260-88

U.S. DEPARTMENT OF COMMERCE/National Bureau of Standards

Standard Reference Materials:

1982 Compilation of

Elemental Concentration Data

for NBS Biological, Geological,

and Environmental Standard

Reference Materials

100

.U57

260-33

198^
NATIONAL BUREAU OF STANDARDS

The National Bureau of Standards' was established by an act of Congress on March 3, 1901.

The Bureau's overall goal is to strengthen and advance the Nation's science and technology

and facilitate their effective application for public benefit. To this end, the Bureau conducts

research and provides: (1) a basis for the Nation's physical measurement system, (2) scientific and technological services for industry and government, (3) a technical basis for equity in trade, and (4) technical services to promote public safety. The Bureau's technical work is per- formed by the National Measurement Laboratory, the National Engineering Laboratory, and

the Institute for Computer Sciences and Technology.

THE NATIONAL MEASUREMENT LABORATORY provides the national system of

physical and chemical and materials measurement; coordinates the system with measurement

systems of other nations and furnishes essential services leading to accurate and uniform

physical and chemical measurement throughout the Nation's scientific community, industry,

and commerce; conducts materials research leading to improved methods of measurement,

standards, and data on the properties of materials needed by industry, commerce, educational

institutions, and Government; provides advisory and research services to other Government

agencies; develops, produces, and distributes Standard Reference Materials; and provides

calibration services. The Laboratory consists of the following centers:

Absolute Physical Quantities2 — Radiation Research — Chemical Physics —

Analytical Chemistry — Materials Science

THE NATIONAL ENGINEERING LABORATORY provides technology and technical ser- vices to the public and private sectors to address national needs and to solve national

problems; conducts research in engineering and applied science in support of these efforts; builds and maintains competence in the necessary disciplines required to carry out this research and technical service; develops engineering data and measurement capabilities;

provides engineering measurement traceability services; develops test methods and proposes

engineering standards and code changes; develops and proposes new engineering practices;

and develops and improves mechanisms to transfer results of its research to the ultimate user. The Laboratory consists of the following centers:

Applied Mathematics — Electronics and Electrical Engineering2 — Manufacturing

Engineering — Building Technology — Fire Research — Chemical Engineering2

THE INSTITUTE FOR COMPUTER SCIENCES AND TECHNOLOGY conducts

research and provides scientific and technical services to aid Federal agencies in the selection,

acquisition, application, and use of computer technology to improve effectiveness and

economy in Government operations in accordance with Public Law 89-306 (40 U.S.C. 759),

relevant Executive Orders, and other directives; carries out this mission by managing the

Federal Information Processing Standards Program, developing Federal ADP standards

guidelines, and managing Federal participation in ADP voluntary standardization activities; provides scientific and technological advisory services and assistance to Federal agencies; and

provides the technical foundation for computer-related policies of the Federal Government.

The Institute consists of the following centers:

Programming Science and Technology — Computer Systems Engineering.

'Headquarters and Laboratories at Gaithersburg, MD, unless otherwise noted; mailing address Washington, DC 20234. 'Some divisions within the center are located at Boulder, CO 80303.
NATIONAL BUREAU

OF STANDARDS

LIBRARY Standard Reference Materials:

oc

1982 Compilation of Elemental Concentration

Data for NBS Biological, Geological, and

Environmental Standard Reference Materials

C.2-

E.S. Gladney1

, C.E. Burns1

, D.R. Perrin 1

, I.Roelandts2

, and T.E. Gills3

1. Los Alamos National Laboratory

Los Alamos, NM 87545

2. Universite de Liege

Liege, Belgium

3. National Bureau of Standards

Washington, DC 20234

U.S. DEPARTMENT OF COMMERCE, Malcolm Baldrige, Secretary

NATIONAL BUREAU OF STANDARDS, Ernest Ambler, Director

Issued March 1 984
Library of Congress Catalog Card Number: 84-601009

National Bureau of Standards Special Publication 260-88

Natl. Bur. Stand. (U.S.), Spec. Publ. 260-88, 231 pages (Mar. 1984)

CODEN: XNBSAV

U.S. Government Printing Office

Washington: 1984

For sale by the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402
PREFACE

Standard Reference Materials (SRM's) as defined by the National Bureau of Standards are "well -characterized materials, produced in quantity, that calibrate a measurement system to assure compatibility of measurement in the

Nation." SRM's are widely used as Drimary standards in many diverse fields of science, industry and technology,

both within the United States and throuqhout the world. For many of the Nation's scientists and technologists it

is of more than passing interest to know the measurements obtained and methods used by the analytical community

when analyzing SRM's. An NBS series of papers, of which this publication is a member, called the NBS Special Publication - 260 Series is reserved for this purpose.

This 260 Series is dedicated to the dissemination of elemental concentration data for NBS bioloqical, geological

and environmental SRM's. More information will be found in this 260 than is generally found in NBS Certificate of

Analysis. This 260 enables the user of these SRM's to assess the validity of data not available in the certificate

of analysis. We hope that this 260 will provide sufficient additional information so that new application of these

SRM's may be sought and found.

Inquiries concerning the technical content of this compilation should be directed to the authors. Other questions

concerned with the availability, delivery, price of specific SRM's should be addressed to:

Office of Standard Reference Materials

National Bureau of Standards

Washington, DC 20234

Stanley D. Rasberry, Chief

Office of Standard Reference Materials
OTHER NBS PUBLICATIONS IN THIS SERIES

Catalog of NBS Standard Reference Materials (1981-83 edition), R. W. Seward, ed., NBS

Spec. Publ. 260 (November 1981). Michaelis, R. E., and Wyman, L. L. Standard

Reference Materials: Preparation of White Cast

Iron Spectrochemical Standards. NBS Misc. Publ. 260-1 (June 1964). COM74-1 1061**

Michaelis, R. E., Wyman. L. L.. and Flitsch, R., Standard Reference Materials: Preparation of NBS Copper-Base Spectrochemical Standards. NBS Misc. Publ. 260-2 (October 1964). COM74-

11063**

Michaelis, R. E., Yakowitz, H., and Moore, G. A., Standard Reference Materials: Metallographic

Characterization of an NBS Spectrometric LowAlloy Steel Standard. NBS Misc. Publ. 260-3 (October 1964). COM74-1 1060** Hague, J. L. Mears, T. W., and Michaelis, R. E., Standard Reference Materials: Sources of

Information, NBS Misc. Publ. 260-4 (February

1965). COM74-11059

Alvarez, R.. and Flitsch R., Standard Reference

Materials: Accuracy of Solution X-Ray Spectrometric Analysis of Copper-Base Alloys. NBS

Misc. Publ. 260-5 (March 1965). PB' 68068**

Shultz, J. I., Standard Reference Materials:

Methods for (he Chemical Analysis of White

Cast Iron Standards, NBS Misc. Publ. 260-6

(July 1975). COM74-11068**

Bell. R. K., Standard Reference Materials:

Methods for the Chemical Analysis of NBS

Copper-Base Spectrochemical Standards. NBS

Misc. Publ. 260-7 (October 1965). COM74-

11067** Richmond, M.S., Standard Reference Materials: Analysis of Uranium Concentrates at the

National Bureau of Standards. NBS Misc. Publ. 260-8 (December 1965). COM74- 1 1066** Anspach, S. C, Cavallo, L. M. Garfinkel, S. B. Hutchinson, J. M. R., and Smith, C. N., Standard Reference Materials: Half Lives of Materials Used in the Preparation of Standard Reference Materials of Nineteen Radioactive Nuclides

Issued by the National Bureau of Standards NBS Misc. Publ. 260-9 (November 1965).

COM74-1 1065**

Yakowitz, H., Vieth, D. L., Heinrich, K. F. J , and

Michaelis. R. E-., Standard Reference Materials: Homogeneity Characterization on NBS Spectrometric Standards II: Cartridge Brass and LowAlloy Steel, NBS Misc. Publ. 260-10 (December

1965). COM74-1 1064** Napolitano. A., and Hawkins, E. G., Standard

Reference Materials: Viscosity of Standard

Lead-Silica Glass, NBS Misc. Publ. 260-11 (November 1966). NBS Misc. Publ. 260-11** Yakowitz, H . Vieth, D. L., and Michaelis, R. E., Standard Reference Materials: Homogeneity

Characterization of NBS Spectrometric Standards III: White Cast Iron and Stainless Steel Powder Compact, NBS Misc. Publ. 260-12

(September 1966). NBS Misc. Publ. 260-12** Spijkerman, J. L., Snediker, D. K., Ruegg, F. C,

and DeVoe, J. R., Standard Reference Materials: Mossbauer Spectroscopy Standard for the Chemical Shift of Iron Compounds, NBS Misc. Publ. 260-13 (July 1967). NBS Misc. Publ.

260-13**

Menis, O., and Sterling, J. T., Standard Reference

Materials. Determination of Oxygen in Ferrous

Materials - SRM 1090, 1091, and 1092, NBS

Misc. Publ. 260-14 (September 1966). NBS Misc.

Publ. 260-14**

Passaglia, E., and Shouse, P. J. Standard Refer- ence Materials: Recommended Method of Use

of Standard Light-Sensitive Paper for Calibrat- ing Carbon Arcs Used in Testing Textiles for Colorfastness to Light, NBS Misc. Publ. 260-15 (June 1967). (Replaced by NBS Spec. Publ.

260-41.) Yakowitz, H., Michaelis, R. E., and Vieth, D. L., Standard Reference Materials: Homogeneity

Characterization of NBS Spectrometric Standards IV: Preparation and Microprobe Characterization of W-20% MO 'Alloy Fabricated by

Powder Metallurgical Methods, NBS Spec.

Publ. 260-16 (January 1969). COM74-1 1062** Catanzaro, E. J., Champion, C. E., Garner, E. L., Marinenko, G.. Sappenfield, K. M., and Shields. W. R. Standard Reference Materials: Boric

Acid; Isotopic and Assay Standard Reference

Materials, NBS Spec. Publ. 260-17 (February

1970). Out of Print

Geller, S. B., Mantek, P.A., and Cleveland. N. G., Standard Reference Materials: Calibration of NBS Secondary Standard Magnetic Tape

(Computer Amplitude Reference) Using the Reference Tape Amplitude Measurement

"Process A. "NBS Spec. Publ. 260-18 (November

1969). (See NBS Spec. Publ. 260-29.) Paule, R. C. and Mandel, J., Standard Reference

Materials: Analysis of Interlaboratory Measurements on the Vapor Pressure of Gold (Certifica- tion of Standard Reference Material 745). NBS

Spec. Publ. 260-19 (January 1970). PB190071**

Paule, R. C, and Mandel. J.. Standard Reference

Materials: Analysis of Interlaboratory Measurements on the Vapor Pressures of Cadmium and

Silver, NBS Spec. Publ. 260-21 (January 1971). COM74-1 1359** Yakowitz, H., Fiori, C. E.. and Michaelis, R. E., Standard Reference Materials: Homogeneity

Characterization of Fe-3 Si Alloy. NBS Spec.

Publ. 260-22 (February 1971). COM74-1 1357**

Napolitano. A., and Hawkins, E. G., Standard

Reference Materials: Viscosity of a Standard

Borosilicate Glass, NBS Spec. Publ. 260-23

(December 1970). COM7 1-001 57**

Sappenfield. K. M., Marineko, G., and Hague. J.

L., Standard Reference Materials: Comparison

of Redox Standards, NBS Spec. Publ. 260-24 (January 1972). COM72-50058**

Hicho. G. E.. Yakowitz, H., Rasberry. S. D., and

Michaelis. R. E.. Standard Reference Materials: A Standard Reference Material Containing

Nominally Four Percent Austenite. NBS Spec.

Publ. 260-25 (February 1971). COM74-1 1356** Martin. J. F., Standard Reference Materials:

National Bureau of Standards-US Steel Corportion Joint Program for Determining Oxygen and

Nitrogen in Steel, NBS Spec. Publ. 260-26

(February 1971). 85 cents* PB 81 176620

Garner, E. L., Machlan, L. A., and Shields. W. R., Standard Reference Materials: Uranium

Isotopic Standard Reference Materials. NBS

Spec. Publ. 260-27 (April 1971). COM74-

1 1358**

Heinrich. K. F J., Myklebust. R. L . Rasberry. S. D., and Michaelis. R. E., Standard Reference Materials: Preparation and Evaluation of SRM's 481 and 482 Gold-Silver and GoldCopper Alloys for Microanalysis, NBS Spec.

Publ. 260-28 (August 1971). COM7 1-50365**

iv
Geller, S. B., Standard Reference Materials: Cali- bration of NBS Secondary Standard Magnetic

Tape (Computer Amplitude Reference) Using

the Reference Tape Amplitude Measurement

"Process A-Model 2," NBS Spec. Publ. 260-29 (June 1971). COM7I-50282

Gorozhanina, R. S., Freedman, A. Y., and

Shaievitch, A. B. (translated by M. C. Selby),

Standard Reference Materials: Standard

Samples Issued in the USSR (A Translation from the Russian). NBS Spec. Publ. 260-30 (June

1971). COM7I-50283**

Hust, J. G., and Sparks, L. L., Standard Reference

Materials: Thermal Conductivity of Electrolytic Iron SRM 734 from 4 to 300 K, NBS Spec. Publ. 260-31 (November 1971). COM71-50563**

Mavrodineanu, R., and Lazar, J. W., Standard

Reference Materials: Standard Quartz Cuvettes,

for High Accuracy Spectrophotometry, NBS

Spec. Publ. 260-32 (December 1973). 55 cents* SNO03-O03-O1213-1 Wagner, H. L., Standard Reference Materials: Comparison of Original and Supplemental

SRM 705, Narrow Molecular Weight Distri- bution Polystyrene, NBS Spec. Publ. 260-33 (May 1972). COM72-50526**

Sparks, L. L., and Hust, J. G., Standard Reference

Materials: Thermoelectric Voltage, NBS Spec.

Publ. 260-34, (April 1972). COM72-5037 1 **

Sparks, L. L., and Hust. J. G., Standard Refer- ence Materials: Thermal Conductivity of

Austenitic Stainless Steel, SRM 735 from 5 to 280 K, NBS Spec. Publ. 260-35 (April 1972.) 35 cents* COM72-50368**

Cali, J. P., Mandel, J., Moore, L. J., and Young, D.

S., Standard Reference Materials: A Referee Method for the Determination of Calcium in Serum, NBS SRM 915, NBS Spec. Publ. 260-36 (May 1972). COM72-50527**

Shultz, J. I. Bell., R. K. Rains, T. C. and Menis.

O., Standard Reference Materials: Methods of

Analysis of NBS Clay Standards. NBS Spec.

Publ. 260-37 (June 1972). COM72-50692**

Richmond, J. C, and Hsia, J. J., Standard Refer- ence Materials: Preparation and Calibration of Standards of Spectral Specular Reflectance,

NBS Spec. Publ. 260-38 (May 1972). COM72-

50528**

Clark. A. F., Denson, V.A.. Hust. J. G.. and

Powell. R. L., Standard Reference Materials The Eddy Current Decay Method for Resistivity Characterization of High-Purity Metals. NBS

Spec. Publ. 260-39 (May 1972). COM72-50529**

McAdie, H. G., Garn, P.D., and Menis, O., Standard Reference Materials: Selection of Thermal

Analysis Temperature Standards Through a Cooperative Study (SRM 758, 759. 760), NBS

Spec. Publ. 260-40 (August 1972.) COM72-

50776** Wood, L. A., and Shouse, P J.. Standard

Reference Materials: Use of Standard LightSensitive Paper for Calibrating Carbon Arcs Used in Testing Textiles for Colorfastness to

Light, NBS Spec. Publ. 260-41 (August 1972) COM72-50775**

Wagner, H. L. and Verdier, P. H., eds.. Standard

Reference Materials: The Characterization of Linear Polyethylene, SRM 1475, NBS Spec.

Publ. 260-42 (September 1972). COM72-

50944**

Yakowitz, H., Ruff, A. W.. and Michaelis, R. E., Standard Reference Materials: Preparation and

Homogeneity Characterization of an Austenitic Iron-Chromium-Nickel Alloy, NBS Spec. Publ. 260-43 (November 1972). COM73-50760**

Schooley, J. F., Soulen, R. J., Jr., and Evans, G. A.,

Jr., Standard Reference Materials: Preparation

and Use of Superconductive Fixed Point

Devices, SRM 767, NBS Spec. Publ. 260-44 (December 1972). COM73-50037**

Greifer. B., Maienthal, E. J. Rains, T. C, and

Rasberry, S. D.. Standard Reference Materials: Powdered Lead-Based Paint, SRM 1579. NBS

Spec. Publ. 260-45 (March 1973). COM73-

50226**

Hust, J. G., and Giarratano, P. J., Standard Refer- ence Materials: Thermal Conductivity and

Electrical Resistivity Standard Reference Materials: Austenitic Stainless Steel. SRM's 735 and

798, from 4 to 1200 k, NBS Spec. Publ. 260-46 (March 1975). SN003-OO3-OI278-5

Hust. J. G., Standard Reference Materials: Electrical Resistivity of Electrolytic Iron. SRM 797. and Austenitic Stainless Steel, SRM 798. from 5

to 280 K, NBS Spec. Publ. 260-47 (February

1974). COM74-50I76**

Mangum. B. W.. and Wise. J. A., Standard Refer- ence Materials: Description and Use of Precision Thermometers for the Clinical Laboratory,

SRM 933 and SRM 934, NBS Spec. Publ. 260-48 (May 1974). 60 cents* SN003-003-0 1 278-5 Carpenter. B. S., and Reimer, G. M.. Standard Reference Materials Calibrated Glass Standards for Fission Track Use, NBS Spec. Publ. 260-49 (November 1974) COM74-5I185

Hust. J. G., and Giarratano, P. J., Standard Refer- ence Materials: Thermal Conductivity and Electrical Resistivity Standard Reference Materials:

Electrolytic Iron. SRM's 734 and 797 from 4 to 1000 K, NBS Spec. Publ. 260-50 (June 1975). $1.00* SN003-003-0 1425-7 Mavrodineanu, R., and Baldwin, J. R., Standard

Reference Materials: Glass Filters As a Standard Reference Material for Spectrophotometry;

Selection; Preparation; Certification; Use-SRM

930. NBS Spec. Publ. 260-51 (November 1975). $1.90* SN003-003-0148I-8

Hust, J. G., and Giarratano. P. J., Standard Refer- ence Materials: Thermal Conductivity and Electrical Resistivity Standard Reference Materials 730 and 799. from 4 to 3000 K, NBS Spec. Publ. 260-52 (September 1975). $1.05* SN003-003-

01464-8 Durst, R. A.. Standard Reference Materials:

Standardization of pH Measurements, NBS

Spec. Publ. 260-53 (December 1975, Revised).

$1.05 SN003-003-01551-2

Burke. R. W., and Mavrodineanu. R. Standard

Reference Materials: Certification and Use of Acidic Potassium Dichromate Solutions as an

Ultraviolet Absorbance Standard, NBS Spec.

Publ. 260-54 (August 1977). $3.00* SNOO3-O03-

01828-7

Ditmars. D. A., Cezairliyan, A., Ishihara, S., and

Douglas, T. B., Standard Reference Materials: Enthalpy and Heat Capacity; Molybdenum

SRM 781. from 273 to 2800 K. NBS Spec. Publ. 260-55 (September 1977). $2.20* SN003-003-

01836-8

Powell. R. L., Sparks, L. L., and Hust. J. G.. Standard Reference Materials: Standard

Thermocouple Materials, Pt.67: SRM 1967, NBS

Spec. Publ. 260-56 (February 1978). $2.20*

SN003-OO3-0 18864

Cali, J. P. and Plebanski. T., Guide to United

States Reference Materials. NBS Spec. Publ. 260-57 (February 1978). $2.20* PB 277173

Barnes. J. D.. and Martin, G. M.. Standard Refer- ence Materials: Polyester Film for Oxygen Gas

Transmission Measurements SRM 1470, NBS

Spec. Publ. 260-58 (June 1979) $2.00* SN003-

003-02077
Chang, T., and Kahn, A. H. Standard Reference

Materials: Electron Paramagnetic Resonance

Intensity Standard; SRM 2601, NBS Spec.

Pub!. 260-59 (August 1978) $2.30* SN003-

003-01975-5

Velapoldi, R. A., Paule, R. C, Schaffer, R . Mandel, J., and Moody, J. R., Standard Refer- ence Materials: A Reference Method for the Determination of Sodium in Serum, NBS Spec.

Publ. 260-60 (August 1978). $3.00* SN003-003

01978-0

Verdier, P. H., and Wagner. H. L., Standard Refer- ence Materials: The Characterization of Linear Polyethylene (SRM 1482, 1483, 1484), NBS

Spec. Publ. 260-61 (December 1978). $1.70* SN003-003-02006-I

Soulen, R. J., and Dove, R. B., Standard Reference

Materials: Temperature Reference Standard

for Use Below 0.5 K (SRM 768). NBS Spec.

Publ. 260-62 (April 1979). $2.30* SN003-003-

02047-8 Velapoldi, R. A., Paule. R. C, Schaffer, R. Mandel, J., Machlan, L. A., and Gramlich. J. W.,

Standard Reference Materials: A Reference Method for the Determination of Potassium in Serum. NBS Spec. Publ. 260-63 (May 1979). $3.75* SN003-003-02068

Velapoldi, R. A., and Mielenz, K. D., Standard

Reference Materials: A Fluorescence Standard

Reference Material Quinine Sulfate Dihydrate

(SRM 936), NBS Spec. Publ. 260-64 (January

1980). $4.25* SN003-003-02I48-2

Marinenko, R. B., Heinrich, K. F. J., and Ruegg,

F. C. Standard Reference Materials: MicroHomogeneity Studies of NBS Standard Reference

Materials, NBS Research Materials, and Other Related Samples. NBS Spec. Publ. 260-65

(September 1979). $3.50* SN003-003-021 14-1 Venable, W. H., Jr., and Eckerle, K. L., Standard

Reference Materials: Didymium Glass Filters for Calibrating the Wavelength Scale of Spectrophotometers (SRM 2009. 2010, 2013). NBS Spec.

Publ. 260-66 (October 1979). $3.50* SN003-003-

02127-0

Velapoldi. R. A., Paule. R. C. Schaffer, R., Mandel,

J.. Murphy. T. J., and Gramlich, J. W., Standard

Reference Materials: A Reference Method forthe Determination of Chloride in Serum, NBS Spec.

Publ. 260-67 (November 1979). $3.75* SN003-

003-02 1 36-9 Mavrodineanu, R. and Baldwin, J. R., Standard

Reference Materials: Metal-On-Quartz Filters as a Standard Reference Material for Spectrophotometry-SRM 2031, NBS Spec. Publ. 260-68

(April 1980). $4.25* SNO03-OO3-O2 167-9

Velapoldi, R. A., Paule, R. C, Schaffer, R., Mandel, J., Machlan, L. A., Garner, E. L., and

Rains, T. C, Standard Reference Materials: A

Reference Method for the Determination of Lithium in Serum. NBS Spec. Publ. 260-69 (July)

1980). $4.25* SN003-003-02214-4

Marinenko, R. B., Biancaniello, F., Boyer, P. A., Ruff, A. W., DeRobertis, L., Standard Reference

Materials: Preparation and Characterization of an Iron-Chromium-Nickel Alloy for Microanalysis, NBS Spec. Publ. 260-70 (May 1981). $2.50* SNOO3-0O3-02328-I Seward, R. W., and Mavrodineanu, R., Standard

Reference Materials: Summary of the Clinical Laboratory Standards Issued by the National Bureau of Standards, NBS Spec. Publ. 260-71 (November 1981). $6.50* SN003-003-02381-7

Reeder, D.J., Coxon. B., Enagonio, D, Christensen,

R. G„ Schaffer, R., Howell, B. F., Paule, R. C,

Mandel, J., Standard Reference Materials: SRM

900, Antiepilepsy Drug Level Assay Standard,

NBS Spec. Publ. 260-72 (June 1981). $4.25*

SN003-003-02329-9

Interrante, C. G., and Hicho, G. E., Standard Refer- ence Materials: A Standard Reference Material Containing Nominally Fifteen Percent Austenite (SRM 486), NBS Spec. Publ. 260-73 (January

1982). $2.75* SN003-003-02386-8

Marinenko, R. B., Standard Reference Materials: Preparation and Characterization of K-411 and

K-414 Mineral Glasses for Microanalysis: SRM

470. NBS Spec. Publ. 260-74 (April 1982). $3.50 SN003-003-023-95-7

Weidner, V. R., Hsia, J. J., Standard Reference

Materials: Preparation and Calibration of First Surface Aluminum Mirror Specular Reflectance Standards (SRM 2003a), NBS Spec. Publ. 260-75 (May 1982). $3.75 SN003-003-023-99-0

Hicho, G. E. and Eaton, E. E., Standard Reference Materials: A Standard Reference Material

Containing Nominally Five Percent Austenite (SRM 485a), NBS Spec. Publ. 260-76 (August

1982). $3.50 SN003-003-024-33-3 Furukawa. G. T., Riddle, J. L., Bigge. W. G., and

Pfieffer, E. R., Standard Reference Materials: Application of Some Metal SRM's as Thermometric Fixed Points, NBS Spec. Publ. 260-77 (August 1982). $6.00 SN003-003-024-34-I

Hicho, G. E. and Eaton, E. E., Standard Reference

Materials: Standard Reference Material Containing Nominally Thirty Percent Austenite (SRM

487), NBS Spec. PUbl. 260-78 (September 1982). $3.75 SN003-003-024-35-0 Richmond, J. C, Hsia, J. J., Weidner, V. R., and

Wilmering, D. B., Standard Reference Materials: Second Surface Mirror Standards of Specular

Spectral Reflectance (SRM's 2023, 2024, 2025), NBS Spec. Publ. 260-79 (October 1982). $4.50 SN003-003-024-47-3

Schaffer, R., Mandel, J., Sun, T., Cohen, A., and

Hertz, H. S., Standard Reference Materials: Evaluation by an ID/ MS Method of the AACC

Reference Method for Serum Glucose, NBS

Spec. Publ. 260-80 (October 1982). $4.75 SN003-

003-024-43-1 Burke, R. W., Mavrodineanu, R. (NBS retired). Standard Reference Materials: Accuracy in Analytical Spectrophotometry, NBS Spec. Publ. 260-81 (April 1983). $6.00 SN003-003-024-84-8

Weidner. V. R., Standard Reference Materials: White Opal Glass Diffuse Spectral Reflectance Standards for the Visible Spectrum (SRM's 2015 and 2016), NBS Spec. Publ. 260-82 (April 1983). $3.75 SN-003-003-024-89-9

Bowers,, G. N„ Jr., Alvarez, R., Cali, J. P. (NBS

retired), Eberhardt, K. R., Reeder, D. J., Schaffer. R., Uriano, G. A.. Standard Reference

Materials: The Measurement of the Catalytic

(Activity) Concentration of Seven Enzymes in NBS Human Serum SRM 909. NBS Spec.

Publ. 260-83 (June 1983). $4.50 SN003-003-024-

99-6

Gills, T. E.. Seward. R. W., Collins, R. J., and

Webster. W. C, Standard Reference Materials: Sampling, Materials Handling, Processing, and

Packaging of NBS Sulfur in Coal Standard

Reference Materials, 2682, 2683, 2684, and 2685,

NBS Spec. Publ. 260-84 (August 1983). $4.50 SN003-003-025-20-8

Swyt, D. A., Standard Reference Materials: A Look

at Techniques for the Dimensional Calibration of Standard Microscopic Particles, NBS Spec. Publ. 260-85 (September 1983). $5.50 SN003-003-

025-21-6

vi
Hicho, G. E. and Eaton, E. E., Standard Reference Materials: A Standard Reference Material

Containing Two and One-Half Percent Austenite,

SRM 488. NBS Spec. Publ. 260-86 (December

1983) SN003-003-025-4I-1 Mangum, B. W., Standard Reference Materials: SRM 1969: Rubidium Triple-Point - A Temperature Reference Standard Near 39.30 °C. NBS

Spec. Publ. 260-87 (December |983). SN003-003-

025-44-5

Gills, T. E., et al., 1982 Compilationof Elemental Concentration Data for NBS Biological,

Geological, and Environmental Standard

Reference Materials. NBS Spec. Publ. 260-88

(In Press).

* Send order with remittance to Superintendent

of Documents, US Government Printing Office Washington, DC 20402. Remittance from

foreign countries should include an additional one-fourth of the purchase price for postage

** May be ordered from: National Technical

Information Services (NTIS). Springfield

Virginia 22151.
CONTENTS

Page

Preface iii 1 . Introduction 2

2. Data Compilation 2

3. Discussion 3

4. Conclusion 3 5. References * v . 4

APPENDICES

APPENDICES

Page

Appendix

A NBS SRM 120A - Collected Data 44

AppendixB NBS SRM 120B - Collected Data 44

Appendix

C NBS SRM 1566 - Collected Data 46

AppendixD NBS SRM 1567 - Collected Data 48

Appendix

E NBS SRM 1568 - Collected Data 50

AppendixF NBS SRM 1569 - Collected Data 52

Appendix 6 NBS SRM 1570 - Collected Data 54

Appendix

H NBS SRM 1571 - Collected Data 59

Appendix I NBS SRM 1572 - Collected Data 80

Appendix

J NBS SRM 1573 - Collected Data 81 Appendix K NBS SRM 1575 - Collected Data 86

AppendixL NBS SRM 1577 - Collected Data 91 Appendix M NBS SRM 1621 - Collected Data .

107

Appendix

N NBS SRM 1621

A - Collected Data 107

Appendix 0 NBS SRM 1622A - Collected Data 107

AppendixP NBS SRM 1623 - Collected Data 107

Appendix

Q NBS SRM 1624 - Collected Data 108

AppendixR NBS SRM 1630 - Collected Data 108

AppendixS NBS SRM 1631

A - Collected Data 109

AppendixT NBS SRM 1631

B - Collected Data 109

Appendix

U NBS SRM 1631

C - Collected Data 109

Appendix

V NBS SRM 1632 - Collected Data 110

AppendixW NBS SRM 1632A - Collected Data 125

AppendixX NBS SRM 1633 - Collected Data 131

Appendix

Y NBS SRM 1633A - Collected Data 148

AppendixZ NBS SRM 1634 - Collected Data 153

Appendix AA NBS SRM 1635 - Collected Data 155

Appendix BB NBS SRM 1641 - Collected Data 159

Appendix CC NBS SRM 1642A - Collected Data 159

Appendix DD NBS SRM 1643 - Collected Data 159

Appendix EE NBS SRM 1643A - Collected Data 160

Appendix FF NBS SRM 1645 - Collected Data 161

Appendix GG NBS SRM 1646 - Collected Data 164

Appendix HH NBS SRM 1648 - Collected Data 165

Appendix II NBS SRM 1A - Collected Data 168

Appendix JJ NBS SRM IB - Collected Data 170

Appendix KK NBS SRM 278 - Collected Data 171 Appendix LL NBS SRM 4350 - Collected Data 173

Appendix MM NBS SRM 4350B - Collected Data 173

Appendix NN NBS SRM 4353 - Collected Data 174

Appendix 00 NBS SRM 610 - Collected Data 174

Appendix PP NBS SRM 612 - Collected Data 176

Appendix QQ NBS SRM 614 - Collected Data 176

Appendix RR NBS SRM 616 - Collected Data 177

Appendix SS NBS SRM 688 - Collected Data 177

Appendix TT NBS SRM 70 - Collected Data 179

Appendix UU NBS SRM 70A - Collected Data 180

Appendix VV NBS SRM 76 - Collected Data 181

Appendix WW NBS SRM 77 - Collected Data 182

Appendix XX NBS SRM 88 - Collected Data 182

Appendix YY NBS SRM 88A - Collected Data 183

Appendix 11 NBS SRM 91 - Collected Data 184

Appendix AAA NBS SRM 950A - Collected Data 185

Appendix BBB NBS SRM 97 - Collected Data 186

Appendix CCC NBS SRM 97A - Collected Data 188

Appendix DDD NBS SRM 98 - Collected Data 189

Appendix EEE NBS SRM 98A - Collected Data 192

Appendix FFF NBS SRM 99 - Collected Data ' 193

Appendix GGG NBS SRM 99A - Collected Data 195

Appendix HHH References for NBS SRM Collected Data 196

vi i i
LIST OF TABLES

Page

1. National Bureau of Standards Biological, Environmental, and Geological Standard Reference Materials 5 2. Literature Surveyed 7

3. Elemental Concentrations in NBS Oyster Tissue, Brewers Yeast, and Citrus Leaves Standard Reference

Materials 8

4. Elemental Concentrations in NBS Wheat Flour, Rice Flour and New Bovine Liver Standard Reference

Materials 9

5. Elemental Concentrations in NBS SRM 1570: Spinach 10

6. Elemental Concentrations in NBS SRM 1571: Orchard Leaves 12

7. Elemental Concentrations in NBS SRM 1573: Tomato Leaves 13

8. Elemental Concentrations in NBS SRM 1575: Pine Needles 15

9. Elemental Concentrations in NBS SRM 1577: Bovine Liver (Older) 17

10. Elemental Concentrations in NBS SRM's 610-616: Trace Elements in Glass 19

11. Elemental Concentrations in NBS Coal Standard Reference Materials 1630, 1632A, and 1635 21 12. Elemental Concentrations in NBS SRM 1632: Trace Elements in Coal 23

13. Elemental Concentrations in NBS SRM 1633: Coal Fly Ash (Older) 24

14. Elemental Concentrations in NBS SRM 1633A: Coal Fly Ash (Newer) 25

15. Elemental Concentrations in Newer NBS Silicate Rock, Sediment and Air Particulate Standard

Reference Materials 26

16. Elemental Concentrations and Uranium Isotope Ratios in Several NBS Standard Reference Materials ... 28

17. Elemental Concentrations in NBS Fuel Oil Standard Reference Materials 29

18. Elemental Concentrations in NBS Sulfur in Coal Standard Reference Materials 30

19. Elemental Concentrations in NBS Water Standard Reference Materials 31 20. NBS Environmental Radioactivity Standard Reference Materials 32

21. Elemental Concentrations in Various NBS Standard Reference Materials 33

22. Elemental Concentrations in Various NBS Standard Reference Materials 34

23. Elemental Concentrations in NBS Clay Standard Reference Materials 35

24. Elemental Concentrations in NBS Feldspar and Phosphate Rock Standard Reference Materials • 36

25. Analytical Methods Code 37

26. "Whole Rock" Concentration Summations of Major and Minor Elements in Coal and Fly Ash SRM's 39

27. Elemental Data Reported by Year 39

28. Distribution of SRM Data by Analytical Technique 39

29. Comment Codes for Appendix Tables 40

30. Multipliers Used for Oxide to Element Conversions 41

LIST OF FIGURES

Page

1. Summary of Elemental Measurements Reported in NBS Biological SRM's 1566-1577A 42

2. Summary of Elemental Measurements Reported in NBS Geological SRM's 278, 610-688 and 1630-1646 .... 43

ix

1982 COMPILATION OF ELEMENTAL CONCENTRATION

DATA FOR NBS BIOLOGICAL, GEOLOGICAL , AND ENVIRONMENTAL

STANDARD REFERENCE MATERIALS

Ernest S. Gladney, Colleen E. Burns, and Daniel R. Perrin

Environmental Surveillance Group, MS K-490

Los Alamos National Laboratory

Los Alamos, New Mexico 87545

Iwan Roelandts

Geologie, Petrol ogie et Geochimie

Universite de Lieqe

B-4000 Sart-Tilman par Liege 1 Belgium

Thomas E. Gills

Office of Standard Reference Materials

National Bureau of Standards

Washington, DC 20234

Concentration data on 88 constituents in 75 NBS Standard Reference Materials have been collected from over 850

iournal articles and technical reports. These data are summarized into mean values with uncertainties expressed

as +/- one standard deviation and compared with available certification data from NBS. Data are presented on the

analytical procedures employed and all raw data are given in the Appendices.

Keywords: Analytical methods, biological, certified, compilation, environmental, geological, information

values, literature values, mean values, Standard Reference Materials.

DISCLAIMER

Certain commercial equipment, instruments, or materials are identified in this report in order to adequately specify the procedure used for data compilation. Such identification does not imply recommendation or endorsement by

the National Bureau of Standards, nor does it imply that the materials or equipment identified are necessarily the

best available for the purpose.

1
1. Introduction

This compilation is a revised, updated, and expanded version of the first edition which appeared in 1980 (1). The

National Bureau of Standards (NBS) has produced over 60 Standard Reference Materials (SRM) for use in biological,

geological, and environmental analytical chemistry. The basic goal of the SRM program is to provide homogeneous

and stable materials of a variety of natural matrices, for use in technique development and in analytical quality

assurance. The function of standard reference materials in the latter role has received recent attention in a series of articles by Taylor (2-4). These standard reference materials carry the full legal weight and authority

of NBS and the U. S. Department of Commerce, as they have been specifically authorized by federal legislation.

The concentrations of as many as 39 constituents have been determined at one of two confidence levels in each SRM:

certified values and non-certified or informational values. The former is the present best estimate of the true

concentration of that constituent and is not expected to deviate from that concentration by more than the stated

uncertainty. These certified concentrations are determined at NBS or with cooperating laboratories using either a definitive method, two or more independent methods, or reference methods. These methods and other certification

criteria are carefully defined by Uriano and Gravatt (5). Constituent concentrations that are labeled as non-cer- tified or informational are those that NBS has not measured by either a definitive or reference method.

A limitation of many of these standard reference materials has been the restricted number of constituents that NBS can afford to certify in each material. Numerous investigators outside NBS have published concentration data on constituents in these reference materials. Although several brief review articles on NBS standard reference materials have appeared in the literature, we believe that the user should have access to both the summarized mean con- centrations and all the data on which they are based. This philosophy was the basis of the previous compilation

effort (1). Since no abstracting service has a category "standard reference materials", the widely scattered data

in reports, articles, books, and proceedings have been collected only with difficulty.

There has been continuing controversy among compilers concerning the determination and reporting of final compositional information on standard reference materials (6-12). Flanagan has used "recommended", "average", and "magnitude" to characterize his "estimates" for major components and trace elements (13). Abbey has coined the term

"usable value" for some of his results and pioneered the "select laboratories" approach to arrive at overall com- positional information (11,14). Gladney and Goode elected to report only "mean values" and associated standard

deviations without further attempt to assess the varying quality of data determined by different analytical techniques (1E>). For the French geostandards (CRPG, ANRT) , Roubault, et al . (16), have considered "recommended", "preferred", and "proposed" values depending on the degree of confidence one can attach to the data. Steele, et al

(17), have reported "recommended" values in the six NIMROC rock samples using some statistical methods. Gladney,

et al . (18), chose the term "consensus values" to describe their mean values calculated for USGS rocks after judgemental elimination of initial outliers.

Approaches to value judgement of data quality can be debated endlessly. The responsibility for the informed end

of these compiled data lies with the individual investigator. Each should read our methodology carefully so that

he may decide for himself its limitations. The values in the tables must not be used uncritically. All data behind our mean values are presented in the appendices so that any investigator may recalculate them to reflect his own experience whenever desired.

2. Data Compilation

A key to the 75 standard reference materials included in this document is provided in Table 1, along with certification and revised certification dates. All NBS certified and informational values for these standard reference

materials are reoorted in the individual mean value tables for ease of comparison. The certified values have un- certainties stated, while informational values do not.

The 54 major journals in analytical chemistry, qeoloqy, petroloqy, geochemistry, and environmental science that were surveyed are shown in Table 2. Less comprehensive coverage of books and institutional reports for 1972-1982

has been achieved. More than 850 different references containing original data on NBS materials were located. All

individual data, their uncertainties (where provided), their references, and the analytical techniques used are given in Appendices A through GGG.

All individual data thus located were assembled using a PDP-11/34 minicomputer with an RSX-11M (version 4.0) operating system, an RA-80 121 Mb fixed-media disc drive, three RL-02 10 Mb cartridge disc drives, and a Datatrieve-1

software package (all are registered trademarks of the Digital Equipment Corporation, Manard, Massachusetts).

Datatrieve-1 1 (version 2.0) is an interactive data storage and maintenance software system which provides facilities for selective data retrival, updating, sorting, formatting, and report generation with a minimum of programming overhead. Data were hand entered into the system via terminal keyboard from copies of the original papers.

Details of our Datatrieve-1 1 based data management system are being published elsewhere (19).

Data were first sorted by material, then constituent, and finally in ascending order of concentration for each con- stituent (this can be accomplished in a single operation within Datatrieve). Some subjective criteria, as discussed by Abbey (10), were used to eliminate data on either end of the reported concentration spectrum that we judged

to be beyond the limits of acceptability. Following these subjective eliminations (less than 0.5°/ of the total

data), an initial mean and standard deviation was computed using all remaining data for a given constituent in each

SRM by passing the Datatrieve ASCII output file through a program which encoded numerical values and performed mean

and standard deviation calculations.

All data points now outside +/- two standard deviations from the initial mean were dropped and a second mean and

standard deviation recomputed. These final means and associated standard deviations are reported in Tables 3 to 24 for up to 88 constituents. The number in parentheses following each entry indicates the number of literature

2
values used to calculate the final mean. Where sufficient data exist, the median was also determined using all

data other than "less-than" values.

The compiled data were then resorted first by material, then constituent, and finally by analytical method. An

iterative mean and standard deviation (using +/- 2s for elimination) were again calculated for groups of analytical

methods which had more than two data points (i.e., ITNA, IENA, RTNA, RENA, NAA, and DNA were all combined into NAA; WSRF, EXRF, and XRF into XRF, etc.). These analytical method means and standard deviations are also included in

the tables when sufficient data exist. The key for analytical methods codes is given in Table 25.

Mean values in Tables 3 to 24 which are based upon less than three data points do not include standard deviations

(e.g., B in 1566, Table 3). In a few cases the data reported had such a wide range as to render the mean +/- one standard deviation value meaningless. Such cases are reported as ranges only (no standard deviation specified).

Additionally, there are a few elements where only upper limit data exist, and these are given as limit values in

the tables (e.g., Be in 1570, Table 5).

3. Discussion

Our mean values for major and minor elements in standard reference materials can be subjected to two tests commonly

used by rock analysts. "Whole rock" summations can be calculated from elemental data when oxygen data are available, or the elements can be converted to stoichiometric oxides and then summed. The latter approach is inappropriate for coals, oils, biologicals, and non-silicate rocks where many elements are not in oxide forms. "Ironoxide compatabil ity" can also be determined when concentration data on the two forms of iron oxide have been established. Since we have not located any reports of oxygen determination in any of the biological standard reference

materials, the summation test cannot yet be applied. Furthermore, the absence of reported iron oxide data render

that test impossible. There is sufficient oxygen data on five coal and fly ash materials to attempt the "whole

rock" summation. It is important that all concentration data used are on a "dry-weight" basis. The large water

content of SRM 1635 makes its compiled data suspect in this regard. The results of this calculation are shown in

Table 26. Summations of 99 to 101% are considered a good indication that the major and minor element data are reasonably accurate and internally consistent. Three of the five materials investigated fall within this range.

The primary reason for the "high" values for 1632A and 1633 is the uncertainty in the carbon (+/- 4%) and silicon

(+/- 1.1%) mean values, respectively. In light of these uncertainties, their summations are also quite acceptable.

In the future it is hoped that good oxygen data will be available so that this approach can be applied to the biologicals. These calculations will be presented on other geological standard reference materials when the quantity

of data is sufficient.

The growth of the body of standard reference material data is shown in Table 27. A summary of total numbers of

elemental measurements reported in this compilation as a function of matrix is shown in Figs. 1 and 2 for biological and geological matrices. There are a total of 6088 reports for biological materials 1566 to 1577A, and a total

of 5105 reports for qeological and environmental materials 278, 610-617, 688, 1630-1635, and 1645-1646. A summary

of these two groups of data by general analytical method is given in Table 28. As seen in the first compilation

(1) neutron activation techniques continue to lead the field followed at some distance by atomic absorption.

The key to the analytical methods code (ANAL-METH) is given in Table 25. The key to the COMMENT code is given in

Table 29. All data reported as oxides in the original references were converted to elemental form using the con- version factors shown in Table 30. The individual data (C0NC), their uncertainties when provided (UNCER), analytical technique used (ANAL-METH), the exact data points eliminated during mean value calculations (* under COMMENT),

and the individual references are given in Tables A to GGG for each SRM. These tables were generated with the

Datatrieve-1 1 reDort writing facilities and the DEC Keypad editor, and printed on a Twintrack Qume printer. Data

which were reported as "greater-than" values have not been included, and "less-than" values are shown as a blank

under concentration with the upper limit given as the uncertainty and with L* under COMMENT. The data have been

sorted in ascending order based upon material, constituent, and concentration using Datatrieve-1 1 . All the references (REF-C0DE and REF-NUM) have been coded and identified in Table HHH. The code consists of the last two digits

of the year of publication plus the first three letters of the first author's last name. The two digit numerical

suffix is provided to enable handling of multiple reports by the same first author in the same year. This particular reference coding system was adopted in preference to sequential numbering used in the first edition (1) to permit rapid searching of the reference file using Datatrieve-1 1 and to permit easy updating of both the reference

and data files without the necessity of renumbering the references. Since over 3400 references with data on various NBS, USGS, and CCRMP materials are now in our system, these considerations are extremely important.

4. Conclusion

Although we have endeavored to achieve as wide a coverage of the literature as possible, we realize that this com- pilation is incomplete. We request that the users of this compilation call our attention to errors or omissions

and they will be corrected or included in future editions. Any investigators with unpublished results on NBS,

U. S. Geological Survey (USGS), or Canadian Certified Reference Materials Project (CCRMP) reference materials are urged to send their data to the first author and it will be placed in our computer data base with appropriate ref- erence to the source.

We are indebted to all the compilers of reference materials data who have preceeded us. We especially thank Sydney

Abbey (Geological Survey of Canada) who has maintained a voluminous correspondence with the first author on various

aspects of data compilation. Our effort has greatly benefited from his willingness to share his experience and his

informed criticism. We also thank William Goode (DEC) who helped us establish our original data management framework and Kathy Derouin (Los Alamos Group HSE-8) who was instrumental in producing the large mean value tables.

This work was performed under the auspices of the U.S. Department of Energy and the U.S. National Bureau of

Standards

3
REFERENCES

1. Gladney, E. S., "Compilation of Elemental Concentration Data for NBS Biological and Environmental Standard

Reference Materials", Los Alamos Scientific Laboratory Report LA-84 38-MS, 1980.

2. Taylor, J. K., Anal. Chem., 53: 1588-1596A (1981).

3. Taylor, J. K., "Reference Materials - How They Are, or How They Should be Used", Presented at the ASTM C-26

meetinq, Knoxville, Tn., 1982.

4. Taylor, J. K. , Anal. Chem., 55: 600-608A (1983).

5. Uriano, G. A., and C. C. Gravatt, Crit. Rev. Anal. Chem., 6: 361-411 (1977).

6. Flanagan, F. J., Geochim, Cosmochim. Acta, 37: 1189-1200 (1973).

7. Abbey, S., ibid., 39: 535-537 (1975).

8. Flanagan, F. J., ibid., 39: 537-540 (1975).

9. Abbey, S., Geostandards Newsletter, 2: 141-146 (1978).

10. Abbey, S., X-ray Spect., 7: 99-121 (1978).

11. Abbey, S., R. A. Meeds, and P. G. Belanger, Geostandards Newsletter, 3: 121-133 (1979).

12. Abbey, S., ibid., 6: 47-76 (1982).

13. Flanagan, F. J., "1972 Compilation of Data on USGS Standards", in Descriptions and Analyses of Eight New USGS

Rock Standards, US Geological Survey Professional Paper 840: 131-183 (1976).

14. Abbey, S., "Standard Samples of Silicate Rocks and Minerals: A Review and Compilation", Geological Survey of

Canada, Paper 72-30 (1972).

15. Gladney, E. S., and W. E. Goode, Geostandards Newsletter, 5: 31-64 (1981).

16. Roubault, M., H. de la Roche, and K. Govindaraju, Sciences de la Terre, Nancy, XI: 105-121 (1966).

17. Steele, T. W., A. Wilson, R. Goudvis, P. J. Ellis, and A. J. Radford, Analyses of the NIMR0C Reference Samples

for Minor and Trace Elements, National Institute for Metallurgy Report 1945, 222 pp.

18. Gladney, E. S., C. E. Burns, and I. Roelandts, Geostandards Newsletter, 7: 3-226 (1983).

19. Gladney, E. S., D. R. Perrin, C. E. Burns, and W. E. Goode, "Data Base Design Geological Reference Materials",

Los Alamos National Laboratory report, in preparation (1983).

4
TABLE 1

NATIONAL BUREAU OF STANDARDS BIOLOGICAL, ENVIRONMENTAL,

AND GEOLOGICAL STANDARD REFERENCE MATERIALS

SRM NUMBER NAME CERTIFICATION DATE

1A Argillaceous Limestone 1931

lb Argillaceous Limestone 1966

lc Argillaceous Limestone 19 78

70 Feldspar 1926

70a Fel dspar 1981

76 Burnt Refractory 1927 , 19 55

77 Burnt Refractory

88 Dolomite 1 Q?ft

88A Dolomite Limestone 171Q&70/ ,171QR?OL 91 Opal Glass 17 J

97 Flint Clay 117O J\ 11 97A Flint Clay 1969

98 Plastic Clay 1931

98A Plastic Clay 1969

99 Soda Feldspar 1931

99A Feldspar 1981

120A Phosphate Rock (Florida) 1961

120B Phosphate Rock (Florida) 19 72,1979

278 Obsidian Rock 1981

610 Trace Elements in Glass (500 ppm) 19 70.1972

612 Trace Elements in Glass (50 ppm) 1970 1972 1982

614 Trace Elements in Glass (1 ppm) 1970 1972 1982

616 Trace Elements in Glass (0.02 ppm) 1Q7fi 17 / W 1Q7? 19ft? s 1 7 / i j 17 688 Basalt Rock 1981

950A Uranium Oxide 1961

9 50B Uranium Oxide 1981

1566 Oyster Tissue 1979,1983

1567 Wheat Flour 1978

1568 Rice Flour 1978

1569 Brewer's Yeast 1976

1570 Trace Elements in Spinach 19 76

1571 Orchard Leaves 1971,1976,1977

1572 Citrus Leaves 1982

1573 Tomato Leaves 19 76

1575 Pine Needles 1976

1577 Bovine Liver 1972,1977

1577a Bovine Liver 1982

1619 Sulfur in Residual Fuel Oil 1981

1620a Sulfur in Residual Fuel Oil 1981

1621 Sulfur in Residual Fuel Oil 1967

1621a Sulfur in Residual Fuel Oil 1980

1621b Sulfur in Residual Fuel Oil 1981

1622a Sulfur in Residual Fuel Oil 19 79

1622b Sulfur in Residual Fuel Oil 1981

1623 Sulfur in Residual Fuel Oil 1971

1623a Sulfur in Residual Fuel Oil 1981

5
TABLE 1 (Cont)

SKM NUMBER NAME CERTIFICATION DATE

1624 Sulfur in Distillate Fuel Oil 19 71 1624a Sulfur in Distillate (Diesel) Fuel Oil 1981

1630 Trace Mercury in Coal 1971

1631A Sulfur in Coal 19 73,19 74 1631B Sulfur in Coal 19 73,19 74 1631C Sulfur in Coal 1973,1974

1632 Trace Elements In Coal 19 74 1632A Trace Elements in Coal (Bituminous) 1983

1633 Trace Elements in Coal Fly Ash 1975

1633A Trace Elements in Coal Fly Ash 19 79

1634 Trace Elements in Fuel Oil 1975

1634A Trace Elements in Fuel Oil 1982

1635 Trace Elements in Coal (Subbituminous) 19 78

1641 Mercury in Water - Concentrate 1975

1642 Mercury in Water - Trace 1974

164 2A Mercury in Water - ng/ml 1977

164 3 Trace Elements in Water 1977

164 3A Trace Elements in Water 1980

164 5 River Sediment 1978

1646 Estuarine Sediment 1982

1648 Urban Particulate Matter 19 78

1649 Urban Dust/Organics 1982

2682 Sulfur in Coal 1982,1983

2683 Sulfur in Coal 1982,1983

2684 Sulfur in Coal 1982,1983

2685 Sulfur in Coal 1982,1983

4350 Environmental Radioactivity Standard:

River Sediment 1975

4 35 OB Environmental Radioactivity 1981

4353 Environmental Radioactivity 1981

6
TABLE 2: LITERATURE SURVEYED

JOURNAL VOLUME NUMBERS

Analysis 1 _ 10

Analys t 97 _ 107

Analyt ica Chimica Act a 53 14 3 Analvt ical Chemi s trv 44 54 Analvt iral Letters 1 15

Anal vf irn1 PrnrppHI n^Q Published bv the Roval SocietV

ofvl f!npm1 VLI will 1 fttrv O L. L Jf\ London^ LIUUUU LI / 17 19 Annales de la Soclete Geologique de Belgique 91 105

Ann! 1 &A Rna r» t* Ton f or> v 25 36

Atoml r Anctomtion Newsletter 1 18

Atomic Spect rose op

y

1 3 Bio lof?i pal Trare E letne nt Research 1 _ 4 Bulletin des Sorl ptp<? Chlminnes Belt?es 80 _ 90

flflnaHl an Tonfnal of Fafth pnppo 9 19 f!anad^ \ja iiau iui! an ijuui TonTnal iiax ofv> jl 'JnpptrnQrrtnv u pc ll i uo »j ij y 20 27

Chemi ral GpoIopv 13 _ 37 Comptes-Rendus Hebdomadal res des Seances de l'Academie

des Sciences (Paris) 272 292

Contributions to Mineralogy and Petrology 36 80

Earth and Planetary Science Letters 1 61 Environmental Letters 1 10

Environmental Pollution 1 _ 29

Environmental Research 1 28

Environmental Science and Technology 5 _ 16

Fresenius' Zeitschrift fur Analytische Chemie 244 313

Geochemistry International (translations from Geokhimiya) 9 18

Geophysical Research Letters 1 9 Geochimica et Cosmochimica Acta 36 _ 46

Geostandards Newsletter 1 _ 6 Geochemical Journal 7 16

International Journal of Applied Radiation and Isotopes 23 33

International Journal of Environmental Analytical Chemistry 1 International Journal of Environmental Studies 1 J.147 Journal of Analytical Chemistry of USSR (translations of

Zhurnal Analiticheskoi Khimii) 26 _ 36

Journal of Environmental Quality 1 11 Journal of Environmental Science and Health 11 17 Journal of Geochemical Exploration 1 17 Journal of Petrology 12 23

Journal of Radioanalytical Chemistry 10 _ 72

Journal of Research of the USGS 1 _ 6 Journal of the Association of Official Analytical Chemists 55 _ 65

Journal of the Geological Society (London) 127 138

Journal of Volcanology and Geothermal Research 1 14 Lithos 4 15

Marine Geology 12 44

Microchemical Journal 17 27

Mikrochimica Acta (Wien) 1972 1982

Mineralogy Magazine 40 46

Nuclear Instruments and Methods 114 172

Precambrian Research 1 18

Proceedings of the Analytical Division of the Chemical

Society (London) 11 16

Radio chimica Acta 17 31

Radiochemical and Radioanalytical Letters 1 54 Sedimentology 16 28

Talanta 19 29

X-Ray Spectrometry 1 11

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TABLE 6

ELEMENTAL CONCENTRATIONS IN NBS SUM 1371: ORCHARD LEAVES

Literature

•Only t

••Only (

Sb

Sc

St

SiSm

Tb

Tc

Tm

U

V

Zn

Zr

IndMdual t by Analytical Technique

Element Units (!«") a ± s (n) Median Range AA ICPES NAA OES PA A XRF Ottan

A| ppb 210 t 330 13) 13 620

Al ppm 320 1 110 (41) 347 99 824 230 ± 1 10 (5) 390 ±60 (19) 200 ± 60 (10) As ppm 10 ±2 10.7 i 1.2 (I2S) 10.5 1.10 38 10.7 ± 1.2 (34) 10.4 ± 1.6 (8) 10.7 ± 1.2 (59) 10 1 ± 1.2 (5) 12.1 1 2.2 (8) 10.9 ± 1.7 (4) COLOR

As llll) ppm 4.9 (1)

At) ppb 1-4 ± 0.4 (13) 1.3 0.78 3.5 1.4 ± 0.4 (3) B ppm 33 i 3 33 i 4 (29) 32.9 . 16 40 33 ± 5 (6) 32 ± 5 (II) 35.3 ± 15 (4) CPAA

Bi ppm 44 43 1 5 (29) 43 0.3 80 45 ± 6 (3)' 42 ± 9 (21) 44 ± 5 (5) Be ppb 27 i 10 24 1 10 (S) 30 13.7 110

Bi ppb 100 92 ± 36 (4) 110 4 64000 110 (3)b POL

Be ppm 10 9.5 1 I.I (46) 9.4 5.0 34 9 7 ± I I (37) 8.2 1 1.3 (9) C % 46.2 ± 0.5 (5) 46.2 45.76 52.0 46.0 ± 0.3 (3) CB

Ca % 2-09 ± 0-03 2.04 ±0.11 (72) 2.04 1.58 5.01 2.04 ± 0.05 (7) 2.04 ± 0.07 (10) 2.03 ±0.13 (22) 2.01 t 0.22 (12) 2.06 ±0.11 (4) 2.02 ± 0.09 (9) 1.99 (2) CPXRF

Cd PPb I10± 10 1 18 ± 24 (57) no 70 2000 119 ± 30 (35) 162 ± 29 (5) 122 ± 31 (13) 129 ± 35 (3) AF

Ce ppm 0.94 ± 0.09 (II) 0.97 0.75 1.2 0.92 ± 0.08 ( 10) CI ppm 690 730 ±40 (31) 730 53 950 730 ± 40 (19) 710 ± 20 (3) 780 ± 20 (3) Co ppb 200 160 ± 40 (38) 180 100 460 180 ± 70 (5) 170 ± 50 (35) Cr Ppm 2.6 ± 0.3 2.5 ± 0.3 (67) 2.6 1.07 5.81 2.5 ±0.3 (15) 2.6 ± 0.6(7) 2.6 ± 0.4 (38) Cs ppb 40 35 ±8 (13) 38 20 150 3B ± IS (13) Ca Ppm 121 1 12.1 ± 1.4 (113) 12 3.6 35 11.9 ±0.7 (30) 118 ± 0.6 (12) 11.9 ± 1.6 (29) 14.8 ± 2.4 (12) 11.7 1 2.8 (14) 11.9 (1) ASV

Dy ppb 80 (2) 53 110

El PPb 30 (1) Eu ppb 23 ± 3 (13) 25 20 300 24 ±3 (14) F ppm 4 3.9 ± 0.5 (9) 394 3.12 10 3.41 (2) COLOR

Fe Ppm 300 i 20 284 ± 28 (109) 289 121 884 270 ± 30 (17) 280 ± 20 (14) 290 ± 20 (37) 230 ± SO 112) 320 ± 20 (3) 290 ± 30 (16) 280 ± 20 <3) COLOR

Ct ppb 80 88 ± 9 (4) 78 100 88 ± 9 (4) Cd PPb 67 ± 56 (3) 1.6 100

46.5 (2) TCGS

100 (I) ASV

II .8 ±0.8 (3) POL*

13.0 ± 3 IS) CPXRF

4.1 ±0.02 (S) 1SE

312. (3) POL1

300 ± 130 14) CPXRF

) analysis reporting

: analyst reporting Ce ppb ISO (1) H % 5.84 ±0.26 (5) 5.91 5.S4 6.10 Hf ppb 26 ± 9 (5) 27 13 37 26 ± 9 (5) He ppb 155 1 IS 155 ± 15 (72) 157 no 305 IS4 ± 13 (30) 162 ± 22 (41) 133 (2) IDMS

Ho

I

ppb

ppb 170

16 (2) 165 ± 40 (9) 173

13- 100

20220 184 ± 21 (7)

1 129 (Ci/8 0.006 (1) In PPb 1.5 ±0.3 (3) 1.23 1 80 1.3 ± 0.3 (3)

Ir ppb 15 (1) K % 1.47 ±0.03 1.43 ±0.07 (67) 1.45 1.05 3.89 1.41 ± 0.05 (7) 1.48 ±0.05 (6) 1.4S ± 0.05 (29) 1.38 ±0.16 (12) 1.57 ±0.14 (9) Li PPm I. II ± 0.13 (21) 1.15 0.70 196 1.07 ±0.16 (19) u ppb 600 710 ± 120 (3) 770 510 13700 Ly PPb 4 ± 4 (5) 3.3 0.61 10 2.8 ± 2.2 (5) Mb ppm 6200 ± 200 6100 ± 400 (52) 6100 4900 7830 5800 ± 300 (8) 6000 ± 400 (10) 6200 ± 400 (17) 6400 ± 400 (12) 6120 ± 30 (4) Mn PPm 91 ±4 89 ± 6 (97) 89 23.1 - 242 88 i 3 (16) 86 ±3(11) 89 ± 7 (35) 89 ± 20 (11) 94 ± 3 (5) 85 ± 17 (16) 91 ± 7 (4) CPXRF

Mo PPb 300 ± 100 280 ± 70 (15) 320 110 15200 200 ± 60 (5)* 290 ± 40 (8) 7000 ± 5000 (6) N * 2 76 ± 0.05 2.72 ±0.05 (16) 2 71 2.59 - 2 81 2.73 ± 0.02 (6)4 N IS A% 0.367 (1) Na ppm 82 ± 6 88 1 14 (37) 86 40 524 87 ± 12 (26) 190 ± 170 (8) 84 ± 4 (3)4 Nb ppb <300(l) Nd ppb 460 ± 130 (3) 320 570 490 ± 140 (3)" Ni PPm 1.3 ±0.2 1.3 ± 02 (42) 131 0.7 4.3 1.6 ± 0.9 (10) 1.5 ± 0.4 (6) 1 4 ± 0.3 (10) 1.4 ±0.1 (3) 1.3 ±0.1 (5) 1.3 ±0 1 (3) COLOR 1.4 (3) POL

2.1 ± 1.2 (3) CPXRF

P PPm 2100 ± 100 2030 ± 140 (401 2000 1400 3100 2040 ± 90 (6) 1980 ± 100 (10) 2050 ± 50 (5) 1900 ± 300 (10) 1900 1 100 ( 3) COLOR 2120 ± SO (4) MM

Pb ppm 45 ± 3 45 ± 3 (84) 45 IS 115 45 ± 3 (41) 44 ± 2 (9) 43 ± 2 (5) 46 ± 4 (5) 46 ± 4 (10) 46 ± 1 (4) ASV 44 i 1 (6) POL

Pd ppb <1 (1) Pr PPb 130 ± 90 (3) 60 230 - 190 ± 70 (3)"

Pi PPb 650 (2) 89 1200 11-2 ± 0.8 (33) 12.7 10.3 (3) 11.0 ±0.6 (10) 12 ± 2 (4) CPXRF

Rb ppm 12 ± 1 11.3 ± 0.9 (50) 11.28 5.0 30 S ppm 1900 2100 ± 300 (14) 2140 1400 7020 2200 ± 300 (5)

ppm

ppb

PPb ppm

ppb

ppb PPm

PPb

ppb

PPb

ppb ppm

ppb

ppb ppb

PPb

ppb

PPb

PPb ppm

PPm

2.9 ± 0.2 (54)

61 ± 14 (22)

81 ± 11 (76) 550 ± 1 10 (6) 113 ± 20 (16) 300 ± 70 (6) 37 ± 4 (39) 8 ± 2 (4) 14 ± 3 (6)

II (I) 55 ± 8 (9) 24 ± 9 (7) 190 ± 110 (3)

7 (2) 29 ±2 (17) 510 ± 110 (34)

18 (2) 480 ( I

)

25 ±9 (7) 25.7 ± 2.4 (135)

2.4 , 10 (5)

304

36.5

29 530

I.I • 5.1 40 - 220

24 1 100 476 2340

16 320

180 4100

14.5. 118

5 10

1.23 80

6.6-90

2.4 - 191 74 300

3.7 • 10 18-56

140 2200

16 20

1 1

- 40 12-81

1.3 210

2.9 ± 0.4 (II)

79 ± 25 (17)

2.6 ± 0.3 (3)

36 ± I (5)

25 ± 2 (16)

2.9 ± 0.3 (4) 62 ± 14 (21) 84 ± 14 (43) 640 ± 230 (5) 112 ± 18 (14)

38 ±4 (13) 8 ± 2 (4) 13 ± 3 (7)

55 ± 8 (9) 70 ± 70 (5)

2B ± 4 (13) 520 ± 120 (28)

26 ± 9 (7) 26 ± 2 (42)

84 ± 5 (9) FLUOR

35 ± 3 (3) CPXRF

77 ± I (3) GC4

28 ± 3 (3) b

30 ± 16 15) CPXRF

12
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22
ELEMENTAL CONCENTRATIONS IN NBS SRM 1632: TRACE ELEMENTS IN COAL

Liirriturt

j^gg

Individual Mora by Analytical Technique

Element Units (1974) ~i ± (n) Median Range AA ICPES NAA PAA XRF Other*

Ag ppb £100 63 ± 13 (5) 65 55 ± 9 (3) Al % 1.73 ±0.11 (28) 1.74 LSI 3.00 1.71 (2) 1.72 ±0.12 (5) 1.76 ± 0.15 (21) As ppm 5.9 ± 0.6 5.8 ± 0.5 (48) 5.8 3.0- 8.9 5.9 ± 0.6 (5) 5.9 (2) 5.7 ± 0.6 (29) 6.0 ± 0.3 (6) 4.8 ± 1.8 (3) 5.4 (1) COLOR

ASH N 13.2 (1) Au

B

ppb ppm58 ± 90 (6) 41 ± 8 (7) 43

0.8529-200

118 45 ± 3 (5) TCOS

Ba ppm 330 ±37 (31) 314 87 - 410 331 ± 32 (25) Be Ppm 1.5 1.62 ± 0.11 (10) 1 64 1.2- 1.85 1.6 ±0.1 (6) 1.8 ± 0.1 (3)" 1.7 (1) I.S (1) FLUOR

Bi ppm 1.05 (1) ._

Br ppm 17.7 ± 1.8 (27) 18 7.8- 38 18 ± 2 (24) 20 ± 3 (3) C % 70.4 ± 1.8 (4) 70 68.93 73.0 71.0 ± 1.7 (3) TCGS

Cl ppm 4200 t 500 (26) 4200 2400- 7000 4400 ± 400 (5)a 4000 ± 600 (16) Cd PPb 190 ± 30 220 ± 40 (24) 210 170 700 230 ± 15 (7) 215 (2) 205 ± 24 (6) 310 (1) IDMS 270 ± 120 (3) SSMS

187 ± 12 (3) TCGS

Ce ppm 21 ± 2 (22) 20 17.3 - 30 20 ± 2 (17) Cl ppm 880 i 70 (26) 890 80 1177 880 ± 70 (2) _. 895 (2) TCGS

Co ppm 6 5.6 ± 0.5 (33) 5.7 3.9 11 6. 1 ± 0.8 (3) 4.9 ±0.9 (3)" 5.8 ± 0.5 (28) Cr ppm 20.2 t 0.5 19.9 ± 1.3 (37) 20 8

- 35 20.3 ± 1.4 (6) 18 ± 3 (3)" 20.2 ± 1.8 (26) Cs ppm 1.52 ±0.19 (24) 1.46 0.35 3.5 1.6 ± 0.4 (24) Cu ppm 18 ± 2 18 ± 2 (28) 17.8 13- 30 18.3 ± 1.8 (7) 18 1 ±0.9 (3)" 15.8 ± 1.5 (6) 28 ± 4 (3)b 18 ± 3 (6) 16.7 ± 1.7 (3) SSMS

Dy ppm 1.25 ±0.22 (10) 1.3 0.57- 2.4 I.I ± 0.3 (9) Er ppm 0.7 (1)

Ell ppb 355 ± 44 (23) 365 210- 500 350 ± 50 (20) F ppm 76 ± 16 (7) 80 51 - 100 76 ± 10 (4) ISE Fe Ppm 8700 ± 300 8600 ± 400 (38) 8600 6500 11300 8700 ± 400 (4) 8400 ± 400 (5) 8600 ± 600 (25) 7700 ± 700 ( 4) ... Gi ppm 5.8 ± 1.1 (16) 5.8 4.5 9.0 5.5 ±0.9 (11)

... _

"Only two analysts reporting. "Only one analyst reporting. Gd ppm ^ 1 j. 1 n /fit £. S ± 1 u (0) 2.35 3.Z x \J.O (J~ Ge ppm 1 A j. ft A IA\ i.O ± liA (4) 2.9 2 70 H % A 1ft . ft I A /It 4. 2U ± 0.16 (3) 4.0 4.30 aii ..I., /it xr^r^c a. 11 clf.lo (J) 1 t.u5 H2O-T % 2.6 (1) Hf 0.98 ± 0.10 (19) 0.96 0.72 1.53 ... 0.96 ±0.11 (19) Hg ppb 130 t 30 120 ± 23 (19) 120 88 950 117 ± 15 (7) 160 ± 50 (II) 100 Or9 Ho

1

ppb PPm243 ± 6 (3)

3.1 ± 0.3 (11) 3.3

240

2.68

250

6.63 — 3.8 ± 1.5 (10)

In ppb 1 10 ± 90 (12) 63 17 230 37 ± 33 (7) 210 (2)

Ir ppb 2.8 ± 0.6 (3) 2.48 3.53 - ... K ppm 2810 ± 140 (32) 2800 2500 4000 2800 ± 200 (5) 2900 ± 200 (23) La ppm 10.4 ± 0.8 (26) 10.5 6.0 11.5 10.5 ± 0.9 (21)

Li PPm 26 ± 2 (3) 24 29 Lu PPb 128 ± 17 (13) 130 100 416 137 ± 28 (12) ... Mg ppm 1600 ± 400 (24) 1600 980 8200 1400 ± 200 (5) 1800 t 500 (16) Mn ppm 40*3 41 ± 3 (41) 41.1 28 47 39 ± 2 (5) 44 ± 2 (3)* 42 ± 2 (25) 38 t 1 (4) Mo ppm 0.29 ± 0.08 (6)

3.8 ± 0.8 (10)

0.30

3.5

0.20 5.0 4.0 (2r 3.3 ± 1.7 (6) 0.26 ± 0.05 (Sf

N % 1.27 ± 0.06 (3) 1.2 1.3 _. 1.27 ± 0.06 (3) TCGS

Na PPm 377 ± 26 (32) 380 325 1200 ... 380 ± 30 (5)" 380 ± 30 (23) Nb ppm 5 (1) ._ Nd PPm 8.8 ± 1.8 (7) 9.5 6.4 17.8 12 ±5 (5) Ni PPm IS i 1 15 ± 2 (37) 15 10 20.4 15.1 ± 1.4 (4) 17 ± 2 (3)" 16.2 ± 3.3 (12) 13.9 ± 0.2 (5) 14 ± 3 (5) 14.7 ± 0.1 (3) IDMS

14.8 (1) POL

15.3 (2) SSMS

O % 15.05 (1) Os ppm < 1 (1) P ppm 150 ± 70 (9) 138 71 270 126 ± 32 (4)* 260 (2) COLOR

Pb ppm 30 ±9 28 ± 4 (28) 28 12 33 28 ± 3 (8) 21 ± 6 (4)» 30 ± 2 (7) 25 ± 8 (4) 28.7 (2) IDMS

28.4 (1) POL

30 ± 3 (3) SSMS

Pd ppb <5 (1) -

Pr PPm 3.4 ± 1.3 (3) 2.C 4.6 -

Pt ppb 230 (2) I8t - 270

20 ± 3 (22) Rb ppm 20 ± 3 (29) 20 IC -30 23 ± 5 (4) ._

fill ppm <5 (1) Ru ppb 18 (1) S H 1.19 ±0.20 (7) 1.29 0.17-2.02

3.4 ± 0.6 (26)

1.32 1.30 ± 0 02 (3) TCGS

Sb PPm 3.5 ±0.5 (31) 3.3 0.6 -6.4 3.6 ± 0.5 (3)"

Sc ppm 3.78 ± 0.22 (25) 3.8 3.4 • 5.4 3.8 ±0.3 (21) 3.00 ± 0.01 (5f Se

Si

ppm %

2.9 ± 0.3 3.0 ±0.3 (41) 3.0 1. -5.5 2.3 (2) 3.18 ± 0.03 (4)b

3.1 ±0.4 (28) 3.6 ± 1.3 (4) 3.05 (1) ASV

3.2 3.17 ±0.16 (8) 3.14 2.1 • 3.92

1.6 ±0.2 (18)

2.95 (2) TCGS

Sm ppm PPm

1.58 ±0.19 (22) 1.6 1.3-2.9

10.2 ± 0.4 (5)" Sn 8.8 ± 2.4 (10) 10 2.0- 125 7.2 ± 2.9 (3)"

Sr PPm 145 ± 24 (30) 148 1.0 280 140 (1) 144 ± 29 (23) 150 ± 5 (4)

Ta ppb 250 ±40 (17) 250 1 70 - 460 260 ± 50 (17) n ppb 270 ± 80 (9) 245 30-5O0 270 ± 80 (9)

Te ppb <IO0 710 ± 280 (3) 500- 1020

3.2 ± 0.5 (20) Th ppm 3.0 3.2 ± 0.2 (22) 3.2 1.3-4.7

Ti PPm

ppb

800 940 ± 110 (35) 938 680- 1550 840 ± 170 (3) 954 ± 16 (S) 1000 ± 140 (19) 920 ± 40 ay

n 590 ± 30 550 ± 50 (8) 555 500 610 530 ± 40 (sy 600 ± 10 (3) SSMS Tm ppb ppm

ppm

ppb PPm

240 ± 1 10 (3) 110 300

1.37 ±0.13 (20) 1.42 ±0.13 (5)° U 1.4 i 0.1 1.37 ± 0.13 (29) 1.4 0.98 - 6.0 35 ± 3 (3)a

1.41 (2) GAMMA 1.21 (2) IDMS

Vw

35 ±3 35 ± 2 (32) 740 ±60 (11)

35 750

24 50 450- 1900

37 ± 4 (5) 35 ± 3 (22) 700± 100 (11)

Y 7.6 ± 0.4 (5) 7.6 7.0 • 8.0 800 ± 140 (17) Yb ppb ppm

790 ± 140 (21) 790 550- 1200

36 ± 2 (6) Zn 37 ±4 37 ± 3 (45) 37.5 30-58 38.4 ± 0.7 (6) 38 ± 2 (3)» 38 ± 6 (20) 37.6 ± 1.2 (6)

1 Zr PPm 34 ± 10 (10) 38 1.56 90 25 (1) 55 ± 26 (6) 36 (2)

23
TABLE 13

ELEMENTAL CONCENTRATIONS IN NBS SRM 1633: COAL FLY ASH (OLDER)

Literature

Individual Meani by Analytical Technique

Element Units (1973) ~i ± • (n) Median Range AA ICPES NAA PAA XRF Others

Ag ppb

-

640 ± 590 (3| 258 1320

Al % 12.6 ± 0.5 (33) 12 6 10.4 14.3 13.0 ± 0.7 (4) 12.5 ± 0.6 (4) 12.6 ± 0.8 (22) 11.7 (1) 13.2 ± 0.7 (3) OES 12.3 ± 0.2 (3) TCGS

As PPm 61 t 6 61 ± 4 (54) 60 46 72 60 ± 5 (5) 56 ± 1 (3) 60 ± 5 (32) 62 ± 2 (9) 64 ± 2 (3) ._ Au ppb — 5.2 ± 2.6 (3) 2.75 1700 6 ± 3 (4) B ppm 440 ± 60 ( 10) 438 100 500 470 ± 30 (5) TCGS

Ba ppm 2650 ± 150 (41) 2630 1800 3400 2600 ± 300 (3) 2600 (2) 2700 ± 200 (33) 2603 ± 6 (3)« 2400 ± 400 (4) Be ppm 12 12.1 ± 0.8 (15) 12 5 14 12.4 ± 0.5 (11) 1 1.5 ± 1.0 (3)

Bi ppm 0.89 (2) 0.7 1.08 — ~

Br ppm 8.4 ± 2.2 (22) 7.7 5.8 12.1 ... 8.6 ± 2.3 (20) ... C % 3.3 ± 0.2 (3) 3.05- 3.45 ... Ca % 4.6 ± 0.3 (40) 4.62 3.50- 5.30 4.5 ± 0.4 (3) 4.64 ± 0.12 (4) 4.5 ± 0.3 (19) 4.7 ± 0.5 (6) 4.7 ± 0.6 (3) TCGS

Cd ppm 1.45 ± 0.06 1.46 ± 0.14 (33) 1.5 0.93- 15 1.46 ±0.16 (13) 155 (2) 1.36 ± 0.20 (5) 1.35 ±0.17 (6) 1.85 (1) 1DMS

1.50 (1) POL 1.53 ± 0.06 (3) TCGS

Ce ppm 149 ± 7 (26) 149.6 125 • 210 150 ± 12 (24) 154 ± 6 (3) 153 ± 1 (4)b TCGS

CI ppm 35 ± 17 (13) 40 19.6 185 ... ... 39 ± 14 (10) 23 ± 3 (3)» Co ppm 38 40 ± 2 (37) 40.1 26- 50 39 ± 4 (5) 36 ± 9 (3) 40 ± 2 (26) 40 ± 3 (5)b Cr ppm 131 ± 2 128 ± 8 (50) 130 112 180 130 ± 5 (8) 122 ± 8 (3) 128 ± 7 (27) 135 ± 6 (5)b 131 ± 17 (5) Cs ppm 8.6 ± 0.7 (24) 8.35 0.63- 13.8 8.4 ± 1.0 (26) 6 ± 4 (3)» . —

Cu ppm 128 ± 5 129 ± 7 (33) 129 70- 198 127 ±4 (10) 128 ± 8 (3) 128 ± II (7) 138 ± 3 (3)a 129 ± 5 (6) 135 ± 9 (3)b TCGS

Dy ppm 10 ± 1 (9) 10.2 7.6- 19 10.0 ± 1.2 (10) ...

