxylate; and IN-KB687, methyl [4-(trifluoromethoxy)phenyl]carbamate, calculated as the stoichiometric equivalent of 

indoxacarb in the commodity.

Commodity Parts per million

Egg 0.20

Poultry, fat 0.20

Poultry, meat 0.06

Poultry, meat byproducts 0.06

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 58424, Sept. 29, 2000, as amended at 67 FR 41807, June 19, 2002; 67 FR 47309, July 18, 2002; 67 FR 58730, Sept. 18, 

2002; 68 FR 25830, May 14, 2003; 68 FR 27746, May 21, 2003; 69 FR 28842, May 19, 2004; 69 FR 29459, May 24, 2004; 69 FR 

32282, June 9, 2004; 72 FR 37641, July 11, 2007; 74 FR 33165, July 10, 2009; 77 FR 8749, Feb. 15, 2012; 78 FR 78738, Dec. 27, 

2013] 

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§180.565 Thiamethoxam; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide thiamethoxam, including its metabolites and 

degradates, in or on the following commodities. Compliance with the tolerance levels specified below is to be determined 

by measuring only thiamethoxam 3-[(2-chloro-5-thiazolyl)methyl]tetrahydro-5-methyl-N-nitro-4H-1,3,5-oxadiazin-4-imine 

and its metabolite CGA-322704 N-[(2-chloro-thiazol-5-yl)methyl]-N′-methyl-N′′-nitro-guanidine, calculated as the 

stoichiometric equivalent of thiamethoxam, in or on the following commodities:

Commodity

Parts 

per

million

Alfalfa, forage 0.05

Alfalfa, hay 0.12

Almond, hulls 1.2

Artichoke, globe 0.45

Avocado 0.40

Barley, grain 0.4

Barley, hay 0.40

Barley, straw 0.40

Bean, succulent 0.02

Berry, low growing, subgroup 13-07G, except cranberry 0.30

Borage, seed 0.02

Brassica, head and stem, subgroup 5-A 4.5

Brassica, leafy greens, subgroup 5-B 3.0

Buckwheat, forage 0.50

Buckwheat, hay 0.02

Buckwheat, straw 0.02

Bushberry subgroup 13-07B, except lingonberry and blueberry, lowbush 0.20

Caneberry subgroup 13-07A 0.35

Canistel 0.40

Canola, seed 0.02

Cattle, meat 0.02

Cattle, meat byproducts 0.04

Citrus, dried pulp 0.60

Coffee, green, bean1 0.20

Corn, field, forage 0.10

Corn, field, stover 0.05

Corn, pop, forage 0.10

Corn, pop, stover 0.05

Corn, sweet, forage 0.10

Corn, sweet, kernel plus cob with husks removed 0.02

Corn, sweet, stover 0.05

Cotton, gin byproducts 1.5

Cotton, undelinted seed 0.10

Crambe, seed 0.02

Cranberry 0.02

Flax, seed 0.02

Food commodities and feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food/feed handling 

establishments

0.02

Fruit, citrus, group 10 0.40

Fruit, pome, group 11 0.2

Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwifruit 0.20

Fruit, stone, group 12 0.5

Goat, meat 0.02

Goat, meat byproducts 0.04

Grain, aspirated fractions 2.0

Grain, cereal, group 15, except barley 0.02

Grape, raisin 0.30

Hog, meat 0.02

Hog, meat byproducts 0.02

Hop, dried cones 0.10

Horse, meat 0.02

Horse, meat byproducts 0.04

Mango 0.40

Milk 0.02

Millet, pearl, forage 0.02

Millet, pearl, stover 0.02

Millet, proso, forage 0.02

Millet, proso, stover 0.02

Millet, proso, straw 0.02

Mustard, seed 0.02

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Nut, tree, group 14 0.02

Oat, forage 0.50

Oat, hay 0.02

Oat, straw 0.02

Onion, dry bulb 0.03

Papaya 0.40

Peanut 0.05

Peanut, hay 0.25

Peanut, meal 0.15

Peppermint, tops 1.5

Pistachio 0.02

Potato 0.25

Radish, tops 0.80

Rapeseed, seed 0.02

Rye, forage 0.50

Rye, straw 0.02

Safflower, seed 0.02

Sapodilla 0.40

Sapote, black 0.40

Sapote, mamey 0.40

Sheep, meat 0.02

Sheep, meat byproducts 0.04

Sorghum, forage 0.02

Sorghum, grain, stover 0.02

Soybean, hulls 0.08

Spearmint, tops 1.5

Star apple 0.40

Sunflower 0.02

Tea, dried1 20

Tomato, paste 0.80

Vegetable, cucurbit, group 9 0.2

Vegetable, fruiting, group 8 0.25

Vegetable, leafy, except brassica, group 4 4.0

Vegetable, legume, group 6 0.02

Vegetable, root, subgroup 1A 0.05

Vegetable, tuberous and corm, except potato, subgroup 1D 0.02

Wheat, forage 0.50

Wheat, hay 0.02

Wheat, straw 0.02

1

There are no U.S. registrations as of March 27, 2013.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[65 FR 79762, Dec. 20, 2000]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.565, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.566 Fenpyroximate; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to 

be determined by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate and its Z-isomer, (Z)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-

phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as the stoichiometric equivalent of 

fenpyroximate.

Commodity Parts per million

Almond, hulls 3.0

Avocado 0.15

Bean, snap, succulent 0.40

Berry, low growing, subgroup 13-07G 1.0

Canistel 0.15

Citrus, dried pulp 2.5

Citrus, oil 10

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Corn, field, forage 2.0

Corn, field, grain 0.02

Corn, field, refined oil 0.05

Corn, field, stover 7.0

Corn, pop, forage 2.0

Corn, pop, grain 0.02

Corn, pop, stover 7.0

Cotton, gin byproducts 10

Cotton, undelinted seed 0.10

Cucumber 0.40

Fruit, citrus, group 10-10 0.50

Fruit, pome, group 11-10 0.30

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0

Fruit, stone, group 12-12 2.0

Grain, aspirated fractions 0.40

Hop, dried cones 10

Mango 0.15

Melon subgroup 9A 0.10

Nut, tree, group 14 0.10

Papaya 0.15

Peppermint, tops 7.0

Pistachio 0.10

Sapodilla 0.15

Sapote, black 0.15

Sapote, mamey 0.15

Spearmint, tops 7.0

Star, apple 0.15

Tea, dried1 20

Vegetable, fruiting, group 8-10 0.20

Vegetable, tuberous and corm, subgroup 1C 0.10

1

There are no U.S. Registrations.

(2) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined 

by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)

methylene]amino]oxy]methyl]benzoate and its metabolites (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)

-methyleneaminooxymethyl]benzoic acid and (E)-1,1-dimethylethyl-2-hydroxyethyl 4-[[[[(1,3-dimethyl-5-phenoxy1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as the stoichiometric equivalent of fenpyroximate.

Commodity Parts per million

Cattle, fat 0.03

Cattle, meat 0.03

Cattle, meat byproducts, except kidney and liver 0.03

Goat, fat 0.03

Goat, meat 0.03

Goat, meat byproducts, except kidney and liver 0.03

Horse, fat 0.03

Horse, meat 0.03

Horse, meat byproducts, except kidney and liver 0.03

Milk 0.015

Sheep, fat 0.03

Sheep, meat 0.03

Sheep, meat byproducts, except kidney and liver 0.03

(3) Tolerances are established for residues of the insecticide fenpyroximate, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined 

by measuring only the sum of fenpyroximate, (E)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)

methylene]amino]oxy]methyl]benzoate and its metabolite (E)-4-[(1,3-dimethyl-5-phenoxypyrazol-4-yl)

-methyleneaminooxymethyl]benzoic acid, calculated as the stoichiometric equivalent of fenpyroximate.

Commodity Parts per million

Cattle, kidney 0.25

Cattle, liver 0.25

Goat, kidney 0.25

Goat, liver 0.25

Horse, kidney 0.25

Horse, liver 0.25

Sheep, kidney 0.25

Sheep, liver 0.25

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(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the insecticide 

fenpyroximate, including its metabolites and degradates in or on the commodities in the table below. Compliance with the 

tolerance levels specified in the table is to be determined by measuring only the sum of fenpyroximate, (E)

-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl) methylene]amino]oxy]methyl]benzoate and its Z-isomer, 

(Z)-1,1-dimethylethyl 4-[[[[(1,3-dimethyl-5-phenoxy-1H-pyrazol-4-yl)methylene]amino]oxy]methyl]benzoate, calculated as 

the stoichiometric equivalent of fenpyroximate.

Commodity Parts per million Expiration/revocation date

Honey 0.10 12/31/13

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 18568, Apr. 10, 2001, as amended at 69 FR 32464, June 10, 2004; 71 FR 49368, Aug. 23, 2006; 72 FR 26321, May 9, 2007; 

74 FR 37617, July 29, 2009; 74 FR 63079, Dec. 2, 2009; 75 FR 80346, Dec. 22, 2010; 77 FR 73951, Dec. 12, 2012; 78 FR 36097, 

June 17, 2013]

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§180.567 Zoxamide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of zoxamide including metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide).

Commodity Parts per million

Grape 3.0

Grape, raisin 15.0

Tomato 2.0

Vegetable, cucurbit, group 9 1.0

(2) Tolerances are established for residues of zoxamide including metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of zoxamide (3,5-dichloro-N-(3-chloro-1-ethyl-1-methyl-2-oxopropyl)-4-methylbenzamide) and its metabolites 

3,5-dichloro-1,4-benzenedicarboxylic acid (RH-1455 and RH-141455) and 3,5-dichloro-4-hydroxymethylbenzoic acid (RH1452 and RH-141452) calculated as the stoichiometric equivalent of zoxamide.

Commodity Parts per million

Onion, bulb, subgroup 3-07A 0.7

Potato 0.060

Potato, granules/flakes 0.30

Potato, wet peel 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 18733, Apr. 11, 2001, as amended at 66 FR 49118, Sept. 26, 2001; 69 FR 16805, Mar. 31, 2004; 71 FR 31104, June 1, 

2006; 71 FR 76200, Dec. 20, 2006; 75 FR 770, Jan. 6, 2010; 79 FR 41915, July 18, 2014]

 Back to Top

§180.568 Flumioxazin; tolerances for residues.

(a) General. Tolerances are established for residues of flumioxazin, 2-[7-fluoro-3,4-dihydro-3-oxo-4-(2-propynyl)

-2H-1,4-benzoxazin-6-yl]-4,5,6,7-tetrahydro-1H-isoindole-1,3(2H)-dione, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only flumioxazin.

Commodity Parts per million

Alfalfa, forage 3.0

Alfalfa, hay 8.0

Almond, hulls 0.70

Artichoke, globe 0.02

Asparagus 0.02

Bushberry subgroup 13-07B 0.02

Cabbage 0.02

Cabbage, Chinese, napa 0.02

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Corn, field, forage 0.02

Corn, field, grain 0.02

Corn, field, stover 0.02

Cotton, gin byproducts 0.60

Cotton, undelinted seed 0.02

Fish, freshwater 1.5

Fruit, pome, group 11 0.02

Fruit, stone, group 12 0.02

Garlic 0.02

Grain, aspirated fractions 100

Grape 0.02

Hop, dried cones 0.05

Leaf petioles subgroup 4B 0.02

Nut, tree, group 14 0.02

Okra 0.02

Olive 0.02

Onion, bulb 0.02

Pea and bean, dried shelled, except soybean, subgroup 6C 0.07

Peanut 0.02

Peppermint, tops 0.04

Pistachio 0.02

Pomegranate 0.02

Prickly pear, fruit 0.07

Prickly pear, pads 0.06

Rapeseed subgroup 20A 0.40

Shallot, bulb 0.02

Soybean, seed 0.02

Spearmint, tops 0.04

Strawberry 0.07

Sugarcane, cane 0.20

Sunflower subgroup 20B 0.50

Vegetable, cucurbit, group 9 0.03

Vegetable, fruiting, group 8 0.02

Vegetable, tuberous and corm, subgroup 1C 0.02

Wheat, forage 0.02

Wheat, grain 0.40

Wheat, hay 0.02

Wheat, straw 6.0 

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 19878, Apr. 18, 2001, as amended at 68 FR 51471, Aug. 27, 2003; 69 FR 16831, Mar. 31, 2004; 69 FR 52198, Aug. 25, 

2004; 71 FR 25956, May 3, 2006; 71 FR 61413, Oct. 18, 2006; 73 FR 11831, Mar. 5, 2008; 73 FR 39251, July 9, 2008; 75 FR 8265, 

Feb. 24, 2010; 75 FR 69009, Nov. 10, 2010; 77 FR 58499, Sept. 21, 2012; 78 FR 20466, Apr. 5, 2013] 

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§180.569 Forchlorfenuron; tolerances for residues.

(a) General. (1) Tolerances are established for residues of forchlorfenuron, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only forchlorfenuron (N-(2-chloro-4-pyridinyl)-N-phenylurea).

Commodity

Parts per

million

Almond 0.01

Almond, hulls 0.15

Bushberry subgroup 13-07B 0.01

Cherry, sweet 0.01

Fig 0.01

Grape 0.03

Grape, raisin 0.06

Kiwifruit 0.04

Pear 0.01

Pistachio 0.01

Plum, prune, fresh 0.01

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(2) Temporary tolerances are established for residues of forchlorfenuron, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring on forchlorfenuron (N-(2-chloro-4-pyridinyl)-N′-phenylurea).

Commodity

Parts per

million

Expiration/

revocation

date

Almond 0.01 12/31/15

Almond, hulls 0.15 12/31/15

Cherry, sweet 0.01 12/31/15

Fig 0.01 12/31/15

Pear 0.01 12/31/15

Pistachio 0.01 12/31/15

Plum, prune, fresh 0.01 12/31/15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 22936, May 7, 2001, as amended at 69 FR 48805, Aug. 11, 2004; 69 FR 58322, Sept. 30, 2004; 73 FR 47846, Aug. 15, 

2008; 78 FR 46283, July 31, 2013; 79 FR 18471, Apr. 2, 2014]

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§180.570 Isoxadifen-ethyl; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. (1) Tolerances are established for residues of isoxadifen-ethyl (ethyl 5,5-diphenyl-2-isoxazoline-3-

carboxylate, (CAS No. 163520-33-0), and its metabolite: 4,5-dihydro-5,5-diphenyl-3-isoxazolecarboxylic acid, when used 

as an inert ingredient (safener) in or on the following raw agricultural commodities:

Commodity Parts per million

Corn, field, forage 0.20 

Corn, field, grain 0.08 

Corn, field, stover 0.40 

Corn, oil 0.50

Corn, pop, grain 0.04 

Corn, pop, stover 0.25 

Corn, sweet, forage 0.30 

Corn, sweet, kernel plus cob with husk removed 0.04 

Corn, sweet, stover 0.45

(2) Tolerances are established for the residues of isoxadifen-ethyl (3-isoxazolecarboxylic acid, 

4,5-dihydro-5,5-diphenyl-, ethyl ester (CAS No. 164520-33-0)), and its metabolites 4,5-dihydro-5,5-diphenyl-3-

isoxazolecarboxylic acid and β-hydroxy-β-benzenepropanenitrile when used as an inert ingredient (safener) in or on the 

following raw agricultural commodities:

Commodity Parts per million

Rice, grain 0.10

Rice, hulls 0.50

Rice, straw 0.25

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 33187, June 21, 2001, as amended at 66 FR 40141, Aug. 2, 2001; 67 FR 12878, Mar. 20, 2002; 69 FR 29890, May 26, 2004; 

72 FR 63997, Nov. 14, 2007]

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§180.571 Mesotrione; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide mesotrione, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only mesotrione, 2-[4-(methylsulfonyl)-2-nitrobenzoyl]-1,3-cyclohexanedione, in or on the 

following raw agricultural commodities:

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Commodity Parts per million

Almond, hulls 0.02

Asparagus 0.01

Berry, group 13 0.01

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Corn, sweet, forage 0.5

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 1.5

Cranberry 0.02

Flax, seed 0.01

Fruit, citrus, group 10-10 0.01

Fruit, pome, group 11-10 0.01

Fruit, stone, group 12-12 0.01

Grass, forage 0.01

Grass, hay 0.01

Grass, seed screenings 0.10

Grass, straw 0.10

Lingonberry 0.01

Millet, forage 0.01

Millet, grain 0.01

Millet, hay 0.02

Millet, straw 0.02

Nut, tree, group 14-12 0.01

Oat, forage 0.01

Oat, grain 0.01

Oat, hay 0.01

Oat, straw 0.01

Okra 0.01

Rhubarb 0.01

Sorghum, grain, forage 0.01

Sorghum, grain, grain 0.01

Sorghum, grain, stover 0.01

Sorghum, sweet 0.01

Soybean, seed 0.01 

Sugarcane, cane 0.01

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 33195, June 21, 2001, as amended at 67 FR 45656, July 10, 2002; 68 FR 273, Jan. 3, 2003; 69 FR 58310, Sept. 30, 2004; 

70 FR 14551, Mar. 23, 2005; 72 FR 71802, Dec. 19, 2007; 73 FR 1512, Jan. 9, 2008; 73 FR 9226, Feb. 20, 2008; 74 FR 67123, 

Dec. 18, 2009; 76 FR 34886, June 15, 2011; 80 FR 30630, May 29, 2015]

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§180.572 Bifenazate; tolerance for residues.

(a) General. (1) Tolerances are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)

hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table. 

Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its 

metabolite, diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester, (calculated as the stoichiometric 

equivalent of bifenazate) in or on the following food commodities:

Commodity Parts per million

Acerola 0.90

Almond, hulls 15 

Apple, wet pomace 1.2

Atemoya 1.6

Avocado 7.0

Bean, dry seed 0.60

Berry, low-growing subgroup 13-07G 1.5

Biriba 1.6

Black sapote 7.0

Caneberry subgroup 13-07A 5.0

Canistel 7.0

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Cattle, fat 0.10

Cherimoya 1.6

Cotton, gin byproducts 35

Cotton, undelinted seed 0.75

Custard apple 1.6

Feijoa 0.90

Fruit, pome, group 11-10 0.7

Fruit, small, vine climbing subgroup 13-07F, except fuzzy kiwifruit 1.0

Fruit, stone, group 12, except plum 2.5

Goat, fat 0.10

Grape 0.75

Grape, raisin 1.2

Guava 0.9

Herb, subgroup 19A, except chervil and chive 300

Hog, fat 0.10

Hop, dried cones 15

Horse, fat 0.10

Jaboticaba 0.90

Ilama 1.6

Longan 5.0

Lychee 5.0

Mango 7.0

Nut, tree, group 14 0.20

Okra 2.0

Papaya 7.0

Passionfruit 0.90

Pea and bean, succulent shelled, subgroup 6B 0.70

Peppermint, tops 25

Pistachio 0.20

Plum 0.20

Pulasan 5.0

Rambutan 5.0

Sapodilla 7.0

Sapote, mamey 7.0

Sheep, fat 0.10

Soursop 1.6

Soybean, succulent shelled 0.70

Spanish lime 5.0

Spearmint, tops 25

Star apple 7.0

Starfruit 0.90

Strawberry 1.5

Sugar apple 1.6

Vegetable, cucurbit, group 9 0.75

Vegetable, fruiting, group 8-10 4.0

Vegetable, legume, edible-podded, subgroup 6A 6.0

Vegetable, tuberous and corm, subgroup 1C 0.10

Wax jambu 0.90

(2) Tolerances are established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl) 

hydrazinecarboxylate) including its metabolites and degradates, in or on the commodities listed in the following table. 

Compliance with the tolerance levels specified are to be determined by measuring only the sum of bifenazate and its 

metabolites diazinecarboxylic acid, 2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester; 1,1′-biphenyl, 4-ol; and 1,1′

-biphenyl, 4-oxysulfonic acid (calculated as the stoichiometric equivalent of bifenazate) in or on the following food 

commodities:

Commodity Parts per million 

Cattle, meat 0.02

Cattle, meat byproducts 0.02

Goat, meat 0.02

Goat, meat byproducts 0.02

Hog, meat 0.02

Hog, meat byproducts 0.02

Horse, meat 0.02

Horse, meat byproducts 0.02

Milk 0.02

Sheep, meat 0.02

Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registration, as defined in §180.1(l), are 

established for residues of bifenazate (1-methylethyl 2-(4-methoxy[1,1′-biphenyl]-3-yl)hydrazinecarboxylate) including its 

metabolites and degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels 

specified are to be determined by measuring only the sum of bifenazate and its metabolite, diazinecarboxylic acid, 

2-(4-methoxy-[1,1′-biphenyl]-3-yl), 1-methylethyl ester, (calculated as the stoichiometric equivalent of bifenazate) in or on 

the following food commodities:

Commodity

Parts per

million

Timothy, forage 200

Timothy, hay 150

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 34569, June 29, 2001]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.572, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.573 Tepraloxydim; tolerances for residues.

(a) General. (1) Tolerances are established for residues of tepraloxydim, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the combined residues of tepraloxydim, (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)

pentane-1,5-dioic acid) and OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as 

tepraloxydim, in or on the commodities.

Commodity Parts per million 

Cotton, undelinted seed 0.2 

Cotton, gin byproducts 3.0 

Flax, seed 0.10

Grain, aspirated fraction 1200.0

Pea and bean, dried shelled, except soybean, subgroup 6C1 0.10

Soybean, seed 6.0 

Soybean, hulls 8.0

Sunflower subgroup 20B1 0.20

1

There are no U.S. registrations for commodities in this subgroup.

(2) Tolerances are established for residues of tepraloxydim, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the combined residues of tepraloxydim (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro2H-pyran-4-yl)-2-cyclohexen-1-one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), 

OH-GP (3-hydroxy-3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), and GL (3-(2-oxotetrahydropyran-4-yl)-1,5-dioic acid), 

calculated as tepraloxydim, in or on the commodities.

Commodity Parts per million 

Cattle, fat 0.15 

Cattle, kidney 0.50 

Cattle, meat 0.20 

Cattle, meat byproducts, except kidney 0.20 

Egg 0.20 

Goat, fat 0.15 

Goat, kidney 0.50 

Goat, meat 0.20 

Goat, meat byproducts, except kidney 0.20 

Hog, fat 0.15 

Hog, kidney 0.50 

Hog, meat 0.20 

Hog, meat byproducts, except kidney 0.20 

Horse, fat 0.15 

Horse, kidney 0.50 

Horse, meat 0.20 

Horse, meat byproducts, except kidney 0.20 

Milk 0.10 

Poultry, fat 0.30 

Poultry, liver 1.00 

Poultry, meat 0.20 

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Poultry, meat byproducts, except liver 0.20 

Sheep, fat 0.15 

Sheep, kidney 0.50 

Sheep, meat 0.20 

Sheep, meat byproducts, except kidney 0.20

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. A tolerance with regional registration, as defined in §180.1(l), is established 

for residues of tepraloxydim, including its metabolites and degradates, in or on the commodities in the table below. 

Compliance with the tolerance levels specified below is to be determined by measuring only the combined residues of 

tepraloxydim (2-[1-[[[(2E)-3-chloro-2-propen-1-yl]oxy]imino]propyl]-3-hydroxy-5-(tetrahydro-2H-pyran-4-yl)-2-cyclohexen-1-

one) and its metabolites convertible to GP (3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid) and OH-GP (3-hydroxy3-(tetrahydropyran-4-yl)pentane-1,5-dioic acid), calculated as tepraloxydim, in or on the commodities.

Commodity Parts per million 

Canola, seed 0.50

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 40150, Aug. 2, 2001, as amended at 72 FR 54588, Sept. 26, 2007; 76 FR 34885, June 15, 2011; 76 FR 82152, Dec. 30, 

2011]

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§180.574 Fluazinam; tolerances for residues.

(a) General. (1) Tolerances are established for residues of fluazinam (3-chloro-N-[3-chloro-2,6-dinitro4-(trifluoromethyl)phenyl]-5-(trifluoromethyl)-2-pyridinamine), including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only fluazinam.

Commodity Parts per million

Apple 2.0

Apple, wet pomace 5.0

Bushberry subgroup 13-07B 7.0

Carrot, roots 0.70

Ginseng 4.5

Lettuce, head 0.02

Lettuce, leaf 2.0

Melon subgroup 9A 0.07

Onion, bulb, subgroup 3-07A 0.20

Pea and bean, dried shelled, except soybean, subgroup 6C, except pea 0.02

Pea and bean, succulent shelled, subgroup 6B, except pea 0.04

Peanut 0.02

Pepper/eggplant subgroup 8-10B 0.09

Potato 0.02

Soybean, seed 0.01

Soybean, hulls 0.05

Turnip, greens 0.01

Vegetable, Brassica leafy, group 5 0.01

Vegetable, legume, edible-podded, subgroup 6A, except pea 0.10

(2) Tolerances are established for residues of fluazinam, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only fluazinam and its metabolite AMGT (3-[[4-amino-3-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]amino]-2-nitro6-(trifluoromethyl) phenyl]thio]-2-(beta-D-glucopyranosyloxy) propionic acid).

Commodity Parts per million

Grape, wine1 3.0

1

 No US registration as of March 15, 2002.

(3) Tolerances are established for residues of fluazinam (3-chloro-N-[3-chloro-2,6-dinitro-4-(trifluoromethyl)phenyl]

-5-(trifluoromethyl)-2-pyridinamine), including its metabolites and degradates, in or on the commodities in the table below. 

Compliance with the tolerance levels specified below is to be determined by measuring only fluazinam, AMPA 

(2-(6-amino-3-chloro-α,α,α-trifluoro-2-nitro-p-toluidino)-3-chloro-5-(trifluoromethyl) pyridine), DAPA (3-chloro2-(2,6-diamino-3-chloro-α,α,α.-trifluoro-p-toluidino)-5-(trifluoromethyl)pyridine), and their sulfamate conjugates.

Commodity

Parts per

million

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Cattle, fat 0.05

Cattle, meat byproducts 0.05

Goat, fat 0.05

Goat, meat byproducts 0.05

Horse, fat 0.05

Horse, meat byproducts 0.05

Sheep, fat 0.05

Sheep, meat byproducts 0.05

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 46738, Sept. 7, 2001, as amended at 67 FR 19130, Apr. 18, 2002; 72 FR 60260, Oct. 24, 2007; 75 FR 26667, May 12, 2010; 

76 FR 3029, Jan. 19, 2011; 77 FR 66729, Nov. 7, 2012]

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§180.575 Sulfuryl fluoride; tolerances for residues.

(a)(1) General. Tolerances are established for residues of sulfuryl fluoride in or on the following commodities from the 

postharvest fumigation with sulfuryl fluoride for the control of insects:

Commodity Parts per million

All processed food commodities not otherwise listed 2.0

Barley, bran, postharvest 0.05 

Barley, flour, postharvest 0.05 

Barley, grain, postharvest 0.1 

Barley, pearled barley, postharvest 0.05 

Cacao bean, roasted bean, postharvest 0.2

Cattle, meat, dried 0.01

Cheese 2.0

Coconut, postharvest 1.0

Coffee, bean, roasted bean, postharvest 1.0

Corn, field, flour, postharvest 0.01 

Corn, field, grain, postharvest 0.05 

Corn, field, grits, postharvest 15.0 

Corn, field, meal, postharvest 0.01 

Corn, pop, grain, postharvest 0.05 

Cotton, undelinted seed, postharvest 0.5

Egg, dried 1.0

Fruit, dried, postharvest 0.05 

Ginger, postharvest 0.5

Grain, aspirated fractions, postharvest 0.05 

Herbs and spices group 19, postharvest 0.5

Hog, meat 0.02

Milk, powdered 2.0

Millet, grain, postharvest 0.1 

Nut, pine, postharvest 0.2

Nut, tree, Group 14, postharvest 3.0 

Oat, flour, postharvest 0.05 

Oat, grain, postharvest 0.1 

Oat, groats/rolled oats, postharvest 0.1 

Peanut, postharvest 0.5

Pistachio, postharvest 3.0

Rice, bran, postharvest 0.01 

Rice, flour, postharvest 0.05

Rice, grain, postharvest 0.04 

Rice, hulls, postharvest 0.1 

Rice, polished rice, postharvest 0.01 

Rice, wild, grain, postharvest 0.05 

Sorghum, grain, grain, postharvest 0.1 

Triticale, grain, postharvest 0.1 

Vegetable, legume, group 6, postharvest 0.5

Wheat, bran, postharvest 0.05 

Wheat, flour, postharvest 0.05 

Wheat, germ, postharvest 0.02 

Wheat, grain, postharvest 0.1

Wheat, milled byproducts, postharvest 0.05 

Wheat, shorts, postharvest 0.05

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(2) To assure safe use of this pesticide commodities treated with sulfuryl fluoride must be aerated for at least 24 hours 

prior to entering commerce. 

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[67 FR 5740, Feb. 7, 2002, as amended at 69 FR 3257, Jan. 23, 2004; 70 FR 40908, July 15, 2005]

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§180.576 Cyhalofop-butyl; tolerances for residues.

(a) General. Tolerances are established for residues of cyhalofop-butyl, including its metabolites and degradates, in or 

on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring cyhalofop butyl [R-( + )-n-butyl-2-(4(4-cyano-2-fluorophenoxy)-phenoxy)propionate], cyhalofop acid [R-( + )-2-(4

(4-cyano-2-fluorophenoxy)-phenoxy)propionic acid], and the di-acid metabolite [(2R)-4-(4-(1-carboxyethoxy)phenoxy)-3-

fluorobenzoic acid].

Commodity Parts per million

Rice, grain 0.40

Wild rice, grain 0.40

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 43256, June 27, 2002, as amended at 74 FR 15880, Apr. 8, 2009; 76 FR 82157, Dec. 30, 2011]

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§180.577 Bispyribac-sodium; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the herbicide bispyribac-sodium, including its metabolites and 

degradates, in or on the commodity listed below. Compliance with the tolerance level specified below is to be determined 

by measuring only bispyribac-sodium, (2,6-bis[(4,6-dimethoxy-2-pyrimidinyl)oxy]benzoic acid, sodium salt), in or on the 

following raw agricultural commodities:

Commodity Parts per million

Fish, freshwater 0.01

Rice, grain 0.02

Rice, straw 0.02

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[66 FR 48097, Sept. 18, 2001, as amended at 76 FR 5716, Feb. 2, 2011]

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§180.578 Acetamiprid; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)

methyl]-N'-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table 

below as a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be 

determined by measuring only acetamiprid in or on the following commodities.

Commodity Parts per million

Almond, hulls 5.0

Asparagus 0.80

Berry, low growing subgroups 13-07G 0.60

Brassica, head and stem, subgroup 5A 1.20

Brassica, leafy greens, subgroup 5B 15

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Bushberry subgroup 13-07B 1.6

Caneberry subgroup 13-07A 1.6

Canola, seed 0.010

Citrus, dried pulp 1.20

Corn, sweet, forage 15

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 30

Cotton, gin byproducts 20.0

Cotton, undelinted seed 0.60

Fruit, citrus, group 10-10 1.0

Fruit, pome, group 11-10 1.0

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.35

Fruit, stone, group 12, except plum, prune 1.20

Grain, aspirated fractions 5.0

Mustard, seed 0.010

Nut, tree, group 14 0.10

Onion, bulb, subgroup 3-07A 0.02

Onion, green, subgroup 3-07B 4.5

Pea and bean, succulent shelled, subgroup 6B 0.40

Pistachio 0.10

Plum, prune, dried 0.40

Plum, prune, fresh 0.20

Soybean, hulls 0.04

Soybean, seed 0.03

Tea, dried1 50.0

Tomato, paste 0.40

Turnip greens 15

Vegetable, cucurbit, group 9 0.50

Vegetable, fruiting, group 8-10 0.20

Vegetable, leafy, except brassica, group 4 3.00

Vegetable, legume, edible podded, subgroup 6A 0.60

Vegetable, tuberous and corm, group 1 0.01

1

There are no U.S. registrations as of February 10, 2010, for the use of acetamiprid on dried tea.

(2) Tolerances are established for residues of the insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′

-cyano-N-methylethanimidamide, including its metabolites and degradates, in or on the commodities in the table below as 

a result of the application of acetamiprid. Compliance with the tolerance levels specified below is to be determined by 

measuring acetamiprid and (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-ethanimidamide in or on the following 

commodities.

Commodity Parts per million

Cattle, fat 0.20

Cattle, meat 0.30

Cattle, meat byproducts 0.70

Egg 0.010

Goat, fat 0.20

Goat, meat 0.30

Goat, meat byproducts 0.70

Hog, fat 0.10

Hog, meat 0.10

Hog, meat byproducts 0.20

Horse, fat 0.20

Horse, meat 0.30

Horse, meat byproducts 0.70

Milk 0.30

Poultry, fat 0.010

Poultry, liver 0.050

Poultry, meat 0.010

Sheep, fat 0.20

Sheep, meat 0.30

Sheep, meat byproducts 0.70

(3) A tolerances of 0.01 ppm is established for residues of the insecticide acetamiprid, including its metabolites and 

degradates, in or on all food/feed items (other than those covered by a higher tolerance in paragraph (a)(1) or (a)(2) of this 

section as a result of the use on growing crops) as a result of the application of acetamiprid in food/feed handling 

establishments. Compliance with the 0.01 ppm tolerance level is to be determined by measuring only acetamiprid (1E)

-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide in or on the commodities.

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

insecticide acetamiprid (1E)-N-[(6-chloro-3-pyridinyl)methyl]-N′-cyano-N-methylethanimidamide, including its metabolites 

and degradates, in or on the commodities in the table below as a result of the application of acetamiprid. Compliance with 

the tolerance levels specified below is to be determined by measuring only acetamiprid in or on the following commodities.

Commodity Parts per million

Clover, forage 0.30

Clover, hay 2.0

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 14659, Mar. 27, 2002, as amended at 68 FR 52352, Sept. 3, 2003; 70 FR 19293, Apr. 13, 2005; 72 FR 67262, Nov. 28, 

2007; 73 FR 2811, Jan. 16, 2008; 75 FR 6582, Feb. 10, 2010; 77 FR 18716, Mar. 28, 2012; 77 FR 43529, July 25, 2012; 78 FR 

36676, June 19, 2013; 80 FR 68778, Nov. 6, 2015]

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§180.579 Fenamidone; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide, fenamidone, including its metabolites and 

degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined by measuring 

only fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), in or on the 

commodities:

Commodity Parts per million 

Bean, succulent, except cowpea 0.80

Brassica, head and stem, subgroup 5A 5.0

Brassica, leafy greens, subgroup 5B 55

Cilantro, leaves 60

Cotton, gin byproducts 0.02

Cotton, undelinted seed 0.02

Ginseng 0.80

Okra 3.5

Onion, bulb, subgroup 3-07A 0.20

Onion, green, subgroup 3-07B 1.5

Pepper, nonbell 3.5

Sunflower 0.02

Tomato, paste 2.2

Tomato, puree 2.0

Turnip, greens 55

Vegetable, cucurbit, group 9 0.15

Vegetable, fruiting, group 8, except nonbell pepper 1.0

Vegetable, leafy, except Brassica, group 4 60

Vegetable, root, except sugar beet, subgroup 1B, except radish 0.15

Vegetable, tuberous and corm, subgroup 1C 0.02

(2) Tolerances are established for residues of the fungicide fenamidone, including its metabolites and degradates, in 

or on the following commodities. Compliance with the tolerance levels is to be determined by measuring fenamidone (4HImidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), and its metabolite RPA 717879 

(2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the commodities:

Commodity Parts per million

Cattle, fat 0.10

Cattle, meat 0.10

Cattle, meat byproducts 0.10

Goat, fat 0.10

Goat, meat 0.10

Goat, meat byproducts 0.10

Milk 0.02

Sheep, fat 0.10

Sheep, meat 0.10

Sheep, meat byproducts 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. A tolerance with regional registration as defined in §180.1(l) is established 

for residues of the fungicide fenamidone, including its metabolites and degradates, in or on the following commodities. 

Compliance with the tolerance levels is to be determined by measuring only fenamidone (4H-Imidazol-4-one, 3,5-dihydro5-methyl-2-(methylthio)-5-phenyl-3 (phenylam-ino)-,(S)-), in or on the commodity:

Commodity Parts per million

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Grape1 1.0

1

Applicable to grapes grown East of the Rocky Mountains.

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide fenamidone, including its 

metabolites and degradates, in or on the following commodities. Compliance with the tolerance levels is to be determined 

by measuring fenamidone (4H-Imidazol-4-one, 3,5-dihydro-5-methyl-2-(methylthio)-5-phenyl-3 (phenylamino)-,(S)-), and 

its metabolite RPA 717879 (2,4-imidazolidinedione, 5-methyl-5-phenyl), in or on the following commodities when present 

therein as a result of application of fenamidone to the crops in paragraph (a)(1).

Commodity

Parts per

million

Grain, cereal, group 15, except rice 0.1

Grain, cereal, forage, fodder and straw, group 16, except rice 0.5

Soybean, forage 0.15

Soybean, hay 0.25

Soybean, seed 0.02

Strawberry 0.02

[67 FR 60976, Sept. 27, 2002, as amended at 69 FR 58066, Sept. 29, 2004; 71 FR 55293, Sept. 22, 2006; 72 FR 60272, Oct. 24, 

2007; 74 FR 34257, July 15, 2009; 76 FR 34885, June 15, 2011; 76 FR 70895, Nov. 16, 2011; 77 FR 32401, June 1, 2012; 79 FR 

13882, Mar. 12, 2014]

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§180.580 Iodosulfuron-Methyl-Sodium; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide Iodosulfuron-Methyl-Sodium (methyl 4-iodo2-[3-(4-methoxy-6-methyl-1,3,5 triazin-2-yl)ureidosulfonyl]benzoate, sodium salt) in or on the following commodities:

Commodity Parts per million

Corn, field, forage 0.05

Corn, field, grain 0.03

Corn, field, stover 0.05

Wheat, forage 0.10

Wheat, grain 0.02

Wheat, hay 0.05

Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 57532, Sept. 11, 2002, as amended at 74 FR 23644, May 20, 2009]

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§180.581 Iprovalicarb; tolerances for residues.

(a) General. Tolerances are established for residues of iprovalicarb, [2-methyl-1[[[(1S)-(4-methylphenyl) ethyl] amino]

carbonyl] propyl]carbamic acid methylethylester, in or on the following commodities.

Commodity Parts per million

Grape1 2.0

Tomato1 1.0

1

There is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 54359, Aug. 22, 2002, as amended at 70 FR 55281, Sept. 21, 2005]

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§180.582 Pyraclostrobin; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the fungicide pyradostrobin, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of pyraclostrobin (carbamic acid, [2-[[[ 1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy] 

methyl]phenyl]methoxy-, methyl ester) and its desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]

methyl] phenylcarbamate), calculated as the stoichiometric equivalent of pyraclostrobin, in or on the commodity.

Commodity Parts per million

Alfalfa, forage 10

Alfalfa, hay 30

Almond, hulls 7.0

Apple, wet pomace 8.0

Artichoke, globe 3.0

Avocado 0.6

Banana 0.04

Barley, grain 1.4

Barley, hay 25

Barley, straw 6.0

Bean, succulent shelled 0.5

Beet, sugar, dried pulp 1.0

Beet, sugar, roots 0.2

Beet, sugar, tops 8.0

Berry, low growing, subgroup 13-07G, except cranberry 1.2

Brassica, head and stem, subgroup 5A 5.0

Brassica, leafy greens, subgroup 5B 16.0

Bushberry subgroup 13-07B 4.0

Caneberry subgroup 13-07A 4.0

Canistel 0.6

Citrus, dried pulp 12.5

Citrus, oil 9.0

Coffee, green bean 1

0.3

Corn, field, forage 5.0

Corn, field, grain 0.1

Corn, field, refined oil 0.2

Corn, field, stover 17.0

Corn, pop, grain 0.1

Corn, pop, stover 17.0

Corn, sweet, forage 5.0

Corn, sweet, kernel plus cob with husks removed 0.04

Corn, sweet, stover 23.0

Cotton, gin byproducts 30

Dill, seed 40

Endive, belgium 4.0

Fruit, citrus, group 10-10 2.0

Fruit, pome, group 11-10 1.5

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0

Fruit, stone, group 12-12 2.5

Grain, aspirated fractions 2.5

Grape, raisin 7.0

Grass, forage 10

Grass, hay 4.5

Grass, seed screenings 27

Grass, straw 14

Herb subgroup 19A 40

Hop, dried cones 23.0

Mango 0.6

Nut, tree, group 14-12, except pistachio 0.04

Oat, grain 1.2

Oat, hay 18

Oat, straw 15

Oilseed group 20 0.45

Papaya 0.6

Pea, succulent 0.2

Pea and bean, dried shelled, except soybean, subgroup 6C 0.5

Peanut 0.05

Peanut, refined oil 0.1

Peppermint, tops 8.0

Persimmon 3.0

Pistachio 0.7

Radish, tops 16

Rye, grain 0.04

Rye, straw 0.5

Sapodilla 0.6

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Sapote, black 0.6

Sapote, mamey 0.6

Sorghum, grain, forage 5.0

Sorghum, grain, grain 0.60

Sorghum, grain, stover 0.80

Soybean, forage 11

Soybean, hay 14

Soybean, hulls 0.06

Soybean, seed 0.04

Spearmint, tops 8.0

Star apple 0.6

Sugarcane, cane 0.20

Vegetable, bulb, group 3-07 0.9

Vegetable, cucurbit, group 9 0.5

Vegetable, foliage of legume, except soybean, subgroup 7A 25.0

Vegetable, fruiting, group 8-10 1.4

Vegetable, leafy, except brassica, group 4 29.0

Vegetable, leaves of root and tuber, group 2, except sugar beet 16.0

Vegetable, legume, edible podded, subgroup 6A 0.5

Vegetable, root, except sugar beet, subgroup 1B 0.4

Vegetable, tuberous and corm, subgroup 1C 0.04

Vegetables, foliage of legume, group 7 25

Wheat, grain 0.02

Wheat, hay 6.0

Wheat, straw 8.5

(2) Tolerances are established for combined residues of the fungicide pyraclostrobin carbamic acid, 

[2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl]phenyl]methoxy-, methyl ester and its metabolites convertible to 

1-(4-chlorophenyl)-1H-pyrazol-3-ol and 1-(4-chloro-2-hydroxyphenyl)-1H-pyrazol-3-ol, expressed as parent compound, in 

or on the following raw agricultural commodities.

Commodity Parts per million

Cattle, fat 0.1

Cattle, liver 1.5

Cattle, meat 0.1

Cattle, meat byproducts, except liver 0.2

Goat, fat 0.1

Goat, liver 1.5

Goat, meat 0.1

Goat, meat byproducts, except liver 0.2

Hog, fat 0.1

Hog, liver 1.5

Hog, meat 0.1

Hog, meat byproducts, except liver 0.2

Horse, fat 0.1

Horse, liver 0.1

Horse, meat 0.1

Horse, meat byproducts, except liver 0.2

Milk 0.1

Poultry, eggs 0.10

Poultry, fat 0.10

Poultry, meat 0.10

Poultry, meat byproducts 0.10

Sheep, fat 0.1

Sheep, liver 1.5

Sheep, meat 0.1

Sheep, meat byproducts, except liver 0.2

(b) Section 18 emergency exemptions. A time-limited tolerance is established for combined residues of the fungicide 

pyraclostrobin, (carbamic acid, [2-[[[1-(4-chlorophenyl)-1H-pyrazol-3-yl]oxy]methyl] phenyl]methoxy-, methyl ester) and its 

desmethoxy metabolite (methyl-N-[[[1-(4-chlorophenyl) pyrazol-3-yl]oxy]o-tolyl]carbamate) in connection with use of the 

pesticide under section 18 emergency exemptions granted by EPA. The time-limited tolerance will expire and is revoked 

on the date specified in the following table.

Commodity

Parts per

million Expiration/revocation date

Endive, belgium 11.0 12/31/13

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

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[67 FR 60901, Sept. 27, 2002, as amended at 69 FR 63100, Oct. 29, 2004; 71 FR 17021, Apr. 5, 2006; 72 FR 54569, Sept. 26, 

2007; 73 FR 15431, Mar. 24, 2008; 73 FR 21842, Apr. 23, 2008; 73 FR 44167, July 30, 2008; 74 FR 11499, Mar. 18, 2009; 74 FR 

51496, Oct. 7, 2009; 75 FR 770, Jan. 6, 2010; 75 FR 42329, July 21, 2010; 75 FR 80346, Dec. 22, 2010; 76 FR 81396, Dec. 28, 

2011; 78 FR 53046, Aug. 28, 2013; 80 FR 19238, Apr. 10, 2015]

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§180.583 Triticonazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide triticonazole, (1RS)-(E)-5-[(4-chlorophenyl)

methylene]-2,2-dimethyl-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol, from the treatment of seed prior to planting in or on 

raw agricultural commodities as follows:

Commodity Parts per million

Grain, cereal, forage, fodder and straw, group 16, except rice 0.10 

Grain, cereal, group 15, except rice 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 60959, Sept. 27, 2002, as amended at 75 FR 4288, Jan. 27, 2010]

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§180.584 Tolylfluanid; tolerances for residues.

(a) General. Tolerances are established for residues of tolylfluanid, 1,1-dichloro-N-[(dimethylamino)-sulfonyl]-1-fluoroN-(4-methylphenyl)methanesulfenamide in or on the following commodities. 

Commodity Parts per million

Apple1 5.0

Grape1 11

Hop, dried cones1 30

Tomato1 2.0

1

 No U.S. registration as of August 31, 2002.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[67 FR 60141, Sept. 25, 2002]

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§180.585 Pyraflufen-ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide, pyraflufen-ethyl, including its metabolites and 

degradates, in the commodities in the table below. Compliance with the plant commodity tolerance levels specified in the 

table is to be determined by measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4-chloro-5-

difluoromethoxy)-1-methyl-1H-pyrazol-3-yl]-4-fluorophenoxy] acetate, and its acid metabolite, E-1, 2-chloro-5-(4-chloro-5-

difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, calculated as the stoichiometric equivalent of 

pyraflufen-ethyl in or on the commodity. Compliance with the livestock commodity tolerance levels specified in the table is 

to be determined by measuring only the sum of the parent pyraflufen-ethyl, ethyl 2-[2-chloro-5-(4-chloro-5-

difluoromethoxy)-1-methyl-1H-pyrazol-3-yl]-4-fluorophenoxy] acetate and its acid metabolites: E-1, 2-chloro-5-(4-chloro-5-

difluoromethoxy-1-methyl-1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, and E-9, 2-chloro-5-(4-chloro-5-difluoromethoxy1H-pyrazol-3-yl)-4-fluorophenoxyacetic acid, both calculated as the stoichiometric equivalent of pyraflufen-ethyl in or on 

the commodity.

Commodity Parts per million

Almond, hulls 0.02

Cattle, fat 0.03

Cattle, meat 0.03

Cattle, meat byproducts 0.03

Corn, field, forage 0.01

Corn, field, grain 0.01

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Corn, field, stover 0.01

Cotton, gin byproducts 1.5

Cotton, undelinted seed 0.04

Fruit, pome, group 11-10 0.01

Fruit, stone, group 12 0.01

Goat, fat 0.03

Goat, meat 0.03

Goat, meat byproducts 0.03

Grape 0.01

Grass, forage, group 17 1.0

Grass, hay, group 17 1.4

Horse, fat 0.03

Horse, meat 0.03

Horse, meat byproducts 0.03

Milk 0.03

Nut, tree, group 14 0.01

Olive 0.01

Peanut 0.01

Peanut, hay 0.07

Pistachio 0.01

Pomegranate 0.01

Potato 0.02

Sheep, fat 0.03

Sheep, meat 0.03

Sheep, meat byproducts 0.03

Soybean, forage 0.05

Soybean, hay 0.10

Soybean, seed 0.01

Wheat, forage 0.02

Wheat, grain 0.01

Wheat, hay 0.01

Wheat, straw 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 23055, Apr. 30, 2003, as amended at 68 FR 27739, May 21, 2003; 69 FR 26312, May 12, 2004; 73 FR 51743, Sept. 5, 2008; 

76 FR 31484, June 11, 2011; 77 FR 75861, Dec. 26, 2012; 78 FR 13263, Feb. 27, 2013]

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§180.586 Clothianidin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide clothianidin, including its metabolites and 

degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)

-N-[(2-Chloro-5-thiazolyl)methyl]-N′ -methyl-N′′ -nitroguanidine, in or on the following raw agricultural commodities:

Commodity Parts per million

Almond, hulls 1.5

Beet, sugar, dried pulp 0.03

Beet, sugar, molasses 0.05

Beet, sugar, roots 0.02

Berry, low-growing, subgroup 13-07H, except strawberry 0.01

Canola, seed 0.01

Cotton, gin byproducts 4.5

Cotton, undelinted seed 0.20

Fig 0.05

Fruit, pome 1.0

Grain, cereal, forage, fodder and straw, group 16, except rice, forage 0.35

Grain, cereal, forage, fodder and straw, group 16, except rice, hay 0.07

Grain, cereal, forage, fodder and straw, group 16, except rice, stover 0.1

Grain, cereal, forage, fodder and straw, group 16, except rice, straw 0.05

Grain, cereal, group 15, except rice 0.01

Grape 0.60

Milk 0.01

Mustard, seed 0.01

Nut, tree, group 14 0.01

Peach 0.80

Pepper 0.80

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Pomegranate 0.20

Potato, chips 0.6

Potato, granules/flakes 1.5

Rice, grain 0.01

Soybean, seed 0.02

Tea, dried1 70

Vegetable, brassica, leafy, group 5 1.9

Vegetable, bulb, group 3-07 0.45

Vegetable, cucurbit, group 9 0.06

Vegetable, fruiting, group 8, except pepper 0.20

Vegetable, leafy, except brassica, group 4 3.0

Vegetable, root, except sugar beet, subgroup 1B 0.8

Vegetable, tuberous and corm, subgroup 1C 0.3

1

No U.S. registrations.

(2) Time-limited tolerances are established for residues of the insecticide clothianidin, including its metabolites and 

degradates. Compliance with the tolerance levels specified below is to be determined by measuring only clothianidin, (E)

-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on the following raw agricultural commodity:

Commodity Parts per million Expiration/revocation date

Rice, seed 0.01 6/23/12

(b) Section 18 emergency exemptions. A time-limited tolerance specified in the following table is established for 

residues of clothianidin, (E)-N-[(2-chloro-5-thiazolyl)methyl]-N'-methyl-N”-nitroguanidine, in or on the specified agricultural 

commodity, resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. This tolerance 

expires on the date specified in the table.

Commodity Parts per million Expiration date

Fruit, citrus, group 10-10 0.07 12/31/17

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. Tolerances are established for the indirect or inadvertent residues of the 

insecticide clothianidin, including its metabolites and degradates. Compliance with the tolerance levels specified below is 

to be determined by measuring only clothianidin, (E)-1-(2-chloro-1,3-thiazol-5-ylmethyl)-3-methyl-2-nitroguanidine, in or on 

the following raw agricultural commodities when present therein as a result of the application of clothianidin to crops listed 

in paragraph (a) of this section:

Commodity Parts per million

Animal feed, nongrass, group 18 0.02

Grass, forage, fodder and hay, group 17 0.02

Soybean, forage 0.02

Soybean, hay 0.02

[74 FR 65028, Dec. 9, 2009, as amended at 76 FR 7718, Feb. 11, 2011; 76 FR 25246, May 4, 2011; 76 FR 34886, June 15, 2011; 

77 FR 52252, Aug. 29, 2012; 78 FR 19136, Mar. 29, 2013; 80 FR 10007, Feb. 25, 2015]

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§180.587 Famoxadone; tolerance for residues.

(a) General. Tolerances are established for residues of the fungicide famoxadone (3-anilino-5-methyl5-(4-phenoxyphenyl)-1,3-oxazolidine-2,4-dione) in or on the following commodities:

Commodity Parts per million

Caneberry subgroup 13-07A 10

Cattle, fat 0.02

Cattle, liver 0.05

Cilantro, leaves 25

Goat, fat 0.02

Goat, liver 0.05

Grape, raisin1 4.0

Hop, dried cone 80

Horse, fat 0.02

Horse, liver 0.05

Milk, fat (reflecting negligible residues in whole milk) 0.06

Onion, bulb, subgroup 3-07A 0.45

Onion, green, subgroup 3-07B 40

Potato 0.02

Sheep, fat 0.02

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Sheep, liver 0.05

Spinach 50

Tomato 1.0

Vegetable, cucurbit, group 9 0.30

Vegetable, fruiting, group 8, except tomato 4.0

Vegetable, leafy, except Brassica, group 4, except spinach 25

1

There are no U.S. registrations as of May 15, 2003.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with a regional registrations. Tolerances with a regional registration as defined in §180.1(l) are 

established for the residues of the fungicide famoxadone, 3-anilino-5-methyl-5-(4-phenoxyphenyl)

-1,3-oxazolidine-2,4-dione) in or on the raw agricultural commodities:

Commodity Parts per million

Grape 2.5

(d) Indirect or inadvertant residues. [Reserved]

[68 FR 39471, July 2, 2003, as amended at 72 FR 28881, May 23, 2007; 74 FR 9364, Mar. 4, 2009; 76 FR 34885, June 15, 2011]

 Back to Top

§180.588 Quinoxyfen; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide quinoxyfen, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only quinoxyfen (5,7-dichloro-4-(4-fluorophenoxy)quinoline).

Commodity Parts per million

Artichoke, globe 1.4 

Berry, low growing, subgroup 13-07G 1.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0

Fruit, stone, group 12 0.70 

Hop, dried cones 3.0

Gourd, edible 0.20 

Lettuce, head 7.0

Lettuce, leaf 19

Melon, subgroup 9A 0.08

Pumpkin 0.20 

Squash, winter 0.20 

Vegetable, fruiting, group 8-10 1.7

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55858, Sept. 29, 2003, as amended at 70 FR 4032, Jan. 28, 2005; 71 FR 50354, Aug. 25, 2006; 74 FR 14743, Apr. 1, 2009; 

78 FR 57280, Sept. 18, 2013]

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§180.589 Boscalid; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide boscalid, including its metabolites and 

degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be 

determined by measuring only boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), in or on the 

following raw agricultural commodities:

Commodity Parts per million

Alfalfa, forage 30.0

Alfalfa, hay 65.0

Almond, hulls 17

Apple, wet pomace 10

Artichoke, globe 6.0

Avocado 1.5

Banana, import1 0.40

Berry, low growing, subgroup 13-07G, except cranberry 4.5

Brassica, head and stem, subgroup 5A 3.0

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Brassica, leafy greens, subgroup 5B 18.0

Bushberry subgroup 13-07B 13.0

Caneberry subgroup 13-07A 10.0

Canistel 1.5

Canola, refined oil 5.0

Citrus, dried pulp 4.5

Citrus, oil 85.0

Coffee, green bean, import1 0.05

Cotton, gin byproducts 55.0

Cucumber 0.5

Dill, seed 100

Endive, Belgium 6.0

Fruit, citrus, group 10-10 2.0

Fruit, pome, group 11-10 3.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 5.0

Fruit, stone, group 12-12 3.5

Grain, aspirated fractions 3.0

Grape, raisin 8.5

Herb subgroup 19A 150

Hop, dried cones 35

Leaf petioles subgroup 4B 45

Leafy greens subgroup 4A, except head lettuce and leaf lettuce 60

Lettuce, head 6.5

Lettuce, leaf 11.0

Mango 1.5

Nut, tree, group 14-12 0.70

Oilseed group 20 3.5

Papaya 1.5

Pea and bean, dried shelled, except soybean, subgroup 6C, except cowpea, field pea and grain lupin 2.5

Pea and bean, succulent shelled, subgroup 6B, except cowpea 0.6

Peanut 0.05

Peanut, meal 0.15

Peanut, refined oil 0.15

Peppermint, tops 30.0

Persimmon 8.0

Sapodilla 1.5

Sapote, black 1.5

Sapote, mamey 1.5

Soybean, hulls 0.2

Soybean, seed 0.1

Soybean, vegetable 2.0

Spearmint, tops 30.0

Star apple 1.5

Turnip, greens 40.0

Vegetable, bulb, group 3-07 5.0

Vegetable, cucurbit, group 9, except cucumber 1.6

Vegetable, fruiting, group 8-10 3.0

Vegetable, legume, edible podded, subgroup 6A 1.6

Vegetable, root, subgroup 1A, except sugar beet, garden beet, radish, and turnip 1.0

Vegetable, tuberous and corm, subgroup 1C 0.05

1

No US registrations as of September 16, 2009.

(2) Tolerances are established for residues of the fungicide boscalid, including its metabolites and degradates, in or 

on the commodities listed below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl), and metabolites 2-chloro-N-(4'-

chloro-5-hydroxy-biphenyl-2-yl) nicotinamide and glucuronic acid conjugate of 2-chloro-N-(4′-chloro-5-hydroxy-biphenyl-2-

yl) nicotinamide, calculated as the stoichiometric equivalent of boscalid in or on the following food commodities:

Commodity Parts per million

Cattle, fat 0.30

Cattle, meat 0.10

Cattle, meat byproducts 0.35

Egg 0.02

Goat, fat 0.30

Goat, meat 0.10

Goat, meat byproducts 0.35

Hog, fat 0.20

Hog, meat 0.05

Hog, meat byproducts 0.10

Horse, fat 0.30

Horse, meat 0.10

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Horse, meat byproducts 0.35

Milk 0.10

Poultry, fat 0.20

Poultry, meat 0.05

Poultry, meat byproducts 0.20

Sheep, fat 0.30

Sheep, meat 0.10

Sheep, meat byproducts 0.35

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fungicide boscalid, 

including its metabolites and degradates, in connection with use of the pesticide under section 18 emergency exemptions 

granted by EPA. Compliance with the tolerance level specified below is to be determined by measuring only boscalid, 

3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′-biphenyl]-2-yl). This tolerance will expire and is revoked on the date 

specified in the following table:

Commodity Parts per million Expiration/revocation date

Endive, Belgian 16 12/31/13

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide 

boscalid, including its metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance 

levels specified below is to be determined by measuring only boscalid, 3-pyridinecarboxamide, 2-chloro-N-(4′-chloro[1,1′

-biphenyl]-2-yl), in or on the following commodities:

Commodity Parts per million

Animal feed, nongrass, group 18, forage, except alfalfa 1.0

Animal feed, nongrass, group 18, hay, except alfalfa 2.0

Animal feed, nongrass, group 18, seed 0.05

Beet, garden, roots 0.1

Beet, sugar, roots 0.1

Cowpea, seed 0.1

Grain, cereal, forage, fodder and straw, group 16, forage 2.0

Grain, cereal, forage, fodder and straw, group 16, stover 1.5

Grain, cereal, forage, fodder and straw, group 16, straw 3.0

Grain, cereal, group 15 0.20

Grass, forage, fodder, and hay, group 17, forage 2.0

Grass, forage, fodder, and hay, group 17, hay 8.0

Grass, forage, fodder, and hay, group 17, seed screenings 0.20

Grass, forage, fodder, and hay, group 17, straw 0.30

Lupin, grain, grain 0.1

Pea, field, seed 0.1

Radish, roots 0.1

Rice, hulls 0.50

Turnip, roots 0.1

Vegetable, foliage of legume, group 7, forage 1.5

Vegetable, foliage of legume, group 7, hay 2.0

Vegetable, foliage of legume, group 7, vines 0.05

Vegetable, leafy, except brassica, group 4, except celery, lettuce and spinach 1.0

Vegetable, leaves of root and tuber, group 2 0.1

[68 FR 44651, July 30, 2003, as amended at 69 FR 19774, Apr. 14, 2004; 70 FR 55293, Sept. 21, 2005; 71 FR 6364, Feb. 8, 2006; 

71 FR 25961, May 3, 2006; 71 FR 76190, Dec. 20, 2006; 73 FR 16558, Mar. 28, 2008; 74 FR 47445, Sept. 16, 2009; 75 FR 770, 

Jan. 6, 2010; 75 FR 29907, May 28, 2010; 75 FR 80346, Dec. 22, 2010; 78 FR 67048, Nov. 8, 2013; 80 FR 14014, Mar. 18, 2015]

 Back to Top

§180.590 2, 6-Diisopropylnaphthalene (2, 6-DIPN); tolerances for residues.

(a) General. Tolerances are established for residues of the growth inhibitor 2,6-DIPN, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only 2,6-Diisopropylnaphthalene.

Commodity Parts per million

Cattle, fat 0.2

Cattle, meat 0.02

Cattle, meat byproducts, except fat 0.02

Goat, fat 0.2

Goat, meat 0.02

Goat, meat byproducts, except fat 0.02

Horse, fat 0.2

Horse, meat 0.02

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Horse, meat byproducts, except fat 0.02

Milk, fat 0.02

Potato, granules/flakes 5.5

Potato, wet peel 6.0

Potato, whole 2.0

Sheep, fat 0.2

Sheep, meat 0.02

Sheep, meat byproducts, except fat 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 52011, Sept. 1, 2006, as amended at 74 FR 66579, Dec. 16, 2009; 77 FR 32406, June 1, 2012]

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§180.591 Trifloxysulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide trifloxysulfuron, N-[[(4,6-dimethoxy-2-pyrimidinyl)

amino]carbonyl]-3-(2,2,2-trifluoroethoxy)-2-pyridinesulfonamide in or on the following raw agricultural commodities.

Commodity Parts per million

Almond 0.02

Almond, hulls 0.01

Fruit, citrus, Group 10 0.03

Cotton, undelinted seed 0.05

Cotton, gin byproducts 1.0

Sugarcane 0.01

Tomato 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 54386, Sept. 17, 2003]

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§180.592 Butafenacil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo2-(2-propenyloxy)ethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate) in or on 

the following raw agricultural commodities: 

Commodity Parts per million

Cotton, gin byproducts 10 

Cotton, undelinted seed 0.50

(2) Tolerances are established for residues of the herbicide butafenacil, (1,1-dimethyl-2-oxo-2-(2-propenyloxy)ethyl 

2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate) and its metabolite CGA-293731 

(1-carboxy-1-methylethyl 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl] benzoate), in or 

on the following livestock commodities:

Commodity Parts per million

Cattle, kidney 0.05 

Cattle, liver 0.50 

Goat, kidney 0.05

Goat, liver 0.50

Hog, kidney 0.05

Hog, liver 0.50 

Horse, kidney 0.05

Horse, liver 0.50

Sheep, kidney 0.05 

Sheep, liver 0.50

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[68 FR 54827, Sept. 19, 2003]

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§180.593 Etoxazole; tolerances for residues.

