# Instructionsfor completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium,cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.
1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet. 2. Please enter the test date on the Boiler Informationworksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet.For example:"ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units
measurethat you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choosethe units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 compositesamples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected
more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of
measure.

# Information
This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium,cobalt, lead, manganese, nickel, and selenium.This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Informationworksheet.

down in the fuel column of the Boiler Information worksheet.If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet.For example:"ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of
measurethat you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choosethe units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 compositesamples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units of

# EIA

Facility Code Facility Name Boiler ID Fuel Type 1 55749 Hardin Generator Project PC1 

# bituminous

# Fuel Type 2 Fuel Type 3 Other Fuel Description

# EIA

Facility Code Facility Name Boiler ID Basis Analyte Analysis Method for each Analyte (example: ASTM D5865-04) 

# 55749 Hardin Generator Project PC1 As Received Higher Heating Value 

# ASTM D5865 55749 Hardin Generator Project PC1 As Received % Moisture 

# ASTM D3302 55749 Hardin Generator Project PC1 As Received % Ash 

# ASTM D3174/5142 55749 Hardin Generator Project PC1 As Received % Sulfur 

# ASTM D4239 55749 Hardin Generator Project PC1 Dry basis Higher Heating Value 

# ASTM D5865 55749 Hardin Generator Project PC1 Dry basis % Ash 

# ASTM D3174/5142 55749 Hardin Generator Project PC1 Dry basis % Sulfur 

# ASTM D4239 55749 Hardin Generator Project PC1 Dry basis Antimony 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Arsenic 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Beryllium 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Cadmium 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Chlorine 

# ASTM D6721 55749 Hardin Generator Project PC1 Dry basis Chromium 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Cobalt 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Fluorine 

# ASTM D3761 55749 Hardin Generator Project PC1 Dry basis Lead 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Manganese 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Mercury 

# ASTM D6722 55749 Hardin Generator Project PC1 Dry basis Nickel 

# ASTM D6357 55749 Hardin Generator Project PC1 Dry basis Selenium 

# SW7740EIA Facility Code Facility Name Boiler ID HAPs Test Group 55749 Hardin Generator Project PC1 Non-dioxin/furan organic HAPs Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) %Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units %Ash (Dry Basis) % Sulfur

(Dry Basis) Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen C1 06/29/2010 06/29/2010 8896.00 Btu/lb 24.01 8.16 0.53 11707 Btu/lb 10.73 0.69 24.01 40.62 10.73 48.65 67.83 4.76 0.89 0.69 15.1 C2 06/29/2010 06/29/2010 8840.00 Btu/lb 23.88 8.43 0.46 11614 Btu/lb 11.08 0.61 23.88 40.22 11.08 48.7 67.09 4.67 0.88 0.61 15.67 C3 06/29/2010 06/29/2010 8907.00 Btu/lb 24.24 8.09 0.52 11757 Btu/lb 10.68 0.69 24.24 40.33 10.68 48.99 68.1 4.78 0.9 0.69 14.85 C4 06/30/2010 06/30/2010 8744.00 Btu/lb 24.24 8.75 0.57 11543 Btu/lb 11.55 0.75 24.24 40.35 11.55 48.1 66.99 4.69 0.87 0.75 15.15 C5 06/30/2010 06/30/2010 8526.00 Btu/lb 23.83 10.32 0.61 11194 Btu/lb 13.54 0.8 23.83 41.02 13.54 45.44 65.18 4.58 0.85 0.8 15.05 Proximate Analyses, % by wt Ultimate Analyses, % by wt Fuel Testing ResultsEIA Facility Code Facility Name Boiler ID HAPs Test Group 55749 Hardin Generator Project PC1 Acid gas HAPs Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur

(Dry Basis) Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen C1 06/29/10 06/29/10 8896.00 Btu/lb 24.01 8.16 0.53 11707 Btu/lb 10.73 0.69 24.01 40.62 10.73 48.65 67.83 4.76 0.89 0.69 15.1 C2 06/29/10 06/29/10 8840.00 Btu/lb 23.88 8.43 0.46 11614 Btu/lb 11.08 0.61 23.88 40.22 11.08 48.7 67.09 4.67 0.88 0.61 15.67 C3 06/29/10 06/29/10 8907.00 Btu/lb 24.24 8.09 0.52 11757 Btu/lb 10.68 0.69 24.24 40.33 10.68 48.99 68.1 4.78 0.9 0.69 14.85 C5 06/30/10 06/30/10 8526.00 Btu/lb 23.83 10.32 0.61 11194 Btu/lb 13.54 0.8 23.83 41.02 13.54 45.44 65.18 4.58 0.85 0.8 15.05 C8 07/02/10 07/02/10 8477.00 Btu/lb 25.33 9.58 0.65 11353 Btu/lb 12.83 0.87 25.33 41.22 12.83 45.95 66.03 4.51 0.85 0.87 14.91 C9 07/02/10 07/02/10 8509.00 Btu/lb 25.53 9.12 0.58 11426 Btu/lb 12.24 0.77 25.53 40.87 12.24 46.89 66.6 4.59 0.86 0.77 14.94 Fuel Testing Results Proximate Analyses, % by wt Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler ID HAPs Test Group 55749 Hardin Generator Project PC1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) % Ash

(as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Ash (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units C4 06/30/10 06/30/10 8744.00 Btu/lb 24.24 8.75 0.57 11543 Btu/lb 11.55 0.75 12 μg/g 0.02 μg/g 1 μg/g 1 μg/g 0.4 μg/g 0.2 μg/g 6 μg/g C6 07/01/10 07/01/10 8508.00 Btu/lb 24.81 9.89 0.64 11316 Btu/lb 13.16 0.85 10 μg/g 0.03 μg/g 1 μg/g 1 μg/g 0.5 μg/g 0.2 μg/g 7 μg/g C7 07/01/10 07/01/10 8572.00 Btu/lb 24.77 9.58 0.63 11394 Btu/lb 12.74 0.84 10 μg/g 0.04 μg/g 1 μg/g 1 μg/g 0.5 μg/g 0.2 μg/g 7 μg/g Fuel Testing ResultsNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Lead (Dry Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen 4 μg/g 83 μg/g 4 μg/g 1 μg/g 52 μg/g 1 μg/g 24.24 40.35 11.55 48.1 66.99 4.69 0.87 0.75 15.15 5 μg/g 99 μg/g 5 μg/g 1 μg/g 59 μg/g 1 μg/g 24.81 40.41 13.16 46.43 65.77 4.55 0.85 0.85 14.82 4 μg/g 100 μg/g 4 μg/g 1 μg/g 60 μg/g 1 μg/g 24.77 40.4 12.74 46.86 66.32 4.61 0.87 0.84 14.62 Proximate Analyses, % by wt Ultimate Analyses, % by wt

## EIA

Facility Code Facility

Name Boiler ID 

# HAPs Test Group 

# 55749 Hardin Generator Project PC1

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

# Fuel Testing Results

## % Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)

## Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)

## Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units

## Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wt

# Note the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wt

# Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bituminous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg

# Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm μg/g