Er ppm II (1) ...

Eii ppm 2.6 1 0.2 (22) 2.58 1.9- 5.3 2.6 ± 0.3 (22) ... _. F ppm 15 (2) 10 20 ~

Fe % — 6.14 ± 0.24 (50) 6.20 4.23 7.0 6.3 ± 0.4 (7) 6.2 ±0.2 (5) 6.2 ± 0.4 (27) 5.4 ± 1.0 (5) 6.10 ± 0.12 (7) 5.9 ± 0.3 (3) 6.3 ± 0.4 (3) TCGS

Ga ppm 42 t 4 (15) 42 40 ± 3 (10) 43 ± 5 (3) Od ppm 11.6 ±0.5 (4) 118 11 - 23 _. Gc ppm 22 ± 4 (4) 25 19 476 — — -

H ppm 1 100 (2) 1000 - 1200 H2 0- % 0.03 (1)

... ... H2OT % 0.17 (1) — ... — —

Hf ppm 7.6 ± 0.5 (20) 7.62 6.5 - 10.8 ... 7.5 ± 0.5 (23) — ... Hg ppb 140 ± 10 136 ± 17 (14) 141 100 -

1 1000 130 ± 9 (4) 145 ± 12 (7) 160 ± 30 (6)b Ho ppm 2.5 ± 1.0 (3) ... ... ...

1 ppm 2.7 ± 0.4 (5) 2.9 2.0 - 3.0 ... — 2.7 ± 0.5 (4) —

In ppb 220 t 80 (10) 280 118- 3000 210 ± 90 (10) 287 ± 6 (3)»

Ir ppb 15 18600 18 ± 2 (3) — _. 250 (2) K % 1.72 1.69 ± 0.09 (40) 1.70 1.29 - 3.30 1.66 ± 0.06 (3) 1.61 ±0.11 (3)1> 1.74 ± 0.11 (24) 1.60 ±0.01 (4)b 1.68 ±0.05 (4) 1.74 ±0.04 (3) TCGS

La ppm 79 ± 5 (28) 80 45 1 10 79 ± 7 (26) 77 ± 5 (3) _. —

Li ppm 170 ± 110 (3) 300 — — —

•Only one analyst reporting.

''Only two analysts reporting.

Lu ppm 1.08 ± 0.23 (11) 1.06 0.87 4.0 1 1 1 l\ tf\ (111 1-13 ± U.JU ( 1 i) Mg % 1.60 ± 0.25 (30) 1.52 1.01 6.30 1.29 ± 0.14 (3) 1.4 ± 0.3 (4) it i at /ni 1.7 ± 0.2 (If) 1 .10 ± U.UJ 1.6 ± 0.2 (3) OES 1.8 ± 0.5 (3) TCGS

Mn ppm 493 ± 7 496 ± 18 (51) 496 351 570 490 ±40 (12) 503 ± 10 (3) AQTl 1 "IA /t<\ AQ1 j. **y "> /SIB j ± t {j)" Cftf J. If) (f.\ jira ± 10 to/ 485 ± 22 (3) OES Mo ppm 28 ± 6 (13) 25.3 0.5 37 27 ± 5 (8) 0.8 ± 0.6 (3)3 N ppm <1000 (1) Na ppm 3100 ± 200 (36) 3200 2600 9700 3160 ± 150 (3) 3000 ± 100 (3)b 3 100 ± 200 (25) 3500 ± JUU (5)0 j tUU ± JtUU I J) uu

Nb ppm 20 ± 1 1 (3) 7 28 Nd ppm 63 ±7(11) 62 58 94 64 ± 7 (10) 62 (2) TCGS

Ni ppm 98 ±3 98 ± 6 (41) 98 69 128 96 ± 9 (8) 107 ± 18 (3) 99 ± 14 (14) 97 ± 5 (9) 98 ± 6 (6) ni 1 i\a inyc »0 ( Jj* 1UM9 qbto n\\l) pni rvL O % 47.02 (1) Os ppb <400 (2) —

P ppm 1020 ± 150 (4) 1140 880 3000 Pb ppm 70 ±4 72 ± 6 (37) 71 40 100 74 ± 7 (13) 74 ± 9 (3) 70 ± 2 (7) 67 ± 3 (4) 78 (2) IDMS 67 (1) POL

en 4 i7 iiih ccuc

Pb-210 pCi/g 3.37 (1) Pd ppb <2 (3)

...

Pr ppm 26 (2) 24 28

Pt ppb 0.7 ± 0.6 (3) 0.4 1.38 Rb pm 112 115 ± 8 (28) 115 70 150 — 1 17 ± 10 (24) 111 ± 15 (5) 1 15 ± 7 (5) Re ppb <200 (1)

... Ml ppb <500 (3)

... ... Ru ppb 0.26 3.0 —

S ppm 4000 ± 300 (4) 4000 2000 9000 •1 IUU i JvW \ Jf 1 VJo

8400 (2) Sb PPm 6.8 ± 0.5 (31) 6.9 4.0 12.1 6.8 ± 0.6 (26) 7.07 ± 0.06 (6) Sc PPm 26.6 ± 1.7 (25) 269 20 41 27 ± 2 (26) 25 ± 4 (3>* Se ppm 9.4 ± 0.5 9.6 ± 0.6 (42) 9.75 3.2 35 7.4 ± 3.7 (3) 9.7 ± 0.7 (28) 9.7 ± 0.3 (6)b 9.6 ± 1.2 (3)

Si % 22.1 ± 1.1 (17) 21.8 16.0 24.5 22.9 ± 0.5 (4) 20.3 ± 0.6 (3)b 22.1 ± 0.8 (3) TA A , T \ IW 20.4 ± 2.4 {i) Sm ppm 12.7 ± 1.1 (21) 12.6 10 20 12.6 ± 1.3 (21) Sn ppm 8.6 i 3.6 (9) 10.2 3 740

1 t t 1 A 1 / 1 \a 12.2 ± O.J (J)" SO4 % 0.98 (1) Sr ppm 1380 1380 1320 ± 70 (5)0 ± 100 ( 36) 1390 126 8000 1500 (2) 1410 ± 120 (26) 1 100 ± 500 (6) Ta ppm 1.91 ± 0 12 (18) 1.95 1.6 - 3.5 1.93 ± 0.23 (22) Tb PPm 1.8 ±0.3 (14) 2.0 0.22 - 3.3 1.8 ± 0.3 (16) Te ppm 1.8 ±0.8 (3) 0.92 9.9 2.31 ± 0.01 (3>a "~

Th ppm 24 24.6 ± 1.4 (22) 24.2 20 32 24.7 ± 1.2 (20) ... _.

Th-228 PCi/g 2 23 (1) ... _.

Th-230 PCi/g 3.74 (1) Th-232 PCi/g 2.45 (1) Ti ppm 7300 ± 300 (35) 7250 3000 8900 7700 ± I0O0 (3) 7200 ± 2O0 (4) 7100 ± 600 (22) 7400 ± 200 (6) 6900 ± 2000 (6) 7120 ± 140 (3) TCGS

Tl ppm 4 3.4 ± 0.6 (7) 3.75 2.0 18 3.64 ±0.12 (6) Tm ppm 1.3 (2) U ppm 1 1.6 ± 0.2 11.8 ± 0.7 (26) 11.85 8.4 15 11.7 ± 1.0 (19) 11.8 ± 0.5 (5)» 11.8 (2) IDMS

U-234 PCi/g 4.07 (1) U-235 PCi/g 0.179 (1) U-238 PCi/g 4.01 (1) V ppm 21'. ±8 221 ± 20 (37) 223 151 410 260 ± 100 (4) 225 ± 7 (3) 228 ± 15 (21) 209 ± 1 (3)* 210 ± 50 (5) W ppm 4.8 ±0.7 (15) 4.8 3.8 - 12.7 4.8 ±0.7 (16) Y ppm 63 ± 7 (10) 66 30 - 150 64 ± 3 (4) 65 ± 4 (3) Yb ppm 6.2 ± 1.0 (19) 6.2 4.7 9.0 6.3 ± 1.0 (18) Zn ppm 210 ± 20 210 ±9 (54) 212 180 700 210 ± 13 (13) 216 ± 8 (5) 215 ± 19 (23) 213 ± 6 (7) 207 ± 7 (7) Zr ppm 300 ± 60 (21) 301 160 -640 350 ± 80 (14) 300 ± 1 (6)b 302 ± 1 1 (3)

24
TABLE 14

ELEMENTAL CONCENTRATIONS IN NBS SRM 1633A: COAL FLY ASH (NEWER)

Literature

NBS

Element Units (1979) x ± s (n) Median

Ag ppb — <600 (1) —

Al % 14 14.4 ± 0.4 (9) 14.2 As ppm 145 ± 15 144 ± 2 (8) 145 B ppm 39.7 ± 1.3 (4) —

Ba ppm 1500 1400 ± 200(14) 1470 Be ppm 12 — —

Br ppm — 2.3 (2) ... Ca % 1.11 ±0.01 1.12 ±0.04 (10) 1.12 Cd ppm 1.0 ±0.15 1.07 (1) ... Ce ppm 180 175 ± 8 (7) 177 CI ppm ... <69 (1) ... Co ppm 46 43 ± 4 (8) 44 Cr ppm 196 ± 6 193 ± 5 (9) 194 Cs ppm 11 10.0 ± 0.4 (7) 10.1 Cu ppm 118 ± 3 120 (1) —

Dy ppm — 15.4 ± 1.2 (5) 15 Eu ppm 4 3.5 ± 0.3 (7) 3.62 Fe % 9.40 ±0.10 9.45 ± 0.17 (10) 9.40 Ga ppm 58 55 ± 3 (5) 55.7 Gd ppm — 19 (2) —

H2 0-T % — 0.35 (1) ... Hf ppm 7.6 7.2 ± 0.5 (8) 73 Hg ppb 160 ± 10 150 (2) ...

I ppm ... <5 (1) ...

In ppb ... 156 (2) ... K % 1.88 ± 0.06 1.89 ±0.06 (11) 1.88 La ppm 83 ± 3 (6) 84 Lu ppm ... 1.1 ±0.3 (3) ... Mg ppm 4550 ± 10 4300 ± 300 (5) 4540

Mn ppm 190 210 ± 35 (10) 191 Mo ppm 29 31 ±4 (3) —

Na ppm 1700 ± 100 1750 ± 120 (10) 1750 Nd ppm — 79 ± 23 (4) 71 Ni ppm 127 ± 4 124 ± 12 (4) —

O % — 47.66 (1) —

P ppm — 1830 ± 150 (3) —

Pb ppm 72.4 ± 0.4 65 (1)

...

Pr ppm ... 18 (2) ... Rb ppm 131 ± 2 140 ± 12 (8) 136 S PPm ... 2700 (1) ... Sb ppm 7 7.1 ±0.6 (6) 7.2 Sc ppm 40 38 ± 3 (8) 40

Se ppm 10.3 ± 0.6 9.5 ± 1.0 (7) 9.4

Si % 22.8 ± 0.8 23.5 ± 0.8 (5) 23.37 Sm ppm — 17 ± 2 (7) 16.6 Sr ppm 830 ± 30 822 ± 25 (8) 819

Ta nnm W,u 1 89 + 0 14 f71 1.8 Tb ppm 2A ± 0.4 (5) 2.3 Te ppm <6.6 (1) Th ppm 24.7 3 24.6 ± 1.0 (8) 24.8

Ti ppm 8000 8100 ± 200 (10) 8200

n ppm 5.7 ± 0.2 4.4 (1) U ppm 10.2 ±0.1 10.4 ± 0.2 (4) 10.4 V ppm 300 289 ± 7 (8) 291 W ppm 5.9 ± 0.7 (4) Yb ppm 8.2 ± 1.3 (4) Zn ppm 220 ± 10 235 ± 16 (7) 230

Zr ppm 370 ± 50 (4)

"Only two analysts reporting.

Individual Means by Analytical Technique

Range NAA TCGS Other

1 1 c i ^ n 1 j.o - I j.U 1 A 1 _i_ n 7 (A\ 14. 1 ± U.Z (**) 14.u yz.) 07 1 AO. y 1

- i4o IAS j_ 7 (<\ 70 a 1 ft jy - nl.O ACl _l 1 tA\ H\J ±1 yH) 1060- 1760 1480 ± 140 (9)

Z.Z 7 7 - OAZ.4 — ... ...

1.05 - 1.29 1.10 ±0.03 (5) 1.29 (2) ...

lOJ 1ft3 - 7ZjU30 1 7ft j- in 1 / D ± 1U \J)a

... —

434J +x 4* ffite \yf** is^ lOJ - 7on ZUU lO'i 1 yj j_± j

s ("Ma yp) q 3 in ft y.j - 1U.0 in1U.0ft j-± n ^ /ft^a \J.J \0}a

14 3 1 ft 8 1 4. J.- 1 0.o i ^ i x i n (a\

J.J 3 S X+ V.J n 3 (6\ \\J)

o.o*t Q OA Qy. 70i\j 0 ak i n ift /ft\a 7.*tJ x u. io 0 7f) 0\

51 -59 57 ± 2 (3)a —

15.3-23.5 —

6.3 - 7.8 7.4 ± 0.5 (6)a ... —

1 ^fi 1^1

151 - 160 — — —

i1 .OU an - l1.77 qq l.OO X v/.U / yjj i.yi 1 Q7 (t) 1

(\i OZ - inn IKPJ OJS3 X+ J3 ift\ \vf nV.yjQ3 - 1.44 1 AA 38nn annn

170 1 i\J - 777 Z 1 1 770 ZZU -4- X 40 (f\\ **\f ion o\

77 3ft Z 1 - JO

i <ftn 77nn 1 JOV - zzuu 1 740 -l 4n /ft^ 1 / 4U x 4VJ \0

91 fin o\

65.6- 122 —

112- 139 — ... ...

1700-2000 —

1 7 Q 1 Q Q 1 l.y - 10.

y

— ... ...

I Z4 - 10 J

114ZAO _L± 14 fOa \J)a

O.j - /.o I.J X U.J \J} 1A A 1 404U -l 7 /ft\a x Z \v)a

7.8 - 10.7 9.9 ± U.o (4)a 18.0-24.2

14.5 - 20.0 17 ±2 (5) 740 - 850 800 ± 37 (6)

1.71 - 2.10 1.91 ± 0.13 (6)a 2.1-2.9 2.5 ± 0.4 (4)a

22.4 - 28 24.8 ± 0.2 (5)a 7800 - 9000 8100 ± 200 (6) 8400 (2)

9.8-11 10.3 ± 0.3 (9) 280 - 360 293 ± 5 (5) 5.4-6.9 5.8 ± 0.8 (4)a

6.9- 10 8.6 ± 1.3 (3)a 218-256 233 ± 20 (3)a 300-410

25
Si i | i !. $ i i»K|3 = "iS;?; | 3 |

j 2 ; ; s

£~s £ S £ S£ £ £SS =

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S £ =S » £? E

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i 2 i i g ! i^-iCiiSSiS-SSS: i-i i Si i |

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_S 55 £ £ - f

5 £ £ £ s _ 5 £ £

^252 = 2 1 ~=S22 § 5 „-S

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26
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lc = 5s?!?5^2 s

= S Si 3jS ££i s

i |fs i i ah i |-a a *2aq3.2 '' ! ! "|. ! s ^ = 3 ~

|

s Us 5 5 I

I i i pSS : 8 : : 3 ~ S 2 : 3 : i * I

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£ » £ § £ S_ 5 £ s ~S » 2=3 JS2£ = S- £§£ 2~ ££§,.

<n« -H -H — -H M «I -H « — «S OO-HO. -H-H « -H w5

5

S

5- ss Si IS I

5 £

3 5 £ |S £2 £ !| | e ~ £ £ 5

2 2 S i ! d 2 i I £ :

: £ 2 2 ; 3 |

: • 2

g ; j 3 j «

22 1 8. * - *L

•H -H -H -H — * JC -H .* -H -H Sq

£ _ ££ - 55 £ £ £

3 £ ^ 52 Si II 2 5 E 2 S 3S

2 i s g i £3 i 5.| i i i Sj2 i i 53 ! i ! 3«s

I 2 =2 2 I 5 Ssl I

U'll.U-till* III* II* lilt llifiililil

itiixi* & & & „ & »xx £ & § & e e £ £ F P E = > * >$ 5 N

27
TABLE 16

ELEMENTAL CONCENTRATIONS AND URANIUM ISOTOPE RATIOS IN SEVERAL NBS STANDARD REFERENCE MATERIALS

SRM

Literature

Certification

Kin INO. Element units IN Dj x ± s (n) Range Date

1619 s ppm 7190 ±70 — — 1981 1620a S % 4.504 ±0.010 — — 1981

1621 s % 1.05 ± 0.02 1.00 ±0.07 (4) 0.90- 1.06 1967 1621a s % 0.94 ± 0.01 0.94 ± 0.03 (6) 0.89-0.973 1980 1621b s % 0.950 ± 0.005 1981 1622a s % 1.96 ± 0.04 1.90 ± 0.20 (4) 1.60-2.02 1979 1622b s % 1.982 ±0.018 1981 1623 s ppm 2680 ± 40 2710 ± 130 (4) 2600 - 2900 1971 1623a s ppm 2400 ± 30 1981 1624 s ppm 2110 ±40 2050 ± 120 (4) 1900-2200 1971 1624a s ppm 1410 ± 20 1981 1631A Ash % 5.00 ± 0.02 1974

s ppm 5460 ± 30 5530 ± 270 (4) 5260 - 5900

1631B Ash % 14.59 ± 0.09 1974

S % 2.016 ± 0.014 1.99 ± 0.05 (4) 1.92-2.04 1631C Ash % 6.17 ±0.02 1974

S % 3.020 ± 0.008 3.04 ± 0.07 (4) 2.98-3.12

1641 Hg ppm 1.49 ± 0.05 1.47 (1) 1975 1642 Hg ppb 1.18 ±0.05 1974 1642A Hg ppb 1.10 ±0.06 1.30 (1) 1977 950A U-238/235 "normal" 138.1 ±0.6 (4) 137.55 - 138.9 1961 950B U-238/234 "normal" 17630 (1) 1978 U-238/235 "normal" 137.4 (1) 1978

28
TABLE 17

ELEMENTAL CONCENTRATIONS IN NBS FUEL OIL STANDARD REFERENCE MATERIALS

1634 1634A

Literature NBS —~ NBS

Element Units (1978) x ± s (n) Median Range (1982)

As ppb 95 81 ± 26 (5) 70 56- 120 120 Au ppb 24 (1) Be ppb <10 6 Br ppb 39.8 ± 0.9 (4) 40 39- 240 <1 Ca ppm 15 (1) 16 Cd ppb <10 5 (1) 2 CI ppm 8.1 ±0.3 (3) 7.8- 18 31 Co ppb 310 ±50 (5) 301 250- 400 300

Cr ppb 90 97 ± 15 (4) 80- 116 700

Cu ppb 220 (1) Fe ppm 13.5 ± 1.0 14.2 ± 2.3 (14) 14.1 10.8- 25 31 Hg ppb 2.3 12 (2) 2.3- 22 <2

K ppm 315 (1) Mn ppb 120 200 ± 90 (4) 110- 320 190 ± 20

Mo ppb 870 (1) 120 Na ppm 11.9 ±0.9 (4) 11.2- 13.2 87 ±4

Ni ppm 36 ±4 36 ± 3 (16) 36.4 31.1 - 39.5 29 ± 1 Pb ppb 41 ± 5 46 (2) 41 - 50 2.80 ± 0.08 S % 2.14 ±0.02 2.13 ±0.11 (9) 2.15 2.0- 2.3 2.85 ± 0.05 Sb ppb 11 ± 2 (3) 10- 14 Se ppb 187 ± 15 (3) 138- 200 150 ± 20 V ppm 320 ± 15 308 ± 16 (14) 312 266 - 326 56 ± 2 Zn ppb 230 ± 50 320 ± 160 (3) 170- 480 2.7 ± 0.2

29
TABLE 18

ELEMENTAL CONCENTRATIONS IN NBS SULFUR IN COAL STANDARD REFERENCE MATERIALS

2682 2683 2684 2685

NBS NBS NBS NBS

Element Units (1982) (1982) (1982) (1982)

Al % 0.46 0.86 1.1 1.7 As ppm 1.0 3.6 3.9 12 Ash % 6.37 ± 0.18 6.85 ± 0.02 11.09 ± 0.18 16.53 ± 0.15 B ppm 39 67 114 109 Ba ppm 382 71 41 105 Br ppm 3.7 17 11 5.6 C % 75 79 68 66 Ca % 1.1 0.20 0.44 0.52 Ce ppm 10 9 12 18 Co ppm 1.7 2.2 3.9 4.6 Cr ppm 15 11 17 22 Cs ppm <0.1 0.4 1.2 1.3 Eu ppb 170 180 230 360 Fe % 0.24 0.76 1.5 2.9 H % 4.7 5.0 4.8 4.6 HjO" % 18 1.4 3.6 1.8 Hf ppb 600 420 570 910

K ppm 100 800 2000 2600 La ppm 5.2 5.1 6.7 10 Mg ppm 6900 1900 3100 4200

Mn ppm 26 13 36 41 N % 0.8 1.6 1.6 1.1 Na ppm 1000 500 300 800

Rb ppm <2 5.3 15 17 S % 0.47 ± 0.03 1.85 ± 0.06 3.00 ±0.13 4.62 ±0.18

Sb ppb 190 280 350 360

Sc ppm 1.5 1.9 2.7 3.7 Se ppm 0.91 1.2 1.9 1.9 Sm ppm 0.78 0.86 1.1 1.7 Th ppm 1.5 1.4 2.0 2.7

Ti ppm 500 400 600 900

U ppb 520 420 900 950

V ppm 15 14 22 31 w ppm 1.8 0.48 0.56 1.2 Zn ppm 8.6 9.5 110 17

30
TABLE 19

ELEMENTAL CONCENTRATIONS IN NBS WATER STANDARD REFERENCE MATERIALS

1643 1643

A

K1DC IN Oj Literature IN DO Literature Jement

• Units x ± s (n) [ i you

j

x ± s (n)

Ag ppb 3.4 ± 0.4 — 2.8 ± 0.3 2.7 (2) Al ppb 77 ± 1 81 ±3 (3) — 57 (1) As ppb 76 ± 1 76 ± 4 (4) 76 ± 7 73 (2) Ba ppb 18 18.3 ± 0.9 (5) 46 ± 2 46 (2) Be ppb 19 ± 1 20 (2) 19 ± 2 Ca ppm 24 (1) 28 (2) Cd ppb 8± 1 <15 (1) 10 ± 1 9.3 ± 3.8 (3) Cr ppb 15 ± 1 17 ± 2 19 (2) Co ppb 17 ± 1 20 (1) 19 ± 2 Cu ppb 16 ± 1 15.7 ± 1.6 (3) 18 ± 2 15 ±4 (3) Fe ppb 75 ± 1 79 (2) 88 ± 4 70 ± 40 (3) Hg ppb 2 <0.2 K ppm 1.6 (2) Mg ppm 5.7 (1) 7.8 (2) Mn ppb 29 ± 1 27.6 ± 1.2 (4) 31 ±2 21 (2) Mo ppb 105 ± 3 107 (2) 95 ± 6 Na ppm 8.8 (1) 9 (2) Ni ppb 49 ± 1 49.8 ± 1.4 (4) 55 ± 3 57 (1) N03 ppm 1.0 (1) Pb ppb 20 ± 1 23 (1) 27 ± 1 32 ± 8 (3) Se ppb 12 ± 1 11 (2) 11 ± 1 10 (1) Sr ppb 212 ±4 239 ± 5 236 (1) Sn ppb <20 (1) V ppb 50 ± 1 45 (2) 53 ± 3 Zn ppb 65 ± 3 62 (2) 72 ±4 66 ± 10 (3)

31
TABLE 20

NBS ENVIRONMENTAL RADIOACTIVITY STANDARD REFERENCE MATERIALS

4350 4350B 4353 NBS NBS NBS

Isotope Units (1975) Literature (1981) Literature (1981) Literature

K-40 pCi/g 1.40 ± 0. 13 ... 15 ... 19.5 ± 1.9 ...

Bq/g 5.4 ± 0.5 x 10 5.6 x

10"' 7.23 ± 0.69 x 10 Mn-54 fCi/g 57 ± 7 Bq/g 2.1 ± 0.2 x 10~ 3 ... ... ...

Fe-55 pCi/g 43 0.46 0.067 Bq/g 1.6 1.7 x 10~ 2 2.49 x 10 Co-60 pCi/g 4.00 ± 0.22 n i *) c 0. 1 /j 0.13 (1) Bq/g \ AO i A AO u 1 A— 1 1.48 ± O.Oo x 10 it.O £t ± \J.LJ X IU

Z.n-o j ILl/g 1 CA i A T J0U ± 4 / bq/g 1 . i U. 1 O X IU

cor-yu r on ano . in ,] vi -vu on i»- 1/

g

l to ± 4Z 1 tu ^UD ± £. 1

LI . In Bq/g 1 .OJ ± U. 15 X IU 5. i x 10 ~j n *7ii v /.DJ iU./oX IU

3D- 125 ICl/g 95 Bq/g 3.5 x 10~ 3

Cs- 1 37 pCi/g 2.70 ±0.12 2.5 (1)

(1 loi n flia 0.783 ± 0.049 0.85 (1) 0.464 ± 0.02 1 0.52 ( 1

Bq/g 1.00 ± 0.04 x 10 2.90 ± 0.18 x 10 1 1£ i A AO IA—

1.76 ± O.Oo x 10 Eu 152 pCi/g C CA A ID 6.50 ± 0.38 AOI/) A A 1 "5 0.824 ± 0.033 Bq/g 2.4 ± 0.1 x 10 3.05 ± 0.12 x 10 Eu-154 pCi/g 1 .4 ± 0.

0. 102 ± 0.015 Bq/g 5.2 ± 0.4 x 10 TO A .. 1 A— 2 3.78 ± 0.57 x 10 Eu-155 fCi/g 380

Bq/g 1.4 x 10~ 2

TI-208 iCi/g ion 380

Bq/g 14 X 10" 2

Pb-2 1pCi/g 1.6 Bq/g 6 x 10~ 2

Bi-212 pCi/g 1.4 Bq/g 5 x 10~ 2 ...

Pb-2 14 pCi/g 1.1 ... ...

Bq/g 4.1 x 10~ 2 ___ ... __.

Bi-2 14 pCi/g 0.92 ... ...

Bq/g 3.4 x 10~ 2 ... ... Ra 226 PCi/g 0.84 ... 0.967 ± 0.097 ... 1 . 1 6 ± 0.08 Bq/g 3.1 x 10" 2 ... 3.58 ± 0.36 x 10" 2 ... 4.30 ± 0.28 x 10"2 ...

Ac-228 pCi/g 0.92 ±0.18 .__ ... 1.88 ± 0.10 Bq/g 3.4 ± 0.7 x 10~ 2 ... r f\Q A t £ .. IA—

6.98 ± 0.36 x 10 Th 228 PCi/g 1.07 0.904 t A 1 i A 1

1.5M ± 0. 10 Bq/g 3.95 x 10" 2 3.35 x 10~ 2 1 AO i A l£ IA- 2 /.Oo ± O.jO X IU Th-230 pCi/g 0.988 n lot 0. /96 n on 1 1\ 0.80 ( 1

1 "id _i_ A AA

Bq/g 3.66 x 10" 2 ~y nc ^ i n—

2.95 x 10 A A1 _i_ A TO v IA- 2 4.4J ± U.ZZ X IU TL 111

1 h-Zi 1 pCi/g 0.84 0.890 1 9.1 j A If)

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-2 £ ni i A K w IA—

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fCi/g 47 ... ...

Bq/g 1.75 x 10" 3 ... ...

U-234 PCi/g 1.34 ... 0.896 ... 1.06 ± 0.04 ...

Bq/g 4.96 x 10~ 2 --_ 3.32 x 10~ 2 3.91 ± 0.14 x 10"2

U-235 fCi/g 50 — 46 ... 51 Bq/g 1.85 x 10" J ___ 1.7 x 10 3 1.9 x 10" 3

U-238 pCi/g 1.14 __. 0.832 ... 1.05 ± 0.05 Bq/g 4.42 x 10" 2 — 3.08 x 10"2 ... ^ on /*\ i a—

3.89 ± 0.20 x 10 Pu-238 fCi/g 2.0 0.35 ± 0.06 0.2 (1) 4.5 ± 0.5 3.5 (1) Bq/g 6.7 x 10" ! 1.3 ±0.2x 10" 5 1.66 ± 0.18 x 10"4

Pu-239 and Pu-240 ra/g 38 ± 3 33 (1) 13.7 ± 0.8 11.6 (1) 217 ± 16 202 (1) Bq/g 1.4 ± 0.1 x 10" 3 5.08 ± 0.29 x 10-" 8.03 ± 0.60 x 10 3

Pu-239 A% 89.91 94.57 Pu-240 A% 9.43 5.23 Pu-241 A% 0.318 0.178 Pu-242 A% 0.336 0.023 Am-241 fCi/g 8.4 4.0 ± 0.8 5 (1) 33.8 ± 2.5 42 (1) Bq/g 3.15 x 10"4 1.5 ± 0.3 x 10"4 1.25 ±0.09x 10" 3

1 ppm 54 (1) 1-129 fCi/g 0.032 (1)

32
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33
TABLE 22

ELEMENTAL CONCENTRATIONS IN VARIOUS NBS STANDARD REFERENCE MATERIALS

77 88 88A 91

sine iviicrmurc 11DJ Ljicraiure Literamre UCCiBIUFC

lenient Units X ± s (n) x ± s (n) x ± s (n) x ± s (n)

Al % 31.42 31.0 (2) 0.035 — 0.10 0.06 (2) 3.18 3.2 (1) B ppm — — — — — — ... 302 (1) Ba ppm — — — — — 13 (1) — 79 (1) Be ppb — — — — — 180 (1) ... —

C % — — 12.90 — 12.7 12.8 (1) — —

Ca % 0.19 0.14 (1) 21.80 21.8 (1) 21.56 21.7 (2) 7.49 7.54 (1) CI ppm — — — — — ... 140 —

Co ppm — — — 0.7 (1) — 3 (1) — 4.5 (1) Cr ppm — — — 3-9 (1) — 11.7 (1) — 26 (2) Cu ppm — — — — ... 2.5 (1) ... 16 (1) Eu ppm — — — — ... 1.2 (1) ... ... F % 5.72 5.68 ± 0.06 (6) Fe % 0.63 0.54 (2) 0.059 0.058 (1) 0.20 0.21 (2) 0.057 0.25 ± 0.24 (4) Ga ppm 12 (I) Gd ppm 3.4 (1) Hg ppb 28 (1) K % 1.75 1.79 (1) 0.025 0.10 0.085 (2) 2.70 2.68 (I)

Li ppm 1600 Mg % 0.30 0.22 (1) 12.95 12.8 13.0 (2) 0.006 (1) Mn ppm 80 (1) 44 230 180 (2) 51 (2) Na % 0.045 0.06 0.007 0.01 (1) 6.29 6.28 (2) Ni ppm 3 (2) 0 % 49.0 (1) P ppm 2000 13 40 145 (2) 96

Pb ppm 27 (1) 900 600 (2) S ppm 270 287 ± 15 (3) 12 (2)

Si % 15.12 15.32 (2) 0.14 0.56 0.41 (1) 31.54 3 1.9 ±0.4 (3) Sr ppm 1200 (1) <80 58 (2) 85 68 (2) 39 (1) Ti % 1.76 1.82 (1) 0.003 0.018 (2) 0.012 0.012 (2) 0.011 0.014 ± 0.002 (3) U ppb 540 (1) V ppm 180 9 (1) 43 (1) Yb ppm 1.2 (1) Zn ppm 4.1 (1) 640

Zr ppm 670 70 47 (I)

34
TABLE 23

ELEMENTAL CONCENTRATIONS IN NBS CLAY STANDARD REFERENCE MATERIALS

97 97A 98 98A

NBS JJterature NBS Literature NBS Literature NBS Literature Element Units (1931) ~x ± s (n) (1969) x ± s (n) (1931) ~x ± s (n) (1969) "x ± s (n)

Al % 20.51 20.5 (2) 20.52 1 1.93 13 53 + 0 07 (51 17.56 B ppm rr"" 64 (2) 69 (II 140 + 80 (4) 1 20 ( 1

1

Ba ppm 170 ± 80 (3) 670 660 (1) 680 + 120 (31 270 320 (2) Be ppm 1.3 (1) 3 6 (11 4 1 (11 5 * 9 (11 I

1 / C ppm ... 3200 (1) 600 (1) 4000 (11 8100 sj 1 W (11 111 Ca ppm 720 790 1 JW i sin + fin Ce ppm 59 (2) 160 (2) 127 (21 200 (2) Co ppm ... 3.7 ± 0.6 (3) ... 4 4 (2) 15 8 + 14 (51 13 (31 Cr rr"' ppm 540 550 ± 60 (6) 200 190 (21 140 150 + 40 (91 200 220 (21 Cs rr' npm 2.4 (1) 1l.U6 fit \l) 1 1 (11 6 2 (11 Cu rr'" ppm 24 18 ± 5 (4) 25 (1) 70 64 ± 24 (6) 120 (1) Dy rrppm 4.3 (I) 8.9 (1) 7.1 (11 V*/ 18 (1) Eu npm rr"1 1.4 (2) V*/ 3 7 ttl 1.9 (21 3.4 (21 Fe % 0.68 0.66 ± 0.01 (4) 0.31 0.30 (1) 1.43 1.32 ± 0.14 (6) 0.94 0.88 (1) Ga ppm 45 (1) 32 (1) 52 (21 23 (1) Hf npm rr 40 (1) 13 (21 7 (11 7 3 (11 Hg ppb 114 (2) 388 (1) 460 (1) 39 (11 K % 0.45 0.41 2.63 0.863 La ppm 34 (1) 70 (2) 94 ± 49 (3) 130 (21 Li ppm 1070 1074 (1) 510 439 (H 140 144 (11 320 290 fl) Lu ppm 0.96 (1) 0.98 (1) 0.65 (1) 1.2 (1) Mg ppm 1600 1450 (2) 900 4300 4100 + 200 (SI 2500

Mn ppm 15 50 ± 43 (3) 40 69 + 12 (61 41 (11 Mo ppm 2 (1) 1I.U0 (11 (l) Na ppm 520 270 1900 610

Nb ppm 36 (1) 39 (1) 40 (1) Nd npm rr"1 19 (1) V*/ 88 (11 49 (11 98 (1) Ni ppm rr"1 34try (2) V**/ 81 (1) 44 ± 8 (3) 160 (1) p nnm rr1" 350 1600 350 370 (21 480

Pb pom rr"1 35 (2) 42 (11 44 (21 69 (11 Rb ppm ... 24 (1) ... 154 (1) 35 (1) S ppm 170 176 ± 22 (3) 308 (1) 280 273 ± 25 (3) 1300 (1) Sb ppm 1.4 (1) 0.8 (1) 1.3 (1) 2.3 (1) Sc ppm 16 (2) 26 (2) 25 ± 4 (3) 32 (2) Se ppm 1.2 ± 0.2 (3)

Si % 20.02 20.0 (1) 20.39 27.60 27.60 ±0.01 (3) 22.85 Sm ppm 5.8 (I) 14 (2) 8.3 (2) 12 (2) Sn ppm 8.6 (2) 6.3 (2) 6.5 (1) 5.0 (2) Sr ppm 73 ± 38 (3) 1500 860 (1) 290 ± 70 (5) 330 440 (1) Ta ppm 4.2 (1) 3.2 (1) 2.2 (1) 2.5 (1) Tb ppm 1.27 (1) 2.8 (1) 1.4 (1) 2.9 (1) Th ppm 37 (1) 31 (1) 20 (1) 24 (1) Ti % 1.43 1.36 (2) 1.14 0.88 0.90 ± 0.06 (6) 0.964

Tl ppb 350 (1) U ppm 6.6 (I) V ppm 220 240 ± 90 (4) 360 (1) 140 180 ± 80 (8) 550 (1) Y ppm 35 (2) 120 (1) 38 ± 9 (3) 180 (1) Yb ppm 7.1 (2) 8.9 (2) 1 1 ± 9 (3) 9.8 (2) Zn ppm 92 (2) 125 (1) Zr ppm 1800 1390 (1) 520 (2) 300 320 ± 40 (5) 740 (1)

35
TABLE 24

ELEMENTAL CONCENTRATIONS IN NBS FEDLSPAR AND PHOSPHATE

ROCK STANDARD REFERENCE MATERIALS

99 99A 120A 120B

NBS Literature NBS Literature NBS Literature NBS Literature Element Units (1931) x ± s (n) (1981) x ± s (n) (1961) x ± s (n) (1979) x ± s (n)

Ae nnm rr111

- 5 (11 Al % 10.08 10.1 (1) 10.8 U.Jv 0 50 0.45 (1) 0 60 + 0 10 (51 B ppm 10 (1) Ba ppm 90 2300 2600 ( 1

61 (11 Be DDm rr"' 7 Q (11 c ooi (ii 0 87 1 04 (11 0 76 11.44 (71 \i)

Ca 0

/0 0.26 1.53 ^i; 16 o 16 1 (91 15 7 ii 7 i no C5\ Cd nnm FF,n 1

ZA (I) Ce nnm FF111 8 ni 5 (11 18? (11 Co nnm 0 74 (21 o i ni 3 (11 Cr nnm 7 + 5 (11 63 (11 ppm 0 7 (11 5 (21 Cu nnm 21 (21 10 (21 Eu nnm FF111 0.35 (1) 0.82 (1) 4H.O8 (11 F % 1 02 1 88 + 0 00 (51 1 84 1 88 4- 0 1 1 (41 Fe nnm FF' 11 470 500 (1) 450 7140 (11 7500 -t 500 (71 Ga 30 (1) Gd ppm 21 (1) Hf ppm 0.9 (1) 0 3 (11 Hg ppb 165 (1) jo58 (11 yi) K % 0.34 4.3 4 27 + 0 1 2 (11 0.083 0 087 0 070 + 0 09 (41 La DDm rr'" 77 (11 80 (11 Mb rrDDm1 " 320 120 no (n 1600 1 400 ( 1

1 700 7000 + 600 (41 Mn DDm <70 30 (2) V / 150 160 (1) 250 210 + 50 (61 Na % 7.96 4.6 4 55 + 0 09 (31 0.30 0.26 0 26 + 0 03 (41 Nd DDm rK"1 127 (11 Ni nnm rr is ni 17 + 6 (31 % 16 0 (11 P % 0.062 0057 (11 0.009 15.0 15.1 14 9 + 09 (51 Pb DDm 110 (2) 10 (21 Rb ppm 23 (1) 104 (2) S ppm 19 (1) 2900 (1) 2200 (1) Sb ppm 0.5 (1) 10 (1) Sc ppm 0.83 (1) 0.23 (1)

Si % 32.06 32.0 (2) 30.4 30.4 (1) 2.18 2.18 ±0.13 (6) Sm ppm 0.5 (1) 38 (1) Sn PPb 450 (1) Sr ppm 220 ± 160 (3) 700 (1) Ta ppm 1.9 (1) Tb ppb 280 (1) Th ppm 1.6 (1) 0.5 (1) 8.5 (2) Ti ppm 100 240 ± 220 (4) 40 720 . 720 (1) 900 850 ± 230 (5) U ppm 1.1 (1) 110 (1) 128.4 ± 0.5 131 (2) V ppm 170 ± 100 (3) Y ppm 10 (1) Yb ppm 1 (1) 13 (1) Zn ppm 16 ± 2 (3) 120 (2) Zr ppm 26 (2) 70 (1) 12 (1)

36
TABLE 25: ANALYTICAL METHODS CODE

CODE SPECIFIC TECHNIQUES

Neutron Activation:

NAA General, Unspecified or Mixed Conditions

ITNA Instrumental Thermal

IENA Instrumental Epi thermal

RTNA Radiochemical Thermal

RENA Radiochemical Epithermal

14 NAA 14 MeV

TCGS Thermal Neutron Capture Gamma Spectrometry

DNA Delayed Neutron Assay

Atomic Absorption - Emission:

AA General, Flame AA, Unspecified or Mixed Conditions

FAA Flame less AA

HAA Hydride Evolution AA

CVAA Cold Vapor AA

FE Flame Emission - Flame Photometry - Atomic Emission

FAE Flameless Atomic Emission

AF Atomic Fluorescence

AE + AF Atomic Emission + Atomic Fluorescence

X-ray Methods:

XRF General or Unspecified

EXRF Energy Dispersive XRF

WXRF Wavelength Dispersive XRF

CPXRF Charged Particle Induced XRF

Optical Emission:

OES General, DC ARC

MPOES Microwave Plasma OES

ICPES Inductively Coupled Plasma OES

DCP Direct Coupled Plasma OES

Gas Chromatography - Mass Spectrometry:

GC Gas Chromatography

IDMS Isotope Dilution Mass Spectrometry

SSMS Spark Source Mass Spectrometry

GC-MS Gas Chromatography-Mass Spectrometry

GCMES Gas Chromatography Microwave Emission

MS Mass Spectrometry without Isotope Dilution

GC-AA Gas Chromatography-Atomic Absorption Spectrometry

37
TABLE 25 (cont.)

Others

AS Alpha Spectrometry

ASV Anodic Stripping Voltammetry

CB Combustion, Elemental Analyzer

CHEM Chemical

CHEML Chemiluminescence , Candoluminescence

COLOR Colorimetry, Photometry, Spectrophotometry

trAA L.narged rartlcle Activation Analysis

CSV Cathodic Stripping Voltammetry

ESCA Electron Spectroscopy for Chemical Applications

FD Freeze Drying

FLUOR Fluorometry

GAMMA Direct Gamma-Ray Counting

GRAV Gravimetry

IC Ion Chromatography

ISE Ion Selective Electrodes

MECA Molecular Emission Cavity Analysis

NM Nuclear Method (General)

NT Nuclear Track

PAA Photon Activation Analysis, X-ray Activation Analysis

POL Polarography

POT Pot entiometry

RR Rapid Rock

SIMS Secondary Ion Mass Spectrometry

TITR Titrime try

TURB Turbi dime try

UU Uns pecif ied

VOLT Voltammetry

VV Various

38
TABLE 26: "WHOLE ROCK" CONCENTRATION SUMMATIONS OF MAJOR AND

MINOR ELEMENTS IN COAL AND FLY ASH SRMS

ELEMENT (%) SRM

16 32 1632A 1633 1633A 1635

Al 1.73 2.95 12.60 14.40 0.31

Ba 0.03 0.01 0.26 0.14

c 70.40 66.00 3.30 62.60

Ca 0.42 0.24 4.60 1.12 0.55

CI 0.09 0.08

Fe 0.86 1.12 6.14 9.45 0.23

H 4.20 3.85 0.11 0.04 4.07

K 0.28 0.41 1.69 1.89 0.01

Mg 0.16 0.12 1.60 0.4 3 0.10

N 1.27 1.23 1.26

Na 0.04 0.08 0.31 0.18 0.24

0 15.05 18.80 47.02 47.66 29.60

P 0.02 0.03 0.10 0.18

S 1.19 1.58 0.40 0.27 0.32

Si 3.17 6.01 22.10 23.50 0.54

Sr 0.01 0.14 0.08 0.01

Ti 0.09 0.16 0.73 0.81 0.02

Total 99.01 102.67 101.10 100.15 99.86

TABLE 27: ELEMENTAL DATA REPORTED BY YEAR

DATE NO. REPORTED MEASUREMENTS

pre 19 72 24 5 19 72 127

1973 349

1974 669

1975 995

19 76 905

1977 1603

1978 1192

1979 1393

1980 1581

1981 14 24 1982 1761

TABLE 28

Distribution of SRM data by Analytical Technique

Analytical Method Geological SRMs Biological SRMs

Neutron Activation 3104 2566

Atomic Absorption 428 1 034

X-ray Fluorescence 4 58 507

Optical Emission 4 53 1323

Mass Spectrometry 99 89

Colorimetry, Spectrophotometry 14 55

Photon Activation 332 104

Other 217 357

TOTAL 5105 6088

39
TABLE 29: COMMENT CODES FOR APPENDIX TABLES

CODE DEFINITION

D Same data apparently reported in two or more references

H Hydride generation

L Limit

R Range

* Not used in mean value calculation

1 Different nebulizers used for independent results

2 V205 catalyst used in dissolution

3 Different electrodes used for independent results

4 Aqueous slurry of reground sample

5 Different radioactive isotopes used for independent results

6 Different methods of standardization used for independent results

7 Different chemical separation methods used for independent results

8 Isotope dilution methods combined with spark source mass spectrometry

9 Gamma-gamma coincidence

10 Different neutron filters used for independent results by epithermal

neutron activation

11 Different dissolution or matrix destruction methods used for independent results

12 Different methods of peak integration or dead time correction used

for independent results by neutron activation

13 Different detectors used for independent results

14 Different furnace configuration used for independent results

15 Different laboratories prepared fused beads used for independent

results

16 Different matrix correction methods used for independent results

17 Different laboratories reporting independent results in the same reference

18 Different bottles of reference material

19 Duplicate entries from same reference from previous data compilation

source - reason unknown

20 Different emission-absorption lines used for independent results

21 Dichromate used for FeO determination

22 Vanadate used for FeO determination

23 Modified Penfield method used for H20+ determination

24 Different irradiation containers used for independent results by

neutron activation

25 Different colorimetric methods used in same reference for independent results

31 Different chemical methods used for independent results

32 Different background correction and/or X-ray tubes and/or crystals

used for independent results by XRF

33 Different pellet sizes used for independent results by XRF

34 Analyzed on dry sample basis

35 Analyzed on as-received basis

36 OES pre-ignition at various temperatures for independent results

40
TABLE 30: MULTIPLIERS USED FOR OXIDE TO ELEMENT CONVERSIONS

OXIDE MULTIPLIER OXIDE MULTIPLIER

A1 20

3 0.529 MnO 0.774

B 2°i 0.311 Mn

203 0.696

BaO 0.896 Mn

3 0

4 0.720

BeO 0.360 Mo0 3 0.667

co 2 0.273 Na

20 0.742

CaO 0.715 Nd 20

3 0.857

CdO 0.875 NiO 0.786

CoO 0.786 p

2 o5 0.436

Cr

203 0.684 PbO 0.928

Cs 20 0.943 Rb 20 0.914

CuO 0.799 Si0

2 0.467

FeO+Fe 2 0 3 1.112 so

3 0.400

FeO 0.777 Sc

2 03 0.652

Fe

2 0

3 0.699 SrO 0.846

Ga 20

3 0.592 Ti02 0.599

H

20 0.112 U

30 8 0.848

K

20 0.830 V 2°5 0.560

La 20

3 0.853 Y2O3 0.787

Li

20 0.465 ZnO 0.803

MgO 0.603 Zr0 2 0.740

41
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43
TABLE A TABLE B

NBS SRM 120A—COLLECTED DATA NBS SRM 120B—COLLECTED DATA

ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

Al (ppm) Ag (ppm)

4500. ICPES 80BRE 01 5 ICPES 81CHU 01

c (%) Al (ppm)

1 OA CB 78TER 01 5100- 100- AA 82 JEN 01 5400- 500. ICPES 82 JEN 01 Ca (%) 5870. onZU • ICPES 81CHU 01 6000. 35 TCGS 78GLA 04

36. 02 TITR 80HIT 02 / / ou - 0 AnA T A 1 36. 1 ICPES 80BRE 01 8500. * SIMS 78M0R 01

F (%) • As (ppm)

3 8 Hi ISE 69EDM 01 5- L* ICPES 81CHU 01

3 8 01 ISE 7 7H0P 01

3 88 11 ISE 69EDM 01 Au (ppm)

3.93 11 ISE 71 PET 01

4- 01 11 ISE 71 PET 01 3. L* ICPES 81CHU 01

Fe (ppm) Ba (ppm)

7340 ICPES 80BRE 01 61 1 2 ICPES 81CHU 01

Hg (ppb) Be (ppm)

57.5 3-6 FAA 82 FLA 01 2.9 0- 06 ICPES 81CHU 01

Mg (ppm) Bi (ppm)

1400. ICPES 80BRE 01 25 • L* ICPES

Mn (ppm) L. (/.)

160 ICPES 80BRE 01 0 983 CB 77TIL 01 1-8 SIMS 78M0R 01

S (ppm)

Ca (%)

oq a a V5 UU - CB 78TER 01

17 8

A SIMS 78M0R 01 Ti (ppm) 32.7 35 TCGS 78GLA 04

33- EXRF 80DAL 01 720- ICPES 80BRE 01 33.78 2. 07 ICPES 82 JEN 01 33.98 0..72 AA 82 JEN 01 U (ppm) 35.06 1 . 16 ICPES 81CHU 01

110- 10 COLOR 810GU 01 Cd (ppm)

22. 10. ICPES 81CHU 01 25.3 AA 76KRI 03

Ce (ppm)

182- 3 6 ICPES 81CHU 01

Co (ppm)

3. 1 ICPES 81CHU 01

Cr (ppm)

63.1 1

.

9 ICPES 81CHU 01

44
TABLE B (cont) TABLE B (cont)

ANAL KEF REF ANAL REF REF CONC " UNCER COMMENT METH CODE NUM CONC ' UNCER COMMENT METH CODE NUM

Cu (ppm) 240. 20. AA 8 2 JEN

246. AA 7.6KRI 86 1 ICPES 81CHU 0

1

260. 7- QO 8 1 CHU

11 3 AA 76KRI 03

Mo (ppm) Eu (ppm)

5 L* ICPES 81CHU

4.8 i ICPES 81CHU 01 Na (ppm)

F (%) 2300. 100, AA 82 JEN 3-78 o. 07 NAA 80NOR 01 26 30. 70. ICPES 81 CHU 3-82 35 TFNA 7QPT A 03 2800. 35 TCGS 78GLA

3-89 0. 21 IC 82 JEN 01 2900. SIMS 78M0R

4.04 0. 47 lOL OS J LiVi 01 Nd (ppm) Fe (ppm)

127

.

25 ICPES 81 CHU

3200. * SIMS 78M0R 01

c Ann ODUiJ inn AA 82 JEN 01 Ni fDDml

7200. .800. ICPES 82 JEN 0

1

7400 35 TCGS 78GLA 04 12. 35 IENA 79GLA

7700- 35 I ENA 79GLA 03 15.4 1 ICPES 81 CHU 7827. AA 76KRI 03 22.9 AA 76KRI

7900- 200. ICPES 81CHU 01 7970- 01 0 (%)

Gd (ppm) 36. 0. 5 14NAA 80NOR

21. 0. 6 ICPES 81CHU 01 P (%)

K (ppm) 12.97 0..79 * IC 82 JEN

13.5 SIMS 78M0R

110. *35 TCGS 78GLA 04 14.7 35 TCGS 78GLA

600. 200. ICPES 82 JEN 0

1

15.19 1 .2 3 ICPES 82 JEN

660. EXRF 80DAL 0

1

15.21 0 .38 ICPES 81 CHU 760. SIMS 78M0R 01 15.9 EXRF 80DAL

800. 100. AA 82 JEN 01 Pb (ppm) 1170. 25. * ICPES 81CHU 01

La (ppm) 25 • 5 ICPES 81 CHU

51 • / AA 7 6KRI

89- 4 • ICPES 81CHU 01

Li (ppm)

2200- EXRF 80DAL

2 . L* ICPES 81CHU 01 Sb (ppm)

Mg (ppm)

10. ICPES 81 CHU

51 • *35 TCGS 78GLA 04

1600- 100. ICPES 82JEN 01 Se (ppm)

1600. 100. AA 82 JEN 01 1870. 60. ICPES 81CHU 01 30. L* ICPES 81 CHU 2800. SIMS 78M0R 01 Si (%) Mn (ppm)

2.01 EXRF 80DAL

130. SIMS 78M0R 01 2.12 35 IENA 79GLA

150- EXRF 80DAL 01 2.12 0 .19 ICPES 82 JEN

2 30. 15- ICPES 82JEN 01 2.19 35 TCGS 78GLA

03

45
TABLE C

TABLE B (cont) NBS SRM 1566—COLLECTED DATA

CONC UNCER COMMENT

ANAL meTM

REF REF CODE NUM

2.21 0.01 AA 82KIS 01 2.41 0.24 AA 82 JEN 01

Sm (ppm)

38- 1 9 ICPES 81CHU 01

^onn (\ r> nm ^ \ ' pui

;

3 L* ICPES 81CHU 01

Sr (ppm)

705. 14. ICPES 81CHU 01

25. L* ICPES 81CHU 01 7.9 0.8 AS 82R0E 01 9-05 0.4 AS 82TH0 02

1 * VHP"1 /

590. SIMS 78M0R 01 740. 20. ICPES 81CHU 01 780. 35 IENA 79GLA 03

950. 35 TCGS 78GLA 04 1200. EXRF 80DAL 01

U (ppm)

30. L* ICPES 81CHU 01 130- 5 AS 82R0E 01 132. 2- AS 82TH0 02

V (ppm)

103. 3-1 ICPES 81CHU 01 120. 10. ICPES 82 JEN 01 280. 40. AA 82 JEN 01

Yb (ppm)

12.7 0.4 ICPES 81CHU 01

Zn (ppm)

107. AA 76KRI 03

127. 39 ICPES 81CHU 01

Zr (ppm)

12. 1.2 ICPES 81CHU 01

CONC

As (ppm)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

12.2 1 .

1

IENA 82GLA 02

12.4 IENA 83GLA 01 13. 1.2 I TOA 79K0B 03

13.17 0.34 HAA 81UTH 01

15 .5 0.3 Ml HAA 82J0N 01

B (ppm)

7. 1 TCGS 82GLA 02

Br (ppm)

45. 1 .4 ITNA 79K0B 03

180. EXRF 81PAR 01

Ca (ppm)

880- 3370. R* AA 80UCH 01

1 J XU a 9(1 i i 1 1 QO TrtM V 1 15 30. 30. 11 ICPES 82J0N 01 4500. EXRF 81 PAR 01

Cd (ppm)

3.2 0.1 FAA 82SUZ 01 3.24 0.29 ASV 82 SAT 02 3.3 0.3 ASV 82GAJ 01 3.4 0.22 FAA 81CHA 01 3.54 0.04 11 ICPES 82 JON 01 3.61 0.03 11 ICPES 82 JON 01

Co (ppb)

340. 20. ITNA 79K0B 03

Cr (ppb)

340. 90. 1

1

ICPES 82J0N 01 600. 200. 11 ICPES 82J0N 01 700. 200. ITNA 79KOB 03

Cu (ppm)

61. XRF 80SUZ 02

61.8 0.9 11 ICPES 82J0N 01 62.9 0.5 11 ICPES 82 JON 01 63. AA 8 OUCH 01 128. 2. ' * AA 81UCH 01 189. * EXRF 81PAR 01

Eu (ppb)

20. 10. ITNA 79KOB 03

F (ppm)

4.9 0.5 ISE 83KNA 01 5.4 1.2 ISE 83GLA 01

46
TABLE C (cont)

UNCER COMMENT

ANAL

METH

REF CODEREF NUM

TABLE C (cont) ANAL REF REF UNCER COMMENT METH CODE NUM

178. 4

.

ITNA 79KOB 03

191 5 11 ICPES 82JON 01

1 OA Q 1 1 1 1ft 9 TAM n i 196. 6 11 ICPES 82 JON 01 203. 8- 11 ICPES 82JON 01 209. AA 8 OUCH 01 576. * EXRF 81PAR 01

Hg (ppb)

40. CVAA 83GLA 01

T ( nnm ^

2 .337 0.074 * RTNA 80GVA 01 2.79 NAA 79HEC 01 3.062 0.128 35 RTNA 81 ALL 01 3.209 0.134 RTNA 81STR 01

U. 1 J** J** Q 1 AT T o 1 ALL C\U 11

K (%)

0.87 0.03 ITNA 79K0B 03

0.977 FE 80UCH 01 0.98 0.04 11 ICPES 82 JON 01

0 .98 0.02 1 1 ICPES 82 JON 01

1 .89 * EXRF 81 PAR 01

Mg (ppm)

1280. AA 80UCH 01 1410. 20. 11 ICPES 82J0N 01 1430. 40. 11 ICPES 82 JON 01

Mn (ppm)

3. * XRF 80SUZ 02

15. 1 .2 ITNA 79K0B 03

17.2 0.6 FAA 81CHA 01 17.2 0.2 11 ICPES 82 JON 01 17.4 0.6 11 ICPES 82J0N 01

17 .8 0.9 1 1 ICPES 82 JON 01

19. AA 80UCH 01 49. * EXRF 81PAR 01

Mo (ppb)

70. L* ICPES 82J0N 01 100. 100. 11 ICPES 82 JON 01

Na (ppm)

4600. 240. ITNA 79KOB 03

4920. FE 80UCH 01

Ni (ppm)

0-92 0.04 11 ICPES 82JON 01 0-97 0 09 11 ICPES 82 JON 01

7600-

7800.

7800.

7900.

Pb (ppb)

400-

200.

300.

100.

6

11 6

11

FAA ICPES

FAA ICPES

81 LAN 01 82J0N 01 81LAN 01

82 JON 01

440. 40. FAA 82RAI 01 450. 6 FAA 81HIN 01 450. 6 FAA 82 KOI 01 470. 10. FAA 81CHA 01 480. 6 FAA 82KOI 01

480. 6 FAA 81HIN 01 500. 20. ASV 82GAJ 01 500. 200. 11 ICPES 82JON 01 500. 300. 11 ICPES 82JON 01 510. 60. ASV 8 2 SAT 02

Rb (ppm)

20. EXRF 81PAR 01

bD tppt>;

13 U . AO ITNA 79KOB 03

Sc (ppb)

89. 6 - ITNA 79KOB 03

Se (ppm)

l ft l . o U • £, HA A ft9MAV U 1 2.22 0.03 11 HAA 82JON 01 2.42 0.08 11 HAA 82JON 01

Sr (ppm)

9.9 1.1 FAA 82SUZ 03

92. EXRF 81 PAR 01

U (ppb)

126. DNA 83GLA 01

V (ppm)

2.44 0.06 11 ICPES 82 JON 01

Zn (ppm)

750. * XRF 80SUZ 02

843. 12. 11 ICPES 82 JON 01 859. 9. 11 ICPES 8 2 JON 01 860. AA 80UCH 01 869. 8- 11 ICPES 8 2 JON 01 870. 35. ITNA 79KOB 03

878. 15. 11 ICPES 82 JON 01 2953. * EXRF 81 PAR 01

47
TABLE D

NBS SRM 1567—COLLECTED DATA TABLE D (cont)

CONC

As (ppb)

UNCER COMMENT

ANAL

METH

KEF CODE

REF NUM

80. L* ICPES 81W0L 01

50. L* HAA 82 JON 01 30. L* IENA 82GLA 02

50. L* HAA 82 JON 01 5.4 0.5 7 RTNA 77GIL 03

5.4 0.5 RTNA 78GIL 01 5.6 1

.

7 RTNA 77GIL 03

6- 1 . H ICPES 82HAH 01 30. 10

.

* COLOR 77BUR 01

d \p pm )

1 .5 TCGS 82GLA 02

30. L* ICPES 82KUE 01 30. L* ICPES 82KUE 01

30. L* ICPES 82KUE 01

Bi (ppb)

8. L* ICPES 82HAH 01

Br (ppm)

9-9 1 .5 I TOA 78GIL 01

Ca (ppm)

173. 38 AA 81YAS 01 179. 38 AA 81YAS 01

181

.

38 AA 81YAS 01 183. 38 AA 81YAS 01 193. ICPES 81W0L 01 194 . 6 - 1

1

ICPES 82 JON 01 195. 2

.

6 ICPES ozKUE Ul 195. 3

.

6 ICPES 82KUE 01 196. 2. 6 ICPES 82KUE 01 197. 38 AA 81YAS 01

199. 38 AA 81YAS 01 199. 4. 11 ICPES 82 JON 01

Cd (ppb)

20. ASV 82GAJ 01 29- 4. ASV 82 SAT 02

30. 20. 6 ICPES 82KUE 01 30. 20. 6 ICPES 82KUE 01 30. 20. 6 ICPES 82KUE 01 40. 10. 11 ICPES 82 JON 01 50. 30. 11 ICPES 82 JON 01

Co (ppb)

21. 4 ITNA 78GIL 01

CONC

Cr (ppb)

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

OCA ICPES 82KUE 01 250. 1 4 L* ICPES 82KUE 0

1

250

.

L* ICPES 82KUE 01 300. 100

.

1

1

ICPES 82 JON 01 400. 200. 1

1

ICPES 82J0N 01

Cs (ppb)

200. L* ITNA 82GLA 02

Cu (ppm)

1 .8 0.2 11 ICPES 82J0N 01

1 .9 0.2 11 ICPES 82JON 01

2. 0.1 ICPES 81KNA 01

2. 0.2 RTNA 78GIL 01

9 £D L V^r El D Q9 VTTF n 1

2 .04 ICPES 81W0L 0

1

L . \J\) 0.04 (,\J ICPES 82KUE 01

9 O.A CO

09 VTTF Ul

t (.ppb;

200

.

L* ISE 83GLA 01 40. 20. ISE 83KNA 01

Fe (ppm)

17. 1 - 11 ICPES 82JON 01 17.1 0.8 11 ICPES 82 JON 01

17 .2 0.6 ITNA 78GIL 01

17.7 0.7 6 ICPES 82KUE 01

17 .9 0.8 11 ICPES 82 JON 01

18. 1

.

11 ICPES 82J0N 01

18.4 1. 6 ICPES 82KUE 01

18.7 2.1 6 ICPES 82KUE 01 19.3 1.1 ICPES 81KNA 01

in r 19 .0 T PDC C Q 1 T.TAT n 1 u 1

Ge (ppb)

20

.

L* ICPES 82HAH 01

Hg (ppb)

1 . 0.3 RTNA 78GIL 01

K (ppm)

1300. 50. 11 ICPES 82JON 01 1310. 40. 11 ICPES 82 JON 01

1320. 10. 6 ICPES 82KUE 01

1320. 10. 6 ICPES 82KUE 01

1330. 20. 6 ICPES 82KUE 01

1392. 37. * ITNA 78GIL 01

48
CONC

Mg (ppm)

TABLE D (cont)

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM CONC

Rb (ppm)

TABLE D (cont)ANAL REF REF UNCER COMMENT METH CODE NUM

398. 10. 6 ICPES 82KUE 01 406. 3. 6 ICPES 82KUE 01 419. 4. 6 ICPES 82KUE 01 420. 10. 11 ICPES 82 JON 01 429. 9. 11 ICPES 82 JON 01

Mn (ppm)

6.7 1.2 * AE+AF 82GOL 01

8. 0.4 11 ICPES 82 JON 01 8.2 0.3 11 ICPES 82 JON 01 8.3 ICPES 81W0L 01

o . 3 u.z 1

1

ICPES 8ZJON 01

O . DD U. 1

J

0

T PT>t? C {5/K.UE. Ul 8.58 0.16 6 ICPES 82KUE 01 8.6 0.4 ITNA 78GIL 01

8.67 0.12 6 ICPES 82KUE 01 9-9 0.5 * ICPES 81KNA 01

no ^ ppd j

380. 30. 6 ICPES 82KUE 01 390. 90. 11 ICPES 82J0N 01 400. 40- 6 ICPES 82KUE 01 420. 40. 6 ICPES 82KUE 01 420. 70. 11 ICPES 82JON 01

Na (ppm)

10.4 2.5 ITNA 78GIL 01

Ni (ppb)

500. L* ICPES 82KUE 01 500. L* ICPES 82KUE 01

Q9VITF ni 160. 40. 11 ICPES 82 JON 01 inn 1 1 1 1 T PPT? Q

P (ppm)

1350. 20. 6 ICPES 82KUE 01 1370. 50- 11 ICPES 82 JON 01 1370. 10. 6 ICPES 82KUE 01 1400. 10. 6 ICPES 82KUE 01 1420. 30. 11 ICPES 82 JON 01

Pb (ppm)

0.1 L* ICPES 82 JON 01 0-02 L* ASV 82GAJ 01 0.1 L* ICPES 82 JON 01 3.8 L* ICPES 82KUE 01 3.8 L* ICPES 82KUE 01 3.8 L* ICPES 82KUE 01 0.018 0.003 ASV 82 SAT 02

0.99 0.16 ITNA 78GIL 01

Sb (ppb)

2. L* ICPES 82HAH 01

38. 1 • RTNA 78GIL 01

Se (ppm)

0.7 * FAA 81MEY 01 076 0-08 11 HAA 82J0N 01

0 82 0 08 ICPES 81W0L 01 0-87 HAA 81 HAH 01 0.87 0.06 H ICPES 82HAH 01 0.901 0.051 HAA 80RAP 02

0.91 0.03 11 HAA 82 JON 01 0.95 0.04 GC MS 81REA 02

0.96 0.08 HAA 81MEY 01

1

.

0.1 11 XRF 80RAP 01

1

.

0.2 HAA 8 IREA 01

1- 0.1 HAA 80VIJ 01 CSV 81HAN 01

1 .03 0.04 HAA 81HAN 01

1 .04 0.01 D* EXRF 80RAP 03

1.05 0.09 7 RTNA 77GIL 03

1 .05 0.09 7 RTNA 77GIL 03

1.1 0.02 XRF 81KNA 01

1.1 0.02 11 XRF 80RAP 01

1.11 0.05 RTNA 78GIL 01

1 .12 0.01 7 RTNA 77GIL 03

1.12 0.01 ITNA 78GIL 01

1 .17 0.18 7* RTNA 77GIL 03

Sn (ppb)

zu?n Tr*BI7 c ILrL D

Q O U AU OZ HAH U

1

U (ppb)

0.95 0.24 35 DNA 80GLA 04

V (ppb)

50. L* ICPES 82J0N 01

Zn (ppm)

10.2 * ICPES 81W0L 01 10.5 0.7 11 ICPES 82J0N 01 10.6 0.7 11 ICPES 82J0N 01 10.6 0.5 11 ICPES 82J0N 01 10.6 0.4 11 ICPES 82JON 01 10.88 0.56 ITNA 78GIL 01

10.9 0.1 6 ICPES 82KUE 01

11. 0.2 6 ICPES 82KUE 01 11.1 0.4 6 ICPES 82KUE 01 11.3 1.1 ICPES 81KNA 01

49
TABLE E

NBS SRM 1568—COLLECTED DATA TABLE E (cont)

Cs (ppb)

ANAL UP REF CONC ' UNCER COMMENT METH CODE HUM CONC ' UNCER COMMENT

iPpb) (7n f hnn i

DO. T * UA A HAA

O 1 TAKT A 1 OZJON 01 A 1 0 .

2

1

1

90. 10

.

COLOR 7 7 BUR 01 1 0 A O 0.2 1

1

320

.

40

.

*1

1

HAA OH JAM A 1 82 JON 01 9£ aUlm A A 1 0.01

OQ A nf\ Z\J / RTNA "7 7f Tl A 1

/ /GIL 0 3 2 .

1

ftU 1 • 1 jy u « HO 7 RTNA 77TTT m 2 .2 A 1 1 0 . 1 J 70

.

7 RTNA 77fiTT * /ulb 0^U

J

400

.

10

.

HAA ft I RAP 0

1

F (ppb)

400. 10. RTNA 78GIL 01 410

.

20

.

HAA a l rap o 1 180. Aft a in i i 1

1

tlAn ft 1 R AP n 1 200.

A- 1ft 7 n U A A Q 1 ITM A A 1 436. 18. HAA 82TAM 01 Fe (ppm)

440 • C A H ICPES OUAU A 1 oz KAH 01 452

.

70. ICPES 81W0L 01 7 1 / • 1 0.4 11 460. 70. IENA 82GLA 02 1 .

3

0.4 1

1

7.6 0.4 11 Cppm) 7 Q 0.4 11

R P c, o . O J 0.94

1

.

L* TCGS 82GLA 02 Q7#UODA 1. 9.4 0.3

(ppb)

Ge (ppb)

aO • Li ft?HAH (11 20. L*

Hg (ppb)

1 .23 0.08 ITNA

5.6 DO

(ppm) 6 .4 1

.