(a) General. Tolerances are established for residues of etoxazole, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only etoxazole (2-(2,6-difluorophenyl)-4-[4-(1,1-dimethylethyl)-2-ethoxyphenyl]-4,5-dihydrooxazole) in or on the 

commodity.

Commodity Parts per million 

Almond, hulls 2.0

Apple, wet pomace 0.50 

Avocado 0.20

Berry, low growing, subgroup 13-07G 0.50

Caneberry subgroup 13-07A 1.5

Canistel 0.20

Cattle, fat 0.02 

Cattle, liver 0.01

Corn, field, forage 0.80

Corn, field, grain 0.01

Corn, field, refined oil 0.03

Corn, field, stover 4.0

Corn, pop, grain 0.01

Corn, pop, stover 4.0

Cotton, gin byproducts 1.0 

Cotton, undelinted seed 0.05 

Fruit, pome, group 11 0.20 

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.50

Fruit, stone, group 12, except plum 1.0

Goat, fat 0.02 

Goat, liver 0.01 

Grape, raisin 1.5 

Hop, dried cones 7.0 

Horse, fat 0.02 

Horse, liver 0.01 

Mango 0.20

Melon subgroup 9A 0.20

Milk, fat 0.01 

Nut, tree, group 14 0.01 

Papaya 0.20

Pepper/eggplant subgroup 8-10B 0.20

Peppermint, oil 20

Peppermint, tops 10

Pistachio 0.01 

Plum 0.15

Plum, prune, dried 0.30

Sapodilla 0.20

Sapote, black 0.20

Sapote, mamey 0.20

Sheep, fat 0.02 

Sheep, liver 0.01 

Spearmint, oil 20

Spearmint, tops 10

Squash/cucumber subgroup 9B 0.02

Star apple 0.20

Tangerine1 0.10 

Tea, dried* 15

Tomato 0.20

1

There are no U.S. registrations for use of etoxazole on tangerines as of September 26, 2003.

*There are currently no U.S. registrations for tea as of April 13, 2011.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect and inadvertant residues. [Reserved]

[68 FR 55493, Sept. 26, 2003, as amended at 70 FR 41625, July 20, 2005; 72 FR 72963, Dec. 26, 2007; 74 FR 25160, May 27, 

2009; 76 FR 20542, Apr. 13, 2011; 77 FR 3621, Jan. 25, 2012]

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§180.594 Thiacloprid; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide thiacloprid, including its metabolites and 

degradates in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only thiacloprid ([3-[(6-chloro-3-pyridinyl)methyl]-2-thiazolidinylidene] cyanamide) 

in or on the commodity.

Commodity Parts per million 

Apple, wet pomace 0.60 

Cattle, fat 0.020 

Cattle, kidney 0.050 

Cattle, liver 0.15 

Cattle, meat 0.030 

Cattle, meat byproducts 0.050 

Cherry subgroup 12-12A 0.5

Cotton, gin byproducts 11.0 

Cotton, undelinted seed 0.020 

Fruit, pome, group 11 0.30 

Goat, fat 0.020 

Goat, kidney 0.050 

Goat, liver 0.15 

Goat, meat 0.030 

Goat, meat byproducts 0.050 

Horse, fat 0.020 

Horse, kidney 0.050 

Horse, liver 0.15 

Horse, meat 0.030 

Horse, meat byproducts 0.050 

Milk 0.030 

Peach subgroup 12-12B 0.5

Pepper 1.0

Plum subgroup 12-12C 0.05

Sheep, fat 0.020 

Sheep, kidney 0.050 

Sheep, liver 0.15 

Sheep, meat 0.030 

Sheep, meat byproducts 0.050

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 55512, Sept. 26, 2003, as amended at 78 FR 8416, Feb. 6, 2013]

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§180.595 Flufenpyr-ethyl; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide, flufenpyr-ethyl; acetic acid, [2-chloro-4-

fluoro-5-[5-methyl-6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], in or on the following commodities: 

Commodity Parts per million

Corn, field, grain 0.01

Soybean, seed 0.01

Sugarcane, cane 0.01

(2) Tolerances are established for residues of the herbicide flufenpyr-ethyl; acetic acid, [2-chloro-4-fluoro-5-[5-methyl6-oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-ethyl ester], and its metabolite, S-3153 acid-4-OH; [2-chloro-4-

hydroxy-5-[5-methyl-6- oxo-4-(trifluoromethyl)-1-(6H)-pyridazinyl]-phenoxy]-acetic acid, free and conjugated, in or on the 

following commodities: 

Commodity Parts per million

Corn, field, forage 0.05

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Corn, field, stover 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved] 

(d) Indirect or inadvertent residues. [Reserved]

[68 FR 54842, Sept. 19, 2003]

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§180.596 Fosthiazate; tolerances for residues.

(a) General. A tolerance is established for residues of the insecticide fosthiazate, including its metabolites and 

degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this 

paragraph is to be determined by measuring only the sum of fosthiazate, O-ethyl S-(1-methylpropyl)(2-oxo-3-thiazolidinyl)

phosphonothioate, and its metabolite, O-ethyl S-(1-methylpropyl)(2-(methylsulfonyl)ethyl)phosphoramidothioate, 

calculated as the stoichiometric equivalent of fosthiazate, in or on the commodity.

Commodity Parts per million

Tomato 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 18275, Apr. 7, 2004, as amended at 76 FR 23498, Apr. 27, 2011]

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§180.597 Mesosulfuron-methyl; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide mesosulfuron-methyl, (methyl 

2-[[[[(4,6-dimethoxy-2-pyrimidinyl) amino]carbonyl]amino]sulfonyl] -4-[[(methylsulfonyl)amino] methyl]benzoate]) in or on 

the following raw agricultural commodities:

Commodity Parts per million

Cattle, meat byproducts 0.01

Goat, meat byproducts 0.01

Grain, aspirated fractions 0.60

Horse, meat byproducts 0.01

Sheep, meat byproducts 0.01

Wheat, forage 0.60

Wheat, germ 0.10

Wheat, grain 0.03

Wheat, hay 0.06

Wheat, straw 0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 18263, Apr. 7, 2004]

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§180.598 Novaluron; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide novaluron, including its metabolites and 

degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table is to 

be determined by measuring only novaluron, (N-[[[3-chloro-4-[1,1,2-trifluoro-2- (trifluoromethoxy)ethoxy]phenyl]amino]

carbonyl]-2,6-difluorobenzamide), in or on the following raw agricultural commodities:

Commodity

Parts per 

million

Apple, wet pomace 8.0

Avocado 0.60

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Bean, dry, seed 0.30

Bean, succulent 0.70

Berry, low growing, subgroup 13-07G, except lowbush blueberry 0.45

Brassica, head and stem, subgroup 5A 0.50

Brassica, leafy greens, subgroup 5B 25

Bushberry subgroup 13-07B 7.0

Carrot 0.05

Cattle, fat 11

Cattle, kidney 1.0

Cattle, liver 1.0

Cattle, meat 0.60

Cattle, meat byproducts, except kidney and liver 11

Cherry subgroup 12-12A 8.0

Corn, sweet, forage 16

Corn, sweet, kernel plus cob with husks removed 0.05

Corn, sweet, stover 50

Cotton, gin byproducts 30

Cotton, undelinted seed 0.60

Egg 1.5

Food commodities and feed commodities (other than those covered by a higher tolerance as a result of use on growing crops) in food and 

feed handling establishments

0.01

Fruit, pome, group 11-10 3.0

Goat, fat 11

Goat, kidney 1.0

Goat, liver 1.0

Goat, meat 0.60

Goat, meat byproducts, except kidney and liver 11

Grain, aspirated fractions 25

Hog, fat 1.5

Hog, kidney 0.10

Hog, liver 0.10

Hog, meat 0.07

Hog, meat byproducts, except kidney and liver 1.5

Horse, fat 11

Horse, kidney 1.0

Horse, liver 1.0

Horse, meat 0.60

Horse, meat byproducts, except kidney and liver 11

Milk 1.0

Milk, fat 20

Peach subgroup 12-12B 1.9

Peanut 0.01

Plum, prune, dried 3.0

Plum subgroup 12-12C 1.9

Poultry, fat 7.0

Poultry, kidney 0.80

Poultry, liver 0.80

Poultry, meat 0.40

Poultry, meat byproducts, except kidney and liver 7.0

Sheep, fat 11

Sheep, kidney 1.0

Sheep, liver 1.0

Sheep, meat 0.60

Sheep, meat byproducts, except kidney and liver 11

Sorghum, grain, forage 6.0

Sorghum, grain, grain 3.0

Sorghum, grain, stover 40

Soybean, seed 0.07

Sugarcane, cane 0.50

Swiss chard 12

Turnip, greens 25

Vegetable, cucurbit, group 9 0.20

Vegetable, fruiting, group 8-10 1.0

Vegetable, tuberous and corm, subgroup 1C 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

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[69 FR 31021, June 2, 2004, as amended at 71 FR 17014, Apr. 5, 2006; 71 FR 61911, Oct. 20, 2006; 73 FR 74982, Dec. 10, 2008; 

74 FR 637, Jan. 7, 2009; 74 FR 20891, May 6, 2009; 74 FR 65033, Dec. 9, 2009; 75 FR 4278, Jan. 27, 2010; 75 FR 29447, May 26, 

2010; 76 FR 55814, Sept. 9, 2011; 78 FR 40033, July 3, 2013; 80 FR 43335, July 22, 2015]

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§180.599 Acequinocyl; tolerances for residues.

(a) General. Tolerances are established for residues of acequinocyl, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of acequinocyl [2-(acetyloxy)-3-dodecyl-1,4-naphthalenedione] and its metabolite, 2-dodecyl-3-

hydroxy-1,4-naphthoquinone, calculated as the stoichiometric equivalent of acequinocyl, in or on the commodity.

Commodity Parts per million

Almond, hulls 2.0

Apple, wet pomace 1.0

Bean, edible podded 0.25

Bean, succulent shelled 0.30

Berry, low growing, subgroup 13-07G 0.50

Caneberry subgroup 13-07A 4.0

Cattle, fat 0.02

Cattle, meat byproducts 0.02

Cherry, sweet 0.50

Cherry, tart 1.0

Citrus, oil 30

Cowpea, forage 6.0

Cowpea, hay 18

Cucumber 0.15

Fruit, citrus, group 10 0.20

Fruit, pome, group 11 0.40

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.6

Goat, fat 0.02

Goat, meat byproducts 0.02

Hop, dried cones 4.0

Horse, fat 0.02

Horse, meat byproducts 0.02

Melon subgroup 9A 0.15

Nut, tree, group 14 0.02

Okra 0.70

Pistachio 0.02

Sheep, fat 0.02

Sheep, meat byproducts 0.02

Soybean, vegetable, succulent 0.25

Vegetable, fruiting, group 8 0.70

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 43533, July 21, 2004, as amended at 73 FR 17910, Apr. 2, 2008; 75 FR 70148, Nov. 17, 2010; 77 FR 25909, May 2, 2012]

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§180.600 Propoxycarbazone; tolerances for residues.

(a) General. (1) Tolerances are established for combined residues of the herbicide propoxycarbazone methyl 

2-[[[(4,5-dihydro-4-methyl-5-oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate and its metabolite 

methyl 2-[[[(4,5-dihydro-3-(2-hydroxypropoxy)-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on 

the following raw agricultural commodities:

Commodity Parts per million

Grass, forage 20

Grass, hay 25

Wheat, forage 17

Wheat, grain 0.02

Wheat, hay 0.15

Wheat, straw 0.05

(2) Tolerances are established for residues of the herbicide propoxycarbazone methyl 2-[[[(4,5-dihydro-4-methyl-5-

oxo-3-propoxy-1H-1,2,4-triazol-1-yl)carbonyl]amino]sulfonyl]benzoate in/on the following raw agricultural commodities:

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Commodity Parts per million

Cattle, meat 0.05

Cattle, meat byproducts 0.3

Goat, meat 0.05

Goat, meat byproducts 0.3

Horse, meat 0.05

Horse, meat byproducts 0.3

Milk 0.03

Sheep, meat 0.05

Sheep, meat byproducts 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 40781, July 7, 2004, as amended at 71 FR 52487, Sept. 6, 2006; 74 FR 9377, Mar. 4, 2009]

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§180.601 Cyazofamid; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide cyazofamid, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only the sum of 4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole1-sulfonamide and its metabolite, 4-chloro-5-(4-methylphenyl)-1H-imidazole-2-carbonitrile, calculated as the stoichiometric 

equivalent of cyazofamid, in or on the following commodities:

Commodity Parts per million

Basil, dried leaves 90 

Basil, fresh leaves 30 

Bean, succulent 0.5 

Bean, succulent shelled 0.08 

Brassica, head and stem, subgroup 5A 1.2

Brassica, leafy greens, subgroup 5B 12.0

Carrot, roots 0.09

Hop dried cones 10.0

Leafy greens subgroup 4A 10 

Turnip, greens 12.0

Vegetable, cucurbit, group 9 0.10

Vegetable, fruiting, group 8-10 0.9 

Vegetable, tuberous and corm, subgroup 1C 0.02

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fungicide 

cyazofamid, including its metabolites and degradates, in or on the commodities in the following table. Compliance with the 

tolerance levels specified in the following table is to be determined by measuring only the sum of cyazofamid, 4-chloro-2-

cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite CCIM, 4-chloro-5-(4-methylphenyl)

-1H-imidazole-2-carbonitrile, calculated as the stoichiometric equivalent of cyazofamid, resulting from use of the pesticide 

under FIFRA section 18 emergency exemptions. The tolerances expire and are revoked on the date specified in the table.

Commodity Parts per million Expiration/revocation date

Basil, dried 144 12/31/14 

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

fungicide cyazofamid, including its metabolites and degradates, in or on the commodities in the following table. 

Compliance with the tolerance levels specified in the following table is to be determined by measuring only the sum of 

4-chloro-2-cyano-N,N-dimethyl-5-(4-methylphenyl)-1H-imidazole-1-sulfonamide and its metabolite, 4-chloro5-(4-methylphenyl)-1H-imidazole-2-carbonitrile, calculated as the stoichiometric equivalent of cyazofamid, in or on the 

following commodities:

Commodity Parts per million

Grape 1.5

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 58299, Sept. 30, 2004, as amended at 73 FR 21839, Apr. 23, 2008; 74 FR 32453, July 8, 2009; 75 FR 40751, July 14, 2010; 

77 FR 4252, Jan. 27, 2012; 77 FR 59119, Sept. 26, 2012]

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§180.602 Spiroxamine; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of the fungicide spiroxamine, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only spiroxamine, [(8-(1,1-dimethylethyl)-N-ethyl-N-propyl-1,4-dioxaspiro[4,5]

decane-2-methanamine) in or on the commodities.

Commodity Parts per million 

Artichoke, globe, import1 0.7 

Asparagus1 0.05 

Banana (import) 3.0 

Grape (import) 1.0 

Hop, dried cones 50

Vegetable, fruiting , crop group 81 1.2 

1

No U.S. registration as of December 1, 2010.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 42570, July 16, 2004, as amended at 75 FR 74640, Dec. 1, 2010]

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§180.603 Dinotefuran; tolerances for residues.

(a) General. (1) Tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)

methyl)guanidine, including its metabolites and degradates, in or on the commodities listed in the following table. 

Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran and its 

metabolites DN, 1-methyl-3-(tetrahydro-3-furylmethyl)guanidine, and UF, 1-methyl-3-(tetrahydro-3-furylmethyl)urea, 

calculated as the stoichiometric equivalent of dinotefuran, in or on the commodities listed in the table below:

Commodity Parts per million

Berry, low growing, except strawberry, subgroup 13-07H 0.2

Brassica, head and stem, subgroup 5A 1.4

Brassica, leafy greens, subgroup 5B 15.0

Cotton, undelinted seed 0.4

Cotton, gin byproducts 8.0

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.9

Grape, raisin 2.5

Onion, bulb, subgroup 3-07A 0.15

Onion, green, subgroup 3-07B 5.0

Peach 1.0

Potato, chips 0.1

Potato, granules/flakes 0.15

Rice, grain 9.0

Tea, dried1 50

Tomato, paste 1.0

Turnip, greens 15.0

Vegetable, fruiting, group 8 0.7

Vegetable, cucurbit, group 9 0.5

Vegetable, leafy, except Brassica, group 4 5.0

Vegetable, tuberous and corm, subgroup 1C 0.05

Watercress 8.0

1

There are no U.S. registrations for tea.

(2) Tolerances are established for residues of dinotefuran, (RS)-1-methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)

guanidine, including its metabolites and degradates, in or on the commodities listed in the following table. Compliance with 

the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran, (RS)-1-methyl-2-nitro3-((tetrahydro-3-furanyl)methyl)guanidine in or on the commodities listed in the table below:

Commodity Parts per million

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.05

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Egg 0.01

Goat, fat 0.05

Goat, meat 0.05

Goat, meat byproducts 0.05

Hog, fat 0.05

Hog, meat 0.05

Hog, meat byproducts 0.05

Horse, fat 0.05

Horse, meat 0.05

Horse, meat byproducts 0.05

Milk 0.05

Poultry, meat byproducts 0.01

Sheep, fat 0.05

Sheep, meat 0.05

Sheep, meat byproducts 0.05

(3) A tolerance of 0.01 parts per million is established for residues of the insecticide dinotefuran, (RS)-1-methyl-2-

nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on all food and/or feed 

commodities (other than those covered by a higher tolerance as a result of use on growing crops or inadvertent residues) 

when residues result from application of dinotefuran in food and/or feed handling establishments where food and/or feed 

products are held, stored, processed, prepared, or served. Compliance with the tolerance level is to be determined by 

measuring only dinotefuran.

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of dinotefuran, (RS)-1-

methyl-2-nitro-3-((tetrahydro-3-furanyl)methyl)guanidine, including its metabolites and degradates, in or on the 

commodities in the table below resulting from use of the pesticide pursuant to FIFRA section 18 emergency exemptions. 

Compliance with the tolerance levels specified below is to be determined by measuring only the sum of dinotefuran and its 

metabolites DN, 1-methyl-3-(tetrahydro-3-furylmethyl)guanidine, and UF, 1-methyl-3-(tetrahydro-3-furylmethyl)urea, 

calculated as the stoichiometric equivalent of dinotefuran, in or on the commodities listed in the table below. The 

tolerances expire and are revoked on the dates specified in the table.

Commodity Parts per million

Expiration/

revocation

date

Fruit, pome, Group 11 2.0 12/31/15

Fruit, stone, Group 12 2.0 12/31/15

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 14546, Mar. 23, 2005, as amended at 74 FR 12601, Mar. 25, 2009; 74 FR 67104, Dec. 18, 2009; 75 FR 770, Jan. 6, 2010; 

77 FR 56138, Sept. 12, 2012; 77 FR 67285, Nov. 9, 2012; 77 FR 70913, Nov. 28, 2012; 78 FR 21272, Apr. 10, 2013; 78 FR 24683, 

Apr. 26, 2013; 79 FR 3512, Jan. 22, 2014]

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§180.604 Mepanipyrim; tolerances for residues.

(a) General. [Reserved]

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect of inadvertent residues. [Reserved]

(e) Revoked tolerances subject to the channel of trade provisions. [Reserved]

(f) Import tolerances. Tolerances are established for the combined residues of mepanipyrim, 4-methyl-N-phenyl6-(1-propynyl)-2-pyrimidinamine, and its metabolite, 4-methyl-N-phenyl-6-(2-hydroxypropylk)-2-pyrimidinamine, both free 

and conjugated in or on the following commodities:

Commodity Parts per million

Grape 1.5

Grape, raisin 3.0

Strawberry 1.5

Tomato 0.5

[68 FR 60827, Oct. 13, 2004]

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§180.605 Penoxsulam; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for the herbicide, penoxsulam (2-(2,2-difluoroethoxy)-N-(5,8-dimethoxy[1,2,4] 

triazolo[1,5-c]pyrimidin-2-yl)-6-(trifluoromethyl)benzenesulfonamide) in/on the following raw agricultural commodities:

Commodity Parts per million

Almond, hulls 0.01 

Fish 0.01

Fish, shellfish, crustacean 0.01

Fish, shellfish, mollusc 0.02

Grape 0.01 

Nut, tree, group 14 0.01 

Pistachio 0.01 

Rice, grain 0.02

Rice, straw 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[69 FR 57197, Sept. 24, 2004, as amended at 72 FR 40763, July 25, 2007; 74 FR 18648, Apr. 24, 2009]

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§180.607 Spiromesifen; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide/miticide spiromesifen, including its 

metabolites and degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below 

is to be determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en4-yl 3,3-dimethylbutanoate] and 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one, calculated as the 

stoichiometric equivalent of spiromesifen, in or on the following primary crop commodities:

Commodity Parts per million

Bean, dry 0.02

Bean, edible podded 0.80

Bean, succulent 0.10

Berry and small fruit, low growing berry, subgroup 13-07G 2.0

Brassica, head and stem, subgroup 5A 2.0

Brassica, leafy greens, subgroup 5B 12

Corn, field, forage 5.0

Corn, field, grain 0.02

Corn, field, stover 8.0

Corn, pop, grain 0.02

Corn, pop, stover 4.0

Corn, sweet, forage 17

Corn, sweet, kernel plus cob with husks removed 0.02

Corn, sweet, stover 12

Cotton, gin byproducts 15

Cotton, undelinted seed 0.50

Cowpea, forage 30

Cowpea, hay 86

Leaf petiole subgroup 4B 6.0

Leafy greens subgroup 4A 12

Pea, dry, seed 0.20

Peppermint, tops 45

Spearmint, tops 45

Tea, dry 40

Tomato, paste 0.80

Vegetable, cucurbit, group 9 0.10

Vegetable, fruiting, group 8 0.45

Vegetable, tuberous and corm, subgroup 1C 0.02

(2) Tolerances are established for residues of the insecticide/miticide spiromesifen, including its metabolites and 

degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 

3,3-dimethylbutanoate] and its metabolites containing the 4-hydroxy-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-

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one and 4-hydroxy-3-[4-(hydroxymethyl)-2,6-dimethylphenyl]-1-oxaspiro[4.4]non-3-en-2-one moieties, calculated as the 

stoichiometric equivalent of spiromesifen, in the following livestock commodities:

Commodity Parts per million

Cattle, fat 0.10

Cattle, meat 0.02

Cattle, meat byproducts 0.20 

Goat, fat 0.10

Goat, meat 0.02

Goat, meat byproducts 0.20

Horse, fat 0.10

Horse, meat 0.02

Horse, meat byproducts 0.20

Milk 0.01

Milk, fat 0.25

Sheep, fat 0.10

Sheep, meat 0.02

Sheep, meat byproducts 0.20

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

residues of the insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed 

below. Compliance with the tolerance levels specified below is to be determined by measuring only the sum of 

spiromesifen [2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate] and 4-hydroxy3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-2-one, calculated as the stoichiometric equivalent of spiromesifen, in or 

on the specified agricultural commodities, resulting from use of the pesticide pursuant to FIFRA section 18 emergency 

exemptions. The tolerances expire and are revoked on the date specified in the table.

Commodity Parts per million Expiration/revocation date

Soybean, forage 30 12/31/14

Soybean, hay 86 12/31/14

Soybean, seed 0.02 12/31/14

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the inadvertent or indirect residues of the 

insecticide/miticide spiromesifen, including its metabolites and degradates, in or on the commodities listed below. 

Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spiromesifen 

[2-oxo-3-(2,4,6-trimethylphenyl)-1-oxaspiro[4.4]non-3-en-4-yl 3,3-dimethylbutanoate], 4-hydroxy-3-(2,4,6-trimethylphenyl)

-1-oxaspiro[4.4]non-3-en-2-one, and its metabolites containing the 4-hydroxy-3-[4-(hydroxymethyl)-2,6-dimethylphenyl]-1-

oxaspiro[4.4]non-3-en-2-one moiety, calculated as the stoichiometric equivalent of spiromesifen, in the following rotational 

crop commodities:

Commodity Parts per million

Alfalfa, forage 1.5

Alfalfa, hay 3.0

Barley, grain 0.03

Barley, hay 0.25

Barley, straw 0.15

Beet, sugar, roots 0.03

Beet, sugar, tops 0.20

Oat, forage 0.20

Oat, grain 0.03

Oat, hay 0.25

Oat, straw 0.25

Vegetable, bulb, group 3-07 0.09

Wheat, forage 0.20

Wheat, grain 0.03

Wheat, hay 0.15

Wheat, straw 0.25

[70 FR 43283, July 27, 2005, as amended at 72 FR 3079, Jan. 24, 2007; 73 FR 13140, Mar. 12, 2008; 73 FR 52606, Sept. 10, 2008; 

74 FR 8492, Feb. 25, 2009; 74 FR 15886, Apr. 8, 2009; 75 FR 5526, Feb. 3, 2010; 75 FR 53586, Sept. 1, 2010; 76 FR 81396, Dec. 

28, 2011; 78 FR 3337, Jan. 16, 2013]

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§180.608 Spirodiclofen; tolerances for residues.

(a) General. (1) Tolerances are established for residues of spirodiclofen, including its metabolites and degradates, in 

or on the commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only 

spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate).

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Commodity Parts per million

Almond, hulls 20.0

Apple, wet pomace 2.4

Avocado 1.0

Black sapote 1.0

Canistel 1.0

Citrus, juice 0.60

Citrus, oil 35

Fruit, citrus, group 10 0.50

Fruit, pome, group 11 0.80

Fruit, stone, group 12 1.0

Grape 2.0

Grape, raisin 6.0

Hop, dried cones 30

Mamey sapote 1.0

Mango 1.0

Nut, tree, group 14 0.10

Papaya 1.0

Pistachio 0.10

Sapodilla 1.0

Star apple 1.0

(2) Tolerances are established for residues of spirodiclofen, including its metabolites and degradates, in or on the 

commodities listed below. Compliance with the following tolerance levels is to be determined by measuring only 

spirodiclofen (3-(2,4-dichlorophenyl)-2-oxo-1-oxaspiro[4.5]dec-3-en-4-yl 2,2-dimethylbutanoate) and its metabolite 

3-(2,4-dichlorophenyl)-4-hydroxy-1-oxaspiro[4,5] dec-3-en-2-one, calculated as the stoichiometric equivalent of 

spirodiclofen.

Commodity Parts per million

Cattle, fat 0.02

Cattle, meat byproducts 0.10

Cattle, meat 0.02

Goat, fat 0.02

Goat, meat byproducts 0.1

Goat, meat 0.02

Horse, fat 0.02

Horse, meat byproducts 0.1

Horse, meat 0.02

Milk 0.01

Milk, fat 0.03

Sheep, fat 0.02

Sheep. meat byproducts 0.1

Sheep. meat 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 40211, July 13, 2005, as amended at 73 FR 25539, May 7, 2008; 75 FR 24434, May 5, 2010; 77 FR 73939, Dec. 12, 2012; 

79 FR 33464, June 11, 2014]

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§180.609 Fluoxastrobin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of fluoxastrobin, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin3-yl)methanone O-methyloxime and its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl]

(5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, calculated as the stoichiometric equivalent of fluoxastrobin.

Commodity Parts per million

Berry, low growing, subgroup 13-07G 1.9

Corn, field, forage 3.0

Corn, field, grain 0.02

Corn, field, stover 4.5

Corn, sweet, forage 13

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 10

Grain, aspirated grain fractions 60

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Leaf petioles subgroup 4B 4.0

Melon subgroup 9A 1.5

Peanut 0.02

Peanut, hay 20.0

Peanut, refined oil 0.06

Rice, grain 4.0

Sorghum, grain, forage 5.0

Sorghum, grain, grain 1.5

Sorghum, grain, stover 5.0

Soybean, forage 9.0

Soybean, hay 1.2

Soybean, hulls 0.20

Soybean, seed 0.05

Squash/cucumber subgroup 9B 0.50

Tomato, paste 1.5

Vegetable, fruiting, group 8 1.0

Vegetable, tuberous and corm, subgroup 1C 0.010

Wheat, forage 7.0

Wheat, grain 0.15

Wheat, hay 17

Wheat, straw 11

(2) Tolerances are established for residues of fluoxastrobin, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only fluoxastrobin, (1E)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)

methanone O-methyloxime, its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl]

(5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime, and its phenoxy-hydroxypyrimidine, 6-(2-chlorophenoxy)-5-

fluoro-4-pyrimidinol, calculated as the stoichiometric equivalent of fluoxastrobin.

Commodity Parts per million

Cattle, fat 0.10

Cattle, meat 0.05

Cattle, meat byproducts 0.20

Goat, fat 0.10

Goat, meat 0.05

Goat, meat byproducts 0.20

Hog, fat 0.03

Hog, meat byproducts 0.06

Horse, fat 0.10

Horse, meat 0.05

Horse, meat byproducts 0.20

Milk 0.03

Milk, fat 0.75

Poultry, liver 0.06

Sheep, fat 0.10

Sheep, meat 0.05

Sheep, meat byproducts 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of 

fluoxastrobin, including its metabolites and degradates, in or on the commodities in the table below, when present therein 

as a result of the application of fluoxastrobin to the growing crops listed in paragraph (a)(1) of this section. Compliance 

with the tolerance levels specified below is to be determined by measuring only fluoxastrobin, (1E)

-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone O-methyloxime and 

its Z isomer, (1Z)-[2-[[6-(2-chlorophenoxy)-5-fluoro-4-pyrimidinyl]oxy]phenyl](5,6-dihydro-1,4,2-dioxazin-3-yl)methanone 

O-methyloxime, calculated as the stoichiometric equivalent of fluoxastrobin.

Commodity Parts per million

Alfalfa, forage 0.050

Alfalfa, hay 0.10

Cotton, gin byproducts 0.020

Grain, cereal, forage, fodder, and straw, group 16, except corn 0.10

Grass, forage 0.10

Grass, hay 0.50

Vegetable, foliage of legume, group 7 0.050

[74 FR 67113, Dec. 18, 2009, as amended at 75 FR 60333, Sept. 30, 2010; 76 FR 50898, Aug. 17, 2011; 77 FR 26471, May 4, 

2012; 77 FR 64915, Oct. 24, 2012; 79 FR 20105, Apr. 11, 2014; 79 FR 59119, Oct. 1, 2014]

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§180.610 Aminopyralid; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide aminopyralid, 4-amino-3,6-dichloro-2-

pyridinecarboxylic acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance 

with the tolerance levels specified below is to be determined by measuring only free and conjugated aminopyralid.

Commodity Parts per million

Corn, field, forage 0.30

Corn, field, grain 0.20

Corn, field, stover 0.20

Grain, aspirated fractions 0.2

Grass, forage 25

Grass, hay 50

Wheat, bran 0.1

Wheat, forage 2.0

Wheat, grain 0.04

Wheat, hay 4.0

Wheat, straw 0.25

(2) Tolerances are established for residues of the herbicide aminopyralid, 4-amino-3,6-dichloro-2-pyridinecarboxylic 

acid, including its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance 

levels specified below is to be determined by measuring only aminopyralid.

Commodity Parts per million

Cattle, fat 0.02

Cattle, kidney 0.3

Cattle, meat 0.02

Cattle, meat byproducts, except kidney 0.02

Goat, fat 0.02

Goat, kidney 0.3

Goat, meat 0.02

Goat, meat byproducts, except kidney 0.02

Horse, fat 0.02

Horse, kidney 0.3

Horse, meat 0.02

Horse, meat byproducts, except kidney 0.02

Milk 0.03

Sheep, fat 0.02

Sheep, kidney 0.3

Sheep, meat 0.02

Sheep, meat byproducts, except kidney 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 46428, Aug. 10, 2005, as amended at 75 FR 17584, Apr. 7, 2010]

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§180.611 Pinoxaden; tolerances for residues.

(a) General. (1) Tolerances are established for the combined residues of pinoxaden (8-(2,6-diethyl-4-methylphenyl)

-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo[1,2-d][1,4,5] oxadiazepin-9-yl 2,2-dimethylpropanoate), and its metabolites 

8-(2,6-diethyl-4-methyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione (M2), and free and conjugated 

forms of 8-(2,6-diethyl-4-hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione (M4), and 

4-(7,9-dioxo-hexahydro-pyrazolo[1,2-d] [1,4,5]oxadiazepin-8-yl)-3,5-diethyl-benzoic acid (M6), calculated as pinoxaden, 

in/on the following commodities:

Commodity Parts per million

Barley, bran 1.6

Barley, grain 0.9

Barley, hay 1.5

Barley, straw 1.0

Egg 0.06

Poultry, fat 0.06

Poultry, meat 0.06

Poultry, meat byproducts 0.06

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Wheat, bran 3.0

Wheat, forage 3.5

Wheat, grain 1.3

Wheat, hay 2.0

Wheat, straw 1.5

(2) For the combined residues of pinoxaden, 8-(2,6-diethyl-4-methylphenyl)-1,2,4,5-tetrahydro-7-oxo-7H-pyrazolo

[1,2-d][1,4,5] oxadiazepin-9-yl 2,2-dimethylpropanoate), and its metabolites M2, 8-(2,6-diethyl-4-methyl-phenyl)

-tetrahydro-pyrazolo[1,2-d][1,4,5]oxadiazepine-7,9-dione, and free and conjugated forms of M4, 8-(2,6-diethyl-4-

hydroxymethyl-phenyl)-tetrahydro-pyrazolo[1,2-d][1,4,5] oxadiazepine-7,9-dione, calculated as pinoxaden, in/on the 

following commodities:

Commodity Parts per million

Cattle, fat 0.04

Cattle, meat 0.04

Cattle, meat byproducts 0.04

Milk 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 43322, July 27, 2005]

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§180.612 Topramezone; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide topramezone, including its metabolites and 

degradates, in or on the following commodities. Compliance with the following tolerance levels is to be determined by 

measuring only topramezone ([3-(4,5-dihydro-3-isoxazolyl)-2-methyl-4-(methylsulfonyl)phenyl](5-hydroxy-1-methyl1H-pyrazol-4-yl)methanone) in or on the following commodities:

Commodity

Parts per

million

Cattle, meat byproducts 0.80

Corn, field, forage 0.05

Corn, field, grain 0.01

Corn, field, stover 0.05

Corn, pop, grain 0.01

Corn, pop, stover 0.05

Corn, sweet, forage 0.05

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.05

Fish-freshwater finfish 0.05

Fish-saltwater finfish 0.05

Fish-shellfish, crustacean 0.05

Fish-shellfish, mollusk 0.05

Goat, meat byproducts 0.80

Hog, meat byproducts 0.40

Horse, meat byproducts 0.80

Poultry, meat byproducts 0.02

Sheep, meat byproducts 0.80

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 48074, Aug. 7, 2013]

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§180.613 Flonicamid; tolerances for residues.

(a) General. (1) Tolerances are established for the residues of the insecticide flonicamid, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its 

metabolites, TFNA (4-trifluoromethylnicotinic acid), TFNA-AM (4-trifluoromethylnicotinamide), and TFNG, 

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N-(4-trifluoromethylnicotinoyl)glycine, calculated as the stoichiometric equivalent of flonicamid, in or on the following 

commodities. 

Commodity Parts per million

Alfalfa, forage 10.0

Alfalfa, hay 1.0

Alfalfa, seed 1.5

Almond, hulls 9.0

Berry, low growing, subgroup 13-07G 1.5 

Brassica, head and stem, subgroup 5A 1.5

Brassica, leafy greens, subgroup 5B 16

Cotton, gin byproducts 6.0

Cotton, hulls 2.0

Cotton, meal 1.0

Cotton, undelinted seed 0.50

Cucumber 1.5 

Fruit, pome, group 11-10 0.20

Fruit, stone, group 12-12 0.60

Hop, dried cones 7.0

Nut, tree, group 14-12 0.15

Okra 0.40

Peppermint, tops 7.0

Potato, granules/flakes 0.40

Radish, tops 16

Rapeseed subgroup 20A 1.5 

Spearmint, tops 7.0

Spinach 9.0

Tomato, paste 2.0

Tomato, puree 0.50

Turnip, greens 16

Vegetable, cucurbit, group 9 1.5

Vegetable, fruiting, group 8-10 0.40

Vegetable, leafy, except brassica, group 4, except spinach 4.0

Vegetable, root, except sugar beet, subgroup 1B 0.60

Vegetable, tuberous and corm, subgroup 1C 0.20

(2) Tolerances are established for the residues of the insecticide flonicamid, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of flonicamid, N-(cyanomethyl)-4-(trifluoromethyl)-3-pyridinecarboxamide, and its metabolites, 

TFNA (4-trifluoromethylnicotinic acid), and TFNA-AM (4-trifluoromethylnicotinamide), calculated as the Stoichiometric 

equivalent of flonicamid, in or on the following commodities.

Commodity Parts per million

Cattle, fat 0.03

Cattle, meat 0.08

Cattle, meat byproducts 0.08

Egg 0.04

Goat, fat 0.03

Goat, meat 0.08

Goat, meat byproducts 0.08

Hog, fat 0.03

Hog, meat 0.03

Hog, meat byproducts 0.03

Horse, fat 0.03

Horse, meat 0.08

Horse, meat byproducts 0.08

Milk 0.05

Poultry, fat 0.03

Poultry, meat 0.03

Poultry, meat byproducts 0.03

Sheep, fat 0.03

Sheep, meat 0.08

Sheep, meat byproducts 0.08

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[70 FR 51614, Aug. 31, 2005, as amended at 71 FR 15608, Mar. 29, 2006; 73 FR 17923, Apr. 2, 2008; 77 FR 67776, Nov. 14, 2012; 

78 FR 75266, Dec. 11, 2013]

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§180.614 Kasugamycin; tolerances for residues.

(a) General. Tolerances are established for residues of kasugamycin, including its metabolites and degradates, in or 

on the commodities listed in the following table. Compliance with the tolerance levels specified is to be determined by 

measuring only kasugamycin (3-O-[2-amino-4-[(carboxyimino-methyl)amino]-2,3,4,6-tetradeoxyα-D-arabino-hexopyranosyl]-D-chiro-inositol) in or on the commodity.

Commodity

Parts per

million

Fruit, pome, group 11-10 0.20

Vegetable, fruiting, group 81 0.04

1

There is no U.S. registration as of September 1, 2005.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 51497, Aug. 29, 2014]

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§180.615 Amicarbazone; tolerances for residues.

(a) General. Tolerances are established for combined residues of the herbicide, amicarbazone [4-amino-4, 5-dihydroN-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and its metabolites DA amicarbazone 

[N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and iPr-2-OH DA 

amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide], 

calculated as parent equivalents, in or on the following commodities:

Commodity Parts per million

Cattle, fat 0.01

Cattle, liver 1.0

Cattle, meat 0.01

Cattle, meat byproducts, except liver 0.10

Corn, field, forage 0.80

Corn, field, grain 0.05

Corn, field, stover 1.0

Goat, fat 0.01

Goat, liver 1.0

Goat, meat 0.01

Goat, meat byproducts, except liver 0.10

Hog, fat 0.01

Hog, liver 0.10

Hog, meat 0.01

Hog, meat byproducts, except liver 0.01

Horse, fat 0.01

Horse, liver 1.0

Horse, meat 0.01

Horse, meat byproducts, except liver 0.10

Milk 0.01

Sheep, fat 0.01

Sheep, liver 1.0

Sheep, meat 0.01

Sheep, meat byproducts, except liver 0.10

Poultry, liver 0.10

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of 

amicarbazone [4-amino-4, 5-dihydro-N-(1,1-dimethylethyl)-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-carboxamide] and 

its metabolites DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-methylethyl)-5-oxo-1H-1,2,4-triazole-1-

carboxamide] and iPr-2-OH DA amicarbazone [N-(1,1-dimethylethyl)-4,5-dihydro-3-(1-hydroxy-1-methylethyl)-5-oxo1H-1,2,4-triazole-1-carboxamide], calculated as parent equivalents, in or on the following commodities when present 

therein as a result of application of amicarbazone to the growing crops in paragraph (a) of this section:

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Commodity Parts per million

Alfalfa, forage 0.05

Alfalfa, hay 0.10

Cotton, gin byproducts 0.30

Cotton, undelinted seed 0.07

Soybean, forage 1.50

Soybean, hay 5.0

Soybean, seed 0.80

Wheat, bran 0.15

Wheat, flour 0.15 

Wheat, forage 0.50

Wheat, germ 0.15 

Wheat, grain 0.10

Wheat, hay 1.0

Wheat, middlings, 0.15 

Wheat, shorts 0.15 

Wheat, straw 0.50

[70 FR 55760, Sept. 23, 2005, as amended at 74 FR 46377, Sept. 9, 2009]

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§180.616 Fenpropimorph; tolerances for residues.

Tolerances are established for the residues of the fungicide fenpropimorph (rel-(2R,6S)-4-[3-[4-(1,1-dimethylethyl)

phenyl]-2-methylpropyl]-2,6-dimethylmorpholine) in or on the following commodity:

Commodity Parts per million

Banana* 2.0

*No U.S. registration as of February 10, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 15612, Mar. 29, 2006]

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§180.617 Metconazole; tolerances for residues.

(a) General. Tolerances are established for residues of metconazole, including its metabolites and degradates, in or 

on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by 

measuring only metconazole [5-[(4-chlorophenyl)methyl]-2,2-dimethyl-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol] as the 

sum of its cis- and trans-isomers in or on the following commodities:

Commodity

Parts per

million

Almond, hulls 4.0

Banana1 0.1

Barley, grain 2.5

Barley, hay 7.0

Barley, straw 7.0

Beet, sugar, dried pulp 0.70

Beet, sugar, molasses 0.08

Beet, sugar, roots 0.07

Bushberry subgroup 13-07B 0.40

Cattle, meat byproducts 0.04

Corn, field, forage 3.0

Corn, field, grain 0.02

Corn, field, stover 30

Corn, pop, grain 0.02

Corn, pop, stover 30

Corn, sweet, forage 3.0

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 30.0

Cotton, gin byproducts 8.0

Cotton, undelinted seed 0.25

Egg 0.04

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Fruit, stone, group 12-12 0.2

Goat, meat byproducts 0.04

Grain, aspirated grain fractions 7.0

Horse, meat byproducts 0.04

Nut, tree, group 14-12 0.04

Oat, grain 1.0

Oat, hay 17

Oat, straw 6.0

Pea and bean, dried shelled, except soybean, subgroup 6C 0.15

Peanut 0.04

Peanut, refined oil 0.05

Rapeseed subgroup 20A 0.08

Rye, grain 0.25

Rye, straw 14

Sheep, meat byproducts 0.04

Soybean, forage 3.0

Soybean, hay 6.0

Soybean, hulls 0.08

Soybean, seed 0.05

Sugarcane, cane 0.06

Sunflower subgroup 20B 0.7

Vegetable, tuberous and corn, subgroup 1C 0.04

Wheat, grain 0.15

Wheat, hay 16

Wheat, milled byproducts 0.20

Wheat, straw 18

1

No U.S. registration as of August 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 56388, Sept. 27, 2006, as amended at 71 FR 76196, Dec. 20, 2006; 73 FR 22828, Apr. 28, 2008; 74 FR 21266, May 7, 2009; 

76 FR 50904, Aug. 17, 2011; 76 FR 81396, Dec. 28, 2011; 77 FR 26456, May 4, 2012; 77 FR 66723, Nov. 7, 2012; 79 FR 12411, 

Mar. 5, 2014; 80 FR 30625. May 29, 2015]

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§180.618 Benthiavalicarb-isopropyl; tolerance for residues.

(a) General. Tolerances are established for the combined residues of benthiavalicarb-isopropyl, isopropyl[(S)-1-[[[(1R)

-1-(6-fluoro-2-benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate and isopropyl[(S)-1-[[[(1S)-1-(6-fluoro-2-

benzothiazolyl)ethyl]amino] carbonyl]-2-methylpropyl]carbamate, in or on the following raw agricultural commodities:

Commodity Parts per million

Grape, imported 0.25

Grape, raisin 1.0

Tomato 0.45

Note: There are no U.S. registrations as of July 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect of inadvertent residues. [Reserved]

[71 FR 52003, Sept. 1, 2006]

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§180.619 Epoxiconazole; tolerances for residues.

(a) General. Tolerances are established for the residues of the fungicide epoxiconazole [(rel-1-[[(2R,3S)

-3-(2-chlorophenyl)-2-(4-fluorophenyl)oxiranyl]methyl]-1H-1,2,4-triazole]) in or on the following commodities:

Commodity Parts per million

Banana* 0.5

Coffee* 0.05

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*

No U.S. Registration as of August 4, 2006

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional Registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 53989, Sept. 13, 2006]

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§180.620 Etofenprox; tolerances for residues.

(a) General. A tolerance is established for residues of the insecticide etofenprox, including its metabolites and 

degradates, in or on the commodity in the table in this paragraph. Compliance with the tolerance level specified in this 

paragraph is to be determined by measuring only etofenprox, 2-(4-ethoxyphenyl)-2-methylpropyl 3-phenoxybenzyl ether, 

in or on the commodity.

Commodity

Parts per

million

Cattle, fat 10.0

Cattle, meat 0.40

Cattle, meat byproducts 10.0

Egg 0.40

All food commodities (including feed commodities) not otherwise listed in this subsection 5.0

Goat, fat 10.0

Goat, meat 0.40

Goat, meat byproducts 10.0

Hog, fat 4.0

Hog, meat 0.20

Hog, meat byproducts 4.0

Horse, fat 10.0

Horse, meat 0.40

Horse, meat byproducts 10.0

Milk 0.60

Poultry, fat 1.0

Poultry, meat 0.01

Poultry, meat byproducts 1.0

Rice, grain 0.01

Sheep, fat 10.0

Sheep, meat 0.40

Sheep, meat byproducts 10.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 23498, Apr. 27, 2011, as amended at 78 FR 70877, Nov. 27, 2013]

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§180.621 Dithianon; tolerances for residues.

(a) General. Tolerances are established for residues of dithianon, including its metabolites and degradates, in or on 

the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only dithianon, 5, 10-dihydro-5,10-dioxonaphtho(2,3-b)-1,4-dithiin-2,3-dicarbonitrile.

Commodity

Parts per

million

Fruit, pome, group 111 5

Grape 2 3

Hop, dried cones1 100

1

No U.S. registration as of September 5, 2006.

2

No U.S. registration as of January 29, 2010.

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 5522, Feb. 3, 2010]

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§180.622 Ethaboxam; tolerances for residues.

(a) General. Tolerances are established for residues of ethaboxam, N-(cyano-2-thienylmethyl)-4-ethyl-2-(ethlyamino)

-5-thiazolecarboxamide in or on the following commodity:

Commodity Parts per million

Grape1 6.0

1

 There is no U.S. registration as of September 27, 2006

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 56392, Sept. 27, 2006]

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§180.623 Flufenoxuron; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide, flufenoxuron, 1-[4-(2-chloro-α,α,α-trifluoro-ptolyloxy)-2-fluorophenyl]-3-(2,6-difluorobenzoyl)urea, in or on the following food commodities.

Commodity Parts per million

Apple1 0.50

Cattle, fat1 4.5

Cattle, meat1 0.10

Cattle, meat byproducts1 0.50

Goat, fat1 4.5

Goat, meat1 0.10

Goat, meat byproducts1 0.50

Grape1 0.70

Grape, raisin1 2.0

Horse, fat1 4.5

Horse, meat1 0.10

Horse, meat byproducts1 0.50

Milk 0.20

Milk, fat1 4.0

Orange1 0.30

Orange, oil1 60

Pear1 0.50

Sheep, fat1 4.5

Sheep, meat1 0.10

Sheep, meat byproducts1 0.50

1

There are no U.S. registrations as of September 30, 2006.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 57436, Sept. 29, 2006]

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§180.624 Metrafenone; tolerances for residues.

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(a) General. Tolerances are established for residues of the fungicide metrafenone, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only metrafenone (3-bromo-6-methoxy-2-methylphenyl)(2,3,4-trimethoxy-6-

methylphenyl)methanone in or on the following commodities:

Commodity Parts per million

Apricot 0.70

Cherry subgroup 12-12A 2.0

Fruit, pome, group 11-10 1.5

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 4.5

Grape, raisin 17

Hop, dried cones 70

Peach subgroup 12-12B 0.70

Vegetable, cucurbit, group 9 0.50

Vegetable, fruiting, group 8-10 0.90

(b) Section 18 emergency exemption. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[71 FR 54917, Sept. 20, 2006, as amended at 75 FR 75393, Dec. 3, 2010; 79 FR 63053, Oct. 22, 2014]

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§180.625 Orthosulfamuron; tolerances for residues.

Link to an amendment published at 80 FR 72599, November 20, 2015.

(a) General. Tolerances are established for residues of orthosulfamuron 1-(4,6-dimethoxypyrimidin-2-yl)

-3-[2-(dimethylcarbamoyl)- phenylsulfamoyl] urea) per se in or on the following commodities:

Commodity Parts per million

Rice, grain 0.05

Rice, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect and inadvertant residues. [Reserved]

[72 FR 8931, Feb. 28, 2007]

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§180.626 Prothioconazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of prothioconazole, 2-[2-(1-chlorocylcopropyl)

-3-(2-chlorophenyl)-2-hydroxypropyl]-1,2-dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only prothioconazole and its metabolite prothioconazole-desthio, or α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)

methyl]-1H-1,2,4-triazole-1-ethanol, calculated as parent in or on the commodity.

Commodity

Parts per

million

Alfalfa, forage 0.02

Alfalfa, hay 0.02

Beet, sugar, roots 0.25

Berry, low growing, except strawberry, subgroup 13-07H 0.20

Bushberry, subgroup 13-07B 2.0

Corn, sweet kernel plus cob with husks removed 0.04

Grain, aspirated grain fractions 11

Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; forage 8.0

Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; hay 7.0

Grain, cereal, forage, fodder and straw, group 16, except sorghum, and rice; stover 10

Grain, cereal, forage, fodder and straw, group 16, except sorghum, straw 5.0

Grain, cereal, group 15, except sweet corn and sorghum 0.35

Pea and bean, dried shelled, except soybean, subgroup 6C 0.9

Peanut 0.02

Potato 0.02

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Rapeseed, seed 0.15

Rice, hulls 0.90

Soybean, forage 4.5

Soybean, hay 17

Soybean, seed 0.15

Vegetable, cucurbit, crop group 9 0.30

(2) Tolerances are established for residues of prothioconazole, 2-[2-(1-chlorocylcopropyl)-3-(2-chlorophenyl)-2-

hydroxypropyl]-1,2-dihydro-3H-1,2,4-triazole-3-thion, including its metabolites and degradates, in or on the commodities in 

the table below. Compliance with the tolerance levels specified below is to be determined by measuring only 

prothioconazole and its metabolites prothioconazole-desthio, or α-(1-chlorocyclopropyl)-α-[(2-chlorophenyl)methyl]

-1H-1,2,4-triazole-1-ethanol, and conjugates that can be converted to these two compounds by acid hydrolysis, calculated 

as parent in or on the commodity.

Commodity Parts per million

Cattle, fat 0.1

Cattle, meat 0.02

Cattle, meat byproducts 0.2

Goat, fat 0.1

Goat, meat 0.02

Goat, meat byproducts 0.2

Hog, meat byproducts 0.05

Horse, fat 0.1

Horse, meat 0.02

Horse, meat byproducts 0.2

Milk 0.02

Poultry liver 0.02

Sheep, fat 0.1

Sheep, meat 0.02

Sheep, meat byproducts 0.2

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 11783, Mar. 14, 2007, as amended at 73 FR 14719, Mar. 19, 2008; 74 FR 14749, Apr. 1, 2009; 74 FR 46699, Sept. 11, 

2009; 75 FR 29914, May 28, 2010; 76 FR 61592, Oct. 5, 2011; 78 FR 67052, Nov. 8, 2013]

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§180.627 Fluopicolide; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fluopicolide [2,6-dichloro-N-[[3-chloro5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide], including its metabolites and degradates, in or on the commodities in the 

table in this paragraph. Compliance with the tolerance levels specified below is to be determined by measuring only 

fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide] in or on the commodity.

Commodity Parts per million

Brassica, head and stem, subgroup 5A 5.0

Grape 2.0

Grape, raisin 6.0

Potato, processed potato waste 1.0

Vegetable, brassica (cole) leafy subgroup 5B 18

Vegetable, bulb, crop group 3-07 7.0

Vegetable, cucurbit, group 9 0.50

Vegetable, fruiting, group 8 1.60

Vegetable, leafy, except brassica, group 4 25

Vegetable, leaves of root and tuber, group 2 15.0

Vegetable root, subgroup 1A 0.15

Vegetable, tuberous and corm subgroup 1C 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide fluopicolide 

[2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide], including its metabolites and degradates, in or 

on the commodities in the table in this paragraph. Compliance with the tolerance levels specified below is to be 

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determined by measuring only fluopicolide [2,6-dichloro-N-[[3-chloro-5-(trifluoromethyl)-2-pyridinyl]methyl]benzamide] in or 

on the commodity.

Commodity

Parts per

million

Corn, field, forage 0.08

Corn, field, grain 0.01

Corn, field, stover 0.20

Wheat, aspirated grain fractions 0.07

Wheat, forage 0.20

Wheat, grain 0.02

Wheat, hay 0.50

Wheat, milled byproducts 0.07

Wheat, straw 0.50

[72 FR 14447, Mar. 28, 2007, as amended at 73 FR 5455, Jan. 30, 2008; 73 FR 30498, May 28, 2008; 76 FR 22054, Apr. 20, 2011; 

79 FR 12401, Mar. 5, 2014; 79 FR 45693, Aug. 6, 2014]

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§180.628 Chlorantraniliprole; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide chlorantraniliprole, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only chlorantraniliprole, 3-bromo-N-[4-chloro-2-methyl-6-[(methylamino)carbonyl]phenyl]

-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide.

Commodity Parts per million

Acerola 2.0

Alfalfa, seed 7.0

Almond, hulls 5.0

Animal feed, nongrass, group 18, forage 25

Animal feed, nongrass, group 18, hay 90

Apple, wet pomace 2.5

Artichoke, globe 4.0

Asparagus 13

Atemoya 4.0

Avocado 4.0

Banana 4.0

Beet, sugar, molasses 9.0

Berry, large shrub/tree, subgroup 13-07C 2.5

Berry, low growing, subgroup 13-07G 1.0

Biriba 4.0

Brassica, head and stem, subgroup 5A 4.0

Brassica, leafy greens, subgroup 5B 11

Bushberry, subgroup 13-07B 2.5

Cacao bean 0.08

Cacao bean, chocolate 1.5

Cacao bean, cocoa powder 1.5

Cacao bean, roasted bean 0.8

Cactus 13

Canistel 4.0

Cattle, fat 0.5

Cattle, meat 0.1

Cattle, meat byproducts 0.5

Cherimoya 4.0

Cherry, sweet 2.0

Cherry, tart 2.0

Citrus, dried pulp 14

Coffee, green bean 0.4

Coffee, instant 2.0

Corn, field, grain 0.04

Corn, field, milled byproducts 0.1

Corn, pop, grain 0.04

Corn, sweet, kernel plus cobs with husk removed 0.02

Cotton, gin byproduct 30

Cotton, hulls 0.40

Cottonseed subgroup 20C 0.3

Crayfish 8.0

Custard apple 4.0

Egg 0.2

Feijoa 4.0

Fig 4.0

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Fruit, caneberry, subgroup 13-07A 1.8

Fruit, citrus, group 10-10 1.4

Fruit, pome, group 11-10 1.2

Fruit, small vine climbing, subgroup 13-07F 2.5

Fruit, stone, group 12-12, except cherry, chickasaw plum, and damson plum 4.0 

Goat, fat 0.5

Goat, meat 0.1

Goat, meat byproducts 0.5

Grain, aspirated grain fractions 640

Grain, cereal, except rice and corn, group 15 6.0

Grain, cereal, forage, fodder and straw, group 16 40

Grape, raisin 5.0

Grass forage, fodder and hay, group 17 90

Guava 4.0

Herb subgroup 19A, dried leaves 90

Herb subgroup 19A, fresh leaves 25

Hog, fat 0.05

Hog, meat 0.02

Hog, meat byproducts 0.05

Hop, dried cones 90

Horse, fat 0.5

Horse, meat 0.1

Horse, meat byproducts 0.5

Ilama 4.0

Jaboticaba 2.0

Longan 4.0

Lychee 2.0

Mango 4.0

Milk 0.1

Nut, tree, group 14 0.04

Olive 4.0

Olive, oil 40

Onion, bulb, subgroup 3-07A 0.30

Onion, green, subgroup 3-07B 3.0 

Papaya 4.0 

Passionfruit 4.0 

Peanut 0.06 

Peanut, hay 90 

Peppermint, tops 9.0

Persimmon 4.0

Pineapple 1.5

Pineapple, process residue 3.0

Pistachio 0.04

Plum, chickasaw 2.0

Plum, damson 2.0

Pomegranate 4.0

Poultry, fat 0.2

Poultry, meat 0.05

Poultry, meat byproducts 0.2

Pulasan 4.0

Rambutan 4.0

Rapeseed subgroup 20A 2.0

Rice, grain 0.15

Rice, hulls 0.4

Sapodilla 4.0

Sapote, black 4.0

Sapote, mamey 4.0

Sapote, white 4.0

Sheep, fat 0.5

Sheep, meat 0.1

Sheep meat byproducts 0.5

Soursop 4.0

Spanish lime 4.0

Spearmint, tops 9.0

Spice, subgroup 19B 90 

Star apple 4.0

Starfruit 4.0

Sugar apple 4.0

Sugarcane, cane 14

Sugarcane, molasses 420

Sunflower subgroup 20B 2.0

Tea, dried 50.0

Ti, leaves 13.0

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Ti, root 0.3

Vegetable, cucurbit, group 9 0.5

Vegetable, foliage of legume, group 7 90

Vegetable, fruiting, group 8-10 1.4

Vegetable, leafy, except brassica, group 4 13

Vegetable, leaves of root and tuber, group 2 40.0

Vegetable, legume, group 6 2.0

Vegetable, root and tuber, group 1 0.30

Wax jambu 4.0

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 5532, Feb. 3, 2010, as amended at 75 FR 17566, Apr. 7, 2010; 76 FR 44821, July 27, 2011; 76 FR 59909, Sept. 28, 2011; 

77 FR 60315, Oct. 3, 2012; 77 FR 75561, Dec. 21, 2012; 78 FR 57285, Sept. 18, 2013; 79 FR 7401, Feb. 7, 2014]

EDITORIAL NOTE: At 78 FR 57285, Sept. 18, 2013, §180.628 was amended by revising the commodity “Egg” in the table in 

paragraph (a); however, no revised text was provided, so the amendment could not be incorporated. 

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§180.629 Flutriafol; tolerances for residues.

(a) General. Tolerances are established for the residues of flutriafol, [(±)-α-(2-fluorophenyl)-α-(4-fluorophenyl)

-1H-1,2,4-triazole-1-ethanol], including its metabolites and degradates in or on the following commodities. Compliance with 

the following tolerances is to be determined by measuring flutriafol only.

Commodity Parts per million

African tree nut 0.02

Almond 0.60

Almond, hull 15

Banana1 0.30

Beet sugar 0.08

Brassica, head and stem (subgroup 5A) 1.5

Brassica, leafy greens (subgroup 5B) 7.0

Brazil nut 0.02

Bur oak 0.02

Butternut 0.02

Cajou 0.02

Cashew 0.02

Castanha-do-maranhao 0.02

Cattle, fat 0.05

Cattle, liver 1.0

Cattle, meat byproducts, except liver 0.05

Cattle, muscle 0.05

Coconut 0.02

Coffee, green, bean1 0.15

Coffee, instant1 0.30

Coquito nut 0.02

Corn, field, forage 5.0

Corn, field, grain 0.01

Corn, field, refined oil 0.02

Corn, field, stover 15

Corn, pop 0.01

Corn, pop, stover 15

Cotton, gin byproducts 6.0

Cotton, undelinted seed 0.50

Dika nut 0.02

Egg 0.01

Fruit, pome, group 11-09 0.40

Fruit, stone, group 12-10 1.5

Goat, fat 0.05

Goat, liver 1.0

Goat, meat byproducts, except liver 0.05

Goat, muscle 0.05

Grain, aspirated fractions 6.0

Grape 1.5

Grape, raisin 2.4

Guiana chestnut 0.02

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Hazelnut 0.02

Heartnut 0.02

Hickory nut 0.02

Hog, fat 0.01

Hog, meat byproducts 0.05

Hog, muscle 0.01

Hop, dried cones 20

Horse, fat 0.05

Horse, liver 1.0

Horse, meat byproducts, except liver 0.05

Horse, muscle 0.05

Japanese horse-chestnut 0.02

Lettuce, head 1.5

Macadamia nut 0.02

Milk 0.02

Mongongo nut 0.02

Monkey-pot 0.02

Pachira nut 0.02

Peanut 0.09

Peanut, hay 15

Pecan 0.02

Poultry, fat 0.01

Poultry, meat byproducts 0.01

Radicchio 1.5

Sapucaia nut 0.02

Sheep, fat 0.05

Sheep, liver 1.0

Sheep, meat byproducts, except liver 0.05

Sheep, muscle 0.05

Sorghum, grain, forage 2.0

Sorghum, grain, grain 1.5

Sorghum, grain, stover 6.0

Soybean, seed 0.35

Strawberry 1.5

Tomato, paste 1.5

Vegetable, cucurbit, group 9 0.30

Vegetable, fruiting, group 8-10 1.0

Vegetable, leafy, except Brassica, crop group 4, except head lettuce and radicchio 10

Walnut, black 0.02

Walnut, English 0.02

Wheat, bran 0.30

Wheat, forage 30

Wheat, germ 0.25

Wheat, grain 0.15

Wheat, hay 15

Wheat, straw 9.0

1

There are no U.S. registrations as of October 22, 2013.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for the indirect or inadvertent residues of the fungicide 

flutriafol, including its metabolites and degradates, in or on the commodities in the table below when present therein as a 

result of the application of flutriafol to the growing crops listed in the table to paragraph (a) of this section. Compliance with 

the following tolerance levels specified below is to be determined by measuring only flutriafol ((±)-α-(2-fluorophenyl)

-α-(4-fluorophenyl)-1H-1,2,4-triazole-1-ethanol) in or on the following commodities:

Commodity Parts per million

Corn, sweet, forage 0.09

Corn, sweet, kernel plus cob with husk removed 0.01

Corn, sweet, stover 0.07

[75 FR 26673, May 12, 2010, as amended at 76 FR 69647, Nov. 9, 2011; 77 FR 47301, Aug. 8, 2012; 77 FR 48901, Aug. 15, 2012; 

78 FR 75262, Dec. 11, 2013; 79 FR 32673, June 6, 2014; 80 FR 5951, Feb. 4, 2015; 80 FR 71952, Nov. 18, 2015]

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§180.630 Flusilazole; tolerances for residues.