142. 3. ICPES 81W0L 01 I (ppm)

144. 38 AA 81YAS 01 145. 38 AA 81YAS 01 0.011 0.001

1 A £ 140 • JO A A D 1 V A C A 1 oil Ad U

1

0.012 0.001 34

1 A A JO AAA A Q 1 V A C A 1 0 1 I AS U

1

1 Aft j • 1 1 ICPES ft 9 TO.N n 1 K (ppm)

148. 3. 11 ICPES 82JON 01 965. 149. 38 AA 81YAS 01 1 1

.

151. 38 AA 81YAS 01 1125. 16

.

1 140

.

30

.

1

1

1 150. o r\ 80

.

1

1

20. ASV 82GAJ 01 Mg (ppm)

25. 2. ASV 82SAT 02

40. 20. 1

1

ICPES 82JON 01 S 1 n 20. oO. OA30

.

1 1 ICPES QO Tr\M n 1 OZJON Ul 510. 10.

(ppb) Mn (ppm)

18. 2. ITNA 78GIL 01 19-1 0.9 19-9 0.4 (ppb) 19.95 0-69

20.1 0.3

80. 80- 11 ICPES 82 JON 01 20.2 0.5

2on 200- 11 ICPES 82 JON 01 21.4 1.4

Mo (ppm)

200. L* ITNA 82GIA 02

1 .59

1 .59

0.07

0.09

ANAL

METH

KEF CODE

REF NUM

ICPES

ICPES ICPES

ICPES

RTNA

ISE

ISE

ICPES ICPES

ICPES

ICPES ITNA

ICPES

ICPES

CVAA RTNA

RTNA RTNA

ICPES ITNA

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ITNA

ICPES

ICPES

ICPES

ICPES

ICPES

82 JON 01 82J0N 01 81W0L 01 81KNA 01 78GIL 01

83KNA 01 83GLA 01

82 JON 01

82 JON 01

82 JON 01 82 JON 01 78GIL 01 81W0L 01 81KNA 01

ICPES 82HAH 01

81KNA 01 78GIL 01

81 ALL 01

81 ALL 01

81W0L 01 78GIL 01

82 JON 01

82 JON 01

82 JON 01

82 JON 01

82 JON 01 81W0L 01 78GIL 01

82 JON 01

82 JON 01 81KNA 01

82 JON 01 82J0N 01

50
TABLE E (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM CONC

1 .6 0.13 ICPES 81WOL 01 U (ppb)

Na (ppm) 0.89

6.9 0.4 ITNA 78GIL 01 V (ppb)

Ni (ppb)

IDO. OA 1 1 ICPES 82J0N 01 Zn (ppm)

160. 30. 11 ICPES 82 JON 01

P (ppm)

19 - 3 19.4

1600. 60. 11 ICPES 82 JON 01 19.8

19-97

1630. 30. 1 1 ICPES 82 JON 0

1

20.

Pb (ppb) 21.3

100. L* ICPES U 1 100. L* ICPES 82JON 01

30. ASV 82GAJ 01

35- 4. ASV 82SAT 02

Rb (ppm)

7.27 0.21 ITNA 78GIL 01

Sb (ppb)

2. L* ICPES 82HAH 01

5. 1 . RTNA 78GIL 01

Se (ppb)

280. 55. FAA 81MEY 01 280. 30. 1

1

HAA 82JON 01 315

.

14 . HAA 81 HAH 01 320

.

40. 1

1

HAA 82 JON 01 320

.

50. HAA 81MEY 01 331

.

29 . ICPES 81WOL 01 338

.

3

.

7 RTNA 77GIL 03

370. 60. H ICPES 82HAH 01 370. 30. HAA 80RAP 02

380. 10. HAA 81HAN 01 380. 50. HAA 80VIJ 01 390. 70. HAA 81REA 01 390. 20. GC MS 81REA 02

400. 100. 11 XRF 80RAP 01 400. 20. XRF o 1 IsJnA A 1 400. 20. 11 XRF 80RAP 01 400. 8. D* EXRF 80RAP 03

420. 30. ITNA 78GIL 01 420. 30. 7 RTNA 77GIL 03

jU • D TH A 78GIL 01 460. 80. 7 RTNA 77GIL 03

480. 70. HAA 82TAM 01

Sn (ppb)

20. L* ICPES 82HAH 01

TABLE E (cont)ANAL REF REF UNCER COMMENT METH CODE NUM

0.22 35 DNA 80GLA 04

LW ICPES 82JON 01

0.7 11 ICPES 82J0N 01 0.4 ICPES 81W0L 01 0.8 1 1 ICPES 82 JON 01 0.69 ITNA 78GIL 01

1 . 11 ICPES 82J0N 01 0.8 11 ICPES 82 JON 01 1.3 * ICPES 81KNA 01

51
TABLE F

NBS SRM 1569—COLLECTED DATA TABLE F (cont)

ANAL KEF REF ANAL REF ILEF CONC UNCER COMMENT METH CODE NVIM CONC UNCER COMMENT METH CODE NUM

Al (ppm) 2.094 11 NAA 79VER 01 2.096 0.02 24* ITNA 78MCC 01 2000. 56. 11 ICPES 82J0N 01 2.1 0.5 ITNA 79K0B 03

2300. 10. ITNA 78BER 01 2 .119 0.025 24 ITNA 78MCC 01 2.12 0.08 ITNA 78BER 01 As (ppb) 2.13 0.12 7 FAA 80CHA 01 2.17 0.11 ITNA 82GLA 02 80. 1

HAA 82 JON 01 Cs (ppb) 560. 30. 11 HAA 82J0N 01 670. 70. I ENA 82GLA 02 200. L* ITNA 82GLA 02

B (ppm)

Cu (ppm)

6.2 TCGS 82GLA 02

ii. L • ITNA 1 O DEj I\ U 1 Br (ppm) i j .

11 • \ \ I CPE S ft? TON D 1 17.7 0.2 11 ICPES 82JON 01 0.65 0.03 ITNA 78BER 01 18.1 0.7 11 ICPES 82J0N 01

6.7 0.4 ITNA \J J 18 .4 0.3 11 ICPES 82JON 01

Ca (ppm) Eu (ppb)

2270. 70. 11 ICPES 82J0N 01 Zv .

i n T TM A

/ y KU d UJ

2290. 10. 11 ICPES 82 JON 01 2420. 40. i

i i

ICPES 82J0N 01

F (ppm)

2490. 10 1ICPES 82 JON 01 14. 0

i. • ISE 83KNA 01

Cd (ppb)

15 . 2

ISE 83GLA 01

80. 40.

Fe (ppm)

11 ICPES 82 JON 01 120. 70. 11 ICPES 82J0N 01 257. 34. *11 ICPES 82J0N 01 180. 70. 11 ICPES 82J0N 01 499. 15. 11 ICPES 82 JON 01 290. 60. 11 ICPES 82 JON 01 590. 24. ITNA 79K0B 03

660. 15. 1

ICPES 82 JON 01 Ce (ppm) en i 05 5 • Id . 1

QOZJUN 0 Tft M A 1 Ul

0.1 ITNA 78BER 01 707. 16. ITNA 78BER 01

2 .3

Ga (ppm)

460. 30. ITNA 78BER 01 7.1 0.5 ITNA 78BER 01

Co (ppb) Hf (ppb)

260. 20. 130. ITNA 7RRFR 01 ITNA 78BER 01 300. 60. ITNA 79K0B 03

Hg (ppb)

Cr (ppm)

22. CVAA 82GLA 02

0.078 0.026 * FAA 74W0L 01 0.7 0.1 *11 ICPES 82 JON 01

I (ppb)

0.87 FAA 80CHA 01 20. I ENA 82 SAT 01 0.04 60. 1.04 7 FAA 80CHA 01

1 .12 0.08 RTNA 78G0E 01

1 .2 0.6 11 ICPES 82 JON 01 K (%)

1.558 0.015 11 RTNA 78MCC 01 1 .4 0.1 11 ICPES 82 JON 01

2. 0-02 NM 80SHI 01 1.45 0.007 11 ICPES 82 JON 01 2.043 11 NAA 79VER 01 1.45 0.05 11 ICPES 82J0N 01 2.074 0.012 11 RTNA 78MCC 01

1 .55 0.05 ITNA 78BER 01 2.08 0.09 IDMS 79VEI 01 1.59 0.04 11 ICPES 82 JON 01 2.082 0.013 24 ITNA 78MCC 01 1 -71 0.12 ITNA 79KOB 03

52
TABLE F (cont) TABLE F (cont)

CONC

Mg (ppm)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

1730. 70. 11 ICPES 82 JON 01 1780. 100. I TOA 78BER 01 1870. 50. 11 ICPES 82 JON 01 1900. 60. 11 ICPES 82 JON 01 1980. 60. 11 ICPES 82J0N 01

Mn (ppm)

7. 0.8 * ITNA 78BER 01 9.1 0.6 11 ICPES 82J0N 01 9.6 0.6 11 ICPES 82 JON 01 10. 1 .5 ITNA 79K0B 03

10.4 0.8 11 ICPES 82 JON 01

10 .9 0.7 1ICPES 82 JON 01

Mo (ppm)

3.3 0.3 11 ICPES 82 JON 01 3.4 0.1 11 ICPES 82 JON 01

3 .8 0.2 1

ICPES 82 JON 01 3.9 0.2 11 ICPES 82 JON 01

Na (ppm)

510. 30. ITNA 78BER 01 42

ITNA 79K0B 03

Nl (ppm)

4.6 0.3 11 ICPES 82 JON 01 4.8 0.1 11 ICPES 82 JON 01 5.9 0.2 11 ICPES 82 JON 01

6. 0.2 11 ICPES 82 JON 01

P (%)

1. 0.04 11 ICPES 82J0N 01

1 AO A A 1 U.U i

1 1 I 1 ICPES oZ JON U

1 .04 0.05 11 ICPES 82 JON 01

1 flR u • u*+ 1 1 U 1

Pb fnnM

200. 200. n ICPES 82J0N 01

C AA 500. C AA 500 . 1

ICPES 82 JON 01

Kb (ppm;

16. 1 ITNA 78BER 01

Sb (ppb)

75. 5. ITNA 78BER 01 230. 50. ITNA 79K0B 03

Sc (ppb)

180. 10. ITOA 78BER 01 220. 30. ITNA 79K0B 03

CONC

Se (ppm)

092

0.98

1.01

Th (ppm)

3.7

Ti (ppm)

38.

U (ppb)

441.

460.

470.

470.

470.

470.

490.

U-238/235

137.7

V (ppm)

1.46

4.1

4.4

Zn (ppm)

30. 59. 63.

64.

64.

65.

65.

66.

70. 70.

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

009

0.05

0.06

0.2

2.

4. 20. 20.

20.

20.

50. 20.

1.3

0.05

0.1 0.1

4.3

6.

2.

5-4.

2.2.

2.

2.

4.

1111

35

35

35

11

11

11

ITOA

HAA

HAA

ITNA

ITOA

IDMS DNA

DNA

DNA

DNA DNA

ITNA

IDMS

ICPES

ITNA ICPES

ITNA ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ICPES

ITOA

ICPES

78BER 01 82 JON 01

82 JON 01

78BER 01

78BER 01

82 CUR 01 81GLA 03

83GLA 01 80G1A 04

82G1A 02

81GLA 04

78BER 01

82 CUR 01

82 JON 01 78BER 01

82 JON 01

79K0B 03

82 JON 01

82 JON 01

82 JON 01 82JON 01 82J0N 01 82J0N 01 82JON 01 78BER 01 82J0N 01

53
TABLE G

NBS SRM 1570—COLLECTED DATA TABLE G (cont)

CONC UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

Ag (ppb)

65. 40. AA 80JAC 01 65. 10. RTNA 80SL0 01

Al (ppm)

482

.

* ICPES 7 8 CAP 0

1

782

.

31

.

1

1

ICPES 82 JON 01 820. 25. ITNA 83GLA 01 824. 10. ITNA 80SLO 01 829. 23. ITNA 77NAD 02

881. ITNA 78CAP 01

1190. *35 ITNA 81GLA 03

A8 (ppb)

100. L* IENA 83GLA 01 62

.

13. *7 FAA 8 2 HOE 02

1 14

.

U A A HAA 77IHN 0 1 147 . 1 • U TXl A KTNA 79HOE A 1 U 1 150. 10. 11 HAA 82JON 01

150. 13. 7 FAA 8 2 HOE 02

152. 5. 7 FAA 8 2 HOE 02

160. FAA 78CAP 01 160. 10

.

1

1

HAA 82 JON 0 1 170. 20. FAA 80DUP 01 170. 10. H ICPES 82HAH 01 170. 40. RTNA 80SLO 01

170. 10. COLOR 77BUR 01 180. 70. IENA 82GLA 02

180. 20. HAA 80TAM 01

Au (ppb)

0.4 RTNA 80SL0 01

2 . ITNA 79REN 03

B (ppm)

20.9 0.3 ICPES 7 9 HER 01

28 • a /. 0.4 TCGS 82GLA A 9

Ba (ppm)

45- L* ITNA 78CAP 01

13.1 1-8 ITNA 7 7 NAD 02

87. 29. ITNA 79REN 03

Be (ppb)

30. L* ICPES 82KUE 01 60. L* ICPES 78CAP 01 30. L* ICPES 82KUE 01 30. L* ICPES 82KUE 01

Bi (ppb)

8. L* ICPES 82 HAH 01

CONC

Br (ppm)

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

03. ITNA oUTOU 0

1

1 /. 1 .4 5 ITNA 80H0E 01

4 J .b O 1 Z • J

c

J

T CM A 79GLA 02

45. 3.3 ITNA 80SL0 01 45.1 0.3 5 IENA 79GLA 02

46. 2- 5 ITNA 80HOE 01 47. 4. ITNA 83GLA 01 47.2 0.5 ITNA 7 7 NAD 02

48 . 9-4 ITNA 7 9 REN 03

48. ITNA 78CAP 01

52. 4.8 ITNA 79KOB 03

S4 •aj • jj U J J j j 1 ft c. D TTM A ft ft TAT I U 1

11 1ft JO • * FYRTT C/At\r ft 1 P AD U l

C (%)

40.82 0.81 CB 80SCH 02

Ca (%)

0.86 ITNA 80T0U 01 0.82 0.11 * ITNA 01

1 .19 0.09 EXRF 79MAT 01

i 9 i AAA A Q 1 PT A o I OLA A/.

1 .24 0.08 1

1

ICPES 82 JON 0

1

1 .25 0.01 1

1

ICPES 82 JON 01

1 .29 0.03 6 ICPES 82KUE 01

1 .347 0.014 NM 81 YUZ 01

i jj A A9C £.0

1 .36 0.04 11 ICPES 82 JON 01 1.37 0.07 5 ITNA 80TOU 01

1.38 0.014 6 ICPES 82KUE 01

1 .39 0.03 11 ICPES 8 2 JON 01 1.4 0.04 6 EXRF 79MAT 01

1 .46 ITNA 78CAP 01

1 .49 0.1 ITNA 77NAD 02

1 .54 0.01 ICPES 79HER 01

1 .62 ICPES 78CAP 01

1 .78 0.25 * ITNA 79REN 03

2 .45 * EXRF 81 PAR 01

£ • j Li TTPF c 7 ftPAP nU l1

1 9 U • 1 D ACU AO V OOP A T OZufiJ

1 .2 FAA ourtUi U 1

1 .23 0. 16 ASV 82SAT 02

1 .3 FAA 82 PRE 01

1 .32 ASV 78CAP 01

1 .38 0.08 RTNA 80SL0 01

1 .4 0.08 11 ICPES 82JON 01

1 .41 0.03 6 ICPES 82KUE 01

1 .42 0.03 6 ICPES 82KUE 01

1 .45 0.07 6 ICPES 82KUE 01

1 .46 0.04 FAA 80LEG 01

1 .46 0.02 NAA 76DER 01

1 .49 0.08 11 ICPES 8 2 JON 01

1 .52 0.07 RTNA 77DER 01

1 .6 0.2 FAA 81KNA 01

54
TABLE G (coin) TABLE G (cont)

CONC UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

1 .67 0.29 SSMS 77PAU 01

1 .7 0.1 RTNA 76GAL 01

1 .7 0.2 AA 80SCH 05

2. 0.1 AA 76GAL 01 2.1 0.2 ICPES 7 9 HER 01 2.2 1. Ml ICPES 82 JON 01 2.8 0.1 *11 ICPES 82 JON 01

CONC

20.5

21. 21.3

21.8

23 9 24.5

24.8

UNCER COMMENT

*11

*11 *11

*11

*11

*11

ANAL

METH

RTNA

RTNA

RTNA

RTNA RTNA

RTNA

ITNA

REF CODE

REF NUM

76STE 01 77MEL 01 76STE 01 76STE 01 76STE 01 76STE 01 76STE 01

Ce (ppb)

240.

CI (ppm)

6000.

6290.

6500.

6800.

7000.

10000.

Co (ppm)

Cs (ppb)

0.9

1.41 1.47

1 .49 1.5

1.5 1.6

1 .65

1 .68 1.7 1.76

3.2

Cr (ppm)

30.

300.

100. 120. 1000.

26.

0.1

0.1 0.05

0.1 0-2

0.1

0-03

0.1 0.01

0.2

35

L*

RTNA

ITNA ITNA

CPXRF

ITNA

ITNA

ITNA

ITNA PAA

ITNA AA

RTNA

ITNA

ITNA ITNA FAA

RTNA

ITNA ITNA AA

80SL0 01

81GLA 04 78CAP 01

7 9 REN 02

80SL0 01 83GLA 01

7 7 NAD 02

80TOU 01 80YAM 01 78CAP 01 80JAC 01 80SLO 01 79K0B 03

79REN 03

80T0U 01 82H0E 01 77MEL 01 76GAL 01 77NAD 02

76GAL 01

3.06 0.3 AA 80JAC 01 3.5 0.3 6 ICPES 82KUE 01 3.54 0.3 6 ICPES 82KUE 01 3.6 0.5 11 ICPES

* 82J0N 01 3.75 11 AA 79HOE 02

4.3 0.5 ITNA 7 7 NAD 02

4.3 0.7 6 ICPES 82KUE 01 4.4 FAA 82H0E 01 4.4 11 AA 7 9 HOE 02 4.5 0.2 RTNA 76GAL 01

4.5 0.3 ITNA 79K0B 03

4.51 11 AA 79H0E 02

4.6 0.2 11 ICPES 82J0N 01

4.7 0.3 D* DCP 81 REE 01 4.7 0.3 DCP 79REE 01 4.7 0.4 ITNA 82GLA 02

4.8 ITNA 78CAP 01

5.2 0.5 ITNA 76GAL 01

5.2 1-5 AE+AF 82G0L 01 5.8 0.2 AA 76GAL 01

6. 0.7 PAA 80YAM 01 6.2 0.1 ICPES 7 9 HER 01 7.5 1.6 ITNA 79REN 03

200. L* ITNA 82GLA 02

48. 5. ITNA 77NAD 02

64. 2. ITNA 83GLA 01 270. 40. RTNA 77MEL 01 320. 40. ITNA 79REN 03

i in rtm 1

9.1 0.4 * AA 76GAL 01 10.9 0.6 RTNA ftO 1 0\J OLi\J ?! 0 10.9 0-3 1

1

ICPES 82 JON 01 11.1 0.2 11 ICPES 82 JON 01 11.1 0.5 1

1

ICPES 82 JON 01 11.2 0.4 11 ICPES 82 JON 01 11.4 0.5 RTNA 79K0B 01 11.5 0.5 SSMS 77PAU 01 11.5 0.4 FAE 76EPS 01 11.6 0.7 T TM A 1 1 PJrt U 5 n 7 K1NA 78K0B 01

11 .8 0.3 RTNA 77DER 01 11.8 0.3 6 ICPES 82KUE 01 11.8 2.5 VV 80SCH 05

12. 0.3 6 ICPES 82KUE 01 12.06 0.03 COLOR 7 7 BUR 01 12.1 0.2 ICPES 79HER 01 12.1 AA 80EVA 01 12.1 0.1 COLOR 7 6EPS 01 12.2 0.1 6 ICPES 82KUE 01 12.3 T PDF C 7 Q r AD U 1

1 Z . J 1

1

AA 79H0E 02

1 L .0 FAA 78CAP 01 12.6 1.4 6 EXRF 79MAT 01 12.7 0.4 AA 7 6EPS 01 13. 1. D* DCP 81 REE 01

13. 1 . DCP 7 9 REE 01 13.2 *11 AA 79H0E 02

Eu (ppb)

200. L* ITNA 78CAP 01

14. 1 . ITNA 79K0B 03

20. 1 ITNA 7 7 NAD 02

F (ppm)

4.3 0.4 ISE 83KNA 01 4.4 0.3 ISE 83GLA 01

Fe (ppm)

178. 2. D* DCP 81 REE 01 470. 50. 6 ICPES 82KUE 01 478. ICPES 78CAP 01

55
TABLE G (cont)ANAL REF REF CONC UNCER COMMENT METH CODE NUM

491

.

20. 11 ICPES 82J0N 01 494. FAA 78CAP 01 510. ITNA 78CAP 01 511. 7. ICPES 79HER 01 518. 8. 11 ICPES 82 JON 01 522. 14. 11 COLOR 82SCH 03

525. 11

.

6 EXRF 79MAT 01 530. 11. 6 ICPES 82KUE 01 540. 18. ICPES 80SCH 05

540. 23. ITNA 79K0B 03

540. 10. 6 ICPES 82KUE 01 541

.

15 . 1

1

ICPES 82 JON 01

. AA 80EVA 01

Sift Q HUbUZ Ul

551

.

i i 1 X A A 7QUAT? AO 556

.

1 l i i X X pat np Q o c raj a *j 557. 8. RTNA 80SL0 01 557. 19. 11 ICPES 82 JON 01 557

.

8. ITNA 79DAS 01 566. 18. ITNA 77NAD 02

570. 11 AA 79H0E 02

597. 6. 6 EXRF 79MAT 01 600. 90. 35 ITNA 81GLA 03

660. it UNA 7QD17W Cil /yKJiN U J 763. 34. * RTNA 77MEL 01 1200. * EXRF 81PAR 01 Ge (ppb)

20. L* ICPES 82HAH 01

H (%)

5.54 0.08 CB 80SCH 02 5.6 0.1 35 TCGS 79GLA 04

Hf (ppb)

40

.

20

.

RTNA 80SL0 01

Hg (ppb)

25. 11 CVAA 79H0E 02

26 . 8- RTNA 80SLO 01 30. 5

.

CVAA 82GLA 02 33

.

16 . CVAA 82D00 01 34. 3. ITNA 7 7 NAD 02

110. 20. * RTNA 77MEL 01

I (ppm)

1 .08 0.16 IENA 82 SAT 01 1.1 0.2 PAA 77WIL 01

1 .267 0.054 35 RTNA 81 ALL 01

1 .325 0.055 RTNA 81STR 01

1 .325 0.055 34 RTNA 81 ALL 01

In (ppb)

1.2 0.1 RTNA 78K0B 01

1 .3 0.2 RTNA 79K0B 01

CONC

TABLE G (cont)ANAL REF REF UNCER COMMENT METH CODE NUM

K (%)

J .ZD U.Z J

T TH A 79REN A 7

1 ">Q j .zy A 1 Q T C DT? O 7 9 HER a t U I 7 A 7 a i i U . 1 1 ITNA 7 7 NAD UZ

J OZ a i 0.1 6 ICPES 82KUE 01

J J J n n 7 o U • U jZ O ICPES OZK.UL A 1 Ul

7 ^ A ITNA oUEDD 0

1

3.56 1 AA 78SZY 01 3.57 0.04 6 ICPES 82KUE 01 3.59 ICPES 79C00 01

3 6 0 2 11 ICPES 82J0N 01

73-Dft, A AQ T TU A 1 i N A 79K0B A 7

J .61 1 AA 78SZY 01

7 £.1 3.61 0.35 ITNA 82EHM 01

3 .7 0.04 1

1

ICPES 82 JON 01 3.7 0.1 11 ICPES 82J0N 01 ITNA 78CAP nU i1 3.74 0.07 ITNA 80SLO 01

3 .9 0.

1

1

1

ICPES 82 JON 01 4.04 0.06 *6 EXRF 79MAT 01

A ft 5 ft HI D E.AIVT 7QMAT U 1 7.95 * EXRF 81 PAR 01

(ppb)

700. L* ITNA 78CAP 01 260. 50. RTNA 80SL0 01 320. 30. ITNA 7 7 NAD 02

350. 60. ITNA 79REN 03

(ppb)

5 . L* RTNA 80SLO 01

(ppm)

7000. * ICPES 78CAP 01 7300. 500. ITNA 80SLO 01 8400. FAA 78CAP 01 8550. 65. 6 ICPES 82KUE 01 8600. 400. 1

1

ICPES 82 JON 01 8600. 230. 6 ICPES 82KUE 01 8700. 100. ICPES 7 9 HER 01 8790. 150. 6 ICPES 82KUE 01 8800. 100. 11 ICPES 82 JON 01 8900. 300. 1

1

ICPES 82JON 01 9000. 600. ITNA 78CAP 01 9000. 200. 11 ICPES 82JON 01 9800. ITNA 77NAD 02

(ppm)

1 .3 0.1 D* DCP 81 REE 01 49. 2. *11 ICPES 82 JON 01 102. 3. * AA 76GAL 01

118. 3. * ITNA 76GAL 01 146. 32. AE+AF 82GOL 01 155. FAA 78CAP 01 156. 11 AA 7 9 HOE 02

156. 5- ITNA 79KOB 03

157. ICPES 78CAP 01

56
TABLE G (cont) TABLE G (cont) ANAL R£F REF CONC ' UNCER COMMENT METH V\JaJC Hl/M

158. 7

.

1

1

ICPES ft? TON 0 1 159

.

AA 7QHOF 0? 160. 35 ITNA Olu Ijrt U H 160. 3

.

1

1

ICPES O? TfiM 0 1

1 D 1 •

f.D . T TM A 1 1NA / / NAD U Z 10 2 . 9

.

ITNA 83GLA 01

lb d .

•35 . 6 EXRF /9MAT 01

1 D D . J > 0

qoZNUIj ? vm? mU 1 166

.

CJ .1 1 X 1 ICPES ft? TON 0 1 166

.

J . ICPES 79HFR 01 167. 6. 1

1

ICPES 82J0N 01 168. 3

.

VV R0SCH OS

169. 4. ITNA 80SL0 01 170. AA 80EVA 01 171 . 1

.

6 ICPES 82KUE 01

171 . ITNA 78CAP 01 172

.

5. 6 ICPES 82KUE 01 178. 2. DCP 79REE 01 184. 10. 6 EXRF 79MAT 01 187.9 18.9 PAA 80YAM 01 200. * ITNA 79REN 03 EXRF 81PAR 01

Mo (ppb)

300

.

L* ICPES 82KUE 01 5000. L* ICPES 78CAP 01 inn jUU . T * Lj ft 9 VI IP O 1 300. L* ICPES 82KUE 01 200. 100. 11 ICPES 82J0N 01 200. 100. 11 ICPES 82 JON 01 300. 100. RTNA 80SLO 01 300. 100. 11 ICPES 82JON 01 400

.

200

.

1 1 ICPES a? ion 0

1

5 .62 0.11 CB 80SCH 02

6. 0.4 35 TCGS 79GLA 04

Na (%)

1.13 0.02 ITNA 80SL0 01

1 .28 0.1 ITNA 82SCH 05

1.31 0.07 ITNA 7 7 NAD 02

1 .33 0.05 ITNA 79KOB 03

1 A "3 T TM A 1 INA

1 .44 ITNA 7oCAP 01

1 .48 35 ITNA 81GLA 04

1 C A

1 .54 0. 14 ITNA /yRLN OJ

1 OD l AAA A 1QC7V O

1

1 . J O

ii rtrt A A 7QC7Y fl 1

Ni (ppm)

1 .3 0.1 * DCP 79REE 01 2.3 0.5 * RTNA 80SL0 01 4.1 0.5 ITNA 7 7 NAD 02

4.9 0.2 11 ICPES 82 JON 01 5.1 0.1 11 ICPES 82 JON 01 5.12 VOLT 81PIH 01 5.4 1. 6 EXRF 79MAT 01

CONC

ANAL REF REF UNCER COMMENT METH CODE HUM

5.4 0.1 11 ICPES 82JON 01 U • 1

1 1 1 1 ICPES 82 JON 0

1

5.51 0.32 6 ICPES 82KUE 01 6.03 0.52 6 ICPES 82KUE 01 6.1 0.2 PAA 80YAM 01 6.17 0.72 6 ICPES 82KUE 01 6.5 0.2 RTNA 78KOB 01 6.5 0.3 RTNA 79KOB 01 7.5 0.5 RTNA 77MEL 01

8.1 FAA 82HOE 01

8 .

1

0 .

2

7QHFR 0 1

(ppm)

A son ICPES 78CAP 0

1

5100. FAA 79EDI 01 5200. 200. 11 ICPES 82JON 01 5240. 70

.

tD ICPE S ft? OZ VTTP 1 J.J i nV il 5300. 100. 1

1

ICPES 82 JON 01

5 300 70- 6 ICPES 82KUE 01 5350. 45. 6 ICPES 82KU2' 01

5 360. 270. ICPES 810WE 01 5400. ICPES 79ED1 01 5500. 200. 1 1 ICPES 82 JON 01 5600. 400. 7 NM 81 SHI 0! 5700. 200. 1 1 ICPES 82 JON 01

6 000

.

100. ICPES 79HER 01 (ppm)

3.5 L* ICPES 7 8 CAP 01

3.8 L* ICPES 82KUE 01 3.8 L* ICPES 82KUE 01 3.8 L* ICPES 82KUE 01 0.8 0.3 11 ICPES 82JON 01 0.8 0.1 11 ICPES 82JON 01

1

.

0.1 FAA 80LEC 01

1 - 0.8 ICPES 79HER 01 1.02 FAA 82HOE 01 1.03 0.15 ASV 82GAJ 01

1 .04 0.09 ASV 80SZY 01 1.09 0.06 FAA 79DAB 02

1.1 0.2 FAA 81KNA 01 1.1 0.1 AA 80SCH 05

1.1 0.08 ASV 82SAT 02

1.1 1

1

FAA 79H0E 02 1.12 0.03 SSMS 77PAU 01

1 . 16 0 .08 FAA 82 RAI 0

1

1.2 FAA 80PRE 01 1.25 ASV 7 8 CAP 01 1.3 6 FAA 81HIN 01

1 .3 0.4 HAA 82WEI 01

1 .3 FAA 82PRE 01

1 .3 6 FAA 82KOI 01

1 .4 6 FAA 81HIN 01 1.4 6 FAA 82KOI 01

2. 1 .4 * PAA 80YAM 01

(ppb)

2 . L* RTNA 81BYR 01

57
TABLE G (cont) TABLE G (cont)

ANAL REF REF ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

Pr (.ppb;

60. L* RTNA 80SL0 01

Rb (ppm)

10. ITNA 78CAP 01

11 . 1

35 ITNA 81GLA 03

11.32 3 .

7QDFM no

1 1 .6 0.3 TA TMA inn 77NAn n7

17 . 3. PKTMA 1 ISA 7/ 7MFT / I LEI L. HI\J 1 39 . * EXRF Q 1 n AD A 1

S ( DDITI J

2400. 600. CPXRF 79REN 02

Sb (ppb)

1 L J • n ICPES 8 2 HAH 01

27 . 6. ITNA 77NAD 02

31. 1RTNA ftnvn<! n?

38. 3. RTNA 79HOE 01 44. 2. ITNA 7QVOR 1 7 l\\J D niU J 50. ITNA 7BCAP Ul

50. 20. RTNA 80SLO 01 690. 150. * ITNA 79REN 03

Sc (ppb)

340. L* ITNA 80T0U 01

150. 30. 5 ITNA 80T0U 01

160. ITNA 78CAP 01

170. ITNA 80EDD 01

I / u

on RTNA 80SL0 01

170. 4 t ITNA 77NAD 02

180. 10ITNA 79K0B 03

180. 20 - RTNA 77MEL 01 470. 40 - * ITNA 7 9 REN 03

Se (ppb)

100. L* HAA 82 JON 01 100

L* RTNA 77MEL 01

_> » ICPES 82HAH 01 Ann ITNA 78CAP 01

100. L* HAA 82 JON 01 24. 10. 9 ITNA 80WAN 01 25. FAA 78CAP 01

33. 3. 11 GC olUCH 02

33. 3. 11 IjVj Q 1 1 1 m A o 0 1 U L-n O £. 37. FLUOR 79WAT 02

40. 10. RTNA 80KNA 01 42.9 HAA 77IHN 01

60. 20. RTNA 80SL0 01 66. 9. ITNA 77NAD 02

510. 80. * RTNA 82P0L 01

Sm (ppb)

12000. L* ITNA 80T0U 01

33. 4. 5 ITNA 80T0U 01

CONC UNCER COMMENT METH CODE NUM

80. 20. RTNA QAC1 A A 1 200. 140. ITNA 79REN 03

Sn (ppb)

20. L* ICPES 82HAH 01 3.1 ICPES 78CAP 01

Sr (ppm)

79. 1. ICPES 79HER 01 82.5 15.8 AE+AF 82G0L 01 EXRF 81 PAR 01

0.23 ITNA 79REN 03

Th111 fooh'i \\J\JU )

1 10 . 10. ITNA 77NAD 02

150. 40. RTNA 80SLO 01

Tl (ppm)

16.5 ICPES 78CAP 01

Tl (ppb)

31

5. S SMS 1 /PAU O

U (ppb)

42. DNA 83CLA 01 45. 0.8 35 DSA RftCLA 04 69. 120. R* DSA 81CLA 03

V (ppm)

1 .06 0. 17 ITNA 77NAD 02

1.08 0.07 D* DCP 81 REE 01 1.08 0.07 DCP 79REE 01 1.13 0.01 RTNA 78BYR 01 1.2 0.06 ITNA 76GAL 01 1.28 0.07 11 ICPES 82 JON 01 1.34 0.06 11 ICPES 82 JON 01

1.7 * ITNA 78CAP 01

W (ppb)

140. 50. RTNA 80SL0 01

Yb (ppb)

2. 1. RTNA 80SL0 01

Zn (ppm)

42. 2. RTNA 80SL0 01 45.9 2.8 RTNA 77DER 01 46. 2. 11 ICPES 82 JON 01 46. 1. 11 ICPES 82 JON 01

/

58
TABLE H

TABLE G (cont)ANAL REF REF CONC ' UNCER COMMENT METH VWS HUM

46.2 0.6 1

1

46.7 11 AA 7QHOF 0?

47. 0.48 ITNA 7 9 REN 03

48. 2. 11 ICPES 82 JON 01 48. ICPES 78CAP 01 48. 1

.

1

1

ICPES

48

.

•>j .

4ft o

J .

1 1 1

1

ICPES 82 JON 01

Aft ITNA 78CAP 01

AO *> A 1 0.1 PAA 80YAM 01 AO ^ n t 0.7 SSMS 77PAU 01

AO Q 1 .3 6 ICPES 82KUE 01

i1

.

ITNA 77NAD 02

jV .0 1.3 6 ICPES 82 KITE 01 50.8 A A AA B0EVA 01

51 .2 U . D 0

T/»nff C XL-rES oZKUE 01 52

.

J . nrp ULr q 1 ore f\ 1 52. 1 . DCP 7QRFF 01 52. 2.2 ITNA 79KOR m

52.9 2.2 6 EXRF 79MAT 01 53. 3. 11 ICPES 82 JON 01 53. 11 AA 79H0E 02

54. 1. ICPES 7 9 HER 01 57. 8. RTNA 77MEL 01 59.7 FAA 78CAP 01 60.1 2. 6 EXRF 79MAT 01 72.5 1.6 * RTNA 76GAL 01 72.8 1.3 * AA 76GAL 01

119. * EXRF 81PAR 01

NBS SRM 1571—COLLECTED DATA

ONCER COMMENT

ANAL

METH

REF CODE

REF NUM

13. 620.

Al (ppm)

99. 103.

110.

128. 140.

146.

157. 165.

196.

201

.

223.

231.

243.

255.

278.

296.

322.

322.

330.

333.

343.

343.

347 . 347 . 349 .7 350.

359.

37 7. 378. 380.

380.

383.

390.

398. 407.

420.

430.

430.

440.

460.

460.

470.

500.

520. 824.

As (ppm)

1.1 3.5 7.5

8.8.5

20.

100.

5. 60.

22.

140.

8. 20.

30. 22.

18.

460. 460.

7.5

7.5

6.1

4. 21.

13.

100.

50. 24.

11. 58.

40.

33.

7.

180.

50.

6R*

11

R*

R*

35

1.6

1.0.3

ITNA OES RTNA

RTNA

OES

ITNA AA

OES

ICPES ICPES

ICPES

OES

OES

OES

OES

OES

OES

OES

OES

ITNA

14NAA

ICPES NAA

ITNA

ITNA

ITNA POL

POL

ITNA ITNA

IENA

ICPES

ITNA ITNA

14 NAA

ITNA AA

ITNA

ITNA

ITNA

ITNA CPAA

RTNA

ITNA VV

ITNA

ITNA FAA

ITNA

ITNA

CPXRF

SSMS PAA

HAA

02

01

74RAN 02

75BOL 02

80SLO 01 74CAR 03

7 5JON 02

74H0F 01 75MAN 01 75JON 11 81BLA

7 9 ABE 78CAP 01 75J0N 07 75J0N 06 75JON 01 75JON 09 75J0N 04

75JON 08

7 5J0N 05

7 5JON 10 77ZIK 01 81WIL 01

82 JON 01 77LAU 01 76BAT 01 79IMA 03

79IMA

72MAI

77MAI 77G00 01 78LAU 02

79JON 01 79MCQ 01 75RIC 01 83GLA 01 81WIL 02

78CAP 01 79MCQ 01 82EHM 01 74H0F 01 77HAM 01 74RAN 02

80HAN 01 72MOR 03

79KOB 03

81N0N 01 81GLA 03

80CRE 01 77FUJ 01 80SL0 01

01

0101

78KEL 02

80KIR 01 81VER 02

80SEG 01 74L00 01

59
TABLE H (cont)ANAL KEF K£F CONC ' UNCER COMMENT METH CODE NUM

14 .

6 NAA 78GAN 01 14-3 * XRF 78CAM 02

14.3 0.4 * EXRF 77NIE 01

15. 0.1 * RTNA 77BAN 03

15.3 0.5 * EXRF 7 3 SPA 01 15.3 2. * ITNA 79AHM 01 15.4 0.2 *19 ITNA 74RAN 02

110A -

•> LrX Kr "? AM f\ 1 / / CAM U

16. * AA 79HIL 01

17 . k CPXRF 76ZEI 01

17. * CPAA 78MCG 01

Jo . EXRF 81 PAR 01 Ast l 11 ) (.ppm;

4 .9 HAA 76AGG 01

Au ( D dd ^

0.78 0.15 ITNA 7 9 REN 03

0.97 0.09 RTNA 77NAD 01

i PTNA 79MOR 01

1 . TTHA

1 .2 1

"7 Q viiP n 1

1 .4 T TXT A 1 1NA o 1 K.UL U

1 .4 0.5 I ENA

q i vr\ c n i o 1 K.U o U 1

1 .5 4 . DTM A ofiCT OUoLUn C\UI1

1 .5 ITNA 79KUC 01

1 .5 0.5 RTNA 77KUS 01

1 .64 0.1 ITNA 77MIN 01

1 .8 0.3 ITNA 81HAB 01

1 .8 1 IENA 79KUC 01

2 . 0.8 ITNA 81K0S 01

3 .5 0.6 * RTNA 74CAR 03

R ( vt nm ^

lb .

1 0 TTHA on ecu C\ ^ 22.55 *6 AE+AF "7 / nil) j-ll 7 4DAU 0

23

0ES /3J0N 10 24

2 . ICPES /yHbR UI 23 . 13 £.O 07LI . 7 S TON OS

^97/ . 0ES 7 5JON 02

30. 0ES 7 5JON 01 31.2 2.8 NM 79YAN 01

31 .9 4.7 14 FAA 79SZY 01

32. 4. ICPES 79ABE 01

32. 0ES 7 5JON 04

32. 0ES 75J0N 09

19K 0. L

fiu • A•» 1 7 Q ANH 0 1 / J Ail U UI

32 .5 U . D UULUK / 7 I AN U 1 32.8 2 .3 6 TCGS /0GLA UI

J J

4 . CPAA oUrlAN U 1 1 1 Jjt z

1

7QUT7 (\ \ Jj. n v c 1 jJUPJ UO

33. 0ES 7 5JON 07 33.2 0.1 TCGS 79FAI 01 33.3 2.3 6 TCGS 76GLA 01 33.4 0.7 ICPES 81KNA 01 34. 1 11 ICPES 79MIZ 01 35.1 9.9 14 FAA 79SZY 01

36. CPAA 81SAS 02

TABLE H (cont)ANAL REF R£F CONC UNCER COMMENT METH CODE NUM

36. 0ES 7 5J0N 03

36. 3. CPAA 81SAS 01

36. 5- CPAA 7 5MCG 01

38. ftps 75J0N 08

ioJO • 75J0N 11 AO . 1 . 1

I CPE S 7QMT7 01

(ppm)

230. L* ITNA 80TOU 01

240. L* 14 NAA 81WIL 01

0-3 0.1 * CPXRF 77RIN 01 14.7 * SSMS 81VER 02

25.9 6.8 * ITNA 81HAB 01 28. * ITNA 80CRE 01

30. NAA 7 4 BEL 01

37. 11. 5 ITNA 80T0U 01

37 .9 1 IENA 79KUC 01

38. 4.7 CPXRF 80KIR 01

38. 0ES 75JON 05

39.4 ITNA 79KUC 01 40. NAA 77LAU 01 40. 3

9 ITNA 78LAU 02

40. 0ES 7 5JON 03

41. 4. ITNA 79SAT 01 41. 1.3 RTNA 77GUI 03

42. 2. ICPES 79MCQ 01

42. 6- ITNA 78LAU 02

42. 2. ICPES 79MCQ 02

43. 5.7 ITNA 77HAM 01 43. OES 75J0N 11 43.9 1 IENA 79KUC 01 44. 57. R* AA 75MAN 01 44.3 AA 74BUS 02

44.8 2.5 IENA 81K0S 01

45. ITNA 78CAP 01

45. OES 7 5J0N 04

45. 6. VV 81N0N 01 45.3 2.7 ITNA 81K0S 01 46. 6. ITNA 74RAN 02

47. 3. ITNA 81KUL 01

51 . RTNA 72M0R 03

51 .3 4.5 PAA 74CHA 01 ICPES 78DAH 01 52. OES 7 5J0N 01

1.81 * ITNA

62. 21. * ITNA 77ZIK 01

80. 22. * 14 NAA 81WIL 02

(ppb)

60. L* 78CAP 01 13.7 1 .8 5 ICPE S 82SCH 01 14.8 1.6 6 ICPES 82SCH 01 26. 1

FLUOR 77WIC 01 30. 4. VV 74FLO 01

36. 4. 11 FAA 7 50WE 01 67. 7. *11 FAA 750WE 01 110. 10. * GC 73BLA 01

60
TABLE H (cont) ice ur ace Mr

ONC * IJNfFB COMMENT METti CODF MUM

X ' i. J TTNA L inn 7QDTTM / fi^ y noli* u j

ft 7 0.2 RTNA

8.8 0.4 ICPES ftOHAA 01 8.9 2 .2 ICPES ft 1 NAD ni 9. RTNA 7 5ABU 0

9. 0.4 H ICPES 79ROB 01 9.1 1 IENA 79KUC 01 9.2 ITNA 79KUC 01 9.27 HAA 77IHN 01 9.3 35 HAA 77TAM 01

9.1

HAA 76VIJ 02

HAA 81 INI] 01

n 7 a PTNA 7QHFT OA

7 . D PTNA OUoLU VI

0 ^ U.J i i HAA o x ivnr u x 0y <j 0 ft RTNA 79R0S 02 FAA 82HEI 01 9.6 0.3 11 HAA 81 RAP 01

9.68 0. 14 NAA 74HEY 01 9.7 0.4 7 RTNA 77GIL 03

9.7 0.12 RTNA 72BYR 01 9.7 0.3 RTNA 79KAN 02

9.7 0.4 ITNA 75RIC 01 9.7 0.4 RTNA 78GAL 01 9.76 0.17 RTNA 79H0E 01 9.8 0.9 ESCA 78CAR 01

4y ft . o 0.1 HAA 81KNA 01

Q ft y • o U.J RTNA 8? COR f)l o ft n o 1 D V X U \J £. 0 ft nu l • 1

1

HAA ftO i1 prvruap n i VJ X Q ft nKJ . aH |] ICPES RIPIC 01 9.9 0.1 IENA 78WAN 01 9.98 0.31 HAA 80TAM 01 10. RTNA 72M0R 03

10. 14. R* ITNA 79IMA 03

10. HAA 79PEA 01 10. 0.1 VV 81N0N 01

10. RTNA 79BYR 01

10. 2. ITNA 77MIN 01

10. 14. R* ITNA 79IMA 01

101

EXRF 80DYC 01

10

0.4 RTNA 78GIL 01

102

COLOR 79MCQ 01

10 .0.4 IENA 81K0S 01

10 .0.3 7 RTNA 7 7GIL 0 3 10 .1 0.2 19 ITNA 74RAN / " I\ rUl 02\J L- 10.1 ITNA 80CRE 01 10.1 0.8 EXRF 79GIA 01 10.1 0.3 RTNA 78WEE 01 10.14 ASV 78DAV 01 10.2 1

PAA 74CHA 01 10.2 1. NAA 77JER 01 10.2 HAA 80HON 01 10.2 0.2 HAA 77SMI 01 10.2 0.2 COLOR 77BUR 01 10.2 35 XRF 77TAM 01 10.3 0.9 ITNA 81K0S 01 10.3 HAA 81ARA 01 10.3 0.2 HAA 80AGE 02

10.3 0.4 7 RTNA 77GIL 03

10.3 0.2 34 HAA 78FLA 01 10.3 1.6 RTNA 79REN 01

TABLE H (cont)ANAL REF REF CONC UNCER COMMENT METH CODE NUM

10.4 0.4 ITNA 78LAU 02

10.43 0.22 HAA 81UTH 01 10.5 1 IENA 79KUC 01 10.5 1. PAA 76KAT 04

10.5 ITNA 82AKA 01 10.6 ASV 81LEE 01 10.6 0.8 RTNA 740RV 01 10.6 0.3 14NAA 81WIL 01 10.6 0.8 EXRF 73GIA 01 10.6 0.5 14NAA 81WIL 02

10.7 0.4 FAA 78HAY 01

10.7 1. 6 ITNA 74BEC 01 10.8 HAA 81BR0 01 10.8 IENA 83GLA 01 10.8 FAA 78CAP 01

10.8 0.5 IENA 82GLA 02

10.8 0.9 RTNA 76MEL 01

10.8 6 NAA 78GAN 01 10.82 0.25 HAA 77YAS 02

11. ICPES 79MCQ 02

11. 2. RTNA 77KUS 01 11. 1. PAA 76KAT 02

11. 3. ITNA 77ZIK 01

11. ICPES 79MCQ 01

11. 0.6 PAA 78HIS 01

11. 1. HAA 76FI0 01 11.5 0.5 HAA 81YAN 01 11.5 1.5 RTNA 74G0E 01 11.5 0.47 HAA 81YAN 01 11.5 0.3 GCMES 75TAL 01 11.6 0.27 H HAA 76SIE 01 11.6 1 .8 RTNA 79NIC 01 11.6 HAA 77SIE 01 11.6 1.3 ITNA 74NAD 02

11.8 0.8 SSMS 77D0N 01 11.9 0.2 ITNA 81HAB 01 11.9 H FAE 79FEL 01 11.9 0.1 FAA 80DUP 01

11.98 0.08 H ICPES 81PAH 01

12. 0.6 AE+AF 82MAT 01

12. 2.5 ITNA 77HAM 01 12. 3. ITNA 81KUL 01

12. 0.6 11 HAA 82 JON 01

12. 2. HAA 79ST0 01

12. RTNA 74ERD 01

12. 0.38 HAA 82TAM 01

12. 2.6 EXRF 75REU 01

12. 1 . ITNA 76KUC 01 12.15 0.43 NAA 76GUZ 01 12.3 0.2 ITNA 79K0B 03

12.3 0.4 RTNA 73TJI 01

12.7 2. ITNA 82QUR 01 12.7 0.7 ITNA 79JER 01 12.9 0.4 11 HAA 82 JON 01

13. 3. CPAA 77ZIK 01

13. 0.1 ITNA 75BOL 01

13. 1

H ICPES 82HAH 01 13.2 CPXRF 75CAM 01 13.3 0.4 HAA 76WAU 01 13.4 0.93 COLOR 73LEB 01 13.5 HAA 76AGG 01

14. 1

ITNA 78FUR 01

61
TABLE H (cont) TABLE H (cont) ANAL REF REF ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METM CODE NUM

(ppb) 11. ITNA 78CAP 01

1 1 IX* 0.7 5 ITNA 80TOU 01

8- L* ICPES 82HAH 01 12. 1 .3 ITNA 79AHM 01

4. ii

n ICPES 81PAH 01 12. 3. ITNA 77ZTK 01

jy • FAA 79INU 01 12.5 * ITNA 82AKA 01

1 10. 20. POL 77MAI 01 34. * EXRF 81PAR 01

110. 20. POL 72MAI 01

C (%) 1 10

100. POL 74MAI 01 64000. * FAA 82HEI 01 45.76 0.51 CB 82GLA 02

(ppm) 45.8 1 .3 35 CB 79GLA 04

46. 2 . TCGS 7 9 FAI 0

1 Q Li71 ITNA 80T0U 01 46.35 0.31 CB O \J J\jti \J £.

cJ

47. Ej • 7QPT A f\L 5

ITNA 77ZIK 01 52. 5

* TCGS 79AND 01 6.3 2. * EXRF 7 7 FLO 01 Ca (%)

6.6 0.4 *5 I ENA 79GLA 02

6.6 0.4 EXRF 7 3 SPA 01 3

L* 14NAA 81WIL 01

7.1 EXRF 81BIS 01 1 .58 * 35 AA 81GLA 04

7.3 9.3 R* ITNA 79 IMA 03 1 .6 2.26 R* ITNA 79IMA 01 7.3 3.2 CPXRF 80KIR 01 1.6 2.26 R* ITNA 79IMA 03

7.3 9.3 R* ITNA 79 IMA 01 1.63 * OES 7 5J0N 07 7.4 0.2 ITNA 75RIC 01 1.74 * OES 75J0N 05

7.8 0.3 EXRF 80DYC 01 1.8 NAA 77LAU 01 8.2 RTNA 72M0R 03 1 .8 OES 75J0N 02

8.2 0.6 ITNA 80SL0 01 1 .81 0.24 5 ITNA 80TOU 01

Q 1 8 . i 0.5 5 ITNA 80HOE 01 1 .81 ITNA 82AKA 01

R AR u . u / cJ ITNA 80H0E 01 1 .83 0.07 CPXRF 80KIR 01 8.5 0.5 6 ITNA 74BEC 01 1 .86 0.1 14 NAA 77VAN 01 8.7 ITNA 83GLA 01 1.9 0.11 ITNA 79REN 03

8.8 0.6 5 I ENA 79GLA 02 1.91 OES 7 5JON 10 8.8 1 .6 EXRF 75REU 01 1.92 EXRF 81BIS 01

9. 0.5 EXRF 79GIA 01 1 .93 0.07 EXRF 79KUE 01

9. 0.5 ITNA 78LAU 02 1 .932 0 .09 ITNA 77ZIK 01 9.1 0.5 ITNA 78WEE 01 1 .94 OES 7 5JON 04

9.19 1.39 TTNA 7QRFN D3U J 1.96 0.06 FE 78K0R 01 9.2 0.2 ITNA 74RAN 1.96 0.002 1

AA 75ISA 01 9.2 ITNA O \J V_/ 1\ L_i 01 1.97 0.03 11 ICPES 82J0N 01 9.3 0.6 EXRF 73GIA 01 1.97 0.055 PAA 76KAT 04

9.3 1.4 RTNA 78WEE 01 1.97 0.15 14NAA 81WIL 02

9.4 ITNA 79KUC 01 1.97 0.08 TCGS 79AND 01 9.5 1. EXRF 77NIE 01 1 .97 0.05 PAA 76KAT 02

9.5 0.8 RTNA 76MEL 03 1 .98 0.05 ICPES 79MCQ 02

9.5 XRF 78CAM 02 1 .98 0.04 11 ICPES 82 JON 01 9.5 1 I ENA 79KUC 01 1.98 0.08 EXRF 75REU 01 9.5 1 I ENA 79KUC 01 1.98 0.07 ICPES 79MCQ 01

9.6 2.8 ITNA 77HAM 01 1.99 0.06 EXRF 77NIE 01 9.6 1.2 6 NAA 78GAN 01 1 .99 XRF 78CAM 02

9.7 1.1 ITNA 78GIL 01 2. OES 75ISA 01 9.8 0.78 ITNA 77STE 02 2. n or ITNA 80SL0 01 9.8 0.8 RTNA 79CR0 01 2.01 AA 79MCQ 01 9.9 0.2 I ENA 81K0S 0

2.01 fl 1 R RTNA 80CAN 01

10. 1

ITNA 76KUC 01 2.02 0.11 EXRF 82 DAK 01

10. 2.1 VV 81N0N 01 2.02 0.002 11 AA 75ISA 01 10.1 0.8 ITNA 77GUI 02 2.03 ICPES 78DAH 01 10.2 1. ITNA 81KUL 01 2.03 0.04 11 ICPES 82 JON 01 10.5 1.4 ITNA 79CRO 01 2.03 0.02 11 ICPES 82 JON 01 10.5 0.6 ITNA 81K0S 01 2.039 0.06 CPAA 77ZIK 01 10.8 0.9 6 NAA 78GAN 01 2.04 OES 7 5JON 03

10.8 0.4 35 NAA 81GLA 03 2.04 AA 80URE 01 10.9 ITNA 80SAT 01 2.04 0.02 11 AA 78GAI 01

11. 1.2 ITNA 79KOB 03 2.06 COLOR 77HAM 04

62
TABLE H (cont) TABLE H (cont) ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

7 A7

Z .0/ AU .UoAA TFNA 7Q TOW n l 7 AO I .Uo AU .UZAO 1 1 1 1 AAA A 7RfiAT / Ounl

7Z .UoAQ nUtUlni PAA 74CHA 01

2 .08 0.04 ITNA 79KOB 03

2 .08 0.06 ICPES 7 9 ABE 01

2 .08 0ES 75JON 09

2 .08 0ES 75JON 11 2.1 RTNA 72MOR 03

2.1 0.2 14NAA 80FAA 01 2.1 0.08 6 EXRF 79MAT 01 2.1 0.05 ITNA 81K0S 01 2.1 0.2 ITNA 78LAU 02

2.11 ICPES 81WEI 01

2.11 AA 79HIL 01 2.11 0.08 g EXRF 79MAT 01

2 1 12 0.07 IENA 81K0S 01

7 1

1

0.09 ITNA 75RIC 01 2.13 SSMS 81 VER 02

2-13 0.11 TCGS 79FAI 01 2.13 ITNA 7 6 BAT 01 2.14 0.02 ITNA 78FUR 01 2.145 0.017 CPXRF 81R0B 02

2.15 COLOR 80LAU 01

2.15 ITNA 78CAP 01

2.17 OES 75J0N 08

2.17 0.03 EXRF 80DYC 01

2.2 0.1 ITNA 81KUL 01

2 .2 0.02 ICPES 79HER 01

2 .2 0.05 PAA 78HIS 01 2.21 0.15 ITNA 77HAM 01 2.28 CPAA 80HAN 01 2.29 0.04 VV 81N0N 01 2.29 OES 7 5JON 06

2.41 * OES 75JON 01 2.46 0.09 *5 ITNA 80TOU 01 2.63 * ICPES 78CAP 01

5.01 * EXRF 81 PAR 01

»pb)

300. L* AA 73LOO 03

200. L* PAA 80SEG 01

50000. L* RTNA 72M0R 03

L* PAA 78HIS 01 Z3UU 7 ^ AA • Lt H 7 on ad AU 11

1 AA 1 UU . DAI rUL A 1 U 1

1 Q AA ATT C 7 £ DAT A 7 U L

1 AA 1 UU

.

Li" DAI rUL 7/ O CT V Z ol N A 1 U 1 7 A K1NA Q A CT A AU 11 7 n FAA 7^1 rift n l 72

.

14 . FAA 81 ZAU 01 90. 10

.

FAA 80LEG 01 90. AA 79HIL 01 92. 18. RTNA 73TJI 01 95. 11 FAA 79H0E 02

100. FAA 80PRE 01 100. 40. HAA 82WEI 01

100. AA 73L00 01 100. AA 79NAR 01 100. 4. ASV 8 2 SAT 02

100. 10. POL 74MAI 01 105. 5. FAA 79ST0 01 105. FAA 82H0E 01

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

106. oy - r AA 74RAI 02

108

.

o AT? -LA 17 74RAI 02

109. 7

Z . FAA 79DAB 02

110. 10 . FAA 81KNA 01 110. 10. NAA 77JER 01 110. FAA 82PRE 01 110. 6. AA 80SCH 05

110. FAA 82AKA 01 110. RTNA 79BYR 01 110. 1 A1U • AAA A 82RIT 01

1 10. 10

.

PAA 74CHA 01

1 10

.

10

.

AA 75EPS 01

1 10

.

10. AA 78RIT 01

1 10

.

10. AF 75EPS 01

1 ID . 8. RTNA 78GAL 01

1 ID • 10. FAA R3GLA 01

1 16 . 13- RTNA 80GRE 01 120. 1U • TTTKT A 81K0S 01 120. 1 1 FAA 79HOE 02

120. 80

.

82 JON 01 120. NAA 76GUZ 01 120. 20. 1 1 FAA 78SMI 01 120. RTNA 74ROO 01 120. 20. 11 FAA 78SMI 01

120. 10. RTNA 740RV 01 130. 20

.

TTNA 81K0S 01 130. r AA 82HEI 01 130. cJ . 7 A A / AA 73TAL 01 130. cJ • r AA 74TAL 01 130. 7 7 A A 7 AA 73TAL 01 130. FAA 74TAL 01 140. PAA 82WEI 01 150. SO AA 80AGE 01 150. 50. AA 76GAL 01 150. 60. TCGS 79AND 01 160. 16. FAA 76URE 01 160. 10. ICPES 79HER 01 160. 50. RTNA 8 OVAL 01 160. 70. 11 ICPES 82 JON 01 170. AF 78URE 02

170. 70. 11 ICPES 82 JON 01 180. 16 AA 79AB0 01 200. 100. Ml ICPES 82 JON 01 200. 80. * RTNA 76GAL 01 230. 20. * FAA 73SEG 01

2 30. 60. * ITNA 74RAN 02

580. + 1 £ A A *1d AA 79ABO 01 660. lAn m\j •

4c" AAA A 79MON 01 2000. Aiw 't\ r 79ULL 01

ppm)

2. L* 14 NAA 81WIL 01

2

.

L* 14 NAA 81WIL 02

0.75 0.067 TTNA 77HAM 01 0.84 0.04 ITNA 81K0S 01 0.9 D* RTNA 82LAU 01 0.9 RTNA 77LAU 02

0.91 0.06 RTNA 80SL0 01 0.92 0.14 ITNA 77NAD 02

0.97 ITNA 79KUC 01 0.98 0.07 VV 81N0N 01

63
TABLE H (cont)ANAL

TABLE H (cont)

HFF 111 CONC UNCER COMMENT METH CODE NUM

0.98 0.05 ITNA 78LAU 02

1

NAA 77LAU 01

1 RTNA 72M0R 03

1.1 SSMS 78URE 01

1.2 0.2 * ITNA 81KUL 01

CI (ppm)

1400. L* 14NAA 81WIL 01 53. * SSMS 81VER 02

400. 770. R* ITNA 79IMA 03

400. 770. R* ITNA 79IMA 01 510. *35 ITNA 81GLA 03

580. 27 . * FAA 78TSU 01 630. 24. AA 78TSU 01 632. 80. ITNA 77ZIK 01 638. 27. ISE 81 NAD 01 675. ITNA 78CAP 01 685. 32. PAA 74CHA 01 690. NAA 76GUZ 01 700. 60. 35 ITNA 81GLA 04

706. 26. ITNA 78FUR 01 717. 193. PAA 76KAT 04

719.5 TTHA J. IDA 82AKA 01 720

15

V V a 1 HON 0

720 - 140 • rAA 76KAT 02

730. 60. TTHA O \J Jb \J \J 1 730. 30. 1 UuD 7 9 FAI 0

730

26

Pi AA 7RCAN ("11 732. 29

T TH A / / uui u

732. 29. Pi AA 7AMT1 / OI 1 1 L> CiO U L 739. T1 TNA 1 Pin 7AHAT fl 1 740. 58. T TNA 7 7HAM C\\ 740. 30. TCGS 7 9, ANH 0

* 7 All U Ul 750. 35. ITNA 77STE 0? 750. Ti TNA inn 7/ ARAN *t IVAT* n?\J L 750. 19. ITNA 75RIC 01 755. ITNA 80CRE 01 760. ITNA 83GLA 01 770. XRF 78CAM 02

770. 150. 7QPFN 0? 770. 240. EXRF 77NIE 01 790. RTNA 72M0R 03

800. 40. I ENA 79 JON 01 810

150. EXRF 80DYC 01 950. 70. * 14 NAA 81WIL 02

Co (ppb)

1300. L* ITNA 80TOU 01 6000. L* EXRF 79GIA 01 8000. L* 14NAA 81WIL 01 8000. L* 14NAA 81WIL 02

100. RTNA 72MOR 03

110. 20. 6 NAA 78GAN 01 112. 17. NAA 76GUZ 01 120. 50. AA 76GAL 01 130. NAA 77LAU 01 130. ITNA 79KUC 01 130. ITNA 78CAP 01 130. 10. RTNA 74G0E 01 130. ITNA 80CRE 01 130. 10. ITNA 78LAU 02

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

130. 20. RTNA 77KUS 01 130. 20. 6 ITNA 74BEC 01

1 38 . 10

ITNA 74RAN 02

140. 30. 6 NAA 78GAN 01 140. NAA 74BEL 01 140. 10. ITNA 78GIL 01 142. 7. FAA 75HAG 01 145. ITNA 82AKA 01 150. ITNA 80SAT 01 150. 1 I ENA 79KUC 01 150. 20. 11 FAA 80FUD 01 150. 30. ITNA 76KUC 01 160. 20. RTNA 80SL0 01 160. 10. ITNA 82C0R 01 170. 10. ITNA 79SAT 01 170. 10. ITNA 79K0B 03

180. 30. ITNA 81KUL 01 180. 20. RTNA 77MEL 01 180. 28

ITNA 77HAM 01 190. 40. VV 81N0N 01 190. 5. 11 FAA 80FUD 01 210. 20. 6 ITNA 74BEC 01 210. 20. ITNA 81K0S 01 220. 40. ITNA 78FUR 01 220. 30. ITNA 82QUR 01 230. 50. I ENA 81K0S 01 230. 30. ITNA 79AHM 01 260. 120. 5 ITNA 80TOU 0

297. 26. * COLOR 82KIR 01 300. 40. * ITNA 76GAL 01 300. FAA 82 HOE 01 420. 470. R* ITNA 75RIC 01 460. 100. * ITNA 79REN 03

290. 100. * ITNA 77ZIK 01

(ppm)

5. L* EXRF 79GIA 01

2. L* 14 NAA 81WIL 01

2. L* 14 NAA 81WIL 02

1.07 0.13 6* NAA 78GAN 01

1 .5 * AA 73L00 03

1 .97 0.44 NAA 76GUZ 01

2. 0.13 GC-AA 76WOL 01

2

ICPES 79MCQ 01

2

0.2 6 ITNA 74BEC 01

2

ICPES 79MCQ 02

2. NAA 7 4 BEL 01

2 . AA 79MCQ 01 2.05 11 AA 79HOE 02

2.2 0.4 VV 81N0N 01 2.2 1. CPXRF 80KIR 01 2.2 2.9 R* AA 75MAN 01 2.2 0.3 RTNA 77MEL 01 2.22 0.2 PAA 74CHA 01 2.23 6 NAA 78GAN 01 2.25 11 AA 79H0E 02

2.37 0.07 SSMS 72MAG 01 2.4 0.36 ITNA 77HAM 01 2.4 0.1 11 ICPES 82 JON 01 2.4 0.6 ICPES 81BLA 02

2.4 RTNA 7 5ABU 01 2.4 ITNA 79KUC 01

64
TABLE H (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NVM

1 .4 U . j ITNA 78LAU 02

I .4 U . 1 RTNA 76MEL 03

2 .4 0.1 CHEML 74LI 01

2 .4 0.1 9 ITNA 78LAU 02

2.46 0.025 RTNA 74MCC 01 2.463 0.02 11 RTNA 7 RMf r 01 2.47 0.14 FAA 7 SCAR 0? 2.495 0.014 11 RTNA 7RMCC 01 2.5 1.6 EXRF 73GIA 01 2.5 0.4 ITNA 76KUC 01 2.5 RTNA 72MOR 03

2.574 0.01 ITNA 78MCC 01

2 .58 0.04 ITNA 81K0S 01 2.59 0.15 7 FAA 80CHA 01

2 .6 0.3 1

1

ICPES 82 JON 01

2 .6 0.1 35 FAA 81GLA 03

2 .6 0.4 ITNA 78FUR 01 2.6 0.1 ITNA 79K0B 03

2.6 0.2 NM 80SHI 01 2.6 0.2 6 ITNA 74BEC 01

2 .6 11 AA 79HOE 02

2 .65 0.16 7 FAA 80CHA 01

2 .67 0.15 RTNA 78GAL 01 2.7 0.2 D* DCP 81REE 01 2.7 FAA 82 HOE 01 2.7 AA 81ARA 01

2 .7 0.2 DCP 79REE 01 2.7 0.17 AA 80AGE 01 2.7 0.3 ITNA 82C0R 01 2.7 ITNA 78CAP 01

*) 7 fl 9 ITNA 7 9 SAT 01

2 -8 0 • 2 ICPES 81KNA 01

2 .8 0.2 ITNA 82QUR 01 NAA 77LAU 01

0 ft SSMS 81VER 02

2 .8 0.4 ITNA 74RAN 02

2.8 0.2 ITNA 75RIC 01 2.8 0.2 TTNA J. ILIA 7 Q AHM fi 1 2.8 0.6 FAA 7 AUfiT fi 1 2.82 7 FAA QfimA m

2.9 0.3 RTNA 1 HuUEi \J 1 2.9 0.4 EXRF 80DYC 01 2.9 RTNA 78G0E 01

3. 1. ITNA 77ZIK 01

•s fl 0 AA 76GAL 01

3.14 0.4 ITNA 81HAB 01 3.2 0.3 TJT*M K A 1 IN A

1 AT f\ 1 3.2 0.3 ITNA 81KUL 01 3.3 * TTNA J. J.Ptn OUI>kTi Ul 3.4 0.5 * ITNA 7 6GAL 01 3.67 0.01 ICPE S 79HER 01 5.5 2.2 * PAA ROYAM 01 5.81 0.84 * ITNA 79REN 03

ppb)

60. L* RTNA 72M0R 03

100

.

L* ITNA 82GLA 02

300. L* 14NAA 81WIL 02

20. NAA 77LAU 01 24. 3. 9 ITNA 78LAU 02

28. 5. ITNA 81KUL 01

TABLE H (cont)ANAL REF REF CONC UNCER COMMENT METH CODE NVM

28 . 5

.

ITNA 78LAU 02

29

.

2. ITNA 74RAN 0?

37. 2. TTNA 1 inn O j\j L*rt \j i 37.4 11. NAA 76GUZ 01

38. 7. 6 ITNA 74BEC 01 40. 10. ITNA 79SAT 01 40. 9. VV 81N0N 01 42. ITNA 80CRE 01 42. 1

.

I ENA 81K0S 01 48 . 4. ITNA 81K0S 01 80. 10. * RTNA 77MEL 01 150. 60. * ITNA 79REN 03

J .0 1 T i • 5 ITNA 74H0F 01

8

.

* EXRF 82KEE 01 8.1 2. EXRF 77FL0 01 8.4 0.8 ITNA 78FUR 01 8.9 1 .7 FAA 77FUJ 01 9.4 EXRF 81BIS 01 9.6 1 .7 EXRF 7 3 SPA 01 9.76 0.61 9 ITNA 77GAN 03

y .8 0.6 6 NAA 78GAN 01

Q Q

7 . O

fi a O NAA 78GAN 01

i n 1U • RTNA 72MOR 03

i n 11 . XRF 78LIN 01

1 u

.

oZ . CPXRF 77CAM 01 10. 0.7 AA 78LIN 01

10.3 0.5 FAA 82JEN 02

AA 76KRI 03

10.3 0.6 AA 76GAL 01 10.4 13.3 R* ITNA 79 IMA 03

10.4 2.4 EXRF 7 5REU 01

10.4 l *l *a 1 j. j R* ITNA 79IMA 01 10.5 1 . RTNA 80SLO 01 10.8 0 NAA 72SIN 01

1 1

.

ICPES 81WEI 0!

1 1

.

AE+AF 79ULL 01

11. OES 75JON 10

11. 1 AA 77FRY 01

11. 1 . ICPES 79MCQ 02

11. 1 . RTNA 77KUS 01 11. 15 . R* AA 75MAN 01 11. 1 .5 AA 79M0N 01

1 1

.

1

.

FAA 79KRA 01 11.1 1

.

RTNA 82COR 01 11.2 VV 81N0N 01 11.2 0.18 AA 80AGE 01 11.2 1.3 ITNA 7 4 RAN 02

11.2 1. 6 POL 72SIN 01 11.3 16 AA 7 9 ABO 01 11.4 ICPES 78CAP 01

11 AT K) . z RTNA 74RAV 01

X L • J U • D FAA 83GLA 01

1 1 . J

11 . EXRF 79GIA 01 11.5 1. POL 74MAI 01 11.5 0.5 RTNA 73TJI 01 11.6 0.4 ICPES 81BLA 02

11.6 0.2 AA 75ABU 01 11.6 0.4 RTNA 78GAL 01

11.6 FAA 78CAP 01

65
TABLE H (cont) TABLE H (cont)

CONC

11.7

11.7

11.8

11,

1 1

11.

1 1

12.

12.

12.

12.

12.

12.

12.

12. 12.

12.

12.

12.

12.

12.

12.

12.

12. 12.

12. 12.

12.

12.

12.

12.

12. 12. 12.3

12.3

12.4

12.5

12.5

12.5

12.6

12.62

12.7

12.9

13.

13. 13.

13.

13. 13.

13.

13

1313

1313

13

13.8

14.

14. 14.

14.

14.

14.

UNCER

1.7 0.2

0.7 0.3

1.4

1 .6

0.4

1 .

2.

1

1.4 0.8

0.5

1. 0.2

1.

1

2.

0.2

0.9

1.3

1.1 1.4 0.9

1.6

0.8

0.7

0.6

0.85

1. 0.47

4.2

0.6

0.5

0.1

1.5

1.5 1.3

1.4

2.4.5

1

0-13

COMMENT

11

11

11

11

16

11

6

6

1135

11

6

11

ANAL

METH

CPXRF

ICPES

ITNA RTNA

RTNA FAA

ASV

CPXRF

AA

AA

ICPES

AA

AA

FAA

ICPES

EXRF ICPES

XRF AA

AA

ICPES

OES

CPAA

AA

AA

RTNA

RTNA

FAA

ICPES

ITNA AAPAA

ICPES

VV

RTNA

RTNA AA

VV

FAA

EXRF NAA

POL

AA

ICPES

AA

RTNA AA

CPXRF

OES

AA

AA

SSMS ICPES

ITNA

ITNA EXRF

XRF ITNA

ITNA EXRF

AA

OES

OES

HEF CODE

REF HUM CONC UNCER COMMENT

ANAL METH

HEF CODE

REF

NVIM

81R0B 02

82 JON 01 79K0B 03

78GIL 01

79BYR 01 82GRO 01 79BRI 02

76ZEI 01 79HIL 01 81ARA 01

82 JON 01 77YAN 01 76FUK 01 77L0R 01 79MCQ 01

77NIE 01 82 JON 01 78CAM 02

73TAL 01

79MCQ 01

82 JON 01

7 5JON 02

78MCG 01

73L00 03

78RIT 01 74G0E 01

7 4 CAR 03

73SEG 01

81KNA 01 79SAT 01 79AB0 01 76WIL 01

7 9ABE 01 80SCH 05

76MEL 03

80VAL 01

79H0E 02

79ST0 01 74W0L 01 73GIA 01 76GUZ 01 72SIN 01 72SIN 01 78DAH 01 79H0E 02

77GLA 01 75ISA 01 80KIR 01 75J0N 07

77FRY 01

73TH0 01 72MAG 01

79HER 01 82QUR 01 79AHM 01 79MAT 01 74REU 01

77ZIK 01

74HOF 01 80DYC 01 75ISA 01

7 5J0N 11

7 5JON 04

14. OES 7 5JON 03

14.5 4.7 ITNA 7 7 HAM 01 14.5 1

FAA 82KRI 01

15

OES 75ISA 01

1 e 7 ^ TAW fi ^

1 S S SSMS ft] VFR 0?

It C ITNA Oil rtJVrt \J 1 ID • 7 ^ inw n i 10. 1 £ ADC

17 . OES 7 5JON 00

18.1 * CPXRF 75CAM 01 18.3 6.9 * XRF 77SMI 04

19. * ITNA 78KEL 02

20. * OES 75J0N 08 21. 11. * CPAA 77ZIK 01

27. * OES 7 5B0L 02

30. * XRF 80SUZ 02

35. * EXRF 81 PAR 01

Dy (ppb)

100. L* NAA 771 atj 01 53. 8. ITNA 77NAD 02

110. SSMS 78URE 01

Er (ppb)

100. RTNA 77LAU 02

100. D* RTNA 82LAU 01

30. SSMS 78URE 01

Eu (ppb)

50. L* ITNA i or* kt> r\ i /oCAP Ui

20. SSMS 78URE 01 20. ITNA oULKL Ul on O

L • TTNA 1 Inn 7QT All r.9

/ Ounll 'J i. £11 O 1 K1NA 77T ATI H

1 1 Z 1 . RTNA Otl ATT A 1 OZLAU 01

Z 1 • 1 • ITNA 74RAN 02

22

8. RTNA 80SLO 01

Li. • } • 1 1NA /7MJD Uj

AH T TWA 1 1HA 7 7UAH fi o / / liAV U Z 26. 1 , IENA fll VOQ 01 26. NAA 77LAU 01

27 . 3. ITNA 81K0S 01 27. 6. ITNA 81KUL 01

28. 6.3 ITNA 7 7 HAM 01 31. 4. * ITNA 74BEC 01 120. 20. * RTNA 77KUS 01 300. * RTNA 72M0R 03

F (ppm)

60. L* 14 NAA

14NAA 81WIL 01

3.12 COLOR 79DAB 01 3.6 AA 77TSU 01

3.69 COLOR 79DAB 01 3.8 0.32 ISE 7 9 DAB 01 3.88 ISE 79DAB 01

4. 0.3 ISE 82GLA 02

4.2 0.4 ISE 83GLA 01

66
TABLE H (com) ARAL AUtl UF KEF CONC ' UNCER COMMENT METH CODE NUM

4.4 0.3 ISE 83KNA 01

4 .8 1I • MCMb 7 7CTT? 0,9 / /OIL

10. * CPAA 80HAN 01

>pm)

121. * CPAA 78MCG 01

121. * CPXRF 76ZEI 01

145. A» • *1 1 AA 78GAI 01

151

.

0ES 75JON 09 174. 0ES 75JON 06

190. * 0ES 75JON 11 0ES 75JON 02

205. 37. ITNA 81HAB 01 213. 0ES 75JON 03

220. 6. 1 1 AA 78GAI 01

225. DO . XRF 77SMI 04

229. XRF 78LIN 01 229. 0ES 75J0N 08

232. 0ES 7 5JON 04

235. ICPES 78CAP 01

235. AA 76FUK 01 237. 1X 1J . CHEML 72SEI 01 238. AA 76KRI 03

239. 0ES 75ISA 01 240. 330. R* AA 75MAN 01 245. 35. ICPES 7 9ABE 01 246

.

FAA 78CAP 01

250. AA 73LOO 03

250. 42.5 1

1

AA 75ISA 01 250. in30 . RTNA 74CAR 03

253. ITNA 80SAT 01 254. q. EXRF 80DYC 01 255. 5, 1

1

COLOR 82SCH 03

256. 11. 11 ICPES 82 JON 01

256. 1

.

AA 78LIN 01 259. ITNA 78CAP 01

260. 90

.

ITNA 78GIL 01 261. SSMS 81VER 02

261

.

39.1 11 AA 75ISA 01 262. 5. ICPES 7 9HER 01 9A7 ICPES 78DAH 01 267. 2 .9 CPXRF 81R0B 02

lb 1 • 6. itrL O 7QMm 0 9 9711 U.n ITNA 80CRE 01 270- C A50 ITNA 81GLA 03

270. OES 75B0L 02

271

.

7 RTNA 77MEL 01

271

.

6

.

J 1 COLOR 82SCH 03

272. 16

.

AA 73THO 01 273. 6. ICPES 79MCQ 01

274. 19. EXRF 79GIA 01 276. 8. EXRF 73GIA 01 276. OES 75J0N 05

278. 11. AA 79MCQ 01 279. 70 RTNA 77KUS 01 280. 10. ITNA 78LAU 02

280. NAA 77LAU 01 2«n. 26. ITNA 77HAM 01 28: . COLOR 72SEI 01 2s:. 21. 14 NAA 81 MIL 02

28 J. 23. ITNA 75RIC 01

TABLE H (cont)ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

9ft *\ •3J •

i i 1

1

Ol TAW n 1

9ft iO 1J • CJ - 13r\TWA x iva Q ACT A fll

9ft Zo ^D • Q 1 1 AAT AD Q 0 CAJ A 1 oZbCrl UJ

9ft ZO SJ • RJ . TX TWA X li A

7QnAC Al

9ft 7 AAA A TOUT T A 1 / y rtl L u 1 OO Q Zo o • 1

A

ZU • QoUotn A c ru A £ UD

290. 35

.

I ENA

O 1 VA C A 1 HIKOb 01 290- 6

.

1 1 ICPES 82JON 01 290. 30. CPAA 77ZIK 01

290. RTNA 72M0R 03

290. 12. PAA 74CHA 01 290. 25

.

6 NAA 78GAN 01 290

.

30. ITNA 81K0S 01

Oft A Z9U

.

FAA 7 j SEG 0

1

ZVU

.

JU . ITNA olKUL 01

90. 1 9ZhA • V V Q i Hmi n i 0 1 INUiN U 1 9Q1 xh1 A • 77pt a r\ lie 1 L.U U 1 £7 -> •

1 i X X AA 7QHOF o? 293

.

18 . EXRF / ~ r^u Cj ui

9Q A 9Q <i 1 1 1 1 AAA A

29 5 .7 20 . 1 ITNA ozCOR Ul 296. 12. ICPES 81BLA 02

296. 8. ITNA 82QUR 01 296. 8. ITNA 79AHM 01 297. AA 81ARA 01 297. 10. FAA 8 2 JEN 02

299. 1

.

ITNA 79K0B 03

300

.

50. 14NAA O AT? A A f\ 1 OUrAA Ul inn 1 A PAT AD L>ULiUt\ oz nuk. ui

inn FYRF ftOli DID rt*? nUli 300

.

HU • ITNA

inn JUU .I 7

I I .

1 1 1 1

ft 9 TOM 0 1 inn NAA n aa 7/ AftFl *4 DLL 01U I inn jUu • A1 j

.

T TH A 1 1NA 7/,o am n 9 in i JU 1 Z > j rvnr LXKr "7 1 CD A ni /JbrA Ul

o a o JO 5 . 3Z . ITNA TOP AT rtl /ybAl Ul 304 . 30

.

ITNA 78FUR 01 306. ITNA 79KUC 01 306. 6. EXRF 77NIE 01 310. 54. FAA 77FUJ 01 310

.

XRF "7" O /""* A \i l~\ O 78CAM 02

311.1 10 .4 NAA T crn? Al

/ dGUZ Ul 312. 1 1 .4 POL 72MAI 01 119 J XZ .

1 1 A 7/ 7MAT / rlAX niU X 312

.

1 1 IX. POL 7/HIA, MATInl 01u X 313. ICPES ftlWEI 01 314. 40. EXRF 7 SRFTI 0 1 / JIMiU U 1 315

.

25

.

RTNA 74G0E 01 316

.

OES 75J0N 01

1ill17 • 9^ZD . T ADC C O 1 VM A A

1

01KJ4A Ul

1310.4 1 Q /. lb .7 b ITNA 7 /. HU A A 1 / hBLL U

1

319. 32. XRF 74REU 01

320. 25. 6 NAA 78GAN 01 326. EXRF 82KEE 01 326

.

30. ITNA 77ZIK 01

331 .5 118

.

PAA 76KAT 04

332. 84. PAA 76KAT 02

335. 14. 6 EXRF 79MAT 01 338. 16. 6 EXRF 79MAT 01 343. 6. SSMS 72MAG 01 348. 10. 14NAA 81WIL 01

67
Ge

H (%

TABLE H (cont) TABLE H (cont)

ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE NVIM CONC UNCER COMMENT METH CODE NTJM

JO / . * aL? c 7 C TAM A 71 5JON U/ I.e. 146 . 12. RTNA 82LO 01

n a 5/ U 45. * CPXRr / / CAN O

1466. FAE 76CAV 01 422 . * CPXRF /5CAM 01 146

UU 74FEL 01 450. 70. * ITNA 79REN 03 146

17 . NAA 76GUZ 01 500. * AE+AF 79ULL 01 148. 10. 7 RTNA 72HEI 01 884. * EXRF 81 PAR 01 150. 17 . CVAA 74FIT 01 150. CVAA 81NAR 01 ppb) 150. 5. FAA 72LYO 01 152

6. CVAA 80TON 01 500. L* EXRF 79GIA 01 152 . 5. 2 CVAA 79KNE 01 160. L* IENA 78WAN 01 152

6. RTNA 76MEL 01

78. 25 . NAA 76GUZ 01 8. ft IT A A UVAA 0 AT/ AD A 1 OUK.UK Ul 86. RTNA 72M0R 03 153

14. FAA 7 5KOI 01 89.3 3.6 RTNA 80STU 01

1 CI, 154. 16. 5 RTNA 80GRE 01 100. 10. RTNA 77KUS 01 1 D4

13. r\i a a O VAA 7 o r. aa a i

1 S4 28. RA A ppb) 1 Si 13. FAA 1 DUw U 1

1 SA 20. RTNA TftrTT ill

/ OblL Ul

1 .64 0.24 ITNA 7 7 NAD 02 1 SA 5. R TM A 7/4UKV A ADV A 1 Ul

100. D* RTNA 82LAU 01 155. 5.6 RTNA 72ROO 02

100. RTNA 77LAU 02 155. 6. 11 CVAA 7 7 TAG 01

100. SSMS 78URE 01 155. 15. RTNA 73TJI 01

15 5. 6. RTNA 72ROO 01 ppb)

1 EC

1 J J t 13. 5 RTNA oUGRE Ul 155. 3. RTNA 72RAI 01 400. L* EXRF 79GIA 01 157

20. CVAA 82GLA 02

150. H ICPES 82HAH 01 157

1AF 81EBD 01

1 JO • 10. RA A r AA 7 7 at A A 1 / /OLA U J

) 1 JO . RTNA 7 ART r oi 158

5. RTNA 72LYO 01 5.54 0.08 TCGS 79FAI 01 1 58

ITNA 80SAT VJ v U .Tlx 01W j_

5 .6 0.1 TCGS 79AND 01 159 . 21. CVAA 78MAT 01 5.91 0.3 CB 82GLA 02 i ft n 70. TTMA O 1 vin A 1 O 1 NUL U 1 6.05 0.07 CB 80SCH 02 loU. 20. FAA "7 Q OTA A

/y&iu Ul 6.1 0.1 35 TCGS 79GLA 04 160. 20. CVAA 82CHA 01 160. 12. FAA 72R00 01 ppb) 160. 30. RTNA 8 OVAL 01 160. 12. FAA 74SIE 02

13. RTNA 80SL0 01

1 C A lbO

6. CVAa 7 O D AT A 1 / I KA1 U

23. NAA 77LAU 01 lDU. 40. 6 POT QO T A A A 1 OZJAG Ul

27 . ITNA 80CRE 01 160. RTNA 79DES 01

31. 4. ITNA 78LAU 02

1 C A 1 0 0 . 20. FAA O O TT? \T A 1 OiJLN UZ

37. 5. ITNA 74RAN 02 lol

13. RTNA 7 CT TT A 1 /DLir Ul

1 ft? 10. 7 PTMA 7 9 HPT 0,1 / - tlLi U 1 ppb) 163. 6. 17 CVAA 7 7TAC 0

1 O J . 12. D TM A K UNA OZGK1 Q 9 ADT A 1 Ul

5000. L* 14 NAA 81WIL 01 i ft s 5. 35 LVAA Q 1 AT A A A 0 1 O LatV U*t 1000. L* EXRF 79GIA 01 167

ITNA T /. DT A A 1 74RIC Ul 110. 30 . * RTNA 77BAN 03

1 c o loo. 10. T TM A 1 UNA QOATTD Al o/yUK Ul 120. 10. RTNA 74G0E 01 100. 1 ft Q 10. TTMA 7/7Hn.n Q A VIM 0.1 Ul 120. 20 . RTNA 80SL0 01

1 7 C

1 / 5

5. 17 CVAA T 7T A A A 1 / / i AG U

122. 11 CVAA 79HOE 02 180. 40. 6 DAT Oi J AG U 1 125. IDMS 74RIC 01

1 Q ft loU. 10. ITNA T O T71 TT) A t /oFUR Ul

125 - AA 74RIC 01 180

20. ITNA T / r »\1 AO 74RAN 02

130. CVAA 80NAD 01 loU • 30. RTNA 7 7MFT 01

1 38 . 2 . 11 CVAA 7 7 TAG 01 30. 6

T TM A 1 UNA 7iopr Ai

140. 20. IDMS 72RAI 01 190

40. CVAA 77AND 01

140

10 . PAA 74CHA 01 190. ITNA 75RIC 01

1 4U

10 . NAA 7 7JER 01 200. 30. * ITNA 81HAB 01 140. 10. ITNA 74FRI 01 200. 30. * PAA 80SEG 01 141. 9- SSMS 74ALV 01 200. 80. * ITNA 74GUI 01

142. 27 . CVAA 82D00 01 200. 20. * ITNA 81K0S 01

68
TABLE H (cont) TABLE H (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

203. 11. *17 CVAA 7 7 TAG 0 1 240. *17 CVAA 7 7 TAG 01

305. 70. * ITNA 75LIT 01 190. 10

.

NAA 78GAN 01

Z 10

.

50. ITNA 77ZIK 01

Ho (ppb)

13. D* RTNA 82LAU 01

13. RTNA 77LAU 02

20. SSMS 78URE 01

1 ftftft TL»* UNA 83GLA 01

i nft

1 00 . 50. PAA 77WIL 01

100 . 50. PAA 78HIS 01 160. 20. IENA QO Q AT OA DAI n i 167. 10. RTNA 77R00 01

173.2 4.4 RTNA 80GVA n l 183. 6. 17 NAA 79HEC 01

188. 26. NAA 79 BRA 01 200. 70. RTNA 77STE 02

220. 17 NAA 79HEC 01

1-129 (fci)

0.006 0.002 RTNA 79BRA 01

In (ppb)

1.23 0.11 RTNA n i

1 .6 0.1 RTNA 78KOB 01 1.8 0.8 RTNA 7 7VI1^ mU

1

Ir (ppb)

1 R

X D • 1

J • K 1 IN A 74CAR 03

K (%)

1 -05 1 .41 R* ITNA 79IMA 01

1 .05 1 .406 R* ITNA 7 9 IMA 0 3 1-11 * 0ES 75J0N 05

75J0N 09

1 1 on f\ A 1 Q U -Ulo fT) V D f 81 ROB 02

1 . lb JL OES 7 5JON 03

OES 75JON 11

1 1 C\ 1 14 NAA 77SEG 01

1 1 c

1 AA 78SZY 01

1 * Jj 7 5JON 04

1 .36 0.01 AA 78GAI 01

1 17 U • 14 79JON 01

T TM A 1 1 IMA 80CRE 01

1 .37 0.06 ITNA 74RAN 02

1 17 A 11

A A AA 78SZY 01

1

1

• IRJO u • u*+ T TH A 1 UNA 75RIC 01 1.38 OES 75ISA 01 1.39 CPAA 80HAN 01 1.4 0.2 35 ITNA 81GLA 04

1 .4 ITNA 82AKA 01

1 .4 0 01 11 AA 78GAI 01

CONC

La (ppn)

0.7

0.8

0.89

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

1 .4 0.06 ITNA 78LAU 02

1 .4 0.098 6 NAA 78GAN 01

1 .4 OES 7 5JON 02

1 .41 0.03 TCGS 79AND 01

1 .41 OES 7 5JON 07

1 .42 0.04 ITNA 81K0S 01

1 .42 EXRF 81BIS 01

1 .42 0.09 ITNA 7 6KUC 0

1

1 .42 ITNA 78CAP 0

1

1 .43 0.04 EXRF 79KUE 01

1 .43 0.07 1

1

ICPES 82 JON 01

1 .43 0.06 FE 78KOR 01

1 .437 0.079 NAA 76GUZ 01

1 .44 11 AA 75ISA 01 1.44 0.04 RTNA 76MEL 03

1 .445 0.11 PAA 76KAT 04

1.45 ITNA 79KUC 01 1.45 ICPES 79COO 01 1.45 OES 75JON 01

1.45 0.08 PAA 76KAT 02

1 .45 11 AA 75ISA 01

1 .46 0. 14 14NAA 80FAA 01

1 .46 0.11 EXRF 82DAK 01

1 .46 0.07 ITNA 79AHM 01

1 .46 0.2 14 NAA 81WIL 02

1 .47 NAA 77LAU 0

1

1 .47 0.

1

ITNA 79REN 03

1 .47 0.02 11 ICPES 82 JON 01

1 .47 0.12 ITNA 79KOB 03

1 .47 0.07 11 ICPES 82JON 01

1 .48 AA 79HIL 01

1 .48 ICPES 81WEI 01

1 .49 0.03 ITNA 78GIL 01

1 .49 1 IENA 79KUC 01

1 .49 0.194 ITNA 77HAM 01

1 .49 0.04 TCGS 79FAI 01

1 .496 0.043 ITNA 78FUR 0

1

1 . J

ft 1 I'D ITNA 7 6 BAT 01

1 . J n hp. V V 81N0N ft 1 1*3 TTMA X inn 7 P.VF1 1.31 ft ft A U . UD Q ft]/ T D ft 1

1 .51 0.06 EXRF 77NIE ft 1 u 1

1 .51 XRF 7 8 CAM 02

1 .54 OES 75JON 08

1 .54 0.03 ITNA 80SLO 01 1.56 0.05 11 ICPES 82 JON 01

1.57 0.08 EXRF 75REU 01 1.57 0.25 14NAA 81WIL 01

1 .58 0.08 6 NAA 78GAN 01

1 .59 OES 75JON 10 1.62 OES 75JON 06

1.66 0.8 *6 EXRF 79MAT 01

1 .7 0.07 * ICPES 79HER 01

1 .74 0.04 * EXRF 80DYC 01

1 .81 0.08 6* EXRF 79MAT 01 3.89 * EXRF 81PAR 01

0.1 0.05

1 .25 R*

ITNA RTNA

ITNA

77ZIK 01 80SLO 01 79IMA 03

69
TABLE H (cont)

Lu

ANAL KEF REF CONC UNCER COMMENT METH CODE NUM CONC

0.89 1 .25 R* ITNA 79 IMA 01 6000.

0.95 ITNA 79KUC 01 6000.

0.98 ITNA Q Af"D C A 1 OUL.KL Ul f. r\r\r\ D UUU . 0.99 0.08 6 ITNA 7 A WC A 1 / 4 DC, L U 1 6000.

1

NAA 771 / / LirtU Ai] 01U X D WU .

1

LI" DTHA ft91 O L LiAU AIT ft. U 11 6000.

1

PTMA 771 AIT ft.9 / / LA u u z. 6000-

1

U A A 7AHPT ftl 6000.

1 .1 0.1 ITNA "7 Ol ATI AO

1 .15 0.1 IENA

O 1 VA C A 1 £ 1 AA 0 1U0 .

1 .18 0.09 ITNA 81K0S 01 6100.

1.2 ITNA 78CAP 01 6100.

1 .2 0.1 RTNA 76MEL 03 6100.

1 .2 RTNA 72MOR 03 6100.

1.2 0.165 ITNA 77HAM 01 6100.

1 .2 SSMS 78URE 01 6100.

1 .2 0.1 T TM A 1 1TJA q i inn a i o 1 K.U L Ul 6150.

1.22 0.02 W 81N0N 01 6150.

1 OA

1 .24 n aq 0 -Uo TTN A X 1HA 7Qpru a o 0 1 DU • 1.3 0.1 ITNA 7 4RAN 02 6173.8

1 . / a £ u . 0

ic I\l Pi A 7 7VTK f)l A 1 7 A

1 .96 A AO it 1 1NA 7 7MA r\ A 0 / / NAD U Z C 1 A A bzUu

D (J . (PPt>) A7AA

DZ_>i5 . 900. LrAA Qi c AC A 1 o 1 o Ao U 1

£. inn

510. 660. R* AA 75MAN 01 6300.

570. 70. AA 83GLA 01 6300.

770. 30. ITNA 77HEY 01 6A00

800. 200. CPAA 80HAN 01 6400

13700. 1500. * NT 7 4 CAR 02 AD JUU ^ AA • AO DUU ^ AA • (ppb) D JJUt

(\O (\C\C\ DUU . O Azu

T * MANAAA 7 7T ATT fl T D / UU •

1 U • T * TTM A 1 1NA 7 ftT ATT ft 0 1 OLtAU U Z ftD 7nn / UU • a c 1 0 .0 1 A AO u . uy T TM A 1 1 IN A 7/ 7ma / PJA1Jn n?U Z D OUU • 0.9 0.1 ITNA 81K0S 01 6800.

3 .3

T\* Ux Kl NA QO T A IT A 1 oZ L.AU U 1 £ Q A A 3.3 RTNA 7 "7T A IT AO / /LAU U Z 7000.

6. RTNA 80SL0 01 7030.

10. SSMS 78URE 01 7100.

7830.

(ppm) Mn (,ppm;

4000. 6250. R* ITNA 79IMA 01

i 4000. 6250. R* ITNA 79IMA 03

4900. ICPES 78CAP 01 j t, . 5140. 190

VV Q 1 MAM A 1 O 1 NUN U

C *1AA 5 300. * IT A A r AA 7 or AP 0

/ O^Ar U i 6S

^ AAA NAA 7 71 ATI 01 65. JUU « ICPE S 7 9 ARF 01 68 .2

- AA 80URE 01 7?

J JUU . ^nn JUU • IENA 79 TON 01 / Z . C / Art DOOO. 1 A A lUU • AAA A 7QMPO ni 73.5

5700. AT7C U to 7 ^ TAN O ^ 77

5700. 60. ICPES 79MCQ 0 2 79

5700. O AoU

lure, d 7QWPA A 1 /ycly^Kl Ul Q A 5800. 100. ii AA 78GAI 01 80.

5800. 730. ITNA 77HAM 01 80.

5900. 1

ii AA 75ISA 01 80.

5980. 70. ii ICPES 82 JON 01 80.

TABLE H (cont)ANAL REF REF UNCER COMMENT METH CODE NUM

RTNA 72MOR 03

500. CPXRF 80KIR 01 500. ITNA 78LAU 02

100. 1

AA 78GAI 01 200. 11 ICPES 82J0N 01 500. 14 NAA 80FAA 01

2 11 AA 75ISA 01 0ES 7 5J0N 09 0ES 7 5J0N 07

400. ITNA 80SL0 01 AA 79HIL 01 200. 11 ICPES 82J0N 01

100. PAA 74CHA 01 1100. 14 NAA 81WIL 02

200. PAA 78HIS 01 0ES 7 5J0N 10 ICPES 78DAH 01 100. PAA 76KAT 04

70. PAA 76KAT 02

179. NAA 76GUZ 01 173. ITNA 75PIE 01 100. 11 ICPES 82J0N 01 0ES 75J0N 08 OES 75JON 02

315. ITNA 77ZIK 01

700. TCGS 79FAI 01 ITNA 78CAP 01

130. ITNA 78FUR 01 ICPES 81WEI 01

OES 75ISA 01 OES 7 5JON 06

100. COLOR 74SLE 01 480. ITNA 79KOB 03

OES 7 5JON 1

CPAA 80HAN 01 100. ICPES 7 9 HER 01 1000. 14 NAA 77SEG 01

OES 7 5JON 03

OES 75JON 04 ITNA 7 6BAT 01 170. * 14 NAA 81WIL 01

* OES 75JON 01

* ITNA 75RIC 01

4.4 6* ITNA 74HOF 01

16 . * EXRF 77FLO 01

* OES 7 5JON 07 90. R* ITNA 79IMA 01 90. R* ITNA 79IMA 03

8.2 * XRF 7 7 SMI 04

* OES 75JON 06

1. *11 AA 78GAI 01

* ITNA 82AKA 01 SSMS 81VER 02

3. RTNA 76MEL 03

ICPES 78CAP 01

AA 73LOO 03

3. XRF 78LIN 01 OES 75ISA 01 OES 7 5JON 11

70
TABLE H (cont) TABLE H (cont)

ANAL HEF REF ANAL cr Del: CONC ' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

80.6 2.9 CPXRF 81 ROB 02 92. 1 . DCP 79REE 01 80.7 3.3 ITNA 81HAB 01 92. 1 . D* DCP 81 REE 01

81 . 4. RTNA 77KUS 01 92 . 3. ITNA 75RIC 01

81 .3 FAA 78CAP 01 92. AA 76KRI 03

82. 7. EXRF 79KUE 01 92.4 0.8 ICPES 81KNA 01 82. EXRF 82KEE 01 93. ITNA 80SAT 01 82. 99. R* AA 75MAN 01 93. OES 7 5JON 05

82 . 3. IENA 79J0N 01 93. XRF 78CAM 02

82. 4.2 AA 78LIN 01 93. 6. EXRF 77NIE 01 83.3 ICPES 78DAH 01 93.8 17.2 PAA 80YAM 01 83.4 FAA 7 7 SHE 02 94. 3.5 6 NAA 78GAN 01 84. 1

.

11 ICPES 82 JON 01 94.5 5. PAA 76KAT 04

84. NAA 77LAU 01 94.8 4. ITNA 82QUR 01 84. 4. ITNA 78LAU 02 94 .8 4. ITNA 79AHM 01 85. 4. EXRF 80DYC 01 95. 7.3 CPXRF 80KIR 01 85. 10. 6 EXRF 79MAT 01 95. 4. PAA 76KAT 02

85. ITNA 78CAP 01 95 12 ITNA 79 SAT 01 85. 2. 11 ICPES 82 JON 01 95. AE+AF 79ULL 01 85.6 2.8 6 ITNA 74H0F 01 95.4 2.1 ITNA 76GAL 01 86. RTNA 72M0R 03 96. ICPES 81WEI 01 86. ASV 80CHR 01 96. OES 75J0N 03

86. ITNA 83GLA 01 96. 5. PAA 78HIS 01 86. 1

.

ICPES 79MCQ 02 96.2 4.8 AA 76GAL 01

86. 2

.

1

1

ICPES 82 JON 01 96.8 3.6 AA 73TH0 01 86. AA 76FUK 01 97. 10. ITNA 77ZIK 01

86. 2

.

ICPES 79MCQ 01 97. OES 75J0N 10 86.5 4.9 EXRF 79GIA 01 97.4 CPXRF 75CAM 01 87. FAA 73SEG 01 98. XRF 80SUZ 02

87. 11 AA 79HOE 02 98. 20. TCGS 79FAI 01 87. FAA 73SEG 01 100. ITNA 78KEL 02

87. 11 AA 79HOE 02 101. OES 7 5J0N 01 87.1 1.6 RTNA 73HEY 01 101. 10. XRF 74REU 01 87.8 5.9 RTNA 74RAV 01 103. 5. * VV 81N0N 01 88. 4.4 .11 AA 75ISA 01 107. 3. * SSMS 72MAG 01 88. OES 75J0N 02 110. * ITNA 79REN 03

88. 0ES 7 5J0N 04 110. 9. *6 EXRF 79MAT 01 88.2 3.4 PAA 74CHA 01 131. * OES 7 5JON 08 88.6 2.2 EXRF 73GIA 01 144. * OES 7 5J0N 09 88.8 11 AA 79H0E 02 242. * EXRF 81 PAR 01 89. 3. W 80SCH 05

89. 1 . 11 ICPES 82 JON 01 Mo (ppb)

89. 5. ITNA 78GIL 01 89. 2.67 11 AA 75ISA 01 5000. L* ICPES 78CAP 01

89. 4.4 ITNA 79K0B 03 1400. L* 14 NAA 81WIL 01 89. 4. ITNA 74RAN 02 5000. L* RTNA 72M0R 03

89. 0.6 ICPES 79HER 01 1000. L* PAA 78HIS 01 89. 4. AA 79MCQ 01 800. L* 14 NAA 81WIL 02

89.9 ITNA 7 6 BAT 01 110. 80. *11 ICPES 82 JON 01 90. 7. ITNA 77HAM 01 200. FAA 7 9 BEN 01 90. 3. ICPES 7 9 ABE 01 200. 100. 11 ICPES 82J0N 01 90. ITNA 80CRE 01 200. 100. 11 ICPES 82JON 01 90. 6. ITNA 76KUC 01 200. 200. 11 ICPES 82 JON 01 90. 1

.

ITNA 80SLO 01 240. 20. RTNA 78NAD 01 90. 0.9 11 AA 78GAI 01 240. 21. RTNA 82HAD 01 90. 12. CPXRF 77CAM 01 250. 1 IENA 79KUC 01

91 . 4. MD FAA 79WES 01 280. 20. ICPES 82LYO 01

91 . EXRF 81BIS 01 300. 60. RTNA 77DIK 01

91 . 2. 6 NAA 78GAN 01 300. 30. RTNA 74G0E 01

91 .1 18. EXRF 75REU 01 320. 60. RTNA 80SLO 01

91 .6 1.08 NAA 76GUZ 01 320. 1 IENA 79KUC 01 92. 4. 35 ITNA 81GLA 04 327 . 70. NAA 76GUZ 01 92. 3. ITNA 78FUR 01 390. 40. FAA 81NEU 01

71
TABLE H (cont) TABLE H (cont) ANAL REF *EF ANAL REF R£F

N

CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

400. 100. PAA 80SEG 01 86. 5. ITNA 77ZIK 01 2260. 210. * PAA 74CHA 01 87. 11. PAA 76KAT 02

2300. * OES 7 5JON 10 87. CPAA 80HAN 01 3300. * OES 75J0N 11 87. 16. PAA 76KAT 04

4000. 2000. * CPAA 77ZIK 01 88. 6.8 ITNA 79K0B 03

4600. * OES 7 5J0N 03 88. 142. R* ITNA 79 IMA 01 6200. * OES 75J0N 01 88. 142. R* ITNA 79 IMA 03

10500. * OES 7 5J0N 07 90. 8. ITNA 81K0S 01 15200. * OES 7 5JON 02 92. ITNA 80CRE 01

92 . 35 ITNA 81GLA 04

(%) 100. OES 7 5JON 01 100. OES 75JON 05

2.59 0.11 * CB 82GLA 02 10 Jo ITNA 82AKA 01

2 .61 0.05 14NAA 80FAA 01 1 10

35 ITNA 81GLA 03

2.62 0.03 CB 80SCH 02 114. 2. NAA 78GAN 01

2 .7 0.01 11 TITR 82LIA 01 120. 40. ITNA 79REN 03

2.7 0.4 14NAA 77SEG 01 140. 12. ICPES 79ABE 01 2.7 0.09 TCGS 79FAI 01 150. * OES 75JON 04

2.7 0.09 13 NT 74CAR 01 154. * OES 75JON 09

2 .7 0.4 35 TCGS 79GLA 04 155. * ITNA 78CAP 01

O "7 1 0.01 TITR 80GIN 01 16 L

*1 AA 78SZY 01

2 .72 11 TITR 82LIA 01 170. 30. * IENA 79JON 01

2 .74 COLOR 80GIN 01 244

* 1 A A 7 Q C7Y n i KJ 1 2.74 0.02 11 TITR 82LIA 01 400 * OES 75JON 11 2.74 0.01 1 1 TITR flOT OZ Li T

J_rtA mU i 524. * OES 75JON 08 2.75 0.03 11 TITR 82LIA 01 2.755 0.038 GRAV 74CAR 01 Nb (ppm)

Z • / 0 0.09 13 NT 74CAR 01

7 ft 1 0.15 TCGS 7 9 AND 01 0.3 L* PAA 78HIS 01

Nd (ppb)

u • JO / 0.002 MS 73CAR 01 1000. L* NAA 77LAU 01

(ppm) 320. 90. ITNA 7 7 NAD 02

480. SSMS 78URE 01 70. L* 14NAA 81WIL 02 570. RTNA 77LAU 02

25. L* ITNA 74H0F 01 570. D* RTNA 82LAU 01

360. L* UNAA 81WIL 01 Nl (ppm)

100. L* ITNA 74H0F 01 40. * OES 7 5J0N 03 5. L* 14 NAA 81WIL 02

74. OES 7 5JON 06 10. L* AA 76KRI 03

7 c NAA 77LAU 01 2.5 L* PAA 78HIS 01

/ 0 . NAA 7 4 BEL 01 0.7 CPXRF 75CAM 01 77 RTNA 72M0R 03

1 . 1 IENA 79KUC 01

7 7 / / - 6- ITNA 80SL0 01

1 .1 16 AA 79ABO 01

7 7

/ / • 4 . RTNA 76MEL 03

1 .14 0.08 FAA 79STO 01

1 Q /o. 3. ITNA 74RAN 02 1.15 0.07 1

ICPES 82JON 01

78

5. ITNA 76KUC 01 1.15 0.09 1

ICPES 82 JON 01

79.3 5. PAA 74CHA 01

1 .18 0.08 AA 80AGE 01 80. 2. FE 81MIZ 01

1 .2 0.5 EXRF 79GIA 01 80. ITNA 78LAU 02

1 .2 0.063 5 COLOR 78FUD 01 80.6 1.3 • FE 78KOR 01 1 .2 0.4 FAA 82GR0 01

81 . 17 . ITNA 78FUR 01 1 .2 1. EXRF 77NIE 01

81 . ITNA 79KUC 01 1 .2 0.07 6 COLOR 78FUD 01

81 .5 3. ITNA 79AHM 01 1 .2 XRF 78CAM 02

81 .8 1 .83 NAA 76GUZ 01 1 .24 0.07 11 ICPES 82J0N 01

BO 1 I ENA 79KUC 01 1 .27 0.08 PAA 74CHA 01 83. 8.5 ITNA 77HAM 01 1.27 0.08 11 ICPES 82 JON 01 83. 5. ITNA 75RIC 01 1 .28 0.16 NAA 76GUZ 01 84. 4. ITNA 78GIL 01 1 .3 AA 73L00 03

84.4 ITNA 7 6BAT 01

1 .3 0.1 RTNA 75ABU 01

86. 1. VV 81N0N 01 1 .3 0.07 VOLT 81PIH 01

72
TABLE H (conl) TABLE H (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

1 .3 0.2 9 ITNA 7 QT AIT U I

1 .3 0.4 EXRF 73GIA A 1 U 1 1.31 0.1/ 17 A A r AA Q AriAP. n l 1.31 0.11 ITNA / jr It A 1 U 1 u . U J TOT OR 7 7 BUR 01

1 A n i POL 72MAI 01

1 .4 1 I ENA 79KUC 01

1 .4 0.3 RTNA 77MEL 01

1 .4 FAA 82 HOE 01

1 .4 0.1 POL 77MAI 01

1 .4 0.1 POL 74MAI 01

1 .4 0.6 ITNA 74RAN 02

1 A FAA 73SEG 01

l c

I .) a *> U • Z PAA 01

1 .5 0.3 EXRF A 1 U

1

1 .5 0.3 RTNA 80SL0 A 1 0 1

1 .5 0.3 PAA 80YAM A 1

1 .6 0.4 AA 7 QTJT T / OKI 1 A 1

1 .7 0.1 D* DCP Q 1 DT7TT A 1

1 .7 0.

1

DCP 79REE A 1

1 .8 0.2 ICPES 7 Q A Br AU 11 NAA 7 7LAU 0 1 2.1 0.02 ICPES 7 9 HER 01 2.2 0.7 * 14 NAA 81WIL 01 2.6 1

.

* CPXRF 80KIR 01 2.9 1

.

* CPXRF 7 7 CAM 01

4. * AE+AF 79ULL 01

4

.

1 .3 * AA 79M0N 01 4.3 * 16 AA 79ABO 01

1400. * OES 7 5JON 04

1500. OES 75JON

1560. * ICPES 78CAP 01 1770. 90. ICPES 810WE 01

1800. 100. COLOR 79MCQ 01

1800. OES 7 5JON 07

1800. OES 75JON 1

1

1900. 200. 6 FAA 81LAN 01 1900. 40. ICPES 79MCQ 02

1900. OES 7 5JON 06

i7UUt i nn A 1

l a aa OES 7 5J0N 1 A1U 1000

.

EXRF 77NIE 01

i qia fVYI AD 7 7U A M A A 7 n/U. t i 1

1

ICPES 82 JON A 1 U 1

1 Q ftA 1 7 OU • A A i i 1

1

T rnr c QO TAM A 1 zuuu 9 aaa

.

0

IT A A

r AA Ol T AM ol LAN A 1 (J 1 2000. 400

.

v^r A Rr A

1

2000. COI OR 79HIL 0 1 2000. 100. 5 FAA 81 LAN 01 2000. CPAA 80HAN 01 2000. ICPES 79EDI 01 2000. 100. 14 NAA 81WIL 01 2000. 500. ICPES 7 9 ABE 01 2000. 200. 14 NAA 81WIL 02

2060. 40. 11 ICPES 82JON 01 2070. 70. 7 NM 81 SHI 01 2070. 100. I ENA 79JON 01 2090. 60. 11 ICPES 82JON 01

2096.7 70.14 NAA 76GUZ 01 2100. 80. 12 FAA 78EDI 01

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

2100. 130. 7 NM 81 SHI 01 2100. OES 75JON 02

2100. 100. 14 NAA 80FAA 01 2100. FAA 79EDI 01

2100. OES 75JON 09 2110. 110. 7 NM 81SHI 01 2130. 20. ICPES 79HER 01 2160. 50. 12 FAA 78EDI 01 2190. 110. 7 NM 81SHI 01

2 300. OES 75JON 08

2 380. 180. EXRF 7 5REU 01 2400. OES 75J0N 03

2500. 400. * 14 NAA 77SEG 01

3100. * OES 7 5J0N 01

Pb (ppm)

15. 5.1 * CPXRF 80KIR 01

17 .6 * SSMS 81VER 02

26. * AA 76FUK 01 28.5 3.6 * FAA 77FUJ 01

31. 2. * ICPES 81 NAD 01

37 . AA 73L00 03

38

.

3. FAA 77LOR 01 40. 2. EXRF 7 3 SPA 01 40. 4

.

PAA 78HIS 01 40.7 3. EXRF 79GIA 01

41

.

ICPES 78DAH 01

41

.

2 . AA 83GLA 01

41 . 1 . ICPES 79HER 01 42. 1 .7 AA 80AGE 01 42. FAA 82H0E 01 42. 4. ITNA 77GUI 02

42. 4. NAA 76MIL 02

42. 1 . ICPES 79MCQ 02

42. 9. 14NAA 81WIL 02

42. FAA 78URE 02

42. 3. ICPES 79MCQ 01 42.2 11 FAA 79H0E 02

42.9 11 FAA 79H0E 02

43. FAA 80PRE 01 43. SSMS 74LUT 01 43.2 5.1 FAA 82 JEN 02

43.3 AA 76KRI 03

43.4 6 POL 72SIN 01 43.7 0.9 HAA 76VIJ 01 44. 2. NAA 77JER 01 44. 4. FAA 81KNA 01 44. FAA 79HEI 03

44. 2. FAA 80LEG 01

44. 2.3 6 POL 72SIN 01

44. 2. 11 ICPES 82JON 01 44. 2. AA 7 5ABU 01 44. FAA 73SEG 01 44.2 2.1 PAA 74CHA 01 44.3 FAA 79YAS 01 44.5 1.7 POL 74MAI 01 44.5 6.2 XRF 77SMI 04

44.6 1.7 POL 72MAI 01 44.6 1.7 POL 77MAI 01 44.67 1.53 ASV 7 7KON 01 44.9 1

.

ASV 82 SAT 02

44.9 ICPES 78CAP 01

73
TABLE H (cont)ANAL MP REF CONC ' UNCER COMMENT METH CODE NUM

45. 6 FAA 81JAC 01 45. 3.6 AA 79MON 01 45. 2. PAA 74LUT 01 45. 0.5 AA 73TAL 01 45. POL 74LUT 01 45.3 1.13 FAA 82 VAN 01 45.3 0.7 FAA 79DAB 02

45.3 CPXRF 75CAM 01 45.4 2. EXRF 73GIA 01 45.5 1

.

RTNA 72GIB 01 45.9 0.14 FAA 79ST0 01 46. 1. 11 ICPES 82 JON 01 46. 2. AA 80SCH 05

46. 2. FAA 79KRA 01 46. 2 . AA 77YAN 01 46. FAA 82 PRE 01 46

.

52. R* AA 75MAN 01

Ao . 4 AA 74BOP 01

i.e. c HO . 5 lo AA 79AB0 01 46 .8 5.6 HAA 82 WEI 01

47 . ICPES 81WEI 01 47. AA 79HIL 01

47 . 6 FAA 81JAC 01 47. 2.5 ASV 79BRI 02

47. 5. ASV 81DOG 01

47. 6. EXRF 79KUE 01 47. 4. ICPES 79ABE 01

47 .1 4.7 XRF 74REU 01

47.3 5.6 FAA 82WEI 01

48

.

5. AA 78RIT 01

48 . 5. AA 82RIT 01

Aft £ o ft J .o EXRF 75REU 01

*T7 0 PAA 80SEG 01

/ A49 . DCP 78NAK 01

49 . 5. EXRF 77NIE 01

49 .3 16 AA 79AB0 01

49 .3 1.5 PAA 80YAM 01 50. 11. AA 79MCQ 01

50. 5. EXRF 77FLO 01 50. FAA 74BRA 03

50. AE+AF 79ULL 01

50. AA 76FUK 01

51

.

3. LXKr oUDxL Ul

52.6 FAA 78CAP 01

54. 10. * CPXRF 77CAM 01 57. 12. * 14NAA 81WIL 01

57. 17. * ppA A 777TV fil 85. * OES 75B0L 02

115. * ft i pad m

(ppb)

1

.

L* RTNA 81BYR 01

(ppb)

60. SSMS 78URE 01 110. RTNA 80SL0 01 230. D* RTNA 82LAU 01 230. RTNA 77LAU 02

CONC UNCER

TABLE H (cont) ANAL REF REF COMMENT METH CODE NUM

(ppb)

ID .A K 1 N A 77NAD 0

lZUU • JUO. RTNA 7 4 CAR 03

(ppm)

15.5 L* ITNA 80T0U 01

5. 2. * EXRF 77FL0 01 9.8 1.3 XRF 7 7 SMI 04

10. 1. EXRF 79KUE 01

10. 1.5 CPXRF 80KIR 01

10. 1

.

14NAA 81WIL 02

10

.

NAA 77LAU 01

1 A 0.9 ITNA 79AHM 01

1 A ITNA 80CRE 01

1 f\ 0 il t ni a 1C.NA 79KUC A 1 U

in o u. / ITNA 7 5RIC 0

l a o f\ A U*D T TH A T/.O ill A O

10 .5 ITNA 78CAP 0

10.5 ITNA 79KUC 01 10.6 1 IENA 79KUC 01 10.8 0.4 ITNA 79SAT 01 10.95 0.08 ITNA 81K0S 01

11. 2. RTNA 77MEL 01

11. 16. R* AA 75MAN 01 11. 0.8 EXRF 73GIA 01

1 1

.

1

.

EXRF 80DYC 01

1 1

.

1

.

ITNA 78LAU 02

11

.

RTNA 72MOR 03

1 1

.

1

.

ITNA 77ZIK 0

1

11. i • 7 7 CAM 01

11 O 11 mi A A EXRF 7 3 SPA A 1 01

11 O 1 1 mi A O U.J TmA 81K0S A 1 Ul

11 .2 1.5 ITNA 81HAB 01

I 1 Oft I I »io A AO MANAAA "7 A 1 U 1

i i i 1 1 • j0 Q 1 • y

ej TTNA A 1 11 "X l 1 j ^ 0 n l \j i 1111.4A IT VD 1? O 1 IT C A 1 Ul

11 C 11.5 A L\ U.D EXRF 79GIA A 1 Ul

11.5 1

.

EXRF 77NIE 01 11.5 XRF 78CAM 02

11 .7 0.1 ITNA 78GIL 01

11.8 1.2 35 ITNA 81GLA 03

11 .8 ITNA 80SAT 01

11 .9 0.8 NAA 78GAN 01

12. 0.7 ITNA 82COR 01 12. 1.5 ITNA 77HAM 01 12. NAA 7 4 BEL 01

12. 0.04 ITNA 78FUR 01

12. 2. ITNA 76KUC 01 12. 1.1 6 ITNA 74BEC 01 12.1 1. 9 ITNA 78LAU 02

12.5 1. PAA 76KAT 04

12.5 0.6 PAA 78HIS 01 12.8 0.6 14NAA 81WIL 01

13. 2. ITNA 81KUL 01

13. 1

.

PAA 76KAT 02

13. 3.5 CPXRF 81 ROB 02

13. 0.9 VV 81N0N 01 14.8 * CPXRF 75CAM 01

74
TABLE H (cont) TABLE H (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE MUM

15 .61 3.01 * ITNA 79REN 03

19.9 SSMS 81VER 02

28. * EXRF 81PAR 01 30. * CPXRF 76ZEI 01

30. * CPAA 78MCG 01

pm)

1400. 600. * CPXRF 79REN 02

1660. 220. TCGS 79AND 01 1690. 5. TITR 80SMI 01 1700. 200. TCGS 79FAI 01 1860. 180. COLOR 82 BAR 01 1950. 200. XRF 82 BAR 01 2120. 50. EXRF 7/NIE 01 2120. XRF IOC AM f\ O 2150. 90 A tt voir / JtxILU \J l

2 150. zuu • U D 7 7T AM Ci 1 2200

.

103. OUN1IV. \J i 2300. 200. TCGS 77JUR 01 2400. FE 79B0G 01 2400. TURB 79B0G 01

27 00. 400. XRF 81 NAD 01 7020. 2620. * EXRF 77NIE 01

ppm)

99. L* ITNA 80TOU 01

1.1 0.2 A ITNA 77ZIK 01

2 .2 0.2 HAA 74L00 01 2.3 0.3 *H ICPES 79R0B 01 2.5 ITNA 78CAP 01

2.5 3.6 R* ITNA 79IMA 03

2.5 3.6 R* ITNA 79IMA 01 2.55 11 FAA 79H0E 02

2.55 1

1

FAA 79H0E 02

2.57 0.19 ITNA 79REN 03

2.62 6 NAA 78GAN 01 2.7 0.4 14NAA 81WIL 02

2.7 ITNA 80CRE 01 2.7 0.1 ITNA 781AU 02

2.7 NAA 77LAU 01

2 .7 1 I ENA 79KUC 01

9 *? L.I U .4 6 ITNA 7hBEC 01

9 7 L • / nU.J9 £O 1 I IMA / H J5L L U

1

L.I 9 7 n 9 U . L K1NA / hOOL Ul

9 7 L.I A 9 0. i ITNA 74RAN 02

9 79 Cm 1 L A 9 D.L ITNA oZQUR 01

9 71 L.I L A A

1

0.01 ITNA 79AHM 01

2 .77 0.02 H ICPES 81PAH 01

2 .8 0.1 RTNA 78GAL 01 2.8 0.1 H ICPES 82 HAH 01 2.8 0.2 ITNA 81K0S 01 2.8 HAA 80H0N 01 2.8 1 I ENA 79KUC 01 2.8 0.1 7 RTNA 77GIL 03

2.8 11 HAA 82KUE 03

2 .8 ITNA 79KUC 01 2-85 0.06 RTNA 80SL0 ui

2.86 0.08 RTNA 78GIL 01

2.88 0.05 7 RTNA 77GIL 0 3 2.9 0.1 IENA 81K0S 01

ANAL REF REF CONC ' UNCER COMMENT METH CODE HUM

2.9 0.2 ITNA 78VAL 01 2.9 0.5 RTNA 79REN 01

2.9 0.09 RTNA 79HOE 01 2.92 0.08 7 RTNA 77GIL 03

2.99 0.05 HAA 76FIO 01 2.99 0.45 RTNA 79ROS 02

3. RTNA 72MOR 03

3. 0.2 FAA 80NAK 01

3. 11 HAA 82KUE 03

3. RTNA 79BYR 01 3.02 0.26 HAA 79VIJ 01

3.1 0.03 W 81N0N 01

3.1 0.1 ITNA 79SAT 01

3.1 0.7 ITNA 77HAM 01 3.14 0.13 RTNA 72BYR 01 3.15 0.26 PAA 74CHA 01 3.16 0.26 NAA 77JER 01 3.2 0.2 GCMES 75TAL 01

3.25 0.3 PAA 76KAT 04

3.3 0.3 ITNA 81KUL 01 3.3 0.2 5 ITNA 80T0U 01

3.3 11 HAA 82KUE 03

3.3 0.6 RTNA 77KUS 01 3.3 0.14 ITNA 79K0B 03

3.3 0.2 PAA 76KAT 02

3.5 0.2 * PAA 78HIS 01 3.5 0.3 * FAA 78HAY 01

3.78 0.02 * ITNA 81HAB 01 3.8 0.6 *6 NAA 78GAN 01

3.8 0.2 * RTNA 73TJI 01

5.1 1.1 * 14NAA 81WIL 01

>pb)

2000. L* 14NAA 81WIL 01 97. L* ITNA 80TOU 01

40. 3. 6 ITNA 74BEC 01 40. 6 NAA 78GAN 01 40. 10. 6 NAA 78GAN 01 41. 4. VV 81N0N 01

44. 3. ITNA 74RAN 02

52. 3. ITNA 79CHA 04

54. 4. RTNA 80SLO 01

Dl . D . u i 60. 1 . ITNA 78LAU 02

62 . 2 • T TU A XT.NA 7 QVAH A 9 U J £9 MA A NAA ft 1 u I £ 9 8

.

ITNA 76KUC A 1 U 1 65. NAA 77LAU 01 65. 3. ITNA 75RIC 01 66. 6. ITNA 79SAT 01

67. 5. ITNA 81HAB 01 67. ITNA 78CAP 01 73. ITNA 80CRE 01 75. 5. 5 ITNA 80T0U 01

80. 6. ITNA 79REN 03

80. ITNA 79KUC 01 90. 20. ITNA 81KUL 01 no. * SSMS 78URE 01 170. 50. * RTNA 77MEL 01

200. * RTNA 72M0R 03

220. 10. * PAA 74CHA 01

75
TABLE H (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

(ppbT

100. L* HAA 82J0N 01 300. L* EXRF 79GIA 01 1600. L* ITNA 74GUI 01 100. L* HAA 82 JON 01

24. 6.7 * FAA 81MEY 01

53. * FLUOR 79TAM 01 55. 9. HAA 76FI0 01 56. 20. RTNA 79R0S 02

57. 6.3 ITNA 77HAM 01 58. 14. RTNA 73TJI 01

60. 20. RTNA 74GOE 01 65. 14. 9 ITNA 80WAN 01 68. FAA 82HEI 01 70. 200. R* RTNA 81GLA 03

70. FAA 78CAP 01

70. 20. HAA 82TAM 01 70. 4. ICPES 80HAA 01

70. 10. H ICPES 82HAH 01 74. ITNA 81HAN 01 74. ITNA 81MEY 01

75. 5. 7 RTNA 77GIL 03

76. 10. ITNA 79AHM 01 76. 3

1GC 81UCH 02

76. 1 .3 HAA 81HAN 01 77. 6. FAA 79V0B 01

77. 5. FLUOR 76CHA 02

77. 2. 11 GC 81UCH 02

77. 17 FLUOR 74AND 01 78. 7. 34 HAA 78FLA 01 78. 7.2 HAA 81MEY 01 78. 11. RTNA 82P0L 01 78. HAA 77IHN 01 78. 5. GC 77P00 01 78. 4. ITNA 77GUI 02

79. 12. RTNA 72R00 03

79. 12. RTNA 77R00 02

79 .8 8. NAA 76GUZ 01 80. 30. ITNA 81K0S 01 80

4. FLUOR 80KOH 01 80. 10. 9 ITNA 79PAV 02

80. RTNA 72M0R 03

80. 10. 9 ITNA 79V0B 01 80. 10. RTNA 75ABU 01

80. 20. SSMS 77R00 02

80. 17 FLUOR 74AND 01 80. 10. RTNA 80KNA 01 80. 10. RTNA 740RV 01 80. 20. HAA 80AGE 02

80. NAA 78GAN 01 80. 1. - FAA 80NEV 01

82

20. IENA 81K0S 01 82. 24. HAA 76IHN 02

83. 12. 9 ITNA 77V0B 01 83. 4. VV 81N0N 01

83. 4. GCMES 74TAL 02

83. 4. DCP 81 CAR 02

84. 8. RTNA 78GIL 01

85. 4. ITNA 79SAT 01 86. 10. ITNA 78GIL 01

87. 3. FLUOR 74LEI 01

TABLE H (cont)ANAL REF REF CONC UNCER COMMENT METH CODE NUM

87. 10. 7 RTNA 77GIL 03

87. 7. HAA 75SIE 01 87. 17 FLUOR 74AND 01 87. 3. 6 FLUOR 750LS 01 88. 7. RTNA 73HEY 01 88. 11. FLUOR 74IHN 02

88. 16. ASV 7 6AND 01 89. 17. ITNA 77VOB 01 89. 3. 6 FLUOR 7 50LS 01 90. HAA 80HON 01 90. 10. ITNA 82QUR 01 90. 10. 7 RTNA 77GIL 03

90. 20. ITNA 79PAV 02

90. 10. RTNA 78GAL 01

90. 30. ITNA 78LAU 02

90. 10

RTNA 7 7 BAN 03

100. 20

6 ITNA 74BEC 01 100. ITNA 79V0B 01 100. 20. 9 ITNA 78LAU 02

100. ITNA 80CRE 01 100. 40. NAA 74LEI 01 110. 20. RTNA 80SL0 01 110. 30. AA 79PAV 02

118. 79. HAA 77IHN 03

130. 40. * RTNA 77MEL 01

140. * ITNA 74RAN 02

200. ITNA 78CAP 01 1100. 170. * HAA 74CHU 01

(ppm)

475.8 12.3 ITNA 75PIE 01 475.8 12 .29 NAA 76GUZ 01 480. 14. CPXRF 80KIR 01 500. 200. 14NAA 80FAA 01 600. VV 81N0N 01

7 50. NAA 78GAN 01 1000. 160. * 14 NAA 77SEG 01

2340. 60. * IENA T ft T f\ XT f\ 1 79 JON Ul

(ppb)

3100. L* ITNA 80TOU 01

16. 3. * IENA 81K0S 01

19. 4

* ITNA 81K0S 01 88. 8. 5 ITNA 80T0U 01 90. SSMS 78URE 01 90. i An ITNA 79IMA 01 100. RTNA 77LAU 02

100. D* RTNA 82LAU 01

100. 30. T TWA 77MAH fi 9 / / run/ \j £. 100. ITNA 79KUC 01 100. NAA ~t "7T An A 1 / / LAU U

100- 1 IENA 79KUC 01

105. 4. RTNA 80SLO 01 110. 10. ITNA 78LAU 02

110. ITNA 80CRE 01 110. 30. TCGS 79FAI 01 130. 40. ITNA 7 7 HAM 01 140. RTNA 72M0R 03

140. 1 IENA 79KUC 01 140. 40. ITNA 74RAN 02

76
TABLE H (cont) TABLE H (cont)

ANAL REF REF CONC UNCER rnuucwr LUMMtn 1 METH CODE MUM UNCER COMMENT

150. 20. vv 81NON 01 Ta (ppb)

170. 30. * TCGS 79AND 01 320. 120. ITNA 79REN 03 5.

7. 2. (ppb) 10. 10. 3. 1500. L* ICPES 78CAP 01

180. 10. H ICPES 82HAH 01 Tb (ppb)

284. 4. 5 RTNA 74BYR 01 290. 25. RTNA 77BYR 01 1.23 0.12 * 304. 15. 5 RTNA 74BYR 01 9. 1. 340. 90. ICPES 80HAA 01 12. 2. 375. 25. COLOR 820MA 01 13. 4100. * RTNA 72BOW 01 13.

14. D*

(ppm) 15.

18. 1. 14.5 2.5 * FAA 77FUJ 01 80. * 18.1 * SSMS 81VER 02

23. * OES 7 5JON 03 Te (ppb)

28. 0.6 PAA 78HIS 01 28. 28.3 R* AA 7 5MAN 01 11. 3. 35 31. 3.3 CPXRF 80KIR 01 31.3 4.1 XRF 77SMI 04 Th (ppb)

31.7 4.8 14NAA 7 7 VAN 01 33.1 EXRF 81BIS 01 1000. L*

34. 1. FAA 82SUZ 03 6.6 0.3 * 34.3 0.5 EXRF 73SPA 01 6.8 0.4 * 35. NAA 77LAU 01 44.

35. 3. 9 ITNA 78LAU 02 44. 1 35. 2. EXRF 80DYC 01 50. 10. 35. OES 75J0N 04 52. 4. 35. 3. ICPES 7 9ABE 01 59. 13. 35.2 ICPES 78DAH 01 59. 20.

36. CPAA 78MCG 01 60.

36. CPXRF 76ZEI 01 60.

36. 6. ITNA 78LAU 02 69. 1 36.2 2. PAA 74CHA 01 90. 50. * 36.3 1.3 EXRF 79GIA 01 36.5 2. EXRF 77FL0 01 Ti (ppm)

36.5 4. EXRF 75REU 01

36.5 0.3 ICPES 79HER 01 2.4 0.4 * 36.5 1. PAA 76KAT 04 6.6 0.5 * 36.6 1.2 EXRF 73GIA 01 7.6 * 37. 1. ICPES 79MCQ 02 14.2

37. 1. PAA 76KAT 02 17.2 0.3

37 . 1. ITNA 79SAT 01 18. 8.5

37. 2. ICPES 79MCQ 01 26. 3. 37.2 0.2 IENA 81K0S 01 26.

37.4 8.3 CPXRF 81R0B 02 30. 4.

38. 5. NAA 78GAN 01 40.

38.7 1.5 ITNA 81K0S 01 60. * 39. 2. 14 NAA 81WIL 02 96. 12. * 40. RTNA 72M0R 03 191. 33. * 41. 3. RTNA 77KUS 01 42.2 4.2 XRF 74REU 01 Tl (ppb)

44.2 2.85 NAA 76GUZ 01 45. 15. CPAA 77ZIK 01 20000. L*

45. OES 75J0N 01 74.

45. 2. ITNA 7 4RAN 02 200. 40. 53. 4. * 14NAA 81WIL 01 300- 100- 118. * EXRF 81PAR 01

ANAL

METH

REF CODE

REF NUM

NAA

ITNA ITNA

ITNA

ITNA RTNA

ITNA

RTNA

RTNA ITNA NAA

ITNA

SSMS

RTNA

EXRF

IENA ITNA ITNA IENA

RTNA

ITNA

ITNA

ITNA

ITNA NAA

IENA

VV

CPAA

ICPES

ICPES

SSMS

COLOR

EXRF

14 NAA

SSMS

14 NAA

ITNA NAA PAA

ITNA

ITNA FAA PAA

PAA

77LAU 01 78LAU 02

80CRE 01 74RAN 02

77NAD 02

80SLO 01 78LAU 02

77LAU 02

82LAU 01

80CRE 01 77LAU 01 74RAN 02

78URE 01

75GLA 01

79GIA 01 81K0S 01 81KOS 01 79KUC 01 79KUC 01 80SL0 01 78LAU 02

81KUL 01 74RAN 02

80CRE 01 77LAU 01 79KUC 01 81N0N 01

77ZIK 01 79ABE 01 78CAP 01 81VER 02

82KIR 02

79GIA 01 81WIL 01 78URE 01 81WIL 02

78LAU 02

77LAU 01

78HIS 01 81HAB 01

74RAN 02

82HEI 01 80SEG 01

78HIS 01

77
TABLE H (cont) TABLE H (cont) ANAL REF UF ANAL W *EF CONC UNCER COMMENT METH CODE NUM CONC ' UNCER COMMENT METH CODE NUM

Tin (ppb) 580. 70. ITNA 75RIC 01 580. ITNA 76BAT 01

i a RTNA 77LAU 02 598. 32. ITNA 80HEY 01

1 A RTNA 82LAU 01 600. 90 RTNA 79BLO 01

1 7 1

J . / Z U - 1 j ITNA 77NAD 02 f\ AA 9 A A ITNA 78LAU 02

10 . S SMS 78URE 01 £ 1 A o lu

9 9 15. ITNA 73PIE 01 622

23. 1

RTNA 72LEV 01 U (ppb) 643. 129. RTNA 76GUI 01

700. 100. ITNA 79K0B 03

20. L* RTNA 80SL0 01 750. 1 10. VV 81N0N 01 2000. L* EXRF 79GIA 01 Q AA BUD. ITNA 78CAP 01

18. 3. * IENA 79FAA 01 Q AA 9 A ITNA 76GAL 01

255. PAA 80SEG 01 ??nn 1UU. if ICPES 79ABE 01 25 . 4

35 RTNA 75GLA 01 300. ITNA 81GLA 03

9 ^ 0 Z J • Z1 K 1 1MR 78DER 01 640. 310

UU 7 5GUI 01

ZD • o

j • i\ 1 IMA 72BEC 03

97 QO a ITNA 81KUL 01 U fnnhl

9R£. O •

O.J • RTNA 80AUG 01

282NT 72BEC 03 TLiTM* RTNA 72MOR 03

283. IENA 81K0S 01 1

10 . RTNA 80SLO 01

9Q o,j * RTNA 80AUG 01 20

7

RTNA 77KUS 01

i t nuc 1 UMb 72BEC 03

30. 4. 13 PAA qi cpr U 1 Y (ppb)

30. 35 DNA 81GLA 04

30. 6. 13 PAA 81SEG 01 1 100. L* 14NAA 81WIL 02

30.6 0.6 35 DNA 80GLA 04 1 100. L* 14 NAA 81WIL 01 99 Q T TV A 1 i IMA 74WEA 01 1000. L* EXRF 79GIA 01 32. 5 m ITNA 81K0S 01 480. SSMS 78URE 01 33. 2. DNA 83GLA 01 56. 9. *35 DNA 81GLA 03 VVi yd ^^ppo; !^nK^

V (ppb) C A50. ITNA 78LAU 02

1 1 . RTNA 80SLO 01 1000. L* NAA 77LAU 01 20. SSMS 78URE 01

Li rvmr CiAivr 79GIA 01 21. 1. ITNA 77NAD 02

a no. Li RTNA 72M0R 03

25. D* RTNA 82LAU 01

1 /• A

H AA T XL* ITNA 74RAN 02 25. RTNA 77LAU 02 1

c+b* TTM A X IMA 74HOF 01 29. 3. ITNA 81K0S 01

9 /. A OA 1 1 RTNA 72LEV 01 31. 1

IENA 81K0S 01 9A 1 OA ITTT UU 7 5WEL 02 40. NAA 77LAU 01

370. 1 1 • FAA 77MYR 01

97 7 1 A D TU A K1NA 80HEY 01 Zn (ppm)

90 A Q flfi R* 1 1NA 79IMA 01 390

980. R* ITNA 79IMA 03 40. L* 14NAA 81WIL 02

400. 100. ITNA 77ZIK 01 1 10

L* 14 NAA 81WIL 01

401

16RTNA 81C0R 02 10000. L* ITNA 80TOU 01

401

16

RTNA 79C0R 01 12. EXRF 82KEE 01 408. 16

RTNA 80HEY 01 13. OES 75B0L 02

409 . 41

RTNA 72DAM 01 15 . 3. CPXRF 77CAM 01

4 10

15 - RTNA 80HEY 01 17 . * AA 76KRI 03

4 35

RTNA 80HEY 01 17.1 2. * EXRF 77FLO 01 AAA Art R TMA K IWA 79BL0 01 18. * OES 7 5JON 09

A 7 1 14 . 1

RTNA 78BYR 01 19. 4. ICPES 79HER 01

Aft A noZo * COLOR 82KIR 01 20. 3. ITNA 81KUL 01

J

^ AAUU .

1 en

1 j u. R TU A KlNA 77GUI 03 20. 6. CPAA 77ZIK 01 530. 50. 11 ICPES 82 JON 01 2 1

1

ICPES 79ABE 01 535. NAA 80KOS 02 21. 2. ITNA 75RIC 01 535. 30. 11 RTNA 78BYR 01 21.7 2.8 ITNA 81HAB 01 540. 20. 11 ICPES 82 JON 01 22. 3.1 CPXRF 80KIR 01 570. 110. ITNA 81HAB 01 22. ITNA 79KUC 01 570. 140. 6 ITNA 74HOF 01 22. 1. EXRF 80DYC 01

580. 130. ITNA 77HAM 01 22.5 0.8 AA 76GAL 01

78
TABLE H (cont) TABLE H (cont)

ANAL REF REF CONC " UNCER COMMENT METH CODE NUM

23. AA 73L00 03

23. EXRF 81BIS 01 23. 0ES 7 5JON 02

23. 1. RTNA 77MEL 01 23. 2.1 XRF 78LIN 01 23. ITNA 78CAP 01

23- 1 - RTNA 76MEL 03

23. AE+AF 79ULL 01

23.1 ICPES 78CAP 01

23.3 2.7 RTNA 74RAV 01 23.5 0.9 n ICPES 82 JON 01 23.5 1.8 AA 73THO 01 23.7 0.8 EXRF 73GIA 01 23.75 ITNA 82AKA 01

23.9 3.2 PAA 80YAM 01 24. 0.4 VV 81N0N 01 24. 1

.

AA 83GLA 01 24

.

i AA 77FRY 01

z*+ 9A • FAA 73SEG 01

9AZ H . 98 R* AA 75MAN 01 9A o£. •

1

1

1

1

AA 78GAI 01

9 A 11 . RTNA 740RV 01 9A AA 81ARA 01 24. 1 . 11 AA 78GAI 01 24. 3. AA 77YAN 01 24 .2 1.5 PAA 74CHA 01 24.2 1.5 NAA 77JER 01 24.3 0.3 11 ICPES 82 JON 01 24.5 0.6 RTNA 80SL0 01 24.5 3. EXRF 77NIE 01 24.5 XRF 78CAM 02

24.6 0.9 SSMS 72MAG 01

24 .6 RTNA 79BYR 01

9 A 7 z** . / 9Z «Z9 £O EXRF 79MAT 01 Zt9 A .0P. 1 1 1.1 ITNA 78GIL 01

9 A fi Z 4 . o1 0 1 .7 ITNA 7 9 SAT 01

9 ^ ICPES 81WEI 01

9 * Z J • ITNA 80CRE 01

9 S 11

1 1 1 1 ICPES 82 JON 01 25

.

RTNA 72M0R 03

25 ITNA 80SAT 01 25. 0ES 75J0N 0 3 25. 3. FAA 82 JEN 02

25. 1.6 EXRF 73SPA 01 25. 1. 11 ICPES 82 JON 01 25. 3. ITNA 78LAU 02

25. 2. 9 ITNA 781AU 02

25. 1. AA 78RIT 01 25 .07 0.76 NAA 76GUZ 01 25 .

1

0.7 AF 75EPS 01

25 .

1

0.8 AA 75EPS 01

25 .

3

SSMS 81VER 02

25 .

3

0.5 AA 80AGE 01 25 .3 2.5 6 EXRF 79MAT 01 25.3 2.1 EXRF 79GIA 01 25.5 1.1 6 ITNA 74BEC 01 25.5 11 AA 79H0E 02

25.6 3.4 EXRF 75REU 01 25.6 7.64 AA 79M0N 01 25.9 FAA 78CAP 01

26. 1

.

11 ICPES 82J0N 01 26. 3.4 ITNA 77HAM 01

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

26. 2.1 AA 78LIN 01

26. 3. ICPES 80SCH 05

26. 1. ICPES 79MCQ 01

26. 1. 11 ICPES 82 JON 01 26. 5. AA -y r k tit i r\ i 7 5ABU 01

o^26

.

1

.

ICrb o /yncy uz

26

.

o2

.

1

1

ICPES OZJUN Ul lb . MA & /HDCaLj Ul

o c lb

.

o

5 . c voir 70VTTP rtl AU9fi . a , ITNA 76KUC 01 26 . 0ES 7 5JON 11 26. 3. RTNA 74CAR 03

26. 0ES 7 5JON 05

26

.

OES 75JON 10 96 1 .3 1

1

AA 75ISA 01 9£ 1 9 9 Z .Z ITNA R2C0R 01

oc 1 A £ 0 1 inn TLvpr / *T DLj \j 01Ul 26 .8 1 o

1 .2 T TUA 1 1NA O 1 NU D Ul

0£ ft 26 .9 1 o

1 .2 PTWA 7^TTT / J 1 J 1 01Ul

27. 7. ITNA 77ZIK 01

27 . AA 79HIL 01

O"! 27 . 2

.

RTNA 77KUS 01

97LI %i 1

1

I CPE S oZJON 01

97 ICPES 70HAU f\ T /oDAH Ul

97 A*+ . PAA r AA 7 £V AT ft A 97 MNAAA A 7 7T ATT HI / /LAU U

I

97 ft.PC / 5JUN Uo

97LI • l A A AA 7 7 T7TJ V rt 1

11 • oZ . RTNA 74G0E 01 27

.

3. PAA 76KAT 02

27 . 2. FAA 74TAL 01 27. 2. 7 AA 73TAL 01

27.2 2.4 ITNA 74RAN 02

27.3 2.1 ITNA 82QUR 01 27.3 2.1 ITNA 79AHM 01

27 .4 2.7 XRF 74REU 01

27 .5 11 AA 79H0E 02

O "7 C 11 .6 1.3 CPXRF 81R0B 02

90 e

!>

.

FAA 7-7L0R 01 9R »j . C A£i 7 A TAT rtl / H 1AL U

1

28

.

Ii

.

lAjjr o 1 tULCi U 1 9R 1i . nrp

9« o

j . 71 AC J. A 17 / j 1AL U

1

9fl Zo • OES 75ISA 01 28 .

1

CPXRF 75CAM 01 28 .3 2.6 6 POL 72SIN 01 28.3 0.8 ITNA 79K0B 03

28.5 0.8 ICPES 81KNA 01 29. 5. NAA 78GAN 01 29. 2. ITNA 74GUI 01

29. 32. R* ITNA 79IMA 01 29

.

0.87 1

1

AA 75ISA 01

o ft 29

.

32. R* ITNA 79 IMA 03

9 Q zy

.

*1

.

FAA "7 Atf Ti A ft 1 79KRA 01 29 .

3

9 s PAA / OWiL U

1

29.5 6 AA 72SIN 01 29.6 16 AA 79 ABO 01 29.6 16 AA 79ABO 01 29.63 1.8 ITNA 7 9REN 03

29.8 6 POL 72SIN 01 30. 2. 5 ITNA 80TOU 01

30. 2. AA 79MCQ 01

79
TABLE I

TABLE H (cont) NBS SRM 1572—COLLECTED DATA

CONC UNCER COMMENT

ANAL

M£TH

REF CODE

REF NUM

4 TTMA 7QF1IR i orun nU ii 30. 3

.

PAA O \J ULjU 30.5 1 .2 RTNA 76GAL 0

1

31. OES 75JON 04

32. OES 75JON 07

34. 3. * PAA 78HIS 01 35.6 11.4 it XRF 7 7 SMI 04

38. 6. * FAA 77FUJ 01

41. * OES 75JON 08

45. * XRF 80SUZ 02

56. * CPAA 78MCG 01

56. * CPXRF 76ZEI 01 77. * EXRF 81PAR 01

81

.

* OES 7 5JON 01

(ppm)

5. L* 14NAA 81WIL 01

3. L* EXRF 79GIA 01 1.3 0.3 PAA 78HIS 01 1.6 0.2 9 I TOA 78LAU 02

2.1 NAA 77LAU 01

3. 1. 14NAA 81WIL 02

3.8 CPAA 77ZIK 01

210. 20. * PAA 74CHA 01

CONC

Ca (%)

3

3,

Cu (ppm)

16.

17.

Fe (ppm)

95.

96.

K (ppm)

17800.

18000.

Mg (ppm)

5600.

5700.

Mn (ppm)

23.

25.

U (ppb)

41.

Zn (ppm)

30. 31.

07

14

UNCER COMMENT

0.005

0.005

0.56

0.14

7.6

8.6

4.

11.

1.7

3.