(a) General. [Reserved]

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(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of the fungicide, 

flusilazole, (1-[[bis(4-fluorophenyl)methylsilyl]methyl]-1H-1,2,4-triazole) in connection with use of the pesticide under 

Section 18 emergency exemptions granted by EPA. The tolerances expire and are revoked on the dates specified in the 

following table.

Commodity Parts per million Expiration/revocation date

Soybean, aspirated grain fractions 2.6 12/31/10

Soybean, seed 0.04 12/31/10

Soybean, oil 0.10 12/31/10

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[72 FR 49660, Aug. 29, 2007]

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§180.631 Pyrasulfotole; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide pyrasulfotole, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of pyrasulfotole ((5-hydroxy-1,3-dimethyl-1H-pyrazol-4-yl)[2-(methylsulfonyl)

-4-(trifluoromethyl)phenyl]methanone) and its desmethyl metabolite (5-hydroxy-3-methyl-1H-pyrazol-4-yl)

[2-(methylsulfonyl)-4-(trifluoromethyl)phenyl]methanone), calculated as the stoichiometric equivalent of pyrasulfotole, in or 

on the commodities:

Commodity Parts per million 

Aspirated grain fractions 0.40

Barley, grain 0.02

Barley, hay 0.30

Barley, straw 0.20

Cattle, fat 0.03

Cattle, liver 3.0

Cattle, meat 0.02

Cattle, meat byproducts, except liver 0.70

Eggs 0.02

Goat, fat 0.03

Goat, liver 3.0

Goat, meat 0.02

Goat, meat byproducts, except liver 0.70

Grass, forage 25

Grass, hay 3.5

Hog, fat 0.02

Hog, liver 0.30

Hog, meat 0.02

Hog, meat byproducts, except liver 0.05

Horse, fat 0.03

Horse, liver 3.0

Horse, meat 0.02

Horse, meat byproducts, except liver 0.70

Milk 0.03

Oat, forage 0.10

Oat, grain 0.08

Oat, hay 0.50

Oat, straw 0.20

Poultry, fat 0.02

Poultry, meat 0.02

Poultry, meat byproducts 0.20

Rye, forage 0.20

Rye, grain 0.02

Rye, straw 0.20

Sheep, fat 0.03

Sheep, liver 3.0

Sheep, meat 0.02

Sheep, meat byproducts, except liver 0.70

Sorghum, grain, forage 1.5

Sorghum, grain, grain 0.70

Sorghum, grain, stover 0.80

Wheat, forage 0.20

Wheat, grain 0.02

Wheat, hay 0.80

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Wheat, straw 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 45649, Aug. 15, 2007, as amended at 76 FR 23898, Apr. 29, 2011]

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§180.632 Fenazaquin; Tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide fenazaquin, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only fenazaquin, or 4-[2-[4-(1,1-dimethylethyl)phenyl]-ethoxy]quinazoline.

Commodity

Parts per

million

Almond 0.02

Almond, hulls 4.0

Apple 0.2

Cherry 2.0

Citrus Oil 10

Fruit, Citrus, Group 10 except Grape fruit 0.5

Pear 0.2

(b) Section is emergency exempotions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 44393, Aug. 8, 2007, as amended at 80 FR 25958, May 6, 2015]

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§180.633 Florasulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide florasulam N-(2,6-difluorophenyl)-8-fluoro-5-

methoxy(1,2,4)triazolo(1,5-c)pyrimidine-2-sulfonamide in or on the following commodities:

Commodity Parts per million

Barley, grain 0.01

Barley, hay 0.05

Barley, straw 0.05

Oat, forage 0.05

Oat, grain 0.01

Oat, hay 0.05

Oat, straw 0.05

Rye, forage 0.05

Rye, grain 0.01

Rye, straw 0.05

Wheat, forage 0.05

Wheat, grain 0.01

Wheat, hay 0.05

Wheat, straw 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 55077, Sept. 28, 2007]

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§180.634 Tembotrione; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the herbicide tembotrione, including its metabolites and 

degradates, in or on the commodities listed in the table to this paragraph. Compliance with the tolerance levels specified 

below is to be determined by measuring only the sum of tembotrione, 2-[2-chloro-4-(methylsulfonyl)-3-

[(2,2,2-trifluoroethoxy)methyl]benzoyl]-1,3-cyclohexanedione and its metabolite, 2-[2-chloro-4-(methylsulfonyl)-3-

[(2,2,2-trifluoroethoxy) methyl]benzoyl]-4,6-dihydroxy-1,3-cyclohexanedione, calculated as the stoichiometric equivalent of 

tembotrione, in or on the following commodities.

Commodity Parts per million

Cattle, liver 0.40

Cattle, meat byproducts, except liver 0.07

Corn, field, forage 0.60

Corn, field, grain 0.02

Corn, field, stover 0.45

Corn, pop, grain 0.02

Corn, pop, stover 0.35

Corn, sweet, forage 0.35

Corn, sweet, stover 0.60

Goat, liver 0.40

Goat, meat byproducts, except liver 0.07

Horse, liver 0.40

Horse, meat byproducts, except liver 0.07

Poultry, liver 0.07

Sheep, liver 0.40

Sheep, meat byproducts, except liver 0.07

(2) Tolerances are established for residues of the herbicide tembotrione, including its metabolites and degradates, in 

or on the commodities listed in the table to this paragraph. Compliance with the tolerance levels specified below is to be 

determined by measuring only tembotrione, 2-[2-chloro-4-(methylsulfonyl)-3-[(2,2,2-trifluoroethoxy)methyl]benzoyl]

-1,3-cyclohexanedione in or on the following commodities.

Commodity Parts per million

Corn, sweet, kernel plus cob with husks removed 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[72 FR 55085, Sept. 28, 2007, as amended at 74 FR 47894, Sept. 18, 2009]

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§180.635 Spinetoram; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide spinetoram, expressed as a 

combination of XDE-175-J: 1-H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione, 2-[(6-deoxy-3-O-ethyl-2,4-di-O-methyl-aL-mannopyranosyl) oxy]-13-[[(2R,5S,6R)-5- (dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl] oxy]-9-

ethyl-2,3,3a,4,5,5a,5b,6,9, 10,11,12,13,14,16a,16b- hexadecahydro 14-methyl-, (2R,3aR,5aR,5bS,9S, 

13S,14R,16aS,16bR); XDE-175-L: 1H-as-indaceno[3,2-d]oxacyclododecin-7,15-dione, 2-[(6-deoxy-3-O- ethyl-2,4-di-Omethyl-a-L-mannopyranosyl)oxy]-13-[[(2R,5S,6R)-5-(dimethylamino)tetrahydro-6-methyl-2H-pyran-2-yl]oxy]-9-

ethyl-2,3,3a,5a,5b,6,9, 10,11,12,13,14,16a,16b- tetradecahydro-4,14-dimethyl-, (2S,3aR,5aS,5bS,9S, 

13S,14R,16aS,16bS); ND-J: (2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR)-9-ethyl-14-methyl-13-[[(2S,5S,6R)-6- methyl5-(methylamino)tetrahydro- 2H-pyran-2-yl]oxy]-7,15-dioxo-2,3,3a,4,5,5a,5b,6,7,9, 10,11,12,13,14,15,16a,16boctadecahydro-1H-as- indaceno[3,2-d]oxacyclododecin-2-yl 6-deoxy-3-O-ethyl-2,4-di-O-methyl- alpha-Lmannopyranoside; and NF-J: (2R,3S,6S)-6-([(2R,3aR,5aR,5bS,9S, 13S,14R,16aS,16bR)- 2-[(6-deoxy-3-O-ethyl-2,4-di-Omethyl-alpha-L-mannopyranosyl) oxy]-9-ethyl-14-methyl-7,15-dioxo-2, 3,3a,4,5,5a,5b,6,7,9, 10,11,12,13,14,15,16a,16boctadecahydro-1H-as- indaceno[3,2-d]oxacyclododecin-13-yl] oxy)-2-methyltetrahydro- 2H-pyran-3-yl(methyl)formamide, 

in or on the following raw agricultural commodities:

Commodity Parts per million

Acerola 0.30

Almond, hulls 19

Amaranth grain, grain 1.0

Apple, wet pomace 0.50

Artichoke, globe 0.30

Asparagus 0.04

Atemoya 0.30

Avocado 0.30

Banana 0.25

Beet, sugar, molasses 0.75

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Biriba 0.30

Brassica, head and stem, subgroup 5A 2.0

Brassica, leafy greens, subgroup 5B 10

Bushberry, subgroup 13B 0.25

Caneberry, subgroup 13A 0.70

Canistel 0.30

Cattle, fat 5.5

Cattle, liver 0.85

Cattle, meat 0.20

Cattle, meat byproducts (except liver) 0.60

Cherimoya 0.30

Citrus, dried pulp 0.50

Citrus, oil 3.0

Corn, sweet, kernel plus cob with husks removed 0.04

Cotton, gin byproducts 1.5

Cotton, undelinted seed 0.04

Cranberry 0.04

Custard apple 0.30

Date 0.10

Egg 0.04

Feijoa 0.30

Fig 0.10

Fruit, citrus, group 10 0.30

Fruit, pome, group 11 0.20

Fruit, stone, group 12 0.20

Goat, fat 5.5

Goat, liver 0.85

Goat, meat 0.20

Goat, meat byproducts (except liver) 0.60

Grain, aspirated fractions 20

Grain, cereal, group 15, except rice, sorghum, pearl millet and proso millet 0.04

Grain, cereal, group 16, forage 3.5

Grain, cereal, group 16, hay 10

Grain, cereal, group 16, stover 10

Grain, cereal, straw, group 16, except rice 1.0

Grape 0.50

Grape, raisin 0.70

Guava 0.30

Herb, dried, subgroup 19A 22

Herb, fresh, subgroup 19A 3.0

Hog, fat 0.40

Hog, meat 0.04

Hog, meat byproducts 0.04

Hop, dried cones 22

Horse, fat 5.5

Horse, liver 0.85

Horse, meat 0.20

Horse, meat byproducts (except liver) 0.60

Ilama 0.30

Jaboticaba 0.30

Juneberry 0.25

Lingonberry 0.25

Longan 0.30

Lychee 0.30

Mango 0.30

Milk 0.30

Milk, fat 7.5

Millet, pearl, grain 1.0

Millet, proso, grain 1.0

Nut, tree, group 14 0.10

Okra 0.40

Onion, green 2.0

Papaya 0.30

Passionfruit 0.30

Pea and bean, dried shelled, except soybean, subgroup 6C 0.04

Pea and bean, succulent shelled, subgroup 6B 0.04

Peanut 0.04

Peanut, hay 11

Peppermint, tops 3.5

Pineapple 0.04

Pineapple, processed residue 0.15

Pistachio 0.10

Pomegranate 0.30

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Poultry, fat 0.10

Poultry, meat 0.04

Poultry, meat byproducts 0.04

Pulasan 0.30

Rambutan 0.30

Salal 0.25

Sapodilla 0.30

Sapote, black 0.30

Sapote, mamey 0.30

Sapote, white 0.30

Sheep, fat 5.5

Sheep, liver 0.85

Sheep, meat 0.20

Sheep, meat products (except liver) 0.60

Sorghum, grain, grain 1.0

Soursop 0.30

Soybean, seed 0.04

Spanish lime 0.30

Spearmint, tops 3.5

Spice, subgroup 19B, except black pepper 1.7

Star apple 0.30

Star fruit 0.30

Strawberry 1.0

Sugar apple 0.30

Ti, leaves 10

Vegetable, bulb, group 3, except green onion 0.10

Vegetable, cucurbit, group 9 0.30

Vegetable, foliage of legume, group 7 8.0

Vegetable, fruiting, group 8 0.40

Vegetable, leafy, except Brassica, group 4 8.0

Vegetable, leaves of root and tuber, group 2 10

Vegetable, legume, edible podded, subgroup 6A 0.30

Vegetable, root and tuber, group 1 0.10

Watercress 8.0

Wax jambu 0.30

(b) Section 18 emergency exemptions. [Reserved] 

(c) Tolerances with regional registration. [Reserved] 

(d) Indirect and invertent residues. [Reserved] 

[72 FR 57499, Oct. 10, 2007, as amended at 73 FR 14714, Mar. 19, 2008; 74 FR 40759, Aug. 13, 2009]

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§180.636 1,3-dichloropropene; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide cis- and trans-1,3-dichloropropene 

and its metabolites cis- and trans-3-chloroacrylic acid, and cis- and trans-3-chloroallyl alcohol in or on the following 

commodities.

Commodity Parts per million

Grape 0.018

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 8218, Feb. 13, 2008]

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§180.637 Mandipropamid; tolerances for residues.

(a) General. Tolerances are established for residues of mandipropamid, including its metabolites and degradates, in 

or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined 

by measuring only mandipropamid (4-chloro-N-[2-[3-methoxy-4-(2-propynyloxy)phenyl]ethyl]-α-(2-propynyloxy)

benzeneacetamide) in or on the commodity.

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Commodity Parts per million

Basil, dried leaves 200

Basil, fresh leaves 30

Bean, snap 0.90

Brassica, head and stem, subgroup 5A 3

Brassica, leafy greens, subgroup 5B 25

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.4

Ginseng 0.30

Grape, raisin 3.0

Hop, dried cones 50

Onion, bulb, subgroup 3-07A 0.05

Onion, green, subgroup 3-07B 4.0

Potato, wet peel 0.03

Vegetable, cucurbit, group 9 0.6

Vegetable, fruiting, group 8-10 1.0

Vegetable, leafy except Brassica, group 4 20

Vegetable, tuberous and corm, subgroup 1C 0.01

(b) Section 18 emergency exemptions. Time-limited tolerances are established for residues of mandipropamid, 

including its metabolites and degradates, in or on the commodities listed in the table below resulting from use of the 

pesticide pursuant to FFIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified below is 

to be determined by measuring only mandipropamid (4-chloro-N-[2-[3-methoxy-4-(2-propynyloxy)phenyl]ethyl]

-α-(2-propynyloxy)benzeneacetamide) in or on the commodity. The tolerances expire on the date specified in the table.

Commodity Parts per million Expiration/revocation date

Basil, dried 240 12/31/15

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent tolerances. [Reserved]

[73 FR 2816, Jan. 16, 2008, as amended at 74 FR 33169, July 10, 2009; 76 FR 55804, Sept. 9, 2011; 77 FR 74119, Dec. 13, 2012; 

78 FR 76992, Dec. 20, 2013]

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§180.638 Pyroxsulam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide pyroxsulam, N-(5,7-dimethoxy[1,2,4]triazolo

[1,5-a]pyrimidin-2-yl)-2-methoxy-4-(trifluoromethyl)-3-pyridinesulfonamide in or on the raw agricultural commodities:

Commodity Parts per million

Wheat, forage 0.06

Wheat, grain 0.01

Wheat, hay 0.01

Wheat, straw 0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 10402, Feb. 27, 2008]

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§180.639 Flubendiamide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined 

by measuring only flubendiamide N2

-[1, 1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4- [1,2,2,2-tetrafluoro1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following commodities:

Commodity Parts per million

Almond, hulls 9.0

Apple, wet pomace 5.0

Corn, field, forage 8.0

Corn, field, grain 0.03

Corn, field, stover 15

Corn, pop, grain 0.02

Corn, pop, stover 15

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Corn, sweet, forage 9.0

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 25

Cotton gin byproducts 60

Cotton, undelinted seed 0.90

Fruit, pome, group 11 1.5

Fruit, stone, group 12 1.6

Grape 1.4

Nut, tree, group 14 0.06

Okra 0.30

Vegetable, cucurbit, group 9 0.20

Vegetable, fruiting, group 8 0.60

Vegetable, leafy, except Brassica, group 4 11

(2) Tolerances are established for residues of flubendiamide, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified in the table is to be determined by 

measuring only flubendiamide N2

-[1,1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4-[1,2,2,2-tetrafluoro1-(trifluoromethyl)ethyl]phenyl]-1,2-benzenedicarboxamide, in or on the following commodities:

Commodity Parts per million

Alfalfa, forage 25

Alfalfa, hay 65

Artichoke, globe 1.6

Berry, low growing, subgroup 13-07G, except cranberry 1.5

Brassica, head and stem, subgroup 5A 3.0

Brassica, leafy greens, subgroup 5B 25

Cattle, fat 0.70

Cattle, meat 0.08

Cattle, meat byproducts 0.60

Egg 0.40

Fruit, small fruit vine climbing except fuzzy kiwifruit, subgroup 13-07F 1.4

Goat, fat 0.70

Goat, meat 0.08

Goat, meat byproducts 0.60

Grain, aspirated grain fractions 153

Hog, fat 0.15

Hog, meat 0.03

Hog, meat byproducts 0.15

Horse, fat 0.70

Horse, meat 0.08

Horse, meat byproducts 0.60

Milk 0.15

Milk, fat 1.0

Pea and bean, dried shelled, except soybean, subgroup 6C 0.60

Pea and bean, succulent shelled, subgroup 6B 0.05

Peanut, hay 60

Peanut, meal 0.03

Peanut, nutmeat 0.02

Peanut, refined oil 0.03

Pistachio 0.06

Poultry, fat 3.0

Poultry, liver 0.60

Poultry, meat 0.10

Rice, grain1 0.50

Safflower, seed 5.0

Sheep, fat 0.70

Sheep, meat 0.08

Sheep, meat byproducts 0.60

Sorghum, grain, forage 12

Sorghum, grain, grain 5.0

Sorghum, grain, stover 14

Soybean, forage 18

Soybean, hay 60

Soybean, hulls 0.80

Soybean, seed 0.25

Sugarcane, cane 0.30

Sunflower, seed 5.0

Turnip, greens 25

Vegetable, foliage of legume, except soybean, subgroup 7A 35

Vegetable, legume, edible podded, subgroup 6A 0.50

1

There are no U.S. registrations for rice, grain.

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(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of flubendiamide, including its metabolites 

and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified in the table is 

to be determined by measuring only flubendiamide N2-[1, 1-dimethyl-2-(methylsulfonyl)ethyl]-3-iodo-N1-[2-methyl-4- 

[1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl]phenyl]-1, 2-benzenedicarboxamide, in or on the following commodities:

Commodity Parts per million

Barley, hay 0.04

Barley, straw 0.07

Buckwheat 0.07

Clover, forage 0.15

Clover, hay 0.04

Grass, forage 0.15

Grass, hay 0.04

Millet, pearl, forage 0.15

Millet, pearl, hay 0.04

Millet, proso, forage 0.15

Millet, proso, hay 0.04

Millet, proso, straw 0.07

Oats, forage 0.15

Oats, hay 0.04

Oats, straw 0.07

Rye, forage 0.15

Rye, straw 0.07

Teosinte, forage 0.15

Teosinte, hay 0.04

Teosinte, straw 0.07

Triticale, forage 0.15

Triticale, hay 0.04

Triticale, straw 0.07

Wheat, forage 0.15

Wheat, hay 0.03

Wheat, straw 0.03

[76 FR 16307, Mar. 23, 2011, as amended at 76 FR 55273, Sept. 7, 2011; 77 FR 73945, Dec. 12, 2012]

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§180.640 Pyridalyl; tolerances for residues.

(a) General. Tolerances are established for residues of pyridalyl, pyridine,2-[3-[2,6-dichloro-4-[(3,3-dichloro-2-

propenyl)oxy]phenoxy]propoxy]-5-(trifluoromethyl, in or on the following raw agricultural commodities:)

Commodity Parts per million

Brassica, head and stem, subgroup 5A 3.5

Mustard greens 30

Turnip greens 30

Vegetable, fruiting, group 8 1.0

Vegetables, leafy, except Brassica, group 4 20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 25533, May 7, 2008]

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§180.641 Spirotetramat; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide spirotetramat, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-

en-4-yl-ethyl carbonate) and its metabolites cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-

one, cis-3-(2,5-dimethylphenyl)-3-hydroxy-8-methoxy-1-azaspiro[4.5]decane-2,4-dione, cis-3-(2,5-dimethylphenyl)-8-

methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl beta-D-glucopyranoside, and cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-

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methoxy-1-azaspiro[4.5]decan-2-one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following 

commodities.

Commodity Parts per million

Acerola 2.5

Almond, hulls 9.0

Artichoke, globe 1.5

Aspirated grain fractions 10.0

Avocado 0.60

Berry, low growing, except strawberry, subgroup 13-07H 0.30

Black sapote 0.60

Brassica, head and stem, subgroup 5A 2.5

Brassica, leafy, subgroup 5B 8.0

Bushberry subgroup 13-07B 3.0

Canistel 0.60

Citrus, oil 6.0

Coffee, green bean 0.20

Coffee, instant 0.50

Corn, sweet, kernel plus cob with husks removed 1.5

Cotton gin byproducts1 10.0

Cotton, undelinted seed1 0.30

Feijoa 2.5

Fruit, citrus, group 10-10 0.60

Fruit, pome, group 11-10 0.70

Fruit, stone, group 12 4.5

Grape, raisin 3.0

Guava 2.5

Hop, dried cones 10.0

Jaboticaba 2.5

Longan 13.0

Lychee 13.0

Mamey sapote 0.60

Mango 0.60

Nut, tree, group 14 0.25

Papaya 0.40

Passionfruit 2.5

Persimmon 2.5

Pineapple 0.30

Pistachio 0.25

Pomegranate 0.50

Potato, flakes 1.6

Pulasan 13.0

Rambutan 13.0

Sapodilla 0.60

Small fruit vine climbing subgroup, except fuzzy kiwifruit, subgroup 13-07F 1.3

Soybean forage 8.0

Soybean hay 16.0

Soybean seed 5.0

Spanish lime 13

Star apple 0.60

Starfruit 2.5

Strawberry1 0.40

Taro, leaves 9.0

Vegetable, bulb, group 3-07 0.80

Vegetable, cucurbit, group 9 0.30

Vegetable, foliage of legume, except soybean, subgroup 07A 7.0

Vegetable, fruiting, group 8-10 2.5

Vegetable, leafy, except brassica, group 4 9.0

Vegetable, legume, group 06, except soybean 2.5

Vegetable, tuberous and corm, subgroup 1C 0.60

Watercress 2.0

Wax jambu 2.5

White sapote 0.60

1

Import tolerance only. There are no U.S. registrations for cotton or strawberry.

(2) Tolerances are also established for residues of the insecticide spirotetramat, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of spirotetramat (cis-3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-

en-4-yl-ethyl carbonate]) and its metabolite cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-

one, calculated as the stoichiometric equivalent of spirotetramat, in or on the following commodities:

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Commodity Parts per million

Cattle, fat 0.02

Cattle, meat 0.02

Cattle, meat byproducts 0.20

Eggs 0.02

Goat, fat 0.02

Goat, meat 0.02

Goat, meat byproducts 0.20

Hog, meat byproducts 0.02

Horse, fat 0.02

Horse, meat 0.02

Horse, meat byproducts 0.20

Milk 0.01

Poultry, meat byproducts 0.02

Sheep, fat 0.02

Sheep, meat 0.02

Sheep, meat byproducts 0.20

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. Tolerances with regional registrations are established for residues of the 

insecticide spirotetramat, including its metabolites and degradates, in or on the commodities in the table below. 

Compliance with the tolerance levels specified below is to be determined by measuring only the sum of spirotetramat (cis3-(2,5-dimethlyphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl-ethyl carbonate) and its metabolites cis3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]dec-3-en-2-one, cis-3-(2,5-dimethylphenyl)-3-hydroxy-8-

methoxy-1-azaspiro[4.5]decane-2,4-dione, cis-3-(2,5-dimethylphenyl)-8-methoxy-2-oxo-1-azaspiro[4.5]dec-3-en-4-yl betaD-glucopyranoside, and cis-3-(2,5-dimethylphenyl)-4-hydroxy-8-methoxy-1-azaspiro[4.5]decan-2-one, calculated as the 

stoichiometric equivalent of spirotetramat, in or on the following commodities.

Commodity Parts per million

Banana 4.0

(d) Indirect or inadvertant residues. [Reserved]

[73 FR 39256, July 9, 2008, as amended at 76 FR 28681, May 18, 2011; 77 FR 8746, Feb. 15, 2012; 77 FR 75859, Dec. 26, 2012; 

78 FR 28512, May 15, 2013; 78 FR 66651, Nov. 6, 2013]

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§180.642 Gentamicin; tolerances for residues.

(a) General. [Reserved]

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

residues of gentamicin in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to 

FIFRA section 18 emergency exemptions. The tolerances expire and are revoked on the date specified in the following 

table.

Commodity Parts per million Expiration/revocation date

Apple 0.10 12/31/10

(c) Tolerance with regional restrictions. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[73 FR 44162, July 30, 2008]

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§180.643 Uniconazole; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide/plant growth regulator uniconazole-P, (E)-(S)

-1-(4-chlorophenyl)-4,4-dimethyl-2-(1H-1,2,4-triazol-1-yl)pent-1-en-3-ol, its R-enantiomer and its Z-isomer in or on the 

following raw agricultural commodities:

Commodity Parts per million

Vegetable, fruiting, group 8 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertant residues. [Reserved]

[73 FR 51736, Sept. 5, 2008]

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§180.644 Cyprosulfamide; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide safener cyprosulfamide, 

N-[[4-[(cyclopropylamino)carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, in or on the following raw agricultural 

commodities:

Commodity Parts per million

Corn, field, forage 0.20

Corn, field, grain 0.01

Corn, field, stover 0.20

Corn, pop, grain 0.01

Corn, pop, stover 0.20

Corn, sweet, forage 0.40

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.35

(2) Tolerances are established for residues of the herbicide safener cyprosulfamide, N-[[4-[(cyclopropylamino)

carbonyl] phenyl]sulfonyl]-2-methoxybenzamide, and its metabolite 4-(aminosulfonyl)-N-cyclopropylbenzamide, calculated 

as cyprosulfamide, in or on the following raw agricultural commodities:

Commodity Parts per million

Cattle, meat byproducts 0.02

Goat, meat byproducts 0.02

Horse, meat byproducts 0.02

Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[73 FR 60974, Oct. 15, 2008]

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§180.645 Thiencarbazone-methyl; tolerances for residues.

(a) General. (1) Tolerances are established for residues of thiencarbazone-methyl [methyl 4-[[[(4,5-dihydro-3-

methoxy-4-methyl-5-oxo-1H-1,2,4-triazol-1-yl)-carbonyl]amino]sulfonyl]-5-methyl-3-thiophenecarboxylate], per se, in or on 

the following food and feed commodities:

Commodity Parts per million

Corn, field, forage 0.04

Corn, field, grain 0.01

Corn, field, stover 0.02

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Corn, sweet, forage 0.05

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.05

Wheat, forage 0.10

Wheat, grain 0.01

Wheat, hay 0.01

Wheat, straw 0.01

(2) Tolerances are established for combined residues of thiencarbazone-methyl and its metabolite BYH 18636-MMT 

[5-methoxy-4-methyl-2,4-dihydro-3H-1,2,4-triazol-3-one], calculated as the parent compound, in or on the following food 

commodities of animal origin:

Commodity Parts per million

Cattle, meat 0.02

Cattle, meat byproducts 0.02

Goat, meat 0.02

Goat, meat byproducts 0.02

Horse, meat 0.02

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Horse, meat byproducts 0.02

Milk 0.02

Sheep, meat 0.02

Sheep, meat byproducts 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent combined residues of 

thiencarbazone-methyl and its metabolite BYH 18636-MMT-glucoside [2-hexopyranosyl-5-methoxy-4-methyl-2,4-dihydro3H-1,2,4-triazol-3-one], calculated as the parent compound, in or on the following food commodities:

Commodity Parts per million

Soybean, forage 0.04

Soybean, hay 0.15

[73 FR 60968, Oct. 15, 2008]

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§180.646 Ipconazole; tolerances for residues.

(a) General. Tolerances are established for residues of ipconazole, including its metabolites and degradates, in or on 

the commodities listed in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only ipconazole (2-[(4-chlorophenyl)methyl]-5-(1-methylethyl)-1-(1H-1,2,4-triazol-1-ylmethyl)cyclopentanol) in or 

on the commodity.

Commodity Parts per million

Cotton, gin byproducts 0.01

Cotton, undelinted seed 0.01

Grain, cereal, forage, fodder and straw, group 16, except rice 0.01

Grain, cereal group 15, except rice 0.01

Peanut 0.01

Soybean, forage 0.01

Vegetable, legume, group 6 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[73 FR 69559, Nov. 19, 2008, as amended at 79 FR 15240, Mar. 19, 2014]

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§180.647 d-Phenothrin; tolerances for residues.

(a) General. A tolerance of 0.01 parts per million is established for residues of the insecticide d-phenothrin in or on all 

food/feed crops following wide-area mosquito adulticide applications.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 32443, July 8, 2009]

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§180.648 Meptyldinocap; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the fungicide meptyldinocap, 2-(1-methylheptyl)

-4,6-dinitrophenyl (2E)-2-butenoate and 2,4-DNOP, 2,4-dinitro-6-(1-methylheptyl)phenol expressed as meptyldinocap in or 

on the following commodities:

Commodity Parts Per Million

Grape 0.20

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 48396, Sept. 23, 2009]

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§180.649 Saflufenacil; tolerances for residues.

(a) General. (1) Tolerances are established for residues of saflufenacil, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of saflufenacil, 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-

fluoro-N-[[methyl(1-methylethyl)amino]sulfonyl]benzamide, and its metabolites N-[2-chloro-5-(2,6-dioxo-4-(trifluoromethyl)

-3,6-dihydro-1(2H)-pyrimidinyl)-4-fluorobenzoyl]-N′-isopropylsulfamide and N-[4-chloro-2-fluoro-5-({[(isopropylamino)

sulfonyl]amino}carbonyl)phenyl]urea, calculated as the stoichiometric equivalent of saflufenacil, in or on the commodities.

Commodity Parts per million

Alfalfa, forage 0.08

Alfalfa, hay 0.10

Almond, hulls 0.10

Banana1 0.03

Barley, bran 1.5

Barley, grain 1.0

Barley, straw 15

Coffee, green bean1 0.03

Cotton, gin byproducts 0.45

Cottonseed subgroup 20C 0.20

Fruit, citrus, group 10 0.03

Fruit, pome, group 11 0.03

Fruit, stone, group 12 0.03

Grain, aspirated grain fractions 50

Grain, cereal, forage, fodder and straw group 16 (except barley and wheat straw) 0.10

Grain, cereal, group 15 (except barley and wheat grain) 0.03

Grape 0.03

Grass, forage 15

Grass, hay 20

Grass, seed screenings 0.15

Grass, straw 0.15

Mango1 0.03

Nut, tree, group 14 0.03

Olive 0.03

Pea and bean, dried shelled, except soybean, subgroup 6C 0.30

Pea and bean, succulent shelled, subgroup 6B 0.03

Pea, hay 17

Pistachio 0.03

Pomegranate 0.03

Rapeseed subgroup 20A 0.45

Soybean, hulls 0.50

Soybean, seed 0.10

Sugarcane, cane2 0.05

Sugarcane, molasses2 0.08

Sunflower subgroup 20B 1.0

Vegetable, foliage of legume, group 7 (except pea, hay) 0.10

Vegetable, legume, edible podded, subgroup 6A 0.03

Wheat, grain 0.60

Wheat, straw 6.0

1

No U.S. registration as of December 7, 2011.

2

No U.S. registration as of February 21, 2014.

(2) Tolerances are established for residues of saflufenacil, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only saflufenacil, 2-chloro-5-[3,6-dihydro-3-methyl-2,6-dioxo-4-(trifluoromethyl)-1(2H)-pyrimidinyl]-4-fluoro-N-[[methyl

(1-methylethyl)amino]sulfonyl]benzamide, in or on the commodities.

Commodity Parts per million

Cattle, fat 0.04

Cattle, liver 50

Cattle, meat 0.02

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Cattle, meat byproducts, except liver 0.30

Fish-freshwater finfish 0.01

Fish-shellfish, crustacean 0.01

Goat, fat 0.04

Goat, liver 50

Goat, meat 0.02

Goat, meat byproducts, except liver 0.30

Hog, fat 0.01

Hog, liver 2.0

Hog, meat 0.01

Hog, meat byproducts, except liver 0.02

Horse, fat 0.04

Horse, liver 50

Horse, meat 0.02

Horse, meat byproducts, except liver 0.30

Milk 0.01

Sheep, fat 0.04

Sheep, liver 50

Sheep, meat 0.02

Sheep, meat byproducts, except liver 0.30

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[74 FR 46689, Sept. 11, 2009, as amended at 76 FR 27261, May 11, 2011; 76 FR 76309, Dec. 7, 2011; 79 FR 9866, Feb. 21, 2014; 

79 FR 52219, Sept. 3, 2014; 80 FR 22420, Apr. 22, 2015; 80 FR 73667, Nov. 25, 2015]

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§180.650 Isoxaben; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide isoxaben, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only isoxaben, N-[3-(1-ethyl-1-methylpropyl)-5-isoxazolyl]-2, 6-dimethoxybenzamide, in or on 

the commodity.

Commodity

Parts per

million

Almond, hulls 0.40

Grape 0.01

Nut, tree, Group 14 0.02

Pistachio 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 69360, Nov. 12, 2010]

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§180.651 Imazosulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide imazosulfuron, including its metabolites and 

degradates, in or on the following commodities. Compliance with the tolerance levels specified in the following table below 

is to be determined by measuring only imazosulfuron, 2-chloro-N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]

imidazo-[1,2-α]pyridine-3-sulfonamide, in or on the commodity.

Commodity Parts per million

Melon subgroup 9A 0.02

Pepper, bell 0.02

Pepper, non-bell 0.02

Rice, grain 0.02

Tomato 0.02

Vegetable, tuberous and corm, subgroup 1C 0.02

(b) Section 18 emergency exemptions. [Reserved]

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(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[75 FR 81884, Dec. 29, 2010, as amended at 78 FR 44444, July 24, 2013]

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§180.652 Ethiprole; tolerances for residues.

(a) General. Tolerances (without U.S. registrations) are established for residues of the insecticide ethiprole, including 

its metabolites and degradate, in or on the following commodities listed in the table. Compliance with the tolerance levels 

specified in the table is to be determined by measuring only ethiprole [5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-

[(ethyl)-sulfinyl]-1H-pyrazole-3-carbonitrile], in or on the following commodities:

Commodity

Parts per

million

Rice, grain1 1.7

Tea, dried1 30

1

There are no U.S. registrations for rice and tea.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 18921, Apr. 6, 2011]

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§180.653 Indaziflam; tolerances for residues.

(a) General. Tolerances are established for residues of the herbicide indaziflam, N-[(1R,2S)-2,3-dihydro-2,6-dimethyl1H-inden-1-yl]-6-(1-fluoroethyl)-1,3,5-triazine-2,4-diamine, including its metabolites and degradates, in or on the 

commodities in the following table. Compliance with the tolerance levels specified in the table below is to be determined by 

measuring only indaziflam, in or on the commodity.

Commodity

Parts per

million

Almond, hulls 0.15

Banana1 0.01

Coffee, green bean1 0.01

Fruit, citrus, group 10-10 0.01

Fruit, pome, group 11-10 0.01

Fruit, stone, group 12 0.01

Grape 0.01

Nut, tree, group 14 0.01

Olive 0.01

Palm, oil1 0.03

Pistachio 0.01

Sugarcane, refined sugar1 0.01

1

No U.S. Registrations as of 12/02/2013.

2

Tolerance without a corresponding U.S. registration.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 18905, Apr. 6, 2011, as amended at 79 FR 4630, Jan. 29, 2014]

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§180.654 Isopyrazam; tolerances for residues.

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(a) General. Tolerances are established for residues of the fungicide isopyrazam, including its metabolites and 

degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the 

following table is to be determined by measuring only isopyrazam (3-(difluoromethyl)-1-methyl-N-[1,2,3,4-tetrahydro9-(1-methylethyl)-1,4-methano-naphthalen-5-yl]-1H-pyrazole-4-carboxamide), as the sum of its syn-isomer 

(3-(difluoromethyl)-1-methyl-N-[(1RS, 4SR, 9RS)-1,2,3,4-tetrahydro-9-(1-methylethyl)-1,4-methanonaphthalen-5-yl]

-1H-pyrazole-4-carboxamide) and anti-isomer (3-(difluoromethyl)-1-methyl-N-[(1RS, 4SR, 9SR)-1,2,3,4-tetrahydro9-(1-methylethyl)-1,4-methano-naphthalen-5-yl]-1H-pyrazole-4-carboxamide) in or on the commodity.

Commodity Parts per million

Apple1 0.70

Banana1 0.05

Peanut1 0.01

1

There are no U.S. registrations for use of isopyrazam on apple, banana, or peanut.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 61596, Oct. 5, 2011, as amended at 78 FR 78745, Dec. 27, 2013]

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§180.655 Flazasulfuron; tolerances for residues.

(a) General. Tolerances are established for residues of flazasulfuron, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only flazasulfuron (N-[[(4,6-dimethoxy-2-pyrimidinyl)amino]carbonyl]-3-(trifluoromethyl)-2-pyridinesulfonamide).

Commodity Parts per million

Almond, hulls 0.01

Fruit, citrus, group 10-10 0.01

Grape 0.01

Nut, tree, group 14-12 0.01

Sugarcane 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 10968, Feb. 24, 2012, as amended at 79 FR 52989, Sept. 5, 2014]

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§180.656 Amisulbrom; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide amisulbrom, including its metabolites and 

degradates, in or on the commodities listed below. Compliance with the tolerance levels is to be determined by measuring 

only amisulbrom, 3-[(3-bromo-6-fluoro-2-methyl-1H-indole-1-yl) sulfonyl]-N, N-dimethyl-1H-1, 2, 4-triazole-1-sulfonamide].

Commodity1 Parts per million

Grape 0.40

Grape, raisin 1.0

Tomato 0.50

Tomato, paste 1.2

1

There is no U.S. registration for use of amisulbrom on grape or tomato.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[76 FR 59914, Sept. 28, 2011]

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§180.657 Metaflumizone; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide metaflumizone, including its metabolites and 

degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the 

following table is to be determined by measuring only the sum of metaflumizone (E and Z isomers; 2-[2-(4-cyanophenyl)

-1-[3-(trifluoromethyl) phenyl]ethylidene]-N-[4-(trifluoromethoxy)phenyl] hydrazinecarboxamide) and its metabolite 

4-{2-oxo-2-[3-(trifluoromethyl) phenyl]ethyl}-benzonitrile, calculated as the stoichiometric equivalent of metaflumizone, in or

on the following commodities:

Commodity Parts per million

Almond, hulls 0.04

Eggplant1 1.5

Fruit, citrus, group 10-10 0.04

Fruit, pome, group 11-10 0.04

Fruit, stone, group 12-12 0.04

Grape 0.04

Nut, tree, group 14-12 0.04

Pepper1 1.5

Tomato1 0.60

Tomato, paste1 1.2

1

There are no U.S. registrations as of April 4, 2014.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 10386, Feb. 22, 2012, as amended at 79 FR 18810, Apr. 4, 2014; 80 FR 66800, Oct. 30, 2015]

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§180.658 Penthiopyrad; tolerances for residues.

(a) General. (1) Tolerances are established for residues of penthiopyrad, including its metabolites and degradates, in 

or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only penthiopyrad (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxamide).

Commodity Parts per million

Alfalfa, forage 7.0

Alfalfa, hay 20

Almond, hulls 6.0

Apple, wet pomace 1.5

Barley, grain 0.15

Barley, hay 80

Barley, milled byproducts 0.90

Barley, straw 1.0

Beet, sugar, dried pulp 1.5

Beet, sugar, roots 0.5

Berry, low growing, subgroup 13-07G 3.0

Brassica, head and stem, subgroup 5A 5.0

Brassica, leafy greens, subgroup 5B 50

Buckwheat, grain 0.15

Canola 1.5

Corn, field, forage 40

Corn, field, grain 0.01

Corn, field, refined oil 0.05

Corn, field, stover 15

Corn, pop, grain 0.01

Corn, sweet, kernel plus cob with husks removed 0.01

Cotton, seed 1.5

Cotton, gin byproducts 15

Fruit, pome, group 11-10 0.50

Fruit, stone, group 12 4.0

Grain, aspirated fractions 30

Millet, spp. 0.80

Nut, tree, group 14 0.06

Oat, forage 40

Oat, grain 0.15

Oat, hay 80

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Oat, straw 1.0

Pea and bean, dried shelled, except soybean, subgroup 6C 0.40

Peanut 0.04

Peanut, hay 30

Peanut, refined oil 0.06

Pistachio 0.06

Potato, processed potato waste 0.20

Rye, forage 40

Rye, grain 0.15

Rye, straw 1.0

Sorghum, forage 40

Sorghum, grain, grain 0.80

Sorghum, stover 15

Soybean, seed 0.40

Sunflower, seed 1.5

Teosinte, grain 0.15

Tomato, paste 3.5

Triticale, forage 40

Triticale, grain 0.15

Triticale, hay 80

Triticale, straw 1.0

Vegetable, bulb, group 3-07 3.0

Vegetable, cucurbit, group 9 0.60

Vegetable, foliage of legume, group 7, hay 200

Vegetable, foliage of legume, group 7, vines/forage 50

Vegetable, fruiting, group 8-10 3.0

Vegetable, leafy, except brassica, group 4 30

Vegetable, leaves of root and tuber, group 2 50

Vegetable, legume, edible podded, subgroup 6A 4.0

Vegetable, legume, succulent shelled, subgroup 6B 0.40

Vegetable, root, subgroup 1B, except sugar beet 3.0

Vegetable, tuber and corm, subgroup 1C 0.06

Wheat, forage 40

Wheat, grain 0.15

Wheat, hay 80

Wheat, milled byproducts 0.30

Wheat, straw 1.0

(2) Tolerances are established for residues of penthiopyrad, including its metabolites and degradates, in or on the 

commodities in the table below. Compliance with the tolerance levels specified below is to be determined by measuring 

only the sum of penthiopyrad (N-[2-(1,3-dimethylbutyl)-3-thienyl]-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carboxamide) 

and its metabolite (1-methyl-3-trifluoromethyl-1H-pyrazole-4-carboxamide), calculated as the stoichiometric equivalent of 

penthiopyrad, in or on the commodity.

Commodity Parts per million

Cattle, fat 0.03

Cattle, meat 0.03

Cattle, meat byproducts 0.09

Goat, fat 0.03

Goat, meat 0.03

Goat, meat byproducts 0.09

Horse, fat 0.03

Horse, meat 0.03

Horse, meat byproducts 0.09

Milk 0.02

Sheep, fat 0.03

Sheep, meat 0.03

Sheep, meat byproducts 0.09

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 14297, Mar. 9, 2012]

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§180.659 Pyroxasulfone; tolerances for residues.

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(a) General. (1) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolite, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)

-1H-pyrazol-4-carboxylic acid (M-3), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million

Corn, field, grain 0.02

Corn, pop, grain 0.015

Corn, sweet, kernel plus cob with husks removed 0.015

Cotton, undelinted seed 0.04

Wheat, grain 0.03

(2) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]

sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolites, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)

-1H-pyrazol-4-yl]methanesulfonic acid (M-1); 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-carboxylic acid 

(M-3); and [5-(difluoromethoxy)-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-25), calculated as the 

stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million

Corn, field, forage 0.09

Corn, field, stover 0.15

Corn, pop, stover 0.15

Corn, sweet, forage 0.10

Corn, sweet, stover 0.15

Cotton, gin byproducts 0.20

Soybean, forage 1.0

Soybean, hay 2.0

Wheat, forage 6.0

Wheat, hay 1.0

Wheat, straw 0.60

(3) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, 

in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only the sum of pyroxasulfone, 3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol-4-yl]methyl]

sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole, and its metabolites, 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)

-1H-pyrazol-4-carboxylic acid (M-3); [5-(difluoromethoxy)-3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-25); 

and 3-[1-carboxy-2-(5,5-dimethyl-4,5-dihydroisoxazol-3-ylthio)ethylamino]-3-oxopropanoic acid (M-28), calculated as the 

stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million

Soybean, seed 0.06

(4) Tolerances are established for residues of the herbicide pyroxasulfone, including its metabolites and degradates, 

in or on the commodities in the following table. Compliance with the tolerance levels specified in the following table is to be

determined by measuring only the sum of pyroxasulfone [3-[[[5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1H-pyrazol4-yl]methyl]sulfonyl]-4,5-dihydro-5,5-dimethylisoxazole] and its metabolites [5-(difluoromethoxy)-1-methyl3-(trifluoromethyl)-1H-pyrazol-4-yl]methanesulfonic acid (M-1) and 5-(difluoromethoxy)-1-methyl-3-(trifluoromethyl)-1Hpyrazol-4-carboxylic acid (M-3), calculated as the stoichiometric equivalent of pyroxasulfone, in or on the commodity.

Commodity Parts per million

Milk 0.003

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 12213, Feb. 29, 2012, as amended at 78 FR 13257, Feb. 27, 2013; 78 FR 46279, July 31, 2013; 79 FR 34633, June 18, 

2014]

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§180.660 Pyriofenone; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide pyriofenone, including its metabolites and 

degradates, in or on the following commodities listed in the table. Compliance with the tolerance levels specified in the 

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table is to be determined by measuring only pyriofenone, (5-chloro-2-methoxy-4-methyl-3-pyridinyl)(2,3,4-trimethoxy-6-

methylphenyl) methanone, in or on the following commodities:

Commodity Parts per million

Grape1 0.30

Grape, raisin1 0.50

1

There are no U.S. registrations for grape and grape, raisin.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 13506, Mar. 7, 2012]

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§180.661 Fluopyram; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide Fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)

-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates in or on the commodities in the 

table below. Compliance with the tolerance levels specified in the table is to be determined by measuring only fluopyram in 

or on the commodity.

Commodity

Parts

per million

Almond, hull 8.0

Apple 0.30

Apple, wet pomace 0.60

Banana1 1.0

Bean, dry 0.09

Beet, sugar, root 0.04

Cotton, gin byproducts 0.70

Cotton, undelinted seed 0.01

Cherry 0.60

Grape, wine 2.0

Nut, tree, group 14 0.05

Peanut 0.09

Pistachio 0.05

Potato 0.02

Potato, processed potato waste 0.08

Soybean, seed 0.04

Strawberry 1.5

Watermelon 1.0

1

There are no U.S. registrations.

(2) Tolerances are established for residues of the fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]

ethyl]-2-(trifluoromethyl)benzamide, including its metabolites and degradates. Compliance with the tolerance levels 

specified in the table below is to be determined by measuring only the sum of fluopyram and its metabolite, 

2-(trifluoromethyl)benzamide, calculated as the stoichiometric equivalent of fluopyram, in or on the commodity.

Commodity

Parts per

million

Cattle, fat 0.05

Cattle, meat 0.05

Cattle, meat byproducts 0.40

Egg 0.06

Goat, fat 0.11

Goat, meat 0.15

Goat, meat byproducts 1.1

Hog, fat 0.02

Hog, meat 0.02

Hog, meat byproducts 0.03

Horse, fat 0.11

Horse, meat 0.15

Horse, meat byproducts 1.1

Milk 0.06

Poultry, fat 0.03

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Poultry, meat 0.03

Poultry, meat byproducts 0.10

Sheep, fat 0.11

Sheep, meat 0.15

Sheep, meat byproducts 1.1

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. It is recommended that tolerances be established for indirect or inadvertent 

residues of fungicide fluopyram, N-[2-[3-chloro-5-(trifluoromethyl)-2-pyridinyl]ethyl]-2-(trifluoromethyl)benzamide, including 

its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

in the table is to be determined by measuring only fluopyram in or on the commodity.

Commodity

Parts per

million

Alfalfa, forage 0.45

Alfalfa, hay 1.1

Canola, seed 1.8

Grain, cereal, except rice, group 15 0.03

Grain, cereal, forage, fodder and straw, group 16 2.0

Soybean, forage 4.0

Soybean, hay 15

Soybean, seed 0.10

[77 FR 10975, Feb. 24, 2012, as amended at 79 FR 75065, Dec. 17, 2014]

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§180.662 Trinexapac-ethyl; tolerances for residues.

(a) General. Tolerances are established for residues of the plant growth inhibitor, trinexapac-ethyl, including its 

metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring both trinexapac-ethyl, ethyl 4-(cyclopropylhydroxymethylene)

-3,5-dioxocyclohexanecarboxylate and the associated metabolite, trinexpac, 4-(cyclopropylhydroxymethylene)

-3,5-dioxocyclohexanecarboxylic acid, calculated as the stoichiometric equivalent of trinexapac-ethyl, in or on the 

commodity.

Commodity

Parts per

million

Barley, bran 2.5

Barley, grain 2.0

Barley, hay 0.8

Barley, straw 0.4

Cattle, fat 0.02

Cattle, meat 0.02

Cattle, meat byproducts 0.04

Goat, fat 0.02

Goat, meat 0.02

Goat, meat byproducts 0.04

Grass, forage 1.5

Grass, hay 4.0

Grass, seed screenings 40.0

Grass, straw 10.0

Hog, fat 0.02

Hog, meat 0.02

Hog, meat by-products 0.03

Horse, fat 0.02

Horse, meat 0.02

Horse, meat byproducts 0.04

Oat, forage 1.0

Oat, grain 4.0

Oat, hay 1.5

Oat, straw 0.9

Rice, bran 1.5

Rice, grain 0.4

Rice, straw 0.07

Rice, wild, grain 0.4

Rye, bran 6.0

Rye, grain 4.0

Rye, hay 1.5

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Rye, straw 0.9

Sheep, fat 0.02

Sheep, meat 0.02

Sheep, meat byproducts 0.04

Sugarcane, cane 0.8

Sugarcane, molasses 2.5

Wheat, bran 6.0

Wheat, forage 1.0

Wheat, grain 4.0

Wheat, hay 1.5

Wheat, middlings 10.5

Wheat, straw 0.9

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 12745, Mar. 2, 2012, as amended at 77 FR 60919, Oct. 3, 2012; 80 FR 28848, May 20, 2015]

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§180.663 Ametoctradin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide ametoctradin, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only ametoctradin (5-ethyl-6-octyl[1,2,4]triazolo[1,5-a]pyrimidin-7-amine).

Commodity

Parts per

million

Brassica, head and stem, subgroup 5A 9.0

Brassica, leafy greens, subgroup 5B 50

Grape 4.0

Grape, raisin 8.0

Hop, dried cones 10.0

Onion, bulb, subgroup 3-07A 1.5

Onion, green, subgroup 3-07B 20.0

Spinach 50.0

Vegetable, cucurbit, group 9 3.0

Vegetable, fruiting, group 8-10 1.5

Vegetable, leafy, except Brassica, group 4, except spinach 40.0

Vegetable, tuberous and corm, subgroup 1C 0.05

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 21734, May 9, 2012]

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§180.664 Penflufen; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide penflufen, including its metabolites and 

degradates, in or on the following commodities listed in the table. Compliance with the tolerance levels specified in the 

table is to be determined by measuring only penflufen N-[2-(1,3-dimethylbutyl)phenyl]-5-fluoro-1,3-dimethyl-1H-pyrazole-4-

carboxamide, in or on the following commodities.

Commodity Parts per million

Alfalfa, forage 0.01

Alfalfa, hay 0.01

Cotton, gin by-products 0.01

Grain cereal, forage, fodder and straw, group 16 0.01

Grain, cereal, group 15 0.01

Oilseed, group 20 0.01

Vegetable, foliage of legume, group 7 0.01

Vegetable, legume, group 6 0.01

Vegetable, tuberous and corm subgroup 1C 0.01

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(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 28281, May 14, 2012]

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§180.665 Sedaxane; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide sedaxane, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only sedaxane, N-[2-[1,1′-bicyclopropyl]-2-ylphenyl]-3-(difluoromethyl)-1-methyl1H-pyrazole-4-carboxamide, as the sum of its cis- and trans-isomers in or on the commodity.

Commodity Parts per million

Barley, grain 0.01

Barley, hay 0.04

Barley, straw 0.01

Beet, sugar, roots 0.01

Canola, seed 0.01

Corn, field, forage 0.01

Corn, field, grain 0.01

Corn, field, stover 0.01

Corn, pop, grain 0.01

Corn, pop, stover 0.01

Corn, sweet, forage 0.01

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 0.01

Cotton, undelinted seed 0.01

Cotton, gin byproducts 0.01

Oat, forage 0.015

Oat, grain 0.01

Oat, hay 0.06

Oat, straw 0.01

Pea and bean, dried shelled, except soybean, subgroup 6C 0.01

Potato 0.02 

Potato, wet peel 0.075 

Rapeseed, subgroup 20A 0.01

Rye, forage 0.015

Rye, grain 0.01

Rye, straw 0.01

Sorghum, grain, forage 0.01

Sorghum, grain, grain 0.01

Sorghum, grain, stover 0.01

Soybean, forage 0.05

Soybean, hay 0.04

Soybean, seed 0.01

Vegetable, foliage of legume, except soybean, subgroup 7A 0.01

Wheat, forage 0.015

Wheat, grain 0.01

Wheat, hay 0.06

Wheat, straw 0.01

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect inadvertent residues. [Reserved]

[77 FR 36924, June 20, 2012, as amended at 78 FR 33748, June 5, 2013; 78 FR 60719, Oct. 2, 2013; 80 FR 43329, July 22, 2015]

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§180.666 Fluxapyroxad; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fluxapyroxad, including its metabolites and 

degradates, in or on the commodities listed in the table below. Compliance with the tolerance levels specified below is to 

be determined by measuring only fluxapyroxad, 3-(difluoromethyl)-1-methyl-N-(3′,4′,5′-trifluoro[1,1′-biphenyl]-2-yl)

-1H-pyrazole-4-carboxamide in or on the commodity.

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Commodity

Parts 

per

million

Almond, hulls 4.0

Apple, wet pomace 2.0

Beet, sugar 0.1

Beet, sugar, dried pulp 0.1

Beet, sugar, tops 7.0

Berry, low growing, subgroup 13-07G 4.0

Bushberry, subgroup 13-07B 7.0

Caneberry, subgroup 13-07A 5.0

Cattle, fat 0.05

Cattle, meat 0.01

Cattle, meat byproducts 0.03

Corn, field, grain 0.01

Corn, oil 0.03

Corn, pop, grain 0.01

Corn, sweet, kernels plus cobs with husks removed 0.15

Cotton, gin byproducts 20

Cotton, undelinted seed 0.30

Egg 0.002

Fish-freshwater finfish 0.01

Fish-shellfish, crustacean 0.01

Fruit, pome, group 11 0.8

Fruit, small, vine climbing, except fuzzy kiwifruit, subgroup 13-07F 2.0

Fruit, stone, group 12-12 3.0

Goat, fat 0.05

Goat, meat 0.01

Goat, meat byproducts 0.03

Grain, aspirated fractions 20.0

Grain, cereal, forage, fodder and straw, group 16 20

Grain, cereal, group 15, (except corn, field, grain; except corn, pop, grain; except corn, kernels plus cobs with husks removed; except rice; except 

wheat

3.0

Grape, raisin 5.7

Hog, meat byproducts 0.01

Horse, fat 0.05

Horse, meat 0.01

Horse, meat byproducts 0.03

Milk 0.005

Nut, tree, group 14-12 0.06

Oilseeds, group 20 (except cottonseed) 0.9

Pea and bean, dried shelled except soybean, subgroup 6C 0.4

Pea and bean, succulent shelled, subgroup 6B 0.5

Peanut 0.01

Peanut, refined oil 0.02

Plum, prune, dried 3.0

Potato, wet peel 0.1

Rice, bran 4.5

Rice, bran 8.5

Rice, grain 5.0

Rice, hulls 8.0

Rice, hulls 15.0

Sheep, fat 0.05

Sheep, meat 0.01

Sheep, meat byproducts 0.03

Soybean, hulls 0.3

Soybean, seed 0.15

Sugarcane, cane 3.0

Vegetable, brassica leafy, group 5 4.0

Vegetable, bulb, group 3-07 1.5

Vegetable, cucurbit, group 9 0.50

Vegetable, foliage of legume, group 7 30

Vegetables, fruiting, group 8 0.7

Vegetable, leafy, except brassica, group 4 30

Vegetable, legume, edible podded, subgroup 6A 2.0

Vegetable, root, except sugarbeet, subgroup 1B 0.90

Vegetable, tuberous and corm, subgroup 1C 0.02

Wheat, bran 0.6

Wheat, grain 0.3

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. Tolerances are established for the combined indirect or inadvertent residues of 

the fungicide fluxapyroxad, including its metabolites and degradates, in or on the commodities listed in the table below. 

Compliance with the tolerance levels specified below is to be determined by measuring only fluxapyroxad, 

3-(difluoromethyl)-1-methyl-N-(3′,4′,5′-trifluoro[1,1′-biphenyl]-2-yl)-1H-pyrazole-4-carboxamide in or on the commodity.

Commodity

Parts per

million

Nongrass animal feeds, group18 0.30

Peppermint, tops 0.01

Spearmint, tops 0.01

[77 FR 28275, May 14, 2012, as amended at 77 FR 46307, Aug. 3, 2012; 79 FR 10677, Feb. 26, 2014; 80 FR 45078, July 29, 2015]

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§180.667 Cyflufenamid, tolerance for residues.

(a) General. Tolerances are established for residues of the fungicide cyflufenamid, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only cyflufenamid, [N(Z)]-N-[[(cyclopropylmethoxy)amino][2,3-difluoro-6-(trifluoromethyl)phenyl]

methylene]benzeneacetamide.

Commodity Parts per million

Apple, wet pomace 0.10

Berry, low growing, subgroup 13-07G, except cranberry 0.20

Fruit, pome, group 11 0.06

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 0.15

Grape, raisin 0.30

Vegetable, cucurbit, group 9 0.07

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 38210, June 27, 2012]

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§180.668 Sulfoxaflor; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide sulfoxaflor, including its metabolites and 

degradates, in or on the commodities in the table. Compliance with the tolerance levels specified is to be determined by 

measuring only sulfoxaflor (N-[methyloxido[1-[6-(trifluoromethyl)-3-pyridinyl]ethyl]-γ4

-sulfanylidene]cyanamide).

Commodity Parts per million

Almond, hulls 6.0

Barley, grain 0.40

Barley, hay 1.0

Barley, straw 2.0

Bean, dry seed 0.20

Bean, succulent 4.0

Beet, sugar, dried pulp 0.07

Beet, sugar, molasses 0.25

Berry, low growing, subgroup 13-7G 0.70

Cattle, fat 0.10

Cattle, meat 0.15

Cattle, meat byproducts 0.40

Cauliflower 0.08

Citrus, dried pulp 3.6

Cotton, gin byproducts 6.0

Cotton, hulls 0.35

Cottonseed subgroup 20C 0.20

Fruit, citrus, group 10-10 0.70

Fruit, pome, group 11-10 0.50

Fruit, small, vine climbing, subgroup 13-07F, except fuzzy kiwi fruit 2.0

Fruit, stone, group 12 3.0

Goat, fat 0.10

Goat, meat 0.15

Goat, meat byproducts 0.40

Grain, aspirated fractions 20.0

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Grape, raisin 6.0

Hog, fat 0.01

Hog, meat 0.01

Hog, meat byproducts 0.01

Horse, fat 0.10

Horse, meat 0.15

Horse, meat byproducts 0.40

Leafy greens, subgroup 4A 6.0

Leafy petiole, subgroup 4B 2.0

Milk 0.15

Nuts, tree, group 14 0.015

Onion, bulb, subgroup 3-07A 0.01

Onion, green, subgroup 3-07B 0.70

Pistachio 0.015

Poultry, eggs 0.01

Poultry, fat 0.01

Poultry, meat 0.01

Poultry, meat byproducts 0.01

Rapeseed, meal 0.50

Rapeseed subgroup 20A 0.40

Sheep, fat 0.10

Sheep, meat 0.15

Sheep, meat byproducts 0.40

Soybean, seed 0.20

Tomato, paste 2.60

Tomato, puree 1.20

Vegetable, brassica, leafy, group 5, except cauliflower 2.0

Vegetable, cucurbit, group 9 0.40

Vegetable, fruiting, group 8-10 0.70

Vegetable, leaves of root and tuber, group 2 3.0

Vegetable, legume, foliage, group 7 3.0

Vegetable, root and tuber, group 1 0.05

Watercress 6.0

Wheat, forage 1.0

Wheat, grain 0.08

Wheat, hay 1.5

Wheat, straw 2.0

(b) Section 18 emergency exemptions. Time-limited tolerances specified in the following table are established for 

residues of sulfoxaflor (N-[methyloxido[1-[6-(trifluoromethyl)-3-pyridinyl]ethyl]- λ4

-sulfanylidene]cyanamide), including its 

metabolites and degradates, in or on the specified agricultural commodities, resulting from use of the pesticide pursuant to 

FIFRA section 18 emergency exemptions. Compliance with the tolerance levels specified in the following table is to be 

determined by measuring only sulfoxaflor in or on the commodity. The tolerances expire on the date specified in the table.

Commodity

Parts

per

million Expiration/revocation date

Sorghum, forage 0.40 12/31/17

Sorghum, grain 0.30 12/31/17

Sorghum, stover 0.90 12/31/17

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 59565, Sept. 28, 2012, as amended at 78 FR 38227, June 26, 2013; 80 FR 4515, Jan. 28, 2015]

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§180.669 Picoxystrobin; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide picoxystrobin, including its metabolites and 

degradates, in or on the commodities listed below. Compliance with the tolerance levels specified below is to be 

determined by measuring only picoxystrobin, methyl (αE)-α-(methoxymethylene)-2-[[[6-(trifluoromethyl)-2-pyridinyl]oxy]

methyl]benzeneacetate.

Commodity

Parts per

million

Barley, bran 0.5

Barley, grain 0.3

Cattle, fat 0.01

Cattle, meat 0.01

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Cattle, meat byproducts 0.01

Corn, field, refined oil 0.07

Eggs 0.01

Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.01

Grain, aspirated grain fractions 10

Grain, cereal, forage, fodder, and straw, group 16, forage 15

Grain, cereal, forage, fodder, and straw, group 16, hay 5

Grain, cereal, forage, fodder, and straw, group 16, stover 10

Grain, cereal, forage, fodder, and straw, group 16, straw 2

Grain, cereal, group 15, except rice and barley 0.04

Hog, fat 0.01

Hog, meat 0.01

Hog, meat byproducts 0.01

Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.01

Milk 0.01

Pea and bean, dried shelled, except soybean, subgroup 6C 0.06

Poultry, fat 0.01

Poultry, meat 0.01

Poultry, meat byproducts 0.01

Rapeseed subgroup 20A 0.08

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.01

Soybean, forage 1

Soybean, hay 3

Soybean, hulls 0.2

Soybean, seed 0.05

Vegetable, foliage of legume, except soybean, subgroup 7A 40

Wheat, bran 0.06

Wheat, germ 0.09

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[77 FR 72231, Dec. 5, 2012]

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§180.671 Fenpyrazamine; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide fenpyrazamine, in or on the following 

commodities. Compliance with the tolerance levels specified in the following table is to be determined by measuring only 

fenpyrazamine S-allyl 5-amino-2-isopropyl-4-(2-methylphenyl)-3-oxo-2,3-dihydropyrazole-1-carbothioate, in or on the 

following commodities:

Commodity

Parts per

million

Almond 0.02

Almond, hulls 1.5

Berry, low growing, subgroup 13-07G 3

Bushberry subgroup 13-07B 5

Caneberry subgroup 13-07A 5

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3

Ginseng 0.7

Grape, juice 4

Lettuce, head 1.5

Lettuce, leaf 2

Pistachio 0.02

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

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[78 FR 14465, Mar. 6, 2013]

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§180.672 Cyantraniliprole; tolerances for residues.

(a) General. Tolerances are established for the combined residues of the insecticide cyantraniliprole, 3-bromo1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[(methylamino)carbonyl]phenyl]-1H-pyrazole-5-carboxamide, including its 

metabolites and degradates, in or on commodities in the following table. Compliance with the tolerance levels specified in 

the following table is to be determined by measuring only cyantraniliprole in or on the commodity.

Commodity Parts per million

Almond, hulls 8.0

Brassica head and stem (subgroup 5A) 3.0

Brassica leafy vegetables (subgroup 5B) 30

Bushberry (subgroup 13-07B) 4.0

Cattle, fat 0.01

Cattle, meat 0.01

Cattle, meat byproducts 0.01

Cherry (subgroup 12-12A) 6.0

Citrus, oil 2.4

Cotton, gin byproducts 10

Fruit, citrus (group 10-10) 0.70

Fruit, pome (group 11-10) 1.5

Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.01

Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.01

Milk 0.01

Nut, tree (group 14-12) 0.04

Oilseed (group 20) 1.5

Onion, bulb (subgroup 3-07A) 0.04

Onion, green (subgroup 3-07B) 8.0

Peach (subgroup 12-12B) 1.5

Plum (subgroup 12-12C) 0.50

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.01

Vegetable, cucurbit (group 9) 0.40

Vegetable, fruiting (group 8-10) 2.0

Vegetable, leafy (except Brassica) (group 4) 20

Vegetable, tuberous and corm (subgroup 1C) 0.15

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for indirect or inadvertent tolerances for residues of 

cyantraniliprole, 3-bromo-1-(3-chloro-2-pyridinyl)-N-[4-cyano-2-methyl-6-[(methylamino)carbonyl]phenyl]-1H-pyrazole-5-

carboxamide, including its metabolites and degradates, in or on commodities in the following table. Compliance with the 

tolerance levels specified in the following table is to be determined by measuring only cyantraniliprole in or on the 

commodity.

Commodity Parts per million

Animal feed, nongrass (group 18) 0.20

Grain, cereal, forage, fodder and straw (group 16) 0.50

Grass forage, fodder and hay (group 17) 0.50

Peanut, hay 0.01

Vegetable, foliage of legume (group 7) 0.70

Vegetable, leaves of root and tuber vegetables (group 2) 0.04

Vegetable, root (subgroup 1A) 0.02

[79 FR 6833, Feb. 5, 2014]

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§180.673 Triforine; tolerances for residues.

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(a) General. Tolerances are established for residues of triforine, including its metabolites and degradates. Compliance 

with the tolerance levels specified in the following table is to be determined by measuring only triforine (N,N′

-[1,2-piperazinediylbis(2,2,2-trichloroehylidene)]bis[formamide]), in or on the following commodities.

Commodity

Parts per

million

Blueberry1 1.0

Tomato1 0.5

1

There are no U.S. registrations for blueberry and tomato.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[78 FR 32151, May 29, 2013. Redesignated at 78 FR 36677, June 19, 2013]

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§180.674 Proquinazid; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide, proquinazid, including its metabolites and 

degradates, in or on the commodities listed in the following table. Compliance with the tolerance levels specified in the 

following table is to be determined by measuring only proquinazid, [6-Iodo-2-propoxy-3-propyl-3H-quinazolin-4-one), in or 

on the following commodities:

Commodity

Parts per

million

Grape1 0.50

Grape, raisin1 1.0

1

No U.S. registrations for Proquinazid.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 18815, Apr. 4, 2014]

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§180.675 Tolfenpyrad; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide tolfenpyrad, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only tolfenpyrad, 4-chloro-3-ethyl-1-methyl-N-[4-(p-tolyloxy)benzyl]pyrazole-5-carboxamide.

Commodity Parts per million

Almond hulls 6.0

Citrus, dried pulp 8.0

Citrus, oil 70.0

Cotton, gin byproducts 15.0

Cotton, undelinted seed 0.70

Fruit, stone, group 12-12 2.0

Fruits, citrus, group 10-10 1.5

Grape 2.0

Grape, raisin 6.0

Nuts, tree, group 14-12 0.05

Persimmon 2.0

Plum, prune 3.0

Pomegranate 2.0

Potato 0.01

Tea 30.0

Vegetable, leafy, except Brassica, group 4 30.0

(2) Tolerances are established for residues of the insecticide tolfenpyrad, including its metabolites and degradates, in 

or on the commodities in the following table. Compliance with the tolerance levels specified below is to be determined by 

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measuring only the sum of tolfenpyrad, 4-chloro-3-ethyl-1-methyl-N-[4-(p-tolyloxy)benzyl]pyrazole-5-carboxamide, and its 

metabolite 4-[4-[(4-chloro-3-ethyl-1-methylpyrazol-5-yl)carbonylamino-methyl]phenoxy]-benzoic acid, calculated as the 

stoichiometric equivalent of tolfenpyrad.

Commodity Parts per million

Cattle, fat 0.01

Cattle, meat 0.01

Cattle, meat byproducts 0.35

Goat, fat 0.01

Goat, meat 0.01

Goat, meat byproducts 0.35

Horse, fat 0.01

Horse, meat 0.01

Horse, meat byproducts 0.35

Milk 0.03

Sheep, fat 0.01

Sheep, meat 0.01

Sheep, meat byproducts 0.35

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registration. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 1605, Jan. 9, 2014]

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§180.676 Fenpropidin; tolerances for residues.

(a) General. Tolerances are established for the residues of fenpropidin, including its metabolites and degradates, in or 

on the commodities in the table below. Compliance with the tolerance levels specified below is to be determined by 

measuring only fenpropidin (1-[3-[4-(1,1-dimethylethyl)phenyl]-2-methylpropyl]piperidine).

Commodity 

Parts per

million

Banana1 10 

1

There are no U.S. registrations as of December 13, 2013.

(b) Section 18 tolerance. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 8096, Feb. 11, 2014]

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§180.677 Cyflumetofen; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide cyflumetofen, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels for cyflumetofen is to be 

determined by measuring only cyflumetofen, 2-methoxyethyl α-cyano-α-[4-(1,1-dimethylethyl)phenyl]-β-oxo2-(trifluoromethyl)benzenepropanoate, in or on the commodity.

Commodity

Parts per

million

Almond, hulls 4.0

Citrus, oil 16

Fruit, citrus, group 10-10 0.30

Fruit, pome, group 11-10 0.30

Grape 0.60

Nut, tree, group 14-12 0.01

Strawberry 0.60

Tomato 0.40

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

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(d) Indirect or inadvertent residues. [Reserved]

[79 FR 29108, May 21, 2014]

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§180.678 Tricyclazole; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide tricyclazole, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only tricyclazole (5-methyl-1,2,4-triazolo[3,4-b ]benzothiazole).

Commodity

Parts

per million

Rice, grain1 3.0

1

There are no U.S. Registrations on Rice as of June 11, 2014.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[79 FR 33468, June 11, 2014]

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§180.679 Flupyradifurone; tolerances for residues.

(a) General. Tolerances are established for residues of the insecticide flupyradifurone, including its metabolites and 

degradates, in or on the commodities in the following table. Compliance with the tolerance levels specified in the following 

table is to be determined by measuring only flupyradifurone, 4-[[(6-chloro-3-pyridinyl)methyl](2,2-difluoroethyl)amino]- 2

(5H)-furanone.

Commodity Parts per million

Alfalfa, forage 9.0

Alfalfa, hay 20

Almond, hulls 15

Bean, succulent 0.20

Berry, low growing, except cranberry subgroup 13-07G 1.5

Brassica, head and stem subgroup 5A 6.0

Brassica, leafy greens subgroup 5B 40

Bushberry, except cranberry subgroup 13-07B 4.0

Cactus, fruit 0.30

Cactus, pads 0.70

Cattle, fat 0.20

Cattle, meat 0.30

Cattle, meat byproducts 1.0

Coffee, green bean1 1.5

Corn, field, grain 0.05

Corn, pop, grain 0.05

Corn, sweet, kernels plus cobs with husks removed 0.05

Cotton, gin byproducts 40

Cottonseed, subgroup 20C 0.80

Egg 0.01

Fruit, citrus, dried pulp 10

Fruit, citrus, group 10-10 3.0

Fruit, pome, group 11-10 0.70

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0

Goat, fat 0.20

Goat, meat 0.30

Goat, meat byproducts 1.0

Grain, aspirated grain fractions 40

Grain, cereal, forage, fodder and straw, group 16 30

Grain, cereal, group 15, except rice and corn 3.0

Grape, raisin 5.0

Hog, fat 0.01

Hog, meat 0.01

Hog, meat byproducts 0.04

Hops, dried cones 10

Horse, fat 0.20

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Horse, meat 0.30

Horse, meat byproducts 1.0

Leaf petioles, subgroup 4B 9.0

Leafy greens, subgroup 4A 30

Milk 0.15

Nut, tree, group 14-12 0.02

Onion, bulb, subgroup 3-07A 0.09

Onion, green, subgroup 3-07B 3.0

Pea and bean, dried, shelled except soybean, subgroup 6C 3.0

Pea, succulent 2.0

Peanut 0.04

Peanut, hay 20

Pitaya 0.30

Sheep, fat 0.20

Sheep, meat 0.30

Sheep, meat byproducts 1.0

Soybean, seed 1.5

Taro leaves 30

Turnip greens 40

Vegetable, cucurbit, group 9 0.40

Vegetable, foliage of legume, group 7 30

Vegetable, fruiting, group 8-10 1.5

Vegetable, legume, edible podded, subgroup 6A 3.0

Vegetable, root, except sugar beet, subgroup 1B 0.90

Vegetable, tuberous and corm, subgroup 1C 0.05

1

No U.S. registration.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional restrictions. Tolerances are established for residues of the insecticide flupyradifurone, 

including its metabolites and degradates, in or on the commodities in the following table. Compliance with the tolerance 

levels specified in the following table is to be determined by measuring only flupyradifurone, 4-[[(6-chloro-3-pyridinyl)

methyl](2,2-difluoroethyl)amino]- 2(5H)-furanone.

Commodity Parts per million

Clover, forage 20

Clover, hay 30

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 3487, Jan. 23, 2015]

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§180.680 Fluensulfone; tolerances for residues.

(a) General. Tolerances are established for residues of the nematicide fluensulfone, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only 3,4,4-trifluoro-but-3-ene-1-sulfonic acid, calculated as the stoichiometric equivalent of 

fluensulfone.

Commodity

Parts per

million

Tomato, paste 1.0

Vegetables, cucurbits, group 9 0.50

Vegetables, fruiting, group 8-10 0.50

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertant residues. [Reserved]

[79 FR 56968, Sept. 24, 2014, as amended at 80 FR 56395, Sept. 18, 2015]

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§180.681 Isofetamid; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide isofetamid, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

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determined by measuring only isofetamid, N-[1,1-dimethyl-2-[2-methyl-4-(1-methylethoxy)phenyl]-2-oxoethyl]-3-methyl-2-

thiophenecarboxamide, in or on the following commodities:

Commodity

Parts per

million

Almond 0.01

Almond, hulls 0.01

Berry, low growing, subgroup 13-07G 4.0

Canola, refined oil 0.03

Flax, seed, oil 0.03

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 3.0

Grape, raisin 5.0

Lettuce, head 5.0

Lettuce, leaf 7.0

Mustard, seed, oil 0.03

Rapeseed subgroup 20A 0.015

Sesame, oil 0.03

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 45443, July 30, 2015]

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§180.682 Bicyclopyrone; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the herbicide bicyclopyrone (4-hydroxy-3-

[[2-[(2-methoxyethoxy)methyl]-6-(trifluoromethyl)-3-pyridinyl]carbonyl]bicyclo[3.2.1]oct-3-en-2-one), including its 

metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring only the sum of the common moieties SYN503780 (2-[(2-methoxyethoxy)methyl]

-6-(trifluoromethyl)-3-pyridinecarboxylic acid) and CSCD686480 (2-[(2-hydroxyethoxy)methyl]-6-(trifluoromethyl)-3-

pyridinecarboxylic acid), calculated as the stoichiometric equivalent of bicyclopyrone, in or on the commodities.

Commodity

Parts per

million

Corn, field, forage 0.30

Corn, field, grain 0.02

Corn, field, stover 0.40

Corn, pop, grain 0.02

Corn, pop, stover 0.40

Corn, sweet, forage 0.40

Corn, sweet, kernel plus cob with husks removed 0.03

Corn, sweet, stover 0.70

Sugarcane, cane1 0.02

Cattle, meat byproducts 1.5

Goat, meat byproducts 1.5

Sheep, meat byproducts 1.5

Horse, meat byproducts 1.5

Hog, meat byproducts 0.15

1

There are no U.S. Registrations on Sugarcane as of March 13, 2015.

(2) [Reserved]

(b) [Reserved]

[80 FR 22654, Apr. 23, 2015]

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§180.684 Benalaxyl-M; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide benalaxyl-M, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only benalaxyl [methyl N-(2,6-dimethylphenyl)-N-(phenylacetyl)-DL-alaninate] in or on the 

commodity.

Commodity Parts per million

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Grape1 3.0

Tomato1 0.20

1

There is no U.S. registration for use on this commodity as of July 30, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 45448, July 30, 2015]

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§180.685 Oxathiapiprolin; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the fungicide oxathiapiprolin, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only oxathiapiprolin, 1-[4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2-thiazolyl]-1-

piperidinyl]-2-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-ethanone, in or on the commodity.

Commodity Parts per million

Brassica, head and stem, subgroup 5A 1.5

Ginseng 0.15

Grape1 0.70

Leafy greens subgroup 4A 15

Onion, bulb, subgroup 3-07A 0.04

Onion, green, subgroup 3-07B 2.0

Pea, edible-podded 1.0

Pea, succulent shelled 0.05

Tomato, dried 3.0

Vegetable, cucurbit, group 9 0.20

Vegetable, fruiting, group 8-10 0.50

Vegetable, tuberous and corm, subgroup 1C 0.01

1

There is no associated U.S. registration as of September 4, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. Tolerances are established for residues of the fungicide oxathiapiprolin, including 

its metabolites and degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified 

below is to be determined by measuring only oxathiapiprolin, 1-[4-[4-[5-(2,6-difluorophenyl)-4,5-dihydro-3-isoxazolyl]-2-

thiazolyl]-1-piperidinyl]-2-[5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]-ethanone, in or on the commodity.

Commodity Parts per million

All other food commodities/feed commodities (other than those covered by a tolerance as a result of use on growing crops) 0.10

[80 FR 53473, Sept. 4, 2015]

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§180.686 Benzovindiflupyr; tolerances for residues.

(a) General. Tolerances are established for residues of the fungicide benzovindiflupyr, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only benzovindiflupyr (N-[9-(dichloromethylene)-1,2,3,4-tetrahydro-1,4-methanonaphthalen-5-yl]

-3-(difluoromethyl)-1-methyl-1H-pyrazole-4-carboxamide) in or on the commodity.

Commodity Parts per million

Barley, grain 1.5

Barley, hay 15.0

Barley, straw 15.0

Cattle, fat 0.02

Cattle, liver 0.06

Cattle, meat 0.01

Cattle, meat byproducts, except liver 0.01

Coffee, green bean1 0.09

Corn, field, forage 3.0

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Corn, field, grain 0.02

Corn, field, stover 15.0

Corn, pop, grain 0.02

Corn, pop, stover 15.0

Corn, sweet, forage 4.0

Corn, sweet, kernel plus cob with husks removed 0.01

Corn, sweet, stover 5.0

Cottonseed, subgroup 20C 0.15

Cotton, gin byproducts 3.0

Fruit, pome, group 11-10 0.20

Fruit, small vine climbing, except fuzzy kiwifruit, subgroup 13-07F 1.0

Goat, fat 0.02

Goat, liver 0.06

Goat, meat 0.01

Goat, meat byproducts, except liver 0.01

Grain, aspirated fractions 15.0

Grape, raisin 3.0

Horse, fat 0.02

Horse, liver 0.06

Horse, meat 0.01

Horse, meat byproducts, except liver 0.01

Milk 0.01

Milk, fat 0.02

Oat, grain 1.5

Oat, hay 15.0

Oat, straw 15.0

Pea and bean, dried shelled, except soybean, subgroup 6C 0.20

Pea, field, hay 7.0

Pea, field, vine 1.5

Peanut 0.01

Peanut, hay 15.0

Potato, processed potato waste 0.10

Rapeseed, subgroup 20A 0.15

Rye, grain 0.1

Rye, hay 15.0

Rye, straw 15.0

Sheep, fat 0.02

Sheep, liver 0.06

Sheep, meat 0.01

Sheep meat byproducts, except liver 0.01

Soybean, forage 15.0

Soybean, hay 50.0

Soybean, hulls 0.20

Soybean, seed 0.07

Sugarcane, cane1 0.04

Tomato, dried 4.0

Vegetable, cucurbit, group 9 0.30

Vegetable, fruiting, group 8-10 1.5

Vegetable, tuberous and corm, subgroup 1C 0.02

Wheat, forage 4.0

Wheat, grain 0.10

Wheat, hay 15.0

Wheat, straw 15.0

1

There is no U.S. registration for use of benzovindiflupyr.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 59633, Oct. 2, 2015]

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§180.687 Teflubenzuron; tolerances for residues.

(a) General. (1) Tolerances are established for residues of the insecticide teflubenzuron, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only teflubenzuron (N-[[(3,5-dichloro-2,4-difluorophenyl)amino]carbonyl]-2,6-difluorobenzamide).

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Commodity Parts per

million

Apple1 1.0

Broccoli1 0.20

Cauliflower1 0.01

Citrus, oil1 100

Coffee, bean, green1 0.60

Corn, field, grain1 0.01

Corn, field, refined oil1 0.02

Lemon1 0.80

Mango1 1.5

Melon, subgroup 9A1 0.30

Orange1 0.60

Papaya1 0.50

Pineapple1 0.80

Soybean, seed1 0.05

Soybean, hulls1 0.15

Sugarcane, cane1 0.01

Sunflower, seed1 0.30

Tomato1 1.5

1

There are no U.S. registrations as of October 30, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues. [Reserved]

[80 FR 66809, Oct. 30, 2015]

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§180.688 Diethofencarb; tolerance for residue.

(a) General. (1) Tolerances are established for residues of the fungicide diethofencarb, including its metabolites and 

degradates, in or on the commodities in the table below. Compliance with the tolerance levels specified below is to be 

determined by measuring only diethofencarb (1-methylethyl N-(3,4-diethoxyphenyl)carbamate).

Commodity

Parts per

million

Banana* 0.10

*There is no U.S. registration for use on this commodity as of November 4, 2015.

(b) Section 18 emergency exemptions. [Reserved]

(c) Tolerances with regional registrations. [Reserved]

(d) Indirect or inadvertent residues [Reserved]

[80 FR 68261, Nov. 4, 2015]

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Subpart D—Exemptions From Tolerances

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§180.900 Exemptions from the requirement of a tolerance.

An exemption from a tolerance shall be granted when it appears that the total quantity of the pesticide chemical in or 

on all raw agricultural commodities for which it is useful under conditions of use currently prevailing or proposed will 

involve no hazard to the public health.

[69 FR 23117, Apr. 28, 2004]

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§180.905 Pesticide chemicals; exemptions from the requirement of a tolerance.

(a) When applied to growing crops, in accordance with good agricultural practice, the following pesticide chemicals 

are exempt from the requirement of a tolerance:

(1) Petroleum oils.

(2) Piperonyl butoxide.

(3) Pyrethrins.

(4) Sabadilla.

(b) When applied to growing crops, in accordance with good agricultural practice, the pesticides rotenone or derris or 

cube roots are exempt from the requirement of a tolerance. There are no U.S. registrations for use of rotenone, derris, or 

cube roots on food commodities as of March 23, 2011.

(c) These pesticides are not exempted from the requirement of a tolerance when applied to a crop at the time of or 

after harvest.

[77 FR 59128, Sept. 26, 2012]

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§180.910 Inert ingredients used pre- and post-harvest; exemptions from the requirement of a tolerance.

Residues of the following materials are exempted from the requirement of a tolerance when used in accordance with 

good agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to growing crops or 

to raw agricultural commodities after harvest:

Inert ingredients Limits Uses

Acetic acid Catalyst

Acetic anhydride Solvent, cosolvent

Acetone Do.

Alkanoic and alkenoic acids, mono- and diesters of α-hydro-ω-hydroxypoly (oxyethylene) with molecular weight (in 

amu) range of 200 to 6,000

Emulsifiers

Alkyl (C8-C24) benzenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts Surfactants, related 

adjuvants of 

surfactants

C10-C18-Alkyl dimethyl amine oxides (CAS Reg. Nos. 1643-20-5, 2571-88-2, 2605-79-0, 3332-27-2, 61788-90-7, 

68955-55-5, 70592-80-2, 7128-91-8, 85408-48-6, and 85408-49-7)

15% by weight in 

pesticide 

formulation

Surfactant 

α-alkyl(C6- C15)-ω-hydroxypoly(oxyethylene)sulfate, and its ammonium, calcium, magnesium, potassium, sodium, 

and zinc salts, poly(oxyethylene) content averages 2-4 moles (CAS Reg. Nos.: 3088-31-1, 3694-74-4, 9004-82-4, 

9004-84-6, 9021-91-4, 9086-52-6, 13150-00-0, 15826-16-1, 25446-78-0, 26183-44-8, 27140-00-7, 27731-62-0, 

32612-48-9, 34431-25-9, 35015-74-8, 50602-06-7, 52286-18-7, 52286-19-8, 54116-08-4, 55901-67-2, 61702-

79-2, 61894-66-4, 62755-21-9, 63428-85-3, 63428-86-4, 63428-87-5, 65086-57-9, 65086-79-5, 65104-74-7, 

65122-38-5, 67674-66-2, 67762-19-0, 67762-21-4, 67845-82-3, 67845-83-4, 67923-90-4, 68037-05-8, 68037-

06-9, 68171-41-5, 68424-50-0, 68511-39-7, 68585-34-2, 68610-66-2, 68611-29-0, 68611-55-2, 68649-53-6, 

68890-88-0, 68891-29-2, 68891-30-5, 68891-38-3, 69011-37-6, 73665-22-2, 75422-21-8, 78330-16-2, 78330-

17-3, 78330-25-3, 78330-26-4, 78330-27-5, 78330-28-6, 78330-29-7, 78330-30-0, 96130-61-9, 106597-03-9, 

110392-50-2, 119432-41-6, 125301-88-4, 125301-89-5, 125301-92-0, 125736-54-1, 157707-85-2, 160104-51-8, 

160901-27-9, 160901-28-0, 160901-29-1, 160901-30-4, 161025-28-1, 161074-79-9, 162063-19-6, 219756-63-5)

Not to exceed 30% 

of formulation

Surfactants, related 

adjuvants of 

surfactants.

α-alkyl (C12-C15)-ω-hydroxypoly (oxypropylene) poly (oxyethylene) copolymers (where the poly (oxypropylene) 

content is 3-60 moles and the poly (oxyethylene) content is 5-80 moles)

Not more than 

20% of pesticide 

formulations

Surfactant

α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene) polymers where the alkyl chain contains a 

minimum of six carbons (CAS Reg. No.: 9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3; 

9038-43-1; 9040-05-5; 9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-52-8; 26468-86-0; 

26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-01-1; 34398-05-5; 37251-67-5; 37311-00-5; 37311-

01-6; 37311-02-7; 37311-04-9; 39587-22-9; 50861-66-0; 52232-09-4; 52292-17-8; 52609-19-5; 57679-21-7; 

59112-62-8; 60828-78-6; 61702-78-1; 61725-89-1; 61791-13-7; 61791-20-6; 61791-28-4; 61804-34-0; 61827-

42-7; 61827-84-7; 62648-50-4; 63303-01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 

64425-86-1; 65104-72-5; 65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-08-0; 68002-96-0; 68002-

97-1; 68131-39-5; 68131-40-8; 68154-96-1; 68154-97-2; 68154-98-3; 68155-01-1; 68213-23-0; 68213-24-1; 

68238-81-3; 68238-82-4; 68409-58-5; 68409-59-6; 68439-30-5; 68439-45-2; 68439-46-3; 68439-48-5; 68439-

49-6; 68439-50-9; 68439-51-0; 68439-53-2; 68439-54-3; 68458-88-8; 68526-94-3; 68526-95-4; 68551-12-2; 

68551-13-3; 68551-14-4; 68603-20-3; 68603-25-8; 68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 68954-

94-9; 68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 69013-19-0; 69227-20-9; 69227-21-0; 69227-22-1; 

69364-63-2; 70750-27-5; 70879-83-3; 70955-07-6; 71011-10-4; 71060-57-6; 71243-46-4; 72066-65-0; 72108-

90-8; 72484-69-6; 72854-13-8; 72905-87-4; 73018-31-2; 73049-34-0; 74432-13-6; 74499-34-6; 78330-19-5; 

78330-20-8; 78330-21-9; 78330-23-1; 79771-03-2; 84133-50-6; 85422-93-1; 97043-91-9; 97953-22-5; 102782-

43-4; 103331-86-8; 103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 106232-83-1; 111905-54-5; 116810-

31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 121617-09-2; 126646-02-4; 126950-62-7; 127036-

24-2; 139626-71-4; 152231-44-2; 154518-36-2; 157627-86-6; 157627-88-8; 157707-41-0; 157707-43-2; 159653-

49-3; 160875-66-1; 160901-20-2; 160901-09-7; 160901-19-9; 161025-21-4; 161025-22-5; 166736-08-9; 169107-

21-5; 172588-43-1; 176022-76-7; 196823-11-7; 287935-46-0; 288260-45-7; 303176-75-2; 954108-36-2)

Surfactants, related 

adjuvants of

surfactants.

α-alkyl (minimum C6 linear, branched, saturated and/or unsaturated)-ω-hydroxypolyoxyethylene polymer with or 

without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, 

Not to exceed 30% 

of formulation

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calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum 

oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. Nos.: 9004-80-2, 9046-

01-9, 26982-05-8, 31800-89-2, 37280-82-3, 37281-86-0, 39341-09-8, 39341-65-6, 39464-66-9, 39464-69-2, 

42612-52-2, 50643-20-4, 50668-50-3, 51325-10-1, 51884-64-1, 52019-36-0, 57486-09-6, 58206-38-5, 58318-

92-6, 58857-49-1, 59112-71-9, 60267-55-2, 61837-79-4, 62362-49-6, 62482-61-5, 63747-86-4, 63887-54-7, 

63887-55-8, 66020-37-9, 66272-25-1, 66281-20-7, 67711-84-6, 67786-06-5, 67989-06-4, 68070-99-5, 68071-

17-0, 68071-35-2, 68071-37-4, 68130-44-9, 68130-45-0, 68130-46-1, 68130-47-2, 68186-29-8, 68186-34-5, 

68186-36-7, 68186-37-8, 68238-84-6, 68311-02-4, 68311-04-6, 68332-75-2, 68389-72-0, 68400-75-9, 68413-

78-5, 68425-73-0, 68425-75-2, 68439-39-4, 68458-48-0, 68511-15-9, 68511-36-4, 68511-37-5, 68551-05-3, 

68585-15-9, 68585-16-0, 68585-17-1, 68585-36-4, 68585-39-7, 68603-24-7, 68607-14-7, 68610-64-0, 68610-

65-1, 68649-29-6, 68649-30-9, 68650-84-0, 68815-11-2, 68855-46-9, 68856-03-1, 68890-90-4, 68890-91-5, 

68891-12-3, 68891-13-4, 68891-26-9, 68908-64-5, 68909-65-9, 68909-67-1, 68909-69-3, 68921-24-4, 68921-

60-8, 68954-87-0, 68954-88-1, 68954-92-7, 68987-35-9, 69029-43-2, 69980-69-4, 70247-99-3, 70248-14-5, 

70844-96-1, 70903-63-8, 71965-23-6, 71965-24-7, 72480-27-4, 72623-67-7, 72623-68-8, 72828-56-9, 72828-

57-0, 73018-34-5, 73038-25-2, 73050-08-5, 73050-09-6, 73361-29-2, 73378-71-9, 73378-72-0, 73559-42-9, 

73559-43-0, 73559-44-1, 73559-45-2, 74499-76-6, 76930-25-1, 78041-18-6, 78330-22-0, 78330-24-2, 82465-

25-6, 84843-37-8, 91254-26-1, 93925-54-3, 95014-34-9, 96416-89-6, 99924-51-3, 103170-31-6, 103170-32-7, 

106233-09-4, 106233-10-7, 108818-88-8, 110392-49-9, 111798-26-6, 111905-50-1, 116671-23-9, 117584-36-8, 

119415-05-3, 120913-45-3, 121158-61-0, 121158-63-2, 123339-53-7, 125139-13-1, 125301-86-2, 125301-87-3, 

126646-03-5, 129208-04-4, 129870-77-5, 129870-80-0, 130354-37-9, 136504-88-6, 143372-50-3, 143372-51-4, 

144336-75-4, 146815-57-8, 151688-56-1, 154518-39-5, 154518-40-8, 155240-11-2, 159704-69-5, 160498-49-7, 

160611-24-5, 171543-66-1, 172027-16-6, 172274-69-0, 176707-42-9, 181963-82-6, 188741-55-1, 191940-53-1, 

210493-60-0, 210993-53-6, 246159-55-7, 251298-11-0, 261627-68-3, 290348-69-5, 290348-70-8, 317833-96-8, 

340681-28-9 , 422563-19-7, 422563-26-6, 522613-09-8, 717140-06-2, 717140-09-5, 717827-29-7, 762245-80-7, 

762245-81-8, 866538-89-8, 866538-90-1, 873662-29-4, 913068-96-9, 936100-29-7, 936100-30-0, 1072943-56-6, 

1087209-87-7, 1174313-54-2, 1187742-89-7, 1187743-35-6, 1205632-03-6, 1233235-49-8, 1451002-50-8, 

1456802-88-2, 1456802-89-3, 1456803-12-5)

Surfactants, related 

adjuvants of 

surfactants.

N-alkyl (C8-C18) primary amines and their acetate salts where the alkyl group is linear and may be saturated 

and/or unsaturated (CAS Reg. Nos. 61790-57-6, 61790-58-7, 61790-59-8, 61790-60-1, 61788-46-3, 61790-33-8, 

68155-38-4)

Concentration in 

formulated enduse products not 

to exceed 10% by 

weight in herbicide 

products, 4% by 

weight in 

insecticide 

products, and 4% 

by weight in 

fungicide products

Surfactants, related 

adjuvants of 

surfactants

Alkyl (C8-C18) sulfate and its ammonium, calcium, isopropylamine, magnesium, potassium, sodium, and zinc salts Surfactants.

Aluminum hydroxide Diluent, carrier

Aluminum oxide Diluent

Aluminum stearate Surfactant

Amides, C5-C9, N-[3-(dimethylamino) propyl] (CAS Reg. No. 1044764-00-2) Surfactant

Amides, C6-C12, N-[3-(dimethylamino) propyl] (CAS Reg. No. 1044764-06-8) Surfactant

Ammonium bicarbonate Surfactant, 

suspending agent, 

dispersing agent

Ammonium carbamate Synergist in aluminum 

phosphide 

formulations

Ammonium chloride Intensifier when used 

with ammonium nitrate 

as a dessicant or 

defoliant. Fire 

suppressant in 

aluminum phosphide 

and magnesium 

phosphide 

formulations

Ammonium hydroxide Solvent, cosolvent, 

neutralizer, solubilizing 

agent

Ammonium salts of fatty acids (C8-C18 saturated) (CAS Reg. No. 5972-76-9, 63718-65-0, 16530-70-4, 32582-95-9, 

2437-23-2, 191799-95-8, 16530-71-5, 93917-76-1, 5297-93-8, 94266-36-1, 1002-89-7)

Surfactant

Ammonium stearate Surfactant

Ammonium sulfate Solid diluent, carrier

Ammonium thiosulfate Intensifier when used 

with ammonium nitrate 

as desiccant or 

defoliant

Amyl acetate Solvent, cosolvent, 

attractant

Ascorbyl palmitate Preservative

Attapulgite-type clay Solid diluent, carrier, 

thickener

Bacillus thuringiensis fermentation solids and/or solubles Diluent, carrier

Bentonite Solid diluent, carrier

Benzoic acid Preservative for 

formulation

Bicyclo[3.1.1]hept-2-ene, 2,6,6-trimethyl-, homopolymer (Alpha-pinene, homopolymer)(CAS Reg. No. 25766-18-1) Surfactants, related 

adjuvants of 

surfactants

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Bicyclo[3.1.1]heptane, 6,6-dimethyl-2-methylene-, homopolymer (Beta-pinene, homopolymer) (CAS Reg. No. 

25719-60-2)

Surfactants, related 

adjuvants of 

surfactants

Bicyclo[3.1.1]hept-2-ene, 2,6,6-trimethyl-, polymer with 6,6-dimethyl-2-methylenebicyclo [3.1.1] heptane 

(Copolymer of alpha- and beta-pinene) (CAS Reg. No. 31393-98-3)

Surfactants, related 

adjuvants of 

surfactants

2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52-51-7) 0.04% or less by 

weight of the total 

pesticide 

formulation

In-can preservative

Butane Propellant

n-Butanol (CAS Reg. No. 71-36-3) Solvent, cosolvent

n-Butyl benzoate (CAS Reg. No.136-60-7) Solvent

Butylated hydroxyanisole Antioxidant

Butylated hydroxytoluene Do.

Calcareous shale Solid diluent carrier

Calcite Do.

Calcium carbonate Do.

Calcium chloride Stabilizer

Calcium phosphate Solid diluent, carrier

Calcium hydroxide Do.

Calcium hypochlorite Sanitizing and 

bleaching agent

Calcium lactate pentahydrate (CAS Reg. No. 5743-47-5) Nutrient, stabilizer

Calcium oxide Solid diluent, carrier

Calcium salt of partially dimerized rosin, conforming to 21 CFR 172.210 Coating agent

Calcium silicate Solid diluent, carrier

Calcium stearate Do.

Carbon Dioxide (CAS Reg. No. 124-38-9) None Propellant

Carrageenan, conforming to 21 CFR 172.620 Minimum 

molecular weight 

(in amu): 100,000

Thickener

Cetyl alcohol (CAS Reg. No. 36653-82-4) Not more than 

5.0% of pesticide 

formulation

Evaporation retardant

Charcoal, activated Meets 

specifications in 

the Food Chemical 

Codex

Carrier

Coconut shells Solid diluent and 

carrier

Cod liver oil Solvent, cosolvent

Croscarmellose sodium (CAS Reg. No. 74811-65-7) Disintegrant, solid 

diluent, carrier, and 

thickener

n-Decyl alcohol (CAS Reg. No. 112-30-1) Solvent or co-solvent

Dialkyl (C8-C18) dimethyl ammonium chloride Not more than 

0.2% in silica, 

hydrated silica

Flocculating agent in 

the manufacture of 

silica, hydrated silica 

for use as a solid 

diluent, carrier

Diatomite (diatomaceous earth) Solid diluent carrier

Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-75-4)

Surfactant

Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-83-4)

Surfactant

Diethylaminoethanol, ethoxylated, reaction product with fatty acid dimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-72-1)

Surfactant

Diethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-81-2)

Surfactant

Diethylene glycol abietate Surfactants, related 

adjuvants of 

surfactants

1,1-Difluoroethane (CAS Reg. No. 75-37-6) For aerosol 

pesticide 

formulations used 

for insect control in 

food- and feedhandling 

establishments 

and animals

Aerosol propellant

1,2-Dihydro-6-ethoxy-2,2,4-trimethylquinolene Not more than 

0.02% of pesticide 

formulation

Antioxidant

Diisopropanolamine (CAS Reg. No. 110-97-4) Not to exceed 10% 

by weight of 

pesticide 

formulation

Neutralizer or 

stabilizer

Diisopropyl adipate (CAS Reg. No. 6938-94-9) Solvent, co-solvent.

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40% in mosquito 

control 

formulations

Dimethyl adipate (CAS no. 627-93-0) None Solvent/co-solvent

Dimethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-42-5)

Surfactant

Dimethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-67-4)

Surfactant

Dimethylaminoethanol, ethoxylated, reaction products with fatty acid dimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-38-9)

Surfactant

Dimethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-49-2)

Surfactant

Dimethyl ether (methane, oxybis-) (CAS Reg. No. 115-10-6) Propellant

Dimethyl glutarate (CAS no. 1119-40-0) None Solvent/co-solvent

3,6-Dimethyl-4-octyn-3,6-diol Not more than 

2.5% of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

Dimethyl succinate (CAS no. 106-65-0) None Solvent/co-solvent

Di-n-butyl carbonate (CAS Reg. No. 542-52-9) Solvent

Dipropylene glycol Solvent, cosolvent

Disodium phosphate Anticaking agent, 

conditioning agent

Disodium zinc ethylenediaminetetraacetate dihydride Sequestrant

Distillates, (Fishcher-Tropsch), heavy, C18-C50, branched, cyclic and linear (CAS Reg. No. 848301-69-9) Solvent, diluent and/or 

dust suppressant

Dolomite Solid diluent, carrier

Epoxidized linseed oil Surfactants, related 

adjuvants of 

surfactants

Epoxidized soybean oil Do.

Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No. 107-36-8) Chelator, sequestrant, 

or conditioning agent

Ethanesulfonic acid, 2-hydroxy-, ammonium salts (CAS Reg. No. 57267-78-4) Do.

Ethanesulfonic acid, 2-hydroxy-, calcium salts (CAS Reg. No. 10550-47-7) Do.

Ethanesulfonic acid, 2-hydroxy-, magnesium salts (CAS Reg. No. 17345-56-1) Do.

Ethanesulfonic acid, 2-hydroxy-, potassium salts (CAS Reg. No. 1561-99-5) Do.

Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS Reg. No. 1562-00-1) Do.

Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS Reg. No. 129756-32-7) Do.

Ethyl acetate Solvent, cosolvent

Ethyl alcohol Do.

Ethyl esters of fatty acids derived from edible fats and oils Solvent, cosolvent

Ethyl maltol (CAS Reg. No.4940-11-8) Not more than 0.2 

% of the pesticide 

formulation

Odor masking agent

Ethylene glycol (CAS Reg. No. 107-21-1) Without limitation Encapsulating agent 

for pesticides being 

applied post-harvest 

as residual, and crack 

and crevice sprays in 

and around food and 

nonfood areas of 

residential and 

nonresidential 

structures, including 

food handling 

establishments 

Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, the ethylene oxide content averages 3.5, 10 or 30 

moles (CAS Reg. No. 9014-85-1)

Surfactants, related 

adjuvants of 

surfactants

(S,S)-Ethylenediamine disuccinic acid trisodium salt (CAS Reg. No. 178949-82-1) Sequestrant or 

chelating agent

Ethylenediaminetetraacetic acid 3% of pesticide 

formulation

Sequestrant

Ethylenediaminetetraacetic acid, tetrasodium salt 5% of pesticide 

formulation

Sequestrant

2-Ethyl-1-hexanol (CAS Reg. No. 104-76-7) Not more than 

10% of pesticide

Solvent, adjuvant of 

surfactants

Fatty acids, conforming to 21 CFR 172.860 Binder, defoaming 

agent, lubricant

FD&C Blue No. 1 Not more than 

0.2% of pesticide 

formulation

Dye

FD&C Red No. 40 (CAS Reg. No. 25956-17-6) conforming to 21 CFR 74.340 Not to exceed 

0.002% by weight 

of pesticide 

formulation

Dye, coloring agent

Ferric Citrate (CAS Reg. No. 2338-05-8) Stabilizer

Ferric sulfate Solid diluent, carrier

Furcelleran Thickener

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D-glucopyranose, oligomeric, C10-16-alkyl glycosides (CAS Reg. No. 110615-47-9) Surfactant

D-glucopyranose, oligomeric, 6-(dihydrogen citrates), C8-20 branched and linear alkyl glycosides, sodium salts 

(CAS Reg. No. 1079993-97-7)

Surfactant

D-glucopyranose, oligomeric, 6-(hydrogen sulfosuccinates), C8-20 branched and linear alkyl glycosides, sodium 

salts (CAS Reg. No. 1079993-92-2)

Surfactant

D-glucopyranose, oligomeric, lactates, C8-20 branched and linear alkyl glycosides (CAS Reg. No. 1079993-94-4) Surfactant

Glycerides, edible fats and oils derived from plants and animals, reaction products with sucrose (CAS Reg. Nos. 

100403-38-1, 100403-41-6, 100403-39-2, 100403-40-5)

Emulsifier, dispersing 

agent

Glycerol mono-, di-, and triacetate Solvent, cosolvent

Glyceryl monostearate Emulsifier

Granite Do.

Graphite Solid diluent, carrier

Gum arabic (acacia) Surfactant, 

suspending agent, 

dispersing agent

Gypsum Solid diluent, carrier

Hexamethylenetetramine For use in citrus 

washing solutions 

only at not more 

than 1%

Preservative

3-hexen-1-ol, (3Z)- (CAS Reg. No. 928-96-1) Not more than 

0.4% of the 

pesticide 

formulation

Odorant, alerting 

agent

n-Hexyl alcohol (CAS Reg. No. 111-27-3) Solvent, cosolvent

C9 rich aromatic hydrocarbons (CAS Reg. No. 64742-95-6) Solvent

C10-11 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5) Solvent

C11-12 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5) Solvent

Hydrochloric acid Solvent, neutralizer

Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-06-4)

Surfactant

Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-17-7)

Surfactant

Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid dimers, minimum number average 

molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-00-8)

Surfactant

Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid trimers, minimum number average 

molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-09-7)

Surfactant

Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-22-4

Surfactant

Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-28-0)

Surfactant

Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid dimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173189-20-2)

Surfactant

Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173189-25-7)

Surfactant

Hydroxyethylidine diphosphonic acid (HEDP) (CAS Reg. No. 2809-21-4) For use in 

antimicrobial 

pesticide 

formulations at not 

more than 1 

percent

Stabilizer, chelator

Iron oxide Solid diluent, carrier

Isobutane (CAS Reg. No. 75-28-5) None Propellant

Isopropyl myristate (CAS Reg. No. 110-27-0) Solvent

Kaolinite-type clay Solid diluent, carrier

Lactic acid Solvent

Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283-86-9) Solvent

Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No. 186817-80-1) Solvent

Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651-69-7) Solvent

Lauryl alcohol Surfactant

Lignin (CAS Reg. No. 9005-53-2) Surfactant, related 

adjuvants of 

surfactants

Lignin, alkali (CAS Reg. No. 8068-05-1) Do.

Lignin, alkali, oxidized, sodium salt (CAS Reg. No. 68201-23-0) Do.

Lignin alkali reaction products with disodium sulfite and formaldehyde (CAS Reg. No. 105859-97-0) Do.

Lignin alkali reaction products with formaldehyde and sodium bisulfite (CAS Reg. No. 68512-35-6) Do.

Lignosulfonic acid (CAS Reg. No. 8062-15-5) Do.

Lignosulfonic acid, ammonium calcium salt (CAS Reg. No. 12710-04-2) Do.

Lignosulfonic acid, ammonium magnesium salt (CAS Reg. No. 123175-37-1) Do.

Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061-53-8) Do.

Lignosulfonic acid, ammonium sodium salt (CAS Reg. No. 166798-73-8) Do.

Lignosulfonic acid, calcium magnesium salt (CAS Reg. No. 55598-86-2) Do.

Lignosulfonic acid, calcium salt (CAS Reg. No. 8061-52-7) Do.

Lignosulfonic acid, calcium sodium salt (CAS Reg. No. 37325-33-0) Do.

Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg. No. 68611-14-3) Do.

Lignosulfonic acid, magnesium salt (CAS Reg. No. 8061-54-9) Do.

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Lignosulfonic acid, potassium salt (CAS Reg. No. 37314-65-1) Do.

Lignosulfonic acid, sodium salt (CAS Reg. No. 8061-51-6) Do.

Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No. 68855-41-4) Do.

Lignosulfonic acid, sodium salt, polymer with formaldehyde and phenol (CAS Reg. No. 37207-89-9) Do.

Lignosulfonic acid, sodium salt, sulfomethylated (CAS Reg. No. 68512-34-5) Do.

Lignosulfonic acid, zinc salt (CAS Reg. No. 57866-49-6) Do.

d-Limonene (CAS Reg. No. 5989-27-5) Solvent, fragrance

Magnesium carbonate Anticaking agent, 

conditioning agent

Magnesium chloride Safener

Magnesium lime Solid diluent, carrier

Magnesium oxide Do.

Magnesium silicate Do.

Magnesium stearate Surfactant

Magnesium sulfate Solid diluent, carrier, 

safener

Methyl alcohol Solvent

Methyl n-amyl ketone (CAS Reg. No. 110-43-0) Solvent, cosolvent

Methyl 5-(dimethylamino)-2-methyl-5-oxopentanoate (1174627-68-9) Solvent

Methyl esters of fatty acids derived from edible fats and oils Solvent, cosolvent

Methyl esters of higher fatty acids conforming to 21 CFR 573.640 Antidusting agent, 

surfactant

Methyl isobutyl ketone Solvent

2-methyl-2,4-pentanediol (CAS Reg. No. 107-41-5) Without limitation Growing crops and 

food animals

2-methyl-1,3-propanediol (CAS Reg. No. 2163-42-0) Solvent, surfactant

Methylated silicones Antifoaming agent

Mono-, di-, and trimethylnapthalenesulfonic acids and napthalenesulfonic acids formaldehyde condensates, 

ammonium and sodium salts (CAS Reg. Nos 9008-63-3, 9069-80-1, 9084-06-4, 36290-04-7, 91078-68-1, 141959-

43-5, 68425-94-5)

Surfactants, related 

adjuvants of 

surfactants

Mica Solid diluent, carrier

Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or 178.3620(a) (CAS Reg. No. 8012-95-1) Diluent, carrier, and 

solvent

Monoammonium phosphate No more than 

3.75% by weight in 

formulation

Postharvest 

fumigation in 

formulation with 

aluminum phosphide

Mono- and diglycerides of C8-C18 fatty acids Surfactants, related 

adjuvants of 

surfactants

Montmorillonite-type clay Solid diluent, carrier

Nonyl, decyl, and undecyl glycoside mixture with a mixture of nonyl, decyl, and undecyl oligosaccharides and 

related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% 

solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% 

C9, 40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8)

Surfactant.

α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate 

esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the 

phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 

or 30 moles (CAS Reg. Nos. 51811-79-1, 59139-23-0, 67922-57-0, 68412-53-3, 68553-97-9, 68954-84-7, 99821-

14-4, 152143-22-1, 51609-41-7, 37340-60-6, 106151-63-7, 68584-47-4, 52503-15-8, 68458-49-1)

Not to exceed 7% 

of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of nonylphenol (nonyl 

group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide; if a blend of 

products is used, the average number of moles of ethylene oxide reacted to produce any product that is a 

component of the blend shall be in the range of 4-14 or 30-90

Surfactants, related 

adjuvants of 

surfactants

α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) sulfate, ammonium, calcium, magnesium, potassium, sodium, and 

zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS 

Reg. Nos. 9014-90-8, 9051-57-4, 9081-17-8, 68649-55-8, 68891-33-8

Not to exceed 7% 

of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

1-Octanal (CAS Reg. No. 124-13-0) Not more than 

0.2% of the 

pesticide 

formulation

Odor masking agent

n-Octyl alcohol (CAS Reg. No. 111-87-5) Solvent or co-solvent

Octyl and decyl glucosides mixture with a mixture of octyl and decyloligosaccharides and related reaction products 

(primarily n- decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain 

alcohols (C8(45%), C10 (55%)) with anhydrous glucose

Surfactants, related 

adjuvants of 

surfactants

Oleic acid Diluent

Oleic acid diester of α-hydro-ω-hydroxypoly (oxyethylene); the poly(oxyethylene) having average molecular weight 

(in amu) 400

Surfactants, related 

adjuvants of 

surfactants

α-Oleoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600 Emulsifier

Oleyl alcohol (CAS Reg. No. 143-28-2 15% Cosolvent

Oxalic acid No more oxalic 

acid should be 

used than is 

necessary to 

chelate calcium 

and in no case 

should more than 

2 lb oxalic acid per 

acre be used

Calcium chelating 

hard water inhibitor

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Palmitic acid Diluent

Pentaerythritol ester of maleic anhydride modified wood rosin Plasticizer

Petrolatum, conforming to 21 CFR 172.880 Coating agent

Petroleum hydrocarbons, light odorless conforming to 21 CFR 172.884 Solvent, diluent.

Petroleum hydrocarbons, synthetic isoparaffinic, conforming to 21 CFR 172.882 Do.

Petroleum naphtha, conforming to 21 CFR 172.250(d) Component of coating 

agent

Petroleum wax, conforming to 21 CFR 172.886(d) Coating agent

Phosphoric acid Buffer

Polyethylene, conforming to 21 CFR 177.1520(c) Binder, carrier, and 

coating agent

Polyethylene glycol[α-hydro-ω-hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms 

to 21 CFR 178.3750

Surfactants, related 

adjuvants of 

surfactants

Polyglycerol esters of fatty acids conforming to 21 CFR 172.854 Surfactants, related 

adjuvants of 

surfactants

Polyglyceryl phthalate ester of coconut oil fatty acids, including fatty acid coco polymers with glyceryl and phthalic 

anhydride (CAS No. 67746-02-5) and coconut oil polymer with glyceryl and phthalic anhydride (CAS No. 66070-

87-9)

None Surfactants, related 

adjuvants of 

surfactants

Poly(oxy-1,2-ethanediyl), α-(carboxymethyl)-ω-(nonylphenoxy) produced by the condensation of 1 mole of 

nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-90 moles of ethylene oxide. 

The molecular weight (in amu) ranges are 454-894 and 1598-4238

Surfactant

Poly(oxy-1,2-ethanediyl), α-[tris(1-phenylethyl)phenyl]-ω-hydroxy-, (CAS Reg. No. 99734-09-5) For use in postharvest 

applications; not to 

exceed 15% by 

weight in pesticide 

formulations

Surfactants

Polyoxyethylene (20) sorbitan monostearate Surfactants, related 

adjuvants of 

surfactants

[Poly[oxy(methyl-1,2-ethanediyl)], α-[2-bis(2-hydroxyethyl)amino]propyl]-ω-hydroxy,-ether with α-hydro-ωhydroxypoly(oxy-1,2-ethanediyl) (1:2), mono-C12-16 alkyl ethers, (CAS Reg. No. 176022-82-5)

Not to exceed 15% 

in the formulated 

product; only for 

use with 

glyphosate

Surfactant

Polysorbate 65, conforming to 21 CFR 172.838 Emulsifier

Potassium aluminum silicate Solid diluent, carrier

Potassium benzoate (Cas No. 582-25-2) None Preservative

Potassium hydroxide Neutralizer

Potassium phosphate Buffer

Potassium sulfate Solid diluent

Propane Propellant

1,3-Propanediol (CAS Reg. No. 504-63-2) Solvent, co-solvent, 

diluent, or freeze-point 

depressant

2-Propanol, 1,1′,1′′-nitrilotris- (CAS No. 122-20-3) Without limitation Neutralizer

n-Propanol Solvent, cosolvent

2-Propenoic acid, 2-methyl-, polymer with ethyl 2-propenoate and methyl 2-methyl-2-propenoate, ammonium salt 

(CAS Registration No. 55989-05-4), minimum number average molecular weight (in amu), 18,900.

Encapsulating agent, 

dispensers, resins, 

fibers and beads

Propyl gallate Antioxidant

Propyl p-hydroxybenzoate Preservative for 

formulations

Propylene glycol Solvent, cosolvent.

Propylene glycol alginate (as defined in 21 CFR 172.858) Defoaming agent

Propylene glycol monomethyl ether (CAS No. 107-98-2) none solvent

Pyrophyllite Solid diluent, carrier

Rhizobium inoculants (e.g. Sinorhizobium, Bradyrhizobium & Rhizobium) All leguminous food 

commodities

Rosin, partially dimerized (as defined in 21 CFR 172.615) Surfactants, related 

adjuvants of 

surfactants

Rosin, partially hydrogenated (as defined in 21 CFR 172.615) Do.

Rosin, wood Do.

Salts of fatty acids, conforming to 21 CFR 172.863 Binder, emulsifier, 

anticaking agent

Sand Solid diluent, carrier

Shellac, bleached; refined, food grade, arsenic and rosin-free Coating agent

Silver nitrate (Cas Reg. No. 7761-88-8) For use on 

potatoes as postharvest treatment 

to control 

sprouting at no 

more than 0.06% 

by weight in 

pesticide 

formulations

Stabilizer

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Soapstone Solid diluent

Sodium acid pyrophosphate Surfactant, 

suspending agent, 

dispersing agent, 

buffer

Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. 68909-83-1, 68909-84-2, 68909-82-0, 27213-90-7, 26264-

58-4, 27178-87-6, 111163-74-7, 908356-16-1, 25417-20-3, 25638-17-9, 145578-88-7, 1322-93-6, 1323-19-9, 

7403-47-6, 68442-09-1, 127646-44-0, 908356-18-3)

Limited to no more 

than 30% by 

weight in pesticide 

end-use products

Surfactants, related 

adjuvants of 

surfactants

Sodium aluminum silicate Solid diluent, carrier

Sodium dioctylsulfosuccinate Surfactants, related 

adjuvants of 

surfactants

Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006-15-3) Surfactants, related 

adjuvants of 

surfactants

Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127-39-9) Surfactants, related 

adjuvants of 

surfactants

Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922-80-5) Surfactants, related 

adjuvants of 

surfactants

Sodium DL-lactate (CAS Reg. No. 72-17-3) Surfactant

Sodium hexametaphosphate Surfactant, emulsifier, 

wetting agent, 

suspending agent, 

dispersing agent, 

buffer

Sodium hydroxide Neutralizer

Sodium L-lactate (CAS Reg. No. 867-56-1) Surfactant

Sodium metasilicate Surfactants, 

emulsifiers, wetting 

agents, dispersing 

agents, buffer

Sodium monoalkyl and dialkyl (C6-C16) phenoxy benzenedisulfonates and related acids (CAS Reg. Nos. 147732-

59-0, 147732-60-3, 169662-22-0, 70191-75-2, 36445-71-3, 39354-74-0, 70146-13-3, 119345-03-8, 149119-20-0, 

149119-19-7, 119345-04-9, 28519-02-0, 25167-32-2, 30260-73-2, 65143-89-7, 70191-76-3)

Not to exceed 20% 

in pesticide 

formulations

Surfactants, related 

adjuvants of 

surfactants

Sodium α-olefinsulfonate (sodium C14-C16) (Olefin sulfonate) Surfactants, related 

adjuvants of 

surfactants

SodiumN-oleoyl- N-methyl taurine (CAS Reg. No. 137-20-2) Surfactants, related 

adjuvants of 

surfactants

Sodium and potassium salts of N-alkyl (C8-C18)-beta-iminodipropionic acid where the C8-C18 is linear and may be 

saturated and/or unsaturated (CAS Reg. Nos. 110676-19-2, 3655-00-3, 61791-56-8, 14960-06-6, 26256-79-1, 

90170-43-7, 91696-17-2, 97862-48-1)

Concentration in 

formulated enduse products not 

to exceed 30% by 

weight in pesticide 

formulations

Surfactants, related 

adjuvants of 

surfactants

Sodium salt of sulfated oleic acid Surfactants, related 

adjuvants of 

surfactants

Sodium silicate Surfactant, emulsifier, 

wetting agent, 

stabilizer, inhibitor

Sodium starch glycolate (CAS Reg. No. 9063-38-1) Granular and 

tableted products 

only; not to exceed 

8% of the 

formulated product

Disintegrant

Sodium sulfate Solid diluent, carrier

Sodium tripolyphosphate Buffer, surfactant, 

suspending agent, 

dispersing agent, 

anticaking agent, 

conditioning agent

Sorbic acid (CAS Reg. No. 110-44-1) Preservative for 

formulations

Sorbitan fatty acid esters (fatty acids limited to C12, C14, C16, and C18 containing minor amounts of associated fatty 

acids) and their derivatives; the poly(oxyethylene) content averages 5-20 moles

Surfactants, related 

adjuvants or 

surfactants.

Soybean flour Expires May 24, 

2005.

Surfactant

Soybean oil-derived fatty acids Solvent, cosolvent

Stearic acid Diluent

α-Stearoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600 Emulsifier

α-Stearoyl-ω-hydroxypoly(oxyethylene); the poly(oxyethylene) content averages either 8, 9, or 40 moles; if a blend 

of products is used, the average number of moles ethylene oxide reacted to produce any product that is a 

component of the blend shall be either 8, 9, or 40

Surfactants, related 

adjuvants of 

surfactants

Sucrose octaacetate Adhesive

Sulfite liquors and cooking liquors, spent, oxidized (CAS Reg. No. 68514-09-0)

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Surfactant, related 

adjuvants of 

surfactants

Sulfuric acid (CAS Reg. No.7664-93-9) Not to exceed 10% 

of the pesticide 

formulation; nonaerosol 

formulations only

pH Control agent

Sweet orange peel tincture (CAS Reg. No. 8028-48-6) Not to exceed 10% 

(weight/weight) in 

pesticide 

formulation

Surfactant, fragrance, 

related adjuvants of 

surfactants

Synthetic paraffin and its succinic derivatives conforming to 21 CFR 172.275 Carrier, binder, and 

carrying agent

Synthetic petroleum wax, conforming to 21 CFR 172.888 Binder, carrier, and 

coating agent

Talc Solid diluent, carriers

Tall oil; fatty acids not less than 58%, rosin acids not more than 44%, unsaponifiables not more than 8% Surfactants, related 

adjuvants of 

surfactants

Tartrazine Dye

Terpenes and terpenoids, turpentine oil, alpha-pinene fraction, polymd. (CAS Reg. No. 70750-57-1) Surfactants, related 

adjuvants of 

surfactants

1,1,1,2-Tetrafluoroethane, (CAS Reg. No. 811-97-2) Aerosol propellant

Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No. 29118-24-9) Propellant

Tetrahydrofurfuryl alcohol (THFA) (CAS Reg. No 97-99-4) Expires February 

9, 2008

Solvent/cosolvent

N,N,N′,N′′,-tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Reg. No. 102-60-3) Concentration in 

formulated enduse products not 

to exceed 20% by 

weight in pesticide 

formulations

Stabilizer for 

formulation.

α-[p-(1,1,3,3-tetramethylbutyl)phenyl]-ω-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of 

p-(1,1,3,3-tetramethylbutyl)phenol with a range of 1-14 or 30-70 moles of ethylene oxide: If a blend of products is 

used, the average range number of moles of ethylene oxide reacted to produce any product that is a component of 

the blend shall be in the range of 1-14 or 30-70 (CAS Reg. Nos. 9036-19-5, 9002-93-1)

Not to exceed 7% 

of pesticide 

formulation

Surfactants related 

adjuvants of 

surfactants

2,4,7,9-Tetramethyl-5-decyn-4, 7-diol Not more than 

2.5% of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

Tetrasodium pyrophosphate Anticaking agent, 

conditioning agent

Thiosulfuric acid, disodium salt, anhydrous. (CAS Reg. No 7772-98-7) Dechlorinator, 

reducing agent

Thiosulfuric acid, disodium salt, pentahydrate. (CAS Reg. No. 10102-17-7) Do.

d-Alpha tocopherol (CAS Reg. No. 9-02-9 None Safener

d-Alpha tocopheryl acetate (CAS Reg. No. 58-95-7) None Do.

dl-Alpha tocopherol (CAS Reg. No.10191-41-0) None Do.

dl-Alpha tocopheryl acetate (CAS Reg. No. 7695-91-2) None Do.