12

5

11

11

11

11

1111

11

11

1111

11

11

ANAL

METM

AA

AA

AA

AA

AAAA

REF REF CODE NUM

75ISA 01 75ISA 01

75ISA 01 75ISA 01

75ISA 01 75ISA 01

1.5 0.62

11

11

AAAA

AA

AA

AA

AA

DNA

AA

AA

75ISA 01 75ISA 01

75ISA 01 75ISA 01

75ISA 01 75ISA 01

83GLA 01

75ISA 01 75ISA 01

80
TABLE J

NBS SRM 1573—COLLECTED DATA

ANAL REF REl CONC UNCER COMMENT METH CODE NUM

Ag (ppb)

180. 50. RTNA 80SLO 01

ppm)

182. OES 75JON 02

228. OES 7 5JON 11 280. OES 7 5JON 07 286. OES 75JON 08 296. OES 75JON 06

356. OES 75JON 03

382. OES 7 5JON 04

,391

OES 75J0N 09 495. OES 75JON 05

835. OES 75JON 01 1170. 60. 11 ICPES 82JON 01 1225 . 239. ITNA 77NAD 02

1280. ITNA 82GLA 02

1300. 80. ITNA 80SLO 01

As (ppb)

118. 10. 7* FAA 82H0E 02

170. 10. 7* FAA 82H0E 02

200. 40. RTNA 80SL0 01 225. 3. RTNA 79HOE 01 230. 30. 11 HAA 81 RAP 01

240. I ENA 83GLA 01 245. 5. 7 FAA 82HOE 02

250. 30. 11 HAA 81 RAP 01

250. 30. HAA 81KNA 01 260. 30. ITNA 77NAD 02

260. 80. HAA 81YAN 01

260. 30. 11 HAA 81RAP 01

260. HAA 81ARA 01 270. H ICPES 81PIC 01 290. 10. 11 HAA 82J0N 01 290. 10. COLOR 77BUR 01 290. 20. 11 HAA 82J0N 01

300. 30. FAA 80DUP 01

310. 10. HAA 80TAM 01 330. 30. * IENA 82G1A 02

Au (ppb)

0.8 0.1 RTNA 80SLO 01

B (ppm)

25.5 1.1 ICPES 79HER 01 26. OES 7 5JON 10

28. OES 75JON 02

29. OES 75JON 07

30. OES 7 5JON 04

32. 3. 35 TCGS 81GLA 04

32. OES 75J0N 06

32. OES 7 5JON 01

32. OES 7 5JON 03

35. OES 75JON 09

36. 3. TCGS 82GLA 02

37. OES 75JON 05

TABLE J (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

37. OES 7 5J0N 08

42. * OES 75J0N 11

Ba (ppm)

40. OES 75J0N 03

47. OES 75J0N 04

49. OES 75JON 1 1 56.5 11.24 NAA 76GUZ 01 58. OES 75J0N 05

59. OES 7 5J0N 01 63. 5. ITNA 77NAD 02

69. 14. ITNA 79REN 03

Br (ppm)

C (%)

Ca (%)

19. 1.5 5 ITNA 80HOE 01 19.8 0.6 5 JENA 79GLA 02

20.1 1.2 5 ITNA 80HOE 01 20.8 2.4 ITNA 80SLO 01

21. 3. ITNA 79REN 03

21. 1.2 5 IENA 79GLA 02

21.9 0.2 ITNA 77NAD 02

25.31 1. ITNA 77STE 02

29. 2. *35 NAA 81GLA 03

54. * EXRF 81PAR 01

37 .67 0.45 CB 82GLA 02

37 .92 0.26 CB 80SCH 02

2.22 0.08 ITNA 80SLO 01 2.38 * OES 7 5JON 04

2.4 0.07 ITNA 79REN 03

2.42 OES 7 5JON 07 2.43 OES 75JON 03

2.55 OES 75JON 02

2.62 OES 7 5JON 08 2.64 OES 7 5JON 10 2.65 0.07 6 EXRF 79MAT 01 2.705 0.206 NAA 76GUZ 01 2.75 0.005 11 AA 75ISA 01 2.8 OES 7 5JON 11 2.87 0.005 11 AA 75ISA 01 2.91 OES 75JON 05

2.92 0.08 6 EXRF 79MAT 01 2.92 OES 7 5JON 09 2.99 0.05 11 ICPES 82 JON 01 3.04 0.05 11 ICPES 82JON 01 3.08 0.05 11 ICPES 82JON 01

3.1 ITNA 82GLA 02

3.1 0.03 11 ICPES 82JON 01 3.19 OES 75JON 06

3.28 OES 75JON 01 3.41 0.09 ICPES 79HER 01 3.49 0.12 * ITNA 77NAD 02

5. 82 * EXRF 81 PAR 01

81
TABLE J (cont)

ANAL REF REF CONC rnuucMT LUMMtn 1 METH CODE NUM

(V oDin^ r r

,u /

11 .0A * 1 1 FAA 8 OPRE 01

2 .

1

6 POL 72SIN 01 2.2 11 FAA 80PRE 01 2.3 0.1 FAA 80LEG 01 2.3 11 FAA 8OPRE 01 2.3 11 FAA 8OPRE 01 2.3 11 FAA 8OPRE 01 2.3 FAA 8 OP RE 01

2 .4 0.01 1

1

ICPES 82J0N 01

Z .4 u . zz

co POL 72SIN 01

Z mJ FAA 82PRE 01 Z.J AOAQVV 01

L • JJ ft HQ 1 1 1 1 ICPES 82 JON 01

£ • J D U • UD 1 1 I 1 ICPES 82 JON 01 2.6 0.1 11 ICPES 82 JON 01 2.7 0.4 RTNA 80SL0 01

2.7 ASV 74COP 01

2.74 0.2 ASV QIC *T> 82SAT

2 .8 0.2 AA 80SCH 05

2.8 0.2 FAA 83GLA 01 2.9 0.1 FAA 81KNA 01

3.3 0.2 * ICPES 79HER 01

(ppm)

1

.

0.1 RTNA 80SL0 01

(%)

1 .04 A AO 0.02 ITNA 80SL0 01

1 .05 0.072 ITNA 77STE 02

1 .085 0.12 NAA 76GUZ 01

1.1 0.07 ITNA 77NAD 02

(ppb)

400. 106. NAA 76GUZ 01

467. 25. ITNA 77GUZ 01 495. FAA 82HOE 01 510. 10. 11 FAA 80FUD 0

1

540. 30. RTNA 80SLO A t 01 550. 10

.

1

1

FAA 80FUD 01

ft in in ITNA 77NAD 02

UOUt ftHO in ITNA 79REN 03

( ppm)

2 .28 0.06 *11 ICPES 82JON 01

3.1 11 AA 79HOE 02

3.107 1 .08 NAA 76GUZ 01 3.7 0.3 ITNA 82GLA 02

3.8 0.3 35 FAA 81GLA 03

3 .8 0.2 11 ICPES 8 2 JON 01 3.9 0.3 ITNA 77NAD 02

3.94 11 AA 7 9 HOE 02

4.3 AA 81ARA 01 4.3 FAA 8 2 HOE 01 4.5 1.6 ITNA 79REN 03

4.6 11 AA 79HOE 02

5.9 0.2 * ICPES 7 9 HER 01

CONC

Cs (ppb)

43.

54.

56.

140.

Cu (ppm)

3.7.7

7.7

8.2

9.9.4

9.5

9.8

10.

10.1

10.4

10.4

10.4

10.5

10.8

10.81

TABLE J (cont) ANAL REF REF UNCER COMMENT METH CODE NUM

10

10

1111

1112. 12. 12.

12.2

13.

13.5

14.1

14.1

15.

15.

15.

15.

17.

17. 20.

25.

Eu (ppb)

15. 25.

55.

F (ppm)

5.5.7

6.

200.

2.4.

6. 30.

L* ITNA ITNA

ITNA ITNA

ITNA

82GLA 02

77NAD 02

83GLA 01 77GUZ 01 79REN 03

* AA 81ARA 01 0.5 6 POL 72SIN 01

6 POL 72SIN 01 0.4 11 ICPES 82 JON 01 OES 75JON 02

6 NAA 72SIN 01 0.2 11 ICPES 82 JON 01 0.4 11 ICPES 82 JON 01 OES 7' 5JON w/O 1/11 0\J 3J 0.4 RTNA 74RAV 01 0.6 VV 80SCH ns

0.2 ICPES 79HER 01 0.5 11 ICPES 82 JON 01 0.8 RTNA 80SL0 01

0.1 COLOR 76ZAN 02

0.02 COLOR 77BUR 01 0.1 D* AA 76ZAN 02

0.1 AA 76ZAN 01 OES 75J0N 04

11 AA 79H0E 02

0.2 AA 76EPS 02

11 AA 79HOF O?

0.17 11 AA 75ISA 01 0.14 11 AA 75ISA 01 1.3 6 EXRF 79MAT 01 OES 75JON 10 0.4 AA

5.64 NAA

1.3 ITNA 77GUZ 01 OES 75J0N 09 OES 75J0N 11 OES 7 5JON 06

OES 75JON 01 OES 75J0N 05

OES 75JON 08

* OES 7 5JON 07

* EXRF 81 PAR 01

2. ITNA 77GUZ 01

5. ITNA 7 7 NAD 02

8. RTNA 80SL0 01

1. MS 77STE 02

0.2 ISE 83KNA 01 0.7 ISE 83GLA 01

82
TABLE J (cont) TABLE J (cont)

ANAL UF KEF ANAL REF REF CONC UNCER COMMENT METH CODE NVIM CONC UNCER COMMENT METH CODE MUM

Fe (ppm) I (ppb)

55. * OES 7 5JON 01 280. 30j\j . ft*) CAT rtl 162. * OES 75JON 09 300. inn PA A 77UT1 ni 220. * AA 81ARA 01 390. 120. RTNA 77STE 02

266. OES 75JON 06 In ( BDh^ 267. OES 7 5JON 03

340- OES 75JON 02

o A t 34Z. OES 75JON 04 U»70 0.08 RTNA 7ARAV 01

j DU . OES 7 5JON 11 K (X) it V • OES 75JON 08

442115. 11 AA 75ISA 01 463. 157. 11 AA 75ISA 01 3

0.29 * ICPES 79HER 01 469.25 118.3 NAA \ ft 7 TAW ft? 478. Ave Ubd 7CTAU ftc "X Q 1 J >ol hpq 7 Q TAW 1 ft / 3JUIN 1 U 507.6 14.3 TTMA 1 l\a\}L Ul J .to AWC Utb 7 C TAU ft T /3JUN 07 531. 14. 11 DO TAW AI A ACQ »UD D l A A AA 78SZY 01

534. 7 S TAW 1 ft *

A

• K1> n ns T •PAT A ITNA 79REN 03

552. OES 7^.TOW ft 7 A 1

*» • 1 / i A A AA 7 QC7V A t /Soil Ul

568. 3. ICPES 79HER / 7llul\ 01V A A ?Q

0.2

OES 7 5. TAW ft A 575. 10. 11 COLOR 1

ICPES ft? TAN ft 1 597. 11 COLOR ft? SCH 03

A 0.2

OES 75JON 08

604. 11. 11 COLOR A2SCH 03 A A 11 ICPES 82 JON 01 623. 10. 6 EXRF 79MAT 01

A A 0.1 11 ICPES 82 JON 01 625. 14. 11 ICPES 82 JON 01 A A 97 0.281 NAA 76GUZ 01 642. 17. 11 ICPES 82 JON 01 A A7 0.15 ITNA ftft<n a fti 658

18. 11 ICPES 82 JON 01 A A7 0.24 1 Inn 77WAA ft? 661

14. ITNA 77NAD 02 4.49 7 Q PA A A 1 fyyJJvJ Ul

665. 11 AA 79HOE 02 4.51 OES 7 DJON OV 670. 50. 35 ITNA 81GLA 03 4.58 OES 75J0N 03

672. 11 AA 79HOE 02 4.58 0.004 11 AA 75ISA 01 685. 20. ICPES 80SCH 05 4.6 0.2 11 ICPES 82 JON 01

698. VOLT 81SZY 01 4.6 0.008 11 AA 75ISA 01 706. 12. ITNA 79DAS 01 4.6 OES 7 5J0N 06

706. 12. RTNA 80SLO 01 4.74 OES 7 5JON 05

730. 90. ITNA 7 9REN 03 4.79 n oa e.D 7QMAT 01 831. 1U . EXRF 79MAT 01 4.8 OES 7f JOs TONvn A1 A1 1170. * EXRF 81PAR 01 5.16 0.06 *6 EXRF 79MAT 01 5.72 * OES 7 5JON 01 Fe(II) (ppm) 9 .24 * EXRF 81PAR 01

540. VOLT 81SZY 01 La (ppb)

Fe(III) (ppm) 346

79

ATA A NAA

640. 40. ITNA 77NAD Uz

158. VOLT 81SZY 01 770. 110. RTNA 80SL0 01 800. 200. ITNA 79REN 03

Ga (ppb)

Lu (ppb)

69.3 67. NAA 76GUZ 01 12. 1i. * RTNA 80SL0 01 H (%)

Mg (ppm)

c3 • 0.1 35 TCGS 79GLA 04

3.1 0.2 CB 82GLA 02 6000. OES 75J0N 08

C 1 A 5 .14 0.07 CB 80SCH 02 6000. 600. ITNA 80SL0 01 6100. 600. ICPES . 79HER 01 Hg (ppb) 6300. OES 75J0N 09 6600. OES 75J0N 07 90. 8. ITNA 77NAD 02 6700. 200. 11 ICPES 82 JON 01

91

11. CVAA 82GLA 02 6700. 3. 11 AA 75ISA 01 128. 118. NAA 76GUZ 01 6700. 3. 11 AA 75ISA 01

83
TABLE J (cont) TABLE J (cont) ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

Mn

6800. OES 7 5JON 10

i N (%) liiii'i oy uu

o a a 1

ICPES 82JON (J 1 bVUO

OES 75JON 4.9 0.2 35 TCGS 6900. 200, 11 ICPES 82JON 01 79CLA 04

7000. OES 7 5JON 03 4.94 0.11 CB 80SCH 02

7000. 200. 1

ICPES 82JON 01

4 .95 0.08 CB 82GLA n9u z 7100. OES 7 5JON 02 Na (ppm)

7 9nn inn ITNA 77NAD n 9

/ 4UU

7 ti 7AM n c. 350. 7400. Arc 7 ^ TflN 06 OES 75JON 04

7400. 7 ^ 1AM 1

388.

46 .

25

OES 75JON 02

7800. * OES 75JON 01 459

/,7 c NAA

ITNA

76GUZ

80SLO

0101 (ppm)

/i Q Q

1 AA 78SZY 01

500

9nn zuu

ITNA 79REN 03

138. * OES 7 5JON 07 522

531

bUz . 610

1 9 13. ITNA 77NAD 02

189. 7 *\ TO.M 04

1 OES 75JON 08

189. ATT C OEb 7 5J0N 10 AA 78SZY 01 OES 75JON 06

197. AFC 7 ^ TO.N 09 650. OES 7 5JON 03

198. OES 7 5JON 06 800. OES 7 5JON 01 200. ITNA 79REN 03 820

OES 7 5JON 09 209.18 9.93 NAA 76GUZ 01 Q c,n OES 75JON 05

05

209 .2 11 .9 ITNA 77GUZ 01 1090

70. ITNA 82 SCH

2 10

OES 7 5JON 02 1600. * OES 7 5 TON 1

9£ 1 . 1 AA 77GUZ 01

9 1 ^ Z 13 . OES 7 5JON i i 1

Nd (ppb)

9 1

Z ID •

l 7 AA 75ISA nU i

9 17 Z 1 / • E3 . ICPES 8 2 JON n i \j i 700. 100. RTNA 80SLO 01

9Z 11 7/ • AA 79HOE 09UZ

9— 101R . 1 J . AA 75ISA 01 Ni (ppm)

Z Z 1 . -> - ICPES 82J0N nU i1 222

5j J ICPES 82JON 01 1.1 0.08 1

ICPES 82JON 01

223AA 7 9 HOE 02 1 .12 0.06 11 ICPES 82 JON 01 223. 7. 6 EXRF 79MAT 01 1 .12 0.08 11 ICPES 82J0N 01

2 27 . OES 7 5JON 05 1 .2 0.3 ITNA 77NAD 02

230. 5. 11 ICPES 82JON 01 1 .3 0.2 11 ICPES 82JON 01

2 30. OES 75JON 03 5.9 0.6 * ICPES 79HER 01 231. 10. ITNA 80SL0 01 0.3 0.2 * RTNA 80SLO 01

2 34. 5

VV 80SCH 05

235 . 5. ICPES 79HER 01 P (ppm)

Z jo .

1 7 ITNA 77NAD U L /Hi . OES 7 5JON Uo 2400

OES 75JON 04

TCI OES 75JON A 1 2800

OES 7 5JON 10 Zoo. ITNA 82GLA 9 i n n OES 75JON 07 ZDD • QO - D EXRF 79MAT n i 9J 9nn zuu • 9nn zuu • b FAA 81LAN 01

A 1 A * EXRF 81 PAR nU i1 3200.

3300. 200

g

OES

FAA

7 5JON

81LAN

n c. nU l1

( ppm) 3300.

3300.

OES

OES

7 5JON

7 5JON

09

1

0.4 0.2 11 ICPES 82 JON 01 3300. OES 7 5JON UO 0.5 0.1 < 11 ICPES 82JON 01 3 300. OES 7 5JON

0.5 0.1 11 ICPES 82JON 01 3 320 - 160. ICPES 810WE nU i1 0.5 0.3 11 ICPES 82 JON 01 3400. 100. 11 ICPES 82 JON 01 0.62 0.04 ITNA 77NAD 02 i Ann FAA 79EDI n 1 U 1 0.65 0.1 RTNA 80SLO 01 3400. OES 7 5JON 03

2.8 * OES 75JON 10 3400. ICPES 79EDI 01 4.2 * OES 75JON 11 3420. 89.5 NAA 76GUZ 01 4.5 OES 75JON 03 3500. 200. 6 FAA 81 LAN 01 11.7 * OES 7 5JON 01 3500. 100. 11 ICPES 82JON 01 14.6 * OES 7 5JON 07 3500. 100. 11 ICPES 82JON 01 17.9 * OES 7 5JON 02 3500.

3700.

100.

100.

11 ICPES

ICPES

82 JON

79HER

01

01

84
TABLE J (cont) TABLE J (cont)

CONC

3800.

5000.

Pb (ppm)

UNCER COMMENT

ANAL

METH

OES

OES

REF CODE

REF NUM

75JON 02

7 5JON 01

3.2 *6 POL 72SIN 01

•4. ASV 74COP 01

A.

3

0.2 1

1

ICPES 82 JON 01

4.5 0.1 6 POL 72SIN 01

4.9 11 FAA 80PRE 01

5. 0.2 1

1

ICPES 82 JON 01

D

TTrAAA A ft 1 TAP V L 5.5 0.4 FAA 80LEG 0 1 5.5 FAA 79H0E 02

J . D g FAA 81 JAC 01

S .6 0.2 ASV 82SAT 02

1 1 1 1 PA A

S ft eD PA A Rl TTTN nU i1 5 ft 5 FAA 82K0I 01 5.8 6 FAA 81HIN 01

S ft 0 ft U A A rum n\j ii 5 .8 FAA 82K0I 01 5.9 1

1

FAA 8OPRE 01

5 .95 0.06 FAA 79DAB 02

6. 11 FAA 80PRE 01

6. ASV 82GAJ 01

6. FAA 82H0E 01 6.1 0.3 AA 80SCH 05

6.1 1

1

FAA 79H0E 02

6.2 0.3 FAA 81KNA 01 6.2 PA A 6.3 11 FAA 80PRE 01 6.55 0.22 ASV 80SZY 01

6.6 FAA 82PRE 01 7.1 0.9 FAA 82WEI 01

7.5 11 FAA 80PRE 01 8.3 1.1 * ICPES 79HER 01

it Q 1 D AT? U

1

(ppb)

40. RTNA 80SLO 01

vppm;

IS 1

A

JL J • ID 1 • 5D NAA 76GUZ 01 15.21 2.3 ITNA 79REN 03

16.4 0.5 ITNA 77GUZ 01 16.5 0.7 ITNA 77NAD 02

22. 3. 35 ITNA 81GLA 03

40. * EXRF 81 PAR 01

(ppb)

30. 1

.

RTNA 79H0E 01 30. 2. RTNA 80KOS 02

34. HAA 82KUE 03

40. 2. ITNA 7 7 NAD 02

120. 50. * ITNA 79REN 03

CONC

Sc (ppb)

138.

160.

170. 208.

220.

Se (ppb)

49. 50.

57.

61 . 84.

Sm (ppb)

110.

200.

Sr (ppm)

36. 38.

38. 45.

54. 65.5

102.

Ta (ppb)

430.

Tb (ppb)

4.

Th (ppb)

190.

220.

Ti (ppm)

68.

U (ppb)

20.

50.2

54.

60.

63.

UNCER ANAL REF REF COMMENT METH CODE NUM

7 ITNA 77GUZ 01 JU

.

ITNA 79REN 03

3. ITNA 77NAD 02

89. NAA 76GUZ 01 30. RTNA 80SL0 01

100. L* HAA 82 JON 01 100. L* HAA 82 JON 01

5. ITNA 77NAD 02

20. RTNA 80KNA 01

3. 11 GC 81UCH 02

2

,

i i 1

1

81UCH 02

oy ITNA 80WAN 01

15

.

RTNA 80SLO 01 90

.

ITNA 7 9REN 03

0.6 ICPES 79HER 01 OES 7 5JON 03

1. OES 7 5JON 04 ITNA 77NAD 02

5.84

OES 75JON 01

NAA 76GUZ 01

* EXRF 81 PAR 01

300.

1.

20.

30.

20.2.3

120.

3.

ITNA 79REN 03

RTNA 80SL0 01

ITNA 77NAD 02 RTNA 80SLO 01

ITNA 77NAD 02

R*

35

RTNA RTNA

DNA

DNA DNA

80SL0 01 78DER 01 83GLA 01 81G1A 03

80GLA 04

85
TABLE K

TABLE J (cont) NBS SRM 1575—COLLECTED DATA

ANAL REF REF ANAL R CONC UNCER COMMENT METH CODE NUM CONC ' UNCER COMMENT METH C(

Ag (ppb)

V (ppm)

150. 50. RTNA

1 .19 0.01 11 ICPES 82JON 01

1.27 0.035 RTNA 78BYR 01 Al (ppm)

1.3 0.2 ITNA 7 7 NAD 02

1.42 0.08 11 ICPES 82J0N 01 255. * OES

287. * OES

W (ppb) 405. OES

449. OES

40. L* RTNA 80SL0 01 465. OES

473. OES

Yb (ppb) 483. OES

521. OES

80. 20. RTNA 80SL0 01 526. 17. 11 ICPES

565. 44. ITNA

Zn (ppm) 582. 47. CPXRF

585. AA

26. * OES 75J0N 09 620. 35 ITNA

29. * ASV 74COP 01 750. 200. * ITNA

48. * OES 75J0N 10 1243. * OES

50. OES 7 5JON 03

52. 1. 11 ICPES 82J0N 01 As (ppb)

54. 4. RTNA 80SL0 01

56. 2. 11 ICPES 82 JON 01 150. 50. RTNA

57. 2. 11 ICPES 82 JON 01 154. 5. 7 FAA

58. OES 7 5JON 06 180. 15. 7 FAA

58. OES 7 5JON 01 181 . 3. RTNA

58.03 3.33 NAA 76GUZ 01 187. 6. 7 FAA

58.9 11 AA 79H0E 02 190. 10. 11 HAA

59. 2. 11 ICPES 82JON 01 190. 30. 11 HAA

59. OES 75JON 11 200. 30. ITNA

59. 3. 11 ICPES 82 JON 01 200. 20. 7 RTNA

60. OES 7 5JON 02 210. 10. COLOR

60. 3. 1

1

ICPES 82 JON 01 215. 6. HAA

61. 6 AA 72SIN 01 220. 40. I ENA

62. 4. ITNA 77NAD 02 230. 20. FAA

62 4 6 ITNA 79REN 03 230. HAA

62. 3. 11 ICPES 82 JON 01 240. 20. 7 RTNA

62.5 AA 81ARA 01 62.9 6 POL 72SIN 01 Au (ppb)

62.9 1.7 6 POL 72SIN 01 63. 2.5 11 AA 75ISA 01 0.3 0.08 ITNA

64. 3. 11 ICPES 82 JON 01 0.9 0.1 RTNA

65. 7. ICPES 80SCH 05

65. OES 75J0N 07 B (ppm)

65. OES 7 5JON 05

65. 3.25 11 AA 75ISA 01 13. OES

68. 11 AA 79H0E 02 13. OES

72.8 2. 6 EXRF 79MAT 01 13.3 0.7 ICPES

73. 3. ICPES 79HER 01 15. OES

75. * OES 75J0N 08 15. OES

78. 2.1 *6 EXRF 79MAT 01 16. 4. ITNA

86. * OES 75J0N 04 16.1 0.1 TCGS

124. * EXRF 81PAR 01 17. 1 . 35 TCGS

17- OES

18. OES

19. OES

20. OES

20. OES

20. OES

REF

80SL0 01

75J0N 11

7 5J0N 02

7 5JON 06

7 5J0N 07

7 5JON 05

75JON 08

75JON 04

75J0N 03

82J0N 01 77NAD 02

80KIR 01 81ARA 01 81GLA 03

80SL0 01

7 5JON 01

80SL0 01 82HOE 02

82HOE 02

79HOE 01

82 HOE 02

82 JON 01

82 JON 01

77NAD 02

77GIL 03

77BUR 01 81UTH 01 82GLA 02

80DUP 01

81ARA 01 77GIL 0 3

79REN 03

80SLO 01

75JON 08

75J0N 09

7 9 HER 01 75JON 05

7 5JON 02

82SCH 05

82GLA 02

81GLA 04

7 5JON 01 75J0N 07

7 5JON 06

75JON 03

75J0N 11

7 5JON 04

86
TABLE K (cont) TABLE K (cont)

ANAL REF KEF ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

' UNCER COMMENT METH CODE NUM

220. 30. FAA 83GLA 01 Ba (ppm) 250. 10. FAA 80LEG 01

75JON 03

260. 10. ICPES

3. OES 300. 40. A A 80SCH 05

6. OES 75JON 05 300. 100. 11 ICPES 82 JON 01

6.1 0.4 ITNA 77NAD 02 310. 30. FAA 81KNA 01

7. ftF<? 7 5JON

7. OES 75JON 04 Ce (ppb)

8. OES 75JON 01

Br (ppm)

150. 30. RTNA oOSLO 01

CI (ppm)

5.4 1.2 CPXRF 80KIR 01 6.1 0.09 ITNA 79REN 03 243. 20. ITNA TTMAn AO / / NAD UZ

6.25 0.2 ITNA 80H0E 01 280. 30. X inn OUOLU Q ACT A ftl Ul 6.4 0.8 5 I ENA 79G1A 02 510. 120. 7QRFN O? 6.43 0.08 ITNA 77NAD 02 551. 37. ITNA 7 7CTF 07

6.8 0.5 5 IENA 79GLA 02

7.4 0.3 ITNA 77STE 02 Co (ppb)

8. ITNA 83GLA 01

30. * EXRF 81PAR 01 110. 1?A A f AA OZnulj Ul

c (%)

110. RTNA 80SLO 01 130. 20. ITNA 77NAD 02

134. 6. ITNA 77GUZ 01 50.37 0.16 CB 80SCH 02 340. 180. * ITNA 79REN 03

50.4 1.3 3D CB 79GLA 04

en ~i U .7 CB 82GLA 02 Cr (ppm)

54. 2. 35 TCGS 79GLA 04

Ca (ppm)

1.3 0.2 *11 T CDTJ C 2.25 11 AA

2.25 11 AA

3100. 200. * ITNA 80SLO 01 2.39 1 1 AA /9HOE \)Z 3300. * OES 75JON 07 2.41 0.11 TTUA I IN A 3700. 500. CPXRF 80KIR 01 2.6 0.2 ICPES O 1 VU A A 1 3800. OES 75J0N 05 2.6 0.1 T TM A 1 IwA QOPT A AO 3800. OES 7 5J0N 02 2.8 r aa

3800. OES 75J0N 1

1

2.9 0.2 11 ICPES 82 JON 01

3900. OES 7 5J0N 09 3.1 0.6 ICPES 7 9HER 01 4000. 100. 11 ICPES 8 2 JON 01 3.93 0.05 * ITNA 7 9 REN 03

4000. OES 75J0N 06

4090. 20. 1

1

ICPES 82J0N 01 Cs (ppb)

4100. 30. 11 ICPES 82 JON 01

4110. 30. 11 ICPES 82 JON 01 200. L* UNA QOpT A AO OZuJUri UZ 4290. 60. ICPES 79HER 01 101. 3. ITNA O "J \T A T\ AO 7 /NAD UZ

4290. 40. NM 81YUZ 01 104. 4. ITNA oJGLA Ul 4300. 600. ITNA 79REN 03 1 15. 7. T TM A 1 INA T7PH7 A1 / tUUL Ul 4500. 400. ITNA 77NAD 02 160. 60. TTWA 4600. OES 7 5JON 03

4660. AA 83GLA 01 Cu (ppm)

4800. OES 7 5J0N 04

4900. OES 7 5J0N 01 0.7 * OES 7 5JON 09

5300. * OES 7 5JON 08 2. OES 7 5JON 02

13100. * EXRF 81 PAR 01 2.41 0.09 RTNA 77DER 01

Cd (ppb)

2.5 0.3 11 ICPES 82 JON 01 2.7 0.2 11 ICPES 82 JON 01

140.

2.8 0.3 FAE 76EPS 01 70. 1

1

ICPES 82J0N 01 2.9 0.1 COLOR 76ZAN 02

160. 90. 11 ICPES 82 JON 01 2.9 0.2 11 ICPES 82 JON 01 180. 30. RTNA 80SL0 01 2.9 0.1 COLOR 76EPS 01 180. 90. 11 ICPES 82J0N 01 2.94 0.01 COLOR 77BUR 01 200. FAA 80PRE 01 3. 0.15 ICPES 81KNA 01 206. 10. RTNA 77DER 01 3. 0.5 11 ICPES 82 JON 01 210. FAA 82PRE 01 3. 0.52 CPXRF 80KIR 01

87
TABLE K (cont) TABLE K (cont)

ANAL REF UEF CONC UNCER COMMENT METH CODE NUM

3. 0-3 vv 80SCH 05

3. 0.3 D* AA 76ZAN 02

3. 0.3 AA 76ZAN 01 3.2 0.2 D* DCP 81REE 01 3.2 0.2 DCP 79REE 01 3.2 0.4 AA 76EPS 02

3.2 0.4 AA 76EPS 01 3.27 0.05 RTNA 80SLO 01

3.45 11 AA 79HOE 02

3.55 11 AA 79H0E 02

3.6 0.3 FAA 82KRI 01

4. OES 75JON 04

4.1 0.8 ICPES 7 9HER 01 4.5 OES 75J0N 07

5. OES 7 5JON 06

6. OES 75JON 08

it 8. * OES 7 5JON 01

ao

* OES 7 5JON 05

8. * OES 7 5JON 11 11. * AA 81ARA 01

C 1 5 J

* VBT? OOCTT7 f\0

Eu (ppb)

6. 2.6 ITNA 77GUZ 01 6.5 0.8 ITNA 77 NAD 02

F (ppm)

2.5 0.3 ISE 83KNA 01 2.9 0.8 ISE 83GLA 01 3.7 0.8 MS 77STE 02

Fe (ppm)

47. * OES 7 5J0N 09

106. * OES 7 5JON 06

118. OES 7 5JON 02

120. OES 75JON 03

142. OES 75JON 11 156. OES 7 5JON 01 170. 10. RTNA 80SLO 01 170. 10. ITNA 7 9 DAS 01 174. 0.9 11 COLOR 82SCH 03

174. 6. 11 COLOR 82SCH 03

175. 7. 11 ICPES 82 JON 01 177. 4. 11 ICPES 82 JON 01

182. OES 7 5JON 08

183. 3. ICPES 79HER 01 185. 11 AA 79H0E 02

185. 11 AA 79H0E 02

188. 17. CPXRF 80KIR 01 193. OES 75J0N 07 194. 10. ICPES 80SCH 05

194. 6. 1COLOR 82SCH 03

194. 4. 11 ICPES 82 JON 01 195. 10. 11 ICPES 82 JON 01

195.7 5.4 ITNA 77GUZ 01 196. 7. ITNA 7 7 NAD 02

198. 8. AF 81H0R 01 204. 12. ICPES 81KNA 01

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

254. OES 7 5JON 05

260. * OES 7 5J0N 04

280. 50. * ITNA 79REN 03

595. * AA 81ARA 01 790. * EXRF 81PAR 01

H (%)

6.39

6.5

6.54

Hf (ppb)

10.

Hg (ppb)

121.

133.

147.

157.

160.

I (ppb)

140.

150.

K (ppm)

0.07

0.1 0.08

8.

18. 20.

200.

20.

50.

35

11

L*

CB

TCGS

CB

RTNA

ITNA CVAA

CVAA

CVAA

RTNA

PAA

IENA RTNA

80SCH 02

79GLA 04

82GLA 02

80SL0 01

77NAD 02

79HOE 02

82GLA 02

80DUM 01 80SL0 01

77WIL 01 82SAT 01 77STE 02

2700. OES 75JON 05

3200. OES 7 5JON 09 3300. 100. ICPES 79HER 01 3400. 200. 11 ICPES 82 JON 01 3500. 500. CPXRF 80KIR 01 3530. 80. 11 ICPES 82 JON 01

3600. 100. ITNA 77NAD 02

3600. ICPES 79COO 01 3620. 40. 11 ICPES 82 JON 01 3700. 200. ITNA 79REN 03

3700. OES 7 5JON 03

3800. OES 7 5 JON 04

3850. 80. 11 ICPES 82 JON 01 4000. 100. ITNA 80SLO 01

4000. OES 7 5JON 01 4400. * OES 7 5JON 02

5100. * OES 75JON 06

5800. * OES 7 5JON 11

6 500. * OES 7 5JON 07

9100. * EXRF 81 PAR 01

(ppb)

130. 20. RTNA 80SLO 01 140. 10. ITNA 77NAD 02

210. 30. ITNA 79REN 03

(ppb)

1 .3 0.3 RTNA 80SL0 01

88
TABLE K (cont)ANAL REF REF CONC UNCER

Mg (ppm)

900.

1100. 100.

1 180. 30.

1 190. 20. 1200. 200.

1200.

1200. 20. 1200.

1200. 30. 1200.

1200.

1300.

1400.

1500. 200.

1500.

1600.

1700.

Mn (ppm)

4 30. 448.

567.

570.

580.

588.

652. 14. 652. 15. 654. 20. 655. 13. 657. 7 . 660. 28 . 668

.

670. 6

.

673

.

10 673. 10

.

677. 12. 678. 7 . 685. 15. 688.

698.

700. 100. 727.

738.

885.

2200.

Mo (ppm)

11

11

11

11

11

11

11

11

D*

11

11

OES

ICPES

ICPES

ICPES

ITNA OES

ICPES

OES

ICPES

OES

OES

OES

OES

ITNA OES

OES

OES

CPXRF

OES

OES

OES

OES

OES

OES

ICPES

ICPES

AA

ICPES

ICPES ITNA OES

ICPES

DCP

DCP VVICPES

ITNA AA

AA

ITNA XRF OES

OES

EXRF

75JON 09 79HER 01 82 JON 01 82J0N 01 80SLO 01

7 5J0N 07 82J0N 01 75JON

82JON

7 5JON 06

7 5J0N 02

75JON 03

7 5JON 08 77NAD 02

7 5JON 11

7 5JON 05

75JON 04

80KIR

01

01

01

75JON 09

7 5JON 01

7 5JON 06

7 5JON 02

75JON 04

75JON 0 3 82 JON 01

82 JON 01 77GUZ 01 82JON 01 82JON 01 77NAD 02

7 5JON 05

79HER 01 81REE 01 79REE 01 80SCH 05

81KNA 01 80SL0 01 79H0E 02

79H0E 02

79REN 03

80SUZ 02

7 5J0N 08

7 5J0N

81PAR

07

01

0.1 RTNA 80SLO 01 0.1 0.1 11 ICPES 82J0N 01 0.13 0.06 11 ICPES 82JON 01

0.2 0.1 11 ICPES 82J0N 01 0.2 0.1 11 ICPES 82JON 01

1 .5 OES 75JON 11

1 .7 OES 75JON 01

2.5 OES 7 5JON 07 3.6 * OES 75J0N 03

18.5 * OES 75J0N 02

CONC

N (%)

TABLE K (cont)ANAL REF REF UNCER COMMENT METH CODE NUM

1.11

1 .2 1.3

Na (ppm)

18. 20.

26.

30. 40.

70. 71.

78. 100.

100.

190.

Nd (ppb)

200.

Ni (ppm)

0.01

0.14

0.2

45.

100.

35

L*

CB

CB

TCGS

ITNA OES

OES

ITNA OES

ITNA OES

ITNA OES

OES

OES

OES

RTNA

80SCH 02

82GLA 02

79GLA 04

80SLO 01 75J0N 06 75JON 03

77NAD 02

7 5JON 09 79REN 03

75J0N 11 83GLA 01 75JON 08 75JON 01

7 5JON 05

75JON 04

80SLO 01

2.07 0.07 11 ICPES 82JON 01 2.2 0.2 ITNA 77NAD 02

2.2 0.1 11 ICPES 82JON 01 2.24 0.06 11 ICPES 82 JON 01 2.3 0.2 RTNA 80SLO 01 2.3 0.2 ICPES 79HER 01 2.39 0.09 11 ICPES 82J0N 01 2.63 VOLT 81PIH 01 2.7 1.1 CPXRF 80KIR 01

2.9 0.1 * DCP 79REE 01 2.9 0.1 D* DCP 81 REE 01 4. * FAA 82H0E 01

(ppm)

1000. 300. CPXRF 80KIR 01 1000. OES 75JON 04

1100. FAA 79EDI 01 1100. OES 75JON 09 1100. ICPES 79EDI 01 1170. 50. ICPES 810WE 01 1170. 40. 11 ICPES 82J0N 01 1180. 10. ICPES 79HER 01

1 190. 50. 11 ICPES 82J0N 01 1190. 20. 11 ICPES 82J0N 01 1200. OES 7 5JON 05

1260. 20. 11 ICPES 82JON 01 1300. OES 7 5JON 08 1300. OES 7 5JON 06

1400. OES 75JON 07 1400. OES 7 5JON 1 1 1600. OES 7 5JON 02

1800. * OES 7 5JON 03

2100. * OES 75JON 01

89
TABLE K (cont) TABLE K (cont)

ANAL UF XEF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

53. 8

.

ITNA 79REN 03

Pb (ppm) 130. * RTNA 80SLO 01

*T A 7 .4 1.3 * iiA t\.r Se (ppb)

0.4 11 Tfpr c ft9 TON 0 1 9.8 FAA 80PRE 01 100. L* HA A Q 9 TAW A 1 9.8 0.3 11 ICPES 82J0N 01 100. L* TJA A HAA Q 0 ir\ U A 1 oZJUN Ul

10 .4 FAA 82PRE 01 A

1

1. 11 onWJ Q i riru a i O 1 ULn U Z 1Ulfl • A* ASV 82GAJ 01 A 'J 1. 11 0 1 TTfU A 0 0 1 UL.H U Z 6 FAA 81HIN 01 4 4 . 8. T TWA 7 7 NAT*1 A9

i o s 6 FAA R2KOT 01 a 10. RTNA oUKNA Ul

10 .8 0.6 FAA 80LEG 01 j J

.

10. 9 ITNA ROWAN 0

1

10.9 0.3 FAA 81KNA 01 Q t 16. * 10 .93 0.91 ASV 80SZY 01

XI. 1

.

ICPES 79HER 01 >i ^pm;

1 1

.

6 FAA 81HIN 01

1

1

0.6 FAA 79nAB o? ? Aft 36. CJUnXK ftAVTP AlUl

i i x 1 • 6 r rtrt A9VOT Ozi 1\<J 1 01U 1

1

1

X 1 • 11 FAA r AA /jHUIj UZ Sm (ppb)

11 1 11*1 0.3 AA or\cru a ^ oUbOH Uj

11 o 11./ 1.1 nil HAA 0 0 t TC T A 1 20. 2. RTNA 80SL0 01

11 o F A A

r AA 130. 120. ITNA 79REN 9 J lull 03\J -J ii •> 11.2 11 V A A r AA 7Qunr AO /yHUc. uz 13.7 1 1 Q 1 .2 * FAA 82WEI 01

* EXRF 81PAR 01 4.7 0.2 AF 81H0R 01 4.9 U. 1 ICPES 79HER 01 5. OES 7 5JON 0 3 2. L* RTNA 81BYR 01 5.5 0.57 CPXRF 80KIR 01 10. OES 7 5JON 04

Pr (ppb) 20. * OES 7 5JON 01

70. L* RTNA 80SL0 01 Ta (ppm)

Rb (ppm) 1.74 0.27 ITNA 79REN 03

1

1

IX. 0.2 ITNA 7 7NAD 0 2 Tb (ppb)

12.22 0.85 TTNA 1 1 nr. 11CAY? 01

1 / . 5 3.9 ITNA 79REN 0 3 60. 10. RTNA 80SL0 01 13.1 2.6 CPXRF 80KIR 01

35. * EXRF 81 PAR 01 Th (ppb)

S (ppm) 34. 1

.

ITNA 77NAD 02

35. 5. RTNA 80SL0 01 580. 140. /"UV LrAKrO F 7QD17K1 AO 1500. 300. CPXRF 80KIR 01 U (ppb)

13. Z . RTNA 80SLO 01

15. DNA 83GLA 01 180

.

14 . 7 QVT T ft 1 15. U.J RTNA

180. 10. ITNA 77NAD 0 2 18. 6. 35 DNA 80GLA 04

lac 10 J • 2. RTNA 79HOE 01 20. 48. R* LinA RimjV 03

187. 7. HAA 78KUB 02

190. 10

.

RTNA 80SLO 01

198. 3. RTNA 80K0S 02

V (ppb)

220. 10 . 7 RTNA 77GIL 03

346. 18. RTNA 78BYR 01 220. 20

.

7 RTNA 77GIL 03

370. 90. 11 ICPES 82J0N 01 1140. 440. * ITNA 79REN 0 3 410. 60. 11 ICPES 82 JON 01

Sc (ppb)

470. 80. ITNA 77NAD 02

27. W (ppb)

4. ITNA 77GUZ 01 42. 2. ITNA 7 7 NAD 02 50. 10. RTNA 80SLO 01

90
TABLE L

TABLE K (cont) ANAL KEF REF CONC ' UNCER COMMENT METH CODE NUM

Zn (ppm)

5. A ULo

51. 9. CPXRF 79REN Oi

52. 1. I TOA 77NAD 02

53.5 2. RTOA 80SL0 01 57. 0ES 75JON 11 60. 3. 11 ICPES 82 JON 01 60.3 1.3 RTOA 77DER 01 61. 4. 11 ICPES 82 JON 01

63. J .

1 1 1

1

ftO Tf\M n 1 & A 7 ICPES 79HER 01

0<f - A 1 1 1 i ICPES 82 JON 01

D J. AA 81ARA 01 03. £0 • 7QHFN 01

O J o 4. 1

1

ICPES 82 JON 01 DO . 0ES 75J0N 06

67. XRF 80SUZ 02

bo - c3 •

i i 1 1 ft? TON 01

Aft DO • 0ES 7 5JON 08

71. l- D* DCP 81 REE 01 71. l. DCP 79REE 01 71. 10. 11 ICPES 82 JON 01 72. 0ES 7 5JON 02

74. 9. 11 ICPES 82 JON 01 74. 0ES 75J0N 03

82. 0ES 7 5JON 05

85. 0ES 75JON 07 87. 0ES 75JON 01 99. 10. * ICPES 80SCH 05

110. 12. * CPXRF 80KIR 01 141. * OES 7 5JON 04

NBS SRM 1577—COLLECTED DATA

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

(ppb)

130. L* RTOA 76GAU 01

5. *17 UU 74MAS 01 40. 8. RTOA 79WAR 02

51. 11. RTOA 77LIE 01 51. 11. RTOA 75LIE 01 60. ITNA 770SB 01 60. 1. FAA 75PIC 01 65. 5. RTOA 80SL0 01 65. 10. SSMS 77PAU 01

66. 21. ITNA 79CHA 04

Aft DO • C0 • T TH A I INA /oohH Ul

72. 13. AA 80JAC 01

a n tJU. 6

.

ITNA 79CHA 02

91. 26. * ITNA 73COR 01 194. *17 UU 74MAS 01 300. 100. *34 CPXRF 78J0L 01

400. * OES 75B0L 02

2000. 600. * RTNA 74SCH 03

(ppm)

15. L* ICPES 78CAP 01 80. L* 14NAA 81WIL 02

80. L* 14NAA 81WIL 01

1 .8 0.2 * ITNA 77G00 01 2.21 0.15 * ITNA 82EHM 01

5. ICPES 79MCQ 01

6. 3. ITNA 83GLA 01

6. 2. ICPES 7 9 ABE 01

7. 17 UU 74MAS 01 8. 0.6 11 ICPES 81BLA 02

8.2 0.8 11 ICPES 81BLA 02

11.3 2.9 6 ITNA 74H0F 01 15.3 1.1 ITNA 80SLO 01 20.4 2.9 6 ITNA 74H0F 01 20.8 0.7 RTOA 77BU0 01

23.4 0.6 RTNA 79WAR 02

23.6 2. ITNA 79CHA 02

30. 65. R* ITNA 79IMA 01 30. 65. R* ITNA 7 9 IMA 03

37. 6. ITNA 77ZIK 01

42. 13. ITNA 7 7 HAM 01 45.6 * . ITNA 73NAD 01 65. * ITNA 78CAP 01

As (ppb)

100. L* HAA 82JON 01 1300. L* UNAA 81WIL 02

200. L* EXRF 77NIE 01 104. L* ITNA 74NAD 02

100. L* ITNA 73NAD 01

700. L* CPXRF 77WIL 02

300, L* EXRF 79GIA 01 1300. L* 14NAA 81WIL 01

100. L* HAA 82JON 01

23. 12. HAA 82TAM 01 30. 15. I ENA 78WAN 01

40. 10. RTOA 80SL0 01

91
TABLE L (cont) TABLE L (cont) ANAL AEF REF CONC ' UNCER COMMENT METH CODE NUM

An RTNA 7SAR11 01 41. UMAAA A 7QT717A fl 1 43.3 U A A KAA / / 1 nN U 1 46

.

2

.

T>TV A RTNA fynOh Ul 47

.

5

.

HAA 82 SUB Ul 49

.

6. HAA 7 or 10 Ul 50. 10

.

U A A HAA oUAGE UZ

50. 10

.

miHAA /4L0U Ul

Eft !>U. 1]MAAA A JZ j

j . n/vn 7RFT /or Lit\A 01\j i 52

.

7

.

ITNA 79CHA 02

52. 3. AA 79FLA 02

52 .9 1 .9 H RTNA 790RV 01

0

4b * 7 RTNA O 1 NUli Ul

*iA A RTNA 78flAT 01 34 . A RTMA Ol D Itv Ul

ej • PTNA K 1NA

7 RTNA 7QUAR H9

34 * un r AH / 7T ILL. U 1 54

.

r5

.

n TV A R 1NA "7 QUA V (\ 1 /ynAi Ul

3D. J • MAA NAA 77PTT f. 1 / /ulL U

1

j j • 3 RTNA 77GTT 0^

3, HAA 81UTH 01 56. 4. RTNA 75LIE 01

56. 4. RTNA 77LIE 01 56.6 1 .2 NAA 74HEY 01

57. ASV 7 8DAV 01

58

.

3. RTNA 79HEI 04

JO . 3 RTNA 79RDS 02

JO . D q NAA 7fifi!JZ 01 rA

. 7 RTMA o 1 nUI' U 1 59

.

nmi a RTNA /DSTL UZ

63. 4

.

RTNA 740RV 01 64. 17 UU 7 4MAS 0

1

66. ASV 81 LEE 01 00 . z J

.

RINA 7 / C fu A 0 oy

.

i 71 / u u 7AMAQ / tPlAO 01U 1 p,n ou

.

RTNA 77TJI 01

100. 10. GCMES 75TAL 01 100. ITNA 770SB 01 150. ICPES 80HAA 01 200. 300. *6 CPXRF 77WIL 03

280. 100. *34 CPXRF 78J0L 01

500. * FAA 78CAP 01

600. 500. 6* CPXRF 77WIL 03

u • 1 I u • gnu a a fl 1

T * Ki N

A

OUoLU Ul

u • Z j u . 10 TJTM A K11NA / / 1 J 1 U 1

1 .7 0.4 RTNA 77KUS 01 4.9 0.8 RTNA 74SCH 03

6. 1. ITNA 79CHA 02

7. 0.8 RTNA 79WAR 02

29.2 2.1 * RTNA 77NAD 01

ppm)

2.24 6 AE+AF 74DAU 01

2.34 6 AE+AF 74DAU 01

3.2 0.2 TCGS 79FAI 01

4. 1. ICPES 79ABE 01

CONC

Ba (ppm)

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

0.12

0.13

0.22

1.8

2.92

Be (ppb)

3.5. 17.

Br (ppm)

4.3

4.7

6.1

35

4

78

7

7

7

78.

8.8.8.22

8.4

8.5

8.5

8.5

8.6

8.8

8.8

8.8

8.9

9.

9.

9.9.3

9.3

9.3

9.34

9.37

9.4

9.5

9.5

9.7

9.8

10.

10. 10.4

11.

11.

11. 11.1

12.

13.4

22.

20.

30.0.13

0.02

0.39

3. 60.

1.3.4.

9.9

0.8

0.6

5

5

1

5

1 0.4

0.6

1. 9.9

9.9

0.4 0.4

0.3

1.4 2.1

1.0.6

0.6

0.8

3.0.82

0.4

1.

1.0.7

2.3

1.6

4.

L*

L*

14 NAA

ITNA RTNA

ICPES

RTNA RTNA

ITNA

81WIL 02

78CAP 01 76GAU 01

78DAH 01 79WAR 02

77GUI 03

73NAD 01

10.

L* ICPES 82SCH 01 L* ICPES 78CAP 01

6 ICPES 82SCH 01 FAA 750WE 01 FLUOR 77WIC 01

L* ITNA 80TOU 01 *17 UU 74MAS 01

it CPXRF 77RIN 01 CPXRF 77WIL 02

17 UU 74MAS 01 EXRF 80DYC 01

5 ITNA 80HOE 01

5 IENA 79GLA 02

RTNA 77TJI 01 RTNA 76GAU 01

5 IENA 79GLA 02 RTNA 79WAR 02 ITNA 83GLA 01 ITNA 79CHA 02

R* ITNA 79IMA 03

R* ITNA 79IMA 01 NAA 78GAN 01 EXRF 79GIA 01

5 ITNA 80H0E 01 EXRF 77NIE 01 ITNA 77HAM 01 CPXRF 78VIS 01 ITNA 78BEH 01 ITNA 77JUR 02

1 IENA 79KUC 01 ITNA 80MAE 01 CPXRF 79REN 02 ITNA 74DON 01 ITNA 73NAD 01 XRF 77SMY 01 ITNA 80CRE 01

6 CPXRF 77WIL 03

1 IENA 79KUC 01 ITNA 79KUC 01 CPXRF 80MAE 01 CPXRF 82 ROE 02 ITNA 82AKA 01

CPXRF 80KIR 01 ITNA 78CAP 01

5 ITNA 80TOU 01 RTNA 74SCH 03 ITNA 77ZIK 01 *17 UU 74MAS 01

* ITNA 77ZIK 01

92
TABLE L (cont)

CONC

C (%)

ANAL REF KEF UNCER COMMENT METH CODE NUM CONC

Cd (ppb)

TABLE L (cont)ANAL REF REF UNCER COMMENT METH CODE NUM

49.6 1.5 35 CB 79GLA 04

AO ft 7 n n7 n?VJZ 51

.

2 . 35 TCGS n/. 52. 2

.

TCGS /y fai n i

f \

i nnn 1UUU. T * 1 /. U A A O 1 T.7T T n o Uz

LK 1 /. U A A 7 AW / /VAN n i U

?nn T * TTNA 1 inn 7/ 0.MAH JPiAX' n i snnn 14NAA ftl TJTT n i 30. * AE+AF 79ULL 01

71

.

23. * EXRF 77NIE 01 80. 30. ITNA 74WES 01 90. 13. CPXRF finMAF 01

94

.

112. AA 79MAN 01

inn ITNA 7 8FUR ni inn ?nzu . RTNA 76GAU n i inn CPXRF 77WIL 02

i n i AA 79L0C 01 ini IU j •

1 9 1 Z • 7QMAM n i inA l 7 hit u u 7 AMA^ ni

infi 1J • 9Z AA 74WES 01

107

.

ITNA 82AKA 01 107. 232. R* ITNA 7 9 IMA 03

107. 232. R* ITNA 79IMA 01 108. 9. CPAA 77ZIK 01

114. 2. 1 ICPES 78SUD 01 115. 12. RTNA 80CAN 01

1 16

.

2

.

1 AA 77UCH 02

1 16

.

2. AA 801 ID 01

1 lfi 9

,

ICPES 78SUD 0

1117. 1 Q 9z

.

ii A A nou z

1I 9nZU . 9z .

i i 1

TPPF <S ft9 OZ JUW THN ni Izl

.

o3 . i i 1CW ILrtoc Q0 inw n i

11 99Z i. o onu A A oUilAA ni

11 99Z Z 3 7 ClU 11

1 99. 1 Z J •

i 71/ AAA A n i 124. in ITNA 79CHA 02

124.67 8.48 NAA 76GUZ 01 125. 13. RTNA 79WAR 02

125. 8. ITNA 75PIE 01 127. 7. AA 80UCH 01 127. 12. ICPES 79MCQ 02

127. 5. AA 7 SHIN 01

130. 10. ITNA 77ZIK 0

130. 30. ITNA 83GLA 01 131. 9. CPXRF 80KIR 01 131. 8. CPXRF 78VIS 01 131. RTNA 75STE 02

134. 18. ICPES 7 9 ABE 01 135. ICPES 78DAH 01 137.5 18. PAA 76KAT 04

140. ICPES 78CAP 01

151. 7.4 * CPXRF 81 ROB 02

158. 15. * EXRF 80DYC 01 309. * ITNA 78CAP 01

210.

230.

240.

240.

246.

250.

250.

250.

250.

253.

260.

260.

260.

260.

260.

260.

260.

260.

260.

266.

266.

269.

270.

270.

270.

270.

270.

270.

270.

270.

270.

270.

270.

280.

280.

280.

280.

280.

283.

283.

283.

288.

288.

288.

288.

290.

290.

290.

290.

290.

290.

290.

290.

290.

290.

290.

1600.

100.

2500.

100.

42.

10.

56.

30. 20.

24.

30.

30. 20.

10. 20.

30. 27.

20.

13. 50.

20.

10. 20.

30. 60.

80.

20.

50.

30. 50.

29.

26.

35.

35.

10. 30.

30.

10. 20.

20.

30.

13.

L*

L*L*

L*

**11

17

11

11

11

17

1717

11

17

11

17

OES

POL

ICPES

POL

ASV

FAA FAA

UU

NAA

AA

VV

AF

FAA AE+AF

ASV

FAA RTNA

FAA

FAA AA

RTNA

FAA RTNA

RTNA

FAA RTNA

FAA AA

AA

AA

AA

AA

TCGS

UU

FAA UU

UU

SSMS FAA AA

ASV

AA

FAA RTNA

UU

RTNA

FAA

RTNA

RTNA

FAA

FAA

FAA FAA RTNA NAA

ASV

AA

UU

RTNA AA

7 5B0L 02

72SIN 01 78CAP 01

72SIN 01 79ST0 01

75BL0 01

82SUZ 01 74MAS 01 76GUZ 01 78EVA 01 79CHA 02

75EPS 01 75BL0 01 74RAI 02

81DAN 01

82AKA 01 80SL0 01 75SLA 01

78PIE 01 74ULL 01

740RV 01 79DAB 02

74SCH 03

79MAY 01

74RAI 02

74R00 01 81KNA 01 77FRI 01

7 9 WAR 01 81BLA 0 3 75EPS 01 79LAK 01

79FAI 01

74MAS 01 74GR0 01 74MAS 01 74MAS 01 77PAU 01

82HOE 01 81BLA 0 3 74COP 01

80SCH 05

79ST0 01 75HAL 01 74MAS 01 80GRE 01 81ZAU 01

77LIE 01 75LIE 01 80LEG 01

83GLA 01 80JAR 01

7 9 WAR 01 77BAJ 02

76DER 01

81 DAN 01

79FLA 02

74MAS 01 79DER 01 73TAL 01

93
TABLE L (cont) ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

290. 17 UU 74MAS 01 290. 30. RTNA 74HEN 01 300. 40. 7 RTNA 81KUC 01 300. 20. RTNA 77TJI 01

300. ASV 82GAJ 01 300. ICPES 80HAA 01 300. 70. AA 80AGE 01 300. 20- RTNA 78GAL 01

300. 50. AA 75HIN 01 300. 23. AF 75WOR 01 300. 25. FAA 74TAL 01 300. 700. AA 76LAN 01 300. 25. 7 AA 73TAL 01

300. 30. RTNA 76GAU 01

300. 18. 7 AA 73TAL 01

300. 800. 6 FAA 76LAN 01 300. 18. FAA 74TAL 01

310. 7 RTNA 81KUC 01

310. 50. FAA 80P0L 01

310. RTNA 75STE 02

3 10

.

20. FAA 78GR0 01

^ in 1

1

FAA 81DAN 01

J LSJ a 130. 5 FAA 76LAN 01 320. 40. 11 AA 81BLA 03

320. 11 FAA 81DAN 01 337. 58. * RTNA 79PIA 01 350. 50. * 1

1

ICPES 82 JON 01 390. 70. *11 ICPES 82 JON 01 550. 450. * AA 79M0N 01 560. 130. *34 CPXRF 78J0L 01

(ppb)

3000. L* 14NAA 81WIL 01

13. 17 UU 74MAS 01

18. 4. RTNA 80SL0 01

21.5 RTNA 77LAU 02

22

.

RTNA 82LAU 01 46

.

14 . RTNA 76GAU 01

(ppm)

5400. L* 14NAA 81WIL 01

1880. *17 UU 74MAS 01 2155. 170. *34 CPXRF 78JOL 01 2410. 600. EXRF 77NIE 01 2460. 35 ITNA 81GLA 04

2480. 17 UU 74MAS 01 2500. 130. 35 ITNA 81GLA 03

2530. ITNA 78CAP 01

2542. 300. ITNA 77ZIK 01

2550. 100. ITNA 74WES 01 2570. 3110. R* ITNA 79IMA 01 2570. 3110. R* ITNA 79IMA 03

2590. 17 UU 74MAS 01 2610. 200. ITNA 79CHA 02

2610. 17 UU 74MAS 01 2615. 192. RTNA 74SCH 03

2632. 67. ITNA 77GUI 02

2632. 67. NAA 76MIL 02

2650. 100. ITNA 80SLO 01

2680. 80. RTNA 79WAR 02

2685. 16 5. PAA 76KAT 04

TABLE L (cont)ANAL REF REF CONC UNCER COMMENT METH CODE NUM

2690. 170. EXRF 80DYC 01 2700. 70. ITNA 83GLA 01 2750. ITNA 73NAD 01

27 50. 110. ITNA 78FUR 01 2760. ITNA 82AKA 01 2793

.

294 .4 MA A 2830. 200. NAA 78GAN 01

1 Q AA ITNA 80CRE 01 3000. 100. TCGS 79FAI 01

3000. 190. ITNA 77HAM 01 3200. 800. CPXRF 79REN 02

3500. 200. * 14NAA 81WIL 02

1 1663. *17 UU 7 4MAS 01 (ppb)

6000. L* EXRF 79GIA 01 120. *17 UU 74MAS 01 170. 10. NAA 78GAN 01

170. ITNA 73NAD 01

170. 20

.

ITNA 79CHA 02

17 UU 74MAS 01 178. j . 1 Q I T A D AO

180. 10

.

RTNA i\ l Pitt 77PTT m

180. 30. TTNA 7 QUA p n

1

180. 10

.

MA A 188. 97 K A A T CC 11*7 C\ 1

i T PH A

i on onzu • cO ITNA 74BEC 01 200

.

16

.

FAA 74WES 01

203. RTNA 75STE 02

210. ITNA 79KUC 01 210. 30. AA 79FLA 02

210. 40. FAA 7 9 WAR 01 210. 20. ITNA 74WES 01 217 . 13. ITNA 81KRI 01 220. RTNA 75ABU 01

223. 1 1

.

RTNA 77LIE 01

O O "> 11. RTNA 75LIE 01

£. LJ • 7

/ . COLOR 82KIR 01

1

1

J . 17 UU 74MAS 01

Z JU

.

20

.

RTNA 80SL0 01

2 30

.

20. 6 ITNA 74BEC 01

2 30. 100. ITNA 77ZIK 01

233. 5. RTNA 79DER 01 240. 10. ITNA 73COR 01 240. ITNA 80CRE 01 240. CHEML 79MIL 01

240. 37. ITNA 77HAM 01 240. 14. I ENA 75MAZ 01 240. 30. ITNA 78BEH 01 240. 20. RTNA 74HEN 01

7 RTNA 81KUC 01

O. 1 5 1 • ITNA 81HOL 01

*> Aft Z » • T T*RT A 1 INA / y IE. 1 U 1 L J U = ir\ jU • nj 1TMT Q 1 MA D A 1 o 1 MAK U

1

250. ITNA 82AKA 01 257. 2. ITNA 74LIN 01

260. 7. 7 RTNA 81KUC 01 260. 10. ITNA 79 SAT 01

260. 21. RTNA 76GAU 01

260. 17 UU 74MAS 01 265. AA 7 9ABU 01

94
TALBE L (cont) ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

269. 30. AA 80JAC 01

27 5. FAA 82HOE 01 280. NAA 79MIL 01 290. ITNA 78CAP 01

300. ICPES 80HAA 01 300. ITNA 770SB 01 310. 120. 14NAA 81WIL 02

j 1U oU. D TM A K.11NA U j 310. 120. 14NAA 81WIL 01 uu 74MAS 01 360. 60. ITNA 78FUR 01 370. 60. * RTNA 77MEL 01 390. *17 UU 74MAS 01 400- * FAA 7 5 SLA 01 410. 120. * RTNA 77KUS 01 246. 14. RTNA 77TJI 01

Ippb)

300. L* 14 NAA 81WIL 01

3400. L* AA 79M0N 01

100. L* RTNA 77MEL 01 300. L* 14NAA 81WIL 02

4000. L* EXRF 79GIA 01 400. L* ITNA 78CAP 01

5. 1600. R* VV 7 7PAR 01 22. 10. ICPES 81BLA 01

35. 4. 1

1

FAA 80KUM 01 35. 3

.

GC 8 1 BLA 01 44.9 5. 11 RTNA 76PIE 01 51. 17 UU 74MAS 01 53. 9. FAA 74WOL 01 60. 12. AA 80JAC 01 60. 30. RTNA 74SCH 03

72. 8- 11 ICPES 81 BLA 02

74. 5. RTNA 77LIE 01 78.9 11 NAA 79VER 01 80.6 11 NAA 79VER 01 85. 9. RTNA 78GAL 01 88. 7 RTNA 81KUC 01 88. 8. 11 FAA 80KUM 01 92. 10. 7 RTNA 81KUC 01 92. 9. 11 ICPES 81 BLA 02

94. 8. 7 FAA 80CHA 01 94.8 19.5 11 RTNA 76PIE 01 98. 5. RTNA 75LIE 01 115. 42. RTNA 79PLA 01 120. 70. ITNA 78BEH 01 120. 40. AA 79FLA 02

123. 6. RTNA 77LIE 01 130. 17 UU 74MAS 01 130. ITNA 80CRE 01 130. 50. RTNA 77TJI 01

130. 30. RTNA 78G0E 01 140. 17 UU 74MAS 01 144. 23. 7 FAA 80CHA 01 150. 30. ITNA 74D0N 01

150. 10. NAA 78GAN 01 150. 17 UU 74MAS 01 160. 60. RTNA 76GAU 01 160. 5. 11 RTNA 78MCC 01 163. 10. RTNA 74MCC 01

TABLE L (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

180. 100. CPXRF 78VIS 01 190. 10. FAA 79WAR 01 200. 20. D* DCP 81REE 01 200. 20. DCP 79REE 01

210. 31. ITNA 74MCC 01 210. 40. ITNA 7 9 WAR 01 210. 30. ITNA 78MCC 01 210. 70. RTNA 7 9 WAR 02

210. 2. 11 RTNA 78MCC 01 280. 200. ITNA 79SAT 01 400. 500. 11 ICPES 82 JON 01 400. 500. 11 ICPES 82 JON 01 490. 17 UU 74MAS 01 500. 3500. R* ITNA 73NAD 01

540. 17 UU 74MAS 01 600. ITNA 79KUC 01 870. 60. CHEML 74LI 01 1000. 600. *11 RTNA 7oSTE 01 1160. 600. ITNA 76STE 01 1300. *17 UU 7AMAS 01 1400. 800. *11 RTNA 7fcCTF fit 1570. *17 HIT u u

7 A MA C fll 1600. 800. *11 OTV A /Dole. Ul

1700. 900. *11 BTU A /OolCi Ul 1900. 1000. *11 K1MA / DO IE U

1

2400. 700. 77UTT O*? 61000. 3000. *11 FAA 80KUM 01

Cs (ppb)

200. L* 14 NAA 81WIL 02

11.5 1. ITNA 81KRI 01

12. ITNA 81M0L 01

13. 1. ITNA 77JUR 02

13. 1. ITNA 78BEH 01 14. 2. RTNA 7 5LIE 01 14.9 2.2 RTNA 77LIE 01 15. 2. RTNA 7QWATJ fl? 15. 17 UU 74MAS 01

16. 3. TJ. TNA inn. 7 Q c AT O 1 / 7 DAI U 1 16. 4. RTNA 76GAU 01

18. 9. ITNA 73C0R 01 19.2 17 UU 74MAS 01 24

.

* ITNA 80CRE 01 35

.

* ITNA 73NAD 01 44. *17 UU 74MAS 01 130. 30. * RTNA 77MEL 01

Cu (ppm)

6500. L* ITNA 80TOU 01

93. 12. *6 ITNA 74H0F 01 138. 18.8 * FAA 74GR0 01 146. 40. * ITNA 77ZIK 01

148. 19 . * FAA 77FUJ 01

151. 191

.

R* ITNA 79IMA 03

151. 191 . R* ITNA 79IMA 01 153. * CPXRF 78UEM 01 154. 43. * CPAA 77ZIK 01 161. 12. * RTNA 77KUS 01 167. 17 UU 74MAS 01 167. XRF 80SUZ 02

168. 8. 1 ICPES 78SUD 01

95
TABLE L (com) TABLE L (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

1

1 7H/ u • QO • R TM A OUoLU Ul

1 7 ^ l 7i / TTIT u u 7AMAQ fil

1 7 ^ 1 / J m J 1 J .7 "XL PTiV D C 7 Q TAT fl 1 / OJVL Ul

11 7/ A4 i. • C AKT OUDIL. Ul

1 7 S 1 71 / u u 7AMAQ ft 1

1 7 q L.D TTMA i inn / HnVV Ul

1 7 7 1 / / a1 Q T TM A 1 1INA oUlUU Ul ITT 177

.

1 . AA 79MCQ 01

177. 7. RTNA 77TJI 01 180. 17 UU 74MAS 01 180. 8. 1

1

ICPES 81BLA 02

180. 3. AA 73TAL 01 181

.

124. ITNA 82KIM 01 181

.

17 UU 74MAS 01

1 QO lOZ • oO . 7

7 RTNA olKUC 01

1 ft? lure d 7ftcnn n i / O jU U U i 183. 8. 35 RTNA 77GLA 01 183. 19. CPXRF 79MAN 01 183

.

o . PAA / on 1L \J l 184. 5. SSMS 77PAU 01 185. 9 1

1

ICPES 82 JON 01

1 O J . 7 DTMA r\ 1 lin 7ftrAT ft l IOC 185. 6.8 1

1

RTNA 74WES 01 185. FAA 78CAP 01

186. 2. ICPES 79MCQ 02

186. 16. EXRF 77NIE 01 186. 5.5 11 FAA 74WES 01 186. 5.5 6 CPXRF 77WIL 03

110/. ft 7 7/ K1NA o i win n i OlKUL. Ul 10/. 1 ft 7 9 ^ A A O UA»£ U 1 187

.

4. J J ICPES ft 1 RI A 0 7 187. 8. RTNA 75LIE 01 187. 8. RTNA 77LTE 01 187

.

13. ITNA 7AnnN oi 187. co TTNA 1 1PIA / or un. ul

1 fl 7 A lo/«4 15.5 A A AA 7 OMAM A 1 /7MUN Ul

188. 6. AA 79FLA 02

188. 10 . RTNA 79WAR 02

188. 9. AA 7 5HIN 01 188. 1. ICPES 79MCQ 01

188. 9.8 11 FAA 74WES 01 188. 10. ITNA 79WAR 01 188

.

3. RTNA 74HEN 01

1107ft Q • ITNA 82AKA 01 189

.

1 9 oUKIR 01

i1 oft Qy . A 1 i 1 I ICPES 82 JON 01

1 O 7 . A

** • CPXRF 81 ROB 02

189. fx TTAA r AA 01 CLE Ul 189. 11 AAA A

/ / UCH U 2 189. 9 AAA A OUIID 01

101 ft Q7. oL . 1 AA 77UCH 02

ion ioy

.

7. ICPES 78JAC 01 190. 3. FAA 7 9 WAR 01 190. 11 AA 81M0H 01 190. 24. ITNA 77HAM 01 190. 10. ICPES 79 ABE 01 190. 8. VV 80SCH 05

190. 15. ASV 81D0G 01

191. 6 NAA 72SIN 01 191

.

10.5 NAA 76GUZ 01 191. 34. XRF 77SMI 04

191. 6.2 11 RTNA 74WES 01

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

191. 11 FAA 81DAN 01 192. 4. EXRF 79GIA 01 192. 4. FAA 81 CLE 02

192. 9. 6 FAA 76LAN 01 193. 14. RTNA 77GIL 03

193. 11 FAA 81DAN 01 193. 14. NAA 77GIL 01 194. 31. AA 79LAK 01 194. 13. 6 CPXRF 77WIL 03

194. FAA 75SLA 01 194. 17 UU 74MAS 01 194. 1. AA 75ABU 01 194. 17 UU 74MAS 01 195. 10. ICPES 81KNA 01 195. 4. AA 80UCH 01 195. 3. AA 79WAR 01 195. 6 POL 72SIN 01 195. 5. RTNA 76GAU 01 195. AE+AF 79ULL 01 196. 8. CPXRF 77WIL 02

196. 9. AA 81KRI 01 196. 28. RTNA 82KTM 01 196. 9. FAA 75SME 01 196. 14.7 RTNA 79PLA 01 196. 6. 6 FAA 76LAN 01

197. 16. CPXRF 80MAE 01 197. 13. 6 POL 72SIN 01 197. 4. ITNA 79SAT 01 197. NAA 78GAN 01

198. 9. ITNA 79CHA 02

198. AA 80EVA 01 199. 12. ITNA 83GLA 01 199. 6. ITNA 80MAE 01 200. 11 AA 81M0H 01

200. 2. RTNA 79DER 01 201. ICPES 78DAH 01 201.7 7.9 RTNA 77BUO 01 204. 9. CPXRF 78VIS 01 204. ICPES 80HAA 01 205. 6 AA 72SIN 01 206. 5. RTNA 74RAV 01 207. 11 ASV 81 DAN 01 208. 11. AA 76LAN 01

208. 27. RTNA 74SCH 03

210. ICPES 78CAP 01

210. 12.5 FAA 75PIC 01 213. 17 UU 74MAS 01 216. 22. 32 CPXRF 77CR0 01 216. 11 ASV 81 DAN 01 9A1 A^ A r*"D A A LrAA /oMCG Ul

241. 54. *32 CPXRF 77CRO 01

7 A 1 O J • CPXRF 76ZEI 01 270. 90. * 14 NAA 81WIL 02

277. 14. * AA 79MAT 02

394. 3. * AA 81UCH 01

(ppb)

2.4 0.8 RTNA 76GAU 01

96
TABLE L (cont) TABLE L (cont)

ANAL REF REF ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

ZD / . ITNA 78CAP 01 Er (ppb) 258.

258. 10.

7

1

1

RTNA

ICPES

81KUC 01 82 JON 01 0.5 L* RTNA 82LAU 01 259. 12. 11 ICPES 81BLA 02

0.5 L* RTNA 76GAU 01 260.9 12.89 NAA 76GUZ 01 0.5 RTNA 77LAU 02 262.

262. 7. ITNA ICPES

73NAD 01 78JAC 01 Eu (ppb) 262.

262.

13.

10. ICPES

FAA

79ABE 01

81 CLE 01 0.235 0.024 RTNA 76GAU 01 26 3. 12. CPXRF 81R0B 02

0.35 RTNA 77LAU 02 264. 3. 11 ICPES 82 JON 01 0.35 RTNA 82LAU 01 264. 29

.

ITNA 78BEH 01

i3

.

ITNA 78CAP 01 9A A ZD 4 . £O • 1

1

ICPES ozJON 01

i /. rt 140. ITNA 80CRE 01 1£ c ZD D . 19

.

ITNA ft i Trn t r\ i 81KRI 01 310. * ITNA 73NAD 01 265.