Tricalcium phosphate Surfactant, 

suspending agent, 

dispersing agent, 

anticaking agent, 

conditioning agent

Trisodium phosphate Surfactant, emulsifier, 

wetting agent

Vermiculite Solid diluent, carrier.

Vitamin E (CAS Reg. No. 1406-18-4) None Safener

Walnut shells Leaching inhibitor, 

binder for waterdispersible 

aggregates, sticker 

and suspension 

stabilizer

Wintergreen oil Attractant

Wood flour Derived from wood 

free of chemical 

preservatives

Solid diluent and 

carrier

Xanthan gum-modified, produced by the reaction of xanthan gum and glyoxal (maximum 0.3% by weight) Not more than 

0.5% of pesticide 

formulation

Surfactant

Xylene meeting the specifications listed in 21 CFR 172.884(b)(4) In pesticide 

formulations for 

grain storage only

Solvent, cosolvent

Zeolite (hydrated alkali aluminum silicate) Solid diluent, carrier

Zinc oxide Coating agent

Zinc sulfate (basic and monohydrate) Do.

Zinc sulfate (basic and monohydrate) Solid diluent, carrier

[69 FR 23117, Apr. 28, 2004]

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EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.910, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.920 Inert ingredients used pre-harvest; exemptions from the requirement of a tolerance.

The following materials are exempted from the requirement of a tolerance when used in accordance with good 

agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to growing crops only:

Inert ingredients Limits Uses

Acetophenone Attractant

Adenosine (CAS Reg. No. 58-61-7) Maximum of 0.5% of formulation Synergist

Alder bark Seed germination stimulator

Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. Nos. 683-10-3, 2601-33-4 and 693-

33-4

20% by weight in pesticide 

formulation

Surfactant

α-Alkyl (minimum C6 linear, branched, saturated and/or unsaturated)-ωhydroxypolyoxyethylene polymer with or without polyoxypropylene, mixture of di- and 

monohydrogen phosphate esters and the corresponding ammonium, calcium, magnesium, 

monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum 

oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles (CAS Reg. 

Nos. 9046-01-9, 37280-82-3, 39464-66-9, 42612-52-2, 50643-20-4, 52019-36-0, 58318-

92-6, 60267-55-2, 61837-79-4, 67711-84-6, 68070-99-5, 68071-35-2, 68071-17-0, 68130-

47-2, 68186-37-8, 68186-36-7, 68311-02-4, 68425-73-0, 68458-48-0, 68511-37-5, 68610-

65-1, 68585-36-4, 68649-29-6, 68815-11-2, 68908-64-5, 68891-13-4, 73038-25-2, 78330-

24-2, 108818-88-8, 154518-39-5, 317833-96-8, 873662-29-4, 936100-29-7, 936100-30-0)

Not to exceed 30% of pesticide 

formulation

Surfactants, related 

adjuvants of surfactants

N-alkyl(C8-C18) dimethylamidopropylamines where the alkyl group is linear and may be 

saturated and/or unsaturated (CAS Reg. Nos. 109-28-4, 3179-80-4, 7651-02-7, 22890-

10-4, 22890-11-5, 39669-97-1, 45267-19-4, 68140-01-2, 1147459-12-8, 146987-98-6)

Not to exceed 20% by weight in 

herbicide formulations

Surfactants, related 

adjuvants of surfactants

N-alkyl (C8-C18) primary amines and their acetate salts where the alkyl group is linear and 

may be saturated and/or unsaturated (CAS Reg. Nos. 61790-57-6, 61790-58-7, 61790-

59-8, 61790-60-1, 61788-46-3, 61790-33-8, 68155-38-4)

Concentration in formulated end-use 

products not to exceed 10% by 

weight in herbicide products, 4% by 

weight in insecticide products, and 

4% by weight in fungicide products

Surfactants, related 

adjuvants of surfactants

N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl) C8-C18 saturated and unsaturated 

alkylamines; the poly(oxy-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 10213-

78-2, 25307-17-9, 26635-92-7, 26635-93-8, 288259-52-9, 58253-49-9, 61790-82-7, 

61791-14-8, 61791-24-0, 61791-26-2, 61791-31-9, 61791-44-4, 68155-33-9, 68155-39-5, 

68155-40-8,70955-14-5, 73246-96-5, 1266162-49-5)

Not to exceed 25% in herbicide 

formulations and 10% in insecticide 

and fungicide formulations

Surfactants, related 

adjuvants of surfactants

N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18

saturated and unsaturated alkylamines; the poly(oxy-1,2-ethanediyl/oxy

(methyl-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 68213-26-3, 68153-97-9, 

75601-76-2)

Not to exceed 25% in herbicide 

formulations and 10% in insecticide 

and fungicide formulations

Surfactants, related 

adjuvants of surfactants

Aluminum sulfate Safener adjuvant

Ammonium chloride (CAS Reg. No. 12125-02-9) Carrier/nutrient

Ammonium formate (CAS Reg. No. 540-69-2) Complexing or fixing agent 

Ammonium nitrate (CAS Reg. No. 6484-52-2) Adjuvant/ intensifier for 

herbicides

Ammonium polyphosphate (CAS Reg. No. 68333-79-9) Sequestrant, buffer, or 

surfactant

Barium sulfate Carrier

1,4-Benzenedicarboxylic acid, dimethyl ester, polymer with 1,4-butanediol, adipic acid, and 

hexamethylene diisocyanate, minimum number average molecular weight (in amu) 30,000 

(CAS Reg. No. 55231-08-8)

For use in honeybee hive miticide 

formulations

Component of controlled 

release agent

1,2-Benzisothiazolin-3-one Not more than 0.1% of formulation. 

Not more than 0.02 lb to be applied 

per acre

Preservative/stabilizer

Boric acid Sequestrant

Buffalo gourd root powder (Cucurbita foetidissima root powder); or, Zucchini juice 

(Cucurbita pepo juice) or Hawkesbury melon Citrullus lanatus.

No more than 2.5 lbs/acre/season 

(3.4 gm/acre/season of 

Cucurbitacin)

Gustatory stimulant

Butyl stearate Defoamer

γ-Butyrolactone Solvent

C.I. Pigment Blue #15 (CAS Reg. No. 147-14-8; containing no more than 50 ppm 

polychlorinated biphenyls (PCBs))

For seed treament use only Dye, coloring agent

C.I. Pigment Green #7 (CAS Reg. No. 1328-53-6; containing no more than 50 ppm 

polychlorinated biphenyls (PCBs))

For seed treatment use only Dye, coloring agent

C.I. Pigment Red #112 (CAS Reg. No. 6535-46-2) Seed treatment use only. Limited to 

10% w/w of pesticide formulation

Coloring agent

C.I. Pigment Violet #23 (CAS Reg. No. 6358-30-1; containing no more than 20 ppb of 

polychlorinated dibenzo-p-dioxins and/or polychlorinated dibenzofurans)

For seed treatment use only Dye, coloring agent

C.I. Pigment Yellow 1 (CAS Reg. No. 2512-29-0) Not to exceed 10% (weight/weight) 

in pesticide formulation

Colorant

Calcium gluconate (CAS Reg. No. 299-28-5) Sequestrant

Camphor (CAS Reg. No. 76-22-2) Not more than 5% weight to weight 

(w/w) of pesticide formulations

Deodorant, melting point 

adjustment

Carbon Black (CAS Reg. No. 1333-86-4) For seed treatment use only Colorant

Carbonic acid, dipotassium salt (CAS Reg. No. 584-08-7) Buffering agent

Carbonic acid, dipotassium salt, trihydrate (CAS Reg. No. 18662-52-7) Buffering agent

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Carboxymethyl guar gum sodium salt (CAS Reg. No. 39346-76-4) Without limitation Thicker/drift reduction agent

Carboxymethyl-hydroxypropyl guar (CAS Reg. No. 68130-15-4) Without limitation Thicker/drift reduction agent

Carous chloride 10 ppm in formulation Tagging agent

Carrageenan, conforming to 21 CFR 172.260 Not more than 0.15% of pesticide 

formulation

Thickener and stabilizer for 

pesticide formulations 

applied to seeds before 

planting

Chlorobenzene Contains not more than 1% 

impurities. Not for use after edible 

parts of plant begin to form. Do not 

graze livestock in treated areas 

within 48 hours after application

Solvent, cosolvent

5-Chloro-2-methyl-4-isothiazolin-3-one (in combination with 2-methyl-4-isothiazolin-3-one) Not more than 0.0022% (22.5 ppm) 

in the formulation; 0.00022% (or 

2.25 ppm) in the final solution 

applied to growing crops

Preservative

Choline chloride (CAS Reg. No. 67-48-1) As a solvent

Choline hydroxide (CAS Reg No. 123-41-1) Without limitation Neutralizer

Cis-isomer of 1-(3-chloroallyl)-3,5,7-triaza-1-azoniaadamantane chloride (CAS Reg. No. 

51229-78-8)

Maximum of 0.14% by weight of 

formulation

Preservative

Coco alkyl dimethyl amines (CAS Reg. No. 61788-93-0) Not to exceed 0.5% in pesticide 

formulation

Emulsifier

Copper naphthenate Not more than 2.5% of formulation; 

application limited to before edible 

portions of plants begin to form

Mercaptan scavenger in 

technical pesticide

Cyclohexane Solvent, cosolvent

Cyclohexanone Do.

Cysteine (CAS Reg. No. 52-90-4) Maximum of 0.5% of formulation Synergist

D&C Green No. 6 Dye

D&C Red No. 17, technical grade Dye

D&C Red No. 33 (CAS Reg. No. 3567-66-6); meeting the specifications listed in 21 CFR 

74.1333

Dye

D&C Violet No. 2, technical grade Not more than 0.005% of pesticide 

formulation

Dye

Decanamide, N,N-dimethyl (CAS Reg. No. 14433-76-2) Emulsifier, solvent, cosolvent

Diammonium phosphate (CAS Reg. No. 7783-28-0) Buffer, surfactant

dibenzylidene sorbitol (32647-67-9) Thinning agent

Diethanolamine Stabilizer, inhibitor for 

formulations used before 

crop emerges from soil

Diethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 26545-53-9, 

67815-95-6, 67889-94-5, 67889-95-6, 68259-34-7, 68478-47-7, 68567-68-0, 68815-34-9, 

68815-37-2, 68891-02-1, 68953-97-9, 84989-15-1, 85338-09-6, 90194-39-1, 90194-40-4, 

90218-08-9)

Not to exceed 7% of pesticide 

formulation

Surfactants, related 

adjuvants of surfactants.

Diethylene glycol Deactivator, adjuvant for 

formulations used before 

crop emerges from soil

Diethylene Glycol (CAS No. 111-46-6) Without limitation Solvent, stabilizer and/or 

antifreeze

Diethylene glycol and diethylene glycol monobutyl, monoethyl, and monomethyl ethers Deactivator for formulations 

used before crop emerges 

from soil, stabilizer

Diethylene glycol mono butyl ether (CAS Reg. No. 112-34-5) Without limitation Pesticide inert ingredient as 

a solvent, stabilizer and/or 

antifreeze

Diethylene Glycol MonoEthyl Ether (CAS Reg. No. 111-90-0) Without limitation Solvent, stabilizer and/or 

antifreeze

Dimethylaminopropylamine, isopropylamine, ethanolamine, and triethanolamine salts of 

alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 3088-30-0, 12068-12-1, 26264-05-1, 

26836-07-7, 27323-41-7, 55470-69-4, 58089-99-9, 61886-59-7, 61931-76-8, 67924-05-4, 

68110-32-7, 68259-35-8, 68411-31-4, 68442-72-8, 68567-69-1, 68584-24-7, 68584-25-8, 

68648-81-7, 68648-96-4, 68649-00-3, 68815-30-5, 68815-35-0, 68910-32-7, 68953-93-5, 

68953-98-0, 70528-84-6, 72391-21-0, 84961-74-0, 85480-55-3, 85480-56-4, 85995-82-0, 

90194-42-6, 90194-53-9, 90194-54-0, 90194-55-1, 90218-09-0, 90218-11-4, 90218-35-2, 

96687-54-6, 99924-49-9, 121617-08-1, 157966-96-6, 193562-36-6, 319926-68-6, 877677-

48-0, 1093628-27-3)

Surfactants, related 

adjuvants of surfactants.

3,6-Dimethyl-4-octyn-3,6-diol In pesticide formulations, for soil 

prior to planting or to plants before 

edible parts form

Surfactants, related 

adjuvants of surfactants

Dimethyl sulfoxide Solvent or cosolvent for 

formulations used before 

crop emerges from soil or 

prior to formation of edible 

parts of food plants

Dimethyl sulfoxide (CAS No. 67-68-5) For pesticide formulations used 

before crop emerges from soil or 

prior to formation of edible parts of 

food plants; for pesticide 

formulations used after crop 

emerges but before harvest, 

provided that the potential for 

increased residues of the 

Solvent or co-solvent

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formulation's active ingredient(s) in 

or on food commodities has been 

assessed

Dipotassium hydrogen phosphate Buffering agent

Dipropylene glycol monomethyl ether Stabilizer

Douglas-fir bark, ground Solid diluent, carrier

Dysprosium chloride 10 ppm in formulation Tagging agent

1,2-ethanediamine,N,N,N′′, N′′-tetramethyl-, polymer with 1,1′-oxybis[2-chloroethane] (CAS 

Reg. No. 31075-24-8)

For use in pesticide formulations 

applied to cotton or wheat only

Adjuvant or water conditioner

(S,S)-Ethylenediaminedisuccinic acid (CAS Reg. No. 20846-91-7) Sequestrant or chelating 

agent

Ethylene glycol Antifreeze, deactivator for all 

pesticides used before crop 

emerges from soil and in 

herbicides before or after 

crop emerges

Ethylene glycol (CAS Reg. No. 107-21-1) Without limitation Pesticide inert ingredient as 

a solvent, stabilizer and/or 

antifreeze.

Ethylene glycol monobutyl ether

2-Ethylhexanol Cosolvent, defoamer, solvent 

for all pesticides used before 

crop emerges from soil and 

in herbicides before or after 

crop emerges

Europic chloride 10 ppm in formulation Tagging agent

FD&C Blue No. 1 (CAS Reg. No. 3844-45-9) For seed treatment use only Dye, coloring agent

FD&C Blue No. 1, methyl-polyethylene glycol derivative (CAS Reg. No. 9079-34-9) For seed treatment use only; 

Number average molecular weight 

(in amu) is greater than 1,000; Not 

to exceed 5% of the formulated 

pesticide product

Dye, coloring agent

FD&C Blue No. 1, polyethylene glycol derivative (CAS Reg. No. 9079-33-8) For seed treatment use only; 

Number average molecular weight 

(in amu) is greater than 1,000; Not 

to exceed 5% of the formulated 

pesticide product

Dye, coloring agent

FD&C Red No. 40 (CAS Reg. No. 25956-17-6) For seed treatment use only. Not to 

exceed 2% by weight of the 

pesticide formulation

Dye, coloring agent

Ferric chloride Not greater than 2% of 

suspending, dispersing 

agent, pesticide formulation

Fluoroapatite Solid diluent, carrier

Folic acid (CAS Reg. No. 59-30-3) Maximum of 0.5% of formulation Synergist

Gluconic acid (and sodium salt) Sequestrant

l-Glutamic acid (C5 H9 NO4; CAS Reg. No. 56-86-0) Seet treatment use only Plant nutrient

[alpha]-D-glucopyranoside, 2-ethylhexyl 6-O-[alpha]-D glucopyranosyl- (CAS Reg. No. 

330980-61-5)

Surfactant

[alpha]-D-glucopyranoside, 2-ethylhexyl (CAS Reg. No. 125590-73-0) Surfactant

Glutamine (CAS Reg. No. 56-85-9) Maximum of 0.5% of formulation Synergist

Glycerol—propylene oxide polymer (CAS Reg. No. 25791-96-2) Component in water-soluble 

film

Glyceryl triacetate Stabilizer

Glyceryl tris-12-hydroxystearate Flow control agent

Graphite Treatment aid for seeds

Guar hydroxypropyltrimethylammonium chloride (CAS Reg. No. 71329-50-5) Thickener/drift reduction 

agent

Hexamethylenetetramine Stabilizer for carriers in solid 

pesticide formulations

2-(2′-hydroxy-3′,5′-di-tert-amylphenyl) benzotriazole (CAS Reg. No. 25973-55-1) Maximum concentration of 0.6% in 

insecticide formulations applied to 

adzuki beans, canola, chickpeas, 

cotton, faba beans, field peas, 

lentils, linola, linseed, lucerne, 

lupins, mung beans, navy beans, 

pigeon peas, safflower, sunflower, 

and vetch

Ultraviolet (UV) stabilizer

2-Hydroxy-4-n-octoxybenzophenone (CAS Reg. No. 1843-05-6) Not more than 0.2 pt of pesticide 

formulation

Light stabilizer

Hydroxypropyl guar gum Thickener

Isobornyl acetate Solvent

Isobutyl alcohol Do.

Isobutylene-butene copolymers For soil application only Binder

Isooctadecanol Not more than 2% of pesticide 

formulation

Defoaming agent

Lanthanum chloride 10 ppm in formulation Tagging agent.

Magnesium nitrate (in combination with 2-methyl-4-isothiazolin-3-one and 5-chloro-2-

methyl-4-isothiazolin-3-one)

None Preservation

Maleic acid and maleic anhydride Stabilizer

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For pesticide formulations applied to 

apples with a minimum preharvest 

interval of 21 days

Manganese carbonate Plant nutrient

D-mannose (CAS Reg. No. 3458-28-4) Sequestrant, binder, filler

Mesityl oxide Not for use after edible parts of plant 

begin to form. Do not graze 

livestock in treated areas within 48 

hours after application

Solvent, cosolvent

Methionine (CAS Reg. No. 59-51-8) Maximum of 0.5% of formulation Synergist

Methyl alcohol Do.

Methyl ethyl ketone Surfactant

Methyl p- hydroxybenzoate Preservative for formulations

Methyl isobutyl ketone Solvent, cosolvent

2-Methyl-4-isothiazolin-3-one (in combination with 5-chloro-2-methyl-4-isothiazolin-3-one) Not more than 0.0022% (22.5 ppm) 

in the formulation; 0.00022% (or 

2.25 ppm) in the final solution 

applied to growing crops

Preservative

Mono-, di-, and trimethylnapthalenesulfonic acids and napthalenesulfonic acids 

formaldehyde condensates, ammonium and sodium salts (CAS Reg. Nos. 9008-63-3, 

9069-80-1, 9084-06-4, 36290-04-7, 91078-68-1, 141959-43-5, 68425-94-5)

Surfactants, related 

adjuvants of surfactants

Methyl oleate Surfactant

2-Methyl-2,4-pentanediol Solvent for formulations used 

before crop emerges from 

soil

Methyl poly(oxyethylene)C8-C18 alkylammonium chlorides where the poly(oxyethylene) 

content is n = 2-15 and where C8-C18 alkyl is linear and may be saturated or unsaturated 

(CAS Reg. Nos. 3010-24-0, 18448-65-2, 70750-47-9, 22340-01-8, 67784-77-4, 64755-

05-1, 61791-10-4, 28724-32-5, 28880-55-9, 68187-69-9, 68607-27-2, 60687-90-3

Concentration in formulated end use 

products not to exceed 10% by 

weight in herbicide products and 5% 

by weight in all other pesticide 

products

Surfactants, related 

adjuvants of surfactants

N-Methylpyrrolidone (CAS Reg. No. 872-504) Solvent, cosolvent

Mixed phytosterols (consisting of campesterol, sitosterol and stigmasterol, with minor 

amounts of associated plant sterols) derived from edible vegetable oils

Surfactant

Mono- and bis-(1H, 1H, 2H, 2H-perfluoroalkyl) phosphates where the alkyl group is even 

numbered and in the C6-C12 range

Not more than 0.5% of pesticide 

formulation. Expires February 9, 

2008

Surfactant, related adjvants 

of surfactants

Mono- and dialkyl (C8-C18) methylated ammonium chloride compounds, where the alkyl 

group(s) (C8-C18) are derived from coconut, cottonseed, soya, tallow, or hogfat fatty acids

Surfactants, related 

adjuvants of surfactants

Morpholine 4-C6-12 Acyl Derivatives (CAS Reg. No. 887947-29-7) As a solvent

Nicotinamide (CAS Reg. No. 98-92-0) Maximum of 0.5% of formulation Synergist

α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene); produced by the condensation of 1 mole 

of nonylphenol (nonyl group is a propylene trimer isomer) with an average of 4-14 or 30-

100 moles of ethylene oxide; if a blend of products is used, the average number of moles 

of ethylene oxide reacted to produce any product that is a component of the blend shall be 

in the range 4-14 or 30-100

Surfactant

Octanamide, N,N-dimethyl (CAS Reg. No. 1118-92-9) Emulsifier, solvent, cosolvent

α-Oleoyl-ω-(oleoyloxy) poly(oxyethylene) derived from α-hydro-ω-hydroxypoly

(oxyethylene) (molecular weight 600 amu)

Component of defoamers

Oxo-decyl acetate (CAS reg. No. 108419-33-6) Solvent

Oxo-heptyl acetate (CAS Reg. No. 90438-79-2) Solvent

Oxo-hexyl acetate (CAS Reg. No. 88230-35-7) Solvent

Oxo-nonyl acetate (CAS Reg. No. 108419-34-7) Solvent

Oxo-octyl acetate (CAS Reg. No. 108419-32-5) Solvent

Oxo-tridecyl acetate (CAS Reg. No. 108419-35-8) Solvent

Phenol Solvent, cosolvent

Phenol, 2-(2H-benzotriazol-2-yl)-6-dodecyl-4-methyl-, (CAS Reg. No. 23328-53-2) Not more than 10% by weight of 

pesticide formulations

UV stabilizer.

Phenolsulfonic acid—formaldehyde—urea condensate and its sodium salt Applied to growing plants only Dispersant surfactant

(Phthalocyaninato (2)) copper; (C.I. pigment blue No. 15) When used as a colorant in lowdensity plastic filmsColoring agent, pigment

Pigment red 48 For seed treatment use only Dye

α-Pinene Not more than 2% of formulation by 

weight

Stabilizer

Poly(oxy-1,2-ethanediyl), α-isotridecyl-ω-methoxy (CAS Reg. No. 345642-79-7) At a maximum of 10% in formulation Surfactant

Poly(oxy-1,2-ethanediyl), α-(3-carboxy-1-oxosulfopropyl)-ω-hydroxy-, (C10-C12)-alkyl 

ethers, disodium salts, polyoxylene content averages 4-5 moles (CAS Reg. No. 68815-

56-5)

Not to exceed 0.125% for seed 

treatment use only

Surfactant.

Poly(oxy-1,2-ethanediyl), α-(3-carboxy-1-oxosulfopropyl)-ω-hydroxy-, (C10-C16)-alkyl 

ethers, disodium salts, polyoxyethylene content averages 5 moles (CAS Reg. No. 68954-

91-6)

Not to exceed 0.125% for seed 

treatment use only

Surfactant

Poly(oxyethylene) adducts of mixed phytosterols (such sterols to consist of campesterol, 

stigmasterol and sitosterol with minor amounts of associated plant sterols) derived from 

edible vegetable oils; polyoxyethylene content averaging 5-26 moles

Surfactant, related adjuvants

Polyoxyethylene polyoxypropylene mono(di-sec-butylphenyl) ether (CAS Reg. No. 69029-

39-6)

Limited to herbicide formulations 

only, and to no more than 30% by 

weight in herbicide formulations 

intended for application to turf

Surfactants, related 

adjuvants of surfactants

Poly(oxyethylene) (5) sorbitan monooleate Surfactants, related 

adjuvants of surfactants

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Polysorbate 60, conforming to 21 CFR 172.836 Surfactant

Potassium dihydrogen phosphate Buffering agent

2-Propanamine, compound with α-phosphono-ω-butoxypoly (oxy-1,2-ethanediyl) (2:1) 

(CAS Reg. No. 431040-31-2)

Not more than 15% in the 

formulated product

Surfactant

2-Propanamine, compounds with polyethylene glycol dihydrogen phosphate C8-10- alkyl 

ether (2:1) (CAS Reg. No. 431062-72-5)

Not more than 15% in the 

formulated product

Surfactant

Propylene glycol monomethyl ether Solvent

Pyridoxine (CAS Reg. No. 65-23-6) Maximum of 0.5% of formulation Synergist

Rosin, dark wood (as defined in 21 CFR 178.3870(a)(1)(v)) Surfactants, related 

adjuvants of surfactants

Rosin, gum Do.

Rosin, tall oil Do.

Scandium chloride 10 ppm in formulation Tagging agent

Sodium bisulfate (CAS Reg. No. 7681-38-1) Acidifying/buffering agent

Sodium 1,4-dicyclohexyl sulfosuccinate Surfactants, related 

adjuvants of surfactants

Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006-15-3) Surfactants, related 

adjuvants of surfactants

Sodium dihydrogen phosphate (CAS Reg. No. 7558-80-7) conforming to 21 CFR 

182.6778

Buffering agent

Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127-39-9) Surfactants, related 

adjuvants of surfactants

Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922-80-5) Surfactants, related 

adjuvants of surfactants

Sodium metaborate Sequestrant

Sodium molybdate Plant nutrient

Sodium nitrate Solid diluent

Sodium nitrite Not more than 3% of pesticide 

formulation

Stabilizer, inhibitor.

Sodium o-phenylphenate Not more than 0.1% of pesticide 

formulation

Preservative for formulation

Sodium salt of the insoluble fraction of rosin Surfactants, related 

adjuvants of surfactants

Sodium salts of N-alkyl (C8-C18)-beta-iminodipropionic acid where the C8-C18 is linear 

and may be saturated and/or unsaturated (CAS Reg. Nos. 3655-00-3, 61791-56-8, 14960-

06-6, 26256-79-1, 90170-43-7, 91696-17-2, 97862-48-1)

Concentration in formulated end-use 

products not to exceed 30% by 

weight in pesticide formulations

Surfactants, related 

adjuvants of surfactants

Sodium tetraborate Not more than 2% of pesticide 

formulation

Buffering agent; corrosion 

inhibitor

Sulfonic acids, C13-17-sec-alkane, sodium salts (CAS Reg. No. 85711-69-9) Not to exceed 40% by weight in 

non-residential use pesticide 

formulation only

Surfactant

Sulfonic acids, C14-17-sec-alkane, sodium salts (CAS Reg. No. 97489-15-1) Not to exceed 40% by weight in 

non-residential pesticide formulation 

only

Surfactant

Tallowamine, ethoxylated, mixture of dihydrogen phosphate and monohydrogen 

phosphate esters and the corresponding ammonium, calcium, potassium, and sodium 

salts of the phosphate esters, where the poly(oxyethylene) content averages 2-20 moles 

(CAS Reg. No. 68308-48-5)

Not to exceed 20% of pesticide 

formulation

Surfactants, related 

adjuvants of surfactants

Tannin Dispersing agent

Tertiary butylhydroquinone Antioxidant

1-Tetradecanamine, N,N-dimethyl-, N-oxide (CAS Reg. No. 3332-27-2) Component in water-soluble 

film

Tetraethylene glycol (CAS Reg. No. 112-60-7) Solvent

N,N,N′,N′′-Tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Reg. No. 102-60-3) Concentration in formulated end-use 

products not to exceed 20% by 

weight in pesticide formulations

Stabilizer for formulations 

2,4,7,9-Tetramethyl-5-decyne 4,7-diol In pesticide formulations, for 

application to soil prior to planting or 

to plants before edible parts form

Surfactants, related 

adjuvants of surfactants

Tetrapotassium pyrophosphate (CAS Reg. No. 7320-345) Not to exceed 10% of formulation Sequestrant, anticaking 

agent, conditioning agent

Titanium dioxide (CAS Reg. No. 13463-67-7) Pigment/coloring agent in 

plastic bags used to wrap 

growing banana 

(preharvest), colorant on 

seeds for planting

Toluenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and 

zinc salts

Solvent, cosolvent

Triethanolamine Stabilizer, inhibitor for 

formulations used before 

crop emerges from soil

Triethanolamine (CAS Reg. No. 102-71-6) Stabilizer, inhibitor 

Triethylene glycol Deactivator

Triethyl phosphate Stabilizer for formulations 

used before crop emerges 

from soil

Trimethylolpropane (CAS Reg. No. 77-99-6) Not to exceed 15% by weight of the 

film

Component in water-soluble 

film

Surfactant.

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α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene), the poly(oxyethylene) 

content averages 4-150 moles)

Not more than 15% of the 

formulation

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene); mixture of 

monohydrogen and dihydrogen phosphate esters and the corresponding ammonium, 

calcium, magnesium, potassium, sodium, and zinc salts, the poly(oxyethylene) content 

averages 4-150 moles)

Not more than 15% of the 

formulation

 Do.

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene) sulfate, and the 

corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts, the 

poly(oxyethylene) content averages 4-150 moles

Not more than 15% of the pesticide 

formulation

 Do.

Tryptophan (CAS Reg. No. 73-22-3) Maximum of 0.5% of formulation Synergist

Valeric acid, normal Not more than 2% in pesticide 

formulations

Stenching agent or odorant

Xylene Solvent, cosolvent

Xylenesulfonic acid its ammonium calcium, magnesium, potassium, sodium, and zinc salts Surfactants, related 

adjuvants of surfactants

Yucca extract from Yucca schidigera Wetting agent

Ytterbium chloride 10 ppm in formulation Tagging agent

Yttrium chloride 10 ppm in formulation Tagging agent

Zinc orthophosphate Plant nutrient and safener

Zinc stearate, conforming to 21 CFR 182.5994 and 582.5994 Flow control agent

[69 FR 23124, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.920, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

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§180.930 Inert ingredients applied to animals; exemptions from the requirement of a tolerance.

The following materials are exempted from the requirement of a tolerance when used in accordance with good 

agricultural practice as inert (or occasionally active) ingredients in pesticide formulations applied to animals:

Inert ingredients Limits Uses

Acetic acid (CAS Reg. No. 64-19-7) Not more than 

0.5% of pesticide 

formulation

Catalyst

Acetic anhydride Solvent, cosolvent, 

stabilizer

Acetone (Cas Reg. No. 67-64-1) Solvent or cosolvent

Alkanoic and alkenoic acids, mono- and diesters of α-hydro-ω-hydroxypoly(oxyethylene) with molecular weight (in 

amu) range of 200 to 6,000

Emulsifiers

Alkyl (C8-C24) benzenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts Surfactants, 

emulsifier, related 

adjuvants of 

surfactants

Alkyl (C12-C16) dimethyl ammonio acetate (CAS Reg. Nos. 683-10-3, 2601-33-4 and 693-33-4 20% by weight in 

pesticide 

formulation

Surfactant

α-alkyl(C6- C15)-ω-hydroxypoly(oxyethylene)sulfate, and its ammonium, calcium, magnesium, potassium, sodium, 

and zinc salts, poly(oxyethylene) content averages 2-4 moles (CAS Reg. Nos.: 3088-31-1, 3694-74-4, 9004-82-4, 

9004-84-6, 9021-91-4, 9086-52-6, 13150-00-0, 15826-16-1, 25446-78-0, 26183-44-8, 27140-00-7, 27731-61-9, 

27731-61-9, 27731-62-0, 32612-48-9, 34431-25-9, 35015-74-8, 50602-06-7, 52286-18-7, 52286-19-8, 54116-08-4, 

55901-67-2, 61702-79-2, 61894-66-4, 62755-21-9, 63428-85-3, 63428-86-4, 63428-87-5, 65086-57-9, 65086-79-5, 

65104-74-7, 65122-38-5, 67674-66-2, 67762-19-0, 67762-21-4, 67845-82-3, 67845-83-4, 67923-90-4, 68037-05-8, 

68037-06-9, 68171-41-5, 68424-50-0, 68511-39-7, 68585-34-2, 68610-66-2, 68611-29-0, 68611-55-2, 68649-53-6, 

68890-88-0, 68891-29-2, 68891-30-5, 68891-38-3, 69011-37-6, 73665-22-2, 75422-21-8, 78330-16-2, 78330-17-3, 

78330-25-3, 78330-26-4, 78330-27-5, 78330-28-6, 78330-29-7, 78330-30-0, 96130-61-9, 106597-03-9, 110392-

50-2, 119432-41-6, 125301-88-4, 125301-89-5, 125301-92-0, 125736-54-1, 157707-85-2, 160104-51-8, 160901-

27-9, 160901-28-0, 160901-29-1, 160901-30-4, 161025-28-1, 161074-79-9, 162063-19-6, 219756-63-5)

Not to exceed 

30% of formulation

Surfactants, related 

adjuvants of 

surfactants.

α-alkyl (C12-C15)-ω-hydroxypoly (oxypropylene)poly (oxyethylene)copolymers (where the poly(oxypropylene) 

content is 3-60 moles and the poly(oxyethylene) content is 5-80 moles), the resulting ethoxylated propoxylated 

(C12-C15) alcohols having a minimum molecular weight (in amu) of 1,500, CAS Reg. No. 68551-13-3

Not to exceed 

20% of pesticide 

formulations

Surfactant

α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene) polymers where the alkyl chain contains a 

minimum of six carbons (CAS Reg. No.: 9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3; 

9038-43-1; 9040-05-5; 9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-52-8; 26468-86-0; 

26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-01-1; 34398-05-5; 37251-67-5; 37311-00-5; 37311-01-6; 

37311-02-7; 37311-04-9; 39587-22-9; 50861-66-0; 52232-09-4; 52292-17-8; 52609-19-5; 57679-21-7; 59112-62-8; 

60828-78-6; 61702-78-1; 61725-89-1; 61791-13-7; 61791-20-6; 61791-28-4; 61804-34-0; 61827-42-7; 61827-84-7; 

62648-50-4; 63303-01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 64425-86-1; 65104-72-5; 

65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-08-0; 68002-96-0; 68002-97-1; 68131-39-5; 68131-40-8; 

68154-96-1; 68154-97-2; 68154-98-3; 68155-01-1; 68213-23-0; 68213-24-1; 68238-81-3; 68238-82-4; 68409-58-5; 

68409-59-6; 68439-30-5; 68439-45-2; 68439-46-3; 68439-48-5; 68439-49-6; 68439-50-9; 68439-51-0; 68439-53-2; 

68439-54-3; 68458-88-8; 68526-94-3; 68526-95-4; 68551-12-2; 68551-13-3; 68551-14-4; 68603-20-3; 68603-25-8; 

68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 68954-94-9; 68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 

69013-19-0; 69227-20-9; 69227-21-0; 69227-22-1; 69364-63-2; 70750-27-5; 70879-83-3; 70955-07-6; 71011-10-4; 

71060-57-6; 71243-46-4; 72066-65-0; 72108-90-8; 72484-69-6; 72854-13-8; 72905-87-4; 73018-31-2; 73049-34-0; 

74432-13-6; 74499-34-6; 78330-19-5; 78330-20-8; 78330-21-9; 78330-23-1; 79771-03-2; 84133-50-6; 85422-93-1; 

97043-91-9; 97953-22-5; 102782-43-4; 103331-86-8; 103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 

106232-83-1; 111905-54-5; 116810-31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 121617-09-2; 

126646-02-4; 126950-62-7; 127036-24-2; 139626-71-4; 152231-44-2; 154518-36-2; 157627-86-6; 157627-88-8; 

Surfactants, related 

adjuvants of 

surfactants.

eCFR — Code of Federal Regulations Page 380 of 441

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157707-41-0; 157707-43-2; 159653-49-3; 160875-66-1; 160901-20-2; 160901-09-7; 160901-19-9; 161025-21-4; 

161025-22-5; 166736-08-9; 169107-21-5; 172588-43-1; 176022-76-7; 196823-11-7; 287935-46-0; 288260-45-7; 

303176-75-2; 954108-36-2)

α-alkyl (minimum C6 linear, branched, saturated and/or unsaturated)-ω-hydroxypolyoxyethylene polymer with or 

without polyoxypropylene, mixture of di- and monohydrogen phosphate esters and the corresponding ammonium, 

calcium, magnesium, monoethanolamine, potassium, sodium, and zinc salts of the phosphate esters; minimum 

oxyethylene content is 2 moles; minimum oxypropylene content is 0 moles, (CAS Reg. Nos.: 9004-80-2, 9046-

01-9, 26982-05-8, 31800-89-2, 37280-82-3, 37281-86-0, 39341-09-8, 39341-65-6, 39464-66-9, 39464-69-2, 

42612-52-2, 50643-20-4, 50668-50-3, 51325-10-1, 51884-64-1, 52019-36-0, 52019-38-2, 52019-38-2, 57486-09-6, 

58206-38-5, 58318-92-6, 58857-49-1, 59112-71-9, 60267-55-2, 61837-79-4, 62362-49-6, 62482-61-5, 63747-86-4, 

63887-54-7, 63887-55-8, 66020-37-9, 66272-25-1, 66281-20-7, 67711-84-6, 67786-06-5, 67989-06-4, 68070-99-5, 

68071-17-0, 68071-35-2, 68071-37-4, 68130-44-9, 68130-45-0, 68130-46-1, 68130-47-2, 68186-29-8, 68186-34-5, 

68186-36-7, 68186-37-8, 68238-84-6, 68311-02-4, 68311-04-6, 68332-75-2, 68389-72-0, 68400-75-9, 68413-78-5, 

68425-73-0, 68425-75-2, 68439-39-4, 68458-48-0, 68511-15-9, 68511-36-4, 68511-37-5, 68551-05-3, 68585-15-9, 

68585-16-0, 68585-17-1, 68585-36-4, 68585-39-7, 68603-24-7, 68607-14-7, 68610-64-0, 68610-65-1, 68649-29-6, 

68649-30-9, 68650-84-0, 68815-11-2, 68855-46-9, 68856-03-1, 68890-90-4, 68890-91-5, 68891-12-3, 68891-13-4, 

68891-26-9, 68908-64-5, 68909-65-9, 68909-67-1, 68909-69-3, 68921-24-4, 68921-60-8, 68954-87-0, 68954-88-1, 

68954-92-7, 68987-35-9, 69029-43-2, 69980-69-4, 70247-99-3, 70248-14-5, 70844-96-1, 70903-63-8, 71965-23-6, 

71965-24-7, 72480-27-4, 72623-67-7, 72623-68-8, 72828-56-9, 72828-57-0, 73018-34-5, 73038-25-2, 73050-08-5, 

73050-09-6, 73361-29-2, 73378-71-9, 73378-72-0, 73559-42-9, 73559-43-0, 73559-44-1, 73559-45-2, 74499-76-6, 

76930-25-1, 78041-18-6, 78330-22-0, 78330-24-2, 82465-25-6, 84843-37-8, 91254-26-1, 93925-54-3, 95014-34-9, 

96416-89-6, 99924-51-3, 103170-31-6, 103170-32-7, 106233-09-4, 106233-10-7, 108818-88-8, 110392-49-9, 

111798-26-6, 111905-50-1, 116671-23-9, 117584-36-8, 119415-05-3, 120913-45-3, 121158-61-0, 121158-63-2, 

123339-53-7, 125139-13-1, 125301-86-2, 125301-87-3, 126646-03-5, 129208-04-4, 129870-77-5, 129870-80-0, 

130354-37-9, 136504-88-6, 143372-50-3, 143372-51-4, 144336-75-4, 146815-57-8, 151688-56-1, 154518-39-5, 

154518-40-8, 155240-11-2, 159704-69-5, 160498-49-7, 160611-24-5, 171543-66-1, 172027-16-6, 172274-69-0, 

176707-42-9, 181963-82-6, 188741-55-1, 191940-53-1, 210493-60-0, 210993-53-6, 246159-55-7, 251298-11-0, 

261627-68-3, 290348-69-5, 290348-70-8, 317833-96-8, 340681-28-9, 422563-19-7, 422563-26-6, 522613-09-8, 

717140-06-2, 717140-09-5, 717827-29-7, 762245-80-7, 762245-81-8, 866538-89-8, 866538-90-1, 873662-29-4, 

913068-96-9, 936100-29-7, 936100-30-0, 1072943-56-6, 1087209-87-7, 1174313-54-2, 1187742-89-7, 1187743-

35-6, 1205632-03-6, 1233235-49-8, 1451002-50-8, 1456802-88-2, 1456802-89-3, 1456803-12-5)

Not to exceed 

30% of formulation

Surfactants, related 

adjuvants of 

surfactants.

N-alkyl (C8-C18) primary amines and their acetate salts where the alkyl group is linear and may be saturated 

and/or unsaturated (CAS Reg. Nos. 61790-57-6, 61790-58-7, 61790-59-8, 61790-60-1, 61788-46-3, 61790-33-8, 

68155-38-4)

Concentration in 

formulated enduse products not 

to exceed 10% by 

weight in herbicide 

products, 4% by 

weight in 

insecticide 

products, and 4% 

by weight in 

fungicide products

Surfactants, related 

adjuvants of 

surfactants

Alkyl (C8-C18) sulfate and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts Surfactant

N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl) C8-C18 saturated and unsaturated alkylamines; the poly

(oxy-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 10213-78-2, 25307-17-9, 26635-92-7, 26635-93-8, 

288259-52-9, 58253-49-9, 61790-82-7, 61791-14-8, 61791-24-0, 61791-26-2, 61791-31-9, 61791-44-4, 68155-

33-9, 68155-39-5, 68155-40-8,70955-14-5, 73246-96-5, 1266162-49-5)

Not to exceed 

25% in herbicide 

formulations and 

10% in insecticide 

and fungicide 

formulations

Surfactants, related 

adjuvants of 

surfactants

N,N-Bis-α-ethyl-ω-hydroxypoly(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl) C8-C18 saturated and unsaturated 

alkylamines; the poly(oxy-1,2-ethanediyl/oxy(methyl-1,2-ethanediyl) content is 2-60 moles (CAS Reg. Nos. 68213-

26-3, 68153-97-9, 75601-76-2)

Not to exceed 

25% in herbicide 

formulations and 

10% in insecticide 

and fungicide 

formulations

Surfactants, related 

adjuvants of 

surfactants 

Ascorbyl palmitate Preservative

Attapulgite-type clay Solid diluent, carrier

Barium sulfate (CAS Reg. No. 7727-43-7) Carrier, density 

control agent

Benzoic acid Preservative for 

formulations

2-Bromo-2-nitro-1,3-propanediol (CAS Reg. No. 52-51-7) 0.04% or less by 

weight of the total 

pesticide 

formulation

In-can preservative

Butane Propellant

n-Butanol (CAS Reg. No. 71-36-3) Solvent for blended 

emulsifiers

n-Butyl benzoate (CAS RN 136-60-7) Solvent

Butylated hydroxyanisole Antioxidant

Butylated hydroxytoluene Do.

Calcium carbonate Solid diluent, carrier

Calcium chloride Stabilizer

Calcium silicate, hydrated calcium silicate Anticaking agent, 

solid diluent, carrier

C9 rich aromatic hydrocarbons (CAS Reg. No. 64742-95-6) Solvent.

C10-11 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5) Solvent.

C11-12 rich aromatic hydrocarbons (CAS Reg. No. 64742-94-5) Solvent.

Calcium stearate (CAS Reg. No. 1592-23-0) Stabilizer, component 

of plastic animal tag

Calcium sulfate Solid diluent, carrier

Carbon black (CAS Reg. No. 1333-86-4) Colorant/pigment in 

animal tag

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Carbon Dioxide (CAS Reg. No. 124-38-9) None Propellant

Carrageenan, conforming to 21 CFR 172.620 Minimum 

molecular weight 

(in amu): 100,000

Thickener

Cyclohexanone Solvent, cosolvent

D&C Green No. 6 Dye, coloring agent

D&C Red No. 17 Do.

D&C Violet No. 2 Do.

Dialkyl (C8-C18) dimethylammonium chloride Not more than 

0.2% in silica 

hydrated silica

Flocculating agent in 

the manufacture of 

silica hydrated silica 

for use as a solid 

diluent, carrier

Diatomite (diatomaceous earth) Solid diluent, carrier

Diethanolamine salts of alkyl (C8-C24) benzenesulfonic acid (CAS Reg. Nos. 26545-53-9, 67815-95-6, 67889-94-5, 

67889-95-6, 68259-34-7, 68478-47-7, 68567-68-0, 68815-34-9, 68815-37-2, 68891-02-1, 68953-97-9, 84989-15-1, 

85338-09-6, 90194-39-1, 90194-40-4, 90218-08-9)

Not to exceed 7% 

of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants.

Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-75-4)

Surfactant

Diethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-83-4)

Surfactant

Diethylaminoethanol, ethoxylated, reaction products with acid trimers, minimum number average molecular weight 

(in amu), 1,200 (CAS Reg. No. 1173188-81-2)

Surfactant

Diethylaminoethanol, ethoxylated, reaction product with fatty acid dimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-72-1)

Surfactant

Diethylphthalate Solvent, cosolvent

1,1-Difluoroethane (CAS Reg. No. 75-37-6) For aerosol 

pesticide 

formulations used 

for insect control in 

food- and feedhandling 

establishments 

and animals

Aerosol propellant

Dimethyl ether (CAS Reg. No. 115-10-6) Propellant

Dimethylaminoethanol, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-42-5)

Surfactant

Dimethylaminoethanol, ethoxylated, propoxylated reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-67-4)

Surfactant

Dimethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-38-9)

Surfactant

Dimethylaminoethanol, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173188-49-2)

Surfactant

Dimethylaminopropylamine, isopropylamine, ethanolamine, and triethanolamine salts of alkyl (C8-C24) 

benzenesulfonic acid (CAS Reg. Nos. 3088-30-0, 12068-12-1, 26264-05-1, 26836-07-7, 27323-41-7, 55470-69-4, 

58089-99-9, 61886-59-7, 61931-76-8, 67924-05-4, 68110-32-7, 68259-35-8, 68411-31-4, 68442-72-8, 68567-69-1, 

68584-24-7, 68584-25-8, 68648-81-7, 68648-96-4, 68649-00-3, 68815-30-5, 68815-35-0, 68910-32-7

68953-93-5, 68953-98-0, 70528-84-6, 72391-21-0, 84961-74-0, 85480-55-3, 85480-56-4, 85995-82-0, 90194-42-6, 

90194-53-9, 90194-54-0, 90194-55-1, 90218-09-0, 90218-11-4, 90218-35-2, 96687-54-6, 99924-49-9, 121617-

08-1, 157966-96-6, 193562-36-6, 319926-68-6, 877677-48-0, 1093628-27-3).

Surfactants, related 

adjuvants of 

surfactants.

3,6-Dimethyl-4-octyne-3,6-diol Not more than 

2.5% of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

Dimethylpolysiloxane (CAS Reg. No. 9016-00-6) Defoaming agent

Di-n-butyl carbonate (CAS Reg. No. 542-52-9) Solvent

Dipropylene glycol monomethyl ether Surfactants, related 

adjuvants of 

surfactants

Epoxidized soybean oil (CAS Reg. No. 8013-07-8) Stabilizer, plasticizer, 

component animal tag

Ethanesulfonic acid, 2-hydroxy- (CAS Reg. No. 107-36-8) Chelator, sequestrant, 

or conditioning agent.

Ethanesulfonic acid, 2-hydroxy-, ammonium salts (CAS Reg. No. 57267-78-4) Do.

Ethanesulfonic acid, 2-hydroxy-, calcium salts (CAS Reg. No. 10550-47-7) Do.

Ethanesulfonic acid, 2-hydroxy-, magnesium salts (CAS Reg. No. 17345-56-1) Do.

Ethanesulfonic acid, 2-hydroxy-, potassium salts (CAS Reg. No. 1561-99-5) Do.

Ethanesulfonic acid, 2-hydroxy-, sodium salts (CAS Reg. No. 1562-00-1) Do.

Ethanesulfonic acid, 2-hydroxy-, zinc salts (CAS Reg. No. 129756-32-7) Do.

Ethyl alcohol Solvent, cosolvent

Ethyl maltol (CAS Reg. No.4940-11-8) Not more than 0.2 

% of the pesticide 

formulation

Odor masking agent

Ethylene oxide adducts of 2,4,7,9-tetramethyl-5-decynediol, the ethylene oxide content averages 3.5, 10 or 30 

moles (CAS Reg. No. 9014-85-1)

Surfactants, related 

adjuvants of 

surfactants

2-Ethyl-1-hexanol (CAS Reg. No. 104-76-7) Not more than 

10% of pesticide

Solvent, adjuvant of 

surfactants

FD&C Blue No. 1 Dye, coloring agent

FD&C Yellow No. 6 Aluminum Lake (CAS Reg. No. 15790-07-5) Not more than 2% 

by weight of 

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pesticide 

formulation

Pigment in animal tag 

and similar slowrelease devices

D-glucopyranose, oligomeric, C10-16-alkyl glycosides (CAS Reg. No. 110615-47-9) Surfactant

Glycerol monooleate Surfactants, related 

adjuvants of 

surfactants

Glyceryl monostearate Emulsifier

Glyceryl tris-12-hydroxystearate Flow control agent

Graphite Solid diluent, carrier

n-Hexyl alcohol (CAS Reg. No. 111-27-3) Solvent, cosolvent

Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-06-4)

Surfactant

Hydroxyethylmorpholine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173188-67-4)

Surfactant

Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid dimers, minimum number average 

molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-00-8)

Surfactant

Hydroxyethylmorpholine, ethoxylated, reaction products with fatty acid trimers, minimum number average 

molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-09-7)

Surfactant

Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid dimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-22-4)

Surfactant

Hydroxyethylpiperidine, ethoxylated, propoxylated, reaction products with fatty acid trimers, minimum number 

average molecular weight (in amu), 1,200 (CAS Reg. No. 1173189-28-0)

Surfactant

Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid dimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173189-20-2)

Surfactant

Hydroxyethylpiperidine, ethoxylated, reaction products with fatty acid trimers, minimum number average molecular 

weight (in amu), 1,200 (CAS Reg. No. 1173189-25-7)

Surfactant

2-(2′-Hydroxy-5′-methylphenyl)benzotriazole (CAS Reg. No. 2440-22-4) Not more than 

0.5% by weight of 

pesticide 

formulation

Ultraviolet light 

absorber/stabilizer in 

animal tag and similar 

slow-release devices

Iron oxide (CAS Reg. No. 1309-37-1) Colorant in pesticide 

formulations for 

animal tags

Isobutane (CAS Reg. No. 75-28-5) None Propellant

Isopropyl myristate, CAS Reg. No. 110-27-0 Solvent

Kaolinite-type clay Solid diluent, carrier

Kerosene, U.S.P. reagent Solvent, cosolvent

Lactic acid Solvent

Lactic acid, 2-ethylhexyl ester (CAS Reg. No. 6283-86-9) Solvent

Lactic acid, 2-ethylhexyl ester, (2S)- (CAS Reg. No. 186817-80-1) Solvent

Lactic acid, n-propyl ester, (S); (CAS Reg. No. 53651-69-7) Solvent

Lignin (CAS Reg. No. 9005-53-2) Surfactant, related 

adjuvants of 

surfactants

Lignin, alkali (CAS Reg. No. 8068-05-1) Do.

Lignin, alkali, oxidized, sodium salt (CAS Reg. No. 68201-23-0) Do.

Lignin alkali reaction products with disodium sulfite and formaldehyde (CAS Reg. No. 105859-97-0) Do.

Lignin alkali reaction products with formaldehyde and sodium bisulfite (CAS Reg. No. 68512-35-6) Do.

Lignosulfonic acid (CAS Reg. No. 8062-15-5) Do.

Lignosulfonic acid, ammonium calcium salt (CAS Reg. No. 12710-04-2) Do.

Lignosulfonic acid, ammonium magnesium salt (CAS Reg. No. 123175-37-1) Do.

Lignosulfonic acid, ammonium salt (CAS Reg. No. 8061-53-8) Do.

Lignosulfonic acid, ammonium sodium salt (CAS Reg. No. 166798-73-8) Do.

Lignosulfonic acid, calcium magnesium salt (CAS Reg. No. 55598-86-2) Do.

Lignosulfonic acid, calcium salt (CAS Reg. No. 8061-52-7) Do.

Lignosulfonic acid, calcium sodium salt (CAS Reg. No. 37325-33-0) Do.

Lignosulfonic acid, ethoxylated, sodium salt (CAS Reg. No. 68611-14-3) Do.

Lignosulfonic acid, magnesium salt (CAS Reg. No. 8061-54-9) Do.

Lignosulfonic acid, potassium salt (CAS Reg. No. 37314-65-1) Do.

Lignosulfonic acid, sodium salt (CAS Reg. No. 8061-51-6) Do.

Lignosulfonic acid, sodium salt, oxidized (CAS Reg. No. 68855-41-4) Do.

Lignosulfonic acid, sodium salt, polymer with formaldehyde and phenol (CAS Reg. No. 37207-89-9) Do.

Lignosulfonic acid, sodium salt, sulfomethylated (CAS Reg. No. 68512-34-5) Do.

Lignosulfonic acid, zinc salt (CAS Reg. No. 57866-49-6) Do.

d-Limonene (CAS Reg. No. 5989-27-5) Solvent, fragrance

Magnesium carbonate Solid diluent, carrier

Magnesium silicate, hydrated magnesium silicate Do.

Methane sulfonic acid (CAS Reg. No. 75-75-2) Not to exceed 

3.0% by weight in 

pesticide 

formulation

Acidifying agent

Methyl alcohol Solvent, cosolvent

Methyl n-amyl ketone (CAS Reg. No. 110-43-0) Solvent, cosolvent

Methyl esters of higher fatty acids conforming to 21 CFR 573.640 Antidusting agent

Methyl-p-hydroxybenzoate (Methyl paraben) Meets 

specifications of 

Preservative

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Food Chemicals 

Codex; not to 

exceed 0.1% in 

formulations

Methyl isobutyl ketone Solvent, cosolvent

2-methyl-2,4-pentanediol (CAS Reg. No.-107-41-5) Without limitation Growing crops and 

food animals

2-methyl-1,3-propanediol (CAS Reg. No. 2163-42-0) Solvent, surfactant

Mineral oil, U.S.P., or conforming to 21 CFR 172.878 or 178.3620(a), (b) Solvent, diluent

Montmorillonite-type clay Solid diluent, carrier

Nonyl, decyl, and undecyl glycoside mixture with a mixture of nonyl, decyl, and undecyl oligosaccharides and 

related reaction products (primarily decanol and undecanol) produced as an aqueous-based liquid (50 to 65% 

solids) from the reaction of primary alcohols (containing 15 to 20% secondary alcohol isomers) in a ratio of 20% C9, 

40% C10, and 40% C11 with carbohydrates (average glucose to alkyl chain ratio 1.3 to 1.8)

Surfactant

α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) mixture of dihydrogen phosphate and monohydrogen phosphate 

esters and the corresponding ammonium, calcium, magnesium, potassium, sodium, and zinc salts of the 

phosphate esters; the nonyl group is a propylene trimer isomer and the poly(oxyethylene) content averages 4-14 or 

30 moles (CAS Reg. Nos. 51811-79-1, 59139-23-0, 67922-57-0, 68412-53-3, 68553-97-9, 68954-84-7, 99821-

14-4, 152143-22-1, 51609-41-7, 37340-60-6, 106151-63-7, 68584-47-4, 52503-15-8, 68458-49-1)

Not to exceed 7% 

of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

α-(p-Nonylphenol)-ω-hydroxypoly(oxyethylene) sulfate, ammonium, calcium, magnesium, potassium, sodium, and 

zinc salts the nonyl group is propylene trimer isomer and the poly(oxyethylene) content averages 4 moles (CAS 

Reg. Nos. 9014-90-8, 9051-57-4, 9081-17-8, 68649-55-8, 68891-33-8

Not to exceed 7% 

of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) produced by the condensation of 1 mole of nonylphenol (nonyl 

group is a propylene trimer isomer) with an average of 4-15 or 30-90 moles of ethylene oxide; if a blend of products 

is used, the average number of moles of ethylene oxide reacted to produce any product that is a component of the 

blend shall be in the range of 4-15 or 30-90 moles

Surfactants, 

emulsifier, related 

adjuvants of 

surfactants.

Octadecyl 3,5-di-tert-butyl-4-hydroxyhydro cinnamate (CAS Reg. No. 2082-79-3) Not more than 

0.5% by weight of 

pesticide 

formulation

Thermal 

stabilizer/antioxidant 

in animal tag and 

similar slow-release 

devices

1-Octanal (CAS Reg. No. 124-13-0) Not more than 

0.2% of the 

pesticide 

formulation

Odor masking agent

Octyl and decyl glucosides mixture with a mixture of octyl and decyl oligosaccharides and related reaction products 

(primarily n-decanol) produced as an aqueous-based liquid (68-72% solids) from the reaction of straight chain 

alcohols (C8(45%), C10) with anhydrous glucose

Thermal 

stabilizer/antioxidant 

in animal tag and 

similar slow-release 

devices

Octyl epoxytallate (CAS Reg. No. 61788-72-5) Plasticizer, 

component animal tag

Oleic acid, conforming to 21 CFR 172.862 (CAS Reg. No. 112-80-1) Defoaming agent

α-Oleoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600 Emulsifier

α-Oleoyl-ω-(oleyloxy)poly(oxyethylene) derived from α-hydro-ω-hydroxypoly(oxyethylene), molecular weight (in 

amu) 600

Emulsifier, defoaming 

agent

Petroleum hydrocarbons, light, odorless, conforming to 21 CFR 172.884 or 178.3650 Solvent, diluent

Petroleum hydrocarbons, synthetic isoparaffinic, conforming to 21 CFR 172.882 or 178.3530 Do.

Phenol Solvent, cosolvent

α-Pinene Not more than 2% 

of formulation by 

weight

Stabilizer

Polyethylene (CAS Reg. No. 9002-88-4) conforming to 21 CFR 172.615 Component of plastic 

slow release tag

Polyethylene glycol [α-hydro-ω-hydroxypoly(oxyethylene)]; mean molecular weight (in amu) 194 to 9,500 conforms 

to 21 CFR 178.3750

Surfactants, related 

adjuvants of 

surfactants

Potassium benzoate (Cas No. 582-25-2) None Preservative

Potassium hydroxide Meeting Food 

Chemicals, Codex 

specifications

Neutralizer

Propane Propellant

1,2,3-Propanetriol, homopolymer diisooctadecanoate (CAS Reg. No. 63705-03-3) Emulsifier

n-Propanol Solvent, for blended 

emulsifiers

2-Propenoic acid, 2-methyl-, polymer with ethyl 2-propenoate and methyl 2-methyl-2-propenoate, ammonium salt 

(CAS Registration No. 55989-05-4), minimum number average molecular weight (in amu), 18,900.

Encapsulating 

agent,dispensers, 

resins, fibers and 

beads

Propylene glycol Solvent, cosolvent

Propylene glycol monomethyl ether Deactivator, 

emmolient

Propyl gallate Antioxidant

Propyl p-hydroxybenzoate (Propyl paraben) Meets 

specifications of 

Food Chemicals 

Codex; not to 

exceed 0.1% in 

formulations

Preservative

Pyrophylite Solid diluent, carrier

Silica, hydrated silica

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Anticaking agent, 

solid diluent, carrier

Silica aerogel (finely powdered microcellular silica foam having a minimum silica content of 89.5%) Component of 

antifoaming agent

Soapstone Solid diluent

Sodium alkyl naphthalenesulfonates (CAS Reg. Nos. 68909-83-1, 68909-84-2, 68909-82-0, 27213-90-7, 26264-

58-4, 27178-87-6, 111163-74-7, 908356-16-1, 25417-20-3, 25638-17-9, 145578-88-7, 1322-93-6, 1323-19-9, 

7403-47-6, 68442-09-1, 127646-44-0, 908356-18-3)

Limited to no more 

than 30% by 

weight in pesticide 

end-use products

Surfactants, related 

adjuvants of 

surfactants

Sodium 1,4-dihexyl sulfosuccinate (CAS Reg. No. 3006-15-3) Surfactants, related 

adjuvants of 

surfactants

Sodium 1,4-diisobutyl sulfosuccinate (CAS Reg. No. 127-39-9) Surfactants, related 

adjuvants of 

surfactants

Sodium dioctylsulfosuccinate Surfactants, related 

adjuvants of 

surfactants

Sodium 1,4-dipentyl sulfosuccinate (CAS Reg. No. 922-80-5) Surfactants, related 

adjuvants of 

surfactants

Sodium hydroxide Neutralizer

Sodium monoalkyl and dialkyl (C6-C16) phenoxy benzenedisulfonates and related acids (CAS Reg. Nos. 147732-

59-0, 147732-60-3, 169662-22-0, 70191-75-2, 36445-71-3, 39354-74-0, 70146-13-3, 119345-03-8, 149119-20-0, 

149119-19-7, 119345-04-9, 28519-02-0, 25167-32-2, 30260-73-2, 65143-89-7, 70191-76-3)

Not to exceed 

20% in pesticide 

formulations

Surfactants, related 

adjuvants of 

surfactants

Sodium N-oleoyl-N-methyl taurine (CAS Reg. No. 137-20-2) Surfactants, related 

adjuvants of 

surfactants

Sodium and potassium salts of N-alkyl (C8-C18)-beta-iminodipropionic acid where the C8-C18 is linear and may be 

saturated and/or unsaturated (CAS Reg. Nos. 110676-19-2, 3655-00-3, 61791-56-8, 14960-06-6, 26256-79-1, 

90170-43-7, 91696-17-2, 97862-48-1)

Concentration in 

formulated enduse products not 

to exceed 30% by 

weight in pesticide 

formulations

Surfactants, related 

adjuvants of 

surfactants

Sodium starch glycolate (CAS Reg. No. 9063-38-1) Granular and 

tableted products 

only; not to exceed 

8% of the 

formulated product

Disintegrant

Sodium sulfate Solid diluent, carrier

Sorbitan fatty acid esters (fatty acids limited to C12, C14, C16, and C18 containing minor amounts of associated fatty 

acids) and poly(oxyethylene) derivatives of sorbitan fatty acid esters; the poly(oxyethylene) content averages 16-20 

moles

Buffering agent; 

corrosion inhibition

Sorbitol Antidusting agent.

Stearic acid (CAS Reg. No. 57-11-4) Lubricant, component 

animal tag

α-Stearoyl-ω-hydroxypoly(oxyethylene), average molecular weight (in amu) of 600 Emulsifier

α-Stearoyl-ω-hydroxypoly(oxyethylene); the poly(oxyethylene) content averages 8, 9, or 40 moles; if a blend of 

products is used, the average number of moles of ethylene oxide reacted to produce any product that is a 

component of the blend shall be 8, 9, or 40

Surfactants; related 

adjuvants of 

surfactants

Sulfite liquors and cooking liquors, spent, oxidized (CAS Reg. No. 68514-09-0) Surfactant, related 

adjuvants of 

surfactants

Sulfur (CAS Reg. No. 7704-34-9) Stabilizer

Talc Do.

Tall oil; fatty acids not less than 58%, rosin acids not more than 44%, unsaponifiables not more than 8% Surfactants, related 

adjuvants of 

surfactants

Tartrazine Dye, coloring agent

N,N,N′,N′′,-tetrakis-(2-hydroxypropyl) ethylenediamine (CAS Reg. No. 102-60-3) Concentration in 

formulated enduse products not 

to exceed 20% by 

weight in pesticide 

formulations

Stabilizer for 

formulation.

Trans-1,3,3,3-tetrafluoroprop-1-ene (CAS Reg. No. 29118-24-9) Propellant.

2,4,7,9-Tetramethyl-5-decyne-4.7-diol Not more than 

2.5% of pesticide 

formulation

Surfactants, related 

adjuvants of 

surfactants

Titanium dioxide (CAS Reg. No. 13463-67-7) Pigment/colorant in 

pesticide formulations 

for animal tag

Toluenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts Do.

Triacetin (glyceryl triacetate) Solvent, cosolvent

Trisodium phosphate Precipitant, buffer, 

filler

Xylene Solvent, cosolvent

Xylenesulfonic acid and its ammonium, calcium, magnesium, potassium, sodium, and zinc salts Surfactants, related 

adjuvants of 

surfactants

Zinc oxide Solid diluent, carrier

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Zinc stearate, conforming to 21 CFR 182.5994 and 582.5994 Water repellant, 

dessicant, and 

coating agent.

Zinc stearate (CAS Reg. No. 557-05-1) Water repellant, 

desiccant, and 

coating agent; 

stabilizer, component 

of plastic animal tag

Zinc sulfate (basic and monohydrate) Water repellant, 

dessicant, and 

coating agent

[69 FR 23130, Apr. 28, 2004]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.930, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.940 Tolerance exemptions for active and inert ingredients for use in antimicrobial formulations (Foodcontact surface sanitizing solutions).

Residues of the following chemical substances are exempted from the requirement of a tolerance when used in 

accordance with good manufacturing practice as ingredients in an antimicrobial pesticide formulation, provided that the 

substance is applied on a semi-permanent or permanent food-contact surface (other than being applied on food 

packaging) with adequate draining before contact with food.

(a) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation may be 

applied to: Food-contact surfaces in public eating places, dairy-processing equipment, and food-processing equipment 

and utensils.

Pesticide Chemical CAS Reg. No. Limits

Acetic acid 64-19-7 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Allyl cylcohexylpropionate 2705-87-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

α-alkyl-ω-hydroxypoly 

(oxypropylene) and/or poly 

(oxyethylene) polymers where the 

alkyl chain contains a minimum of 

six carbons

9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3; 9038-43-1; 9040-05-5; 

9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-52-8; 26468-86-0; 

26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-01-1; 34398-05-5; 37251-67-5; 

37311-00-5; 37311-01-6; 37311-02-7; 37311-04-9; 39587-22-9; 50861-66-0; 52232-09-4; 

52292-17-8; 52609-19-5; 57679-21-7; 59112-62-8; 60828-78-6; 61702-78-1; 61725-89-1; 

61791-13-7; 61791-20-6; 61791-28-4; 61804-34-0; 61827-42-7; 61827-84-7; 62648-50-4; 

63303-01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 64425-86-1; 

65104-72-5; 65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-08-0; 68002-96-0; 

68002-97-1; 68131-39-5; 68131-40-8; 68154-96-1; 68154-97-2; 68154-98-3; 68155-01-1; 

68213-23-0; 68213-24-1; 68238-81-3; 68238-82-4; 68409-58-5; 68409-59-6; 68439-30-5; 

68439-45-2; 68439-46-3; 68439-48-5; 68439-49-6; 68439-50-9; 68439-51-0; 68439-53-2; 

68439-54-3; 68458-88-8; 68526-94-3; 68526-95-4; 68551-12-2; 68551-13-3; 68551-14-4; 

68603-20-3; 68603-25-8; 68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 68954-94-9; 

68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 69013-19-0; 69227-20-9; 69227-21-0; 

69227-22-1; 69364-63-2; 70750-27-5; 70879-83-3; 70955-07-6; 71011-10-4; 71060-57-6; 

71243-46-4; 72066-65-0; 72108-90-8; 72484-69-6; 72854-13-8; 72905-87-4; 73018-31-2; 

73049-34-0; 74432-13-6; 74499-34-6; 78330-19-5; 78330-20-8; 78330-21-9; 78330-23-1; 

79771-03-2; 84133-50-6; 85422-93-1; 97043-91-9; 97953-22-5; 102782-43-4; 103331-86-8; 

103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 106232-83-1; 111905-54-5; 

116810-31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 121617-09-2; 

126646-02-4; 126950-62-7; 127036-24-2; 139626-71-4; 152231-44-2; 154518-36-2; 

157627-86-6; 157627-88-8; 157707-41-0; 157707-43-2; 159653-49-3; 160875-66-1; 

160901-20-2; 160901-09-7; 160901-19-9; 161025-21-4; 161025-22-5; 166736-08-9; 

169107-21-5; 172588-43-1; 176022-76-7; 196823-11-7; 287935-46-0; 288260-45-7; 

303176-75-2; 954108-36-2

Aluminum sulfate 10043-01-3 When ready for use, the enduse concentration is not to 

exceed 50 ppm

2-propen-1-aminium, 

N,N-dimethyl-N-propenyl-, 

chloride, homopolymer

26062-79-3 When ready for use, the enduse concentration is not to 

exceed 0.6%

Ammonium chloride 12125-02-9 When ready for use, the enduse concentration is not to 

exceed 48 ppm

Amylopectin, acid-hydrolyzed, 

1-oxtenylbutanedioate

113894-85-2 None

Amylopectin, hydrogen 

1-octadecenylbutanedioate

125109-81-1 None

Butryic acid 107-92-6 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Butyl alcohol 71-36-3

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When ready for use, the enduse concentration is not to 

exceed 100 ppm

n-Butyl benzoate 136-60-7 When ready for use, the enduse concentration is not to 

exceed 15,000 ppm

Citral 5392-40-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Citronellol 106-22-9 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Citronellyl acetate 150-84-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Copper sulfate pentahydrate 7758-99-8 When ready for use, the enduse concentration is not to 

exceed 80 ppm

β-Damascone, (Z)- 23726-92-3 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Decanal 112-31-2 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Decanoic acid 334-48-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

1-Decanol 112-30-1 When ready for use, the enduse concentration is not to 

exceed 100 ppm

(E)-4-Decenal 65405-70-1 When ready for use, the enduse concentration is not to 

exceed 100 ppm

D-Glucopyranose, oligomeric, 

decyl octyl glycosides

68515-73-1 None

2,6-Dimethyl-5-heptanal 106-72-9 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Di-n-butyl carbonate 542-52-9 When ready for use, the enduse concentration is not to 

exceed 15,000 ppm

2-Dodecanol, (2E)- 20407-84-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Ethanol 64-17-5 None

Ethyl 2-methylbutyrate 452-79-1 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Ethylenediaminetetraacetic acid 

(EDTA), tetrasodium salt

64-02-8 None

FD&C Green No. 3 CAS Reg. No. 2353-45-9 None

FD&C Red No. 40 25956-17-6 When ready for use, the enduse concentration is not to 

exceed 20 ppm.

FD&C Yellow No. 5 1934-21-0 When ready for use, the enduse concentration is not to 

exceed 1000 ppm

(E)-Geraniol 106-24-1 When ready for use, the enduse concentration is not to 

exceed 100 ppm

(E)-Geraniol acetate 105-87-3 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Heptanal 111-71-7 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Heptanoic acid 111-14-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Heptyl alcohol 111-70-6 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Hexanal 66-25-1 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Hexanoic acid 142-62-1 When ready for use, the enduse concentration is not to 

exceed 100 ppm

n-Hexanol 111-27-3 When ready for use, the enduse concentration is not to 

exceed 100 ppm

(Z)-3-Hexenol 928-96-1

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When ready for use, the enduse concentration is not to 

exceed 100 ppm

(Z)-3-Hexenol acetate 3681-71-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Hexyl acetate 142-92-7 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Hydrogen peroxide 7722-84-1 When ready for use, the enduse concentration is not to 

exceed 91 ppm

Hypochlorous acid, sodium salt 7681-52-9 When ready for use, the enduse concentration of all 

hypochlorous acid chemicals 

in the solution is not to 

exceed 200 ppm determined 

as total available chlorine

Iodine 7553-56-2 When ready for use, the total 

end-use concentration of all 

iodide-producing chemicals 

in the solution is not to 

exceed 25 ppm of titratable 

iodine

Lauric acid 143-07-7 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Lauric aldehyde 112-54-9 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Lauryl alcohol 112-53-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

d-Limonene 5989-27-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Lipase, triacylglycerol 9001-62-1 When ready for use, the enduse concentration is not to 

exceed 500 ppm

Magnesium oxide 1309-48-4 None

Methane sulfonic acid 75-75-2 When ready for use, the end 

use concentration is not to 

exceed 5,000 ppm

Methylene blue 61-73-4 When ready for use, the enduse concentration is not to 

exceed 0.4 ppm

Methyl-α-ionone 127-42-4 When ready for use, the enduse concentration is not to 

exceed 100 ppm

3-Methyl-2-butenyl acetate 1191-16-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

2-Methylundecanal 110-41-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

2-Methyl-1,3-propanediol 2163-42-0 None

Myristaldehyde 124-25-4 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Myristic acid 544-63-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Neryl acetate 141-12-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Nitric acid 7697-37-2 When ready for use, the enduse concentration is not to 

exceed 1,000 ppm

Nonanal 124-19-6 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Nonanoic acid 112-05-0 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Nonyl alcohol 143-08-8 When ready for use, the enduse concentration is not to 

exceed 100 ppm

α-(p-Nonylphenyl)-ω-hydroxypoly 

(oxyethylene) average poly

(oxyethylene) content 11 moles)

None None

Octadecanoic acid, calcium salt 1592-23-0 None

1315321-93-7

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9-Octadecenoic acid (9Z)-, 

sulfonated, oxidized

When ready for use, the enduse concentration is not to 

exceed 250 ppm.

9-Octadecenoic acid (9Z)-, 

sulfonated, oxidized, potassium 

salts

1315321-94-8 When ready for use, the enduse concentration is not to 

exceed 250 ppm.

9-Octadecenoic acid (9Z)-, 

sulfonated, oxidized, sodium salts

1315321-95-9 When ready for use, the enduse concentration is not to 

exceed 250 ppm.

Octanal 124-13-0 When ready for use, the enduse concentration is not to 

exceed 100 ppm

1-Octanesulfonic acid, sodium 

salt

5324-84-5 When ready for use, the enduse concentration is not to 

exceed 46 ppm

Octanoic acid 124-07-2 When ready for use, the enduse concentration is not to 

exceed 52 ppm

Octanoic acid 124-07-2 When ready for use, the enduse concentration is not to 

exceed 100 ppm

1-Octanol 111-87-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Oxirane, methyl-, polymer with 

oxirane, minimum molecular 

weight (in amu), 1900

9003-11-6 None

Palmitic acid 57-10-3 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Peroxyacetic acid 79-21-0 When ready for use, the enduse concentration is not to 

exceed 58 ppm

Peroxyoctanoic acid 33734-57-5 When ready for use, the enduse concentration is not to 

exceed 52 ppm

Phosphonic acid, 

(1-hydroxyethylidene)bis2809-21-4 When ready for use, the enduse concentration is not to 

exceed 14 ppm

Phosphoric acid, trisodium salt 7601-54-9 When ready for use, the enduse concentration is not to 

exceed 5916 ppm

Potassium bromide 7758-02-3 When ready for use, the enduse concentration is not to 

exceed 46 ppm total 

available halogen

Potassium iodide 7681-11-0 When ready for use, the total 

end-use concentration of all 

iodide-producing chemicals 

in the solution is not to 

exceed 25 ppm of titratable 

iodine

1,3-Propanediol 504-63-2 None

Propionic acid 79-09-4 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Propylene glycol 57-55-6 None

Quaternary ammonium 

compounds, alkyl (C12-C18) 

benzyldimethyl, chlorides

8001-54-5 When ready for use, the enduse concentration of all 

quaternary chemicals in the 

solution is not to exceed 200 

ppm of active quaternary 

compound

Quaternary ammonium 

compounds: n-alkyl (C12-18) 

dimethyl benzyl ammonium 

chloride

68424-85-1 When ready for use, the enduse concentration of all 

quaternary chemicals in 

solution is not to exceed 400 

ppm of active quaternary 

compound

Quaternary Ammonium 

Compounds: n-alkyl (C 12-14) 

dimethyl ethylbenzyl ammonium 

chloride, average molecular 

weight (in amu), 377 to 384

85409-23-0 When ready for use, the enduse concentration of all 

quaternary chemicals in 

solution is not to exceed 400 

ppm of active quaternary 

compound.

Quaternary ammonium 

compounds n-alkyl (C12-C18) 

dimethyl ethylbenzyl ammonium 

chloride average molecular 

weight (in amu) 384

None When ready for use, the enduse concentration of all 

quaternary chemicals in the 

solution is not to exceed 200 

ppm of active quaternary 

compound

Quaternary ammonium 

compounds, Di-n-Alkyl (C8-10) 

None When ready for use, the enduse concentration of these 

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dimethyl ammonium chloride, 

average molecular weight (in 

amu) 332 to 361

specific in quaternary 

ammonium compounds is not 

to exceed 240 ppm of active 

quaternary ammonium 

compound; the end-use 

concentration of all 

quaternary chemicals in the 

solution is not to exceed 400 

ppm of active quaternary 

compound

Quaternary ammonium 

compounds, didecyl dimethyl 

ammonium carbonate/didecyl 

dimethyl ammonium bicarbonate

148788-55-0/148812-654-1 When ready for use, the enduse concentration of these 

specific ammonium 

compounds is not to exceed 

400 ppm of active quaternary 

ammonium compound

Silver ions resulting from the use 

of electrolytically-generated silver 

ions stabilized in citric acid as 

silver dihydrogen citrate (does not 

include metallic silver)

14701-21-4 When ready for use, the enduse concentration of silver 

ions is not to exceed 50 ppm 

of active silver

Sodium bisulfate 7681-38-1 When ready for use, the enduse concentration is not to 

exceed 2,000 ppm.

Sorbitan, mono-9-octadecenoate, 

poly(oxy-1,2-ethanediyl) derivs., 

(Z)-

9005-65-6 None

Stearic acid. 57-11-4 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Sulfuric acid 7664-93-9 Food-contact surfaces in 

public eating places, dairyprocessing equipment, and 

food-processing equipment 

and utensils in antimicrobial 

formulations. Not to exceed 

600 ppm.

Sulfuric acid monododecyl ester, 

sodium salt (sodium lauryl sulfate)

151-21-3 When ready for use, the enduse concentration is not to 

exceed 350 ppm

Trans-1,3,3,3-tetrafluoroprop-1-

ene

29118-24-9 None

1,3,5-Triazine-2,4,6(1H,3H,5H)

-trione, 1,3-dichloro-, sodium salt

2893-78-9 When ready for use, the enduse concentration of all di- or 

trichloroisocyanuric acid 

chemicals in the solution is 

not to exceed 100 ppm 

determined as total available 

chlorine

2-Tridecanal 7774-82-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

3,5,5-Trimethylhexanal 5435-64-3 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Undecanal 112-44-7 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Undecyl alcohol 112-42-5 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Valeraldehyde 110-62-3 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Valeric acid 109-52-4 When ready for use, the enduse concentration is not to 

exceed 100 ppm

Xylenesulfonic acid, sodium salt 1300-72-7 When ready for use, the enduse concentration is not to 

exceed 500 ppm

(b) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation may be 

applied to: Dairy processing equipment, and food-processing equipment and utensils.

Pesticide Chemical

CAS Reg. 

No. Limits

>Acetic acid 64-19-7 When ready for use, the end-use concentration is not to exceed 1200 ppm

Acetic acid, chloro-, sodium salt, reaction products with 

4,5-dihydro-2-undecyl-1H-imidazole-1-ethanol and 

sodium hydroxide

68608-66-2 When ready for use, the end-use concentration is not to exceed 42 ppm chloroacetic 

acid

Benzenesulfonic acid, dodecyl- 27176-87-0 When ready for use, the end-use concentration is not to exceed 5.5 ppm

Butanedioic acid, octenyl- 28805-58-5 When ready for use, the end-use concentration is not to exceed 156 ppm

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Butoxy monoether of mixed (ethylene-propylene) 

polyalkylene glycol, minimum average molecular weight 

(in amu), 2400

None None

Calcium chloride 10043-52-4 When ready for use, the end-use concentration is not to exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of a mixture of not 

less than 56% octanoic acid and not less than 40% 

decanoic acid

None When ready for use, the end-use concentration is not to exceed 39 ppm

Decanoic acid 334-48-5 When ready for use, the end-use concentration is not to exceed 90 ppm

Ethanesulfonic acid, 2-[cyclohexyl (1-oxohexadecyl) 

amino]-, sodium salt

132-43-4 When ready for use, the end-use concentration is not to exceed 237 ppm

Ethylenediaminetetraacetic acid (EDTA), disodium salt 139-33-3 When ready for use, the end-use concentration is not to exceed 1400 ppm

FD&C Yellow No. 5 (Tartrazine) (conforming to 21 CFR 

74.705)

1934-21-0 None

D-Gluconic acid, monosodium salt 527-07-1 When ready for use, the end-use concentration is not to exceed 760 ppm

Hydriodic acid 10034-85-2 When ready for use, the total end-use concentration of all iodide-producing 

chemicals is not to exceed 25 ppm of titratable iodine

Hydrogen peroxide 7722-84-1 When ready for use, the end-use concentration is not to exceed 465 ppm

Hypochlorous acid 7790-92-3 When ready for use, the end-use concentration of all hypochlorous acid chemicals in 

the solution is not to exceed 200 ppm determined as total available chlorine

Iodine 7553-56-2 When ready for use, the total end-use concentration of all iodide-producing 

chemicals in the solution is not to exceed 25 ppm of titratable iodine

Lactic acid 50-21-5 When ready for use, the end-use concentration is not to exceed 138 ppm

Nonanoic acid 112-05-0 When ready for use, the end-use concentration is not to exceed 90 ppm

1-Octanamine, N,N-dimethyl- 7378-99-6 When ready for use, the end-use concentration is not to exceed 113 ppm

1,2-Octanedisulfonic acid 113669-58-2 When ready for use, the end-use concentration is not to exceed 102 ppm

1-Octanesulfonic acid 3944-72-7 When ready for use, the end-use concentration is not to exceed 172 ppm

1-Octanesulfonic acid, sodium salt 5324-84-5 When ready for use, the end-use concentration is not to exceed 297 ppm

1-Octanesulfonic acid, 2-sulfino- 113652-56-5 When ready for use, the end-use concentration is not to exceed 102 ppm

Octanoic acid 124-07-2 When ready for use, the end-use concentration is not to exceed 176 ppm

Oxychloro species (including chlorine dioxide) generated 

by acidification of an aqueous solution of sodium chlorite

None When ready for use, the end-use concentration is not to exceed 200 ppm of chlorine 

dioxide as determined by the method titled, Iodometric Method for the Determination 

of Available Chlorine Dioxide (50-250 ppm available chlorine dioxide)

Peroxyacetic acid 79-21-0 When ready for use, the end-use concentration is not to exceed 315 ppm

Peroxyoctanoic acid 33734-57-5 When ready for use, the end-use concentration is not to exceed 122 ppm

Phosphonic acid, (1-hydroxyethylidene)bis- 2809-21-4 When ready for use, the end-use concentration is not to exceed 34 ppm

Phosphoric acid 7664-38-2 None

Phosphoric acid, monosodium salt 7558-80-7 When ready for use, the end-use concentration is not to exceed 350 ppm

Potassium iodide 7681-11-0 When ready for use, the total end-use concentration of all iodide-producing 

chemicals in the solution is not to exceed 25 ppm of titratable iodine

Propanoic acid 79-09-4 When ready for use, the end-use concentration is not to exceed 297 ppm

2,6-Pyridinedicarboxylic acid 499-83-2 When ready for use, the end-use concentration is not to exceed 1.2 ppm

Sulfuric acid monododecyl ester, sodium salt (sodium 

lauryl sulfate)

151-21-3 When ready for use, the end-use concentration is not to exceed 350 ppm

(c) The following chemical substances when used as ingredients in an antimicrobial pesticide formulation may be 

applied to: Food-processing equipment and utensils.

Pesticide Chemical 

CAS Reg. 

No. Limits

Acetic acid 64-19-7 When ready for use, the end-use concentration is not to 

exceed 1,200 ppm

Acetic acid, chloro-, sodium salt, reaction products with 4,5-dihydro-2-undecyl-1Himidazole-1-ethanol and sodium hydroxide68608-66-2 When ready for use, the end-use concentration is not to 

exceed 42 ppm chloroacetic acid

Ammonium chloride 12125-02-9 When ready for use, the end-use concentration is not to 

exceed 48 ppm

Benzenesulfonic acid, dodecyl- 27176-87-0 When ready for use, the end-use concentration is not to 

exceed 400 ppm

Benzenesulfonic acid, dodecyl-, sodium salt 25155-30-0 When ready for use, the end-use concentration is not to 

exceed 430 ppm

[1,1′-Biphenyl]-2-ol 90-43-7 When ready for use, the end-use concentration is not to 

exceed 400 ppm

Boric acid, sodium salt 7775-19-1 None

Butanedioic acid, octenyl- 28805-58-5 When ready for use, the end-use concentration is not to 

exceed 156 ppm

Butanedioic acid, sulfo-, 1,4-dioctyl ester, sodium salt 1639-66-3 None

Butoxy monoether of mixed (ethylene-propylene) polyalkylene glycol, cloudpoint of 90 

- 100o

C in 0.5 aqueous solution, average molecular weight (in amu), 3300

None None

Butoxy monoether of mixed (ethylene-propylene) polyalkylene glycol, minimum 

average molecular weight (in amu), 2400

None None

Calcium chloride 10043-52-4 When ready for use, the end-use concentration is not to 

exceed 17 ppm

n-Carboxylic acids (C6-C12), consisting of a mixture of not less than 56% octanoic acid 

and not less than 40% decanoic acid

None When ready for use, the end-use concentration is not to 

exceed 39 ppm

3-Cyclohexene-1-methanol,α,α,4-trimethyl- 98-55-5 None 

1-Decanaminium, N-decyl-N, N-dimethyl-, chloride 7173-51-5 When ready for use, the end-use concentration is not to 

exceed 200 ppm of active quaternary compound

Decanoic acid 3347-48-5

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When ready for use, the end-use concentration is not to 

exceed 234 ppm

Ethanesulfonic acid, 2-[cyclohexyl (1-oxohexadecyl) amino]-, sodium salt 132-43-4 When ready for use, the end-use concentration is not to 

exceed 237 ppm

Ethanol 64-17-5 None

Ethanol, 2 butoxy- 111-76-2 None

Ethanol, 2-(2-ethoxyethoxy)- 111-90-0 None

Ethylenediaminetetraacetic acid (EDTA), disodium salt 139-33-3 When ready for use, the end-use concentration is not to 

exceed 1400 ppm

Ethylenediaminetetraacetic acid (EDTA), tetrasodium salt 64-02-8 None

Fatty acids, coco, potassium salts 61789-30-8 None

Fatty acids, tall-oil, sulfonated, sodium salts 68309-27-3 When ready for use, the end-use concentration is not to 

exceed 66 ppm

FD&C Yellow No. 5 (Tartrazine) (conforming to 21 CFR 74.705) 1934-21-0 None

D-Gluconic acid, monosodium salt 527-07-1 When ready for use, the end-use concentration is not to 

exceed 760 ppm

Hydriodic acid 10034-85-2 When ready for use, the total end-use concentration of 

all iodide-producing chemicals in the solution is not to 

exceed 25 ppm of titratable iodine

Hydrogen peroxide 7722-84-1 When ready for use, the end-use concentration is not to 

exceed 1100 ppm

Hypochlorous acid 7790-92-3 When ready for use, the end-use concentration of all 

hypochlorous acid chemicals in the solution is not to 

exceed 200 ppm determined as total available chlorine

Hypochlorous acid, calcium salt 7778-54-3 When ready for use, the end-use concentration of all 

hypochlorous acid chemicals in the solution is not to 

exceed 200 ppm determined as total available chlorine

Hypochlorous acid, lithium salt 13840-33-0 When ready for use, the end-use concentration of all 

hypochlorous acid chemicals in the solution is not to 

exceed 200 ppm determined as total available chlorine 

and 30 ppm lithium

Hypochlorous acid, potassium salt 7778-66-7 When ready for use, the end-use concentration of all 

hypochlorous acid chemicals in the solution is not to 

exceed 200 ppm determined as total available chlorine

Hypochlorous acid, sodium salt 7681-52-9 When ready for use, the end-use concentration of all 

hypochlorous acid chemicals in the solution is not to 

exceed 200 ppm determined as total available chlorine

Iodine 7553-56-2 When ready for use, the total end-use concentration of 

all iodide-producing chemicals in the solution is not to 

exceed 25 ppm of titratable iodine

Lactic acid 50-21-5 None

Magnesium oxide 1309-48-4 None

Methylene blue 61-73-4 When ready for use, the end-use concentration is not to 

exceed 0.4 ppm

Neodecanoic acid 26896-20-8 When ready for use, the end-use concentration is not to 

exceed 174 ppm

Nonanoic acid 112-05-0 When ready for use, the end-use concentration is not to 

exceed 90 ppm

α-(p-Nonylphenyl)-ω-hydroxypoly (oxyethylene) maximum average molecular weight 

(in amu), 748

None None

α-(p-Nonylphenol)-ω-hydroxypoly (oxyethylene) average poly(oxyethylene) content 11 

moles

None None

α-(p-Nonylphenyl)-ω-hydroxypoly (oxyethylene) produced by the condensation of 1 

mole p-nonylphenol with 9 to 12 moles ethylene oxide

None None

α-(p-Nonylphenyl)-ω-hydroxypoly (oxyethylene), 9 to 13 moles ethylene oxide None None 

Octadecanoic acid, calcium salt 1592-23-0 None

9-Octadecenoic acid (9Z)-, sulfonated 68988-76-1 When ready for use, the end-use concentration is not to 

exceed 312 ppm

9-Octadecenoic acid (9Z)-sulfonated, sodium salts 68443-05-0 When ready for use, the end-use concentration is not to 

exceed 200 ppm

1-Octanamine, N,N-dimethyl- 7378-99-6 When ready for use, the end-use concentration is not to 

exceed 113 ppm

1,2-Octanedisulfonic acid 113669-58-2 When ready for use, the end-use concentration is not to 

exceed 102 ppm

1-Octanesulfonic acid 3944-72-7 When ready for use, the end-use concentration is not to 

exceed 172 ppm

1-Octanesulfonic acid, sodium salt 5324-84-5 When ready for use, the end-use concentration is not to 

exceed 312 ppm

1-Octanesulfonic acid, 2-sulfino- 113652-56-5 When ready for use, the end-use concentration is not to 

exceed 102 ppm

Octanoic acid 124-07-2 When ready for use, the end-use concentration is not to 

exceed 234 ppm

Oxirane, methyl-, polymer with oxirane, minimum molecular weight (in amu), 1900 9003-11-6 None

Oxirane, methyl-, polymer with oxirane, block, average molecular weight (in amu), 

1900

106392-12-5 None

Oxirane, methyl-, polymer with oxirane, block, minimum average molecular weight (in 

amu), 2000

None None

Oxirane, methyl-, polymer with oxirane, block, 27 to 31 moles of polyoxypropylene, 

average molecular weight (in amu) 2000

None None

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Oxychloro species (predominantly chlorite, chlorate and chlorine dioxide in an 

equilibrium mixture) generated either (i) by directly metering a concentrated chlorine 

dioxide solution prepared just prior to use, into potable water, or (ii) by acidification of 

an aqueous alkaline solution of oxychloro species (predominately chlorite and 

chlorate) followed by dilution with potable water

None When ready for use, the end-use concentration is not to 

exceed 200 ppm of chlorine dioxide as determined by 

the method titled, “Iodometric Method for the 

Determination of Available Chlorine Dioxide (50-250 

ppm available chlorine dioxide)”

Oxychloro species (including chlorine dioxide) generated by acidification of an 

aqueous solution of sodium chlorite

None When ready for use, the end-use concentration is not to 

exceed 200 ppm of chlorine dioxide as determined by 

the method titled, “Iodometric Method for the 

Determination of Available Chlorine Dioxide (50-250 

ppm available chlorine dioxide)”

2,4-Pentanediol, 2-methyl- 107-41-5 None

Peroxyacetic acid 79-21-0 When ready for use, the end-use concentration is not to 

exceed 315 ppm

Peroxyoctanoic acid 33734-57-5 When ready for use, the end-use concentration is not to 

exceed 122 ppm

Phenol, 4-chloro-2-(phenylmethyl)- 120-32-1 When ready for use, the end-use concentration is not to 

exceed 320 ppm

Phenol, 4-(1,1-dimethylpropyl)- 80-46-6 When ready for use, the end-use concentration is not to 

exceed 80 ppm

Phosphonic acid, (1-hydroxyethylidene)bis- 2809-21-4 When ready for use, the end-use concentration is not to 

exceed 34 ppm

Phosphoric acid 7664-38-2 None

Phosphoric acid, monosodium salt 7558-80-7 When ready for use, the end-use concentration is not to 

exceed 350 ppm

Phosphoric acid, trisodium salt 7601-54-9 When ready for use, the end-use concentration is not to 

exceed 5916 ppm

Poly(oxy-1,2-ethanediyl), α-[(1,1,3,3-tetramethylbutyl) phenyl]-ω-hydroxy-, produced 

with one mole of the phenol and 4 to 14 moles ethylene oxide

None None

Potassium bromide 7758-02-3 When ready for use, the end-use concentration of all 

bromide-producing chemicals in the solution is not to 

exceed 200 ppm total available halogen

Potassium iodide 7681-11-0 When ready for use, the total end-use concentration of 

all iodide-producing chemicals in the solution is not to 

exceed 25 ppm of titratable iodine

Propanoic acid 79-09-4 When ready for use, the end-use concentration is not to 

exceed 297 ppm

2,6-Pyridinedicarboxylic acid 499-83-2 When ready for use, the end-use concentration is not to 

exceed 1.2 ppm

Quaternary ammonium compounds, alkyl (C12-C18) benzyldimethyl, chlorides 8001-54-5 When ready for use, the end-use concentration of this 

specific quaternary compound is not to exceed 200 ppm 

within the end-use total concentration that is not to 

exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12-C14) dimethyl ethylbenzyl ammonium 

chloride, average molecular weight (in amu), 377 to 384

None When ready for use, the end-use concentration of this 

specific quaternary compound is not to exceed 200 ppm 

within the end-use total concentration that is not to 

exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, n-alkyl (C12-C18) dimethyl ethylbenzyl ammonium 

chloride average molecular weight (in amu) 384

None When ready for use, the end-use concentration of this 

specific quaternary compound is not to exceed 200 ppm 

within the end-use total concentration that is not to 

exceed 400 ppm active quaternary compound

Quaternary ammonium compounds, di-n-Alkyl (C8-C10) dimethyl ammonium chloride, 

average molecular weight (in amu), 332 to 361

None When ready for use, the end-use concentration of this 

specific quaternary compound is not to exceed 240 ppm 

within the end-use total concentration that is not to 

exceed 400 ppm active quaternary compound

Sodium-α-alkyl(C12-C15)-ω-hydroxypoly (oxyethylene) sulfate with the poly

(oxyethylene) content averaging one mole

None None

Sodium bromide 7647-15-6 When ready for use, the end-use concentration of all 

bromide-producing chemicals in the solution is not to 

exceed 200 ppm total available halogen

Sodium iodide 7681-82-5 When ready for use, the total end-use concentration of 

all iodide-producing chemicals in the solution is not to 

exceed 25 ppm of titratable iodine

Sulfuric acid monododecyl ester, sodium salt (sodium lauryl sulfate) 151-21-3 None

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro- 2782-57-2 When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is 

not to exceed 100 ppm determined as total available 

chlorine

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, potassium salt 2244-21-5 When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is 

not to exceed 100 ppm determined as total available 

chlorine

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3-dichloro-, sodium salt 2893-78-9 When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is 

not to exceed 100 ppm determined as total available 

chlorine

1,3,5-Triazine-2,4,6(1H,3H,5H)-trione, 1,3,5-trichloro- 87-90-1 When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is 

not to exceed 100 ppm determined as total available 

chlorine

1,3,5-Triazine, N,N′,N′′-trichloro-2,4,6-triamino- 7673-09-8 When ready for use, the end-use concentration of all dior trichloroisocyanuric acid chemicals in the solution is 

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not to exceed 200 ppm determined as total available 

chlorine

[69 FR 23136, Apr. 28, 2004, as amended at 71 FR 30811, May 31, 2006; 71 FR 45423, Aug. 9, 2006; 71 FR 46125, Aug. 11, 2006; 

72 FR 51186, Sept. 6, 2007; 73 FR 37858, July 2, 2008; 73 FR 49107, Aug. 20, 2008; 73 FR 53725, Sept. 17, 2008; 74 FR 27454, 

June 10, 2009; 74 FR 38944, Aug. 5, 2009; 74 FR 40509, Aug. 12, 2009; 75 FR 40735, July 14, 2010; 76 FR 55267, Sept. 7, 2011; 

77 FR 45498, Aug. 1, 2012; 77 FR 50617, Aug. 22, 2012; 77 FR 53150, Aug. 31, 2012; 77 FR 68692, Nov. 16, 2012; 78 FR 35147, 

June 12, 2013; 78 FR 46264, July 31, 2013; 78 FR 48621, Aug. 9, 2013; 78 FR 59269, Sept. 26, 2013; 78 FR 65565, Nov. 1, 2013; 

78 FR 67042, Nov. 8, 2013; 78 FR 78731, Dec. 27, 2013; 79 FR 6096, Feb. 3, 2014; 79 FR 26152, May 7, 2014; 79 FR 32666, June 

6, 2014; 79 FR 33473, June 11, 2014; 79 FR 52993, Sept. 5, 2014; 79 FR 66312, Nov. 7, 2014; 80 FR 11593, Mar. 4, 2015; 80 FR 

28842, May 20, 2015; 80 FR 32033, 32038, June 5, 2015; 80 FR 34070, June 15, 2015; 80 FR 48752, Aug. 14, 2015; 80 FR 50211, 

Aug. 19, 2015; 80 FR 61122, Oct. 9, 2015; 80 FR 62466, Oct. 16, 2015]

 Back to Top

§180.950 Tolerance exemptions for minimal risk active and inert ingredients.

Unless specifically excluded, residues resulting from the use of the following substances as either an inert or an active 

ingredient in a pesticide chemical formulation, including antimicrobial pesticide chemicals, are exempted from the 

requirement of a tolerance under FFDCA section 408, if such use is in accordance with good agricultural or manufacturing 

practices.

(a) Commonly consumed food commodities. Commonly consumed food commodities means foods that are commonly 

consumed for their nutrient properties. The term commonly consumed food commodities shall only apply to food 

commodities (whether a raw agricultural commodity or a processed commodity) in the form the commodity is sold or 

distributed to the public for consumption.

(1) Included within the term commonly consumed food commodities are:

(i) Sugars such as sucrose, lactose, dextrose and fructose, and invert sugar and syrup.

(ii) Spices such as cinnamon, cloves, and red pepper.

(iii) Herbs such as basil, anise, or fenugreek.

(2) Excluded from the term commonly consumed food commodities are:

(i) Any food commodity that is adulterated under 21 U.S.C. 342.

(ii) Both the raw and processed forms of peanuts, tree nuts, milk, soybeans, eggs, fish, crustacea, and wheat.

(iii) Alcoholic beverages.

(iv) Dietary supplements.

(b) Animal feed items. Animal feed items means meat meal and all items derived from field crops that are fed to 

livestock excluding both the raw and processed forms of peanuts, tree nuts, milk, soybeans, eggs, fish, crustacea, and 

wheat. Meat meal is an animal feed composed of dried animal fat and protein that has been sterilized. Other than meat 

meal, the term animal feed item does not extend to any item designed to be fed to animals that contains, to any extent, 

components of animals. Included within the term animal feed items are:

(1) The hulls and shells of the commodities specified in paragraph (a)(2)(ii) of this section, and cocoa bean.

(2) Bird feed such as canary seed.

(3) Any feed component of a medicated feed meeting the definition of an animal feed item.

(c) Edible fats and oils. Edible fats and oils means all edible (food or feed) fats and oils, derived from either plants or 

animals, whether or not commonly consumed, including products derived from hydrogenating (food or feed) oils, or 

liquefying (food or feed) fats. 

(1) Included within the term edible fats and oils are oils (such as soybean oil) that are derived from the commodities 

specified in paragraph (a)(2)(ii) of this section when such oils are highly refined via a solvent extraction procedure. 

(2) Excluded from the term edible fats and oils are plant oils used in the pesticide chemical formulation specifically to 

impart their characteristic fragrance and/or flavoring.

(d) [Reserved] 

(e) Specific chemical substances. Residues resulting from the use of the following substances as either an inert or an 

active ingredient in a pesticide chemical formulation, including antimicrobial pesticide chemicals, are exempted from the 

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requirement of a tolerance under FFDCA section 408, if such use is in accordance with good agricultural or manufacturing 

practices. 

Chemical CAS No.

Acetic acid, sodium salt 127-09-3

Alpha-cyclodextrin 10016-20-3

Amylopectin, acid-hydrolyzed, 1-octenylbutanedioate 113894-

85-2

Amylopectin, hydrogen 1-octadecenylbutanedioate 125109-

81-1

Animal glue None

Ascorbic acid (vitamin C) 50-81-7

Beeswax 8012-89-3

Benzoic acid, sodium salt 532-32-1

Beta-cyclodextrin 7585-39-9

Carbonic acid, monopotassium salt 298-14-6

Carbonic acid, monosodium salt (sodium bicarbonate) 144-55-8

Carnauba wax 8015-86-9

Carob gum (locust bean gum) 9000-40-2

Castor oil 8001-79-4

Castor oil, hydrogenated 8001-78-3

Cellulose 9004-34-6

Cellulose acetate 9004-35-7

Cellulose, carboxy methyl ether, sodium salt 9004-32-4

Cellulose, 2-hydroxyethyl ether 9004-62-0

Cellulose, 2-hydroxypropyl ether 9004-64-2

Cellulose, 2-hydroxypropyl methyl ether 9004-65-3

Cellulose, methyl ether 9004-67-5

Cellulose, mixture with cellulose carboxymethyl ether, sodium salt 51395-75-6

Cellulose, pulp 65996-61-4

Cellulose, regenerated 68442-85-3

Citric acid 77-92-9

Citric acid, 2-(acetyloxy)-, tributyl ester 77-90-7

Citric acid, calcium salt 7693-13-2

Citric acid, calcium salt (2:3) 813-94-5

Citric acid, dipotassium salt 3609-96-9

Citric acid, disodium salt 144-33-2

Citric acid, monohydrate 5949-29-1

Citric acid, monopotassium salt 866-83-1

Citric acid, monosodium salt 18996-35-5

Citric acid, potassium salt 7778-49-6

Citric acid, triethyl ester 77-93-0

Citric acid, tripotassium salt 866-84-2

Citric acid, tripotassium salt, monohydrate 6100-05-6

Citric acid, sodium salt 994-36-5

Citric acid, trisodium salt 68-04-2

Citric acid, trisodium salt, dihydrate 6132-04-3

Citric acid, trisodium salt, pentahydrate 6858-44-2

Coffee grounds 68916-18-7

Dextrins 9004-53-9

1,3-Dioxolan-2-one, 4-methyl-(propylene carbonate) 108-32-7

Fumaric acid 110-17-8

Gamma-cyclodextrin 17465-86-0

Gellan gum 71010-52-1

D-Glucitol (sorbitol) 50-70-4

Glycerol (glycerin) (1,2,3-propanetriol) 56-81-5

Guar gum 9000-30-0

Humic acid 1413-93-6

Humic acid, potassium salt 68514-28-3

Humic acid, sodium salt 68131-04-4

Lactic acid, n-butyl ester 138-22-7

Lactic acid, n-butyl ester, (S) 34451-19-9

Lactic acid, ethyl ester 97-64-3

Lactic acid, ethyl ester,(S) 687-47-8

Lanolin 8006-54-0

Lecithins 8002-43-5

Lecithins, soya 8030-76-0

Licorice Extract 68916-91-6

Maltodextrin 9050-36-6

Paper None

Potassium chloride 7447-40-7

2-Propanol (isopropyl alcohol) 67-63-0

Red cabbage color, expressed from edible red cabbage heads via a pressing process using only acidified water None

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Silica, amorphous, fumed (crystalline free) 112945-

52-5

Silica, amorphous, precipitated and gel 7699-41-4

Silica gel 63231-67-4

Silica gel, precipitated, crystalline-free 112926-

00-8

Silica, hydrate 10279-57-9

Silica, vitreous 60676-86-0

Soap (The water soluble sodium or potassium salts of fatty acids produced by either the saponification of fats and oils, or the neutralization of 

fatty acid)

None

Sorbic acid, potassium salt 24634-61-5

Soapbark (Quillaja saponin) 1393-03-9

Sodium alginate 9005-38-3

Sodium chloride 7647-14-5

Syrups, hydrolyzed starch, hydrogenated 68425-17-2

Ultramarine blue (C.I. Pigment Blue 29) 57455-37-5

Urea 57-13-6

Vanillin 121-33-5

Xanthan gum 11138-66-2

[67 FR 36537, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.950, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.960 Polymers; exemptions from the requirement of a tolerance.

Residues resulting from the use of the following substances, that meet the definition of a polymer and the criteria 

specified for defining a low-risk polymer in 40 CFR 723.250, as an inert ingredient in a pesticide chemical formulation, 

including antimicrobial pesticide chemical formulations, are exempted from the requirement of a tolerance under FFDCA 

section 408, if such use is in accordance with good agricultural or manufacturing practices. 

Polymer CAS No.

Acetic acid ethenyl ester, polymer with ethane, ethenyltriethoxysilane 

and sodium ethenesulfonate (1:1); minimum number average 

molecular weight (in amu), 16,200

913187-38-9

Acetic acid ethenyl ester, polymer with ethenol and (α)-2-

propenyl-(ω)-hydroxypoly (oxy-1,2-ethanediyl) minimum number 

average molecular weight (in amu), 15,000

137091-12-4 

Acetic acid ethenyl ester, polymer with 1-ethenyl-2-pyrrolidinone 25086-89-9

Acetic acid ethenyl ester, polymer with oxirane, minimum number 

average molecular weight (in amu), 17,000

25820-49-9

Acetic acid ethenyl ester, polymer with sodium 2-methyl-2-[(1-oxo-2-

propen-1-yl)amino]-1-propanesulfonate (1:1), hydrolyzed, minimum 

number average molecular weight (in amu), 61,000

924892-37-5

Acrylic acid-benzyl methacrylate-1-propanesulfonic acid, 2-methyl-2-

[(1-oxo-2-propenyl)amino]-, monosodium salt, minimum number 

average molecular weight (in amu), 1500

1152297-42-1

Acrylic acid, polymerized, and its ethyl and methyl esters None 

Acrylic acid-sodium acrylate-sodium-2-methylpropanesulfonate 

copolymer, minimum average molecular weight (in amu), 4,500

97953-25-8 

Acrylic acid-stearyl methacrylate copolymer, minimum number 

average molecular weight (in amu), 2,500

27756-15-6 

Acrylic acid, styrene, α-methyl styrene copolymer, ammonium salt, 

minimum number average molecular weight (in amu), 1,250

89678-90-0

Acrylic acid terpolymer, partial sodium salt, minimum number 

average molecular weight (in amu), 2,400

151006-66-5

Acrylic polymers composed of one or more of the following 

monomers: Acrylic acid, methyl acrylate, ethyl acrylate, butyl 

acrylate, hydroxyethyl acrylate, hydroxypropyl acrylate, hydroxybutyl 

acrylate, carboxyethyl acrylate, methacrylic acid, methyl 

methacrylate, ethyl methacrylate, butyl methacrylate, isobutyl 

methacrylate, hydroxyethyl methacrylate, hydroxypropyl 

methacrylate, hydroxybutyl methacrylate, lauryl methacrylate, and 

stearyl methacrylate; with none and/or one or more of the following 

monomers: Acrylamide, N-methyl acrylamide, N,N-dimethyl 

acrylamide, N-octylacrylamide, maleic anhydride, maleic acid, 

monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl 

maleate; and their corresponding sodium, potassium, ammonium, 

isopropylamine, triethylamine, monoethanolamine, and/or 

triethanolamine salts; the resulting polymer having a minimum 

number average molecular weight (in amu), 1,200

None

Acrylonitrile-butadiene copolymer conforming to 21 CFR 180.22, 

minimum average molecular weight (in amu), 1,000

9003-18-3 

Acrylonitrile-styrene-hydroxypropyl methacrylate copolymer, 

minimum number average molecular weight (in amu), 447,000

None

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α-alkyl (C12-C15) - ω- hydroxypoly(oxypropylene)poly(oxyethylene)

copolymers (where the poly(oxypropylene) content is 3-60 moles 

and the poly(oxyethylene) content is 5-80 moles), the resulting 

ethoxylated propoxylated (C12-C15) alcohols having a minimum 

molecular weight (in amu), 1,500

68551-13-3

α-alkyl-ω-hydroxypoly (oxypropylene) and/or poly (oxyethylene) 

polymers where the alkyl chain contains a minimum of six carbons 

and a minimum number average molecular weight (in amu) 1,100

9002-92-0; 9004-95-9; 9004-98-2; 9005-00-9; 9035-85-2; 9038-29-3; 9038-43-1; 

9040-05-5; 9043-30-5; 9087-53-0; 25190-05-0; 24938-91-8; 25231-21-4; 26183-

52-8; 26468-86-0; 26636-39-5; 27252-75-1; 27306-79-2; 31726-34-8; 34398-

01-1; 34398-05-5; 37251-67-5; 37311-00-5; 37311-01-6; 37311-02-7; 37311-

04-9; 39587-22-9; 50861-66-0; 52232-09-4; 52292-17-8; 52609-19-5; 57679-

21-7; 59112-62-8; 60828-78-6; 61702-78-1; 61725-89-1; 61791-13-7; 61791-

20-6; 61791-28-4; 61804-34-0; 61827-42-7; 61827-84-7; 62648-50-4; 63303-

01-5; 63658-45-7; 63793-60-2; 64366-70-7; 64415-24-3; 64415-25-4; 64425-

86-1; 65104-72-5; 65150-81-4; 66455-14-9: 66455-15-0; 67254-71-1; 67763-

08-0; 68002-96-0; 68002-97-1; 68131-39-5; 68131-40-8; 68154-96-1; 68154-

97-2; 68154-98-3; 68155-01-1; 68213-23-0; 68213-24-1; 68238-81-3; 68238-

82-4; 68409-58-5; 68409-59-6; 68439-30-5; 68439-45-2; 68439-46-3; 68439-

48-5; 68439-49-6; 68439-50-9; 68439-51-0; 68439-53-2; 68439-54-3; 68458-

88-8; 68526-94-3; 68526-95-4; 68551-12-2; 68551-13-3; 68551-14-4; 68603-

20-3; 68603-25-8; 68920-66-1; 68920-69-4; 68937-66-6; 68951-67-7; 68954-

94-9; 68987-81-5; 68991-48-0; 69011-36-5; 69013-18-9; 69013-19-0; 69227-

20-9; 69227-21-0; 69227-22-1; 69364-63-2; 70750-27-5; 70879-83-3; 70955-

07-6; 71011-10-4; 71060-57-6; 71243-46-4; 72066-65-0; 72108-90-8; 72484-

69-6; 72854-13-8; 72905-87-4; 73018-31-2; 73049-34-0; 74432-13-6; 74499-

34-6; 78330-19-5; 78330-20-8; 78330-21-9; 78330-23-1; 79771-03-2; 84133-

50-6; 85422-93-1; 97043-91-9; 97953-22-5; 102782-43-4; 103331-86-8; 

103657-84-7; 103657-85-8; 103818-93-5; 103819-03-0; 106232-83-1; 111905-

54-5; 116810-31-2; 116810-32-3; 116810-33-4; 120313-48-6; 120944-68-5; 

121617-09-2; 126646-02-4; 126950-62-7; 127036-24-2; 139626-71-4; 152231-

44-2; 154518-36-2; 157627-86-6; 157627-88-8; 157707-41-0; 157707-43-2; 

159653-49-3; 160875-66-1; 160901-20-2; 160901-09-7; 160901-19-9; 161025-

21-4; 161025-22-5; 166736-08-9; 169107-21-5; 172588-43-1; 176022-76-7; 

196823-11-7; 287935-46-0; 288260-45-7; 303176-75-2; 954108-36-2

Alkyl (C12-C20) methacrylate-methacrylic acid copolymer, minimum 

molecular weight (in amu), 11,900

None

2H-Azepin-2-one, 1-ethenylhexahydro-, homopolymer 25189-83-7

1,3 Benzene dicarboxylic acid, 5-sulfo-, 1,3-dimethyl ester, sodium 

salt, polymer with 1,3-benzene dicarboxylic acid, 1,4-benzene 

dicarboxylic acid, dimethyl 1,4-benzene dicarboxylate and 

1,2-ethanediol, minimum number average molecular weight (in amu), 

2,580

212842-88-1

3,5-Bis(6-isocyanatohexyl)-2H-1,3,5-oxadiazine-2,4,6-(3H,5H)

-trione, polymer with diethylenetriamine, minimum number average 

molecular weight (in amu), 1,000,000

87823-33-4 

Polymer of one or more diglycidyl ethers of bisphenol A, resorcinol, 

glycerol, cyclohexanedimethanol, neopentyl glycol, and polyethylene 

glycol with one or more of the following: Polyoxypropylene diamine, 

polyoxypropylene triamine, N-aminoethyl-piperazine, 

trimethyl-1,6-hexanediamine isophorone diamine, 

N,N-dimethyl-1,3-diaminopropane, nadic methyl anhydride, 

1,2-cyclohexane-dicarboxylic anhydride and 

1,2,3,6-tetrahydrophthalic anhydride, minimum number average 

molecular weight (in amu), 400,000

None

Butadiene-styrene copolymer None

Butanedioic acid, 2-methylene-, homopolymer, sodium salt, 

minimum number average molecular weight (in amu), 3936

26099-89-8

Butanedioic acid, 2-methylene-, polymer with 2,5-furandione, sodium 

and ammonium salts, hydrogen peroxide-initiated, minimum number 

average molecular weight (in amu), 2,500-3,000

556055-76-6

701908-99-8

1,4-Butanediol-methylenebis(4-phenylisocyanate)-poly

(tetramethylene glycol) copolymer, minimum molecular weight (in 

amu) 158,000

9018-04-6 

Butene, homopolymer 9003-29-6

2-butenedioic acid (2Z)-, monobutyl ester, polymer with 

methoxyethene, sodium salt, minimum number average molecular 

weight (in amu), 18,200

205193-99-3

2-Butenedioic acid (Z)-, polymer with ethenol and ethenyl acetate, 

sodium salt, minimum number average molecular weight (in amu), 

75,000

139871-83-3 

Butyl acrylate-vinyl acetate-acrylic acid copolymer, minimum number 

average molecular weight (in amu), 18,000

65405-40-5

Carbonic acid, diethyl ester, polymer with α-hydro-ω-hydroxypoly

[oxy(methyl-1,2-ethanediyl)] ether with 2-ethyl-2-(hydroxymethyl)

-1,3-propanediol (3:1), ester with α-[[[[5-(carboxyamino)

-1,3,3-trimethylcyclohexyl]methyl]amino]carbonyl]-ω-methoxypoly

(oxy-1,2-ethanediyl), minimum number average molecular weight (in 

amu), 1,900

1147260-65-8

Castor oil, ethoxylated, dioleate, minimum number average 

molecular weight (in amu), 1260.

110531-96-9

Castor oil, ethoxylated, oleate, minimum number average molecular 

weight (in amu), 1,600

220037-02-5

Castor oil, polymer with adipic acid, linoleic acid, oleic acid and 

ricinoleic acid, minimum number average molecular weight (in amu), 

3,500

1357486-09-9

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Castor oil, polyoxyethylated; the poly(oxyethylene) content averages 

5-54 moles

None 

Cellulose carboxymethyl ether, potassium salt, minimum number 

average molecular weight 9587 Daltons

54848-04-3

Chlorinated polyethylene 64754-90-1 

Cross-linked nylon-type polymer formed by the reaction of a mixture 

of sebacoyl chloride and polymethylene polyphenylisocycanate with 

a mixture of ethylenediamine and diethylenetriamine

None 

Cross-linked polyurea-type encapsulating polymer None

Dimethylpolysiloxane minimum number average molecular weight (in 

amu), 6,800

63148-62-9

Dimethyl silicone polymer with silica, minimum number average 

molecular weight (in amu), 1,100,000

67762-90-7

α-(o,p-Dinonylphenyl)-ω-hydroxypoly(oxyethylene) produced by 

condensation of 1 mole of dinonylphenol (nonyl group is a propylene 

trimer isomer) with an average of 140-160 moles of ethylene oxide

9014-93-1

Docosyl methacrylate-acrylic acid copolymer, or docosyl 

methacrylate-octadecyl methacrylate-acrylic acid copolymer, 

minimum number average molecular weight (in amu), 3,000

None 

1,12-Dodecanediol dimethacrylate polymer, minimum molecular 

weight (in amu), 100,000

None

α-(p-Dodecylphenyl)-ω-hydroxypoly(oxyethylene) produced by the 

condensation of 1 mole of dodecylphenol (dodecyl group is a 

propylene tetramer isomer) with an average of 30-70 moles of 

ethylene oxide

9014-92-0

26401-47-8

1,2-Ethanediamine, N1-(2-aminoethyl)-, polymer with 

2,4-diisocyanato-1-methylbenzene, minimum number average 

molecular weight (in amu), one million

35297-61-1

1, 2-Ethanediamine, polymer with methyl oxirane and oxirane, 

minimum number average molecular weight (in amu), 1,100

26316-40-5

Ethylene glycol dimethyacrylate-lauryl methacrylate copolymer, 

minimum molecular weight (in amu), 100,000

None 

Ethylene glycol dimethacrylate polymer, minimum molecular weight 

(in amu), 100,000

None 

Fatty acids, tall-oil, ethoxylated propoxylated, minimum number 

average molecular weight (in amu), 2,009

67784-86-5

Formaldehyde, polymer with α-[bis(1-phenylethyl)phenyl]-ωhydroxypoly(oxy-1,2-ethanediyl), number average molecular weight 

(in amu), 1,803

157291-93-5

Formaldehyde, polymer with 2-methyloxirane and 4-nonylphenol, 

minimum number average molecular weight (in amu), 4,000

37523-33-4

Fumaric acid-isophthalic acid-styrene-ethylene/propylene glycol 

copolymer, minimum average molecular weight (in amu), 1 × 1018

None 

2,5-Furandione, polymer with ethenylbenzene, hydrolyzed, 

3-(dimethylamino)propyl imide, imide with polyethylenepolypropylene glycol 2-aminopropyl me ether, 2,2′-(1,2-diazenediyl)

bis[2-methylbutanenitrile]-initiated, minimum number average 

molecular weight (in amu), 5,816

1062609-13-5

2,5-Furandione, polymer with ethenylbenzene, reaction products 

with polyethylene-polypropylene glycol 2-aminopropyl Me ether; 

minimum number average molecular weight (in amu), 14,000

162568-32-3

2,5-Furandione, polymer with methoxyethene, butyl ethyl ester, 

sodium salt, minimum number average molecular weight (in amu), 

18,200

1471342-08-1

Hexadecyl acrylate-acrylic acid copolymer, hexadecyl acrylate-butyl 

acrylate-acrylic acid copolymer, or hexadecyl acrylate-dodecyl 

acrylate-acrylic acid copolymer, minimum number average molecular 

weight (in amu), 3,000

None

Hexamethyl disilizane, reaction product with silica, minimum number 

average molecular weight (in amu), 645,000

68909-20-6

1,6-Hexanediol dimethyacrylate polymer, minimum molecular weight 

(in amu), 100,000

None

α-Hydro-ω-hydroxy-poly(oxyethylene) C8 alkyl ether citrates, poly

(oxyethylene) content is 4-12 moles, minimum number average 

molecular weight (in amu) 1,300

330977-00-9

α-Hydro-ω-hydroxy-poly(oxyethylene) C10-C16-alkyl ether citrates, 

poly(oxyethylene) content is 4-12 moles, minimum number average 

molecular weight (in amu) 1,100

330985-58-5

α-Hydro-ω-hydroxy-poly(oxyethylene) C16-C18-alkyl ether citrates, 

poly(oxyethylene) content is 4-12 moles, minimum number average 

molecular weight (in amu) 1,300

330985-61-0

α-Hydro-ω-hydroxypoly(oxyethylene), minimum number average 

molecular weight (in amu), 17,000

25322-68-3

α-Hydro-ω-hydroxypoly(oxyethylene)poly (oxypropylene) poly

(oxyethylene) block copolymer; the minimum poly(oxypropylene) 

content is 27 moles and the minimum molecular weight (in amu) is 

1,900

None 

α-Hydro-ω-hydroxypoly(oxypropylene); minimum molecular weight 

(in amu) 2,000

None

12-Hydroxystearic acid-polyethylene glycol copolymer, minimum 

number average molecular weight (in amu), 3,690

70142-34-6

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Isodecyl alcohol ethoxylated (2-8 moles) polymer with chloromethyl 

oxirane, minimum number average molecular weight (in amu) 2,500

None

Lauryl methacrylate-1,6-hexanediol dimethacrylate copolymer, 

minimum molecular weight (in amu), 100,000

None

Maleic acid-butadiene copolymer None 

Maleic acid monobutyl ester-vinyl methyl ether copolymer, minimum 

average molecular weight (in amu), 52,000

25119-68-0 

Maleic acid monoethyl ester-vinyl methyl ether copolymer, minimum 

average molecular weight (in amu), 46,000

25087-06-3 

Maleic acid monoisopropyl ester-vinyl methyl ether copolymer, 

minimum average molecular weight (in amu), 49,000

31307-95-6 

Maleic anhydride-diisobutylene copolymer, sodium salt, minimum 

number average molecular weight (in amu) 5,0007-18,000

37199-81-8

Maleic anhydride-methylstyrene copolymer sodium salt, minimum 

number average molecular weight (in amu), 15,000

60092-15-1

Maleic anhydride-methyl vinyl ether, copolymer, average molecular 

weight (in amu), 250,000

None 

Methacrylic acid-methyl methacrylate-polyethylene glycol methyl 

ether methacrylate copolymer, minimum number averge molecular 

weight (in amu), 3,700

100934-04-1

Methacrylic acid-methyl methacrylate-polyethylene glycol 

monomethyl ether methacrylate graft copolymer, minimum number 

average molecular weight (in amu), 1,800

111740-36-4

Methacrylic copolymer, minimum number average molecular weight 

(in amu), 15,000

63150-03-8

Methyl methacrylate-methacrylic acid-monomethoxypolyethylene 

glycol methacrylate copolymer,) minimum number average 

molecular weight (in amu), 2,730

119724-54-8

Methyl methacrylate-2-sulfoethyl methacrylatedimethylaminoethylmethacrylate-glycidyl methacrylate-styrene-2-

ethylhexyl acrylate graft copolymer, minimum average molecular 

weight (in amu), 9,600

None

Methyl vinyl ether-maleic acid copolymer), minimum number average 

molecular weight (in amu), 75,000

25153-40-6 

Methyl vinyl ether-maleic acid copolymer, calcium sodium salt, 

minimum number average molecular weight (in amu), 900,000

62386-95-2 

Monophosphate ester of the block copolymer α-hydro-ω-hydroxypoly

(oxyethylene) poly(oxypropylene) poly(oxyethylene); the poly

(oxypropylene) content averages 37-41 moles, average molecular 

weight (in amu), 8,000

None 

α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) mixture of 

dihydrogen phosphate and monohydrogen phosphate esters and the 

corresponding ammonium, calcium, magnesium, 

monoethanolamine, potassium, sodium, and zinc salts of the 

phosphate esters; the nonyl group is a propylene trimer isomer and 

the poly(oxyethylene) content averages 30 moles

None

α-(p-Nonylphenyl)-ω-hydroxypoly(oxyethylene) sulfate, and its 

ammonium, calcium, magnesium, monoethanolamine, potassium, 

sodium, and zinc salts; the nonyl group is a propylene trimer isomer 

and the poly(oxyethylene) content averages 30-90 moles of ethylene 

oxide

None

α-(p-Nonylphenyl-ω-hydroxypoly(oxypropylene) block polymer with 

poly(oxyethylene); polyoxypropylene content of 10-60 moles; 

polyoxyethylene content of 10-80 moles; molecular weight (in amu), 

1,200-7,100.