1£ C ZD D .

5. 11. GC

RTNA

81BLA 01

7 9 WAR 02

F (ppb) 265.

26 5.

25.

16

.

NAA

ITNA

78GAN 01 74WES 01

1 c rtrtrtrt 350000. 14NAA 81WIL 01 265. 30. ITNA 79CHA 02

A rt 40

.

20. ISE 83KNA 01 266. 9. ICPES 80SCH 05

120. ISE 83GLA 01 266.

266.

10.

10.

1111 AA

AA

74WES 01 78G0R 01 Fe (ppm) 266.

267.

5.

5.

11 ICPES

EXRF

81BLA 02

79GIA 01 110. 5. * AA 7 5HIN 01 268. 24. EXRF 77NIE 01 132. *17 UU 74MAS 01 268. 38. VV 79LAK 01 137. 5. * 14NAA 81WIL 01 268

.

25

.

1 ICPES 78SUD 01 155. 49

.

*1 1 AA 78G0R 01 ZD 7 . 10

.

ICPES 81KNA 01 186. 37

.

* AA 79MAN 0

1

LI u. T rtulT C 7 QT1AU rt 1 ZUD

.

CPXRF 78UEM 01 270. 47 T TH A 7 AT\AM rt 1 209

.

7ft * 1111 ICPES 82 JON 01 tVI \J •

1 9 1 Z . TTMA 7 1 /YlD rt 1 220 16 - RTNA 7 rt 1 / 7MEL u

1

97n 9ft. zu

.

MA A 7 7f Tl rt 1 226

.

17 UU 74MAS 01 97Z/U.n 1 1 1Z. COLOR 78G0R 01 229

.

1 7 UU 74MAS 01 97 1 Z / 1 • 97LI T TXT A 1 1 IN A

Q 1 V4rtl rt 1 olMUL Ul

9 Ifi 37 . FAA 77FUJ 01 97 1 ^ LI 1 .D IX .D 1AJ4 LPXRr 7 TrtT rt 1 /oJOL Ul

1 1C 5. RTNA 75LIE 01 272. 3

.

AA 82TIN 01 236

.

5. RTNA 77LIE 01 272

.

15

.

7 RTNA 81KUC 01 240. 17 UU 74MAS 01 272. 71

.

XRF 77SMI 04

240. 7. EXRF 80DYC 01 272

.

27 . RTNA 76GAU 01

240. 12. RTNA 77TJI 01 27 2

.

9.5 11 AA 74WES 01 241. 8. 1 ICPES 78SUD 01 17 1 Li 3. 9

.

FAA 81CHA 01 242. 17 UU 74MAS 01 27 3

.

8.5 6 CPXRF 77WIL 0 3 243. 14. FAA 81 CLE 02

17 1 11 3. 5

.

ITNA 80MAE 01 244. 6. ICPES 79MCQ 01 97 A Z / 4 • D . A A AA oOUCH 01 244. 2

.

ICPES 79MCQ 02 97 A ^ Z / * . D

9ft Lo .

13 A A FAA "7 Cv AT f\ I. 1 oKAT 0 4 Z44 • 10. AA 79MCQ 01 27 6. 1z

.

ii AAA A / / U<-n U l OA 7 t lui . 5 AA 79L0C 01 97 fi T7A A r AA

O Aft 16

.

CPXRF 80MAE 01 97 7 1Z . T TATA i XNA "7 A T TV f\ 1 /^LIN 01 94Q Z47 . RTNA 75STE 02 17 7 a LI 1 .9 16 .7 6 ITNA ^ / T>T7 /> rt 1 74BEC 01 ZD U . 22. ITNA 77HAM 01 17 Q Z7 8. AA 80EVA 01 250. 12. CPXRF 78VIS 01 278. 14

.

CPAA 77ZIK 01 252. 25. ICPES 81BLA 01 279. 20. RTNA 77GIL 0 3 252. ITNA 79KUC 01 280. 30. ITNA 77ZIK 01

25 3. FAA 78CAP 01 282. ICPES 80HAA 01

1 C / 254. ICPES 78CAP 01 283. 60. CPAA 78MCG 01

o ^ ZD D . 8. ITNA 79SAT 01 283. 68. CPXRF 76ZEI 01

255. 30. ITNA 78FUR 01 28 5. 17 UU 74MAS 01 255. 15. ITNA 79ZEI 01 287. 17. CPXRF 77WIL 02

256. 3. AA 801 ID 01 289. 52. 32 CPXRF 77CR0 01 256.

1 0ES 75BOL 02 290. ITNA 80CRE 01 256. 3. AA 77UCH 02 293. 8. ITNA 7 9 DAS 01 256. 32.

32

CPXRF 79MAN 01 293. 8. RTNA 80SLO 01

257. 30. CPXRF 77CR0 01

97
TABLE L (cont) TABLE L (cont)

ANAL IEF REF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

293. 17 uu 74MAS 01 ~*~"—16. 5. CVAA 80K0R 01 293. 21. 6 CPXRF 77WIL 03 16

.

7 RTNA 81KUC 01 310. 28. * RTNA 74SCH 03 16. 2. AA 79FLA 02

315. * ITNA 770SB 01 16. 2. RTNA 77TJI 01 331. *17 UU 74MAS 01 16. CVAA 7 9 TAG 01 334. 10. 14NAA 81WIL 02 16. l • RTNA 74BYR 03

350. 64. * RTNA 77KUS 01 16 .2 •>j .

11**A FAA 74CHU 03

364. *17 UU 74MAS 01 16.4 t . j NAA 76GUZ 01 1395. * AE+AF 79ULL 01 16.4 U • *4 RTNA 74HEN 01 1433. *17 UU 74MAS 01 16 .5 Ou ft

• o CVAA 72RAI 01 16.8 1 .8 5 RTNA 8 OGRE 01 VPPb) 1 / . Z • RTNA 7 9 WAR 02

1 / . 2

.

RTNA 740RV 01 20000. L* 14NAA 81WIL 02 17 . 4

.

2 CVAA 79KNE 01 500. L* EXRF 79GIA 01 17.3 2.8 5 RTNA 8OGRE 01 240. L* IENA 78WAN 01 17.4 2. RTNA 82GRI 01

4. RTNA 74HEN 01 18. 3

.

RTNA 75LIT 01 1100. 700. CPXRF 77WI1 0? 18. 2. RTNA 79CHA 02

20. 2. CVAA 7 /AND 01 (ppb) 20. UU 74FEL 01 20. 17 UU 74MAS 01

1 .4 L* RTNA 76GAU 01 22. 1

,

* RTNA 75LIE 01

1 .8 RTNA BIT AIT A T 82LAU 01 22.1 6.3 *14 FAA 2.4 RTNA 77LAU 02 22.3 1.3 * RTNA 77LIE 01 30. 10. * r /ui (ppb) 41. *17 UU 74MAS 01

A 7 4. * RTNA 77MEL 01 400. L* EXRF /yciA ui zuu • z i • * ITNA 75LIT 01

(%) Ho (ppb)

6.8 0.3 TCGS 79FAI 01 0 .94 L* RTNA 76GAU 01

7. 0.1 35 TCGS 79GLA. 04 0.2 RTNA 82LAU 01 7.12 0.1 CB 80SCH 02 0.25 RTNA 77LAU 02

(ppb) I (ppb)

1

.

RTNA O \J ljL VJ <J I 180. 12. RTNA 77R00 01

7 .

3

ITNA O \J V*£\ L_j HI z uu

.

10. RTNA 79WAR 02 220. 30. ITNA 79CHA 02

14.8 RTNA 80GVA 01 246. 11. 35 RTNA 81 ALL 01 L* TTNA L I H A 249

.

12. RTNA 81STR 01 200. L* 1 1NA / 4(j Ul U 1 12. 34 RTNA 81 ALL 01 400

.

L* CPXRF 78JOL 01 270. IENA 82SAT 01 800. L* 7 Gr*T A fl1 280. NAA 79HEC 01 13.7 1 .4 14 FAA r AA 7 A put i r\ i 14. 2. 17 A A

/

y

d IU U

1

In (ppb)

14. 2

.

7QMAT C\\ 14.5 1 .7 PTMA 79 D AT n 1 1000. L* RTNA 76GAU 01 14.5 3.4 RTNA IV 1 ll ft 79i}fifl rti

/ Z 1\U U U 1 0 .05 RTNA 74RAV 01 14.5 3.4 RTNA 72R00 02 n no 0.01 RTNA 78KOB 01 14.7 RTNA 75STE 02

15

.

z

.

MPOES 81 TAN 01

4. RTNA 74SCH 03

11 JS ft a O 5.1 14 FAA 74CHU 03 0.5 0:07 * CPXRF 80MAE 01 16. 2. FAA 77GLA 03 0.63 0.11 * 14 NAA 81WIL 01

16. 1.2 FAA 72R00 01 0.667 0.066 * RTNA 74SCH 03

16. CVAA 82GLA 02 0.7 * CPXRF 78UEM 01 16. 3. CVAA 80TON 01 0.725 0.789 R* ITNA 79IMA 03

16. 3. 7 RTNA 81KUC 01 0.725 0.789 R* ITNA 79IMA 01 16. 1 .6 RTNA 79MAY 01 0.742 ITNA 78CAP 01

98
TABLE L (cont) TABLE L (cont)

UNCER COMMENT METH CODE HUM CONC UNCER COMMENT METH CODE MUM

0.753 17 UU 74MAS 01 Lu (ppb)

0 .821 17 uu 74MAS 01 0.84 0.13 32 CPXRF 77CRO 01 0.1 L* RTNA 76GAU 01 0.87 0.13 ITNA 83GLA 01 0.039 RTNA 77LAU 02

0.875 ITNA 80CRE 01 0.039 RTNA 82LAU 01 0.904 17 UU 74MAS 01 0.91 0.08 RTNA 79WAR 02 Mg (ppm)

0.92 0.028 CPXRF 81R0B 02

0.92 1 I ENA 79KUC 01 550. L* ITNA 80SL0 01 0.93 0.05 CPXRF 77WIL 02 290. 40. * 14 NAA 81WIL 01 0.93 0.11 EXRF 77NIE 01 332

.

541

.

R* ITNA 79IMA 01

0 .935 ITNA 82AKA 01 3 32. 541. R* ITNA 79IMA 03

0 .94 0.05 ITNA 80MAE 01 516

.

*17 UU 74MAS 01 0 .948 17 UU 74MAS 01 517. *17 UU 74MAS 01 0.948 17 UU 74MAS 01 555. 21. 1 ICPES 78SUD 01 0.95 0.05 CPXRF 80KIR 01 566. FAA 78CAP 01 0.96 ITNA 73NAD 01 566. 10. AA 79MCQ 01 0.96 ITNA 79KUC 01 567. AA 79L0C 01 0.96 0.06 AA 74WES 01 573. 4. ICPES 79MCQ 02

0.964 CPXRF 76ZEI 01 573. 17 . ICPES 79MCQ 01 0.964 0.004 CPAA 78MCG 01 580. 20. CPXRF 80KIR 01 0.969 0.022 FE 80UCH 01 590. 40. ICPES 79 ABE 01 0.969 0.091 PAA 76KAT 04 593. 10. 1 AA 77UCH 02

0.969 0.078 ITNA 74D0N 01 593. 10. AA 80IID 01 0.969 0.09 ITNA 79CHA 02 595. 6. 6 AA 76H0W 01 0.97 0.05 11 ICPES 82 JON 01 596.5 13.5 PAA 76KAT 04

0.98 17 UU 74MAS 01 597. 10. AA 75HIN 01 0.98 0.1 ITNA 82EHM 01 598. 50. ITNA 77ZIK 01 0.987 17 UU 74MAS 01 598. 14. ITNA 75PIE 01 0.99 0.02 11 ICPES 82 JON 01 600. 9. 1 AA 77UCH 02 0.992 0.022 AA 75HIN 01 601. 6. 6 AA 76HOW 01 0.998 0.064 NAA 76GUZ 01 602. 11. AA 80UCH 01

1. ITNA 770SB 01 604.6 26.84 NAA 76GUZ 01

1. 0.03 TCGS 79FAI 01 605. 32. AA 74WES 01 1.006 1 AA 78SZY 01 608. 6. RTNA 79WAR 02 1.01 0.18 ITNA 77HAM 01 608. 6. ITNA 79WAR 01

1 .015 1 AA 78SZY 01 609. AE+AF 79ULL 01 1.02 0.012 ITNA 78FUR 01 610. 15. FAA 79WAR 01

1 .021 0.048 34 CPXRF 78J0L 01 613. ICPES 78CAP 01

1 .032 0.025 RTNA 75LIE 01 620. 20. ITNA 79CHA 02 1.032 0.025 RTNA 77LIE 01 636. ICPES 78DAH 01 1.04 0.03 ITNA 74WES 01 657. 9. 11 ICPES 82 JON 01 1.06 35 ITNA 81GLA 04 659. 82. ITNA 74WES 01 1.06 0.08 NAA 78GAN 01 660. 20. 11 ICPES 82 JON 01 1.087 0.124 CPXRF 79MAN 01 668. 42. AA 79LAK 01

1 .12 0.02 ITNA 80SLO 01 674. 17 UU 74MAS 01

1 13 004 EXRF 80DYC 01 684. 110. ITNA 78FUR 01 1.18 0.1 * 14 NAA 81WIL 02 700.

700.

20

.

130.

14 NAA

ITNA 81WIL 02

77HAM 01 (ppb) 712. 98. *1 ICPES 78SUD 01 949. ITNA 78CAP 01

10. 1. RTNA 74HEN 01 1040. * ITNA 73NAD 01

12. 9. RTNA 74SCH 03

14. 5. RTNA 80SL0 01 Mn (ppm)

17. RTNA 82LAU 01

17. RTNA 77LAU 02 5.3 0.72 *6 ITNA 74H0F 01 17. RTNA 75LIE 01 8. 1. * CPXRF 80MAE 01 17.3 0.4 RTNA 77LIE 01 8.4 2.1 CPXRF 80KIR 01 20. ITNA 73NAD 01 8.73 FAA 77SHE 02 24.5 1.2 * RTNA 76GAU 01 9. 0.37 FAA 74GR0 01 62. 5. * ITNA 79CHA 02 9. 0.7 VV 80SCH 05

70. * ITNA 78CAP 01 9. 2.2 6 CPXRF 77WIL 03

72. * ITNA 80CRE 01 9.12

9.14

17 UU

ITNA

74MAS 01 73NAD 01

99
TABLE L (cont) TABLE L (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

9.2 0.9 1

ICPES 81BLA 02

9.2 0.7 AA 79FLA 02

1 .8 6 CPXRF 77WTL 03

Q OA UtOj DTHA I\ 1 INrt 7QPT A 01

ft 1 9 .T TH A on a v A n l 9.4 1 .

p vd p LXKr /7Vj 1A U 1 9.42 1

-7 I / ITU u u

"7 /. MA C A 1 n 7 1 1 1 1 O 1 DLi/\ U C. 0\j • jS ITNA R2KIM 01 9.5 1 .4 CPXRF 77WIL 02

9.5 17 UU 74MAS 01 9.6 0.5 RTNA 7 7KUS 01

9.6 0.4 RTNA 74HEN 01 9.6 0.6 11 FAA 74WES 01 9.7 ICPES 78CAP 01

9.7 0.8 11 ICPES 82 JON 01 9.7 0.3 1 ICPES 78SUD 01

9.77 0.79 ITNA 74D0N 01 9.8 1 .

FAA 82GR0 01 9.9 ICPES 78DAH 01 9.9 17 UU 74MAS 01

9 -9 0.47 ITNA 74WES 01

1 0 35 ITNA 81GLA 04

102. EXRF 80DYC 01 10. 1

ICPES 79MCQ 01 10. 11 AA 81M0H 01

10. 0.5 NAA 78GAN 01

10. FAA 75SLA 01 10. 1. ICPES 79MCQ 02

10. 5. AA 76LAN 01

10. 0.7 ITNA 7 9 WAR 01 10. 1.3 ICPES 7 9 ABE 01

10

0.7 RTNA 79WAR 02

10

0.6 6 ITNA 74H0F 01 10.1 1 .2 CPXRF 81R0B 02

10.1 0.2 ITNA 80SLO 01

10 .

1 .

ITNA 79SAT 01

10 .0.1 AA 82 CLE 01

i1U<n i1 3 ft EXRF 77NIE 01 10.1 0.5 1

RTNA 74WES 01 10.15 2.15 PAA 76KAT 04

10.17 0.69 NAA 76GUZ 01 10.2 0.1 AA 80IID 01

10.2 ASV 80CHR 01 10.2 1. 1 AA 77UCH 02

10.2 0.2 AA 75HIN 01 10.2 17 UU 74MAS 01 10.2 0.45 11 RTNA 74WES 01 10.2 17 UU 74MAS 01 10.23 0.43 RTNA 74RAV 01 10.3 0.3 FAA 82CLE 01 10.3 0.3 FAA 81 CLE 02

10.3 0.2 ITNA 82EHM 01 10.3 0.77 ITNA 77RAM 01 10.3 0.8 RTNA 76GAU 01 10.3 0.36 11 FAA 74WES 01 10.4 AA 82 CLE 01 10.4 0.3 1 AA 77UCH 02

10.4 0.4 11 ICPES 82 JON 01

10.4 0.2 FAA 82CLE 01 10.4 0.4 RTNA 77BU0 01

10.4 0.6 11 FAA 75SME 01

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

10.4 FAA 78CAP 01 10.4 1.1 RTNA 74SCH 03

10.4 0.23 FAA 7 5PIC 01 10.5 0.6 ITNA OJU Lift U 1 10.5 0.3 11 ICPES 82 JON 01 10.5 1.1 ITNA 79CHA 02

10.5 16. 6 FAA 7 6LAN 01 10.6 0.7 FAA 81 CLE 01 10.6 1.1 ITNA 78FUR 01 10.7 0.3 ITNA 80MAE 01 10.8 0.8 FAA 7 9 WAR 01 10.8 0.3 RTNA 82KIM 01 10.8 20. 6 FAA 76LAN 01

10.9 2. XRF 7 7 SMI 04

10.9 1 .2 CPXRF 79MAN 01

10.9 1.5 34 CPXRF 78J0L 01

11. 11 AA 81M0H 01

11. 17 UU 74MAS 01 11. 0.4 fli rHA

11. A A OUCiVft U 1 11.2 0.5 PTMA 7 51 TP U 1

1 1.2 0.5 PTMA 77T TV fi 1 11.2 1.4 1 ICPES 78SUD 0

11.4 0.8 11 FAA 75SME 01 11.5 ITNA 78CAP 01

11.5 13.7 R* ITNA 79IMA 03

11.5 17 UU 74MAS 01

1 1 .5 13.7 R* ITNA 79 IMA 01 11.7 0.7 MD FAA 79WES 01 12.5 2. D* DCP 81REE 01 12.5 2. * 7 OTJTTTT U

1 3

3

* ITNA 77ZIK 01

13. 6. * TCGS 79FAI 01

i j • AE+AF 79ULL 01

14. 1

* AA 79MCQ 01

14.2 1.8 * FAA 77FUJ 01

19. 9. * CPXRF 78VIS 01 19. XRF 80SUZ 02

(ppm)

5L* ICPES 78CAP 01

510. L* ITNA 80TOU 01

2. * ICPES 79MCQ 02

2. 1. * CPAA 77ZIK 01

2.2 0.9 CPXRF 80KIR 01 2.5 17 UU 74MAS 01 2.5 0.1 ITNA 78FUR 01

2.6 0.4 14 NAA 81WIL 01

2.8 17 UU 74MAS 01 2.95 0.27 RTNA 76GAU 01

2.97 17 UU 74MAS 01

3. 0.3 RTNA 77GIL 03

3. ITNA 73NAD 01

3. 0.3 NAA 77GIL 01

3.04 0.18 IENA 75MAZ 01 3.06 0.7 34 CPXRF 78J0L 01

3.1 0.5 11 ICPES 82 JON 01

3.1 0.03 RTNA 80KUL 01

3.1 1 IENA 79KUC 01 3.1 FAA 79BEN 01 3.12 0.26 RTNA 78NAD 01

3.19 0.14 RTNA 77LIE 01

100
TABLE L (cont) TABLE L (cont)

ANAL KEF REF CONC UNCER COMMENT METH CODE MUM

3.19 0.14 RTNA 75LIE 01 3.2 0.1 RTNA 77DIK 01

3.2 ITNA 79KUC 01 3.23 0.09 SSMS 77PAU 01

3.3 0.3 11 RTNA 74WES 01 3.3 0.2 RTNA 79WAR 02

3.33 RTNA 75STE 02

3.4 0.2 7 RTNA 81KUC 01 3.4 0.7 5 ITNA 80TOU 01

3.4 0.1 11 ICPES 82 JON 01

3.4 0.36 RTNA 82BYR 01 3.4 0.2 RTNA 80SLO 01 3.4 1 IENA 79KUC 01 3.4 0.15 FAA 74WES 01 3.42 0.11 1

1

RTNA 81C0R 01 3.5 0.2 1 j RTNA 74WES 01

3 S 1 .5 CPXRF 77WIL 02

3.5 0.6 CPXRF 77RTN 01 3.6 0.7 RTNA 74SCH 03

3.6 0.9 CPXRF 80MAE 01 3.6 0.14 11 RTNA 81COR 01 3.7 0.4 14NAA 81WIL 02

3.71 0.25 RTNA 77TJI 01 3.78 0.356 NAA 76GUZ 01

3 .8 7 RTNA olKUC Ul

3.8 ICPES 80HAA 01

/. 1 u .4 "7 QirT c n 1 /OVlb Ul

4.3 1.2 * ITNA 79ZEI 01 4.9 *17 UU 74MAS 01 5.8 0.3 * AA 7 9 FLA 02

N (%)

10.35 0.3 TCGS 79FAI 01 10.4 0.8 35 TCGS 79GLA 04

10.42 0.11 CB 80SCH 02

10.59 0.04 GRAV 74CAR 01 10.59 0.04 D* GRAV 74CAR 05

10.81 0.24 D* NT 74CAR 05

10.82 0.24 NT 74CAR 01

Na (ppm)

1019. *17 UU 74MAS 01 1152. 119. *6 ITNA 74H0F 01 1600. 100. * 14 NAA 81WIL 01 1940. 30. ITNA 80SLO 01 1980. 60. ITNA 78FUR 01 2000. 150. 14NAA 81WIL 02

2000. 500. CPXRF 80KIR 01 2040. ITNA 80CRE 01 2176. 77. 6 ITNA 74H0F 01 2220. 17 UU 74MAS 01 2227. 200. ITNA 77ZIK 01 2230. 210. ITNA 77HAM 01 2250. ITNA 83G1A 01 2250. 17 UU 74MAS 01 2260. 370. ITNA 77JUR 02

2280. 1 IENA 79KUC 01 2280. 300. ITNA 82SCH 05

2300. 2850. R* ITNA 7 9 IMA 03

2300. 2850. R* ITNA 79IMA 01

ANAL REF REF CONC ONCER COMMENT METH CODE NUM

2310. ITNA 79KUC 01 2320. 300. ICPES 7 9 ABE 01 2320. 40. AA 75HIN 01 2330. 60. ITNA 74WES 01 2340. 17 UU 74MAS 01 2355. ITNA 82AKA 01 2370. 40. PAA 76KAT 04

2370. 17 UU 74MAS 01 2400. ITNA 7 3 NAD 01

2400. 200. AA 74WES 01 2400. 35 ITNA 81GLA 03

2410. 10. RTNA 74HEN 01 2420. 50. FE 8 OUCH 01

2425. 17 UU 74MAS 01 2426. 130. ITNA 74DON 01 2430. 150. ITNA 79CHA 02

24 38. ITNA 78CAP 01

2440. 160. RTNA 7 9WAR 02

2455. 1 AA 78SZY 01

2530. 120. NAA 78GAN 01

2540. 1 AA 78SZY 01

2550. 35 ITNA 81GLA 04

2550. 190. ITNA 78BEH 01 2570. 1 IENA 79KUC 01 2570. 17 UU 74MAS 01 2609. 142. NAA 76GUZ 01

26 32. 29. RTNA 77LIE 01 2632. 29. RTNA 75LIE 01

2768. 156. RTNA 74SCH 03

3 100

.

ITNA 770SB 01 3100. 600. * TCGS 79FAI 01

(ppb)

9. RTNA 82LAU 01

14.5 RTNA 77LAU 02

170. 40. RTNA 76GAU 01

(.ppb)

9000. L* 14 NAA 81WIL 01 500. L* EXRF 77NIE 01 60. L* ICPES 82JON 01 720. L* RTNA 81KUC 01 1000. L* RTNA 77MEL 01

500. L* ITNA 75PIE 01 60. L* ICPES 82 JON 01

800. L* EXRF 79GIA 01 500. L* NAA 76GUZ 01 500. L* ICPES 79ABE 01 700. L* RTNA 76GAU 01

50. AA 78EVA 01 62. 18. IENA 75MAZ 01 70. 30. AA 7 9 FLA 02

155. 19. FAA 80DOR 01 180. 20. PAA 79CHA 02

200. 30. RTNA 79WAR 02

210. ITNA 73NAD 01

227. VOLT 81PIH 01 270. 120. RTNA 77TJI 01

470. *7 RTNA 81KUC 01 600. 400. * CPXRF 78VIS 01 700. 500. * CPXRF 77WIL 02
TABLE L (cont) TABLE L (cont)

CONC UNCER COMMENT

ANAL

METH

REF REF CODE NUM

1000690

* AA 79MON 01 1000. 500. * RTNA 80SLO 01 1200. 100. * EXRF 80DYC 01 1300. 200. it CPXRF 79REN 02

a. i i U • j 1 U . 1 * PT5V D 1? 7QDUM no

0 .64 0 .06 1 A M A A 14NAA Q 1 T.TTT ("1 1 81W1L Ul

0.816 0.64 A EXRF 77NIE 01 0.905 NAA 78GAN 01 0.98 ICPES 78CAP 01

0.989 0.046 1 ICPES 78SUD 01

1

0.026 1 ICPES 78SUD 01

1 .OA 0.06 6 FAA 81LAN 01

1 .1 0.006 COLOR 79MCQ 01

1.1 0.02 6 FAA 81LAN 01 1.1 0.15 14 NAA 81WIL 02

1 .13 0.03 ICPES 79MCQ 01

1 .16 0.03 ICPES 7 9ABE 01

1.18 0.03 11 ICPES 82 JON 01

1.21 0.01 11 ICPES 82 JON 01

1 i 1.3 A 1 0.1 LrX Kx (5 UK. IK Ul

1 .349 0.029 NAA 76GUZ 01

(ppb)

11000. L* 14 NAA 81WIL 02

1000. L* EXRF 77NIE 01 500. L* AA 79M0N 01 3500. L* ICPES 78CAP 01

1000. L* EXRF 79GIA 01 500. L* ICPES / y ABh, U

240

o a 8U

r AA / / r U J U

250. A A /OCVA Ul

n£ o Zo I .

1 7 Till u u

7 A MAC n. 1 / tPlAo U 1 ion Z8U

4U • AAA A on apt* n 1 OUftuCi Ul

1 AA 300. /. a40f A A p AA 7 OPDrt A

/ oOKU U

300. o aa l i 1 I ICPES oZJUN Ul

300. 100. CPXRF 78VIS 01 300. FAA 79YAS 01 320. 13. FAA 75PIC 01 320. 60. FAA 7 9 WAR 01 328. 16. 11 IDMS 74CHO 02

330. 10. FAA 80POL 01 330. 700. AA 76LAN 01 330. AA 77FRI 01 330. 10

FAA 79DAB 02

333. 671 1 IDMS 74CHO 02

340. 1 1 FAA 81 DAN 01 340. 40. FAA 76HAD 01 340. 20

AA 79FLA 02

343. 23. AA 76ZAN 02

343. 23

FAA 7oKOI Ul 350. 50. FAA 81KNA 01 350. 50. AA 80SCH 05

350. 40. AA 79WAR 01 350. 15

FAA 81CHA 01 350. 50. FAA 75BEH 01 350. 22000. 6 FAA 76LAN 01 360. 25. 6 POL 72SIN 01 360. 30. SSMS 77PAU 01

360. 30. FAA 79ST0 01

ANAL REF RET CONC UNCER COMMENT METH CODE NUM

360. 11 FAA 81DAN 01 360- 12000- 6 FAA 76LAN 01 370. ASV 82GAJ 01

380. ICPES 80HAA 01 380. FAA 82VAN 01

380. 76. ASV 79ST0 01

JO uAO V 7 imp n 1

ift JO nu > TTA A r AA Q 7 UnT7 n 1 U

1Q f\ c

0 POL 7 2 SIN 01 inn 390. 1

ASV 81 DAN 01

10 n

1ASV 8 1DAN 0

Ann JU • D A A r AA 7 0 a n i OZ

400. 300. 1

Trppc ft 9 TON n, 1 400. 100. PAA 74LUT n 1 420. 140. 34 CPXRF 78J0L 0

450. 30. FAA ROT FG 0

460. 130. FAA 74GR0 01 490. 6 FAA 81HIN 01 490. 6 FAA 82K0I 01 500. *6 FAA 81HIN 01 500. * 0ES 7 5B0L 02

DUU • *0 1? A Ap AA O 1 VAT 8ZK.U1 n 1 U 1 5ZU . -'-17 "1/ nil UU 7 A MA C

/ 4MAa A 1 Ul 3900. 1000. * CPXRF 77WIL 02

5000. * 14NAA 81WIL 01

43000. 4000. FAA 79WES 01

3. L* RTNA 82LAU 01

4. RTNA 77LAU 02

4.6 0.3 RTNA 76GAU 01

(ppm)

9 Q 11 ft . D * ftnMAF n 1 ID . O

z

1 /. M A A 14NAA O 1 1JT1 81W1L A O uz

15 . 2 .5 * O / *34 /iT>tf r> CPXRF 78JOL 01

15 .

A / 4.4 XRF 7 7 SMI 04

lb . D

1 i

1 mi cD ITNA 8UTOU A 1 0 1 Id .0 1 O Z .8 DTXl A R1NA 7 A eni A 1 U J

1 A 7 ID . / 1 1 j • zft 1 Pfift nouz

16 .8 11.79 g CPXRF 77WIL 0 3 16 .8 1 I ENA 79KUC 01

16 .9 ITNA 79KUC 01

17 . 1 . EXRF 80DYC 01

17 . 3. ITNA 77ZIK 01

17 .4 1.8 NAA 78GAN 01

17 .72 1 .8 ITNA 81M0L 01

17 .8 ITNA 78CAP 0

17 Q 7 u . 0 DTWA 7 TV nu 11 1/ .97 n £ 0.6 RTNA 7 7T T17 / /LIE 01

1n 0 0.8 ITNA 79 SAT A 1 Ul

1 018 . 1 . OPXRr 7 7TTT T 7 /WIL A O UZ

1 018 . n 1 0 .

RTNA 7 9 WAR 02

18. ITNA 770SB 01 18.1 0.6 14NAA 81 WIL 01

18.4 0.4 EXRF 79GIA 01 18.4 2. ITNA 81KRI 01

18.5 0.4 ITNA 74LIN 01

18.62 0.95 NAA 76GUZ 01 18.7 0.9 5 ITNA 80T0U 01

18.7 1. ITNA 73C0R 01

102
TABLE L (cont) TABLE L (cont) ANAL KEF HEF ANAL HEF REF CONC ' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

1ft 7 TTMA 34. * ITNA 73NAD 01

18 .7 0.5 TTNA 7/orft FTUnTO 0.1 U

50. ITNA 79KUC 01

1 R 7 1 7

1 / uu 74MAS 01 55. 9. *6 ITNA 74BEC 01 18.7 3.6 EXRF 77NIE 01 69. 24

*6 ITNA 74BEC 01

ID Q IB .8 1 .4 ITNA 79LAK 01 7n *1 I ENA 79KUC 01

18 .8 1 .3 RTNA 76GAU 01 130. 170. R* ITNA 79IMA 01

18 .95 1.65 PAA 76KAT 04 I

1 inJU . 170. R* ITNA 7 9 IMA 03

19

1 .6 ITNA 78BEH 01 Sc (ppb)

19

ITNA 80CRE 01

191 .6 ITNA 77JUR 02

1 o19 . o c i . J TTMA 77HAM Ot 1. L* RTNA 80SLO 01

1Q17 .

11 . 7 7MPT 0 1 800. L* 14 NAA 81WIL 02

19 .2 1.4 ITNA ROMAF 01 L* RTNA 75LIE 01 19.3 2.8 CPXRF 7 9 MAN 01 0.5 L* RTNA 77LIE 01 19.5 2.1 ITNA 79ZFT 01 1 1Li* RTNA 75STE 02

19.8 1.4 6 ITNA 7ARFP 01 • ITNA 78CAP 01

19.9 17 UU 74MAS 01 1I . Li" NAA 78GAN 01 20

2 .4 CrAKr o av to a i oUKIR 01 n 4 17 UU 74MAS 01 20

3

PDV D IT 701TT0 A 1 /oVIS 01 0 .6 0U.I1 RTNA 74HEN 01 20 .

TTNA L Inn 1. ITNA 73NAD 01 20.9 2.5 f, 7 7UTT A 1

/ / W1L U j

10.9 RTNA 76GAU 01

23.3 *17 uu 7AMAS 01 1.1 U.J ITNA 78BEH 01 23.4 *17 uu 74MAS 01 1.1 U.I RTNA 79WAR 02

28. A CPXRF 76ZEI 01 20. 0

A RTNA 77MEL 01

28 . 4.

*17 1TT1 u u /4MA5 01 Se (ppm)

29. * L-rAA 1 oMCG 0

S (ppm)

2

L* 14 NAA 81WIL 01

2. L* ITNA 74GUI 01

3300. 1000.

1.55 L* ITNA 80T0U 01 ai\r 7qppM n.7 / 7KE1PI uz 0.228 0.011 * FLUOR 74IHN 02

7200. 400. 7/ 7/ JUK titd mUl 0.4 0.27 * FAA Rl MFY 0

7200. 200. 70 f A T A 1 /7rAI 01 0.69 0.06 A MA A 7QrAH A 1 9500. 700. CPXRF 80KIR 01 0.75 A CAA r rtjA / 41 nil \j 1 16200. 2000. * ITNA 79CHA 02 0.774 A HAlinnA 77THN n

/ / 1 nxi u 1

Sb fDDhl

0.9 11 FAA R7VFT? Oi «LI\ 01U J 0.91

0.92 0.18 6 FLUORITNA

7RFHA 01 74BEC 01

7. T A RTNA 81KUC 01 0.92 0.04 HAA 82 SUB 01 70 ITNA 78CAP 01 0.95 0.03 HAA 78EGA 01

9

Li" RTNA olKUC 01 n q 7 0.03 ICPES 80HAA 01 50. L* 7 7P TT a 1

/ /OIL U J nu.y0 7711 FLUOR 79TAM 01 500. L* l Ana a ft 1 UTT A O 0 1 WIL U

U.70 n Q ft 0.03 DCP 81 CAR 02

4.

1. RTNA 7QMAV HI n on 0.05 ITNA 76DIK 01

4. RTNA root n m 0.70 0. 15 34 CPXRF 78JOL 01

4. RTNA 7 ST TP n 1 0.98 0.06 AA 79PAV 02

4.8 0.5 RTNA 7 7T TP O 1 0.98 0.03 74TA1, 02

4.8 1.2 DTMA Kl MA "7 O DA e AO 0.98 0.01 HAA nAn 7^PTn / or iu ni\J 1 5. HAA 79EVA 01 1 • 0.2 rpvDU Vjr Aivr ftOMAF ni 5. 2

RTNA 79H0E 01 1 • 0.1 11 HAA 82J0N 01

7. t;j . ITNA 78BEH 01 1 • 11 FAA 07VFR 03

q7 . j . RTNA 74HEN 01 1 • 0.01 ITNA 7QOAT 01

i n RTNA 78GAL 01 1 • HAA 78WEL f <J"LiLl 01V/ X 11. q RTNA 74SCH 03 1 • 17 UU 74MAS 01 ITNA 80CRE 01 1 • 0.02 FAA 76IHN 02

14

10 . T1 TNA 1 tin 7 7*7 TV A 1 * n /. CPXRF 78VIS 01

14

5

NAA 78GAN 01 0.1 RTNA 75ABU 01

15. 4. RTNA 77TJI 01 0.04 FAA 76IHN 01

16. 7. ITNA 73COR 01 1.01 0.04 ITNA 79CHA 04

16. 2. ITNA 79CHA 02 1.02 ITNA 81HAN 01 18. 17 UU 74MAS 01 1.02 0.03 RTNA 77LIE 01 22.9 17 UU 74MAS 01 1.02 0.438 5 RTNA 82TIN 01 26. 1. * RTNA 79WAR 02 1.02 ITNA 81MEY 01

103
TABLE L (cont) TABLE L (cont)

ANAL REF REF CONC ' UNCER COMMENT METH WISE HUM

1 .02 0.04 HAA 80AGE 02

1.02 0.03 9 ITNA 81SUZ 01

1 .02 0.03 RTNA 75LIE 01 1.02 17 UU 74MAS 01

1 .03 6 FAA 77SHU 01

1.03 0.09 ITNA 81M0L 01

1 .03 0.04 11 HAA 82 JON 01

1 .03 0.03 RTNA 77RAI 01

1 .03 0.03 ITNA 79RAI 01

1 .04 0.1 RTNA 80KNA 01

1 .04 0.07 ITNA 74WES 01

1 .04 FLUOR 74IHN 01

1.045 0.04 ITNA 77EGA 01 1.05 0.19 ITNA 79LAK 01

1.05 0.12 RTNA 80SLO 01

1 .05 6 FAA 7 7 SHU 01

1.05 0.05 HAA 80VIJ 01

1.053 0.051 COLOR 79SZY 02

1 .06 FAA 78CAP 01

1.06 0.11 11 RTNA 82P0L 01

1 .06 0.1 RTNA 77TJI 01

1.06 0.06 RTNA 78GAL 01

1.069 0.016 ITNA 82DAM 01

1 .07 RTNA 7 5STE 02

1 .07 0.11 ITNA 78HIR 01 1.07 0.04 GC-MS 81REA 02

1.07 0.19 RTNA 79R0S 02

1.07 0.06 5 ITNA 81SUZ 01

1.07 0.1 RTNA 79MAY 01

1 .07 0.18 RTNA 79PLA 01 1.08 0.12 ITNA 77GUI 02

1.08 0.01 ITNA 74LIN 01

1 .08 0.015 FAA 80NEV 01 1.08 0.2 FAA 79RAI 01 1.08 0.05 ASV 76AND 01

1.08 0.13 6 ITNA 74BEC 01 1.09 0.06 HAA 81HAN 01

1 .09 0.02 34 HAA 78FLA 01

1 .09 0.08 RTNA 79WAR 02

1.09 0.02 AA 79FL\ 02

1 .09 0.05 RTNA 740R7 01 1.1 0.06 11 GC 81UCH 02

1.1 0.06 FLUOR 80KCH 01 1.1 0.2 HAA 82MAY 01

1.1 0.05 11 GC 81UIH 02

1.1 0.1 GC 77PO0 01 1.1 11 FAA 82VER 03

1.1 0.02 XRF 81KNA 01 1.1 0.1 9 ITNA 80WAN 01 1.1 ITNA 80CRE 01 1.1 0.17 9 ITNA 77V0B 01 1.1 0.2 EXRF 79GIA 01

1 .1 ITNA 770SB 01 1.1 0.13 11 RTNA 82P0L 01

1.1 0.4 5 ITNA 80TOU 01

1.1 0.3 ITNA 79ZEI 01

1 .1 FAA 77YAS 01 1.1 0.17 9 ITNA 79PAV 02

1.1 0.17 9 ITNA 77V0B 01

1.1 ITNA 78CAP 01

1.107 0.15 NAA 76GUZ 01 1.11 0.08 13 ITNA 73BL0 02

1.11 0.04 SSMS 77R00 02

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

i.ii 0.05 RTNA 74BYR 03

l.u 0.02 C CMC "7 "7T5 ATT n 1 / /r AU U 1 i.ii 0.1 T TMA 1 In A 7 Q f*t\ A HO i.ii 0.06 HAA 7ATUM /ox mi f)0 u t. 1.12 0.1 ASV ft IPOS 01 1.12 0.08 RTNA 7 7ROO 02

1.12 0.08 11 PTNA l\ 1 tin. 89POT 01 1.12 0.08 RTNA 77ROO O^

1.12 0.12 6 FTr Uwvn HOP. 7 ^OT Q O 1 1.12 0.075 HAA ftlMFY 01 1.12 0.03 ASV 7 SAND 01 1.12 0.09 7 RTNA 81KUC 01 1.13 17 1TIT u u 1.13 0.09 ITNA 73COR 01

1 .133 0122 ITNA 82M0R 02

1.14 0.05 ITNA 80MAE 01 1.14 0.11 ITNA 79PAV 02

1.14 0.11 ITNA 77VOB 01 1.14 0.091 HAA 82TAM 01 1.14 0.11 ITNA 77JUR 02

1.14 0.04 T TM A 1 1NA 7 OMPT/ O 1 1.14 0.11 ITNA /oBEn Ul

1.16 CSV ft 1 HAN 01 1.17 0.06 6 FLUOR 750LS 01 1.18 0.14 RTNA 74HEN 01 1.19 0.11 13 ITNA 73BLO 02

1.2 0.1 TTNA ftOUAN O

1

1.2 1

T TTMA 7QVTTr 01 1.2 0.1 ITNA 8 1 KRT 0

1

1.2 TPPF C. ftOPAA OvIUUi 01\J X 1.2 ITNA 79KUC 01 1.2 0.16 HAA 81REA 01

1 .2 0.155 ITNA 7 7 HAM 01 1.2 7 RTNA ftivnr oi 1.2 FAA r AA 77VA<? 01

1 .2 0.2 HAriAAA Oi PHY 01 1.2 0.1 MA A 77PTT HI / /OIL U

1

1 .2 0.1 CPXRF "7 Tt.TTT AH / /WIL UZ

1.2 0.1

1

RTNA 770MI 01 1.2 0.1 RTNA 77GIL 03

1 .2 0 1 RTNA 77MEL 01

1 .204 HAA 77IHN 03

1 .22 o OA COLOR 81T0E 01

1 .23 17 UU 74MAS 01

1 .24 0.04 GC 81T0E 01

1 .26 17 UU 74MAS 01

1 .26 0.15 5 FLUOR 81SUZ 01 1.3 0.4 * RTNA 74SCH 03

1 .<* 0. 1 o\ju I U Ul 1.4 * FAA ft? Ui TL Nil UU 01KJ L

1 .4 0.5 *6 CPXRF 77WIL 03

1.7 * ITNA 73NAD 01

1.7 0.1 * ITNA 78FUR 01 7.65 0.277 5* RTNA 82TIN 01 13.376 0.926 5* RTNA 82TIN 01

(VI) (ppm)

0.3 0.07 GC 81T0E 01 0.31 0.11 COLOR 81T0E 01

104
TABLE L (cont) TABLE L (cont)

CONC

Si (ppm)

16.7

16.79

Sm (ppb)

UNCER COMMENT

Sr (ppb)

Ta (ppb)

3.

Tb (ppb)

Te (ppb)

90.

Th (ppb)

3.6.8

Ti (ppm)

0.7

0.67

1 .84

15,

1000.

6.

4.0.15

11.0.2

ANAL

METH

ITOA NAA

REF REF CODE NUM

75PIE 01 76GUZ 01

CONC UNCER COMMENT

ANAL

METH

REF REF CODE NUM

1 .7 2.

3.2

Tl (ppb)

0.2

1

.

1.

ICPES 7 9ABE 01 CPAA 77ZIK 01 14NAA 81WIL 01

48. 3. SSMS 77PAU 01

1. 0.2 RTNA 74HEN 01 1.3 0.4 RTNA 80SLO 01 Tm (ppb)

1 .6 RTNA 82LAU 01

1.6 RTNA 77LAU 02 0.3 L* RTNA 76GAU 01

1.9 0.2 RTNA 76GAU 01 0.1 RTNA 82LAU 01

2.8 * ITOA 80CRE 01 0.15 RTNA 77LAU 02

35. 24. * RTNA 74SCH 03

U (ppb)

(ppb)

20. L* ITOA 74WEA 01 240. L* RTNA 81KUC 01 2000. L* EXRF 79GIA 01 1500. L* ICPES 78CAP 01 100. L* RTNA 76GAU 01

600. L* RTNA 75LIE 01 0.99 0.25 35 DNA 80GLA 04

600. L* RTNA 77LIE 01 1 . 1.6 DNA 83GLA 01 10. HAA 79EVA 01 20. 48. R* DNA 81GLA 03

21. 3. RTNA 77BYR 01

V (ppb) 220. 180. ICPES 80HAA 01

1000. L* EXRF 79GIA 01 9000. L* 14NAA 77VAN 01

150. 20. RTNA 76GAU 01

160. ICPES 78DAH 01 160. 20. FAA 82SUZ 03

300. 60. ICPES 79ABE 01 500. 180. *34 CPXRF 78JOL 01

2000. 800. 14NAA 81WIL 02

ITOA 80CRE 01

1.6 L* RTNA 76GAU 01 0.17 RTNA 82LAU 01

0.18 RTNA 77LAU 02

2. ITOA 80CRE 01

RTNA 77DIK 01

L*

R*

L*

L*

L*

EXRF 79GIA 01 RTNA 80SL0 01 ITOA 80CRE 01

14NAA 81WIL 02

ICPES 78CAP 01 EXRF 79GIA 01

COLOR 82KIR 02

20

.

L* RTNA 7 7BUO 01 40. L* ITOA 74H0F 01 6000. L* EXRF 79GIA 01 20. L* ITOA 74H0F 01

15. 5. * COLOR 82KIR 01 33. 3. RTNA 79WAR 02

55. 1. FAA 77MYR 01 56. 7. UU 7 3STE 01 56. 17 UU 74MAS 01 58.6 1.6 RTNA 78BYR 01 59. NAA 80K0S 02

60. 5. RTNA 79CHA 02

60. ICPES 80HAA 01

61 .5 2. RTNA 79COR 01 61.5 2. RTNA 81C0R 02

65. 2. RTNA 82BYR 01 66.2 4.9 RTNA 78ALL 04

90. 60. *11 ICPES 82 JON 01 320. 80. * RTNA 77GUI 03

460. * ITOA 78CAP 01

500. 100. * ITNA 77ZIK 01 600. 100. * ICPES 7 9 ABE 01

(ppb)

5. 3. RTNA 74SCH 03

5. 17 UU 74MAS 01

12. RTNA 76GAU 01

15. RTNA 75STE 02

30. 17 UU 74MAS 01 700. 100. * RTNA 80SLO 01

(ppm)

14. L* 14NAA 81WIL 01

1. L* EXRF 79GIA 01

105
TABLE L (cont) TABLE L (cont)

ANAL UF REF ANAL REF REF CONC UNCER COMMENT METH

' CODE NUM CONC ' UNCER COMMENT METH CODE NUM —

126

FAA 75SLA 01

(ppb) 126.

126 .

4.

4. 7

FAA

AA

74TAL 01

73TAL 01 0.28 RTNA 82LAU 01 127. 9. ITNA 81KRI 01 0.285 RTNA 77LAU 02 127. 11 FAA ft 1 T) AN 01 0.48 0.09 RTNA 76GAU 01 127. 1 I ENA 79KIJC 01 830. * ITNA 73NAD 01 127.

127.

1.8. 11 RTNA

RTNA

80SL0 01 74WES 01 (ppm) 127.

127.9

4.9.1 6 AA

ITNA 80UCH 01 74BEC 01 12000. L* ITNA 80TOU 01 128. 7 RTNA 81KUC 01 13.17 17.59 * AA 79MON 01 128. 14

CPAA 77ZIK 01

32. * ASV 74COP 01 128

5. ITNA 79SAT 01 65. 15. it FAA 77FUJ 01 128. 10. CPXRF 80KIR 01 78. o c ZD . £ 14NAA O 1 T ITT i*\ 1 81WIL 01 128. 7. RTNA 79DER 01 98. 122. R* ITNA 7 9 IMA 01 128. 14

EXRF 77NIE 01 98. 122

R* ITNA 7 9 IMA 03 128. 3.6 1

AA 74WES 01 101

*17 UU 74MAS 01 128. 3. FAA 81 CLE 01 104. CPXRF 78UEM 01 128'. 12. ITNA 79CHA 02

112. XRF 80SUZ 02 128. 6. AA 75HIN 01 112. 15

ICPES O 1 T» T A f\ 1 81BLA 01 128. DCP 78NAK 01

1 12.6 1.1 FAA 81 CLE 02 128.6 0.7 ITNA 82DAM 01

1 16. ITNA 73NAD 01 128.6 AA 79LOC 01 116. 18. CPXRF 80MAE 01 129. ICPES 80HAA 01 117. 13. AA 7 9 MAN 01 129. 3. ITNA 74D0N 01 118. 4. 6 POL 72SIN 01 129. 16. 32 CPXRF 77CR0 01

1 181

ASV 81 DAN 01 129. ITNA 80CRE 01 110 1 IB . 1 1

RTNA 8ZKIM 01 129. 1 IENA 79KUC 01

I in o

1 lo .2 7 O

/ .0 I ENA 75MAZ 01 1 oo I Z7 . A ITNA 79WAR 01 117. £D 70 CT M O 1 129. 4

RTNA 79WAR 02

ll onzu

O .

1 1 1

Q i ht a no ollSLA UZ i on 1 JO . i i AA 81M0H 01

i on 1 ZU •

1 71/ UU /4MAS 01 i on ** • X i ICPES 81BLA 02

ill n 1Z1 .9 RTNA 74RAV 01 i on 1 JO. cD •

il ICPES 78SUD 01 122. 3. NAA 78GAN 01 130. 0ES 75B0L 02

122. 9. ITNA 79LAK 01 130. 7. CPXRF 78VIS 01 122. 3. EXRF 80DYC 01 131. 1 .4 AA 80AGE 01 122. 11 FAA 81DAN 01 131. 13.5 PAA 76KAT 04

123. 5. ITNA 74WES 01 131. 2. ICPES 79MCQ 01

123. 25. ITNA 78FUR 01 131. 17 UU 74MAS 01 123.8 1.2 FAA 74GRO 01 131. 1. ICPES 79MCQ 02

124. 6 POL 72SIN 01 131. 1. AA 75ABU 01

124. 10. ICPES 80SCH 05 131. 1AA 75EPS 01

124. 14

CPXRF 79MAN 01 131 .8 6.5 ITNA 73C0R 01 124. ITNA /oLAP 01 132. 3.3 6 CPXRF 77WIL 03

i o a

1 lh

1/ 1711 UU 7AMAC ni 132. 5. AA 79MCQ 01

1 OA 7 r aa 7 AT AT 01 132. 6. 7 RTNA 81KUC 01

1 O A 1 Z4 . 7

/ . 7 A A AA 71TAT n 1 / 1 1AL U 1 132. 7. AA RnTTTT 01

11/.

1 Z4 . 7 0

/ . J

1 1 1 1 DTM A 7AUPC ni 132. 1. AI / JEtt D 01\J 1

1 24 .4 RTNA 7 cu at n 1 / 5HAL 0

132. 3. fir R 1 Rl A 01 125. 5. NAA 77GIL 01 132. 7. 1 A A 77nni o?

125. - ITNA 79KUC 01 133. 7. 1 1NA 7 7 T1TD OO 125. 5. RTNA 77GIL 03 133. 11 AO V 0

o 1 n&M O 1 I UAN U 1 125. 2. AA 7 9 FLA 02 133. 7. ITNA 78BEH 01 125. 16. ITNA 7 7 HAM 01 133. 6. ICPES 78JAC 01 125. RTNA 75STE 02 133.9 6.8 ITNA 79ZEI 01

125.7 10.6 34 CPXRF 78J0L 01 134. 2. RTNA 77MEL 01

126. 5. ITNA 81M0L 01 134. 7. 11 ICPES 82 JON 01 126. 71

ITNA 82KIM 01 134. 4. 1 AA 77UCH 02

126. 2. ITNA 80MAE 01 134. 2. EXRF 79GIA 01 126. 8. FAA 7 9WAR 01 134. 5. RTNA 77TJI 01

126. 4. SSMS 77PAU 01 134. 7.2 RTNA 79PLA 01 126. 9. RTNA 740RV 01

106
TABLE M

TABLE L (cont)

ANAL REF KEF CONC ' UNCER COMMENT METH CODE NUM

. 134. 6. 1

1

ICPES 82 JON 01 134

.

10

.

FAE 74TAL 01 134. 3. AA 7 9 WAR 01 134. 5. 7 AE+AF 73TAL 01 134. 5. FAE 74TAL 01

1 34

.

10

.

7 AE+AF 7JTAL 01

1 j4

.

1 / Tin U U 7 A MA c r\ 1

1 15 j . RTNA 77LIE 01

1i ISjj . 2

.

1 J ICPES 82 JON 01

1 35

.

ICPES 78CAP 01 135. AE+AF 79ULL 01 135. 5. RTNA 75LIE 01 135. 4. 11 ICPES 82 JON 01

1 35

.

17 UU 74MAS 01

1 IS 1

,

ITNA 74LTN 01

1 JO . co

.

RTNA

1 JO * Q DTWA ftirin 7AUT7H f| 1 lib

.

1 / TTIT UU 7 /.MAC fil 137

.

9 . 5 ITNA 8UTOU U

1

1 37 . 4

.

ITNA T / /I T it A 1 74GUI 01

1 37 .2 5.75 NAA 76GUZ 01

l .

1 7

1 / UU 7 A MA C A 1 /4MAS Ul

1 /.A

1 4 U . 1 1 A A Q 1 MT\U n 1 o 1 PUli U

1

i in TTNA J. AHA

140. ICPES 7 8DAH 0

1

140

.

1 u . RTNA 77VI1Q; 01 140. 29

.

XRF 77*?MT OA

141

.

2

.

DCP 79REE 01 141

.

£. . DPP ft 1 HFF O

1

141

.

1U . J RTNA

141 .7 5.3 g ITNA 7ABEC 01

l A 9 AAA A OUtVn Ul

14'.

.

11. ITNA 1 77TV A 1 //ZIK Ul

1 A 1 1 Q Tpnpc 7Q A TH? A1 144. 1 A A 1 L . b LrXKr 7 7LTTT (11 / / W 1L U J

11 AS** J • FAA r aa 7RPAP 01

1IAS1 j . J . Vrfr ART 77UT1 / / W ! Li 07U £ IAS S 1 ** J . J TTNA L InA O Z rtJVrt Ul

147. 7.3 11 AA 74WES 01 148. 74. CPXRF 76ZEI 01 148. 15. CPAA 78MCG 01

150. 10. PAA 76WIL 01

156. 6.2 * CPXRF 81 ROB 02

157. 20. * ICPES 78SUD 01 159. 8. * RTNA 74SCH 03

160. *17 UU 74MAS 01 160. *17 UU 74MAS 01 162. 31. *32 CPXRF 77CR0 01 200. 40. * 14 NAA 81WIL 02

(ppm)

3. L* EXRF 79GIA 01 0.5 L* 14 NAA 81WIL 02

3. L* 14 NAA 81WIL 01 3.4 0.4 PAA 79CHA 02

4. 3. CPAA 77ZIK 01

NBS SRM 1621—COLLECTED DATA

CONC

S (%)

UNCER COMMENT

ANAL

METH

KEF REF CODE NUM

0.9

0.99

1 .05 1.06

0.1 0.03

0.03

MECA

ICTITR

XRF

80MCC 01 80MCC 01 80MCC 01 80MCC 01

TABLE N

NBS SRM 1621A—COLLECTED DATA

CONC UNCER COMMENT

ANAL

METH

REF REF CODE NUM

s (%)

0.89 0.07

0.93 0.02

0.931 0.01

0.945 0.014

0.97 0.009

0.973 0.008

66

TABLE O

POL

ICPES

ICTITR

EXRF

EXRF

81REL 01 81WAL 02

82VIS 01 82VIS 01 81CHR 01 81CHR 01

NBS SRM 1622A—COLLECTED DATA

CONC

s (%)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

1.6 1.948

2.011

2.02

0.1

0.018

0.015

0.02

POL 81REL 01 EXRF 81CHR 01 EXRF 81CHR 01 ICPES 81WAL 02

TABLE P

NBS SRM 1623—COLLECTED DATA

CONC

S (ppm)

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

2600.

2650.

2700.

2900.

200.

40.

500.

MECA

ICXRF TITR

80MCC 01 80MCC 01 80MCC 01 80MCC 01

107
TABLE Q

NBS SRM 1624—COLLECTED DTA

CONC

S (ppm)

1900. 20 30. 2080.

2200.

UNCER

100.

50. 210. 200.

ANAL COMMENT METH

REF REF CODE NUM

ICPES 81WAL 02 TITR 82VIS 01 IC 82VIS 01 POL 81REL 01

TABLE R

NBS SRM 1630—COLLECTED DATA

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

Al (ppm)

5300.

As (ppm)

19.

Ash (%)

2.2

B (ppm)

5.

Be (ppm)

Br (ppm)

29.

37.

Ca (ppm)

700.

Cd (ppm)

CI (ppm)

2220.

Co (ppm)

3.6

6.

Cr (ppm)

7.1

8.

VV 77GLU 01

VV 77GLU 01

CB 77GLU 01

VV 7 7GLU 01

VV 7 7GLU 01

VV 7 7GLU 01 ITNA 74TAM 01

VV 7 7GLU 01

0.2 L* VV 77GLU 01

VV 7 7GLU 01

0.18

0.35

ITNA 74TAM 01 VV 7 7GLU 01

ITNA 74TAM 01 VV 77GLU 01

CONC

Cu (ppm)

16.

F (ppm)

25.

Fe (%)

UNCER

TABLE R (cont)

ANAL REF REF COMMENT METH CODE NUM

0.51

1 .04

Ga (ppm)

1.07

1.1

Ge (ppm)

1

.

H20- (X)

0.4

Hg (ppb)

104.

105.

105.

106. 118. 120.

124.

125.

127 . 127.

127.

130.

130.

135. 136.

139.

139. 140.

150. 486.

K (ppm)

800.

La (ppm)

4.4

Mg (ppm)

200.

0.02

0.04

30.

11.

10.

11. 10.

6.

5. 12. 10.

10.

7. 12.

7.

60.

VV

VV

ITNA VV

RTNA W

VV

GRAV

CVAA RTNA

RTNA

ITNA

FAE CVAA

CVAA

CVAA

RTNA

RTNA

RTNA RTNA

ITNA OES

FAA

FAA CVAA

VVCVAA

ITNA

VV

ITNA

VV

77GLU 01

7 7GLU 01

74TAM 01 77GLU 01

72SAN 01

7 7GLU 01

7 7GLU 01

77GLU 01

80NAD 01 74RIC 01 72LYO 01 74RIC 01 76CAV 01 73L0 01 82D00 01 75WIM 01 72RAI 01 740RV 01 72R00 01 75LIT 01 74TAM 01

7 5PEC 01 82UCH 02

72R00 01 72RAI 01

7 7GLU 01

75MUR 01 75LIT 01

7 7GLU 01

74TAM 01

7 7GLU 01

108
TABLE R (cont) TABLE R (com)

CONC

Mn (ppm)

6.

Mo (ppm)

2.

Na (ppm)

320.

490.

Nl (ppm)

10.

P (ppm)

17.

Pb (ppm)

4.

S (%)

1.07

1.37

Sb (ppm)

0.6

1.7

Sc (ppm)

1.4

Se (ppm)

2.2.09

2.11

2.11

2.12

2.6

Si (ppm)

7200.

Sn (ppm)

6.

Ti (ppm)

500.

V (ppm)

24.

ANAL UF REF

' UNCEK COMMENT METH CODE NUM

0.51

0.06

0.06

0.09

0.09

0.09

0.21

VV

VV

VV

ITNA

VV

W

W

CBXRF

VV

ITNA

ITNA

VV

RTNA

RTNA

RTNA

ICPES ITNA

VV

VV

VV

VV

77GLU 01

7 7GLU 01

77GLU 01

74TAM 01

77GLU 01

77GLU 01

77GLU 01

77GLU 01 77GLU 01

77GLU 01 74TAM 01

74TAM 01

7 7GLU 01

740RV 01 72ROO 03

77R00 02

80HAA 01 74TAM 01

7 7GLU 01

77GLU 01

77GLU 01

7 7GLU 01

CONC

Zn (ppm)

6.

Zr (ppm)

21.

ANAL REF REF UNCER COMMENT METH CODE NUM

W 77GLU 01

VV 77GLU 01

TABLE S

NBS SRM 1631 A—COLLECTED DATA

CONC

S (ppm)

5260.

5460.

5490.

5900.

UNCER

350.

400.

COMMENT

ANAL REF REF METH CODE NUM

TITR

IC

TITR

TCGS

80ARO 01 77SMI 05

74HIC 01 77JUR 01

TABLE T

NBS SRM 163 IB—COLLECTED DATA

CONC

S (%)

UNCER COMMENT

1.92

1.97

2.02

2.042

0.05

0.067

ANAL

METH

TITR

ICTCGS

TITR

REF CODEREF NUM

74HIC 01 77SMI 05

77JUR 01 80ARO 01

TABLE U

NBS SRM 163 IC—COLLECTED DATA

CONC

s (Z)

2.98

2.99

3.09

3.117

UNCER

0.02

0.09 7

COMMENT

ANAL

METH

TCGS TITR

ICTITR

REF REF CODE NUM

77JUR 01 74HIC 01 77SMI 05

80AR0 01

109
TABLE V

NBS SRM 1632—COLLECTED DATA TABLE V (cont)

CONC

Ag (ppb)

UNCER COMMENT

ANAL

METH

REF R£F CODE MUM

200. L* ICPES 81CHU 01 2500. *34 WXRF 82MIL 01 200. L* ITNA 77CAH 01 220. L* ITNA 82SUZ 02

140. L* ITNA 77MAE 01 400. L* PAA 76CHA 01 100. L* ITNA 75RUC 01 150. L* 0ES 76WEW 01 45. 5. RTNA 77NAD 02

60. 30. ITNA 73ABE 01 60. 30. ITNA 750ND 01 70. 34. SSMS 77PAU 01 80. AA 76WEW 01 1050. 100. * PAA 74CHA 01

(%)

1 .51 0.08 NAA 76HAN 01

1 .57 0.155 ITNA 7 3 SHE 01 1.57 4 AA 79REI 01

1 .59 0.2 ITNA 76RAG 01

1 .6 ICPES 80NAD 01

1 .6 0.2 35 ITNA 81GIA 03

1 .62 0.13 ITNA 78MAC 01

1 .64 ICPES 80NAD 01

1 .66 ICPES 80NAD 01

1 .68 0.04 D* TCGS 80AND 01

1 .68 0.04 TCGS 79FAI 01

1 .71 0.05 ITNA 77MAE 01

1 .71 0.07 ITNA 78LAU 02

1 .72 0.09 ITNA 75RIC 01 1.73 0.04 ITNA 76BLO 01 1.74 0.04 ITNA 77R0W 03

1 .74 0.4 ITNA 76STE 05

1 .76 0.31 ITNA 78NAD 02

1 .76 0.31 ITNA 75NAD 02

1 .78 0.08 ITNA 73ABE 01

1 .8 0.18 ITNA 76WEW 01

1 .82 0.06 ICPES 81CHU 01

1 .85 0.08 ITNA 79GRE 01

1 .85 ITNA 77WEA 01

1 .85 0.13 ITNA 750ND 01

1 .85 0.13 FAA 77PIL 01

1 .86 ICPES 80NAD 01

1 .9 0.19 ITNA 81WAN 01

1 .9 ITNA 75KLE 01 2.1 1 .05 * OES 76WEW 01 2.21 * ITNA 77GLU 01

3. 0.1 * ITNA 82SUZ 02

(ppm)

10. L* ICPES 81CHU 01

6. L* ICPES 80NAD 01

6. L* ICPES 80NAD 01

3- 2. EXRF 73SPA 01 4.5 0.4 * ITNA 75RIC 01 4.6 0.3 ITNA 78NAD 02

4.61 0.32 ITNA 75NAD 02

4.7 0.5 ITNA 78MAC 01

ANAL KEF KEF CONC UNCER COMMENT METH CODE NUM

4.7 1. EXRF 79GIA 01 5. 0.6 H OES 80CLA 01 5.1 0.5 ITNA 76KUC 01 5.31 ICPES 81 NAD 01 5.4 0.5 COLOR 77ARU 01

5.4 0.3 FAE 80DSI 01 5.4 0.1 I ENA 78WAN 01 5.5 ITNA 75KLE 01 5.58 0.73 FAA 82 BEN 01 5.6 FAA 78GUI 01 5.6 0.36 FAA 77ARU 01 5.6 0.2 ITNA 77ARU 01

5.7 0.2 H FAE 79FEL 01 5.7 0.5 ITNA 73ABE 01 5.7 ITNA 77WEA 01 5.7 0.13 RTNA 75RUC 01 5.7 ITNA 77GLU 01

5.7 0.2 FAA 78HAY 01 5.75 0.37 PAA 74CHA 01 5.8 0.3 ITNA 77MAE 01 5.8 0.3 ITNA 76RAG 01 5.8 0.3 PAA 77JER 01 5.8 0.5 ITNA 76BL0 01 5.8 0.4 RTNA 740RV 01 5.8 0.3 PAA 76CHA 01 5.9 0.4 ITNA 81 WAN 01 5.9 0.3 ITNA 79GRE 01 5.9 0.5 ITNA 73SHE 01

6. 0.3 ITNA 78LAU 02

6.1 0.3 GCMES 75TAL 01

6.1 0.55 ITNA 77JER 01 6.1 1.4 ITNA 750ND 01 6.1 0.4 ITNA 77R0W 04

6.2 0.8 6 PAA 82SEG 01 6.2 1.3 ITNA 77CAH 01 6.27 0.89 RTNA 77JER 01 6.3 1. 6 PAA 82SEG 01 6.3 1. PAA 80SEG 01 6.3 0.2 I ENA 77R0W 04

6.4 0.2 IENA 77ROW 03

6.5 1.4 D* NAA 740ND 01

6 .5 U.J ICPES 80HAA 01 6.5 1.2 IENA 76STE 05

NAA 76HAN 01 6.6 34 WXRF 82 MIL 01

6 .6 1 .3 ITNA 76WEW 01

7. * AA 76WEW 01

QO • oL > PAA 750ND 01 8.9 0.2 * ITNA 82SUZ 02

8.9 0.5 * ITNA ~1 C TT1 T /~* f\ 1 /5RUC 01

Ash (%)

13.2 34 CB 82MIL 01

Au (ppb)

30. L* ITNA 73ABE 01 300. L* ICPES 81CHU 01 5000. L* OES 76WEW 01

1 . ITNA 77CAH 01 20. ITNA 75RUC 01

no
TABLE V (cont) TABLE V (cont)

ANAL UF HEF CONC ' UNCER COMMENT METH vwe hum

0.85 0.03 RTNA 77NAD 02

0.99 0.16 RTNA 77NAD 01 146. 48. ITNA 73SHE 01 200. ITNA 77WEA 01

B (ppm)

29

.

ICPES 81 NAD 01

30

.

1.1 OES 76WEW 01 42.1 0.7 D* TCGS 80AND 01 42.1 0.7 TCGS 79FAI 01 43. VV 7 7GLU 01

47. 1.6 6 TCGS 76GLA 01 47.7 1.8 6 TCGS 76GLA 01

1.1 O 4/ . 7 1 .6 6 TCGS 76GLA 01 118. it ITNA 77GLU 01

Ba (ppm)

87. 5. *9 ITNA 82SUZ 02

104. 5. ITNA 82SUZ 02

183

.

ICPES 80NAD 01

ZDb . ICPES oftutn n

i

BONAD 0

1

97 A 31* TTMA 1 iNA 7 tCTI? nc

9fl n Zo u

.

T1 TWA Inn / jrii L u i o.nn T TM A 1 INA

7 ot An no /oLAU Uz omJU1

.

o A WXRF oiuti n i 3UZ . o ITNA o to a*"» n 1 / 6RAG U

1

306

.

20

.

I ENA 77R0W 04

309

.

24. ITNA 77R0W 04

310. 35 ITNA 81GLA 03

310. 30. ITNA 78MAC 01 311. 25. ITNA 78NAD 02

311. 25. ITNA 75NAD 02

314. 43. ITNA 81 WAN 01 314. 20. PAA 74CHA 01 315

.

20

.

PAA 76CHA 01

o on OA20

.

NAA 7 6 HAN 01

0 oo JZZ

.

onZl) . IENA 7 /ROW 03

j J/ . AO**Z . TTMA 1 INA / jont U

1

J JO .

1 ft TFMA 7ACTF / dd l r* UD

**A ^ 7n T TV A 1 INA / owtw ui

o^n T TM A 1 INA / / WEA U

1

left on ITNA /9GRE 01 350. 20 . ITNA 77MAE 01 352. 30. ITNA 750ND 01 354. 84

.

ITNA 79R0S 03

360. 20. 9 ITNA 78LAU 02

366. 34. ITNA 75RUC 01 385. 40. ITNA 77CAH 01 390. 20. ITNA 7 3 ABE 01 405. ITNA 75KLE 01

oooz • U Lb /owciW ui

Be vppm)

V «u/ ftc e 7 tLTCl.T A 1 / owtw UI 1.49 0.03 FLUOR 77WIC 01 1.5 0.1 FAA 750WE 01

1 .5 AA 76WEW 01 1.52 0.11 6 FAA 77GLA 02

1.57 0.12 6 FAA 77G1A 02

CONC UNCER COMMENT

ANAL

METH

HEF REF CODE NUM

7 85

Bi (ppm)

1.05

Br (ppm)

C (%)

68.93

69.6

70.

70.

73.

Ca (ppm)

2400.

2840.

4 AA 79REI 01 0 03 ICPES 81CHU 01 0.4 r AA 76GLA 02

T TM A 1 INA T "7 /IT IT f\ 1 77GLU 01

O AfcY A TV f\ 1 80NAD 01

* ICPES 80NAD 01

1

.

L* WXRF 82MIL 01

1 . L* PAA 76CHA 01

1. L* AA 76WEW 01 1.5 L* OES 76WEW 01 PAA 74CHA 01

7.8 5.8 * ITNA

14

.

2. ITNA

14 .2 ITNA

15

.

1. ITNA

15 .2 1.4 ITNA

15 .2 1.4 ITNA

1 £. O 16 .2 1. 5 IENA

16.6 0.6 NAA

17. 2. ITNA

17. 1. ITNA

17.2 ITNA

17.4 1.1 IENA

17.5 0.3 EXRF

17.9 0.3 5 IENA

18. 34 WXRF

18. 2. ITNA

18.2 2.3 ITNA

18.8 2.4 ITNA

19. 4. ITNA

19.2 0.6 ITNA

19.2 1.2 ITNA

19.3 1.9 ITNA

19.3 ITNA

19.5 0.3 IENA

19.6 0.4 IENA

19.6 0.4 D* IENA

20. 3. ITNA

20. 2. ITNA

20. ITNA

23.7 3.2 * EXRF

38. 1. * ITNA

0.11

2.1

5.

5.

3.

7000.

600.

80.

35 D*

35

L*

*

CB

CB

TCGS

TCGS

TCGS

ITNA

ITNA GAMMA

81WAN 01 76STE 05

75KLE 01 78MAC 01 78NAD 02

75NAD 02

79GLA 02

76HAN 01 73ABE 01 78LAU 02

76RAG 01

83GLA 01 79GIA 01 79GLA 02

82MIL 01 76KUC 01 75RUC 01 77CAH 01 75RIC 01 77R0W 04

77MAE 01 750ND 01 77WEA 01 76STE 05

77R0W 03

77ROW 04

7 3 SHE 01 79GRE 01 77GLU 01

7 3 SPA 01 82SUZ 02

80SCH 02

79GLA 04

80AND 01 79FAI 01 79GLA 04

78LAU 02

82SUZ 02

750ND 01

111
TABLE V (cont) TABLE V (cont)

ANAL UF REF CONC ' UNCER COMMENT METH CODE NUM

3300. 500. D* TCGS 80AND 01 3300. 500. TCGS 79FAI 01 3500. 2800. ITNA 77R0W 03

3500. 300. ITNA 76STE 05

il uu. MA A 7&14AM A. 1 4000

.

ICPES ftONAD 01

<tU JU

.