None 

α-(ρ-Nonylphenyl)poly(oxypropylene) block polymer with poly

(oxyethylene); poly oxyethylene content 30 to 90 moles; minimum 

number average molecular weight (in amu), 1,889

37251-69-7

Octadecanoic Acid, 12-Hydroxy-, Homopolymer Ester with 

2-Methylloxirane Polymer with Oxirane monobutyl Ether, minimum 

number average molecular weight (in amu), 4,500

1373125-59-7

Octadecanoic acid, 12-hydroxy-, homopolymer, octadecanoate 

minimum number average molecular weight (in amu), 1,370

58128-22-6) 

α-cis-9-Octadecenyl-ω-hydroxypoly(oxyethylene); the octadecenyl 

group is derived from oleyl alcohol and the poly(oxyethylene) content 

averages 20 moles

None

Octadecyl acrylate-acrylic acid copolymer, octadecyl acrylatedodecyl acrylate-acrylic acid copolymer, octadecyl methacrylatebutyl acrylate-acrylic acid copolymer, octadecyl methacrylate-hexyl 

acrylate-acrylic acid copolymer, octadecyl methacrylate-dodecyl 

acrylate-acrylic acid copolymer, or octadecyl methacrylate-dodecyl 

methacrylate-acrylic acid copolymer, minimum number average 

molecular weight (in amu) 3,000

None 

Oleic acid diester of α-hydro-ω-hydroxypoly(oxyethylene); the poly

(oxyethylene), average molecular weight (in amu), 2,300

None

2-oxepanone, homopolymer, minimum number average molecular 

weight (in amu) 52,000

24980-41-4

Oxirane, decyl-, reaction products with polyethylene-polypropylene 

glycol ether with trimethylolpropane (3:1)

903890-89-1

Oxirane, hexadecyl-, reaction products with polyethylenepolypropylene glycol ether with trimethylolpropane (3:1)893427-80-0

61419-46-3

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Oxirane, 2-methyl-, polymer with oxirane, dimethyl ether, minimum 

number average molecular weight (in amu), 2,800

Oxirane, methyl-, polymer with oxirane, ether with 2-ethyl2-(hydroxymethyl)-1,3-propanediol (3:1), reaction products with 

tetradecyloxirane

903890-90-4

Oxirane, methyl-, polymer with oxirane, mono[2-(2-butoxyethoxy) 

ethyl] ether, minimum number average molecular weight (in amu), 

2,500

85637-75-8

Oxirane, methyl-, polymer with Oxirane, Monobutyl Ether 9038-95-3

Oxirane, 2-methyl-, polymer with oxirane, minimum number average 

molecular weight (in amu), 1,100

9003-11-6

Oxirane, 2-methyl-, polymer with oxirane, mono 

[2-[2-(2-butoxymethylethoxy)methylethoxy]methylethyl] ether, 

minimum number average molecular weight (in amu), 3,000

926031-36-9

Oxirane, phenyl, polymer with oxirane, monooctyl ether, minimum 

average molecular weight (in amu) 1,200

83653-00-3

Polyamide polymer derived from sebacic acid, vegetable oil acids 

with or without dimerization, terephthalic acid and/or 

ethylenediamine

None

Polyethylene glycol-polyisobutenyl anhydride-tall oil fatty acid 

copolymer, minimum number average molecular weight (in amu), 

2,960

68650-28-2

Polyethylene, oxidized, minimum number average molecular weight 

(in amu), 1,200

None

Polymers produced by the reaction of either 1,6-hexanediisocyanate; 

2,4,4-trimethyl-1,6-hexanediisocyanate; 5-isocyanato1-(isocyanatomethyl)-fxsp0;1,3,3fxsp0;-trimethyIcyclohexane 

(isophoronediisocyanate); 4,4′-methylene-bis-1,1′

-cyclohexanediisocyanate; 4,4′-methylene-bis-1,1′

benzyldiisocyanate; or 1,3-bis-(2-isocyanatopropan-2-yl)benzene 

with polyethylene glycol and end-capped with one or a mixture of 

more than one of octanol, decanol, dodecanol, tetradecanol, 

hexadecanol, octadecanol, and octadec-9-enol or polyethyleneglycol 

ethers of octanol, decanol, dodecanol, tetradecanol, hexadecanol, 

octadecanol, and octadec-9-enol, minimum number average 

molecular weight (in amu), 20,000

1161844-26-3, 1161844-30-9, 1161844-43-4, 1161844-51-4, 1161844-53-6, 

693252-31-2, 162993-60-4, 630102-86-2

Polymethylene polyphenylisocyanate, polymer with ethylene 

diamine, diethylene triamine and sebacoyl chloride, cross-linked; 

minimum number average molecular weight (in amu), 100,000

None

Polyoxyalkylated glycerol fatty acid esters; the mono-, di-, or 

triglyceride mixtures of C8 through C22, primarily C8 through C18

saturated and unsaturated, fatty acids containing up to 15% water by 

weight reacted with a minimum of three moles of either ethylene 

oxide or propylene oxide; the resulting polyoxyalkylated glycerol 

ester polymer minimum number average molecular weight (in amu), 

1,500

61791-23-9, 68201-46-7, 68440-49-3, 68458-88-8, 68606-12-2, 68648-38-4, 

70377-91-2, 70914-02-2, 72245-12-6, 72698-41-3, 180254-52-8, 248273-72-5, 

308063-50-5, 952722-33-7

Polyoxyalkylated sorbitan fatty acid esters with C6 through C22 

aliphatic alkanoic and/or alkenoic fatty acids, branched or linear, the 

resulting polyoxyalkylene sorbitan esters minimum number average 

molecular weight (in amu), 1,300

81776-11-6, 87090-31-1, 88895-72-1, 103171-31-9, 161026-53-5, 1472644-

80-6, 1472644-81-7, 1472644-84-0, 1472644-85-1, 1472644-87-3, 1472644-

88-4, 1472654-83-3, 1472655-32-5, 1472661-05-4, 1472661-17-8, 1472663-

59-4, 1472663-64-1, 1472663-66-3, 1472663-92-5, 1472668-03-3

Polyoxyalkylated trimethylopropanes with 20 to 80 moles of ethylene 

and/or propylene oxide, fatty acid esters with C8 through C22 

aliphatic alkanoic and/or alkenoic fatty acids, branched or linear; 

minimum number average molecular weight (in amu), 3,000

25765-36-0; 29860-47-7; 37339-03-0; 52624-57-4; 58090-24-7; 63964-38-5; 

72939-62-9; 74521-14-5; 75300-70-8; 75300-90-2; 84271-03-4; 84271-04-5; 

86850-92-2; 107120-02-5; 133331-01-8; 137587-60-1; 149797-40-0; 149797-

41-1; 150695-97-9; 152130-24-0; 163349-94-8; 163349-95-9; 163349-96-0; 

163349-97-1; 163349-98-2; 165467-70-9; 183619-46-7; 183619-50-3; 185260-

01-9; 202606-04-0; 210420-84-1; 233660-70-3; 263011-96-7; 283602-94-8; 

701980-40-7; 872038-58-9; 875709-44-7; 875709-45-8; 875709-46-9; 875709-

47-0; 879898-63-2; 910038-01-6; 1190748-04-9; 1225384-02-0; 1428944-41-5; 

1446498-15-2.

Poly(oxy-1,2-ethanediyl), α-hydro-ω-hydroxy-, polymer with 1, 1′

-methylene-bis-[4-isocyanatocyclohexane], minimum number 

average molecular weight (in amu), 1800

39444-87-6

Polyoxyethylated primary amine (C14-C18); the fatty amine is derived 

from an animal source and contains 3% water; the poly(oxyethylene) 

content averages 20 moles

None

Polyoxyethylated sorbitol fatty acid esters; the polyoxyethylated 

sorbitol solution containing 15% water is reacted with fatty acids 

limited to C12, C14, C16, and C18, containing minor amounts of 

associated fatty acids; the poly(oxyethylene) content averages 30 

moles.

None

Polyoxyethylated sorbitol fatty acid esters; the sorbitol solution 

containing up to 15% water is reacted with 20-50 moles of ethylene 

oxide and aliphatic alkanoic and/or alkenoic fatty acids C8 through 

C22 with minor amounts of associated fatty acids; the resulting 

polyoxyethylene sorbitol ester having a minimum molecular weight 

(in amu), 1,300

None

Poly(oxyethylene/oxypropylene) monoalkyl (C6-C10) ether sodium 

fumarate adduct, minimum number average molecular weight (in 

amu), 1,900

102900-02-7 

Poly[oxy(methyl-1,2-ethanediyl)], α-[(9Z)-1-oxo-9-octadecen-1-yl]-ω-

[[(9Z)-1-oxo-9-octadecen-1yl]oxy]-, minimum number average 

molecular weight (in amu) 2,300

26571-49-3

Polyoxymethylene copolymer, minimum number average molecular 

weight (in amu), 15,000

None 

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Poly(oxypropylene) block polymer with poly(oxyethylene), molecular 

weight (in amu), 1,800-16,000

None

Poly(phenylhexylurea), cross-linked, minimum average molecular 

weight (in amu), 36,000

None 

Polypropylene 9003-07-0 

Polystyrene, minimum number average molecular weight (in amu), 

50,000

9003-53-6 

Polytetrafluoroethylene 9002-84-0 

Polyvinyl acetate, copolymer with maleic anhydride, partially 

hydrolyzed, sodium salt, minimum number average molecular weight 

(in amu), 53,000

None

Polyvinylpyrrolidone butylated polymer, minimum number average 

molecular weight (in amu), 9,500

26160-96-3

Polyvinyl acetate, minimum molecular weight (in amu), 2,000 None 

Polyvinyl acetate—polyvinyl alcohol copolymer, minimum number 

average molecular weight (in amu), 50,000

25213-24-5 

Polyvinyl alcohol 9002-89-5 

Polyvinyl chloride None 

Polyvinyl chloride, minimum number average molecular weight (in 

amu), 29,000

9002-86-2

Poly(vinylpyrrolidone), minimum number average molecular weight 

(in amu), 4,000

9003-39-8 

Poly(vinylpyrrolidone-1-eicosene), minimum average molecular 

weight (in amu), 3,000

28211-18-9 

Poly(vinylpyrrolidone-1-hexadecene), minimum average molecular 

weight (in amu), 4,700

63231-81-2 

1-propanesulfonic acid, 2-methyl-2-[(1-oxo-2-propenyl)amino]-, 

monosodium salt, polymer with ethenol and ethenyl acetate, 

minimum number average molecular weight (in amu) 50,000

107568-12-7

2-Propene-1-sulfonic acid sodium salt, polymer with ethenol and 

ethenyl acetate, number average molecular weight (in amu) 6,000-

12,000

None

2-Propenoic acid, butyl ester, polymer with 1,6-diisocyanatohexane, 

N-(hydroxymethyl)-2-methyl-2-propenamide and 2-propenenitrile, 

minimum number average molecular weight (in amu), 100,000

1469998-09-1

2-propenoic acid, butyl ester, polymer with ethenylbenzene, methyl 

2-methyl-2-propenoate and 2-propenoic acid (in amu), 1900.

27306-39-4

2-Propenoic acid, butyl ester, polymer with ethyl 2-propenoate and 

N-(hydroxymethyl)-2-propenamide, minimum number average 

molecular weight (in amu), 30,000

33438-19-6

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene 

14,000 daltons

25153-46-2

2-Propenoic acid, 2-ethylhexyl ester, polymer with ethenylbenzene 

and 2-methylpropyl 2-methyl-2-propenoate, minimum number 

average molecular weight (in amu), 18,000

68240-06-2

2-Propenoic acid, 2-hydroxyethyl ester, polymer with 

α-[4-(ethenyloxy)butyl]-ω-hydroxypoly (oxy-1,2-ethanediyl), minimum 

number average molecular weight (in amu), 17,000

1007234-89-0

[2-propenoic acid, 2-methyl-, C12-16-alkyl esters, telomers with 

1-dodecanethiol, polyethylene-polypropylene glycol ether with 

propylene glycol monomethacrylate (1:1), and styrene 

2,2'-(1,2-diazenediyl)bis[2-methylbutanenitrile]-initiated, minimum 

number average molecular weight (in amu), 4,000

950207-35-9

2-Propenoic acid, methyl ester, polymer with ethenyl acetate, 

hydrolyzed, sodium salts

886993-11-9

2-Propenoic acid, 2-methyl-, 2-ethylhexyl ester, telomer with 

1-dodecanethiol, ethenylbenzene and 2-methyloxirane polymer with 

oxirane monoether with 1,2-propanediol mono(2-methyl-2-

propenoate), hydrogen 2-sulfobutanedioate, sodium salt, 2, 2′

-(1,2-diazenediyl)bis[2-methylpropanenitrile]-initiated, minimum 

number average molecular weight (in amu), 1,200

1283712-50-4

>2-Propenoic acid, 2-methyl-, 2-methylpropyl ester, homopolymer, 

minimum number average molecular weight (in amu), 55,000

9011-15-8

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 

2-propenoic acid, peroxydisulfuric acid ([(HO)S(O)2]2O2) sodium 

salt (1:2)-initiated, compounds with diethanolamine, minimum 

number average molecular weight (in amu), 2,000

1574486-33-1

2-Propenoic acid, 2-methyl-, phenylmethyl ester, polymer with 

2-propenoic acid and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl)

amino]-1-propanesulfonate (1:1), peroxydisulfuric acid ([HO)S(O)2]

202) sodium salt (1:2)-initiated minimum number average molecular 

weight >1,000 Daltons; maximum number average molecular weight 

10,000 Daltons

CASRN 1246766-57-3

2-Propenoic acid, 2-methyl-, polymer with butyl 2-propenoate and 

ethenylbenzene, minimum number average molecular weight (in 

amu), 17,000

25036-16-2

2-Propenoic acid, 2-Methyl-, Polymer with Butyl 2-Propenoate, 

Methyl 2-Methyl-2-Propenoate, Methyl 2-Propenoate and 

2-Propenoic Acid, graft, Compound with 2-Amino-2-Methyl-1-

Propanol

153163-36-1

146753-99-3

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2-Propenoic Acid, 2-Methyl-, Polymer with Ethenylbenzene, 

2-Ethylhexyl 2-Propenoate, 2-Hydroxyethyl 2-Propenoate, 

N-(Hydroxymethyl) -2-Methyl-2-Propenamide and Methyl 2-Methyl-2-

Propenoate, Ammonium Salt

2-Propenoic acid, 2-methyl-, polymers with Bu acrylate, Et acrylate, 

Me methacrylate and polyethylene glycol methacrylate C16-18-alkyl 

ethers, minimum number average molecular weight (in amu), 13,000

890051-63-5

2-Propenoic acid, 2-methyl-, telomer with 2-ethylhexyl 2-propenoate, 

2-propanol and sodium 2-methyl-2-[(1-oxo-2-propen-1-yl) amino]-1-

propanesulfonate (1:1), sodium salt, minimum number average 

molecular weight (in amu): 2,900

1260001-65-7

2-Propenoic acid, monoester with 1,2-propanediol, polymer with 

α-[4-(ethenyloxy) butyl]-ω-hydroxypoly (oxy-1,2-ethanediyl) and 

2,5-furandione, minimum number average molecular weight (in 

amu), 25,000

955015-23-3

2-propenoic acid polymer, with 1,3-butadiene and ethenylbenzene, 

minimum number average molecular weight (in amu), 9400

25085-39-6

2-Propenoic acid, polymer with ethenyl acetate, ethenylbenzene, 

2-ethylhexyl 2-propenoate and ethyl 2-propenoate, minimum number 

average molecular weight (50,149 Daltons)

85075-52-1

2-Propenoic acid, polymer with ethenylbenzene and 

(1-methylethenyl)benzene, minimum number average molecular 

weight (in amu), 2,000

52831-

04-6

2-Propenoic acid, polymer with ethenylbenzene and 

(1-methylethenyl) benzene, sodium salt, minimum number average 

molecular weight (in amu), 2,800

129811-24-1

2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1,2-ethanediyl) and 2,5-furandione, sodium salt, 

minimum number average molecular weight (in amu), 25,000

251479-97-7

2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1,2-ethanediyl) and 1,2-propanediol mono-2-

propenoate, potassium sodium salt, minimum number average 

molecular weight (in amu), 16,000

518026-64-7

2-Propenoic acid, polymer with α-[4-(ethenyloxy) butyl]-ωhydroxypoly (oxy-1, 2-ethanediyl), sodium salt, minimum number 

average molecular weight (in amu), 24,000

250591-84-5

2-Propenoic acid, polymer with 2-propenamide, sodium salt, 

minimum number average molecular weight (in amu), 18,000

25085-02-3

2-Propenoic acid, sodium salt, polymer with 2-propenamide, 

minimum number average molecular weight (in amu), 18,000

25987-30-8

2-Propenoic, 2-methyl-, polymers with ethyl acrylate and 

polyethylene glycol methylacrylate C18-22 alkyl ethers

888969-14-0

2-Pyrrolidone, 1-ethenyl-, polymer with ethenol, minimum number 

average molecular weight (in amu), 23,000

26008-54-8

Silane, dichloromethyl- reaction product with silica minimum number 

average molecular weight (in amu), 3,340,000

68611-44-9

Silane, trimethoxy[3-(oxiranylmethoxy)propyl]-, hydrolysis products 

with silica, minimum number average molecular weight (in amu), 

640,000

68584-82-7

Silicic acid, sodium salt, reaction products with chlorotrimethylsilane 

and iso-propyl alcohol, reaction with poly(oxypropylene)-poly

(oxyethylene) glycol, minimum number average molecular weight (in 

amu), 75,000

None

Sodium polyflavinoidsulfonate, consisting chiefly of the copolymer of 

catechin and leucocyanidin

None 

Soybean oil, ethoxylated; the poly(oxyethylene) content averages 10 

moles or greater

61791-23-9

Starch, oxidized, polymers with Bu acrylate, tert-Bu acrylate and 

styrene, minimum number average molecular weight (in amu), 

10,000

204142-80-3

Stearyl methacrylate-1,6-hexanediol dimethacrylate copolymer, 

minimum molecular weight (in amu), 100,000

None 

Styrene, copolymers with acrylic acid and/or methacrylic acid, with 

none and/or one or more of the following monomers: 

Acrylamidopropyl methyl sulfonic acid, methallyl sulfonic acid, 

3-sulfopropyl acrylate, 3-sulfopropyl methacrylate, hydroxypropyl 

methacrylate, hydroxypropyl acrylate, hydroxyethyl methacrylate, 

hydroxyethyl acrylate, and/or lauryl methacrylate; and its sodium, 

potassium, ammonium, monoethanolamine, and triethanolamine 

salts; the resulting polymer having a minimum number average 

molecular weight (in amu), 1200

None

Styrene-ethylene-propylene block copolymer, minimum number 

average molecular weight (in amu), 125,000

108388-87-0

Styrene, 2-ethylhexyl acrylate, butyl acrylate copolymer, minimum 

number average molecular weight (in amu), 4,200

30795-23-4

Styrene-2-ethylhexyl acrylate-glycidyl methacrylate-2-acrylamido-2-

methylpropanesulfonic acid graft copolymer, minimum number 

average molecular weight (in amu), 12,500

None

Styrene-maleic anhydride copolymer None 

Styrene-maleic anhydride copolymer, ester derivative None 

1398573-80-2

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Tall oil, polymer with polyethylene glycol and succinic anhydride 

monopolyisobutylene derivs., minimum number average molecular 

weight (in amu), 1,200

Tamarind seed gum, 2-hydroxypropyl ether polymer, minimum 

number average molecular weight (in amu), 10,000

68551-04-2

Tetradecyl acrylate-acrylic acid copolymer, minimum number 

average molecular weight (in amu), 3,000

None

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum 

number average molecular weight (in amu), 2,500

104133-09-7

Tetraethoxysilane, polymer with hexamethyldisiloxane, minimum 

number average molecular weight (in amu), 6,500

104133-09-7

α-[p-(1,1,3,3-Tetramethylbutyl)phenyl]-ω-hydroxypoly(oxyethylene) 

produced by the condensation of 1 mole of 

p-(1,1,3,3-tetramethylbutyl)phenol with a range of 30-70 moles of 

ethylene oxide

9036-19-5

9002-93-1

α-[p-(1,1,3,3-Tetramethylbutyl)phenyl] poly(oxypropylene) block 

polymer with poly(oxyethylene); the poly(oxypropylene) content 

averages 25 moles, the poly(oxyethylene) content averages 40 

moles, the molecular weight (in amu) averages 3,400

None 

α-[2,4,6-Tris[1-(phenyl)ethyl]phenyl]-ω-hydroxy poly(oxyethylene) 

poly(oxypropylene) copolymer, the poly(oxypropylene) content 

averages 2-8 moles, the poly(oxyethylene) content averages 16-

30moles, average molecular weight (in amu), 1,500

None 

Urea-formaldehyde copolymer, minimum average molecular weight 

(in amu), 30,000

9011-05-6 

Vinyl acetate-allyl acetate-monomethyl maleate copolymer, minimum 

average molecular weight (in amu), 20,000

None

Vinyl acetate-ethylene copolymer, minimum number average 

molecular weight (in amu), 69,000

24937-78-8 

Vinyl acetate polymer with none and/or one or more of the following 

monomers: Ethylene, propylene, N-methyl acrylamide, acrylamide, 

monoethyl maleate, diethyl maleate, monooctyl maleate, dioctyl 

maleate, maleic anhydride, maleic acid, octyl acrylate, butyl acrylate, 

ethyl acrylate, methyl acrylate, acrylic acid, octyl methacrylate, butyl 

methacrylate, ethyl methacrylate, methyl methacrylate, methacrylic 

acid, carboxyethyl acrylate, and diallyl phthalate; and their 

corresponding sodium, potassium, ammonium, isopropylamine, 

triethylamine, monoethanolamine and/or triethanolamine salts; the 

resulting polymer having a minimum number average molecular 

weight (in amu), 1,200

None

Vinyl acetate-vinyl alcohol-alkyl lactone copolymer, minimum number 

average molecular weight (in amu), 40,000; minimum viscosity of 18 

centipoise

None

Vinyl alcohol-disodium itaconate copolymer, minimum average 

molecular weight (in amu), 50,290

None 

Vinyl alcohol-vinyl acetate copolymer, benzaldehyde-o-sodium 

sulfonate condensate, minimum number average molecular weight 

(in amu), 20,000

None

Vinyl alcohol-vinyl acetate-monomethyl maleate, sodium salt-maleic 

acid, disodium salt-γ-butyrolactone acetic acid, sodium salt 

copolymer, minimum number average molecular weight (in amu), 

20,000

None 

Vinyl chloride-vinyl acetate copolymers None 

Vinyl pyrrolidone-acrylic acid copolymer, minimum number average 

molecular weight (in amu), 6,000

28062-44-4

Vinyl pyrrolidone-dimethylaminoethylmethacrylate copolymer, 

minimum number average molecular weight (in amu), 20,000

30581-59-0 

Vinyl pyrrolidone-styrene copolymer 25086-29-7

[67 FR 36528, May 24, 2002]

EDITORIAL NOTE: For FEDERAL REGISTER citations affecting §180.960, see the List of CFR Sections Affected, which appears in 

the Finding Aids section of the printed volume and at www.fdsys.gov.

 Back to Top

§180.1011 Viable spores of the microorganism Bacillus thuringiensis Berliner; exemption from the requirement 

of a tolerance.

(a) For the purposes of this section the microbial insecticide for which exemption from the requirement of a tolerance 

is being established shall have the following specifications:

(1) The microorganism shall be an authentic strain of Bacillus thuringiensis Berliner conforming to the morphological 

and biochemical characteristics of Bacillus thuringiensis as described in Bergey's Manual of Determinative Bacteriology, 

Eighth Edition.

(2) Spore preparations of Bacillus thuringiensis Berliner shall be produced by pure culture fermentation procedures 

with adequate control measures during production to detect any changes from the characteristics of the parent strain or 

contamination by other microorganisms.

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(3) Each lot of spore preparation, prior to the addition of other materials, shall be tested by subcutaneous injection of 

at least 1 million spores into each of five laboratory test mice weighing 17 grams to 23 grams. Such test shall show no 

evidence of infection or injury in the test animals when observed for 7 days following injection.

(4) Spore preparations shall be free of the Bacillus thuringiensis β-exotoxin when tested with the fly larvae toxicity test 

(“Microbial Control of Insects and Mites,” R.P.M. Bond et al., p. 280 ff., 1971). This specification can be satisfied either by

determining that each master seed lot brought into production is a Bacillus thuringiensis strain which does not produce 

β-exotoxin under standard manufacturing conditions or by periodically determining that β-exotoxin synthesized during 

spore production is eliminated by the subsequent spore-harvesting procedure.

(b) Exemption from the requirement of a tolerance is established for residues of the microbial insecticide Bacillus 

thuringiensis Berliner, as specified in paragraph (a) of this section, in or on honey and honeycomb and all other raw 

agricultural commodities when it is applied either to growing crops, or when it is applied after harvest in accordance with 

good agricultural practices.

[36 FR 22540, Nov. 25, 1971, as amended at 38 FR 19045, July 17, 1973; 42 FR 28540, June 3, 1977; 45 FR 43721, June 30, 

1980; 45 FR 56347, Aug. 25, 1980; 74 FR 26533, June 3, 2009]

 Back to Top

§180.1016 Ethylene; exemption from the requirement of a tolerance.

Ethylene is exempted from the requirement of a tolerance for residues when:

(a) For all food commodities, it is used as a plant regulator on plants, seeds, or cuttings and on all food commodities 

after harvest and when applied in accordance with good agricultural practices.

(b) Injected into the soil to cause premature germination of witchweed in bean (lima and string), cabbage, cantaloupe, 

collard, corn, cotton, cucumber, eggplant, okra, onion, pasture grass, pea (field and sweet), peanut, pepper, potato, sweet 

potato, sorghum, soybean, squash, tomato, turnip, and watermelon fields as part of the U.S. Department of Agriculture 

witchweed control program.

[39 FR 33315, Sept. 17, 1974, as amended at 40 FR 19477, May 5, 1975; 64 FR 31505, June 11, 1999]

 Back to Top

§180.1017 Diatomaceous earth; exemption from the requirement of a tolerance.

(a) Diatomaceous earth is exempted from the requirement of a tolerance for residues when used in accordance with 

good agricultural practice in pesticide formulations applied to growing crops, to food commodities after harvest, and to 

animals. 

(b) Diatomaceous earth may be safely used in accordance with the following conditions. Application shall be limited 

solely to spot and/or crack and crevice treatments in food or feed processing and food or feed storage areas in accordane 

with the precribed conditions: 

(1) It is used or intended for use for control of insects in food or feed processing and food or feed storage areas: 

Provided, That the food or feed is removed or covered prior to such use. 

(2) To assure safe use of the insecticide, its label and labeling shall conform to that registered by the U.S. 

Environmental Protection Agency, and it shall be used in accordance with such label and labeling. 

[65 FR 33716, May 24, 2000]

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§180.1019 Sulfuric acid; exemption from the requirement of a tolerance.

(a) Residues of sulfuric acid are exempted from the requirement of a tolerance when used in accordance with good 

agricultural practice when used as a herbicide in the production of garlic and onions, and as a potato vine dessicant in the 

production of potatoes.

(b) Residues of sulfuric acid are exempted from the requirement of a tolerance in cattle, meat; goat, meat; hog, meat; 

horse, meat; sheep, meat; poultry, fat; poultry, meat; poultry, meat, byproducts; egg; milk; fish, shellfish, and irrigated 

crops when it results from the use of sulfuric acid as an inert ingredient in a pesticide product used in irrigation 

conveyance systems and lakes, ponds, reservoirs, or bodies of water in which fish or shellfish are cultivated. The sulfuric 

acid is not to exceed 10% of the pesticide formulation (non-aerosol formulations only).

[69 FR 40787, July 7, 2004, as amended at 74 FR 26533, June 3, 2009]

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§180.1020 Sodium chlorate; exemption from the requirement of a tolerance.

Sodium chlorate is exempted from the requirement of a tolerance for residues when used as a defoliant or desiccant 

in accordance with good agricultural practice on the following crops:

Bean, dry, seed

Corn, field, forage 

Corn, field, grain 

Corn, field, stover 

Corn, pop, grain 

Corn, pop, stover 

Corn, sweet, forage 

Corn, sweet, stover 

Cotton, undelinted seed 

Flax, seed 

Grain, aspirated fractions 

Guar, seed 

Pea, southern 

Pepper, nonbell 

Potato

Rice, grain 

Rice, straw 

Safflower, seed 

Sorghum, forage, forage 

Sorghum, grain, forage 

Sorghum, grain, grain 

Sorghum, grain, stover 

Soybean, forage 

Soybean, hay 

Soybean, seed 

Sunflower, seed 

Wheat, grain

[74 FR 47457, Sept. 16, 2009]

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§180.1021 Copper; exemption from the requirement of a tolerance.

(a) Copper is exempted from the requirement of a tolerance in cattle, meat; goat, meat; hog, meat; horse, meat; 

sheep, meat; milk, poultry, fat; poultry, meat; poultry, meat byproducts; egg, fish, shellfish, and irrigated crops when it 

results from the use of:

(1) Copper sulfate as an algicide or herbicide in irrigation conveyance systems and lakes, ponds, reservoirs, or bodies 

of water in which fish or shellfish are cultivated. 

(2) Basic copper carbonate (malachite) as an algicide or herbicide in impounded and stagnant bodies of water 

(3) Copper triethanolamine and copper monoethanolamine as an algicide or herbicide in fish hatcheries, lakes, ponds, 

and reservoirs 

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(4) Cuprous oxide bearing antifouling coatings for control of algae or other coatings for control of algae or other 

organisms on submerged concrete or other (irrigation) structures. 

(5) Copper oxide embedded in polymer emitter heads used in irrigation systems for root incursion prevention.

(b) The following copper compounds are exempt from the requirement of a tolerance when applied (primarily) as a 

fungicide to growing crops using good agricultural practices:

Copper compounds CAS Reg. No.

Basic copper carbonate (malachite) 1184-64-1

Copper ammonia complex 16828-95-8

Copper ethylenediamine complex 13426-91-0

Copper hydroxide 20427-59-2

Copper octanoate 20543-04-8

Copper oxychloride 1332-65-6

Copper oxychloride sulfate 8012-69-9

Copper salts of fatty and rosin acids 9007-39-0

Copper sulfate basic 1344-73-6

Copper sulfate pentahydrate 7758-99-8

Cuprous oxide 1317-19-1

(c) Copper sulfate pentahydrate (CAS Reg. No. 7758-99-8) is exempt from the requirement of a tolerance when 

applied as a fungicide to growing crops or to raw agricultural commodities after harvest, and as a bactericide/fungicide in 

or on meat, fat and meat by-products of cattle, sheep, hogs, goats, horses and poultry, milk and eggs when applied as a 

bactericide/fungicide to animal premises and bedding.

(d) Copper (II) hydroxide (CAS Reg. No. 20427-59-2) is exempt from the requirement of a tolerance when applied to 

growing crops or to raw agricultural commodities as an inert ingredient (for pH control) in pesticide products.

[65 FR 68912, Nov. 15, 2000, as amended at 69 FR 4069, Jan. 28, 2004; 71 FR 46110, Aug. 11, 2006; 74 FR 26534, June 3, 2009; 

74 FR 47457, Sept. 16, 2009; 80 FR 37551, July 1, 2015]

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§180.1022 Iodine-detergent complex; exemption from the requirement of a tolerance.

The aqueous solution of hydriodic acid and elemental iodine, including one or both of the surfactants (a) 

polyoxypropylene-polyoxyethylene glycol nomionic block polymers (minimum average molecular weight 1,900) and (b) 

α-(p- nonylphenyl)-omega- hydroxypoly (oxyethylene) having a maximum average molecular weight of 748 and in which 

the nonyl group is a propylene trimer isomer, is exempted from the requirement of a tolerance for residues in egg, and 

poultry, fat; poultry, meat; poultry, meat byproducts when used as a sanitizer in poultry drinking water.

[74 FR 26534, June 3, 2009]

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§180.1023 Propanoic acid; exemptions from the requirement of a tolerance.

(a) Postharvest application of propanoic acid or a mixture of methylene bispropionate and oxy(bismethylene) 

bisproprionate when used as a fungicide is exempted from the requirement of a tolerance for residues in or on the 

following raw agricultural commodities: Alfalfa, forage; alfalfa, hay; alfalfa, seed; barley, grain; Bermudagrass, forage; 

Bermudagrass, hay; bluegrass, forage; bluegrass, hay; bromegrass, forage; bromegrass, hay; clover, forage; clover, hay; 

corn, field, grain; corn, pop, grain; cowpea, hay; fescue, forage; fescue, hay; lespedeza, forage; lespedeza, hay; lupin; oat, 

grain; orchardgrass, forage; orchardgrass, hay; peanut, hay; pea, field, hay; ryegrass, Italian, hay; sorghum, grain, grain; 

soybean, hay; sudangrass, forage; sudangrass, hay; timothy, forage; timothy, hay; vetch, forage; vetch, hay; and wheat, 

grain.

(b) Propanoic acid is exempt from the requirement of a tolerance for residues in or on cattle, meat; cattle, meat 

byproducts; goat, meat; goat, meat byproducts; hog, meat; hog meat byproducts; horse, meat; horse, meat byproducts; 

sheep, meat; sheep meat byproducts; and, poultry, fat; poultry meat; poultry meat byproducts; milk, and egg when applied 

as a bactericide/fungicide to livestock drinking water, poultry litter, and storage areas for silage and grain.

(c) Preharvest and postharvest application of propanoic acid (CAS Reg. No. 79-09-4), propanioc acid, calcium salt 

(CAS Reg. No. 4075-81-4), and propanioc sodium salt (CAS Reg. No. 137-40-6) are exempted from the requirement of a 

tolerance on all crops when used as either an active or inert ingredient in accordance with good agricultural practice in 

pesticide formulations applied to growing crops, to raw agricultural commodities before and after harvest and to animals.

[69 FR 47025, Aug. 4, 2004, as amended at 74 FR 26534, June 3, 2009]

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§180.1025 Xylene; exemption from the requirement of a tolerance.

Xylene is exempted from the requirement of a tolerance when used as an aquatic herbicide applied to irrigation 

conveyance systems in accordance with the following conditions:

(a) It is to be used only in programs of the Bureau of Reclamation, U.S. Department of Interior, and cooperating water 

user organizations.

(b) It is to be applied as an emulsion at an initial concentration not to exceed 750 parts per million.

(c) It is not to be applied when there is any likelihood that the irrigation water will be used as a source of raw water for 

a potable water system or where return flows of such treated irrigation water into receiving rivers and streams would 

contain residues of xylene in excess of 10 parts per million.

(d) Xylene to be used as an aquatic herbicide shall meet the requirement limiting the presence of a polynuclear 

aromatic hydrocarbons as listed in 21 CFR 172.250.

[38 FR 16352, June 22, 1973, as amended at 50 FR 2980, Jan. 3, 1985]

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§180.1027 Nuclear polyhedrosis virus of Heliothis zea; exemption from the requirement of a tolerance.

(a) For the purposes of this section, the viral insecticide must be produced with an unaltered and unadulterated 

inoculum of the single-embedded Heliothis zea nuclear polyhedrosis virus (HzSNPV). The identity of the seed virus must 

be assured by periodic checks.

(b) Each lot of active ingredient of the viral insecticide shall have the following specifications:

(1) The level of extraneous bacterial contamination of the final unformulated viral insecticide should not exceed 107

colonies per gram as determined by an aerobic plate on trypticase soy agar.

(2) Human pathogens, e.g., Salmonella, Shigella, or Vibrio, must be absent.

(3) Safety to mice as determined by an intraperitoneal injection study must be demonstrated.

(4) Identity of the viral product, as determined by the most sensitive and standardized analytical technique, e.g., 

restriction endonuclease and/or SDS-PAGE analysis, must be demonstrated.

(c) Exemptions from the requirement of a tolerance are established for the residues of the microbial insecticide 

Heliothis zea NPV, as specified in paragraphs (a) and (b) of this section, in or on all agricultural commodities.

[60 FR 42460, Aug. 16, 1995, as amended at 74 FR 26534, June 3, 2009]

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§180.1033 Methoprene; exemption from the requirement of a tolerance.

Methoprene is exempt from the requirement of a tolerance in or on all food commodities when used to control insect 

larvae.

[68 FR 34829, June 11, 2003]

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§180.1037 Polybutenes; exemption from the requirement of a tolerance.

(a) Polybutenes are exempt from the requirement of a tolerance for residues in or on the raw agricultural commodity 

cotton, undelinted seed when used as a sticker agent for formulations of the attractant gossyplure (1:1 mixture of (Z,Z)- 

and (Z,E)-7,11-hexadecadien-1-ol acetate) to disrupt the mating of the pink bollworm.

(b) Polybutenes are exempt from the requirement of a tolerance for residues in or on the raw agricultural commodity 

artichoke when used as a sticker agent in multi-layered laminted controlled-release dispensers of (Z)-11-hexaadecenal to 

disrupt the mating of the artichoke plume moth.

[74 FR 26534, June 3, 2009]

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§180.1040 Ethylene glycol; exemption from the requirement of a tolerance.

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Ethylene glycol as a component of pesticide formulations is exempt from the requirement of a tolerance when used in 

foliar applications to peanut plants.

[43 FR 41393, Sept. 18, 1978]

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§180.1041 Nosema locustae; exemption from the requirement of a tolerance.

The insecticide Nosema locustae is exempted from the requirement of a tolerance for residues in or on all raw 

agricultural commodities.

[47 FR 21537, May 19, 1982]

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§180.1043 Gossyplure; exemption from the requirement of a tolerance.

The pheromone gossyplure, a 1:1 mixture of (Z,Z)- and (Z,E)-7,11-hexadecadien-1-ol acetate) is exempt from the 

requirement of a tolerance in or on the raw agricultural commodity cotton, undelinted seed when applied to cotton from 

capillary fibers.

[74 FR 26534, June 3, 2009]

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§180.1049 Carbon dioxide; exemption from the requirement of a tolerance.

The insecticide carbon dioxide is exempted from the requirement of a tolerance when used after harvest in modified 

atmospheres for stored insect control on food commodities. 

[65 FR 33716, May 24, 2000]

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§180.1050 Nitrogen; exemption from the requirements of a tolerance.

The insecticide nitrogen is exempted from the requirements of a tolerance when used after harvest in modified 

atmospheres for stored product insect control on all food commodities. 

[65 FR 33716, May 24, 2000]

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§180.1052 2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine; exemption from the requirement of a tolerance.

2,2,5-trimethyl-3-dichloroacetyl-1,3-oxazolidine is exempted from the requirement of a tolerance when used as an 

inert ingredient in formulations of the herbicides S-ethyl dipropylthiocarbamate, S-propyl dipropylthiocarbamate, and 

S-ethyl diisobutylthiocarbamate applied to corn fields before the corn plants emerge from the soil with a maximum of 0.5 

pound of the inert ingredient per acre.

[45 FR 51201, Aug. 1, 1980]

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§180.1054 Calcium hypochlorite; exemptions from the requirement of a tolerance.

(a) Calcium hypochlorite is exempted from the requirement of a tolerance when used preharvest or postharvest in 

solution on all raw agricultural commodities.

(b) Calcium hypochlorite is exempted from the requirement of a tolerance in or on grape when used as a fumigant 

postharvest by means of a chlorine generator pad.

[59 FR 59165, Nov. 16, 1994, as amended at 74 FR 26534, June 3, 2009]

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§180.1056 Boiled linseed oil; exemption from requirement of tolerance.

Boiled linseed oil (containing no more than 0.33 percent manganese naphthenate and no more than 0.33 percent 

cobalt naphthenate) is exempt from the requirement of a tolerance when used as a coating agent for S-ethyl hexahydroeCFR — Code of Federal Regulations Page 408 of 441

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1H-azepine-1-carbothioate. No more than 15 percent of the pesticide formulation may consist of “boiled linseed oil.” This 

exemption is limited to use on rice before edible parts form.

[46 FR 33270, June 29, 1981]

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§180.1057 Phytophthora palmivora; exemption from requirement of tolerance.

Phytophthora palmivora is exempted from the requirement of a tolerance in or on the raw agricultural commodity fruit, 

citrus.

[74 FR 26534, June 3, 2009]

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§180.1058 Sodium diacetate; exemption from the requirement of a tolerance.

Sodium diacetate, when used postharvest as a fungicide, is exempt from the requirement of a tolerance for residues 

in or on alfalfa, hay; Bermudagrass, hay; bluegrass, hay; bromegrass, hay; clover,hay; corm, field, grain; corn, pop, grain; 

oat, grain; orchardgrass, hay; sorghum, grain, grain; sudangrass, hay; ryegrass, Italian, hay; timothy, hay.

[74 FR 26534, June 3, 2009]

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§180.1064 Tomato pinworm insect pheromone; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for combined residues of both components of the 

tomato pinworm insect pheromone (E)-4-tridecen-1-yl acetate and (Z)-4-tridecen-1-yl acetate in or on all raw agricultural 

commodities (preharvest) in accordance with the following prescribed conditions:

(a) Application shall be limited solely to point source dispensers or point source chopped fibers containing the tomato 

pinworm insect pheromone.

(b) Cumulative yearly application cannot exceed 200 grams of tomato pinworm pheromone per acre.

[58 FR 34376, June 25, 1993]

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§180.1065 2-Amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one; exemption from the 

requirement of a tolerance.

The inert ingredient, 2-amino-4,5-dihydro-6-methyl-4-propyl-s-triazolo(1,5-alpha)pyrimidin-5-one is exempted from the 

requirement of a tolerance when used as an emetic at not more than 0.3 percent in formulations of paraquat dichloride. 

Further restrictions on this exemption are that this ingredient may not be advertised as an emetic and the paraquat product 

may not be promoted in any way because of the inclusion of this inert ingredient.

[70 FR 46431, Aug. 10, 2005]

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§180.1067 Methyl eugenol and malathion combination; exemption from the requirement of a tolerance.

The insect attractant methyl eugenol and the insecticide malathion are exempt from the requirement of tolerances on 

all raw agricultural commodities when used in combination in Oriental fruit fly eradication programs under the authority of 

the U.S. Department of Agriculture, in accordance with the following directions and specifications:

(a) The combination shall be at the ratio of three parts methyl eugenol to one part technical malathion (3:1).

(b) This combination is to be impregnated on a carrier (cigarette filter tips (cellulose acetate); cotton strings; fiberboard 

squares) or mixed with a jel cleared under 40 CFR 180.920 or 180.950.

(c) The maximum actual dosage per application per acre shall be 28.35 grams (one ounce avoirdupois) methyl 

eugenol and 9.45 grams (one-third (0.33) ounce avoirdupois) technical malathion.

[47 FR 9002, Mar. 3, 1982, as amended at 69 FR 23142, Apr. 28, 2004]

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§180.1068 C12-C18 fatty acid potassium salts; exemption from the requirement of a tolerance.

C12-C18 fatty acids (saturated and unsaturated) potassium salts are exempted from the requirement of a tolerance for 

residues in or on all raw agricultural commodities when used in accordance with good agricultural practice.

[60 FR 34871, July 5, 1995]

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§180.1069 (Z)-11-Hexadecenal; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biological insecticide (pheromone) 

(Z)-11-hexadecenal when used as a sex attractant on artichoke plants to control the artichoke plume moth.

[47 FR 14906, Apr. 7, 1982]

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§180.1070 Sodium chlorite; exemption from the requirement of a tolerance.

Sodium chlorite is exempted from the requirement of a tolerance for residues when used in accordance with good 

agricultural practice as a seed-soak treatment in the growing of the raw agricultural commodities vegetable, brassica, 

leafy, group 5 and radish, roots and radish, tops.

[74 FR 26534, June 3, 2009]

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§180.1071 Peanuts, Tree Nuts, Milk, Soybeans, Eggs, Fish, Crustacea, and Wheat; exemption from the 

requirement of a tolerance.

(a) General. Residues resulting from the following uses of the food commodity forms of peanuts, tree nuts, milk, 

soybeans, eggs (including putrescent eggs), fish, crustacea, and wheat are exempted from the requirement of a tolerance 

in or on all food commodities under FFDCA section 408 (when used as either an inert or an active ingredient in a pesticide 

formulation), if such use is in accordance with good agricultural practices:

(1) Use in pesticide products intended to treat seeds.

(2) Use in nursery and greenhouse operations, as defined in 40 CFR 170.3, which includes seeding, potting and 

transplanting activities.

(3) Pre-plant and at-transplant applications.

(4) Incorporation into seedling and planting beds.

(5) Applications to cuttings and bare roots.

(6) Applications to the field that occur after the harvested crop has been removed.

(7) Soil-directed applications around and adjacent to all plants.

(8) Applications to rangelands, which is land, mostly grasslands, whose plants can provide food (i.e., forage) for 

grazing or browsing animals.

(9) Use in chemigation and irrigation systems (via flood, drip, or furrow application with no overhead spray 

applications).

(10) Application as part of a dry fertilizer on which an active ingredient is impregnated.

(11) Aerial and ground applications that occur when no above-ground harvestable food commodities are present 

(usually pre-bloom).

(12) Application as part of an animal feed-through product.

(13) Applications as gel and solid (non-liquid/non-spray) crack and crevice treatments that place the gel or bait directly 

into or on top of the cracks and crevices via a mechanism such as a syringe.

(14) Applications to the same crop from which the food commodity is derived, whether the plant fraction(s) intended 

for harvest are present or not, e.g., applications of peanut meal when applied to peanut plants.

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(b) Specific chemical substances. Residues resulting from the use of the following substances as either an inert or an 

active ingredient in a pesticide formulation are exempted from the requirement of a tolerance under FFDCA section 408, if 

such use is in accordance with good agricultural practices and such use is included in paragraph (a):

Chemical Substance CAS No.

Caseins 9000-71-9

Caseins, ammonium complexes 9005-42-9

Caseins, hydrolyzates 65072-00-6

Caseins, potassium complexes 68131-54-4

Caseins, sodium complexes 9005-46-3

[70 FR 1360, Jan. 7, 2005]

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§180.1072 Poly-D-glucosamine (chitosan); exemption from the requirement of a tolerance.

(a) An exemption from the requirement of a tolerance is established for residues of the biological plant growth 

regulator poly-D-glucosamine when used as a seed treatment in or on barley, beans, oats, peas, rice, and wheat.

(b) An exemption from the requirement of a tolerance is established for residues of the biological plant growth 

regulator poly-D-glucosamine when used as a pesticide in the production any raw agricultural commodity.

[60 FR 19524, Apr. 19, 1995]

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§180.1073 Isomate-M; exemption from the requirement of a tolerance.

The oriental fruit moth pheromone (Isomate-M) (Z-8-dodecen-l-yl acetate, E-8-dodecen-l-yl acetate, Z-8-dodecen-l-ol) 

is exempt from the requirement of a tolerance in or on all the raw agricultural commodities (food and feed) including, 

peach; quince; nectarine; and nut, macadamia when used in orchards with encapsulated polyethylene tubing to control 

oriental fruit moth.

[74 FR 26534, June 3, 2009]

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§180.1074 F.D.&C. Blue No. 1; exemption from the requirement of a tolerance.

F.D.&C. Blue No. 1 is exempted from the requirement of a tolerance when used as an aquatic plant control agent.

[47 FR 25963, June 16, 1982]

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§180.1075 Colletotrichum gloeosporioides f. sp. aeschynomene; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the mycoherbicide Colletotrichum 

gloeosporioides f. sp. aeschynomene in or on the following raw agricultural commodities:

COMMODITY

Aspirated grain fractions

Rice, grain

Soybean, forage

Soybean, hay

Soybean, seed

[47 FR 25742, June 15, 1982, as amended at 74 FR 26534, June 3, 2009]

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§180.1076 Viable spores of the microorganism Bacillus popilliae; exemption from the requirement of a tolerance.

(a) For the purposes of this section the microbial insecticide for which exemption from the requirement of a tolerance 

is being established shall have the following specifications:

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(1) The microorganism shall be an authentic strain of Bacillus popilliae conforming to the morphological and 

biochemical characteristics of Bacillus popilliae as described in Bergey's Manual of Determinative Bacteriology, Eighth 

Edition.

(2) Spore preparations of Bacillus popilliae shall be produced by an extraction process from diseased Japanese 

beetles, and may contain a small percentage of the naturally occurring milky disease bacterium Bacillus lentimorbus.

(3) Each lot of spore preparation, prior to the addition of other materials, shall be tested by subcutaneous injection of 

at least 1 million spores into each of five laboratory test mice weighing 17 grams to 23 grams. Such test shall show no 

evidence of infection of injury in the test animals when observed for 7 days following injection.

(b) Exemption from the requirement of a tolerance is established for residues of the microbial insecticide Bacillus 

popilliae, as specified in paragraph (a) of this section in or on grass, pasture, forage and grass, rangeland, forage when it 

is applied to growing crops in accordance with good agricultural practices.

[47 FR 38535, Sept. 1, 1982, as amended at 74 FR 26535, June 3, 2009]

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§180.1080 Plant volatiles and pheromone; exemptions from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the plant volatiles cyclic decadiene, 

cyclic decene, cyclic pentadecatriene, and decatriene and the pheromone Z-2-isopropenyl-1-methylcyclobutaneethanol; 

Z-3,3-dimethyl-Δ1,β-cyclohexaneethanol; Z-3,3-dimethyl-Δ1,α-cyclohexaneethanal; E-3,3-dimethylΔ1,α-cyclohexaneethanal combination when applied to cotton in hollow synthetic fibers.

[48 FR 28442, June 22, 1983]

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§180.1083 Dimethyl sulfoxide; exemption from the requirement of a tolerance.

Dimethyl sulfoxide (DMSO) [CAS Registry Number 67-68-5] is exempted from the requirement of a tolerance when 

used as an inert solvent or cosolvent in formulations with the following pesticides when used in accordance with good 

agricultural practices in or on the following raw agricultural commodities:

(a) Carbaryl (1-naphthyl methyl-carbamate)

Pea, dry, seed

Pea, succulent

(b) O-O-Diethyl O-(2-isopropyl-6-methyl-4-pyrimidinyl) phosphorothioate

Pea, dry, seed

Pea, succulent

[48 FR 54819, Dec. 7, 1983, as amended at 74 FR 26535, June 3, 2009]

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§180.1084 Monocarbamide dihydrogen sulfate; exemption from the requirement of a tolerance.

Monocarbamide dihydrogen sulfate is exempted from the requirement of a tolerance when used as a herbicide or 

desiccant in or on all raw agricultural commodities.

[53 FR 12152, Apr. 13, 1988]

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§180.1086 3,7,11-Trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-trimethyl-2,6,10-dodecatriene-3-ol; exemption 

from the requirement of a tolerance.

The insect pheromone containing the active ingredients 3,7,11-trimethyl-1,6,10-dodecatriene-1-ol and 3,7,11-

trimethyl-2,6,10-dodecatriene-3-ol is exempted from the requirement of a tolerance in or on all raw agricultural 

commodities.

[52 FR 12165, Apr. 15, 1987; 52 FR 29014, Aug. 5, 1987]

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§180.1087 Sesame stalks; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biorational nematicide sesame 

stalk in or on the following raw agricultural commodities: Almond; almond, hulls; cotton, undelinted seed; cotton, gin 

byproducts; soybean, seed; soybean, forage; soybean, hay; aspirated grain fractions; potato; beet, sugar, roots; beet, 

sugar, tops; tomato; pepper, bell; squash; strawberry; eggplant; cucumber; carrot, roots; radish, roots; radish, top; turnip, 

roots; turnip, tops; onion; pea, dry; pea, succulent; melon; grape; walnut; orange; grapefruit; mulberry; peach; apple; 

apricot; blackberry; loganberry; pecan; cherry; plum, and cranberry.

[74 FR 26535, June 3, 2009]

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§180.1089 Poly-N-acetyl-D-glucosamine; exemption from the requirement of tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical nematicide 

poly-N-acetyl-D-glucosamine on a variety of agricultural crops.

[53 FR 10249, Mar. 30, 1988]

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§180.1090 Lactic acid; exemption from the requirement of a tolerance.

Lactic acid (2-hydroxypropanoic acid) is exempted from the requirement of a tolerance when used as a plant growth 

regulator in or on all raw agricultural commodities.

[53 FR 15286, May 4, 1988]

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§180.1091 Aluminum isopropoxide and aluminum secondary butoxide; exemption from the requirement of a 

tolerance.

Aluminum isopropoxide (CAS Reg. No. 555-31-7) and aluminum secondary butoxide (CAS Reg. No. 2269-22-9) are 

exempted from the requirement of a tolerance when used in accordance with good agricultural practices as stabilizers in 

formulations of the insecticide amitraz [N′-(2,4-dimethylphenyl)-N-[[(2,4-dimethylphenyl)imino]-N-methylmethanimidamide] 

applied to growing crops or animals.

[53 FR 34509, Sept. 7, 1988; 53 FR 36696, Sept. 21, 1988]

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§180.1092 Menthol; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the pesticidal chemical menthol in or 

on honey and honeycomb when used in accordance with good agricultural practice in over-wintering bee hives.

[74 FR 26535, June 3, 2009]

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§180.1095 Chlorine gas; exemptions from the requirement of a tolerance.

Chlorine gas is exempted from the requirement of a tolerance when used preharvest or postharvest in solution on all 

raw agricultural commodities.

[56 FR 21309, May 8, 1991]

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§180.1097 GBM-ROPE; exemption from the requirement of a tolerance.

The grape berry moth pheromone (GBM-ROPE) containing the active ingredients (Z)-9-dedecenyl acetate and (Z)-11-

tetradecenyl acetate is exempt from the requirement of a tolerance in or on the raw agricultural commodity grape when 

used in orchards with encapsulated polyethylene tubing to control grape berry moth.

[74 FR 26535, June 3, 2009]

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§180.1098 Gibberellins [Gibberellic Acids (GA3 and GA4 + GA7), and Sodium or Potassium Gibberellate]; 

exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of gibberellins [gibberellic acids (GA3 

and GA4 + GA7), and sodium or potassium gibberellate] in or on all food commodities when used as plant regulators on 

plants, seeds, or cuttings and on all food commodities after harvest in accordance with good agricultural practices.

[64 FR 31505, June 11, 1999]

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§180.1100 Gliocladium virens isolate GL-21; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biofungicide Gliocladium virens

GL-21 in or on all raw agricultural commodities when used either as a fungicide for inoculation of plant growth media in 

greenhouses or on terrestrial food crops grown outdoors in accordance with good agricultural practices.

[60 FR 48659, Sept. 20, 1995; 60 FR 52248, Oct. 5, 1995]

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§180.1101 Parasitic (parasitoid) and predatory insects; exemption from the requirement of a tolerance.

Parasitic (parasitoid) and predatory insects are exempted from the requirement of a tolerance for residues when they 

are used in accordance with good agricultural and pest control practices to control insect pests of stored raw whole grains 

such as corn, small grains, rice, soybeans, peanuts, and other legumes either bulk or warehoused in bags. For the 

purposes of this rule, the parasites (parasitoids) and predators are considered to be species of Hymenoptera in the genera 

Trichogramma, Trichogrammatidae; Bracon, Braconidae; Venturia, Mesostenus, Ichneumonidae; Anisopteromalus, 

Choetospila, Lariophagus, Dibrachys, Habrocytus, Pteromalus, Pteromalidae; Cephalonomia, Holepyris, Laelius,

Bethylidae; and of Hemiptera in the genera Xylocoris, Lyctocoris, and Dufouriellus, Anthocoridae. Whole insects, 

fragments, parts, and other residues of these parasites and predators remain subject to 21 U.S.C. 342(a)(3).

[57 FR 14646, Apr. 22, 1992]

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§180.1102 Trichoderma harzianum KRL-AG2 (ATCC #20847) strain T-22; exemption from requirement of a 

tolerance.

An exemption from the requirement of a tolerance is established for residues of the biofungicide Trichoderma 

harzianum KRL-AG2 (ATCC #20847); also known as strain T-22 when applied in/or on all food commodities.

[64 FR 16860, Apr. 7, 1999]

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§180.1103 Isomate-C; exemption from the requirement of a tolerance.

The codling moth pheromone (Isomate-C) E,E-8,10-dodecenyl alcohol, dodecanol, tetradecanol is exempt from the 

requirements of a tolerance in or on all raw agricultural commodities when formulated in polyethylene pheromone 

dispensers for use in orchards with encapsulated polyethylene tubing to control codling moth.

[74 FR 26535, June 3, 2009]

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§180.1107 Delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas 

fluorescens; exemption from the requirement of a tolerance.

The delta endotoxin of Bacillus thuringiensis variety kurstaki encapsulated into killed Pseudomonas fluorescens is 

exempt from the requirements of a tolerance in or on all raw agricultural commodities.

[56 FR 28328, June 20, 1991]

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§180.1108 Delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas 

fluorescens; exemption from the requirement of a tolerance.

The delta endotoxin of Bacillus thuringiensis variety San Diego encapsulated into killed Pseudomonas fluorescens is 

exempt from the requirements of a tolerance in or on all raw agricultural commodities.

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[56 FR 28326, June 20, 1991]

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§180.1110 3-Carbamyl-2,4,5-trichlorobenzoic acid; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of 3-carbamyl-2,4,5-trichlorobenzoic 

acid in or on all raw agricultural commodities which occur from the direct application of chlorothalonil to crops in §180.275 

(a) and (b) and/or as an inadvertent residue resulting from the soil metabolism of chlorothalonil when applied to crops in 

§180.275 (a) and (b), and subsequent uptake by rotated crops when used according to approved agricultural practices.

[57 FR 24552, June 10, 1992]

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§180.1111 Bacillus subtilis GB03; exemption from the requirement of a tolerance.

The biofungicide Bacillus subtilis GB03 is exempted from the requirement of a tolerance in or on all raw agricultural 

commodities when used in accordance with good agricultural practices.

[73 FR 50556, Aug. 27, 2008]

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§180.1113 Lagenidium giganteum; exemption from the requirement of a tolerance.

Lagenidium giganteum (a fungal organism) is exempt from the requirement of a tolerance in or on the raw agricultural 

commodities aspirated grain fractions; grass, forage; grass, hay; rice, grain; rice, straw; soybean, seed; soybean, forage; 

soybean, hay; rice, wild, grain.

[74 FR 26535, June 3, 2009]

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§180.1114 Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and Pseudomonas syringae

742RS; exemptions from the requirement of a tolerance.

The biological pesticides Pseudomonas fluorescens A506, Pseudomonas fluorescens 1629RS, and Pseudomonas 

syringae 742RS are exempted from the requirement of a tolerance in or on all raw agricultural commodities when applied 

as a frost protection agent or biological control agent to growing agricultural crops in accordance with good agricultural 

practices.

[57 FR 42700, Sept. 16, 1992]

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§180.1118 Spodoptera exigua nuclear polyhedrosis virus; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the microbial pest control agent Spodoptera 

exigua nuclear polyhedrosis virus when used as a pesticide control agent on all raw agricultural commodities.

[58 FR 25784, Apr. 28, 1993]

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§180.1119 Azadirachtin; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the biochemical azadirachtin, which is isolated 

from the berries of the Neem tree (Azadirachta indica), when used as a pesticide at 20 grams or less per acre on all raw 

agricultural commodities.

[58 FR 8696, Feb. 17, 1993]

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§180.1120 Streptomyces sp. strain K61; exemption from the requirement of a tolerance.

The biological pesticide Streptomyces sp. strain K61 is exempted from the requirement of a tolerance in or on all raw 

agricultural commodities when used as a fungicide for the treatment of seeds, cuttings, transplants, and plants of 

agricultural crops in accordance with good agricultural practices.

[58 FR 21403, Apr. 21, 1993]

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§180.1121 Boric acid and its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric 

oxide (boric anhydride), sodium borate and sodium metaborate; exemptions from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the pesticidal chemical boric acid and 

its salts, borax (sodium borate decahydrate), disodium octaborate tetrahydrate, boric oxide (boric anhydride), sodium 

borate and sodium metaborate, in or on raw agricultural commodities when used as an active ingredient in insecticides, 

herbicides, or fungicides preharvest or postharvest in accordance with good agricultural practices.

[58 FR 44283, Aug. 20, 1993]

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§180.1122 Inert ingredients of semiochemical dispensers; exemptions from the requirement of a tolerance.

(a) All inert ingredients of semiochemical dispenser products formulated with, and/or contained in, dispensers made of 

polymeric matrix materials (including the monomers, plasticizers, dispersing agents, antioxidants, UV protectants, 

stabilizers, and other inert ingredients) are exempted from the requirement of a tolerance when used as carriers in 

pesticide formulations for application to growing crops only. These dispensers shall conform to the following specifications:

(1) Exposure must be limited to inadvertent physical contact only. The design of the dispenser must be such as to 

preclude any contamination by its components of the raw agricultural commodity (RAC) or processed foods/feeds derived 

from the commodity by virtue of its proximity to the RAC or as a result of its physical size.

(2) The dispensers must be applied discretely. This exemption does not apply to components of semiochemical 

formulations applied in a broadcast manner either to a crop field plot or to individual plants.

(b) A semiochemical dispenser is a single enclosed or semi-enclosed unit that releases semiochemical(s) into the 

surrounding atmosphere via volatilization and is applied in a manner to provide discrete application of the semiochemical

(s) into the environment.

(c) Semiochemicals are chemicals that are emitted by plants or animals and modify the behavior of receiving 

organisms. These chemicals must be naturally occurring or substantially identical to naturally occurring semiochemicals.

[58 FR 64494, Dec. 8, 1993]

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§180.1124 Arthropod pheromones; exemption from the requirement of a tolerance.

Arthropod pheromones, as described in §152.25(b) of this chapter, when used in retrievably sized polymeric matrix 

dispensers are exempt from the requirement of a tolerance in or on all raw agricultural commodities when applied to 

growing crops only at a rate not to exceed 150 grams active ingredient/acre/year in accordance with good agricultural 

practices.

[59 FR 14759, Mar. 30, 1994]

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§180.1126 Codlure, (E,E)-8,10-Dodecadien-1-ol; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the insect pheromone codlure, (E,E)-8,10-

dodecadien-1-ol, on all raw agricultural commodities in accordance with the following prescribed conditions:

(a) Application shall be limited solely to codlure dispensers that conform to the following specifications:

(1) Commodity exposure must be limited to inadvertent physical contact. The design of the dispenser must be such as 

to preclude any exposure of its components to the raw agricultural commodity (RAC) or processed foods/feeds derived 

from the commodity due to its proximity to the RAC or as a result of its physical size. Dispensers must be of such size and 

construction that they are readily recognized post-application.

(2) The dispensers must be applied discretely, i.e., placed in the field in easily perceived distinct locations in a manner 

that does not prevent later retrieval. This exemption does not apply to codlure applied in a broadcast manner either to a 

crop field plot or to individual plants.

(b) A codlure dispenser is a single enclosed or semi-enclosed unit that releases codlure into the surrounding 

atmosphere via volatilization and is applied in a manner to provide discrete application (i.e., in easily perceived distinct 

locations in a manner that does not prevent later retrieval) of the codlure into the environment.

[59 FR 9931, Mar. 2, 1994]

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§180.1127 Biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde, cinnamyl alcohol, 

4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 

1,2,4-trimethoxybenzene; exemptions from the requirement of a tolerance.

Residues of the biochemical pesticide plant floral volatile attractant compounds: cinnamaldehyde, cinnamyl alcohol, 

4-methoxy cinnamaldehyde, 3-phenyl propanol, 4-methoxy phenethyl alcohol, indole, and 1,2,4-trimethoxybenzene are 

exempt from the requirement of a tolerance in or on the following raw agricultural commodities: the following field 

crops—alfalfa, clover, cotton, dandelion, peanuts (including hay), rice, sorghum (milo), soybeans, sunflower, sweet 

potatoes, and wheat; the following vegetable crops—asparagus, beans (including forage hay), beets, carrots, celery, cole 

crops (cabbage, broccoli, brussels sprouts, cauliflower), collards (kale, mustard greens, turnip greens, kohlrabi), corn, 

fresh (field, sweet, pop, seed), corn fodder and forage, chinese cabbage, cowpeas, cucurbitis (cucumbers, squash, 

pumpkin), egg plant, endive (escarole), horseradish (radish, rutabagas, turnip roots), leafy greens (spinach, swiss chard), 

lettuce (head leaf), okra, parsley, parsnip, peas, peas with pods, peppers, potatoes, sugar beets, tomatoes; the following 

tree fruit, berry and nut crops—almonds, apples, apricots, berries (blackberry, boysenberry, dewberry, loganberry, 

raspberry), blueberry, cherry, citrus (grapefruit, kumquat, lemon, lime, orange, tangelo, and tangerine) cranberry, grapes, 

melons, (watermelon, honeydew, crenshaw, cantaloupe, casaba, persian), nectarines, pears, pecans, peaches, and 

strawberry as dispersed from the end-use product Corn Rootworm Bait®, a pesticidal bait, in accordance with the 

prescribed conditions in paragraph (a) of this section.

(a) Cumulative yearly application cannot exceed 20 grams of each floral attractant/acre/application.

(b) [Reserved]

[59 FR 15857, Apr. 5, 1994]

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§180.1128 Bacillus subtilis MBI 600; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biofungicide Bacillus subtilis MBI 

600 in or on all food commodities, including residues resulting from post-harvest uses, when applied or used in 

accordance with good agricultural practices.

[74 FR 15869, Apr. 8, 2009]

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§180.1130 N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone; exemptions from the requirement of a 

tolerance.

(a) N-(n-octyl)-2-pyrrolidone and N-(n-dodecyl)-2-pyrrolidone are exempt from the requirement of a tolerance when 

used as solvents in cotton defoliant formulations containing thidiazuron and diuron as active ingredients.

(b) N-(n-octyl)-2-pyrrolidone is exempt from the requirement of a tolerance when used as a solvent in formulations 

containing pyraflufen-ethyl as an active ingredient at a concentration not to exceed 20% by weight.

[79 FR 10682, Feb. 26, 2014]

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§180.1131 Ampelomyces quisqualis isolate M10; exemption from the requirement of a tolerance.

The biological fungicide Ampelomyces quisqualis isolate M10 is exempted from the requirement of a tolerance in or 

on all raw agricultural commodities when used as a fungicide on agricultural crops in accordance with good agricultural 

practices.

[59 FR 33437, June 29, 1994]

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§180.1135 Pasteuria penetrans; exemption from the requirement of a tolerance.

The biological nematicide Pasteuria penetrans is exempted from the requirement of a tolerance in or on all raw 

agricultural commodities, except roots and tubers, when used as a nematicide in the production of fruits and vegetables in 

greenhouses.

[59 FR 66741, Dec. 28, 1994]

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§180.1139 Sodium 5-nitroguaiacolate; exemption from the requirement of a tolerance.

The biochemical sodium 5-nitroguiacolate is exempted from the requirement of a tolerance when used as a plant 

growth regulator in end-use products at a concentration of 0.1% by weight and applied at an application rate of 20 g of a.i. 

per acre or less per application, in or on all food commodities. 

[65 FR 66181, Nov. 3, 2000]

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§180.1140 Sodium o-nitrophenolate; exemption from the requirement of a tolerance.

The biochemical sodium o-nitrophenolate is exempted from the requirement of a tolerance when used as a plant 

growth regulator in end-use products at a concentration of 0.2% by weight and applied at an application rate of 20 g of a.i. 

per acre or less per application, in or on all food commodities. 

[65 FR 66181, Nov. 3, 2000]

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§180.1141 Sodium p-nitrophenolate; exemption from the requirement of a tolerance.

The biochemical sodium p-nitrophenolate is exempted from the requirement of a tolerance when used as a plant 

growth regulator in end-use product at a concentration of 0.3% by weight and applied at an application rate of 20 g of a.i. 

per acre or less per application, in or on all food commodities.

[65 FR 66181, Nov. 3, 2000]

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§180.1142 1,4-Dimethylnaphthalene; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of the plant growth regulator, 

1,4-dimethylnaphthalene (1,4-DMN), when applied postharvest to all sprouting root, tuber, and bulb crops in accordance 

with good agricultural practices.

[77 FR 68697, Nov. 16, 2012]

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§180.1143 Methyl anthranilate; exemption from the requirement of a tolerance.

Residues of methyl anthranilate, a biochemical pesticide, are exempt from the requirement of a tolerance in or on all 

food commodities, when used in accordance with good agricultural practices.

[67 FR 51088, Aug. 7, 2002]

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§180.1144 Candida oleophila isolate I-182; exemption from the requirement of a tolerance.

Candida oleophila isolate I-182, when used as a post-harvest biological fungicide, is exempted from the requirement 

of a tolerance in or on all raw agricultural commodities.

[60 FR 11033, Mar. 1, 1995]

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§180.1145 Pseudomonas syringae; exemption from the requirement of a tolerance.

Pseudomonas syringae is exempted from the requirement of a tolerance on all raw agricultural commodities when 

applied postharvest according to good agricultural practices.

[60 FR 12703, Mar. 8, 1995]

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§180.1146 Beauveria bassiana Strain GHA; exemption from the requirement of a tolerance.

Beauveria bassiana Strain GHA is exempted from the requirement of a tolerance in or on all raw agricultural 

commodities when applied to growing crops according to good agricultural practices.

[60 FR 18547, Apr. 12, 1995]

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§180.1148 Occlusion Bodies of the Granulosis Virus of Cydia pomenella; tolerance exemption.

An exemption from the requirement of a tolerance is established for residues of the microbial pest control agent 

Occlusion Bodies of the Granulosis Virus of Cydia pomonella (codling moth) in or on all raw agricultural commodities.

[60 FR 42450, Aug. 16, 1995]

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§180.1149 Inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera; exemption from the 

requirement of a tolerance.

The microbial pest control agent inclusion bodies of the multi-nuclear polyhedrosis virus of Anagrapha falcifera is 

exempted from the requirement of a tolerance in or on all raw agricultural commodities when used to control certain 

lepidopteran pest species.

[60 FR 37020, July 19, 1995]

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§180.1150 6-Benzyladenine; exemption from the requirement of a tolerance.

The biochemical plant regulator 6-benzyladenine (6-BA) is exempt from the requirement of a tolerance in or on apple 

and pear when applied at a rate of ≤182 grams of active ingredient per acre per season, and in or on pistachio when 

applied at a rate of ≤60 grams of active ingredient per acre per season.

[72 FR 13179, Mar. 21, 2007]

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§180.1153 Lepidopteran pheromones; exemption from the requirement of a tolerance.

Lepidopteran pheromones that are naturally occurring compounds, or identical or substantially similar synthetic 

compounds, designated by an unbranched aliphatic chain (between 9 and 18 carbons) ending in an alcohol, aldehyde or 

acetate functional group and containing up to 3 double bonds in the aliphatic backbone, are exempt from the requirement 

of a tolerance in or on all raw agricultural commodities. This exemption only pertains to those situations when the 

pheromone is: Applied to growing crops at a rate not to exceed 150 grams active ingredient/acre/year in accordance with 

good agricultural practices; and applied as a post-harvest treatment to stored food commodities at a rate not to exceed 3.5 

grams active ingredient/1,000 ft2

/year (equivalent to 150 grams active ingredient/acre/year) in accordance with good 

agricultural practices.

[71 FR 45399, Aug. 9, 2006]

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§180.1154 CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in 

killed Pseudomonas fluorescens, and the expression plasmid and cloning vector genetic constructs.

CryIA(c) and CryIC derived delta-endotoxins of Bacillus thuringiensis var. kurstaki encapsulated in killed 

Pseudomonas fluorescens and the expression plasmid and cloning vector genetic constructs are exempt from the 

requirement of a tolerance when used in or on all raw agricultural commodities.

[60 FR 47489, Sept. 13, 1995]

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§180.1156 Cinnamaldehyde; exemption from the requirement of a tolerance.

Cinnamaldehyde (3-phenyl-2-propenal) is exempted from the requirement of a tolerance in or on all food 

commodities, when used as a fungicide, insecticide, and algaecide in accordance with good agricultual practices.

[64 FR 7804, Feb. 17, 1999; 64 FR 14099, Mar. 24, 1999]

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§180.1157 Cytokinins; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of cytokinins (specifically: aqueous 

extract of seaweed meal and kinetin) in or on all food commodities when used as plant regulators on plants, seeds, or 

cuttings and on all food commodities after harvest in accordance with good agricultural practices.

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[64 FR 31505, June 11, 1999]

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§180.1158 Auxins; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of auxins (specifically: indole-3-acetic 

acid and indole-3-butyric acid) in or on all food commodities when used as plant regulators on plants, seeds, or cuttings 

and on all food commodities after harvest in accordance with good agricultural practices.

[64 FR 31505, June 11, 1999]

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§180.1159 Pelargonic acid; exemption from the requirement of tolerances.

(a) An exemption from the requirement of a tolerance is established for residues of pelargonic acid in or on all food 

commodities when used as a plant regulator on plants, seeds, or cuttings and on all food commodities after harvest in 

accordance with good agricultural practices.

(b) Pelargonic acid when used as an herbicide is exempt from the requirement of a tolerance on all plant food 

commodities provided that:

(1) Applications are not made directly to the food commodity except when used as a harvest aid or desiccant to: any 

root and tuber vegetable, bulb vegetable or cotton.

(2) When pelargonic acid is used as a harvest aid or desiccant, applications must be made no later than 24 hours 

prior to harvest.

(c) An exemption from the requirement of a tolerance is established for residues of pelargonic acid in or on all raw 

agricultural commodities and in processed commodities, when such residues result from the use of pelargonic acid as an 

antimicrobial treatment in solutions containing a diluted end-use concentration of pelargonic acid up to 170 ppm per 

application on food contact surfaces such as equipment, pipelines, tanks, vats, fillers, evaporators, pasteurizers and 

aseptic equipment in restaurants, food service operations, dairies, breweries, wineries, beverage and food processing 

plants.

[62 FR 28364, May 23, 1997, as amended at 64 FR 31505, June 11, 1999; 68 FR 7935, Feb. 19, 2003]

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§180.1160 Jojoba oil; exemption from the requirement of a tolerance.

The insecticide and spray tank adjuvant jojoba oil is exempted from the requirement of a tolerance in or on all raw 

agricultural commodities when applied at the rate of 1.0% or less of the final spray in accordance with good agricultural 

practices, provided the jojoba oil does not contain simmondsin, simmondsin-2-ferulate, and related conjugated 

organonitriles including demethyl simmondsin and didemethylsimmondsin.

[61 FR 2121, Jan. 25, 1996]

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§180.1161 Clarified hydrophobic extract of neem oil; exemption from the requirement of a tolerance.

Clarified hydrophobic extract of neem oil is exempt from the requirement of a tolerance on all food commodities when 

used as a botanical fungicide/insecticide/miticide.

[67 FR 43552, June 28, 2002]

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§180.1162 Acrylate polymers and copolymers; exemption from the requirement of a tolerance.

(a) Acrylate polymers and copolymers are exempt from the requirement of a tolerance when used as inert ingredients 

in pesticidal formulations applied to growing, raw agricultural commodities. This tolerance exemption covers the acrylate 

polymers/copolymers that are intrinsically safe and already listed in TSCA inventory or will meet the polymer tolerance 

exemption from requirements of premanufacturing notification under 40 CFR 723.250. Polymers exempted can be used as 

dispensers, resins, fibers, and beads, as long as the fibers, beads and resins particle sizes are greater than 10 microns 

and insoluble in water. This exemption pertains to the acrylate polymers/copolymers used as inert ingredients for 

sprayable and dispenser pesticide formulations that are applied on food crops. Any acrylate polymers/copolymers used for 

encapsulating material must be cleared as an inert ingredient when used in pesticide formulation applied on food crops.

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(b) For the purposes of this exemption, acrylate polymers/copolymers used as inert ingredients in an end-use 

formulation must meet the definition for a polymer as given in 40 CFR 723.250(b), are not automatically excluded by 40 

723.250(d), and meet the tolerance exemption criteria in 40 CFR 723.250(e)(1), 40 CFR 723.250 (e)(2) or 40 CFR 

723.250(e)(3). Therefore, acrylate polymers and copolymers that are already listed in the TSCA inventory or will meet the 

polymer tolerance exemption under 40 CFR 723.250 as amended on March 29, 1995 are covered by this exemption.

[61 FR 6551, Feb. 21, 1996]

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§180.1163 Killed Myrothecium verrucaria; exemption from the requirement of a tolerance.

Killed Myrothecium verrucaria is exempted from the requirement of a tolerance in or on all raw agricultural 

commodities when applied as a pre-seed or pre- or post-planting soil treatment alone or mixed with water and the mixed 

suspension be applied through drip or border irrigation systems and the indicator mycotoxin levels do not exceed 15 ppm.

[61 FR 11315, Mar. 20, 1996, as amended at 61 FR 58332, Nov. 14, 1996]

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§180.1165 Capsaicin; exemption from the requirement of a tolerance.

Capsaicin is exempt from the requirement of a tolerance in or on all food commodities when used in accordance with 

approved label rates and good agricultural practice.

[63 FR 39521, July 23, 1998]

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§180.1167 Allyl isothiocyanate as a component of food grade oil of mustard; exemption from the requirement of 

a tolerance.

The insecticide and repellent Allyl isothiocyanate is exempt from the requirement of a tolerance for residues when 

used as a component of food grade oil of mustard, in or on all raw agricultural commodities, when applied according to 

approved labeling.

[61 FR 24894, May 17, 1996]

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§180.1176 Sodium bicarbonate; exemption from the requirement of a tolerance.

The biochemical pesticide sodium bicarbonate is exempted from the requirement of a tolerance in or on all raw 

agricultural commodities when applied as a fungicide or post-harvest fungicide in accordance with good agricultural 

practices.

[61 FR 67473, Dec. 23, 1996]

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§180.1177 Potassium bicarbonate; exemption from the requirement of a tolerance.

The biochemical pesticide potassium bicarbonate is exempted from the requirement of a tolerance in or on all raw 

agricultural commodities when applied as a fungicide or post-harvest fungicide in accordance with good agricultural 

practices.

[61 FR 67473, Dec. 23, 1996]

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§180.1178 Formic acid; exemption from the requirement of a tolerance.

The pesticide formic acid is exempted from the requirement of a tolerance in or on honey and honeycomb when used 

to control tracheal mites and suppress varroa mites in bee colonies, and applied in accordance with label use directions.

[74 FR 26535, June 3, 2009]

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§180.1179 Plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and Rhizophoria 

mangle; exemption from the requirement of a tolerance.

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The biochemical pesticide plant extract derived from Opuntia lindheimeri, Quercus falcata, Rhus aromatica, and 

Rhizophoria mangle is exempted from the requirement of a tolerance in or on all raw agricultural commodities when 

applied as a nematicide/plant regulator in accordance with good agricultural practices.

[62 FR 24842, May 7, 1997]

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§180.1180 Kaolin; exemption from the requirement of a tolerance.

(a) The biochemical pesticide kaolin is temporarily exempted from the requirement of a tolerance for residues of the 

insecticide Kaolin, when used on crops (apples, apricots, bananas, beans, cane berries, citrus fruits, corn, cotton, 

cranberries, cucurbits, grapes, melons, nuts, ornamentals, peaches, peanuts, pears, peppers, plums, potatoes, seed 

crops, small grains, soybeans, strawberries, sugar beets, and tomatoes) to control certain insect, fungus, and bacterial 

damage to plants. This temporary exemption from the requirement of a tolerance will permit the marketing of the food 

commodities in this paragraph when treated in accordance with the provisions of experimental use permit 70060-EUP-1, 

which is being issued under the Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA), as amended (7 U.S.C. 136). 

This temporary exemption from the requirement of a tolerance expires and is revoked December 31, 1999. This temporary 

exemption from the requirement of a tolerance may be revoked at any time if the experimental use permit is revoked or if 

any experience with or scientific data on this pesticide indicate that the tolerance is not safe.

(b) Kaolin is exempted from the requirement of a tolerance for residues when used on or in food commodities to aid in 

the control of insects, fungi, and bacteria (food/feed use).

[62 FR 19685, Apr. 23, 1997, as amended at 63 FR 9430, Feb. 25, 1998]

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§180.1181 Bacillus cereus strain BPO1; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance for residues of the Bacillus cereus strain BPO1 in or on all raw 

agricultural commodities when applied/used in accordance with label directions.

[67 FR 70017, Nov. 20, 2002]

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§180.1187 L-glutamic acid; exemption from the requirement of a tolerance.

L-glutamic acid is exempt from the requirement of a tolerance on all food commodities when used in accordance with 

good agricultural practices.

[66 FR 33198, June 21, 2001]

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§180.1188 Gamma aminobutyric acid; exemption from the requirement of a tolerance.

Gamma aminobutyric acid is exempt from the requirement of a tolerance on all food commodities when used in 

accordance with good agricultural practices.

[66 FR 33198, June 21, 2001]

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§180.1189 Methyl salicylate; exemption from the requirement of a tolerance.

The biochemical pesticide methyl salicylate is exempt from the requirement of a tolerance for residues in or on food or 

feed when used as an insect repellant in food packaging and animal feed packaging at an application rate that does not 

exceed 0.2 mg of methyl salicylate per square inch of packaging materials.

[62 FR 61639, Nov. 19, 1997]

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§180.1191 Ferric phosphate; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide, ferric 

phosphate (FePO4, CAS No. 11045-86-0) in or on all food commodities.

[62 FR 56105, Oct. 29, 1997]

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§180.1193 Potassium dihydrogen phosphate; exemption from the requirement of a tolerance.

Potassium dihydrogen phosphate is exempted from the requirement of a tolerance in or on all food commodities when 

applied as a fungicide in accordance with good agricultural practices.

[63 FR 43085, Aug. 12, 1998]

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§180.1195 Titanium dioxide.

Titanium dioxide (CAS Reg. No. 13463-67-7) is exempted from the requirement of a tolerance for residues in or on 

growing crops, when used as an inert ingredient (UV protectant) in microencapsulated formulations of the insecticide 

lambda cyhalothrin at no more than 3.0% by weight of the formulation and as an inert ingredient (UV-stabilizer) at no more 

than 5% in pesticide formulations containing the active ingredient napropamide.

[77 FR 44155, July 27, 2012]

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§180.1196 Peroxyacetic acid; exemption from the requirement of a tolerance.

(a) An exemption from the requirement of a tolerance is established for residues of peroxyacetic acid in or on all food 

commodities, when such residues result from the use of peroxyacetic acid as an antimicrobial treatment in solutions 

containing a diluted end use concentration of peroxyacetic acid up to 100 ppm per application on fruits, vegetables, tree 

nuts, cereal grains, herbs, and spices.

(b) An exemption from the requirement of a tolerance is established for residues of peroxyacetic acid, in or on all food 

commodities when used in sanitizing solutions containing a diluted end-use concentration of peroxyacetic acid up to 500 

ppm, and applied to tableware, utensils, dishes, pipelines, tanks, vats, fillers, evaporators, pasteurizers, aseptic 

equipment, milking equipment, and other food processing equipment in food handling establishments including, but not 

limited to dairies, dairy barns, restaurants, food service operations, breweries, wineries, and beverage and food 

processing plants.

(c) An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide 

peroxyacetic acid and its metabolites and degradates, including hydrogen peroxide and acetic acid, in or on all food 

commodities, when used in accordance with good agricultural practices.

[74 FR 26535, June 3, 2009, as amended at 76 FR 11969, Mar. 4, 2011]

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§180.1197 Hydrogen peroxide; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of hydrogen peroxide in or on all food 

commodities at the rate of ≤1% hydrogen peroxide per application on growing and postharvest crops.

[67 FR 41844, June 20, 2002]

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§180.1198 Gliocladium catenulatum strain J1446; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide, Gliocladium 

catenulatum strain J1446 when used in or on all food commodities.

[63 FR 37288, July 10, 1998]

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§180.1199 Lysophosphatidylethanolamine (LPE); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide 

lysophosphatidylethanolamine in or on all food commodities.

[67 FR 17636, Apr. 11, 2002]

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§180.1200 Pseudomonas fluorescens strain PRA-25; temporary exemption from the requirement of a tolerance.

A temporary exemption from the requirement of a tolerance is established for residues of the microbial pesticide, 

pseudomonas fluorescens strain PRA-25 when used on peas, snap beans and sweet corn and will expire July 31, 2001. 

[63 FR 38498, July 17, 1998]

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§180.1201 Trichoderma harzianum strain T-39; exemption from the requirement of a tolerance.

Trichoderma harzianum strain T-39 is exempt from the requirement of a tolerance on all food commodities.

[65 FR 38757, June 22, 2000]

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§180.1202 Bacillus sphaericus; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticides, Bacillus 

sphaericus when used in or on all food crops.

[63 FR 48597, Sept. 11, 1998]

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§180.1204 Harpin protein; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of individual harpin proteins that meet 

specified physiochemical and toxicological criteria when used as biochemical pesticides on all food commodities to 

enhance plant growth, quality and yield, to improve overall plant health, and to aid in pest management. The 

physiochemical and toxicological criteria identifying harpin proteins are as follows:

(a) Consists of a protein less than 100 kD in size, that is acidic (pI<7.0), glycine rich (>10%), and contains no more 

than one cystine residue.

(b) The source(s) of genetic material encoding the protein are bacterial plant pathogens not known to be mammalian 

pathogens.

(c) Elicits the hypersensitive response (HR) which is characterized as rapid, localized cell death in plant tissue after 

infiltration of harpin into the intercellular spaces of plant leaves.

(d) Possesses a common secondary structure consisting of α and β units that form an HR domain.

(e) Is heat stable (retains HR activity when heated to 65 °C for 20 minutes).

(f) Is readily degraded by a proteinase representative of environmental conditions (no protein fragments >3.5 kD after 

15 minutes degradation with Subtilisin A).

(g) Exhibits a rat acute oral toxicity (LD50) of greater than 5,000 mg product/kg body weight.

[69 FR 24996, May 5, 2004]

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§180.1205 Beauveria bassiana ATCC #74040; exemption from the requirements of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the insecticide Beauveria bassiana

(ATCC #74040) in or on all food commodities when applied or used as ground and aerial foliar sprays for use only on 

terrestrial crops.

[64 FR 22796, Apr. 28, 1999]

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§180.1206 Aspergillus flavus AF36; exemption from the requirement of a tolerance.

(a) An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Aspergillus 

flavus AF36 in or on cotton, gin byproducts; cotton, hulls; cotton, meal; cotton, refined oil; cotton, undelinted seed.

(b) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus AF36 in or on 

pistachio when applied as an antifungal agent and used in accordance with good agricultural practices.

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(c) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus AF36 in or on 

corn, field, forage; corn, field, grain; corn, field, stover; corn, field, aspirated grain fractions; corn, sweet, kernel plus cob 

with husk removed; corn, sweet, forage; corn, sweet, stover; corn, pop, grain; and corn, pop, stover, when applied/used as 

an antifungal agent.

[68 FR 41541, July 14, 2003, as amended at 72 FR 28871, May 23, 2007; 72 FR 72965, Dec. 26, 2007; 74 FR 26535, 26546, June 

3, 2009; 76 FR 16301, Mar. 23, 2011; 77 FR 14291, Mar. 9, 2012]

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§180.1207 N-acyl sarcosines and sodium N-acyl sarcosinates; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the following substances when used 

as inert ingredients (surfactants) at levels not to exceed 10% in pesticide formulations containing glyphosate:

Name CAS Reg. No.

N-acyl sarcosines

 N-cocoyl sarcosine mixture 68411-97-2

 N-lauroyl sarcosine 97-78-9

 N-myristoyl sarcosine 52558-73-3

 N-oleoyl sarcosine 110-25-8

 N-stearoyl sarcosine 142-48-3

Sodium N-acyl sarcosinates

 N-cocoyl sarcosine sodium salt mixture 61791-59-1

 N-methyl-N-(1-oxo-9-octodecenyl) glycine 3624-77-9

 N-methyl-N-(1-oxododecyl) glycine 137-16-6

 N-methyl-N-(1-oxooctadecyl) glycine 5136-55-0

 N-methyl-N-(1-oxotetradecyl glycine 30364-51-3

[64 FR 68046, Dec. 6, 1999]

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§180.1209 Bacillus subtilis strain QST 713 and strain QST 713 variant soil; exemption from the requirement of a 

tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticides Bacillus 

subtilis strain QST 713 and strain QST 713 variant soil when used in or on all food commodities.

[77 FR 73937, Dec. 12, 2012]

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§180.1210 Phosphorous acid; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of phosphorous acid and its ammonium, 

sodium, and potassium salts in or on all food commodities when used as an agricultural fungicide and in or on potatoes 

when applied as a post-harvest treatment at 35,600 ppm or less phosphorous acid.

[71 FR 49373, Aug. 23, 2006]

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§180.1212 Pseudomonas chlororaphis Strain 63-28; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Pseudomonas 

chlororaphis Strain 63-28 in or on all food commodities.

[66 FR 53346, Oct. 22, 2001]

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§180.1213 Coniothyrium minitans strain CON/M/91-08; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Coniothyrium 

minitans strain CON/M/91-08 when used in or on all food commodities.

[66 FR 16874, Mar. 28, 2001]

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§180.1218 Indian Meal Moth Granulosis Virus; exemption from the requirement of a tolerance.

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An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Indian Meal 

Moth Granulosis Virus when used in or on all food commodities.

[68 FR 55875, Sept. 29, 2003]

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§180.1219 Foramsulfuron; exemption from the requirement of a tolerance.

The pesticide foramsulfuron is exempted from the requirement of a tolerance in corn, field, grain/corn, field, forage/ 

corn, field, stover/corn, pop, grain/corn, pop, forage/corn, pop, stover; corn, sweet, forage; corn, sweet, kernel plus cob 

with husks removed; corn, sweet, stover when applied as a herbicide in accordance with good agricultural practices.

[74 FR 26535, June 3, 2009]

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§180.1220 1-Methylcyclopropene; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the 1-Methylcyclopropene in or on 

fruits and vegetables when:

(a) Used as a post harvest plant growth regulator, i.e., for the purpose of inhibiting the effects of ethylene.

(b) Applied or used outdoors for pre-harvest treatments.

[73 FR 19150, Apr. 9, 2008]

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§180.1221 Pseudozyma flocculosa strain PF-A22 UL; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pseudozyma flocculosa strain PF-A22 

UL in or on all food commodities.

[67 FR 60966, Sept. 27, 2002]

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§180.1222 Sucrose octanoate esters; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of sucrose octanoate esters [(α-Dglucopyranosyl-β-D-fructofuranosyl-octanoate), mono-, di-, and triesters of sucrose octanoate] in or on all food 

commodities when used in accordance with good agricultural practices.

[67 FR 60152, Sept. 25, 2002]

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§180.1223 Imazamox; exemption from the requirement of a tolerance.

The herbicide imazamox, (±) 2, -[4,5-dihydro-4-methyl-4-(1-methylethyl)-5-oxo-1H-imidazol-2-yl]-5-(methoxymethyl)-3-

pyridinecarboxylic acid, is exempt from the requirement of a tolerance on all food commodities when applied as a 

herbicide in accordance with good agricultural practices.

[68 FR 7433, Feb. 14, 2003]

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§180.1224 Bacillus pumilus GB34; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Bacillus 

pumilus GB34 when used as a seed treatment in or on all food commodities. An exemption is also granted for such 

residues on treated but unplanted soybean seeds.

[69 FR 76625, Dec. 22, 2004]

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§180.1225 Decanoic acid; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of decanoic acid in or on all raw 

agricultural commodities and in processed commodities, when such residues result from the use of decanoic acid as an 

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antimicrobial treatment in solutions containing a diluted end-use concentration of decanoic acid (up to 170 ppm per 

application) on food contact surfaces such as equipment, pipelines, tanks, vats, fillers, evaporators, pasteurizers and 

aseptic equipment in restaurants, food service operations, dairies, breweries, wineries, beverage and food processing 

plants.

[68 FR 7939, Feb. 19, 2003; 68 FR 17308, Apr. 9, 2003]

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§180.1226 Bacillus pumilus strain QST2808; temporary exemption from the requirement of a tolerance.

A temporary exemption from the requirement of a tolerance is established for residues of the microbial pesticide 

Bacillus pumilus strain QST2808 when used in or on all agricultural commodities when applied/used in accordance with 

label directions.

[68 FR 36480, June 18, 2003]

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§180.1228 Diallyl sulfides; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of diallyl sulfides when used in/on garlic, 

leeks, onions, and shallots.

[68 FR 40808, July 9, 2003]

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§180.1230 Ferrous sulfate; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of ferrous sulfate.

[70 FR 33363, June 8, 2005]

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§180.1231 Lime; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of lime.

[70 FR 33363, June 8, 2005]

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§180.1232 Lime-sulfur; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of lime-sulfur.

[70 FR 33363, June 8, 2005]

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§180.1233 Potassium sorbate; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of potassium sorbate.

[70 FR 33363, June 8, 2005]

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§180.1234 Sodium carbonate; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of sodium carbonate.

[70 FR 33363, June 8, 2005]

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§180.1235 Sodium hypochlorite; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of sodium hypochlorite.

[70 FR 33363, June 8, 2005]

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§180.1236 Sulfur; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of sulfur.

[70 FR 33363, June 8, 2005]

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§180.1237 Sodium metasilicate; exemption from the requirement of a tolerance.

(a) An exemption from the requirement of a tolerance is established for residues of sodium metasilicate in or on all 

food commodities when used in accordance with approved label rates and good agricultural practices as a plant desiccant, 

so long as the sodium metasilicate does not exceed 4% by weight in aqueous solution.

(b) An exemption from the requirement of a tolerance is established for residues of sodium metasilicate in or on all 

food commodities when used in accordance with approved label rates and good agricultural practices as an insecticide 

and fungicide, so long as the sodium metasilicate does not exceed 2.41% by weight in aqueous solution.

[71 FR 19441, Apr. 14, 2006]

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§180.1240 Thymol; exemption from the requirement of a tolerance.

(a) Time-limited exemptions from the requirement of a tolerance are established for residues of thymol on honey and 

honeycomb in connection with use of the pesticide under section 18 emergency exemptions granted by the EPA. These 

time-limited exemptions from the requirement of a tolerance for residues of thymol will expire and are revoked on June 30, 

2007.

(b) An exemption from the requirement of a tolerance for residues of the thymol (as present in thyme oil) in or on food 

commodities when applied/used in/on public eating places, dairy processing equipment, and/or food processing 

equipment and utensils.

[70 FR 37696, June 30, 2005, as amended at 71 FR 2895, Jan. 18, 2006; 74 FR 12617, Mar. 25, 2009]

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§180.1241 Eucalyptus oil; exemption from the requirement of a tolerance.

Time-limited exemptions from the requirement of a tolerance are established for residues of eucalyptus oil on honey 

and honeycomb in connection with use of the pesticide under section 18 emergency exemptions granted by the EPA. 

These time-limited exemptions from the requirement of a tolerance for residues of eucalyptus oil will expire and are 

revoked on June 30, 2007.

[70 FR 37696, June 30, 2005]

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§180.1243 Bacillus subtilis var. amyloliquefaciens strain FZB24; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance for residues of the Bacillus subtilis var. amyloliquefaciens strain 

FZB24 in or on all agricultural commodities when applied/used in accordance with label directions.

[68 FR 44640, July 30, 2003]

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§180.1244 Ammonium bicarbonate; exemption from the requirement of a tolerance.

An exemption from the requirement of tolerance is established for residues of ammonium bicarbonate used in or on 

all food commodities when used in accordance with good agricultural practices.

[69 FR 13745, Mar. 24, 2004]

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§180.1245 Rhamnolipid biosurfactant; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of rhamnolipid biosurfactant when used 

in accordance with good agricultural practices as a fungicide in or on all food commodities.

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[69 FR 16800, Mar. 31, 2004]

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§180.1246 Yeast Extract Hydrolysate from Saccharomyces cerevisiae: exemption from the requirement of a 

tolerance.

This regulation establishes an exemption from the requirement of a tolerance for residues of the biochemical pesticide 

Yeast Extract Hydrolysate from Saccharomyces cerevisiae on all food commodities when applied/used for the 

management of plant diseases.

[69 FR 9958, Mar. 3, 2004]

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§180.1248 Exemption of citronellol from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide citronellol in 

or on all food commodities.

[69 FR 23146, Apr. 28, 2004]

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§180.1250 C8, C10, and C12 fatty acid monoesters of glycerol and propylene glycol; exemption from the 

requirement of a tolerance.

The C8, C10, and C12 straight-chain fatty acid monoesters of glycerol (glycerol monocaprylate, glycerol 

monocaprate, and glycerol monolaurate) and propylene glycol (propylene glycol monocaprylate, propylene glycol 

monocaprate, and propylene glycol monolaurate) are exempt from the requirement of a tolerance in or on all food 

commodities when used in accordance with approved label rates and good agricultural practice.

[69 FR 34944, June 23, 2004]

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§180.1251 Geraniol; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide geraniol in 

or on all food commodities.

[69 FR 23151, Apr. 28, 2004]

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§180.1253 Streptomyces lydicus WYEC 108; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Streptomyces 

lydicus WYEC 108 when used in or on all agricultural commodities when applied/used in accordance with label directions.

[69 FR 31301, June 3, 2004]

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§180.1254 Aspergillus flavus NRRL 21882; exemption from the requirement of a tolerance.

(a) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus NRRL 21882 on 

peanut; peanut, hay; peanut, meal; and peanut, refined oil.

(b) An exemption from the requirement of a tolerance is established for residues of Aspergillus flavus NRRL 21882 on 

corn, field, forage; corn, field, grain; corn, field, stover; corn, field, aspirated grain fractions; corn, sweet, kernel plus cob 

with husk removed; corn, sweet, forage; corn, sweet, stover; corn, pop, grain; and corn, pop, stover.

[75 FR 6576, Feb. 10, 2010]

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§180.1255 Bacillus pumilus strain QST 2808; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Bacillus 

pumilus strain QST 2808 when used in or on all agricultural commodities when applied/used in accordance with label 

directions.

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[69 FR 63954, Nov. 3, 2004]

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§180.1256 Alternaria destruens strain 059; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Alternaria 

destruens Strain 059 when used in or on all raw agricultural commodities when applied/used in accordance with label 

directions.

[70 FR 28459, May 18, 2005]

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§180.1257 Paecilomyces lilacinus strain 251; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Paecilomyces 

lilacinus strain 251 when used in or on all agricultural commodities when applied/used in accordance with label directions.

[70 FR 19283, Apr. 13, 2005]

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§180.1258 Acetic acid; exemption from the requirement of a tolerance.

(a) An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide acetic 

acid when used as a preservative on post-harvest agricultural commodities intended for animal feed, including Alfalfa, 

seed; alfalfa, hay; barley, grain; bermudagrass, hay; bluegrass, hay; bromegrass, hay; clover, hay; corn, field, grain; corn, 

pop, grain; cowpea, hay; fescue, hay; lespedeza, hay; lupin; oat, grain; orchardgrass, hay; peanut, hay; timothy, hay; 

vetch, hay; and wheat, grain, or commodities described as grain or hay.

(b) An exemption from the requirement of a tolerance is established for residues of acetic acid in or on all food crops 

resulting from unintentional spray and drift to non-target vegetation including non-food, food and feed crops when used as 

a non-selective contact herbicide spray.

[75 FR 40741, July 14, 2010]

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§180.1259 Reynoutria sachalinensis extract; exemption from the requirement of a tolerance.

Residues of the biochemical pesticide Reynoutria sachalinensis extract, when derived from the whole plant extract, 

are exempt from the requirement of a tolerance in or on all food commodities.

[70 FR 55277, Sept. 21, 2005]

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§180.1260 Muscodor albus QST 20799 and the volatiles produced on rehydration; exemption from the 

requirement of a tolerance.

An exemption from the requirement of a tolerance is established on all food/feed commodities, for residues of 

Muscodor albus QST 20799, and the volatiles produced on its rehydration, when the pesticide is used for all agricultural 

applications, including seed, propagule and post harvest treatments.

[70 FR 56576, Sept. 28, 2005]

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§180.1261 Xanthomonas campestris pv. vesicatoria and Pseudomonas syringae pv. tomato specific 

Bacteriophages.

An exemption from the requirement of a tolerance is established for residues of Xanthomonas campestris pv. 

vesicatoria and Pseudomonas syringae pv. tomato specific bacteriophages in or on pepper and tomato.

[74 FR 26536, June 3, 2009]

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§180.1262 Sorbitol octanoate; exemption from the requirement of a tolerance.

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An exemption from the requirement of a tolerance is established for residues of sorbitol octanoate in or on all food 

commodities when used in accordance with label directions.

[71 FR 4518, Jan. 27, 2006]

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§180.1263 Tetrahydrofurfuryl alcohol; exemption from the requirement of a tolerance.

Tetrahydrofurfuryl alcohol (THFA, CAS Reg. No. 97-99-4) is exempt from the requirement of a tolerance in or on all 

raw agricultural commodities when used in accordance with good agricultural practices as an inert ingredient applied only:

(a) For use as a seed treatment.

(b) For applications prior to planting and at the time of planting.

(c) For use on cotton.

(d) For use in herbicides with one application to wheat and barley prior to the pre-boot stage, and two applications to 

canola and soybeans pre-bloom.

(e) For use in herbicides with two applications to field corn up to 24 inches tall (V 5 stage).

[71 FR 45415, Aug. 9, 2006]

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§180.1267 Pantoea agglomerans strain C9-1; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pantoea agglomerans strain C9-1 

when used on apples and pears.

[71 FR 24596, Apr. 26, 2006]

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§180.1268 Potassium silicate; exemption from the requirement of a tolerance.

Potassium silicate is exempt from the requirement of a tolerance in or on all food commodities so long as the 

potassium silicate is not applied at rates exceeding 1% by weight in aqueous solution and when used in accordance with 

good agricultural practices.

[71 FR 34272, June 14, 2006]

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§180.1269 Bacillus mycoides isolate J; exemption from the requirement of a tolerance.

Bacillus mycoides isolate J is temporarily exempt from the requirement of a tolerance when used as a fungicide on 

potatoes in accordance with a valid Federal Insecticide, Fungicide, and Rodenticide Act (FIFRA) section 18 emergency 

exemption. This temporary exemption from the requirement of a tolerance expires and is revoked on December 31, 2015.

[78 FR 24353, Apr. 25, 2013]

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§180.1270 Isophorone; exemption from the requirement of a tolerance.

Isophorone (CAS Reg. No. 78-59-1) is exempt from the requirement of a tolerance when used as an inert ingredient 

in pesticide formulations applied to beets, ginseng, rice, spinach, sugar beets, and Swiss chard.

[71 FR 45408, Aug. 9, 2006]

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§180.1271 Eucalyptus oil; exemption from the requirement of a tolerance.

An exemption from the requirement of tolerance is established for residues of eucalyptus oil in or on honey, 

honeycomb, and honeycomb with honey when used at 2g or less eucalyptus oil per hive, where the eucalyptus oil 

contains 80% or more eucalyptol.

[71 FR 53979, Sept. 13, 2006]

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§180.1272 Pantoea agglomerans strain E325; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pantoea agglomerans strain E325 

when used on apples and pears.

[71 FR 54933, Sept. 20, 2006]

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§180.1273 Beauveria bassiana HF23; exemption from the requirement of a tolerance.

Residues of Beauveria bassiana HF23 are exempt from the requirement of a tolerance on all food/feed commodities, 

when the pesticide is used for the treatment of chicken and livestock facilities, including the treatment of chicken and 

livestock manure.

[75 FR 10190, Mar. 5, 2010]

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§180.1274 Tris (2-ethylhexyl) phosphate; exemption from the requirement of a tolerance.

Tris (2-ethylhexyl) phosphate (TEHP, CAS Reg. No. 78-42-2) is exempt from the requirement of a tolerance for 

residues in grain, aspirated fractions; barley, grain, barley, hay, barley, straw; wheat, grain; wheat, forage; wheat, hay; 

wheat, straw when used under the following conditions:

(a) The use is in accordance with good agricultural practices;

(b) Tris (2-ethylhexyl) phosphate is used as an inert ingredient in pesticide formulations with the active ingredients 

pinoxaden, clodinafop-propargyl, and tralkoxydium;

(c) Tris (2-ethylhexyl) phosphate is applied no more than twice per season; and

(d) The applications occur no later than the pre-boot stage (prior to formation of edible grain).

[72 FR 5624, Feb. 7, 2007, as amended at 74 FR 26536, June 3, 2009]

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§180.1275 Pythium; exception from the requirement of a tolerance.

An exemption from the requirement of tolerance is established on all food/feed commodities, for residues of pythium 

oligandrum DV 74 when the pesticide is used on food crops.

[72 FR 27452, May 16, 2007]

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§180.1276 Tobacco mild green mosaic tobamovirus strain U2; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Tobacco mild green mosaic 

tobamovirus strain U2 in or on all commodities of crop groups 17 and 18 when applied as a post-emergent herbicide and 

used in accordance with label directions and good agricultural practices.

[79 FR 75756, Dec. 19, 2014]

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§180.1277 Dibasic esters; exemption from the requirement of a tolerance.

Dibasic esters (CAS Reg. No. 95481-62-2) is exempted from the requirement of a tolerance for residues when used 

as an inert ingredient (solvent and/or anti-freeze) at 10% W/W or less in microencapsulated pesticide formulations with the 

active ingredient cyfluthrin.

[73 FR 10398, Feb. 27, 2008]

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§180.1278 Quillaja saponaria extract (saponins); exemption from the requirement of a tolerance.

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Residues of the biochemical pesticide Quillaja saponaria extract (saponins) are exempt from the requirement of a 

tolerance in or on all food commodities.

[72 FR 41935, Aug. 1, 2007]

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§180.1279 Zucchini yellow mosaic virus—weak strain; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance for residues of the ZYMV-WK strain in or on all raw cucurbit when 

applied/used in accordance with label directions.

[74 FR 26536, June 3, 2009]

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§180.1280 Poly(hexamethylenebiguanide) hydrochloride (PHMB); exemption from the requirement of a tolerance.

Poly(hexamethylenebiguanide) hydrochloride (PHMB)(CAS Reg. No. 32289-58-0) is exempt from the requirement of 

a tolerance for residues of the antimicrobial in or on all food commodities when the residues are the result of the lawful 

application of a food contact surface sanitizer containing PHMB at 550 parts per million (ppm).

[73 FR 1517, Jan. 9, 2008]

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§180.1281 S-Abscisic Acid, (S)-5-(1-hydroxy-2,6,6-trimethyl-4-oxo-1-cyclohex-2-enyl)-3-methyl-penta-(2Z,4E)

-dienoic Acid; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of S-Abscisic Acid in or on all food 

commodities when applied or used preharvest as a plant regulator.

[75 FR 11744, Mar. 12, 2010]

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§180.1282 Bacillus firmus I-1582; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established in/on all food/feed commodities, for residues of 

Bacillus firmus I-1582 when used as a soil application or seed treatment.

[73 FR 25528, May 7, 2008]

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§180.1283 (Z)-7,8-epoxy-2-methyloctadecane (Disparlure); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of (Z)-7,8-epoxy-2-methyloctadecane on 

all food and feed crops that occur when it is used to treat trees, shrubs, and pastures and such use results in unintentional 

spray and drift to non-target vegetation including non-food, food, and feed crops. This active ingredient is also known as 

Disparlure.

[73 FR 33714, June 13, 2008]

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§180.1284 Ammonium salts of higher fatty acids (C8-C18 saturated; C8-C12 unsaturated); exemption from the 

requirement of a tolerance.

Ammonium salts of C8-C18 saturated and C8-C12 unsaturated higher fatty acids are exempted from the requirement of 

a tolerance for residues in or on all food commodities when used in accordance with good agricultural practice.

[74 FR 47457, Sept. 16, 2009]

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§180.1285 Polyoxin D zinc salt; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of polyoxin D zinc salt in or on all 

food commodities when applied as a fungicide and used in accordance with good agricultural practices.

[77 FR 56133, Sept. 12, 2012]

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§180.1287 Extract of Chenopodium ambrosioides near ambrosioides; exemption from the requirement of a 

tolerance.

An exemption from the requirement of a tolerance is established for the residues of Extract of Chenopodium 

ambrosioides near ambrosioides when used as an insecticide/acaricide on all food commodities.

[74 FR 634, Jan. 7, 2009]

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§180.1288 Tristyrylphenol ethoxylates; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of poly(oxy-1,2-ethanediyl), α-[2,4,6-tris

(1-phenylethyl)phenyl]-ω-hydroxy-, (CAS Reg. No. 70559-25-0) and poly(oxy-1,2-ethanediyl), α-[tris(1-phenylethyl)phenyl]

-ω-hydroxy-, (CAS Reg. No. 99734-09-5) on citrus crops, group 10, when used as inert ingredients under the following 

conditions:

(a) They are applied post-harvest;

(b) They are used as inert ingredients in pesticide formulations with azoxystrobin and fludioxonil; and

(c) They constitute no more than 10.0% of the formulated pesticide product.

[74 FR 12625, Mar. 25, 2009]

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§180.1289 Candida oleophila Strain O; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of the microbial pesticide, Candida 

oleophila Strain O, on apples and pears when applied/used as a post-harvest biofungicide.

[74 FR 22464, May 13, 2009]

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§180.1290 Pasteuria usgae; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pasteuria usgae in or on all food 

commodities when applied preharvest and used as a nematicide in accordance with good agricultural practices.

[75 FR 37737, June 30, 2010]

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§180.1291 Cold pressed neem oil; exemption from the requirement of a tolerance.

Residues of the biochemical pesticide cold pressed neem oil are exempt from the requirement of a tolerance in or on 

all food commodities.

[74 FR 55463, Oct. 28, 2009]

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§180.1292 Ulocladium oudemansii (U3 Strain); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established in/on all food commodities for residues of Ulocladium 

oudemansii (U3 Strain), when applied or used pre-harvest-only, excluding applications made post-harvest or to processed 

commodities, as a microbial fungicide in accordance with good agricultural practices.

[74 FR 55458, Oct. 28, 2009]

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§180.1293 Trichoderma gamsii strain ICC 080; exemption from the requirement of a tolerance.

Trichoderma gamsii strain ICC 080 is exempted from the requirement of a tolerance in or on all food and feed 

commodities when applied preharvest and used in accordance with good agricultural practices.

[75 FR 8507, Feb. 25, 2010]

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§180.1294 Trichoderma asperellum strain ICC 012; exemption from the requirement of a tolerance.

Trichoderma asperellum strain ICC 012 is exempted from the requirement of a tolerance in or on all food and feed 

commodities when applied pre-harvest and used in accordance with good agricultural practices.

[75 FR 9530, Mar. 3, 2010]

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§180.1295 Laminarin; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of laminarin in or on all food 

commodities when laminarin is applied preharvest.

[75 FR 8256, Feb. 24, 2010]

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§180.1296 Terpene Constituents α-terpinene, d-limonene and p-cymene, of the Extract of Chenopodium 

ambrosioides near ambrosioides as Synthetically Manufactured; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of the biochemical pesticide Terpene 

Constituents α-terpinene, d-limonene and p-cymene, of the Extract of Chenopodium ambrosioides near ambrosioides as 

Synthetically Manufactured when used as an insecticide/acaricide in or on all food commodities.

[75 FR 39455, July 9, 2010]

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§180.1297 Homobrassinolide; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of homobrassinolide in or on all food 

commodities when applied/used as a plant growth regulator in accordance with good agricultural practices.

[75 FR 39459, July 9, 2010]

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§180.1298 Trichoderma hamatum isolate 382; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Trichoderma hamatum isolate 382 in 

or on all food commodities when applied as a fungicide and used in accordance with good agricultural practices.

[75 FR 43076, July 23, 2010]

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§180.1299 Prohydrojasmon; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide 

prohydrojasmon (PDJ), propyl-3-oxo-2-pentylcyclo-pentylacetate, when used as a plant growth regulator in or on apple 

and grape pre-harvest, in accordance with label directions and good agricultural practices.

[78 FR 75257, Dec. 11, 2013]

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§180.1300 Potassium hypochlorite; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of potassium hypochlorite in or on all 

commodities.

[76 FR 11343, Mar. 2, 2011]

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§180.1301 Escherichia coli O157:H7 specific bacteriophages; temporary exemption from the requirement of a 

tolerance.

A temporary exemption from the requirement of a tolerance is established for residues of lytic bacteriophages that are 

specific to Escherichia coli O157:H7, sequence negative for shiga toxins I and II, and grown on atoxigenic host bacteria 

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when used/applied on food contact surfaces in food processing plants in accordance with the terms of Experimental Use 

Permit (EUP) No. 74234-EUP-2. This temporary exemption expires on April 1, 2013.

[76 FR 20546, Apr. 13, 2011]

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§180.1302 Sodium Ferric Ethylenediaminetetraacetate (EDTA); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of sodium ferric EDTA in or on all food 

commodities when applied as a molluscicide and used in accordance with good agricultural practices.

[76 FR 17561, Mar. 30, 2011]

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§180.1303 Metarhizium anisopliae strain F52; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Metarhizium anisopliae strain F52 in 

or on all food commodities when applied as an insecticide, miticide, or ixodicide and used in accordance with good 

agricultural practices.

[76 FR 26198, May 6, 2011]

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§180.1304 Pseudomonas fluorescens strain CL145A; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pseudomonas fluorescens strain 

CL145A in or on all food commodities when applied as a molluscicide.

[76 FR 52875, Aug. 24, 2011]

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§180.1305 Chromobacterium subtsugae strain PRAA4-1T

; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Chromobacterium subtsugae strain 

PRAA4-1T

 in or on all food commodities when applied as an insecticide or miticide and used in accordance with good 

agricultural practices.

[76 FR 55272, Sept. 7, 2011]

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§180.1306 Isaria fumosorosea (formerly Paecilomyces fumosoroseus) Apopka strain 97; exemption from the 

requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Isaria fumosorosea (formerly 

Paecilomyces fumosoroseus) Apopka strain 97 in or on all food commodities when applied as an insecticide or miticide 

and used in accordance with good agricultural practices.

[76 FR 59905, Sept. 28, 2011]

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§180.1307 Bacteriophage of Clavibacter michiganensis subspecies michiganensis; exemption from the 

requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of lytic bacteriophage of Clavibacter 

michiganensis subspecies michiganensis produced in Clavibacter michiganensis subspecies michiganensis in or on 

tomato when applied as a bactericide in accordance with good agricultural practices.

[76 FR 66192, Oct. 26, 2011]

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§180.1308 Bacillus amyloliquefaciens strain D747; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide, Bacillus 

amyloliquefaciens strain D747 in or on all food commodities when used in accordance with good agricultural practices.

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[77 FR 749, Jan. 6, 2012. Redesignated at 77 FR 2911, Jan. 20, 2012]

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§180.1309 Bacillus subtilis strain CX-9060; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the microbial pesticide Bacillus 

subtilis strain CX-9060, in or on all food commodities, when applied or used in accordance with good agricultural practices.

[77 FR 1637, Jan. 11, 2012]

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§180.1310 Trichoderma virens strain G-41; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Trichoderma virens strain G-41, in or 

on all food commodities, when applied as a fungicide and used in accordance with good agricultural practices.

[77 FR 4908, Feb. 1, 2012]

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§180.1311 Pasteuria nishizawae—Pn1; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pasteuria nishizawae—Pn1 in or on 

all food commodities when applied as a nematicide and used in accordance with good agricultural practices.

[77 FR 8741, Feb. 15, 2012]

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§180.1312 Aureobasidium pullulans strains DSM 14940 and DSM 14941; exemption from the requirement of a 

tolerance.

An exemption from the requirement of a tolerance is established for residues of Aureobasidium pullulans strains DSM 

14940 and DSM 14941 in or on all food commodities when used in accordance with label directions and good agricultural 

practices.

[80 FR 73662, Nov. 25, 2015]

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§180.1313 Bacillus pumilus strain GHA 180; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Bacillus pumilus strain GHA 180 in or 

on all food commodities when used in accordance with good agricultural practices.

[77 FR 19112, Mar. 30, 2012]

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§180.1314 Killed, nonviable Streptomyces acidiscabies strain RL-110T

; exemption from the requirement of a 

tolerance.

An exemption from the requirement of a tolerance is established for residues of killed, nonviable Streptomyces 

acidiscabies strain RL-110T

 in or on all food commodities when applied as a pre- or post-emergent herbicide and used in 

accordance with good agricultural practices.

[77 FR 35295, June 13, 2012]

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§180.1315 Natamycin; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of natamycin in or on mushrooms when 

applied as a fungistat to prevent the germination of fungal spores on mushrooms produced in enclosed mushroom 

production facilities, and in or on pineapples when applied as a fungistat in accordance with label directions and good 

agricultural practices.

[79 FR 75068, Dec. 17, 2014]

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§180.1316 Pasteuria spp. (Rotylenchulus reniformis nematode)—Pr3; exemption from the requirement of a 

tolerance.

An exemption from the requirement of a tolerance is established for residues of Pasteuria spp. (Rotylenchulus 

reniformis nematode)—Pr3 in or on all food commodities when applied as a nematicide and used in accordance with label 

directions and good agricultural practices.

[77 FR 40276, July 9, 2012]

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§180.1317 Pesticide chemicals; exemption from the requirements of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Didecyl dimethyl ammonium chloride 

in or on broccoli resulting from the use of Didecyl dimethyl ammonium chloride as a seed treatment at a treatment 

concentration of 1200 ppm prior to planting by immersion.

[77 FR 47296, Aug. 8, 2012]

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§180.1318 3-decen-2-one; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide, 3-decen-2-

one, in or on potatoes when applied as a potato sprout inhibitor and used in accordance with label directions and good 

agricultural practices.

[78 FR 11766, Feb. 20, 2013]

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§180.1319 Banda de Lupinus albus doce (BLAD); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of Banda de Lupinus albus doce 

(BLAD), a naturally occurring polypeptide from the catabolism of a seed storage protein (β-conglutin) of sweet lupines 

(Lupinus albus), in or on all food commodities when applied as a fungicide and used in accordance with label directions 

and good agricultural practices.

[78 FR 17604, Mar. 22, 2013]

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§180.1320 Methyl jasmonate; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of methyl jasmonate in or on all food 

commodities when methyl jasmonate is applied pre-harvest.

[78 FR 22794, Apr. 17, 2013]

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§180.1321 Complex Polymeric Polyhydroxy Acids; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for the residues of complex polymeric polyhydroxy 

acids in or on all food commodities when applied as a plant growth regulator and used in accordance with good 

agricultural practices.

[78 FR 46267, July 31, 2013]

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§180.1322 Bacillus pumilus strain BU F-33; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Bacillus pumilus strain BU F-33 in or 

on all food commodities when applied to elicit induced systemic resistance in plants and used in accordance with label 

directions and good agricultural practices.

[78 FR 35149, June 12, 2013]

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§180.1323 Ethyl-2E,4Z-decadienoate (Pear Ester); exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical pesticide, ethyl2E,4Z-decadienoate (pear ester), in or on all food commodities, when used in accordance with label directions and good 

agricultural practices.

[78 FR 53054, Aug. 28, 2013]

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§180.1324 GS-omega/kappa-Hxtx-Hv1a; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the pesticide GS-omega/kappa-HxtxHv1a in or on all food commodities when applied or used in accordance with label directions and good agricultural 

practices.

[79 FR 10685, Feb. 26, 2014]

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§180.1325 Heat-killed Burkholderia spp. strain A396 cells and spent fermentation media exemption from the 

requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of heat-killed Burkholderia spp. strain 

A396 cells and spent fermentation media in or on all food commodities when applied as a biological insecticide to 

agricultural crops and used in accordance with label directions and good agricultural practices.

[79 FR 15704, Mar. 21, 2014]

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§180.1326 Pseudomonas fluorescens strain D7; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Pseudomonas fluorescens strain D7 

in or on all food commodities when used in accordance with label directions and good agricultural practices.

[79 FR 60750, Oct. 8, 2014]

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§180.1327 Tetraacetylethylenediamine (TAED) and its metabolite Diacetylethylenediamine (DAED); exemption 

from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the pesticide, 

tetraacetylethylenediamine (TAED), and its metabolite diacetylethylenediamine (DAED), in or on rice and strawberries, 

when used as a fungicide and bactericide in accordance with label directions and good agricultural practices.

[79 FR 59121, Oct. 1, 2014]

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§180.1328 Beauveria bassiana strain ANT-03; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Beauveria bassiana strain ANT-03 in 

or on all food commodities, when applied as a microbial insecticide and used in accordance with label directions and good 

agricultural practices.

[79 FR 77396, Dec. 24, 2014]

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§180.1329 Bacillus subtilis strain IAB/BS03, exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Bacillus subtilis strain IAB/BS03 in or 

on all food commodities when used in accordance with label directions and good agricultural practices.

[80 FR 9217, Feb. 20, 2015]

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§180.1330 1-Octanol; exemption from the requirement of a tolerance.

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An exemption from the requirement of a tolerance is established for residues of 1-octanol in or on root and tuber 

vegetables when applied as a plant growth regulator in accordance with label directions and good agricultural practices.

[80 FR 25953, May 6, 2015]

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§180.1331 Trichoderma asperelloides strain JM41R; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of Trichoderma asperelloides strain 

JM41R in or on all food commodities when used in accordance with label directions and good agricultural practices.

[80 FR 28203, May 18, 2015]

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§180.1332 Lavandulyl senecioate; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the arthropod pheromone, lavandulyl 

senecioate (5-methyl-2-(1-methylethenyl)-4-hexenyl 3-methyl-2-butonate), in or on all raw agricultural commodities when 

applied or used in microbeads/dispensers at a rate not to exceed 150 grams active ingredient/acre/year in accordance 

with good agricultural practices.

[80 FR 49171, Aug. 17, 2015]

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§180.1333 Potassium Salts of Hops Beta acids; exemption from the requirement of a tolerance.

An exemption from the requirement of a tolerance is established for residues of the biochemical potassium salts of 

hops beta acids in or on honey and honeycomb, when used for the control of Varroa mites in accordance with label 

directions and good agricultural practices.

[80 FR 63683, Oct. 21, 2015]

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Subpart E—Pesticide Chemicals Not Requiring a Tolerance or an Exemption From a 

Tolerance

SOURCE: 66 FR 66772, Dec. 27, 2001, unless otherwise noted. 

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§180.2000 Scope.

This subpart sets forth the pesticide chemicals for use in agricultural or other food-related settings for which neither a 

tolerance nor an exemption is deemed to be needed by EPA. 

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§180.2003 Definitions.

(a) Food uses are the uses of a pesticide chemical that are likely to yield residues in food or feed crops, meat, milk, 

poultry or egg.

(b) Non-food uses are those uses that are not likely to yield residues in food or feed crops, meat, milk, poultry or egg. 

[66 FR 66772, Dec. 27, 2001, as amended at 73 FR 60158, Oct. 10, 2008]

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§180.2010 Threshold of regulation determinations.

The following pesticide chemical uses on food or feed, or food or feed crops, do not need a tolerance or exemption 

from the requirement of a tolerance, and may be registered under the Federal Insecticide, Fungicide, and Rodenticide Act, 

7 U.S.C. 136 et seq., without obtaining such tolerance or exemption, based on EPA's determination that the uses are 

below the threshold of regulation.

Pesticide 

Chemical

CAS 

Reg. 

No. Use/Limits Analytical Method

eCFR — Code of Federal Regulations Page 440 of 441

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Thiabendazole 148-

79-8

As a seed treatment for dry pea (including field pea, pigeon 

pea, chickpea or lentil), using a maximum application rate of 

0.075 pounds of active ingredient per 100 pounds of seed. 

Vines or hay grown from treated seed may not be fed to 

livestock.

High Performance Liquid Chromatography/Florescence Detector 

method1

; Modification of Ion-Pairing Liquid Chromatographic 

Determination of Benzimidazole Fungicides in Foods, Gilvydis and 

Walters, JAOAC, vol. 73, no. 5, 1990.

1

Available from: Chief, Analytical Chemistry Branch, Environmental Science Center, 701 Mapes Rd., Ft. Meade, MD 

20755-5350; telephone number: (410) 305-2905; e-mail address: residuemethods@epa.gov

[73 FR 1978, Jan. 11, 2008]

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§180.2020 Non-food determinations.

The following pesticide chemical uses do not need a tolerance or exemption from the requirement of a tolerance 

based on EPA's determination that they are not likely to result in residues in or on food. 

Pesticide Chemical CAS Reg. No. Limits Uses 

Methyl bromide 74-83-9 When applied as a pre-plant soil fumigant All pre-plant soil uses

Potassium triiodide (KI3) 12298-68-9 When applied to growing crops in foreign countries Bananas, grapes, and melons

Rhodamine B 81-88-9 Not to exceed 2% by weight of the formulated product and 60 ppm on the treated seed Dye for seed treatment

[66 FR 66772, Dec. 27, 2001, as amended at 70 FR 40201, July 13, 2005; 71 FR 45402, Aug. 9, 2006]

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