AO a 1 A XT A A 14NAA 77Tf AVT A 1 / /VAN U

1

a A7 a C C A 1 1NA 7 1 CUT? A T / J SHE Ul

4100. 400. ITNA 79GRE 01 4100. 500. ITNA 81WAN 01 4140. 140. ICPES 81CHU 01

4200. 400. PAA 76CHA 01 4200. 300. ITNA 77MAE 01 4200. 600. ITNA 76RAG 01

4200. ICPES 80NAD 01

4200. 500. ITNA 750ND 01

4300. 200. ITNA 78NAD 02

4300. 200. ITNA 75NAD 02

4400. 900. ITNA 76WEW 01 4400. ITNA 75KLE 01 4500. ICPES 8 ONAD 01

4700. 600. PAA 750ND 01

4950. 4 AA 79REI 01 jUUU • Dmun AT OUNAD 0

1

5100. 1000. OES 76WEW 01 5300. 35 ITNA 81GLA 03

7000. * ITNA 77GLU 01

Cd (ppb)

CONC

Ce (ppm)

UNCER COMMENT

ANAL REF REF METH CODE NUM

3000. L* WXRF 82 MIL 01

2100. L* ITNA 7 3 ABE 01 200. L* ICPES 81CHU 01

340. L* ITNA 82SUZ 02

400. L* ITNA 77GLU 01

170. 36. SSMS 77PAU 01

180. 20. D* TCGS 80AND 01 180. 10. AF 75EPS 01 180. 40. 6 PAA 82SEG 01

180. 20. TCGS 79FAI 01

J80. 14. AF 74RAI 01 190. POL 74MAI 01

199. 20. PAA 74CHA 01 200. 20. PAA 77JER 01 200. 100. 6 PAA 82SEG 01

200. 20. RTNA 77JER 01 200. 20. PAA 76CHA 01 200. 50. 6 TCGS 76GLA 01 210. 10. FAA 77GLU 01

210. 20. FAA 74RAI 01 230. 21. 8 SSMS 80KOP 01

230. 10. FAA 74TAL 01 230. 20. RTNA 740RV 01 230. 10. 7 AA 73TAL 01

240. 30. FAA 74TAL 01 240. 30. 7 AA 73TAL 01 250. FAA 78GUI 01

250. 70. PAA 80SEG 01

310. IDMS 75KLE 01 310. AA 76WEW 01 400. 200. * SSMS 77D0N 01 700. 350. * OES 76WEW 01

17 OA 0.089 ITNA 73SHE 01

1 o c loo ITNA 75KLE 01

18 .8 1

.

ITNA 76RAG 01

1 Q T1 . ITNA 78LAU 02

19.5 1. ITNA 750ND 01 19.5 0.7 D* ITNA 77R0W 04

19 -5 07 ITNA 77ROW 03

19.5 0.7 ITNA 77MAE 01 19.7 0.6 ITNA 78NAD 02

19.7 0.2 ITNA 76WEW 01

19 .7 0.56 ITNA 75NAD 02 ITNA 75MIL 01 20. 1 .2 PAA 76CHA 01 20 .

1

3.7 ITNA 77CAH 01

O 1 1 1

.

1

.

ITNA 79GRE 01

7 1 7 J.5 ITNA 81 WAN 01 21.5 1.7 NAA 76HAN 01

22.6 2.2 I ENA 77R0W 04

22.8 0.5 ICPES 81CHU 01 23. OES 82GUP 02

23.3 2.7 ITNA 75RUC 01 24. 34 WXRF 82 MIL 01 26. 5. ITNA 78MAC 01 29. 1. * ITNA 82SUZ 02

29. 1. *12 ITNA 82SUZ 02

30. 15. * OES 76WEW 01

CI (ppm)

80.

750.

760.

800.

810.

810.

817.

828.

844.

844.

846.

860.

866.

880.

890.

890.

890.

890.

895.

895.

915.

920.

930.

945.

945.

990.

1000.

1000.

1177.

20.

75.

50.

30. 96.

22.

37. 37. 44.

54. 40.

50.

100.

125.

15.

15.

30. 48.

35.

35. 20.

35

34

D*

ITNA ITNA

ITNA

ITNA WXRF

ITNA ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

ITNA PAA

ITNA

TCGS

TCGS

ISE

NAA

PAA

ITNA

ITNA

ITNA

ITNA

ITNA

ISE

73ABE 01

7 3 SHE 01 81GLA 03

78MAC 01

82MIL 01

82SUZ 02

81 WAN 01 76RAG 01 77ROW 03

76STE 05

75RUC 01 77CAH 01 75RIC 01 83GLA 01 77WEA 01 79GRE 01 76CHA 01 750ND 01 80AND 01

79FAI 01

81NAD 01 76HAN 01 74CHA 01 75NAD 02

78NAD 02

77MAE 01 75KLE 01

77GLU 01

80NAD 01

112
TABLE V (cont) TABLE V (cont)

ANAL KEF l£F

CONC UNCER COMMENT METH CODE NUM

Co (ppm)

3.9 0.2 * ICPES 81CHU 01

4.7 0.32 0ES 76WEW 01 4.8 0.3 ITNA 76BL0 01 4.9 ICPES 80NAD 0

1

5. 34 WXRF 82MIL a i u 1 5.1 0.6 ITNA 78NAD a *> 5.13 0.57 ITNA 75NAD 02

5.2 0.4 ITNA 73ABE a 1 01 5.3 0.4 T TM A ITNA U

1

5.4 4 AA 79REI A 1 0 1 5.46 0.2 ITNA 70DA C U J 5.48 0.15 ITNA 7 3 SHE A 1 Ul

5.5 0.3 ITNA 77CAH 01 5.5 0.4 PAA 74CHA 01 5.51 0.6 ITNA 7 6 RAG 0

1

5.58 0.21 ITNA 75RUC 01 5.6 0.4 PAA 1 cm A 76CHA A 1 01 5.7 0.1 ITNA 78LAU A 1

5.7 0.4 ITNA 750ND 01

5.7 0.12 I ENA 77ROW A / 04

5.7 ITNA / /WEA A 1 U 1 5.7 0.12 ITNA / / WJVt a a U J

C "TO 5.78 QAM An ouriAjj n\j 11 ^ ft U .0 ITNA 76WEW 01 5.9 a q A A

3 .9 TTNA ± int\ 75KLE 01

0 . n A7 T TM A 1 1INA 7 Q M A r A 1 U 1 6. 0.2 ITNA 79GRE 01 6.01 0.16 ITNA 77R0W 04

6.1 0.1 ITNA 77MAE 01 6.2 ITNA 75MIL 01 6.39 0.74 ITNA 81 WAN 01 6.5 0.2 ITNA 82SUZ 02

6.57 0.47 NAA 76HAN 01 6.9 *35 ITNA 81GLA 03

7. AA 76WEW 01 8.5 4.2 * EXRF 79GIA 01

1 1

.

* ITNA 77GLU 01

>pm)

oo •

•k EXRF A 1 01

15

.

ICPES 80NAD 0 1 lb .

1 o ic 0ES 76WEW A 1 01

1/ . 1

.

ITNA 75RIC A 1 01

17 £. 11 .b 1

.

ITNA 76RAG 01

17 .8 2

.

ITNA 77CAH 01

18

.

ICPES 80NAD 01 18.5 1.7 ITNA 78MAC 01 18.8 1.1 ITNA 76BL0 01

18.9 2.2 ITNA 78NAD 02

18.9 2.2 ITNA 75NAD 02

19. 2. ITNA 7 3ABE 01

19. 3. SSMS 77D0N 01

19. 2.8 ITNA 79ROS 03

19. 0.8 ITNA 7 3 SHE 01

19. AA 76WEW 01 19.5 0.8 PAA 76CHA 01 19.6 0.5 ITNA 77MAE 01 19.6 0.6 AA 79ROS 03

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

19 .7 0.9 D* NAA 740ND 01

19 .7 0.9 ITNA 750ND 01 19.8 FAA 78GUI 01

20. 1. 9 ITNA 78LAU 02

20. 3. ITNA 78LAU 02

20. AA 78GUI 01

20.17 0.76 RTNA 74MCC 01 20.2 0.4 AA 74RAI 01

20.3 2.9 ITNA 75RUC 01 20.5 0.6 ITNA 79GRE 01 20.6 2.3 IENA 77R0W 04

20.6 ITNA 75MIL 01 20.8 0.6 ICPES 81CHU 01

20.8 0.8 ITNA 77R0W 03

OA O A O 0.0 D* ITNA //ROW 04

21. 2. ITNA 75KLE 01 21.5 ITNA 77WEA 01 21.5 1 NAA 76HAN 01 21.6 2.1 PAA 74CHA 01 21.6 2. ITNA 76WEW 01 22. ITNA 77GLU 01

22

.

8

.

EXRF 79GIA 01 23. 4 AA 79REI 01 24. 3. * ITNA 76KUC 01 25.2 3.8 * ITNA 81 WAN 01 32.3 0.9 * ITNA 82SUZ 02

34 .9 0.9 * 12 ITNA 82SUZ 02

(ppm)

0.35 0.04 * PAA 74CHA 01 1.3 0.2 ITNA 78LAU 02

1.3 0.1 PAA 76CHA 01 1.32 0.11 ITNA 78NAD 02

1 .32 0.11 ITNA 75NAD 02

1.36 0.1 IENA 76STE 05

1.4 0.1 ITNA 73ABE 01

1 .4 0.1 9 ITNA 781AU 02

1.4 34 WXRF 82MIL 01

1 .4 ITNA 77WEA 01 1.4 ITNA 75KLE 01 1.4 0.3 ITNA 76WEW 01

1 .4 0.1 ITNA 750ND 01

1 .4 0.08 ITNA 76RAG 01

1 .46 0.11 IENA 77ROW 03

1 .49 0.22 ITNA 77ROW 04

1.52 0.11 IENA 77ROW 04

1.6 0.2 ITNA 79GRE 01

1 .71 0.04 ITNA 77MAE 01 1.73 0.09 ITNA 79ROS 03

1 .8 35 ITNA 81GLA 03

1 .8 0.3 ITNA 77CAH 01

1 .8 0.3 ITNA 75R0C 01 1.8 0.1 NAA 76HAN 01

1 .9 0.2 ITNA 81 WAN 01 2.3 0.1 * ITNA 82SUZ 02

2.55 0.06 * ITNA 73SHE 01 2.6 * ITNA 75MIL 01 3.5 1.3 * ITNA 78MAC 01

113
TABLE V (cont) TABLE V (cont)

CONC

Cu (ppm)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM CONC UNCER COMMENT

ANAL REF REF METH CODE NUM

70. L* ITNA 7 3 ABE 01 120. L* ITNA 82SUZ 02

13. EXRF 82KEE 01 14.1 0.9 ITNA 73SHE 01 15. 1.2 ITNA 77R0W 03

15. 1.2 ITNA 76STE 05

15. 3. SSMS 77D0N 01 15.7 2.7 ITNA 81 WAN 01 16.3 FAA 78GUI 01

16 .8 1

8 SSMS 80K0P 01 16.8 AA 78GUI 01

17 . 0.3 AA 73TAL 01

17 . 4

EXRF 81 KIN 01

17 . - 1

35 RTNA 77G1A 01 17. 7 .5 OES 76WEW 01 17.2 0.5 ICPES A 1 ill A 1 8 1 CHU 0

17.7 1.5 EXRF 79GIA 01 17.9 0.2 AA 74RAI 01

18

ICPES 80NAD 01

18

34 WXRF 82MIL 01

18. XRF 75KLE 01 18.1 0.8 NAA 76HAN 01 18.4 1.1 SSMS 77PAU 01

19. ICPES q riMAn n l 19.4 1 .9 FAA 7 /, n »T A 1 7hRA1 U 1 20. 4 AA 79REI 01 21. AA 76WEW 01 22.6 3. EXRF 73SPA 01 23. ITNA 77GLU 01 24. 3. 6 PAA 82SEG 01

30. 10. * PAA 80SEG 01 30. 10. *6 PAA 82SEG 01

(ppm)

2 .5 L* WXRF 82MIL 01

5L* OES 76WEW 01 0.57 0.04 * NAA 76HAN 01 0.85 0.06 ITNA 73SHE 01 1. 0.1 ITNA 78MAC 01 1.12 0.06 ITNA 76STE 05

1 .12 0.06 ITNA 77R0W 03

1.3 AA 82GIIP 0?

1 .3 0.5 ITNA 75RUC 01

1 .38 0.09 ITNA 75NAD 02

1 .4 0.1 ITNA 78NAD 02

1 .4 ITNA 75MIL 01

1 .59 0.16 ITNA 77CAH 01 2.4 0.2 * ITNA 82SUZ 02

(ppm)

3. L* WXRF 82MIL 01

15. L* OES 76WEW 01 0.7 AA 82GUP 02

(ppb)

1000. L* WXRF 82MIL 01 210. * ITNA 75KLE 01

1 1 UITNA 7 C Tt A/"1 A 1 /DRAG Ul 280. 10

ITNA 1 1 a nr A i 7JABE 01

S i . ITNA 1£CTC AC 300

100. ITNA 78MAC 01 312. 3/ . ITNA /JSHE 01

/. r\ ftU. ITNA 7 CAMTt A 1 / jUINU U 1

J JO

ITNA 7 7 1 TL7 A A 1 / / WL A U 1 OA A 1U . W A A M AA 7 tU AM A 1 / DrtA-N U 1 3An J4U» 40

ITNA

340. 20ITNA 78LAU 02

344. 15. ITNA 79R0S 03

360. 30. ITNA 77CAH 01 370. 20. ITNA 78NAD 02

370. 20ITNA 7 5NAD 0 2 370. 40. ITNA 76WEW 01 380. 40. ITNA 77ROW 04

380. 40. ITNA 79GRE 01 400. AA 82GUP 02

400. ITNA 7 5MIL 01

4 1060. OES 76WEW 01 410. 30. ITNA 75RUC 01

4 20. 20ICPES 81 CHU 01 420. 10. ITNA 77MAE 01 480. 90. * ITNA 81 WAN 01 500. 60. * ITNA 82SUZ 02

F (ppm)

51

ITNA 77GLU 01 65. ISE 83KNA 01

71 . ISE 81NAD 01 nn ISE 74THO 01

O 1 HI . VV 7 7PT IT A 1 87. ISE 74TH0 01 1UU. A A AA 7 £.im 7 Pi 1 / DWEjW U 1

6500. 1300. * OES 76WEW 01 7000. 400. * ITNA 76BL0 01 7150. 800. * EXRF 7 3 SPA 01 7200. * EXRF 82KEE 01 7517 . 1 19

ITNA 7 3 SHE 01 7790. 360. EXRF 79GIA 01 7800. 200. ITNA 75RIC 01 anno ICPES Q AXT AT* A 1 ©UNA!) U 1 8100. 700. ITNA 73ABE 01 8200

ICPES O AM A A A 1 80NAD 01 /UU. ITNA 7 L.V TTA A 1 /oKUC 01 ojuy • 111 L D

Q AWAT\ A 1 OUNAJJ Ul 8350. 120. AA 79ROS 03

8400. 200. ITNA 78LAU 02

8400. 400. D* NAA 740ND 01 8400. 200. D* TCGS 80AND 01 8400. 400. ITNA 750ND 01 8400. 200. ITNA 76RAG 01 8400. ITNA 75KLE 01 8410. 250. I ENA 77ROW 04

8420. 240. TCGS 79FAI 01 8500. 60. ITNA 75NAD 02

8500. 600. ITNA 78NAD 02

8527. AA 78GUI 01

114
TABLE V (cont) TABLE V (cont)

ANAL REF Uf

CONC ' UNCER COMMENT METH CODE NUM

8600. DAT rUl* 7AMAT 01 8600. TTMA 1 1NA 77UFA 01 8630. Zoo • Ei AlU R 1 KIN 01 8690

.

4 1U • PAA r AA 74CHA 01

O "7 Art 8 /OU. JJ ITNA 81GIA 03

q 7no LOO PAA 76CHA 01

R7nn O / \J\J . 200. ITNA 79GRE 01 8730. AA 76WEW 01 8800. ICPES 8ONAD 01

8800. 200. ITNA 77MAE 01 8810. 210. ICPES 81CHU 01

300. ITNA 78MAC 01

y U 1U • 10(1 D* ITNA 77R0W 04

1 JU. ITNA 77ROW 03

9030. TTMA 7 SMT1 n 1 / J FIX La KJ X 9130. 560. ITNA 79R0S 03

9200. 700. ITNA 81 WAN 01 9200. 300. NAA 76HAN 01 9200. 4 AA 79REI 01

9300. O AA 800. T1 TMA inn 77CAH / / \*Afl 01V 1 9300. O AA 800. TTMA 7SR1TC 01

O Q AA 1 AAA 1UUU . * ITNA 76WEW 01

111 1 I 1UUoo . * ITNA 77GLU 01

1 1100

.

300. *12 ITNA 82SUZ 02

1 1300. 500. * ITNA 82SUZ 02

Ga (ppm)

3. L* COLOR 79LTX 01

A =. ** . j ITNA 77GLU 01

AH.JS 0.5 RTNA 75RUC 01

4 .8 0.2 IENA 78WAN 01

eJ .ii • ITNA 78MAC 01

=. 15 J . 1

J

n\j . 3j ITNA 75RUC 01

j.j 0.5 ITNA 77CAH 01

j5 »*+A 0.8 ITNA 7 3SHE 01 5.5 0.7 ITNA 81 WAN 01

5.8 34 WXRF 82MIL 01

5.8 0.4 IENA 77R0W 03

5.8 A / EJ

TT7MA TtOTV 0") 6.1 0.3 EXRF 79GIA 01 6.1 0.6 5 IENA 76STE 05

6.2 0.3 OES 76WEW 01 7.7 1.4 ITNA 82SUZ 02

8.5 XRF 75KLE 01

oy . * NAA 76HAN 01

lju ^ p pm J

15. L* OES 76WEW 01

1 .2 0.06 ICPES 81CHU 01

1 .2 AA 82GUP 02

1 .43 0.05 TCGS 79FAI 01 2.2 0.08 TCGS 80AND 01 2.5 ITNA 75MIL 01

3. 34 WXRF 82MIL 01

3.6 0.4 ITNA 78NAD 02

3.62 0.35 ITNA 75NAD 02

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

Ge (ppm)

2. ITNA 77GLU 01

2.7 0.22 OES 76WEW 01 2.9 0.2 EXRF 79GIA 01

3. 34 WXRF 82MIL 01

70. 5. * ITNA 7 3 SHE 01

X)

4.02 0.05 D* TCGS 80AND 01

4 .02 0.05 TCGS 79FAI 01

4 9fl 0 01 PR ou oi_»n. 09Ui

" . j OU 1

. 1 j j 70P1 A OAU4

-T {.%)

2 .6 FD 80KHA 02

(ppm)

L . Li NAM ftOMTl OU 11 0.72 0.071 * ITNA 79R0S 03

0.81 0 1 ITNA 78LAU 02

0.83 0.06 n* IENA 77ROW 04

0.83 0.06 IENA 77R0W 03

O ft Q \J •Oy O HO u.uz TTMA 7 CUAn / jnAL) o 9 U L 0 fiQ O 09 TTMA j. inn 7AWAH / ortAU 09

0.91 0.11 ITNA 77R0W 04

0.92 0.05 ITNA 7 3 SHE 01 0.95 ITNA 75KLE 01 0.96 ITNA 77WEA 01 0.96 0.06 ITNA 79GRE 01 0.96 0.05 ITNA 750ND 01 0.97 0.1 ITNA 73ABE 01

1. 0.07 ITNA 76RAG 01 1.02 0.03 ITNA 77MAE 01 0.4 ITNA 81 WAN 01

1 -l 0- 15 ITNA 75RUC 01

1 .1 0.2 ITNA 77CAH 01

i !i 0.07 NAA 76HAN 01

, *, ITNA 75MIL 01

1 \ c

1 • 1

J

A 10 U. 11 T TM A 1 iNA *7 &7.7EM.7 A 1 U 1

1 .4 0.09 *9 ITNA 82SUZ 02

1 .53 0.5 * ITNA 82SUZ 02

\YY")

1

1 J500UU • T * WXKr 82MIL 01

1

i 1UU inn . EXRF 79GIA 01

9 90 TTMA 82SUZ 02

88. 5. CVAA 75KLE 01 100. PAA 77JER 01 100. PAA 74CHA 01 100. PAA 76CHA 01 110. ITNA 77WEA 01 110. 10. RTNA 740RV 01 110. 50. ITNA 77JER 01 110. 10. RTNA 75RUC 01 110. 16. RTNA 77JER 01 111. 10. FAA 77GLA 03

117. 13. FAA 7 5K0I 01

15
Ir

TABLE V (cont) TABLE V (cont)

ANAL REF REF ANAL KEF REF CONC ' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

120. CVAA 81NAD 01 K (ppm)

120. CVAA 82NAD 01

122. 29. CVAA 80DUM 01 Id 00

ICPES 80NAD 01 126. 6. CVAA 74RAI 01 2570. 4 AA 79REI 01 136. 9. FAA 82UCH 02 2600. 200. ITNA 76KUC 01 160. 80. ITNA 76WEW 01 2650. 190. ITNA 76BL0 01 160. 40. 12 ITNA 82SUZ 02 2660. 20. ITNA 75RIC 01 180. ITNA 7 7GLU U

z/uu. ICPES 80NAD 01 230. 20. * ITNA 7 0HIAti A 7 /oNAD UZ Z/UU. 300. NAA 76HAN 01 230. 20. ITNA 2700. ICPES 80NAD 01

2 30. 50. * ITNA 7 c. di a A i 2700. 100. PAA

510. 170. * ITNA 7 C.PT c a 1 2700. 200. T TMA 7 AC A 1 950. 90. * TTM A 1 1NA / jjnr, U L 27 50. 100. T\* TfPC Q A AXTT\ A 1 oUANL) Ul

2750. 100. 1 LOb /yrAI Ul

(ppb) 2780. 230. TTMA 7 A 7 / JlNAD U L 2800. 100. T TM A 1 JLNA 71 * -at} A 1 / JAdG Ul 2000. L* WXRF 82MIL 01 2800. 200. TTMA 7 QT A 11 A 9 1500. L* OES 7 6WEW 01 2800. 500. ITNA 7 tSWEW 01 240. 30. I ENA 77ROW 03 2800. 200. ITNA 77MAE 01 240. 30. I ENA 76STE 05 2800

200. ITNA 78NAD 02

250. FAA 82GUP 02 2800. ITNA 77WEA 01

. 2800. 300. ITNA 750ND 01 ppm) 2800. 300. ITNA 77CAH 01 2800

200. ITNA 79GRE 01 1.7 L* TTM A QOCTT7 AO 2840. 80. GAMMA 7 3 ABE 01

2 .68 0.2 DTXTA 771JAA A1 / / 1\U V Ul 2900. ICPES 80NAD 01

2 .78 0.38 ITNA 7 O CUC A 1 / Jbnh, U

2900. ITNA 75MIL 01 2.8 0.4 ITNA "7 CD1T ftl 2900. ITNA 7 5KLE 01 2.8 ITNA 7 /WEA Ul 2900. 200. ITNA 7SP.T1T / j r\u V/ 01tj i 2.9 0.3 ITNA 76STE OD 2980. 240. ITNA 77R0W 03

3. 34 WXRF 82MIL 01 200. ITNA 76STE 05

3.3 0.5 ITNA 77MAE 01 3000. 75. ICPES 81CHU 01 3.3 0.4 ITNA 77CAH 01 3000. 200. ITNA 78MAC 01 3.3 0.3 PAA 78HIS 01 3100. 500. ITNA 81 WAN 01 3.3 0.3 PAA 77WIL 01 3 100

600. OES 76WEW 01 3.7 0.5 I ENA

ft ^rtT A A 1 83GLA 01 j JUU . * ITNA 77GLU 01

4. 1

ITNA 79GRE Ul orAA J3UU. 360. * ITNA 7 3 SHE 01 6.2 1.9 * TTM A J. 1NA O 1 T.TA o l wtfvri]\| 01\j i 200. * ITNA 82SUZ 02

6.63 1.2 * TTMA 1 1 nn 0? La (ppm)

(ppb)

6. 0.17 * OES 76WEW 01 1000. L* WXRF ozniJL ui 7 BQ 0.15 * ITNA 75NAD 02

16.9 1 .2 I ENA / /RUW Uj 7.9 0.2 * ITNA 78NAD 02

16.9 1.7 5 IENA T £ CTT? A C. /Dolt. Uj 8 . J 0.2 ITNA 78MAC 01 17.8 1

5 IENA T/nipp AC 76STE Uj Q 1 0-4 ITNA 76BLO 01 30. 20. ITNA T/n A^ A 1 76RAG 0

0.3 ICPES 81CHU 01 40. 10. ITNA 73SHE 01 y . j 0.5 ITNA 78LAU 02

56. 9. ITNA 82SUZ 02 y .5 0.2 ITNA 76RAG 01

70. ITNA 7 5KLE 01 9.76 0.45 NAA 76HAN 01

180. 20. ITNA T T P All A 1 7 7 CAH 0

1034 WXRF 82MIL 01

200. 120. ITNA 7jOND Ul 10. FAA 82GUP 02

220. 20. T TM A 1 1NA 7cpnp oi / JRU^ U 1 10.3 0.5 D* ITNA 77R0W 04

230. 20. ran 10 .3 1.1 ITNA 76STE 05

230. JU • PAA [An 7 6CHA 01 10 .3 0.3 ITNA 77R0W 03

(ppb) 11/ • j u .y ITNA 81 WAN 01 10.5 ITNA 75KLE 01

50. L* 10.5 0.5 ITNA 7 3 ABE 01

2 .48 0.27 ITNA 73SHE 01 10.6 0.4 ITNA 77CAH 01

2.5 ITNA 77WEA 01 3.53 0.52 RTNA 77NAD 02

116
TABLE V (cont) TABLE V (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC

10.7 ITNA 77WEA 01 2300.

10 .7 0.4 T TM A QOCII7 AO 2300.

10.7 0.3 ITNA 77MAE 01 2480.

10 .7 1 .2 ITNA 750ND 01 2500.

10 .8 0.8 I ENA 77ROW 04 4000.

11. OES 82GUP 02 8200.

11.3 3.3 ITNA 73SHE 01

1 1 1 1 1 • J ITNA 7 5RUC 01 Mn (ppm)

11.3 ITNA 75MIL 01

11 A u o J. CflA 77ROW 03 27 .5

11 A U.J IENA 76STE 05 36

.

11.3 u • / TTNA 7QGRE 01 JO . o j i . (ppm) 37

38

.

24

.

1*1 UCiJ 38 . 25

.

A A 38. ICPES fi 1 CHU 0

1

38.5

39. 39.

39. 1000. L* WXRF 82MIL 01 39.5

7000. L* OES 76WEW 01 40. FAA 82GUP 02 40.

1 Afi ITNA 75MIL 01 40.

1 AG 1

1

IX* D* ITNA 77ROW 04 40.3

109

.

i * li. ITNA 77R0W 03 U 1 120. 10. ITNA 78NAD 02 41.

i oa 1 zU • c

j> » ITNA 75NAD 02 4 1

.

130. 5. ITNA 77MAE 01 41.

J\J . ITNA 77CAH 01 41.

140. 70. ITNA 81 WAN 01 41.1

140. 20. ITNA 78LAU 02 41.1

140. 10

.

ITNA 750ND 01 41.7

140. 20. NAA 76HAN 01 42.

150. 10. ITNA 75RUC 01 42.

150. 20. ITNA 76WEW 01 42.5

2 10. 20. * ITNA 82SUZ 02 42.8

416. 17. * ITNA 7 3 SHE 01 43.

43.

v r r"1 / 43.

43. 980. 250. ITNA 7 3 SHE 01 43.

1 100 . 300. ITNA 77MAE 01 43.5

1 100. ITNA 77GLU 01 43.5

1200. ICPES 8 ONAD 01 43.7

1200. ICPES 80NAD 01 44. 1340. 270. ITNA 82SUZ 02 44.5

1370. 40. ICPES 81 CHU 01 45.

1400. ICPES 80NAD 01 45. 1500. 300. ITNA 78NAD 02 45. 1500. 300. ITNA 75NAD 02 46. 1600. ICPES 80NAD 01 46. 1600. 150. PAA 74CHA 01 47.1

1600. 300. OES 76WEW 01 1600. 200. PAA 76CHA 01 Mo (ppm)

1700. 300. ITNA 77ROW 03

1700. 200. ITNA 79GRE 01 0.2 1700. 300. ITNA 76STE 05 0.2 1900. 400. NAA 76HAN 01 0.3

2000. 500. ITNA 750ND 01 0.3

2000. 400. ITNA 76WEW 01

ANAL REF REF UNCER COMMENT METH CODE NUM

400. ITNA 81 WAN 01 700. ITNA 73ABE 01 ITNA 75KLE 01 800. ITNA 76RAG 01 2000. * ITNA 78LAU 02

2000. * ITNA 78MAC 01

2.4 * ITNA 82SUZ 02

1.8 OES 76WEW 01 FAA 78GUI 01

2. EXRF 81KIN 01 EXRF 82KEE 01 2.6 ITNA 7 3 SHE 01

4 AA 79REI 01

8. 35 ITNA 81GLA 03 AA 78GUI 01

3. EXRF 79GIA 01 ITNA 77GLU 01

34 WXRF 82MIL 01

0. 7 ITNA 76RAG 01

7. ITNA 78NAD 02

4. ITNA 76WEW 01 AA 76WEW 01 6.9 ITNA 75NAD 02

6. ITNA 73ABE 01 ITNA 77WEA 01

6. ITNA 80BUA 01

2. NAA 76HAN 01

1. ITNA 75RIC 01 3.6 ITNA 77R0W 03

3.6 ITNA 76STE 05

0. 5 AA 79ROS 03

ICPES 80NAD 01

1 . ITNA 79GRE 01 5.8 ITNA 81 WAN 01 2.4 ITNA 77CAH 01

1. ITNA 78MAC 01

4. D* NAA 740ND 01

4. ITNA 750ND 01

6. ITNA 76BL0 01

3. PAA 76CHA 01 2.4 D* TCGS 80AND 01

2.4 TCGS 79FAI 01 1.8 ITNA 75RUC 01

2. ITNA 78LAU 02

0.9 ITNA 77MAE 01

3. ITNA 76KUC 01

1.4 ICPES 81 CHU 01 ICPES 80NAD 01

3. ITNA 75KLE 01 ITNA 75MIL 01

4.1 * PAA 74CHA 01

0.04 PAA 76CHA 01 0.02 PAA 74CHA 01

0.1 PAA 80SEG 01 0.1 6 PAA 82SEG 01

117
TABLE V (cont) TABLE V (cont)

ANAL KEF M£F ANAL REF EC CONC UNCER COMMENT meTM CODE NUM CONC ' UNCER COMMENT METH CODE NUM

0.3 0.1 6 PAA 82SEG 01 UKwd t nnfn\ ppm ) 0.41 0.1 ITNA 82SUZ 02

3.08 0.12 D* IENA 77R0W 04

ID . 3.08 0.12 I ENA 77ROW 03 L* OES 76WEW

3.14 0.28 RTNA 78NAD 01

E3 . 34 WXRF 82MIL

3.2 0.4 ITNA 77CAH 01 3.3 ICPES 80NAD 01 NO vppia)

3.4 ITNA 75KLE 01 3.6 0.16 OES 76WEW 01 15. OES 76WEW

4. 34 WXRF 82MIL 01 6.4 1.5 ITNA 7 3 SHE

4.7 ICPES 80NAD 01 7. 34 WXRF 82MIL

5. ITNA 77GLU 01 8. AA 82GUP

5. ITNA 77WEA 01 8.7 1. D* ITNA 77ROW

8.7 1. ITNA 77ROW

%) 9.5 1.9 ICPES 81CHU

10.7 ITNA 75MIL

1 .2 0.2 35 TCGS 79GLA 04 11.3 2. D* TCGS 80AND

1.3 0.02 CB 80SCH 02 11.3 2. TCGS 79FAI

1.3 0.2 D* TCGS 80AND 01 16.9 1.4 * ITNA 82SUZ

1.3 0.2 TCGS 79FAI 01 17.8 3.7 *12 ITNA 82SUZ

Na (ppm)

325. 6. ITNA 75RIC 01 335. ICPES 80NAD 01

340. 10. ITNA 78LAU 02

347. 32. ITNA 75NAD 02

350. 30. ITNA 78NAD 02

350. 20. PAA 76CHA 01 351. 30. PAA 74CHA 01 352. 34. ITNA 77CAH 01

353. 21. ITNA 76KUC 01 360. 10. ITNA 79GRE 01

360. 20. NAA 76HAN 01 368. 9. ITNA 77MAE 01 370. 33. ITNA 73SHE 01 370. ICPES 8 ONAD 01 380. 12. ITNA 76RAG 01

380. 3. ITNA 78MAC 01 380. 25. ITNA 76STE 05

380. 25. ITNA 77R0W 03

380. ICPES 80NAD 01 383. 14. ITNA 75RUC 01 387. 42. ITNA 81WAN 01 390. ITNA 77GLU 01

390. 34 WXRF 82MIL 01

390. ITNA 75KLE 01

400. 900. R* ITNA 81GLA 03

400. 7. ICPES 81CHU 01

400. 30. ITNA 76BLO 01

409. ICPES 80NAD 01

410. ITNA 75MIL 01

414. ITNA 77WEA 01 414. 20. ITNA 750ND 01

415. 42. ITNA 76WEW 01 420. 30. ITNA 73ABE 01 480. *4 AA 79REI 01

840. 30. * ITNA 82SUZ 02

1200. 240. * OES 76WEW 01

Nl (ppm)

10. EXRF 82KEE 01 11. IENA 77R0W 03

12. 0.7 ITNA 78NAD 02

12.1 0.7 ITNA 75NAD 02

13. 3. 9 ITNA 78LAU 02

13.5 1.2 PAA 74CHA 01 14. 1. PAA 80SEG 01

14. 4 AA 79REI 01

14. 1. 6 PAA 82SEG 01

14. 2. PAA 76CHA 01 14. 2. 6 PAA 82SEG 01

14.3 AA 78GUI 01

14.5 1.2 EXRF 79GIA 01 14.5 XRF 75KLE 01 14.7 0.6 6 IDMS 74M00 01 14.7 0.6 6 IDMS 74M00 01

14.8 POL 74MAI 01

14.8 0.7 6 IDMS 74M00 01

15. 3. SSMS 77DON 01 15. 34 WXRF 82MIL 01

15. 1.1 OES 76WEW 01 15. AA 76WEW 01 15.2 0.5 ICPES 81CHU 01 15.5 1.1 8 SSMS 80K0P 01

16. 4. ITNA 73ABE 01 16. 5. ITNA 77CAH 01 16. ICPES 8 ONAD 01 16.4 IENA 77ROW 04

17.1 FAA 78GUI 01

17.5 1. EXRF 81KIN 01

18. 4. ITNA 750ND 01 18. 4. D* NAA 740ND 01

18. 5. NAA 76HAN 01 18.4 2.1 ITNA 75RUC 01 18.9 0.8 ITNA 82SUZ 02

19. ICPES 80NAD 01

20. ITNA 77GLU 01

20.4 1. 12 ITNA 82SUZ 02

118
TABLE V (cont) TABLE V (cont)

CONC

0 (%)

ANAL REF REF UNCER COMMENT METH CODE MUM cone UNCER COMMENT

15 .05 0.11 34 14NAA RfttfHA O UrviLrt

ft ft ( nmn ^

1 - L* RTNA 77NAD 02

P (ppm)

71. AA 7 6WEW 01

92. ICPES 80NAD 01

104. ICPES 80NAD 01

120. VV 77GLU 01

138. 34 WXRF 82MIL 01 150. 9. ICPES 81 CHU 01

156. ICPES 81NAD 01 250. COLOR 80NAD 01

270. COLOR 80NAD 01

Pb (ppm)

12. 120. R* OES 76WEW 01 13.6 6.5 * EXRF 79GIA 01 15. * ICPES 80NAD 01 19.1 ICPES 81NAD 01

20. ICPES 80NAD 01

23. 0.9 EXRF 7 3 SPA 01 23. VV 77GLU 01

24

.

4 AA 79REI 01

26 . 6

.

FAA 76BL0 01 26.1 AA 78GUI 01

27.9 2.5 8 SSMS 80KOP 01

28. 1. 6 PAA 82SEG 01

28. 2. PAA 80SEG 01

28. 5. FAA 75BL0 02

28. 3.6 SSMS 77PAU 01

28. 2. 6 PAA 82SEG 01

28. 4. IDMS 78CAR 02

28.4 POL 74MAI 01

28.5 1.5 ICPES 81CHU 01

28.6 FAA 78GUI 01

29. 0.5 AA 73TAL 01 29. 2. PAA 77JER 01 29.4 IDMS 75KLE 01 30. AA 76WEW 01

31. 3. EXRF 81 KIN 01 32. 2. PAA 77JER 01 32. 34 WXRF 82MIL 01

32. 2. PAA 76CHA 01

32.1 1.8 PAA 74CHA 01

33. 3. SSMS 77D0N 01 33. 2. AA 79ROS 03

(ppb)

5. L* RTNA 77NAD 02

(ppm)

2. L* FAA 82GUP 02

15. L* OES 76WEW 01

2.3.6

4.6

Pt (ppb)

186.

270.

Rb (ppm)

10.

15. 16.3

16.3

18. 18.3

18.3

19.

19. 19.

19. 19.4

19.5

20. 20.

20.

20. 20.

20.1

21.

21. 22.

22.5

22.5

22.8

23.

23. 24.

24.

24.7

26. 28.6

30.

Rh (ppm)

Ru (ppb)

18.

S (%)

0.17

0.17

0.9

0.4

0.5

15000.

2.3

20.

3.

3.7

3.7

1.1 1.6 1.9

1.5

2.

6.2.3

2.

2.4.

2.2.0.6

2.2.9

0.7

3.7 4.8

7.

3.

1

.

1

.

3.2

1.

5.

5000.

1.

3.8

34

12

L*

ANAL

METH

WXRF

ITNA ITNA

REF REF CODE NUM

82MIL 01 82SUZ 02

82SUZ 02

*35

34D*

**12

L*

L*

L*

*

OES RTNA RTNA

ITNA ITNA

ITNA ITNA

WXRF

IENA

IENA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA ITNA ITNA "AA

PAA

EXRF

ITNA

ITNA

OES ITNA

ITNA

ITNA ITNA NAA

XRF

ITNA

ITNA

ITNA

EXRF ITNA

OES

OES

RTNA

ITNA ICPES

CB

ICPES

76WEW 01 77NAD 01

77NAD 02

81WAN 01 81GLA 03

75NAD 02

78NAD 02

82MIL 01

77R0W 04

77ROW 03

7 3 SHE 01 76RAG 01 73ABE 01 76WEW 01 77R0W 04

75KLE 01

78LAU 02

79GRE 01 78LAU 02

7 50NT) 01 76CHA 01 79GIA 01

77WEA 01 750ND 01

76WEW 01 77MAE 01 75RUC 01 77CAH 01 76KUC 01 76HAN 01 75KLE 01 75MIL 01 79R0S 03

82SUZ 02

7 3 SPA 01 82SUZ 02

76WEW 01

76WEW 01 77NAD 02

82SUZ 02

80NAD 01

80NAD 01 80NAD 01

119
TABLE V (cont) , . TABLE V (cont)

ANAL UF REF ANAL R£F R£f CONC ' UNCER COMMENT METH CODE NUM CONC ' UNCER COMMENT METH CODE NUM

0.9 CB 80NAD 01 3.7 ITNA 77WEA 01 1.25 XRF 77GLU 01 3.7 0.1 ITNA 75RIC 01 1.29 0.03 D* TCGS 80AND 01 3.75 0.24 ITNA 79ROS 03

1 .29 0.03 TCGS 79FAI 01 3.8 0.05 D* ITNA 77R0W 04

1 .32 XRF 81NAD 01 3.8 0.4 ITNA 76WEW 01 1.32 0.07 TCGS 77JUR 01 3.8 0.05 ITNA 77R0W 03

1.32 XRF 82NAD 01 3.81 0.47 ITNA 75RUC 01 1.99 * CB 77LAD 01 3.88 0.15 NAA 76HAN 01 2.02 * TITR 77LAD 01 3.9

3.95

0.2

0.06 ITNA IENA

76KUC 01 77R0W 04

pm)

t no i .90 A A /. 0.0A ITNA 78MAC 01

r4 . 0.2 ITNA 79GRE 01

ft A

1

U •K)D it ITNA oz A 1 ftU 9mi. T TWA 0 1 WAIN U 1

1 .8 0.9 * FAA 77ARU 01

A 1 WAKT OOUTl (\ 1 oZMLL Ul

2 .2 ITNA 75MIL 01 A 1 TTO* X Ifln 7 IMT T ft 1

i - i D O D*K

PAT AD 7 7 ADII / / AKU ft 1 4 9 n i T TMA 7 7MAT? HI

2 .6 2

.

ITNA 77ARU 01 4.3 ITNA 7 5KLE 0

1

2.7 5 ITNA 77ROW 04 C A A 1 0. 1 ITNA 82SUZ 02

2 .8 0.7 ITNA 81 WAN 01

2.8 5 IENA 77ROW 04 s>e ippm;

3. 34 WXRF 82MIL 01

3. ITNA 77GLU 01 10

.

L* ICPES 81CHU 01

3. RTNA 75RUC 01 1.1 0.08 CPXRF 80KIR 01

3. 5 ITNA 77R0W 04 2. * HAA 74BYR 02

3. IENA 77ROW 03 2 .3 0.2 *g ITNA 82SUZ 02

3.06 1.4 ITNA 75NAD 02 2.4 0.1 ITNA 78NAD 02

3.09 0.26 PAA 74CHA 01 2 .44 0.08 ITNA 75NAD 02

3.1 1.4 ITNA 78NAD 02 2.5 0.2 ITNA 80WAN 01

3.2 35 ITNA 81GLA 03

O CI Z .51 A 1 1 0.

1

5 a0 SSMS 80K0P 01

3.2 5 IENA 77R0W 04 Z .6 A 1 0. 1 ITNA 82SUZ 02

3.4 0.1 ITNA 76RAG 01 2 .6 0.3 9 ITNA 80WAN 01

3.4 0.8 ITNA 75RUC 01 2 .6 0. 16 FAA 77ARU 01

3.6 1.2 ITNA 77MAE 01 2 .7 0.2 RTNA 740RV 01

3.6 0.8 ITNA 77CAH 01 2.8 ITNA 77GLU 01

3.7 2. ITNA 7 3ABE 01 2.8 0.11 RTNA 75RUC 01

3.8 0.2 ITNA 78MAC 01 2.86 0.13 DCP 81 CAR 02

3.8 0.4 NAA 76HAN 01 2.86 0.13 GCMES 74TAL 02

3.82 0.1 ITNA 78LAU 02 2.86 0.13 GCMES 75KLE 01 3.9 1.3 ITNA 7 50ND 01 2.9 0.1 ICPES 80HAA 01 3.9 0.24 ITNA 77JER 01 2.9 0.2 ITNA 79GRE 01

3.9 0.3 PAA 76CHA 01 2.9 0.2 XRF 77ARU 01

3.9 ITNA 77HEA 01 2.9 0.4 ITNA 76RAG 01

3.9 0.3 PAA 77JER 01 2 .99 0.07 SSMS ~l 7T> AIT f\ 1 / /PAU U

1

4.1 1.2 ITNA 76WEW 01 3

.

A O H AC C oUCLA Ul

4.3 0.3 ITNA 79GRE 01 3

.

1 • D A A rAA one f\ i OUbCAj Ul

4.4 0.3 FAA 78HAY 01 3. 34 WXRF 82MIL 01

4.45 ITNA 75KLE 01 3. 0.4 RTNA 80KNA 01 6.4 1.6 * ITNA 7 3 SHE 01 3.

3.

1.0.36D* PAA

IENA

82SEG 01 77R0W 04

pm) 3. 0.3 PAA 76CHA 01

3. 0.3 IENA 77R0W 03

3.4 0.3 ITNA 77CAH 01 3. 0.4 6 PAA 82SEG 01

3.4 0.3 ITNA 73ABE 01 3.03 0.28 PAA 74CHA 01 3.5 0.1 ITNA 7 8NAD 02 3.05 ITNA 75KLE 01 3.5 0.08 ITNA 75NAD 02 3.05 0.48 ASV 7 6AND 01

3.58 0.35 PAA 74CHA 01 3.1 ITNA 77WEA 01 3.6 0.08 OES 76WEW 01 3.1 0.2 EXRF 79GIA 01 3.6 0.3 PAA 76CHA 01 3.1 0.6 ITNA 78MAC 01 3.68 0.08 ITNA 76RAG 01 3.1 1.6 ITNA 76WEW 01 3.69 0.05 ITNA 78LAU 02 3.2 0.4 ITNA 76BL0 01

3.7 0.3 ITNA 750ND 01 3.2 0.3 ITNA 75RIC 01

120
TABLE V (cont) TABLE V (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NDM

3.3 0.4 ITNA 7 3 ABE 01 3.3 0.2 9 ITNA 78LAU 02

3.3 0.6 ITNA 78LAU 02

3.4 0.2 D* NAA 740ND 01 3.4 0.2 ITNA 750ND 01 3.5 0.3 ITNA 77MAE Ul 3.6 0.4 ITNA 75RUC 01 3.7 0.7 ITNA

3.8 0.51 ITNA 7 3 SHE 01 3.8 0.7 * ITNA 77CAH 01 3.9 0.4 * ITNA 81 WAN 01 4.7 * COLOR 74BYR 02

5.5 0.5 * EXRF 7 3 SPA 01

(%)

2.1 0.42 * OES 76WEW 01

2 .6 *4 AA 79REI 01

2 .95 0.06 TCGS 79FAI 01 2.95 0.06 D* TCGS 80AND 01

3. 0.4 DA A rAA

3.14 ICPES 80NAD 01

3 .17 ICPES 80NAD 01

3.19 ICPES 80NAD 01 3.2 AA 76WEW 01 3-21 ICPES H UNAD O

1

3.5 0.8 14NAA 76BLO Ul 3.92 * VV 7 7GLU 0

1

(ppm)

2. L* WXRF 82MIL 01

15. L* OES 76WEW 01 1.3 0.19 ITNA 73SHE 01 1.3 0.2 ICPES 81CHU 01 1.38 0.1 IENA 76STE 05

1.38 0.09 ITNA 77ROW 04

1.4 FAA 82GUP 02

1.4 0.1 ITNA 78MAC 01 1.4 0.1 IENA 77R0W 03

1.41 0.06 IENA 77R0W 04 1.53 0.02 D* TCGS 80AND 01 1.53 0.02 TCGS 79FAI 01 1.55 0.07 NAA 76HAN 01

1 .6 ITNA 75MIL 01

1.6 0.2 ITNA 77CAH 01 1.66 0.16 ITNA 75NAD 02

1.7 0.3 ITNA 73ABE 01 1.7 ITNA 77WEA 01 1.7 0.2 ITNA 750ND 01 1.7 0.2 ITNA 78NAD 02

1.72 0.08 ITNA 76RAG 01 1.74 0.02 ITNA 78LAU 02

1.8 0.1 ITNA 75RUC 01 1.9 0.2 ITNA 79GRE 01

1 .93 0.14 ITNA 77MAE 01 2.9 0.2 * ITNA 82SUZ 02

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

Sn (ppm)

2. 10. R* OES 76WEW 01

4 . 0.2 ICPES 80HAA 01

5

.

34 WXRF 82MIL 01

8. ICPES 8ONAD 01

9.7 ICPES 80NAD 01

10. 1

.

6 PAA 82SEG 01

10. 1

.

PAA 80SEG 01

10. 1

.

PAA 76CHA 01 10. ITNA 77GLU 01 10.2 1

.

PAA 74CHA 01

11. 0.4 6 PAA 82SEG 01

125

.

20. * ITNA 73SHE 01

ppm)

1.02 0.05 * ITNA 75NAD 02

1 .33 0.1 * PAA 74CHA 01

91 . 9

.

* ITNA 82SUZ 02

93. 9.2 ITNA 73SHE 01 93. 7. 12 ITNA 82SUZ 02

99. 4 AA 79REI 01 112. 26. ITNA 76RAG 01

120. 20. NAA 76HAN 01 123. ITNA 75KLE 01 125. 26. ITNA 78NAD 02

129. ITNA 75MIL 01 131. 23. ITNA 76STE 05

140. 2.8 ICPES 81CHU 01

140. 15. PAA 76CHA 01 140. 40. ITNA 78LAU 02

144. XRF 7 5K1.E 01 145. 9. ITNA 75RUC 01 151. 34 WXRF 82MIL 01 151. 4. EXRF 79GIA 01 155. 15 . EXRF 7 3 SPA 01 155. 6. ITNA 77CAH 01 159. 14. IENA 77R0W 04

160. 10. IENA 77R0W 03

161

.

16. ITNA 750ND 01

161

.

9. 5 IENA 76STE 05

164. 25

.

ITNA 81 WAN 01 164. 14

.

ITNA 77MAE 0

1

165. 21

.

5 IENA 76STE 05

170. 10

.

ITNA 7 3ABE 01

1 7 Ci zu • T TW A 7 QT All nU 7L

1 7 n 1 / • T THA / DWtW C\U 1

1

1 7 n T THA 7 DMA P U

1

190. ITNA 77R0W 04

280. 56. * OES 76WEW 01

:ppb)

1500. L* WXRF 82MIL 01

170. ITNA 75KLE 01 210. 35 ITNA 81GLA 03

210. 20. ITNA 77CAH 01 210. 20. ITNA 75RUC 01 230. 20. ITNA 76RAG 01 240. ITNA 77WEA 01 240. 40. ITNA 750ND 01

121
TABLE V (cont) TABLE V (cont)

ANAL REJF KEF CONC UNCER COMMENT meTM CODE NUM

240. 10. ITNA 78NAD 02

240. 10. I TOA 7 5NAD 02

250. 10. ITNA 77MAE 01 250. 30. NAA 76HAN 01 270. 20. ITNA 79R0S 03

27 3. 6. I ENA 77R0W 03

27 3. 9. D* IENA 7 /ROW 04

290. 50. ITNA 78LAU 02

300. ITNA 75MIL 01 300. ITNA 77ROW 04

350. 20. ITNA 82SUZ 02

360. 28. * ITNA 7 3 SHE 01 460. 50. * ITNA 7 3 ABE 01

(ppb)

500. L* ITNA 77R0W 04

2000. L* WXRF 82MIL 01 15000. L* OES 76WEW 01 400. L* FAA 82GUP 02

30. * ITNA 73SHE 01 200. 40. ITNA 76WEW 01 200. 20. ITNA 76RAG 01 230

.

10

.

T TM A 1 1NA 7/ QlOLiAU AIT mU£

230. 60. ITNA 73ABE 01

Z JU . ITNA 750ND 01 260. 20. ITNA 82SUZ 02

274. 12. IENA 77R0W 03

274. 12. D* IENA 77R0W 04

400. 20. ITNA 75NAD 02

400. 20. ITNA 78NAD 02

500. * ITNA 75MIL 01

(ppb)

600. L* WXRF 82MIL 01 690. L* ITNA 82SUZ 02 1000 L* PAA 76CHA 01 500. FAA 77GLU 01 600. 40. 35 RTNA 75GLA 01 1020. PAA 74CHA 01

(ppm)

15. L* OES 76WEW 01 1.28 0.06 * ITNA 75NAD 02

1.3 0.1 * ITNA 78NAD 02

2.4 0.2 * ITNA 76BL0 01 2.7 0.7 EXRF 79GIA 01 2.87 0.09 ITNA 77R0W 04

2 .87 0.24 ITNA 79R0S 03

2.9 0.1 ITNA 76RAG 01

3. 0.2 ITNA 78LAU 02

3. 34 WXRF 82MIL 01

3. ITNA 75KLE 01 3.1 0.2 ITNA 7 3 SHE 01 3.1 0.2 ITNA 7 50ND 01 3.12 0.1 IENA 77R0W 03

3.12 0.1 D* IENA 77R0W 04

3.2 0.2 ITNA 79GRE 01 3.2 35 ITNA 81GLA 03

3.2 0.3 ITNA 76WEW 01 3.2 0.1 ITNA 77MAE 01

ANAL HEF REF CONC UNCER COMMENT METH i CODE NUM

i mi ITNA 75MIL 01

9 9 U.D NAA "7 £U A XT A 1 / oHAN U 1 3.3 0.6 I TOA 8 1 WAN 01 3.4 0.6 ITNA 73ABE 01 3.45 0.1 GAMMA 750ND 01 3.45 0.1 GAMMA 73ABE 01

3 .5 0.6 ITNA 7 7 PAH 01

3 .65 0.49 ITNA 7 5RUC 01 4.1 0.1 * ITNA 82SUZ 02

*4.6 0.1 *2 ITNA 82SUZ 02

4.7 * DNA 75MIL 01

(ppm)

680. EXRF 82KEE 01 690. AA 79REI 01 790. POL 74MAI 01 800. ITNA 77WEA 01 800. AA 76WEW 01 839

.

172

.

ITNA 7 5NAD 02

840. 200. ITNA 78NAD 02

885. 150. ITNA 76BL0 01 890. 50. ITNA 77R0W 03

890. 35. D* TCGS 80AND 01 890. 35. TCGS 79FAI 01 890. 50. ITNA 76STE 05

890. 200. PAA 750ND 01 900. 180. OES 76WEW 01 900. 100. PAA 76CHA 01 920. 50. NAA 76HAN 01 930. ICPES 80NAD 0

1

1AJH WAivr Q9MTT Q fl 1

4. 1 11 Li U 1 930. ITNA 7 5KLE 01 946. 24

.

ICPES 81CHU 01 951

.

53. EXRF 79GIA 01 960. ICPES 80NAD 01 960. ICPES 80NAD 01 972. ICPES 80NAD 01 973. 50. PAA 74CHA 01 980. 60. ITNA 79GRE 01 995. 100. ITNA 78MAC 01 1000. 260. ITNA 76RAG 01 1028. 30. AA 79R0S 03

1060. 35 NAA 81GLA 03

1075. 100. ITNA 750ND 01 1100. 100. ITNA 81 WAN 01 1100. ITNA 77GLU 01

i \f\r\ 1 1UU

.

i in

I 1U • 1 1NA

l l nn 9nn T TM A 1 1NA 7 OA tip n 1

1 ?f)fi 1 iUU • TTNA i UNA 7RT ATI (*i9 1312. 150. * ITNA

1550. 130. * ITNA 82SUZ 02

(ppb)

2000. L* FAA 77GLU 01 1000. L* WXRF 82 MIL 01 1000. L* AA 76WEW 01 5000. L* OES 76WEW 01 500. 100. PAA 80SEG 01 500. 100. 6 PAA 82SEG 01 512. 60. PAA 74CHA 01 520. 60. PAA 76CHA 01

122
TABLE V (cont) TABLE V (cont)

ANAL REF REF ANAL REF REF CONC " UNCER COMMENT METH CODE HUM CONC ' UNCER COMMENT METH CODE NUM

con 60. SSMS 77PAU 01 11 \j . ITNA 78MAC 01

OWKJ • 100. 6 PAA 82SEG 01 11j j . ITNA 76BL0 01 600. iaa SSMS 77D0N 01 33. 3. ITNA 7 8NAD 02

610. 37. 8 SSMS 80KOP 01 33.6

33.9 3. AA

PAA

78GUI 01 74CHA 01 Tm (ppb) 34. 34. 3.

ICPES

PAA

80NAD 01 76CHA 01 1000. L* WXRF 82MIL 01 35. 2.9 ITNA 77R0W 03

Li 0ES 76WEW 01 35. 2.9 ITNA 76STE 05

110. FAA 82GUP 02 35. ITNA 77WEA 01 300. ITNA 77GLU 01 35 .2 1.5 AA 79R0S 03

300. ITNA 75MIL 01 IS ft ItJo •

1 L

•> ITNA

ITNA

81 WAN 01

79GRE 01

TT 1 ninn 1 Jo . Jo

.

/. H • J • ITNA

NAA

7 3 SHE 01 740ND 01

2 .3 L* EXRF 79GIA 01 Jo

.

J • ITNA 750ND 01 0.98 0.078 ITNA 7 3 SHE 01 1<i AA 76WEW 01

1 .1 nu .usAn Jj RTNA 75GLA 01 36

.

4. ITNA 76WEW 01

1 .2 0.1 ITNA 78NAD 02 36 .2 FAA 78GUI 01

1 .2 0.1 ITNA 75NAD 02 37. 3. ITNA 75RIC 01

1 .2 0.05 IDMS 78CAR 02 37.6 1.4 ITNA 77MAE 01

1 .21 IDMS 75KLE 01 38. 1.2 ICPES 81CHU 01

1 .24 0.05 ITNA 76RAG 01 40. 3. ITNA 75KLE 01 1.25 0.06 ITNA 82SUZ 02 41. 10. ITNA 76RAG 01

1.26 ITNA 75KLE 01 42. 2. * ITNA 82SUZ 02

1 .3 0.1 PAA 80SEG 01 43. *4 AA 79REI 01

1 .3 n i 0 PAA 82SEG 01 * ITNA 77GLU 01

1 .33 DNA 83GLA 01

1 .34 U.J ITNA 78MAC 01 W ( nnh

1

1 .35 ITNA 77WEA 01

1 .37 0 OR ITNA 74WEA 01 1500. L* WXRF 82MIL 01

1 .4 ITNA 81 WAN 01 450. 90. * ITNA 81 WAN 01

1 .4 n i 0 PAA 82SEG 01 630. 60. ITNA 77MAE 01

1 .41 0.07 GAMMA 7 3ABE 01 650. 150. ITNA 76RAG 01

1 .41 0.07 GAMMA 750ND 01 710. 70. IENA 77R0W 04

1.41 0.07 D* NAA 740ND 01 710. 80. ITNA 82SUZ 02

1.43 DNA 75MIL 01 740. 300. ITNA 75RUC 01 1.45 0.04 IENA 77ROW 04 750. 100. IENA 77R0W 03

1 .46 0.02 IENA 76STE 05 750. 170. ITNA 750ND 01

1 .46 0.04 IENA 77ROW 03 750. ITNA 77WEA 01 1.46 0.35 ITNA 7 5RUC 01 780. 80. ITNA 79GRE 01

1 .49 35 DNA 81GLA 03 790. 170. IENA 76STE 05

1 .5 0.1 13 PAA 81SEG 01 870. 200. ITNA 77CAH 01

1 .5 ITNA 75MIL 01 ROD * ITNA 7 3 SHE 01

1 .52 n 1

1

ITNA 76STE 05

1 .6 nv . 9£t i j PAA 81SEG 01 Y (ppm)

1 .6 A 0 NAA 76HAN 01

2

.

X.I "J4 WXRF 82MIL 01 7. AA o2GUP 02

6

.

AA 76WEW 01 7.4 34 WXRF 82MIL 01

7.6 0.81 OES 76WEW 01 V (ppm) 7.9

8.

0.6 EXRF OES

79GIA 01 82GUP 02

24. o0 . EXRF 79GIA 01 30. O . ^CJ3 ITNA 81GLA 03 Yb (ppb)

32. 34 WXRF 82 MIL 01

32. 4. ITNA 78LAU 02 2000. L* WXRF 82MIL 01 32. 1.3 OES 76WEW 01 550. 40. ITNA 7 3 SHE 01 32.5 1.5 NAA 76HAN 01 550. 80. ITNA 76WEW 01 32.7 3.4 ITNA 75NAD 02 670. 20. ICPES 81CHU 01

33. 4. ITNA 7 3 ABE 01 690. 40. ITNA 75NAD 02

33. ICPES 80NAD 01 690. 40. ITNA 78NAD 02

11. f. ITNA 80BUA 01 700. AA 82GUP 02

123
TABLE V (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

700. 100. 1TNA TOT ATT flO 700. 100. ITNA ~i c nvTT\ n l / 50ND 0

1

740

.

An90

.

T TM A 1 1NA / / L,Ari U 1 760. 30

.

ITNA i/n Ar* n l / OKAL> U 1 780. 70. ITNA 75RUC 01 800. ITNA 7 5MIL 01 810. 20. ITNA 77MAE 01 840. 70. ITNA 77ROW 03

840. 70. 5 ITNA 77ROW 04

880. 90. 5 ITNA 77R0W 04

910. 70. OES 76WEW 01 950. 50. I ENA 77R0W 04

1000. 200. NAA 76HAN 01 1000. 200. ITNA 78MAC 01 1030. 80

.

ITNA o o cti *7 n 1

1 200

.

inn zOU

.

UNA O 1 WAN U 1

in ^ppm,)

JO

.

i n10 • MANAAA

/ <*UNU U 1 30. 10 . ITNA / jOND 0

1

32. 3

.

ITNA 78NAD 02

32. 8. SSMS 77DON 01 32. 3. ITNA 75NAD 02

33. 3. 9 ITNA 78LAU 02

34. 1. EXRi? 81KIN 01 34. 4 AA 79REI 01 34. ITNA 77WEA 01 34

.

9. ITNA 77CAH 01

34

.

XRF 7 5KLE 01 34

.

1/ . ITNA / OWLW Dl 35

.

5

.

ITNA 77JER Ul

1 c 30 . z . 1 ZT TMA Q O 011*7 n 0 oZaUZ. UZ

5d . 1 o o y .y EXRF 7Qi*t a f"i 1 /y(jLA Ul

1 c5b . ICPES tJUNAL) U 1 Jo

.

/ . o

n A A r AA q 7 orr n 1 o Z d U 1 36 . 0.6 RTNA T / An f j f\ 1 740RV 01

36 .6 1 .4 EXRF 73SPA 01 37. 3. PAA 77JER 01 37. 3. PAA 76CHA 01

37

.

6

.

I ENA 77R0W 04

37 . AA 76WEW 01

37 . 10. NAA 76HAN 01

37 .2 17 .4 ITNA 75RUC 01

37 .5 2.8 PAA v a m a r» i U

1

1QJo . cJ . C CMC 7 7TJ ATT A 1 / / r AU U

1

1ft JO • \JYVV R9MT1 O i_ 1 I i Li Ul01 38 .

1

1 .4 RTNA 7 7TER 01

38 1

1

0.8 AF 75EPS 01

1ft JO A ii

.

AA

1ft JO . A4 AA 74RAI 01

1ft JO - Js AA 78niIT 01

jy

.

1I . 7 AAA A 77TAT / J IrvLi 01U J 39. 2. ITNA 82SUZ 02

39. 3. PAA 80SEG 01

39. EXRF 82KEE 01 39. ICPES 80NAD 01

39. 1

.

FAA 74TAL 01 39. 6. D* ITNA 77ROW 04

39. 3. 6 PAA 82SEG 01

39. 6. ITNA 77ROW 03

40. 1 .2 ICPES 81CHU 01

TABLE V (cont)

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

40.8 4

.

ITNA O 1 WAIN U 1 42. ITNA / /(jLU U 1 43. 2

.

ITNA /DRAG Ul 45. 17 . nrc OLb / owtw U

1

50. 10

.

ITNA TQT /oUAUATI mUZ

52. 4 . TTWA 7QMAT 01 58. 1 • * TTMA 7 7MAF 01

?pm)

i fin IENA 77ROW 04

i JU» L* ITNA 77R0W 04

1 .56 0.14 * PAA 74CHA 01

16 . 2. PAA 76CHA 01 25. 0.75 ICPES 81CHU 01

25. 3. OES 76WEW 01 28. 24. ITNA 76RAG 01

33. 4. EXRF 79GIA 01

38. 34 WXRF 82 MIL 01 40. 4. 9

' ITNA 78LAU 02

41. ITNA 7 5MIL 01 45. ITNA 75KLE 01 46. AA 76WEW 01 85. 9. *12 ITNA 82SUZ 02

90. 10. * ITNA 82SUZ 02

124
TABLE W

NBS SRM 1632A—COLLECTED DATA TABLE W (cont)

CONC

Ag (ppb)

UNCER COMMENT

ANAL

METH

REF CODE

REF NUM

3000. L* WXRF 82MIL 01 300. ITNA 79CAH 01

Al (%)

2 .8 0.27 CPXRF 80KIR 01 2.9 0.05 TCGS 7 9AND 01

2.9 0.3 ITNA 80GER 01 2.93 0.03 AA 82NAD 02

2 .95 0.04 XRF 79CAH 01

2 .99 0.14 ITNA 83GLA 01

2 .99 0.06 ITNA 820BR 01

3. 0.05 ICPES 82NAD 02

3.01 0.13 D* TCGS 80GER 01 3.01 0.13 D* TCGS 80AND 01

3 .01 0.13 TCGS 79FAI 01

3 .07 0.13 ITNA 80GAR 01

9.47 EXRF 82EBD 02

As (ppm)

0 .4 L . 1 * CPXRF 80KIR 01

7 A * 1 1 FAA 8?FBD 02

0.4 1 1 FA A U L 8 .88 1 1 o

1 .11 O 1 1NALI U 1 9

.

ft /. 0.4 T TM A U 1 9. 0.4 ITNA 81KUL (J 1 9. n FAA 82EBD 02

9.2 34 WXRF 82MIL 01 9.27 AF 82WIL 01 9.34 FAA 82WIL 01 9.4 1.3 ITNA 79CAH 01 9.4 1.3 ITNA 820BR 01 9.54 0.64 HAA 82 NAD 01

9.6 11 FAA 82EBD 02

9.8 11 FAA 82EBD 02

9 .9 0.5 PAA o Af^i? D oUGLR a i U 1 10.2 0.4 ITNA 81JIN 01

11. 2. * ITNA 80GER 01

Ash (Z)

21.7 UU 82EBD 02

21.8 34 CB 82MIL 01

Au (ppb)

C ft 50. ITNA / 7 UAH n 1

3. 1. ITNA 80KOS 01

B (ppm)

22. 3. * ICPES 81NAD 01 50.9 0.5 TCGS 79AND 01 52- 19- ITNA 82SCH 05

52.7 1.8 TCGS 79FAI 01

53. 2. D* TCGS 80GER 01 53. 2. TCGS 80AND 01 55. 4. 35 TCGS 81GLA 04

CONC

Ba (ppm)

UNCER COMMENT

ANAL METH

REF REF CODE NUM

7500. L* ITNA 80T0U 01 100. 13. ITNA 81JIN 01

1 16

.

7

.

5 ITNA 80TOU 0

1

120. 10. ICPES 82 NAD 02

122. 11. ITNA 80GER 01

125. 34 WXRF 82 MIL 01

138. 20. ITNA 79CAH 01 150. 26. ITNA 80GAR 01

Bi (ppm)

1

.

L* WXRF 82MIL 01

Br (ppm)

550. L* ITNA 80TOU 01

39 .6 1 .9 ITNA 820BK Ul 40. 2. ITNA 83GLA 01 41. 4. ITNA 80GER 01 42. 34 WXRF 82MIL 01 43. 0.6 ITNA 81JIN 01 43. 7. ITNA 79CAH 01

4 3. TCP DHtATt ft 1 HI NAD 01 44.5 2.7 5 I ENA 79GLA 02

/. /. ft 44 .V A ft 0.9 5 IENA 7flnt I ft 1 /•JGLA 02

50. 4. *5 ITNA 80T0U 01

c (%)

62.7 0.06 CB 80SCH 02

65. 4. TCGS 79AND 01 71. 4. D* TCGS 80GER 01

71 . 4. D* TCGS 80AND 01

71

.

4. TCGS 79FAI 01

Ca (ppm)

2100. 100. PAA 80GER 01

L ZUU • inn T TW A 1 1 IMA oipi a n

i

2300. 30. AA 82NAD 02

Z jUU • inn 1UU . Arvr 70 cap ni / y uAn V 1 2400. 200. D* TCGS 80GER 01 2400. 200. D* TCGS 80AND 01 2400. 200. ITNA 80GER 01 2400. 30. ICPES 82NAD 02

2400. 200. TCGS 79FAI 01

2400. 200. D* TCGS 7 9 AND 01 2450. 140. ITNA 820BR 01 2700. 175. ITNA 80GAR 01 46500. * EXRF 82EBD 02

Cd (ppb)

600. L* AA 79CAH 01 4000. L* WXRF 82MIL 01 150. 30. TCGS 79AND 01 200. 50. ITNA 80KOS 01 210. 30. D* TCGS 80AND 01 210. 30. D* TCGS 80GER 01 210. 30. TCGS 79FAI 01

125
TABLE W (cont) TABLE W (cont)

CONC

Ce (ppm)

25.7

26. 27.

27.

28.5

28.5

31.1

32.

32.

CI (ppm)

700.

750.

760.

766.

770.

776.

784.

784.

784.

800.

897.

Co (ppm)

56

6

6

6

6

6

7

Cr (ppm)

.86

.55

.668

5

26.

26.

33.3

34.

36.

36.

36.

39. 40.

Cs (ppm)

1.9

2.2.3

2.4

2.4

2.5

2.5

UNCER

7.2

1.7

4.4.0.3

0.4

3.4

COMMENT

ANAL

METH

REF REF CODE NUM

100. 60.

30. 48.

36.

17.

17.

17. 70.

23.

250.

0.21

3.

6.1.6

2.

2.

6.3.5

8.8

0.6

0.3

0.11

0.8

0.2

0.2

34

34

D*D*

L*

34

34

34

CPXRF

ITNA

ITNA ITNA

ITNA ICPES

ITNA WXRF

ITNA

XRF ITNA WXRF

TCGS

ISE ITNA

TCGS

TCGS

TCGS

ITNA

ITNA

ITNA ITNA

WXRF ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

ITNA ITNA

CPXRF AE+AF

WXRF

ITNA

ITNA

ITNA

ITNA

ITNA WXRF

IENA

80KIR 01 79CAH 01

81KUL 01 80KOS 01 81JIN 01

82CR0 01 80GAR 01

82 MIL 01 80GER 01

79CAH 01 83G1A 01

82MIL 01

79AND 01

81NAD 01

820BR 01 80GER 01 80AND 01 79FAI 01 80GER 01 80GAR 01

80T0U 01

81JIN 01 82MIL 01

80GER 01 81KUL 01

80TOU 01

80GAR 01 80KOS 01 79CAH 01

81KUL 01 80K0S 01 81JIN 01 80GER 01 79CAH 01 80GAR 01 80KIR 01 82G0L 01 82MIL 01

79CAH 01 80GER 01 81JIN 01 80GAR 01 81KUL 01

82MIL 01 80KOS 01

CONC

Cu (ppm)

15.9

16.

17. 17.2

Dy (ppm)

1.83

1 .98 2.1

2.2

2.2

2.56

Er (ppm)

0.91

Eu (ppb)

460.

490.

510.

510.

540.

540.

550.

550.

F (ppm)

84.

95.

UNCER COMMENT

ANAL

METH

REF CODEREF NUM

Fe (%)

.07

.1.1.11

.11

.11

.11 .12

.12

.12

.14

.16 .16

.17 6.78

Ga (ppm)

0.4

21

2.5

0.11

0.53

0.1

0.1 0.3

0.26

3.0.05

1000.

20.

10. 82.

30. 80.

80.

30. 30.

7.2

7.84

8.

0.03

0.06

0.02

0.06

0.06

0.02

0.06

0.01

0.01

0.09

0.01

0.03

0.37

0.04

2.5

0.6

0.8

34

L*

5

L*

L*

D*

D*

AA

CPXRF

WXRF

FAA

WXRF ITNA

ITNA ICPES

ITNA

ITNA ITNA

WXRF

ICPES

WXRF

ITNA ICPES ITNA

ITNA

ITNA ITNA

ITNA

ITNA

ISE

ISE

XRF ITNA

ITNA

TCGS

TCGS

AA

TCGS

ITNA ICPES

ITNA AA

ITNA

ITNA

TCGS EXRF

CPXRF

ITNA ITNA

79CAH 01 80KIR 01 82MIL 01 80LAN 01

82MIL 01 820BR 01 80TOU 01 82CRO 01 79CAH 01 80GER 01 80GAR 01

82MIL 01 82CR0 01

82MIL 01 820BR 01 82CRO 01

80GAR 01 81JIN 01

80K0S 01 81KUL 01

79CAH 01 80GER 01

81 NAD 01 83KNA 01

79CAH 01 81KUL 01 81JIN 01

80GER 01 80AND 01

82 NAD 02

79FAI 01 80K0S 01 82NAD 02

80GAR 01 79CAH 01 80GER 01 79CAH 01 79AND 01

82EBD 02

80KIR 01 820BR 01 80GER 01

126
TABLE W (cont) TABLE W (cont)

CONC

8.4

8.5

Gd (ppm)

1.9

1.95

1.95

2.4

3.

3.

Ge (ppm)

2.5

UNCER COMMENT

34

H (%)

68

77

717 H20-T (%)

1.62

Hf (ppm)

1.44

1.55

1.7 1.8

1.9

Hg (ppb)

118.

120.

134.1

134.1

135.

170.

210.

Ho (ppb)

380.

I (ppm)

0.9

1.77

1.8

0.8

0.2

0.03

0.03

0.2

0.05

ANAL

METH

WXRF

ITNA

REF REF CODE NVM

82MIL 01 79CAH 01

0.07

0.1

0.1

0.1

0.01

2.3.8

0.09

0.08

0.1 0.3

0.3

1500.

14. 50.

3.1

18. 20. 90.

2000.

50.

D*

34

34

D*

D*

L*

L*

L*

L*

34

TCGS

TCGS

TCGS

ICPES

TCGS

WXRF

WXRF

TCGS

TCGS

TCGS

TCGS

CB

0.2

FD

WXRF

ITNA ITNA

ITNA

ITNA ITNA

ITNA

WXRF

CVAA

ITNA CVAA

AF

CVAA

CVAA

ITNA

WXRF

ICPES

WXRF

IENA

ITNA

79AND 01 80GER 01 79FAI 01 82CRO 01 80AND 01 82MIL 01

82MIL 01

7 9AND 01

80GER 01 80AND 01 79FAI 01

80SCH 02

80KHA 02

82MIL 01 80T0U 01 81JIN 01 80GER 01 79CAH 01 80GAR 01 80T0U 01

82MIL 01 80NAD 01

80K0S 01 82EBD 01 82WIL 01

82D00 01 81NAD 01

81KUL 01

82MIL 01

82CR0 01

82MIL 01 83GLA 01 80GER 01

CONC

In (ppb)

36.

36. 40.

K (ppm)

3700.

3800.

4000.

4100.

4100.

4200.

4200.

4200.

4200.

4200.

4200.

4 300.

14900.

La (ppm)

10.9

12.8

13.03

14.5

15. 15.1

18.

19.

Li (ppm)

36.2

Lu (ppb)

134.

150.

180.

180.

190.

220.

Mg (ppm)

600.

990.

1020.

1300.

1400.

19900.

Mn (ppm)

20.

26.

28.

UNCER

1000.

4.

3. 10.

50. 200.

100. 200-

200.

200.

200.

200.

150.

200.

645.

0.5

0.5

0.3

0.2

2.6

1.2

2.

0.1

2000.

13.

10. 70.

30. 20. 40.

300.

40.

10. 300.

220.

4.3

6.

COMMENT

L*

ANAL

METH

REF REF CODE NUM

D*D*

34

L*

WXRF

ITNA

ITNA ITNA

XRF ITNA

ITNA TCGS

ICPES

TCGS

TCGS ITNA

TCGS

AA

ITNA

ITNA

EXRF

ITNA

ITNA ITNA

ICPES ITNA

ITNA ITNA

WXRF

34

AA

WXRF

ITNA ICPES ITNA

ITNA

ITNA

ITNA

XRF AA

ICPES

ITNA

ITNA

EXRF

CPXRF

AE+AF

WXRF

82MIL 01 80GER 01 820BR 01 79CAR 01

79CAH 01 820BR 01 81JIN 01

7 9 AND 01 82NAD 02

SOGER 01 80AND 01 80GER 01 79FAI 01 82NAD 02

79CAH 01 80GAR 01 82EBD 02

80K0S 01 820BR 01 81JIN 01 82CRO 01 80GAR 01 79CAH 01 80GER 01 82MIL 01

79CAH 01

82MIL 01

80KOS 01 82CR0 01 80GAR 01 80GER 01 81JIN 01 79CAH 01

79CAH 01 82NAD 02

82NAD 02

80GER 01 80GAR 01 82EBD 02

80KIR 01 82GOL 01 82MIL 01

127
TABLE W (cont) TABLE W (cont)

CONC

29. 29.

29.

29. 31.5

32.

32. 33.7

34. 720.

Mo (ppm)

UNCER

N (Z)

1.19

1.2

26

27

27

27

1

1

1

1

Na (ppm)

680.

720.

760.

800.

810.

825.

850.

860.

884.

940.

1025. 4450.

Nb (ppm)

4.

Nd (ppm)

10.

11.

1 1 .8 11.8

13. 15.6

Ni (ppm)

15.7

18.

19. 19.4

20.4

22.

23.

26.

5.

1.5.

5.1.1

3.9.1.2

COMMENT

D*

0.08

0.1 0.03

0.08

0.08

0.08

38. 40.

160. 50.

30.

40.

32. 260.

125.

0.4

0.4

0.1

3.7

D*

L*

34

D*

D*

34

34

34D*

ANAL

METH

TCGS ITNA

TCGS

TCGS

ITNA ITNA

ITNA

ITNA ICPES EXRF

UF KEF CODE NUM

80GER 01 83GLA 01 80AND 01 79FAI 01 820BR 01 80GER 01 79CAH 01 80GAR 01 82NAD 02

82EBD 02

34

*

ITNA WXRF

CHEML

TCGS

CBTCGS

TCGS TCGS

ITNA

ITNA

ITNA AA

ICPES WXRF

ITNA

ITNA ITNA

XRF

ITNA

EXRF

WXRF

ITNA

WXRF

TCGS TCGS ICPES

ITNA

AA

CPXRF AE+AF

ITNA FAA

WXRF

ITNA PAA

79CAH 01 82MIL 01

81 NAD 01 79AND 01 80SCH 02

80AND 01 80GER 01 79FAI 01

79CAH 01 820BR 01 83GLA 01 82NAD 02

82NAD 02

82MIL 01 80GER 01 81JIN 01 80GAR 01 79CAH 01 82SCH 05

82EBD 02

82MIL 01

80GER 01 82MIL 01 80AND 01 79FAI 01 82CR0 01 81JIN 01

79CAH 01 80KIR 01 82G0L 01 81JIN 01 80LAN 01 82MIL 01 79CAH 01 80GER 01

CONC

0 (2)

18.31

18.4

19.8

P (ppm)

85.

205.

280.

280.

280.

1310.

Pb (ppm)

6.9

8.3

12.4

13. 15.3

Pb-21 (PCi)

0.449

0.449

Pr (ppm)

3.3.3

Rb (ppm)

28.2

29.

29. 29.

29.

29.

29.

30.

34.

UNCER COMMENT

ANAL

METH

R£F REF CODE NUM

S (%)

1.19

1.48

1 .59 1.59

1.59

1.59 1.6

1 .62

Sb (ppb)

410.

530. 530.

0.23

0.7

0.3

17.

80.

50.

0.9

1.9 0.4

2.5

0.024

0.024

0.1

410.

1.1

1.5.

5.5.

1.2.4.6

0.01

0.07

0.02

0.02

0.09

0.02

0.07

150.

50.

50.

34

35

*34

34

D*

34

L*

34

D*

D*

14NAA

14NAA

14NAA

ICPES WXRF

XRF AA

ICPES

EXRF

ICPES

CPXRF HAA

WXRF AA

NM NM

WXRF

ICPES

ITNA

ITNA WXRF

ITNA

ITNA

ITNA IENA PAA

ITNA

CPXRF

XRF

XRF

TCGS

TCGS

TCGS TCGS

CPXRF

UU

HAA

ITNA

ITNA

80KHA 02 80NAD 01 80KHA 02

81NAD 01 82MIL 01 79CAH 01 82NAD 02

82NAD 02

82EBD 02

81NAD 01 80KIR 01 82NAD 01 82MIL 01 79CAH 01

81 CAS 01 80CAS 01

82MIL 01 82CR0 01

80T0U 01 81JIN 01 82MIL 01 80GER 01 81KUL 01 80T0U 01 80KOS 01 80GER 01 79CAH 01 80KIR 01

79CAH 01 81NAD 01 80GER 01 80AND 01

7 9 AND 01 79FAI 01 80KIR 01 82EBD 02

82NAD 01 80KOS 01 81KUL 01

128
TABLE W (cont) TABLE W (cont)

CONC UNCER COMMENT

ANAL

METH

REF REF CODE NUM

600. 90. ITNA 80GER 01 620. 80. ITNA 81 JIN 01 690. 50. 5 ITNA 80T0U 01 800. 50. ITNA 79CAH 01 1000. *34 WXRF 82MIL 01

(ppm)

5.3 1.2 * CPXRF 80KIR 01

6. 0.3 ITNA 81KUL 01

A 9 n 9 u • Z ITNA 79CAH 0 1

c. 9 34 WXRF 82MIL 01 6.3 0.2 5 ITNA 80TOU 01 6.3 0.1 ITNA 80KOS 01- 6.56 0.23 ITNA 80GAR 01 6.7 0.05 ITNA 81 JIN 01 6.8 0.6 ITNA 80GER 01 6.9 0.9 5 ITNA 80T0U 01

(ppm)

9 A L .4 34 WXRF 82MIL 01

ftU.J DTM K1NAA QftVM A U

1

9Z • ^7J / U.Uj T CM A A I U i 9Z • JO T7A rAAA oz Wl L u 1 9Z . 33 A I" Ar Q9LTTT OZ W1L U

1

2 .6 0.3 ITNA 80GER 01

3

.

0.1 ITNA 79CAH 01 3.12 0.17 * HAA 82NAD 01

(%)

3.1 0.14 * CPXRF 80KIR 01 5.8 0.1 D* TCGS 80AND 01 5.8 0.1 D* TCGS 80GER 01 5.8 0.1 TCGS 79FAI 01 5.92 0.01 XRF 79CAH 01 6.05 0.2 TCGS 79AND 01 6.09 0.07 ICPES 82NAD 02 6.21 0.08 AA 82NAD 02

27.79 * EXRF 82EBD 02

(ppm)

1 10

.

ITNA 80TOU 01

1 .1 0.1 * ITNA 80KOS 01

1 .9 0.1 5 ITNA 80T0U 01

2. 34 WXRF 82MIL 01

2.1 0.07 D* TCGS 80GER 01 2.1 0.07 D* TCGS 80AND 01

2.1 0.07 TCGS 79FAI 01

2 .1 0.05 TCGS 7 9 AND 01

2.5 0.4 ITNA 80GAR 01 2.57 0.09 ITNA 81JIN 01 2.6 0.1 ITNA 79CAH 01 2.6 0.1 ICPES 82CR0 01 2.62 0.13 ITNA 820BR 01 2.8 0.3 ITNA 80GER 01

(ppm)

1

.

34 WXRF 8 2 MIL 01 8.08 1.02 HAA 82NAD 01

CONC

Sr (ppm)

83.6

84.

90.

91

.

95.5

Ta (ppb)

390. 400.

450.

Tb (ppb)

290.

300.

320. 330.

Te (ppb)

500.

Th (ppm)

3.1 4.2

4.2

4.3

4.3

48

8

8

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

44

4,5. Th (ppm)

12

2

3

348

88

Th-228 (PCi)

0.499

0.499

Th-2 30 (PCi)

0.452

0.452

7.8 ITNA 820BR 01

9. ITNA

18. 34 WXRF 82MIL 01 ITNA 79CAH 01 11.8 ITNA 81JIN 01

2000. L* WXRF 82MIL 01 50. ITNA

30. ITNA 80GER 01 50. ITNA 81JIN 01

2000. L* WXRF 82MIL 01

30. ITNA 81JIN 01 100. ICPES 82CRO 01 50. ITNA 80GER 01 40. ITNA

/

79CAH 01

600 L* WXRF 82MIL 01 50. HAA 82NAD 01

1600. L* ITNA 80TOU 01 0.5 * CPXRF 80KIR 01 0.3 ITNA 79CAH 01 0.2 5 ITNA 80T0U 01 0.9 ITNA 81KUL 01 0.3 ITNA 80KOS 01 0.04 ITNA 81JIN 01 0.2 ITNA 80GER 01 0.6 ITNA 80GAR 01 WXRF 82MIL 01

1600. L* ITNA 80T0U 01 0.5 * CPXRF 80KIR 01 0.3 ITNA 79CAH 01 0.2 5 ITNA 80TOU 01

u .y ITNA OlKUL Ul

U • j T TM A 1 1NA oUKOb Ul 0.04 ITNA 81 JIN 01 0.2 ITNA 80GER 01 0.6 ITNA 80GAR 01

34 WXRF 82 MIL 01

0.011 D* NM 81 CAS 01 0.011 NM 80CAS 01

0.017 D* NM 81 CAS 01 0.017 NM 80CAS 01

129
TABLE W (cont) TABLE W (cont)

CONC

Th-2 32 (PCi)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM CONC UNCER COMMENT

ANAL

METH

A A Q A A nto Dw VTU NM O 1 C AC HI LAb A 1 U 1

r» a o a U.Ulo MM OUCA& A 1 U 1

Ti (ppm)

1480. 30. TCGS 79AND 01

1550. 40. D* TCGS 80GER 01 1550. 40. D* TCGS 80AND 01 1550. 40. TCGS 79FAI 01

1600. 40. ICPES 82NAD 02

1600. 34 WXRF 82MIL 01

IbzU

TTMA oZUdK U 1 1630. 70. ITNA 80GER 01 1700. 300. CPXRF 80KIR 01 1720. 170. ITNA 80GAR 01 1760. AA 82NAD 02

1800. i n a 100 . VDTJ XRr TO A All a ^ 5990. EXRF 82EBD A 1 uz n i ppm;

1 • T *Li WAKr Q*?MTT OZIllL U 1

Tin f nnk^

1000. L* WXRF 82MIL 01 400. 100 ill L D n i

U ( DPm)

62. L* ITNA 80TOU 01

1. *34 WXRF 82MIL 01

1.1 0.2 ITNA 79CAH 01

1.12 0.4 ITNA 81KUL 01

1 .16 0.11 ITNA 81JIN 01

1 .2 0.1 5 ITNA 80T0U 01

1 .21 0.1 ITNA 80GER 01

1 .24 0.1 I ENA 81KUL 02

1 .24 0i04 I ENA 80KOS 01

1 . uaA o j\j U\ U 1 1.28 0.08 DNA 80GAR 01 1.3 0.1 35 DNA 81GLA 04

1.3 0.11 ITNA 820BR 01

1 .45 0.05 *35 DNA 81GLA 03

U-234 (PCi)

0.448 0.012 NM 8 OCAS 01 0.448 0.012 D* NM 81 CAS 01

U-235 (FCi)

22.8 1.9 NM 80CAS 01 22.8 1.9 D* NM 81 CAS 01

U-238 (PCi)

0.444

0.444

V (ppm)

42.

43.

43.4

44.

45.

46.

46.

46.9

48.

W (ppb)

600.

780.

890.

1000.

Y (ppm)

5.8

8.3

9.5

Yb (ppm)

0.9

0.98

0.98

1.1 1.2

Zn (ppm)

24.3

27.

28.

28.

30.

31.

Zr (ppm)

47.

55.

57.

0.016

0.016

4.2

1.8

3.2.

8.2

2.5

7.

1500.

200.

230.

150.

300.

0.5

0.5

2200.

2.0.01

0.08

0.07

0.1

0.1

4.

6.3.7

3.

6.

6.

5.

D*

34

34

L*

34

NM

NM

REF REF CODE NUM

80CAS 01

81 CAS 01

34

FAA

WXRF

ITNA

ITNA ITNA AE+AF

CPXRF ITNA AE+AF

WXRF

ITNA ITNA

ITNA

ITNA

PAA

ICPES

WXRF

ITNA WXRF

ICPES

ITNA ITNA

ITNA

ITNA

AA

ITNA

CPXRF

WXRF

ITNA ITNA

ITNA

WXRF

PAA

80LAN 01 82MIL 01

820BR 01 80GER 01 83GLA 01 82GOL 01 80KIR 01 80GAR 01 82G0L 01

82MIL 01 80GER 01 820BR 01 81JIN 01 79CAH 01

80GER 01 82CR0 01 82MIL 01

80TOU 01 82MIL 01 82CRO 01 80GER 01 81JIN 01 80T0U 01

79CAH 01

79CAH 01 79CAH 01 80KIR 01 82MIL 01 80K0S 01 80GER 01

80GER 01 82MIL 01

80GER 01

130
TABLE X

TABLE X (cont) NBS SRM 1633—COLLECTED DATA

ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

(ppb) 50. *6 SSMS 78GUI 01

54. 1. IENA 7 8 WAN 01 400. L* PAA 76CHA 01 54. 3. ITNA 78MAC 01 4000. L* EXRF 77GIA 01 54. ITNA 75KLE 01 1000. L* OES 76WEW 01 55. 10. ICPES 81CHU 01 300. L* ICPES 81CHU 01 55. FAA 78GUI 01 100. D* ITNA 78RYA 01 55.8 1.4 H AE+AF 77FEL 01 600. L* IENA 80GLA 03 56. ICPES 80FL0 01 100. L* ITNA 77CHA 01 56. 1. H FAE 79FEL 01 500. L* UU 80HEN 01 56.6 3.6 ITNA 81 WAN 01 400. D* PAA 77CHA 01 57. 3. 35 NAA 81GLA 03

258. 20. RTNA 77NAD 02 57. ICPES 82NYG 01 350. AA 76WEW 01 57. 4. ITNA 750ND 01 1320. 130. PAA 74CHA 01 58. 1. 35 RTNA 78GLA 02

58. 4. D* NAA 740ND 01

(%) 58. 4. FAA 78HAY 01 58. 2. IENA 76STE 05

10.4 0.6 * ITNA 78MAC 01 58. 1. ITNA 76BLO 01 10.96 0.402 * ITNA 73SHE 01 58.1 1.6 RTNA 81 GAL 02

11.6 ICPES 8 ONAD 01 58.1 1.6 RTNA 81GAL 01 11.7 2. XRF 79SMI 01 59. 2. 35 VV 81GLA 04

1 1.8 0.8 ITNA 76BLO 01 59. 4. D* ITNA 78RYA 01

12. 1

ITNA 760ND 01 59. 3.5 HAA 77SMI 01 12.1 0.5 ITNA 76RAG 01 59. 4. ITNA 77CHA 01 12.2 0.5 14NAA 81WIL 02 59. ITNA 78WEA 01 12.2 0.3 ITNA 77MAE 01 59.1 4.8 IENA 77ROW 04

12.3 0.6 D* ITNA 78RYA 01 59.8 2. IENA 77ROW 03

12.3 35 TCGS 78GLA 04 60. 3. GCMES 75TAL 01 12.3 0.5 ITNA 76WEW 01 60. UU 80HEN 01 12.3 0.6 ITNA 77CHA 01 60. 2.6 D* PAA 77CHA 01 12.35 0.25 ITNA 77ROW 03 60. 2.6 NAA 77JER 01 12.35 0.25 ITNA 76STE 05 60. 2.6 PAA 76CHA 01 12.4 0.7 35 ITNA 81GLA 03 60.4 0.8 35 IENA 80GLA 03

12.5 ITNA 75KLE 01 60.7 2.6 PAA 74CHA 01 12.5 0.3 ICPES 80NAD 01 61 . 5. ITNA 73ABE 01 12.6 0.4 ITNA 7 3 ABE 01 61. 4. ITNA 760ND 01 12.6 0.2 D* TCGS 80AND 01 61. 3. RTNA 740RV 01 12.6 0.1 35 ITNA 81GLA 02 61 .5 2.4 ITNA 77R0W 04

12.6 0.2 TCGS 79FAI 01 61 .5 3. PAA 750ND 01 12.6 0.7 AA 760ND 01 62. XRF 78CAM 02 12.7 0.05 FAA 77PIL 01 63. 4

FAE 80DSI 01 12.7 AA 79SIL 01 63. 4. PAA 80SEG 01 12.7 UU 80HEN 01 63. 4. 6 PAA 82SEG 01 12.7 0.5 ITNA 750ND 01 63. 7. EXRF 77GIA 01 12.7 OES 80WAL 01 63. 4. 6 PAA 82SEG 01 12.7 ITNA 78WEA 01 63.7 3.6 HAA 82 NAD 01 12.8 0.3 ITNA 78LAU 02 64. 2. ITNA 78LAU 02

12.8 ROFT n O 1 64. 4. ITNA 76RAG 01 12.99 0.47 oi L>nu u i 64. 1. PAA 76KAT 03

1 J< Z .0 OES 76WEW 01 65. 1

PAA 76KAT 02

13. 0.2 TCGS 7 9AND 01 66. 1

XRF 79 SMI 01

13.6 0.5 14NAA 81WIL 01 66.3 10 .

FAA 82 BEN 01

14. 1. AA 80ST0 02 b 1 .0 U.D ITNA 75NAD 02

14. OES 78SUG 01 68. 6. ITNA 78NAD 02

14.1 2.8 * ITNA 81 WAN 01 68. 12. 14NAA 81WIL 02

14.3 1 1 * ITNA 78NAD 02 68. 15. ITNA 76WEW 01 14.3 1.1 * ITNA 75NAD 02 68. 12. 14 NAA 81WIL 01 69.5 7.6 ITNA 7 3 SHE 01 (ppm) 72. *6 SSMS 78GUI 01

46. * ITNA 78KEL 02

49. 5. * ITNA 76KUC 01

131
TABLE X (cont) TABLE X (cont)

ANAL MF EEF CONC UNCER COMMENT METH CODE NUM

i (PP">)

innnn JUUUU

OES 7 fiWFU 0 1 8000. L* 14NAA 81WIL 01

300. L* ICPES 81CHU 01 500. L* UU 80HEN 01

2.75 0.2 RTNA 77NAD 02

4 .84 0.13 RTNA 7 7 NAD 01 8. 2

D* ITNA 78RYA 01

8. 2. ITNA 77CHA 01 1700. * ITNA 78WEA 01

(ppm)

100. * UU 80HEN 01 320. COLOR 79DAL 01 340. OES 79DAL 01 Trppc J. \sF Lj D 433. 4. D* TCGS 80AND 01 433. 4. TCGS 79FAI 01

443. .5. TCGS 79AND 01 450. 20. ICPES 820WE 01 490. 14. 6 TCGS 7 6GLA 01 492. 13. 6 TCGS 76GLA 01

49 7. 14. 6 TCGS 76GLA 01 500. 29. OES 76WEW 01

. (ppm)

1800. * XRF 76WEW 01 2100. 100. * 14NAA 81WT1 Ul nib 01W

9 **AA i JUU • 1UU • A A 7 tflHTl A 1 9 ^7 A z 51 U • Q rtMAn A 1 OUNAD Ul

z^y u.

TUNA TM A "7 CUTT A 1 /_>nlL Ul

9 ^ nn £ JUU. 9^Z A J U . T TMA o

Q 1 MA M A 1 1 WAIN U 1 9 ^ aa TT1T U U

ftAPTTM oUHEJN A1Ul 2500. 300

ITNA

251050. IENA 77ROW OU

2510. 200. ITNA 760ND 01 2510. 160. ITNA 76RAG 01

2520. AA 79SIL 01 2540. XRF 78CAM 02

2540. 51

IENA 76STE 05

2540. 50. IENA 77R0W 03

2550. 110. 14NAA 81WIL 02

2550. 30. ITNA 77R0W 04

2580. 17 0ITNA 7ftCTf AS

zo9 a aauu • 1 / u • cJ

TTTMA IXIN A OUuLA Q Ar*T A AUJ^ 9£ aa Zb Uu •

1 & A lb U •

13rAAA A

/ OU1A U 1 ZD9 A nnuu

JUL) . TL TMA UNA 7QT ATT A 9 / OLiAU U Z

9ZDA noUU . ID U . n* PArAAA 77mA / / VjIIA niU 1 2610. 2 10

PAA 74CHA 01 26 30. 20. XRF 79SMI 01

2660. 150. ITNA 83GLA 01 2670. 85. EXRF 77GIA 01 2700. ITNA 78WEA 01 2700. 200. ITNA 78NAD 02

2700. 200. ITNA 750ND 01 2700. 200. ITNA 75NAD 02

2710. 190. ITNA 77CHA 01 2710. 190. D* ITNA 78RYA 01 2720. 80. 5 IENA 80GLA 03

ANAL KEF R£F CONC ' UNCER COMMENT METH CODE NUM

27 34. 167. ITNA 7 3 SHE 01

27 50. 140. 5 IENA 80GLA 03

2780. ITNA 75KLE 01 2800. 100. 35 ITNA 81GLA 03

2800. ICPES 80FLO 01

2800. 100. 9 ITNA 78LAU 02

2800. 200. 35 ITNA 81GLA 02

2840. 180. 35 NAA 81GLA 04

2880

i nn TTNA l una 7 7MAT7 / / FIAT. nU t

90 A A 1 9A 1 ZU . Bl A 7 £r\T.Tf / OOWfc A 1 U

90 AA Z? UU . 9 A A ZUU

5 IENA 80GLA 03

3000. 600. OES 76WEW 01 3200

400. it ITNA 78MAC 01 3400. 400. * ITNA 7 3 ABE 01

( DPm)

5. * UU 80HEN 01 10.1 *6 FAA 7 9 GEL 0

10.9 ICPES 80NAD 01

11. ICPES 80FLO 01 11. OES 78SUG 01

12. AA 79SIL 01

12. 1. 35 FAA 76GLA 02

12. AA 76WEW 01 12. 0.8 FAA 750WE 01

12.1 6 FAA 79GEL 01 12.3 0.3 FAA 760WE 01

12.4 0.31 AA 74RAI 01

11 9£ ft . D AU . 9Z D^ c t mil n i U

I Z .D £D

T?A rAAA 70/"TT

/ 7btiL A 1 u 1

11 9£ f, . D AU O^ AAA A 7 £A\TT\ A 1 U 1 1^9 1 J . Z £

0

T? A A rAA 79GEL A 1 01

13.5 6 FAA 7 9 GEL 01

14. 0.95 * OES 76WEW 01

(ppm)

1 . L* PAA 76CHA 01

1

D* PAA 77CHA 01

10. L* OES 7 6WEW 01

0.7 UU 80HEN 01

1 .08 PAA 74CHA 01

(ppm)

10. L* IENA 80GLA 03

5.8 0.8 35 IENA 79GLA 02

6. 2. EXRF 77GIA 01

6. ITNA 75KLE 01

6. 1

ITNA 78MAC 01 6.4 0.2 35 ITNA 81GLA 03

6.5 0.2 5 IENA 80GLA 03

6.7 0.6 ITNA 76RAG 01

6.9 0.3 35 NAA 81GLA 04

7. 1. ITNA 78LAU 02

7.5 0.5 ITNA 78NAD 02

7.52 0.46 ITNA 75NAD 02

7.7 1.5 IENA 76STE 05

8.4 1.5 IENA 77R0W 03

9.2 0.6 ITNA 77ROW 04

9.2 0.8 IENA 77ROW 04

9.5 XRF 78CAM 02

132
TABLE X (cont) TABLE X (cont)

CONC UNCER COMMENT

ANAL

METH

REF REF CODE HUM

ANAL KEF REF

10. UU 80HEN 01 11.2 3.5 D* ITNA 78RYA 01 11.2 3.5 tipuA ITNA 77/niA

/ / U1A niU

1Z • A ITNA 7 3ABE 01

12. 4. ITNA 750ND 01

12. ITNA T Of TT* A A 11 78WEA 01 12.1 1.5 ITNA 7 3 SHE 01

\j V*/

3 .05 a0.03ah 79SIL / u/ X AJ 01V/ A 3.3 HIT UU QAHTTN A1

3.45 0.02 GRAV 79SIL 01

Ca (Z)

3.5 * XRF 76WEW 01

3 .8 *35 TCGS 78GLA 04

5 .Vz 0 .Zo » A A PAA O /. /TJ A A 1 /trCHA 01

A4 l . I a or U • jo T<TM A 1 1NA 7 o OHT? A 1 / Jbrih 01

It* . 9Z 1TIT UU 0 AllTTM A1 H . Z nU 9• £ TTMA X XMA 7 An a i / OKAL* U 1 A4

•> 1

• Z X a aq TTM UNAA 7 0H«ri AO / oNAD 0 L

A 11 4 .Z 1 A AO ITNA 75NAD 02

4.3 0.3 35 ITNA 81GLA 02

4.3 AA 79SIL 01 4.3 0.2 AA 760ND 01 4.34 ITNA 75KLE 01 4.4 0.18 UNAA 81WIL 02

4.4 0.4 D* PAA 77CHA 01 4.4 0.4 PAA 76CHA 01 4.4 0.4 ITNA 750ND 01

4.5 a £ 0.0 35 IENA O AOT A AO 80GLA 03

A 5 Q AtTT A A 1 OUFLU Ul

4.5 0.5 D* ITNA

4.5 0.5 ITNA 77CHA 01

U f> U.J ITNA 7AT All 09

H . D / OWe.Lf U 1 A & 0 4.0/ A A£ 0.00 ICPES 80NAD 01

4 .62 0.15 EXRF 78PEL 01 4.65 0.15 ICPES 81CHU 01

4.69 0.14 ITNA 76STE 05

4.69 0.14 ITNA 77ROW 03

4.7 OES 80WAL 01 4.7 0.3 ITNA 77MAE 01 4.73 0.42 ITNA 81WAN 01

4.75 0.08 D* TCGS 80AND 01

4.75 0.08 TCGS 79FAI 01

A Q 4.0 ICPES Q AM An A 1 oONAD 01

A ft U .70 / OWLW U

A. •> u »

AAA A QAOTA AO ouoiu uz

A 0 u • z /7A1ND Ul

i i X . 1 TTMA X XJMA 7AAMT1 /OUNJJ AlUl

5.04 XRF 78CAM 02

5.09 0.56 14NAA 77VAN 01 5.1 0.05 PAA 76KAT 03

5.1 0.6 ITNA 76WEW 01

5.1 0.03 PAA 76KAT 02

5.11 0.13 XRF 79SMI 01 5.3 0.1 EXRF 77NIE 01 5.3 0.5 PAA 750ND 01

CONC ' UNCER COMMENT METH CODE NUM —

(ppm)

4

L* EXRF 77GIA A 1 01

5. L* OES /OWEW A 1 01 0.93 OAT POT D O /""LI O AU 11

1

TTMA XXWA / OWIjW A1U

1 .2 0.2 PA A rAA OU3CA) 01

1 .2 0.04 7 AA 73TAL 01

1 *z n 1 U . 1 O O A A PAA QO cur niKJ 1

1 .2 A t\h 0.04 T?A A

r AA T ATAT /41AXj 01

1 -Z A 0 0 - Z 0 PAA OZSEG nu 11

1 .3 0.25 FAA 760WE A 1 0 1

1 .4 0.16 TCGS 7 9AND A 1 01

1 .43 0.07 RTNA 81GAL 01 1.43 0.04 RTNA 740RV 01 1.43 FAA 78GUI 01 1.43 0.07 RTNA 81GAL 02

1.45 0.04 AA 75EPS 01

1 .46 AE+AF 77FEL 01

1 .46 0.05 AA 74RAI 01

1.5 0.09 7 AA 73TAL 01

1.5 0.1 NAA 77JER 01 1.5 0.07 D* TCGS 80AND 01 1.5 0.5 ICPES 81CHU 01

1.5 0.1 PAA 76CHA 01 1.5 0.07 TCGS 79FAI 01 1.5 0.1 D* PAA 770.A 01 1.5 POL 74MAI 01 1.5 0.15 FAA 7iRAI 01

1.5 0.09 FAA 74TAL 01

1.52 0.08 AF 75EPS 01

1 .52 0.07 PAA 74CHA 01

1 .53 AA 76WEW 01

1 .55 FAA 79SIL A 1 01

1 .6 A 1 C 0.15 7 AE+AF 73TAL A 1 0 1

1 .6 A O O.Z 0 TCGS 76GLA 01 1.6 0.5 ICPES 80EPS 03

1.6 0.15 FAE 74TAL 01

1 .63 0.07 8 SSMS 80K0P 01

1.69 AA 78GEL 01

1 .7 0.2 AA 760ND 01

1 .85 * IDMS 7 5KLE 01 15. * UU 80HEN 01

(ppm)

125. UU 80HEN 01

12910ITNA 7 3 SHE A 1 01

1 io . 5

14 NAA 81WIL Au 1X

1 JO • Q 14 NAA 81 WIL n 0 u z

114UAfi . ICPES 80FLO u 1

1 A A 140

1 A10 • O" ITNA 78RYA AU 1X 140. 1 A10

ITNA 77CHA A 1 01 141

7

ITNA 81 WAN 01 145. 5. ITNA 78LAU 02

145. 6. ITNA 76WEW 01 146. ITNA 82GLA 02

146. 15. ITNA 750ND 01 146. 17. ITNA 760ND 01

148. 7. 35 ITNA 81GLA 02

148. 6. ITNA 76RAG 01

133
TABLE X (cont) TABLE X (cont)

ANAL REF REF ANAL REF REF UNCER CODE NUM CONC tOMMtnl METH CODE NUM

my1 AQ • 7 jj MAI'JA AA ft l r t a n A 40. 2. ITNA 7 3 ABE 01

1myAQ * AH • AKJ7 7 o cmt a 1 40. 2. ITNA 760ND 01

1 AQ A 9Z • n* 1 1NA 7 7 DAt.T A /. 1

KUW Uh 40. 2

D* PAA 77CHA 01 LHy 1 AQ • A0

oZ • T TM A I 1NA 7 7 DAI T AO / /ROW 0 J 40

4

FAA 760WE 01

1 3 U • 0

9. 9. T CM A

l /ROW 04 40.

0.6 ITNA 83GLA 01

15 2. in PA A 7 fxCU A ft 1 40.3 0.4 ITNA 77ROW 01

1 ^ 9 1 3 Z •i a U" tJA A rAA 7 7 «"TJ A A 1 40.3 0.4 D* UNA 7 7TJAU A A / / KUW UH

1

1 J^ ^J« \j . Jj T TNT A 1 UNA Q 1 CT A A 1 Hi. ICPES 80FL0 01

1 J J . oZ . n A A rAA 7 CV AT AO /oKj\i UJ AH 11 •

l TJ. TMA inn 7 AT ATT 0. 9

15 3. 1. PAA 76KAT 02 Hi. J • T TMA 1 liiA 7 AUP U A 1

/ DWC.W \J I

1 J H . a0 . o c 3d IENA 80GLA 03 41

235 TTMA 1 INA Ol PI A A 1

154

XRF 78CAM 02 AHi.1 nu • ao IENA 77R0W 04

157

3.2 ICPES 81CHU 01 Hi. 1 7 1 .z ICPES 81CHU 01

160. 23. EXRF 77GIA 01 41. 1. 35 ITNA 81GLA 02

161

35

ITNA 75NAD 02 /I C 41.5 1 .Z TTMA 7 1AMT. A 1 161. 35. ITNA 78NAD 02 42. 1.6 D* TTMA / OKln. \J 1 169

ITNA 7 5MIL 01 42. FAA 79SIL 01

11 7/ A0 • A TTKT UNAA 7 QMA A A 1 A9**Z . tD . AAA A 7AnMn / ouriij niu i 9 An ZUU .

i fin 1UU

0ES 7 £1 TCI T A 1 /oWEW 01 LI T TM A 1 1WA 7 1MT T n1

2 1U34

-

* SSMS 78SUG 02 42-

42

3

1 .0

DArAAA ITNA7 AV AT 09

77CHA 01

f DDin) 42.

45.

5

16

PAA

14 NAA

76KAT 03

81WIL 01

jUU - TTMA 7 1 A DD A 1 / jADCi U 1 45. 16. 14NAA 81WIL 02

19.6 0.PAA "1 / All A A 1 7hCHA 01 46. ITNA 75KLE 01 20* 2

ITNA 78NAD 02 50. * UU 80HEN 01 20. 2

ITNA 75NAD 02

25

7

D* PAA 77CHA 01 Cr (ppm)

9 R 7 BAA rAA 7 CPU A A 1 /DOHA Ul

1 9 JZ •1 A1U • T TXT A 1 1NA 7QDVA A1 l sn Li

1 /. M A A 1HNAA O 1 T TT T ft O olwIL 0 2 J £. •

i1Un.

. TTMA 11 nu A AT 150. T * 14NAA 81WIL 01 AH Qo • TTMA 7 RMA r n 1 1 12

XRF /oCAM 02

42. ITNA 78WEA 01 113. 1.5 T TM A 1 IN A 7 CM Aft AO / jNAI) U Z A9HZ. i1Un . TTMA 1 UNA 7 tnun a i / DUNU U

113. 2

ITNA 78NAD 02

50. UU O All ETNT 1 oUHEN Ul 113. FAA 78GUI 01 52

15ITNA 81 WAN 01 1 1H . ICPES O ft RT A T\ ft 1 BONAD 0

56

35 ITNA 81GLA 03 1 17

7

ITNA T £t> ft 1 /DRAG 0.'. 58

ft ITNA / /MAE 01 1 17 . ft SSMS 78GUI 0i

185. 44. ITNA 73SHE 01 1 l ft

1 Iff OA 9 o

ITNA

ITNA

76WEW 01 760ND 01

(ppm) EJ • ITNA 78MAC 01

1 zu

OES 78SUG 01

52L* XRF 78CAM 02 1 20

4

AAA A 7 AAMT. A T / OUNU U

150. L* XRF 81C0H 02 122

12. TTMA 1 inn 7 "3 CUT? A1 / JOac. U 1

l jU . T 4 EXRF / / G LA U

123. OOUTATTT A A 1 LiKJ U 1 9AZD . A T ADD C Q AM A A A 1 (3UNAJJ Ul 124. 14. yijp 7 Q CMT A 1 / " oi l J- U 1 19jii z9 • AAA A 7 7MTT Al / / ni 1 U

126. 1 1

ITNA 7 ART A 0 T 9Z . TTMA L ILIA / OMIIj U 1 127 . 6. D* NAA 7AAMA AT IS A 9 ft PAA 7APUA Al 127. 6. T TMA 7 ^AMA A 1 / jKJvtU Ul

JO . Z

1 1 X • 1 TTMA 7 Am n n l 128. 5. 35 T TM A 1 1NA QipT A ft O olbLA UZ

1A 7 1 Q J .7 TTMA 1 UNA 7 RMAn A 9 / DWAU U Z 128

AA ~7 ft PT T ft 1 79SIL 01

77 /. 4

ITNA TOHAn AO /oNAD UZ 1 7ft 1 Zo cJ . 9.1 JJ ITNA 81GLA 04

38 . ITNA 78WEA 01 1 70. 1 Zo • ITNA 78WEA 01

382

35 IENA 80GLA 03 1 7ft 5 1 Zo . j 0 c: O . D AA 7/MIT 01 38. 0.96 OES 76WEW 01

1 70 1 O 5 .y ICPES 81CHU 01

38. 2. ITNA 78MAC 01 1 ?Q 7 9Cm m 71 ITNA 77ROW 03

38.6 3.7 ITNA 73SHE 01 129.2 2.7 D* ITNA 77R0W 04

39. AA 76WEW 01 130. 4. ITNA 83GLA 01 39.4 1.2 ITNA 76RAG 01 130. UU 80HEN 01 39.8 0.9 ITNA 81 WAN 01 130. AA 76WEW 01 40. 2. 35 NAA 81GIA 04 130. 5. 9 ITNA 78LAU 02

40. 2. PAA 76CHA 01 131. 8. ITNA 73ABE 01

134
TABLE X (cont) TABLE X (cont)

ANAL REF REF CONC WUMMtn 1 Bit i M CODE NUM

ADal1 PA A 7AfHA 01

QO • Ci AIM / OfLiLt v 1 ill 1 J 1 . co

r AA 7 tPU A At / OwlA Ul 131

EXRF 78WEG 01

131

6. D* PAA 77CHA 01 131. 9. ITNA 76KUC 01 131.7 4.6 RTNA 81GAL 01 131.7 4.6 RTNA 81GAL 02

132. 3.3 AA 74RAI 01 132. 10. FAA 760WE 01 132 .3 0.35 RTNA 74MCC 01

1 34 ftV • 33 ITNA OIPT A A 1

11 nJ J . A A AA

1 A l&PiA 7 7 OATJ A A / / KUW U4

IOC 0 . ITNA / / (JHA U

1 . AA 7 O^MIT A 1 /oGUI Ul

1 J50 • D* ITNA "7 ODV A A 1 /oRlA Ul

1J/ •

1 clb • T TMA

J. IN A

0 1 fJA XT Al o 1 WAN U

138

ITNA 75KLE 01 140. 15. ITNA 78LAU 02

l j

DAA rAA 7 £.V AT A 1 / OKA1 U J 142. 9. PAA 76KAT 02

150. 13. OES 76WEW 01 159. 115. EXRF 77GIA 01 175. *6 SSMS 78GUI 01

180. ITNA 75MIL 01

(ppm)

l\) • TLi*** CART 77PTA 01

C Q 5.8 1 A TTH A 1 IMA 7 QH A T"\ A 0

5 .81 1 .4 TTM UNAA 7 QMAn A 7

/ jNAD U Z 7.3 1

ITNA 7 DT AIT (11 /oLAU Uz

7.7 1.3 ITNA 7 £.1 TPI I A 1 7 oWEW U

8. 1

PAA 76CHA 01

8. 1. D* PAA 77CHA 01 8.1 0.5 9 ITNA 781AU 02

8.2 0.4 ITNA 83GLA 01 8.2 0.9 IENA 76STE 05

8.2 0.5 ITNA 760ND 01 8.3 0.4 35 ITNA 81GLA 02

8-3 1

ITNA 7 TAJ A A 1 / /LHA Ul 8.3 0.9 IENA 7 7 DA1 7 A 1 1 1 KU W U 5 8.3 1 • u TTMA UNA 7RPVA ni / OMA U 1 o A ft £ T TM A 1 1NA 7 7PATJ A A 8.42 fi 1 o 1) . 1

T17M A 7 7PA.TJ A A / / RUW U** 8.5 U.D T TH A

1 1NA lOUAP Al/ orlA'j Ul 8.6 ITNA 7 OT re A A 1 /oWLA Ul 8.6 1 . 1 ITNA 750ND 01 8.6 0.8 ITNA 76RAG 01 8.7 0.3 35 IENA 80G1A 03

8.7 0.7 35 NAA 81GLA 04 8.8 0.4 35 ITNA 81GLA 03

8.9 0.8 ITNA 81 WAN 01 9.4 ITNA 75MIL 01 9.9 0.8 ITNA 7 3 ABE 01 10. UU 80HEN 01

10. 1. 14 NAA 81WIL 02

13.8 1.4 ITNA 73SHE 01 0.63 0.06 * PAA 74CHA 01

CONC

Cu (ppm)

70.2

110.

115.

115. 119.

120.

120.

121. 123.

124.

124.

125. 125.

125. 125.

127.

128.

129. 129.

129.

130. 130.

131. 131.

131. 133

133.

134.

135. 136.

136.

137. 140.

140.

140.

142.

145.

198.

Dy (ppm)

7.6

9.9.4 9.4

10.2

10.2

10.3

10.9

10.9

12.1

19.

Er (ppm)

11.

ANAL REF REF UNCER COMMENT METH CODE NUM

300. ITNA 7 3 ABE 01

1.8 * AA 77MIT 01

11

* OES 76WEW 01

8. ITNA 77ROW 03

8. ITNA 76STE 05

5. AA 760ND 01 UU 80HEN 01 ICPES 80FL0 01

A A AA 79SIL U 1 EXRF 78WEG 0 1 XRF 78CAM 02

19FAA 760WE 01 AA 78GUI 01

10. ITNA 77CHA 01 13. EXRF 78PEL 01

10. D* ITNA 78RYA 01 AA 78GEL 01

3 .9 ICPES 81 CHU 01 AA 78WEG 0

EJ • oo oUMJr U 1 AA 76WEW 01

CJ • AAA A c\ *> \JZ 9 7 AAA A 7 A D AT U i 6 SSMS 78GUI 01

ATi+Ar U

FAA 78GUI 01 XRF 75KLE 01

4. EXRF 77GIA 01

11. 6 PAA 82SEG 01

3. XRF 79 SMI 01 ICPES 80NAD 01

6. 35 RTNA 77GLA 01

7. ITNA 76BL0 01

10. XRF 81C0H 02

20. 6 PAA 82SEG 01

20. PAA 80SEG 01

9. ITNA 73SHE 01 *6 SSMS 78GUI 01

61

* ITNA 81 WAN 01

30. L* OES 76WEW 01 2.4 * ITNA 7 3 SHE 01

2. ITNA 78MAC 01 0.5 ITNA 76STE 05 0.5 ITNA 7 7 ROW 03 ITNA 75MIL 01

35 ITNA 81GLA 04 0.4 35 ITNA 81GLA 02 ITNA 75NAD 02

ITNA 78NAD 02

0.6 ITNA 760ND 01

3. * SSMS 78SUG 02

100. L* OES 76WEW 01 300. L* OES 76WEW 01

2. SSMS 78SUG 02

135
TABLE X (cont) TABLE X (cont)

ANAL KEF REF CONC UNCER COMMENT METH CODE NUM

Eu (ppm)

1 .9 0.2 * ITNA 760ND 01

2 . 2. *35 IENA 80GLA 03

2 . * ICPES 80FLO 01 2.3 0.1 ITNA 7 3 ABE 01

2 .39 0.11 ITNA 76RAG 01 2.42 0.16 ITNA 7 3 SHE 01 2.44 0.19 ITNA 76STE 05

2 .49 0.15 35 ITNA 81GLA 02

2 .5 0.4 ITNA 750ND 01 2.5 0.16 35 ITNA 81GLA 04

2.5 ITNA 78WEA 01 2.56 0.07 ITNA 83GLA 01

2 .57 0.19 ITNA 77R0W 03

2.6 0.2 ITNA 81 WAN 01 2.6 0.2 ITNA 76WEW 01 2.62 0.05 ITNA 78NAD 02

2.62 0.05 ITNA 7 5NAD 02

2.69 0.09 ITNA 77R0W 04

2 .7 0.1 ITNA 78LAU 02

2 .79 ITNA 82GLA 02

2.8 0.13 OES 76WEW 01 2.86 ITNA 75KLE 01 2.9 0.2 35 ITNA 81GLA 03

3. 0.15 ICPES 81CHU 01 3.1 ITNA 75MIL 01 5.3 1.2 * SSMS 78SUG 02

F (ppm)

10. UU 80HEN 01 20. AA 76WEW 01

)

4.23 0.3 * PAA 76KAT 03

4.24 0.19 * PAA 76KAT 02

4.4 * AA 78GUI 01 5.278 0.56 * ITNA 7 3 SHE 01 5.6 2.8 OES 76WEW 01 5.6 0.2 ITNA 76WEW 01 5.7 0.3 ITNA 76KUC 01 5.8 0.3 5 IENA 80GLA 03

5.8 OES 78SUG 01 5.8 AA 78WEG 01 5.9 0.2 5 IENA 80GLA 03

5.91 0.16 IENA 7 7 ROW 04

5.94 XRF 78CAM 02

5.96 0.16 XRF 79SMI 01

6. 0.3 ITNA 760ND 01

6. ICPES 80FL0 01

6. XRF 76WEW 01

6. 0.2 ICPES 80EPS 03

6. 0.4 AA 79WEG 01 6.03 0.16 ITNA 81 WAN 01 6.08 0.52 PAA 74CHA 01 6.09 0.03 ITNA 83GLA 01

6.1 0.3 35 NAA 81GLA 04

6.1 0.1 D* TCGS 80AND 01 6.1 0.2 PAA 76CHA 01 6.1 0.1 TCGS 79FAI 01

ANAL REF REF CONC " UNCER COMMENT METH CODE NUM

fi 1 U • L U PAA 77CHA a i U 1 AO •

1IDA U.J EXRF 78PEL U I 6.17 0.41 ITNA 7 5NAD

6.17 0.41 ITNA 78NAD 0 2 6.198 0.102 AA 77MIT 01 6-2 0.3 D* NAA 740ND 01 6.2 0.04 ICPES 80NAD 01 6.2 EXRF 78WEG 01 6.2 OES 80WAL 01 6.2 0.1 AA 760ND 01 6.2 0.4 D* ITNA 78RYA 01 6.2 0.3 ITNA 750ND 01 6.2 0.05 D* ITNA 77ROW nit 6.2 0.4 ITNA 77CHA U 1

fiD • ? n ft XRF 81C0H

& 9 a a ITNA 7 7 ROW U J A 9 A 1 EXRF 77NIE U

t\ 9 9 a ar TCGS 79AND A 1 AOi449 9 a Aft EXRF 77GIA U 1 6.23 0.1 ITNA 78LAU 02

6.23 0.14 35 ITNA 81GLA 02

6.3 0.1 ITNA 78MAC 01 6.3 0.4 35 ITNA 81GLA 03

6.32 ICPES 80NAD 01 6.35 ITNA 78WEA 01 6.37 ITNA 75KLE 01 6.4 0.15 14NAA 81WIL 02

6.4 AA 79SIL 01 6.46 0.14 ICPES 81CHU 01 6.5 UU 80HEN 01 6.51 0.31 ITNA 7 3ABE 01 6.69 ITNA 75MIL 01 6.7 35 7QpI A 04 6.8 0.03 * ITNA 76RAG 01 6.8 0.2 * AA Q rtCT/1 02

6- 95 0 15 * 1 / MA A 01

7. * A A AA "7 ALTCTJ / OWLW 01

>pm)

34.3 1.9 ITNA 81 WAN 01

37

2IENA 78WAN 01

38 .3 6 .

ITNA 73SHE 01 40. 1

XRF 79SMI 01 40.3 2. 5 IENA 76STE 05

40.7 1 .2 IENA 77ROW 03

40.7 1 .2 5 IENA 76STE 05

411

35 IENA 81GLA 04

41

7. EXRF 77GIA 01 43. 1. 35 IENA 80GLA 03

43. 1. 35 IENA 81GLA 03

45. 7. ITNA 760ND 01

48. 6. COLOR 79LIK 01

49. XRF 75KLE 01 50. UU 80HEN 01

58. 10. * FAA 760WE 01

68. 14. * OES 76WEW 01 72. ICPES 80FLO 01

136
TABLE X (cont) TABLE X (cont)

UNCER COMMENT

ANAL meTM

REF REF CODE NUM CONC UNCER COMMENT

ANAL

METH

REF REF CODE NUM

100. L* 0ES 76WEW 01 11. ITNA 75MIL 01 11.4 0.2 TCGS 79FAI 01 11.7 0.4 TCGS 7 9 AND 01

12.1 0.36 ICPES 81CHU 01

17.5 0.3 * TCGS 80AND 01 23. 4. * SSMS 78SUG 02

Ge (ppm)

19. 1. XRF 79SMI 01 20. UU 80HEN 01

25

.

1 .4 0ES 76WEW 01 26. 5. EXRF 77GIA 01 476. 166. ITNA 7 3 SHE 01

H ( DDm)

1000. UU 80HEN 01 1200. 400. TCGS 79AND 01

H20- (%)

0.03 UU 80HEN 01

H20-T (%)

0.17 FD O AVUA AO oOKHA Uz

H2S04 (ppm)

1 AAA 1UUU

.

Tin UU OUnCJN Ul

17 . L* 14NAA 81WIL 01 DO n 7 ITNA 76WEW 01

(\ 7 U • J IENA 77ROW 03

0 . / A 1 U.J TUM A 1LN A

/ •

A. A TTNA

1 O U . u TTMA I I IMA

7 .4 0.5 ITNA TOT Alt AO 78LAU yjl 7,5 0.5 ITNA T T/^LI A A 1

7.5 ITNA 78NAD 02

7.5 0.5 D*. ITNA 78RYA 01 7.5 0.4 ITNA 78MAC 01 7.52 0.02 ITNA T CMA T*\ AO 7 5NAD Ui

/ .0 U*z TTMA 1 UNA OQlfTALrfi 01\J A 7.62 0.56 ITNA 7 3 SHE 01 7.7 0.1 ITNA 81 WAN 01 7.9 ITNA 78WEA 01 7.9 0.4 ITNA 750ND 01

8. 0.4 35 NAA 81GLA 04

8. 0.4 35 ITNA 81GLA 02

8.1 0.1 35 IENA 80GLA 03

8.2 0.8 ITNA 7 3 ABE 01 8.2 0.8 ITNA 760ND 01

8.2 ITNA 7 SMIL 01

10. 2. *35 ITNA 81G1A 03

it TTT1 UU Q AUPM U 1 in n It TTMA 7 Wl 17 U 1

Ha (dpd)

8000. L* 14NAA 81WIL 01

12000. L* EXRF 77GIA 01 400. L* ITNA 76BL0 01 500. L* ITNA 7 3 ABE 01 200. L* ITNA 78NAD 02

200. L* ITNA 75NAD 02

100. UU flOHEN 01

1I 19L7 . 0£. • C\IA ^VAnA OUlinU nU i1

1 07 J - /.111 A L VAA "J CI/ T p n i U

1

i in in NAA 7 7 TTTD n l

1 JKJ . m n*u T>A rAAA / / KMti nu l1 130. 30. PAA 76CHA 01 134. 4

.

CVAA 74RAI 01 135. 10. PAA 74CHA 01 137. 15. RTNA 81GAL 01 137. 15. RTNA 81GAL 02

141. 12. FAA 77GLA 03

145. ITNA 78WEA 01

6

.

RTNA 740RV 01 160. 40. D* ITNA 78RYA 01 lbU. A n ITNA 77CHA u 1 170. 20. 6 PAA 82SEG 01

200. 20. * PAA 80SEG 01 200. 100. *6 PAA 82SEG 01

550. * XRF 76WEW 01 3700. 1100. * ITNA 73SHE 01 11000. * XRF 78CAM 02

Ho (ppm)

10. L* 0ES 76WEW 01 1.94 0.13 IENA 77R0W 03

1.94 0.13 IENA 76STE 05

3.6 0.8 SSMS 78SUG 02

I (ppm)

0.5 L* UU 80HEN 01

6. L* EXRF 77GIA 01 2- 1.2 ITNA 77MAE 01 2.8 1. PAA 77CHA 01 2.9 1.2 PAA 750ND 01

2 9 ITNA 78WEA 01

3. 1. D* ITNA 78RYA 01

3. 1

.

ITNA 77CHA 01

In (ppb)

500. L* UU 80HEN 01 118. 4. 5 IENA 76STE 05

128. 8. IENA 77R0W 03

128. 8. 5 IENA 76STE 05

156. 35. ITNA 7 3 SHE 01 160. 20. ITNA 81 WAN 01 270. 140. ITNA 76RAG 01

280. 30. PAA 74CHA 01

137
TABLE X (cont) TABLE X (cont)

ANAL KEF REF ANAL *EF REF CONC UNCER COMMENT METH CODE NUM CONC ' UNCER COMMENT METH CODE NUM

290. 60. PAA 76CHA 01 1 .9 0.5 * 14NAA 81WIL 01 290. 60. D* PAA 77CHA 01 1 .97

0 ?A

jj TTWA J- inn DIPT A fl A

320. 80. D* TTMA 7QPVA / OKI n ni 2 . 18 A TTMA 320

100. ITNA 750ND 01 3.3 0.66 * OES 7 fiWEW 0

320. 80

ITNA 77CHA 01

i nnn i r» nn ZUUU . JL EXRF 77GIA 01 La (ppm)

45. A.

* 0ES 76WEW 01 64. 2. * ITNA 78NAD 02

inn zuu

ITTI uu ftOHFN 01 (\L 1 * TTMA i. Inn 7 ^MAn r. 9 / jINAJJ U Z 15.6 2.4 PTNA 7 7NAD. u c

Afi DO .

*> T TM A 1 IN A 250. 80. T1 TMA inn 77PUA UO 1

1 A70. UU O T T T7VT 1 80HEN 01 250. 80. D* TTM A ITNA 7 ODV A A 1 Ul 71 O / 1 .7 T TM A I 1NA oJOLA Ul 18600. 3300. ITNA 7 3 SHE 01 77It. m £O • VDO AKr t qcwt n 1 /9bMl Ul

18600. ITNA 78WEA A 1 01 7A /, T 1U A ITNA /oLAv UZ

7 A O /'* .0 ITNA 0*1/17 1 /"\ O 82GLA 02

(%)

7 t A4 • 33 TTMA 1 1NA olOLA Uj

141 L TTMA

1 .29 0.09 JL ITNA 76KUC 01 76.4 ITNA

1 CI 1.51 ICPES 80NAD 01 77. 8 • ITNA 7^SHE 01 1.31 n nc ITNA 78MAC 01 78. XRF 78CAM 02

1 SA n oa ITNA 76BL0 01 78. I CPE S 80F1 0 01

l1 . JOss n i s ITNA 750ND 01 79. 6

35 IENA 80G1.A o\J\J Lin 03KJ J

1 SP 0 OS PAA 76KAT 03 79. 1 .6 ICPES 81 CH1I 0 1

1 C 1 . J7 n os PAA 76KAT 02 80. ITNA 7SMTT m

1 .0 U • 1 £. AA 80ST0 02 niO 1 . o

<c • TTMA 7£T>Ar» 1 / DKAb U 1

1 .0 a aa U .Uo PAA 77CHA / / win 01 01 7 Ol .z 3 • j

T TTM /> / /RUW U j

1 .6 0.04 Q 1 ruiT O I SvilU nU i1 Q 1 0 ol .Z J .z Tru A /oblc. U_>

1 .6 0.06 r AA 7AfUA A.U 1

Q7OZ .

/, H • T TM A 1 1NA 7*1 A DT7 A 1 / jA.de* Ul

1 .6 AFC U 1 Q7oZ • on rvnp tArvr 7 HOT K A

/ /OlA Ul

1 .61 TTMA 1 1NA 7RUP A niUl Q7OZ . ITNA "7 QI TP A A 1 /OWEA Ul

1 .63 0.06 ITNA 77MAE 01 TTMA 1 lNn

1 .63 XRF 78CAM 02 82

2

ITNA 7 SOND 0

1 .65 0 .09 ITNA 78LAU 02 84. 3.6 IENA 77ROW # / AVk_/ T7 04V *T

1 A A XRF 79 SMI 01 84. 3.6 ITNA 77R0W 03

1 .67 0.06 EXRF 78PEL 01 85. 4. ITNA 77CHA 01

1 .68 AA 79SIL 01 85. A. D* ITNA 78RYA 01

1 .69 35 TCGS 78GLA 04 85.3 3.8 ITNA 77ROW 04

1 .69 0.13 ITNA 77CHA 01 86. 2. ITNA 76WEW 01

1 AO U . 1 J u ITNA 78RYA 01 91

7

* ITNA 76STE 05

1 7

1 . / a o 0.2 ITNA 760ND 01 i in * ecu? / OOUu U i

1 7 ITNA 78KEL 02

1.71 0.03 CAMMA 71ARF / JAOEi 01

1 7 1 1 B / 1 aU .1)mi CjAMMA 7 cnMn / DUND U

1 7 1 1 m 11 A A /. U .OA AA 760ND 01 1 .7 U.J * ICPES q i run n

O X V-JT U U x

1 .72 0 .09 ICPES fiONAD 01 Rfl AA 7fiWFW / unL w 01ui

1 .73 0. 18 ITNA 81 WAN 01 i An q \JCtO

1 7 A n 07 EXRF 77NIE 01 300. UU 80HEN 01

1 7 C

1 ./

n 1 0.

TCGS 79AND 01

1 7 S UU 80HEN 01 Lu (ppm)

1 7 S U . lo ITNA 76RAG 01

1 .76 0.05 D* TCGS 80AND 01 50. L* OES 76WEW 01

1 .76 0.05 TCGS 79FAI 01 0.87 ITNA 82GLA 02

1 .77 ITNA 75MIL 01 0.9 0.3 ITNA 81WAN 01

1 .78 0.24 ITNA 78NAD 02 0.94 0.09 D* ITNA 77R0W 04

1 .78 0.23 ITNA 75NAD 02 0.94 0.09 ITNA 77R0W 03

1.8 0.3 14NAA 81WIL 02 1 . 01 ITNA 750ND 01

1.8 0.13 ITNA 77ROW 03 1

0.2 ITNA 76WEW 01 1.8 0.13 ITNA 76STE 05 1 .01 0.02 ITNA 78NAD 02

1.8 ITNA 75KLE 01 1.01 0.02 ITNA 75NAD 02

1 .81 0.15 35 ITNA 81GLA 03 1.1 35 ITNA 81GLA 03

1 .83 0.05 35 IENA 80GLA 03 1.1 0.15 ITNA 77CHA 01

138
TABLE X (cont) TABLE X (cont)

ANAL UF KEF CONC ' UNCER COMMENT METH CODE NUM

Mg (Z)

1.1 0.15 D* ITNA 78RYA 01 1.2 ITNA 75MIL 01

1.7 0.4 SSMS 78SUG 02

2. 0.05 * ITNA 78LAU 02

3.8 0.5 ITNA 73SHE 01

4. 1. * ITNA 78MAC 01

1 .01 * ICPES 80NAD 01

1.2 0.1 AA 760ND 01

1 .22 AA 79SIL 01

1.29 0.02 ICPES 8ONAD 01

1 .32 0.04 ICPES 81CHU 01

1.4 0.4 ITNA 77MAE 01

1.4 0.4 ITNA TOY All no 78LAU UZ

1 .4 OES 785UG 01

1 .44 0.02 PAA /OKAl U3

1 .45 0.05 AA oncTn OUolU fi7 uz

1 .48 0.01 PAA / H\mA Ul

1 .5 1.3 14NAA Oil TT T f\ 1

1 .5 0.2 D* TCGS 80AND 01

1 .5 0.2 TCGS 79FAI 01

1.5 0.15 D* PAA 77CHA 01

1 .5 0.01 PAA 76KAT 02

1 .5 0.3 ITNA 76WEW 01

1 .5 0.15 PAA 76CHA 01 1.52 0.06 ITNA 78NAD 02

1 .52 0.06 ITNA 75NAD 02

1 .597 0.806 ITNA 73SHE 01

1 .6 0.32 OES T /I Y TP 1 T rt 1 76WEW 01

1 .68 0.21 D* ITNA

1 .68 0.21 TTM A 1 LNA 77f*HA 111

1 .78 0.2 T1 THA 1NA 7 7PfiU n ^

1 .78 0.2 T TMA 1 1NA 7AQTF fl 1? / Do LCt \J J

1 .8 ULb ftnuAT OUWrtL nU l

1

1 .8 ICPES 80FL0 01

1 .8 ITNA "7QUT7 A fi 1

1 .8 0.4 ITNA 750ND 01

2. UU 80HEN 01

2. 0.4 ITNA 76RAG 01

2.08 0.43 ITNA 73ABE 01 2.1 0.5 14NAA 81WIL 02

2.19 0.35 ITNA 81WAN 01 2.4 *35 TCGS 78GLA 04

6.3 0.3 * ITNA 78MAC 01

Mn (ppm)

351. *6 SSMS 78GUI 01 420. * ITNA 78KEL 02

422.4 3.9 * AA 77MIT 01 440. * AA 78WEG 01

460. ITNA 75KLE 01 460. 26. OES 76WEW 01 464. 1. ITNA 78NAD 02

464. 1.4 ITNA 75NAD 02

464. 46. ITNA 76KUC 01 466. 31. ITNA 7 3 SHE 01 477. 5. AA 760ND 01

478. FAA 78GUI 01

480. 25. D* TCGS 80AND 01

480. 25. TCGS 79FAI 01

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

480. 10. ITNA 76BLO 01 482. ICPES 80NAD 01

483. 21. XRF 79 SMI 01 485. AA 79SIL 01

488. 50. ITNA 81 WAN 01 488. 14. ITNA 77R0W 01U J 488. 14

.

ITNA 76STE 05

489. 11

.

ITNA 7 3ABE 01 491. 10. PAA 76KAT 02

491. 18. PAA 76KAT 03

492. AA 78GUI 01 493. 4.1 AA 74RAI 01 495. ITNA 78WEA 01 495. 15. D* PAA 77CHA 01 495. 15. PAA 76CHA 01 495. 25. PAA 74CHA 01 496. OES 80WAL 01 496. 19. ITNA 750ND 01 496. 19. D* NAA 740ND 01 498. 11. 35 ITNA 81GLA 03

499. 22. 6 FAA 79GEL 01

499. 25. ITNA 760ND 01

500. UU 80HEN 01 500. EXRF 78WEG 01

500. 15. D* ITNA 78RYA 01 500. 15. ITNA 77CHA 01 500. 17. EXRF 78PEL 01 500. OES 78SUG 01

503. 15. ITNA 7 7 MAE 01 504. 25. ITNA 76WEW 01 505. 9. 35 ITNA 81GLA 02

505. 14. ITNA 76RAG 01 506. AA 76WEW 01 508. XRF 78CAM 02

510. ICPES 80FL0 01 510. 70. XRF 81 COH 02

510. in ITNA 7ftT ATT ("19 513. 15

.

35 I ENA 80GLA 03

516. 16. ICPES 81CHU 01 520. 6. FAA 760WE 01

520. 20. ITNA 78MAC 01 528. 104. EXRF 77GIA 01 528. 6 SSMS 78GUI 01 530. 30. AA 80ST0 02

531. 14. EXRF 77NIE 01 540. * ITNA 75MIL 01 570. 24. *6 FAA 79GEL 01

(ppm)

0.5 0.08 D* PAA 77CHA 01 0.5 0.08 * PAA 76CHA 01

1 .52 0.15 * PAA 74CHA 01 20. UU 80HEN 01 20. ITNA 78WEA 01 22.3 1.6 14NAA 81WIL 02

25. 5. EXRF 77GIA 01 25.3 1.6 D* IENA 77R0W 04

25.3 1.6 I ENA 77R0W 03

28. 1. XRF 79 SMI 01

28. 1.3 14NAA 81WIL 01 28. 1. 35 IENA 81G1A 03

28. 1. 35 IENA 80GLA 03

139
TABLE X (cont) TABLE X (cont)

ANAL REF KEF CONC UNCER COMMENT METH CODE NUM

32. ICPES 80NAD 01 36. 5. FAA 760WE 01 36. 3. 35 RTNA 78GLA 02

37. 1.3 OES 76WEW 01

N (ppm)

1000. L* UU 80HEN 01

Ha (ppm)

2603. 156. k ITNA 76KUC 01 2658. 129. ITNA 73SHE 01 2800. 300. ITNA 76BL0 01 2820. 50. ITNA 78MAC 01 2830. 136. ITNA 76STE 05

2830. 140. ITNA 77R0W 03

2900. ICPES 80NAD 01 2900. OES 78SUG 01 3000. 200. D* TCGS 80AND 01

3000. 70. ICPES 81CHU 01

3000. 200. TCGS 79FAI 01 3000. UU 80HEN 01 3000. AA 79SIL 01

3000 .

100. ITNA 78LAU 02

3000. OES 80WAL 01

3052264. ITNA 81 WAN 01 3070. O A80

ITNA *T "7MA P A 1 / /MAfci 0

3100. 1 Art 300. ITNA /OUNL) Ul

3100. 200. ICPES QAM A A A 1 OUNAD Ul

3130. T TM A 1 iNA Olpi A A 1 OjIjIA Ul 3150. 1 10

14NAA OlWIL Ul 3200. 300. D* ITNA 78RYA 01 3200. 400. ITNA 750ND 01 3200. ITNA 78WEA 01 3200. 300. ITNA 77CHA 01 3200. 200. AA 760ND 01 3220. 50. 35 ITNA 81GLA 03

3240. 100. ITNA 76RAG 01

3290. 110. AA 80ST0 02

3300. 200. ITNA ONAJJ UZ

3300

9 A A 20U. T TM A TQMAn A O

/ o IN/VU U L 3300. 150. iy A A FAA

3300. 100. 35 ITNA o

ct a no oICjLA uz 3300. 150. nil rAA

3330. 170. 14NAA O 1 T TT T AO olwlL UZ 3400. 300. PAA 74CHA 01 3400. 300. ITNA 76WEW 01 3Aoo ITNA 75MIL 01 3600. 35 TCGS 78GLA 04

3700. 200. ITNA 73ABE 01

38 50. 210. * PAA 76KAT 03

3860. 130. PAA 76KAT 02

9700. 1900. * OES 76WEW 01

Nb (ppm)

100. L* OES 76WEW 01 7. UU 80HEN 01 26. 1. XRF 79SMI 01

28. 2. EXRF 77GIA 01

ANAL REF REF CONC UNCER COMMENT METH CODE NUM

li u \ u pui }

1 AA L* OES 76WEW 01

JS71 .oP. L • U n* ITNA 77ROW A A 57.8 ITNA 77ROW A 9 U J DoSR •

1 A1U • ITNA 81 WAN 01 IENA 81GLA HAU<* 60 0£ • ^5JJ IENA 80GLA A9U i

fin s ITNA 75NAD A 9 UZ

61 o

£ • ITNA 78NAD A 9 UZ

62

£ • TCGS 80AND A 1 U 1 62.1 TCGS 79FAI AU 11 66. 7. ITNA 760ND 01

69. 7. D* ITNA 78RYA 01 69. 7. ITNA 77CHA 01 81. ITNA 75MIL 01

90. 13. * SSMS 78SUG 02

94. 19. * ICPES 81CHU 01

NH4 (ppm)

100. L* UU o \j nEji 01

KM fnmnl

69

7

,

* IENA 77ROW 0U 9J 78. * AA 76WEW 01 84

2

35 IENA 81G1A OA

RA O . is IENA 80GLA 09

RS AA 78GUI O 1 7Z • Q7 • cO PAA 82SEG A 1 U

AO92 . 6

PAA 750ND A 1 01

93. 58 SSMS 80KOP 01

93. EXRF 78WEG 01

94. XRF 78CAM 02

94

ICPES 80FLO 01

95. 20. EXRF 78PEL 01

oV5 .

ft7 . ITNA 77CHA A 1 Ul QS Q7 . D ITNA 78RYA A1Ul

063D. e

j . XRF 79SMI 0U 11 Ofi •1j . PAA 76KAT 0U 9Z 9ft js * PAA 76KAT 09

96.4 1I . Z? IDMS 74MOO 0

U 1 Q6 A 1 9 £ IDMS 74MOO U 1 Q A 6 11 . £O IDMS 74MOO 01U 1 o ,c o 70 .O O 9 PAA 74CHA A 1 Ul 97. 5

D* PAA 77CHA 01 97. 5. PAA 76CHA 01 98. FAA 80WAL 01

98. POL 74MAI 01

98. 9. D* NAA 740ND 01 98.5 9.5 IENA 77R0W 04

QQyy . AA 79SIL A 1 U 1 QQ7 7. A AF 80EPS nuz9 QQ 7 3j • 1j AA 77MIT m

1 00 7 PAA 82SEG

100. UU 80HEN 01 100. 7. AA 760ND 01

100. 5. ITNA 78NAD 02

100. 5. ITNA 75NAD 02

100. 3. ICPES 81CHU 01

140
TABLE X (cont) TABLE X (cont)

ANAL UF KEF ANAL REF REF CONC ' UNCER COMMENT METH CODE HUM CONC " UNCER COMMENT METH CODE NUM

100. 20. ITNA 760ND 01 71

.

"

3. PAA 76CHA 01 101. 7. EXRF 77GIA 01 71. 3. D* PAA 77CHA 01 101. 3.3 AA 74RAI 01 72. 5. EXRF 77GIA 01 105. 3. 14NAA 81WIL 01 74. 4. FAA 75BL0 02

105. 13. ITNA 750ND 01 74. 4. FAA 76BL0 01 106. FAA 78GUI 01 74. 9. OES 76WEW 01 106. 12. 14NAA 01 W1L OZ 75. OES O Al TA T A 1 109. XRF 75KLE 01 75. 5. D* NAA 740ND 01

1 10. 7. PAA 80SEG 01 75. 5. PAA 750ND 01 110- 10- 9 ITNA 78LAU 02 76. AE+AF 77FEL 01

120. 7.5 * OES 76WEW 01 77. ICPES 80NAD 01 120. * 0ES 78SUG 01 77. 6. AA 80ST0 02

128. * ICPES 80NAD 01 78.

78.

4.

2.

IDMS

IDMS

75K1E 01 78CAR 02

N02 (ppm) 78.

79.6

2.9.7

AA

HAA

760ND 01 82NAD 01

100. L* UU 80HEN 01 80.

81.

UU

ICPES

80HEN 01 80FL0 01

N03 (ppm) 81.

82. 6. AA

FAA

78WEG 01

760WE 01

100. L* UU 80HEN 01 82.

100. 25. * AA14 NAA

76WEW 01 81WIL 02

0 (Z)

Pb-210 (PCi)

47.02

Os (ppb)

P (ppm)

880.

898.

1090.

1200.

1900.

3000.

Pb (ppm)

40. 62.

62.8

64.

65.

66.

66.

67. 68.

68. 68.

68.8

69. 70.

70.

70.

70.5

70.7

71.

0.08

4000.

400.

8000.

26.

100.

34

L*L*

L*

**35

*6

14NAA 80KHA 02

3.37

3.37

0.13

0.13

13.

12.

6.

6.4.

4.

4.

2.6

3.

RTNA

UU

XRF AA

ICPES

ICPES

UU

COLOR

TCGS

SSMS AA

FAA

ICPES

EXRF

EXRF

XRF

POL

SSMS PAA

PAA

POT

PAA

AA

AA

SSMS FAA PAA

NAA

77NAD 02

80HEN 01

79SMI 01

76WEW 01 80NAD 01 81CHU 01 80HEN 01 80NAD 01 78GLA 04

78GUI 01

78GUI 01 78GUI 01 81CHU 01

78WEG 01

78PEL 01 79SMI 01 74MAI 01 80KOP 02

82SEG 01 80SEG 01

82CHR 01 82SEG 01

78GEL 01

79SIL 01

78GUI 01 78SIE 01 74CHA 01 77JER 01

Pd (ppb)

Pr (ppm)

24.

28.

Pt (ppm)

2. 1000.

4000.

100.

6.

D*

L*

L*

L*

L*

0.4

0.451

1.38

90.

0.011

0.28

L*

NMNM

RTNA UU

EXRF

OES

ICPES

SSMS

OES

UU

RTNA

RTNA

Rb (ppm)

81CAS 01 80CAS 01

77NAD 02

80HEN 01 77GIA 01

76WEW 01 80FL0 01 78SUG 02

76WEW 01 80 HEN 01 77NAD 01 77NAD 02

70. 30. * ITNA 81 WAN 01 95. 1. * PAA 76KAT 02

96. 2. * PAA 76KAT 03

100. 10. 9 ITNA 78LAU 02

102. 5. 14NAA 81WIL 02

105. 10. ITNA 76RAG 01

108. 4. EXRF 77GIA 01 108.4 3.7 IENA 77ROW 03

108.4 3.7 D* IENA 77R0W 04

110. 2. XRF 79SMI 01 no. 9. ITNA 77R0W 04

110. 22. OES 76WEW 01

141
TABLE X (cont) TABLE X (cont)

ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC ' UNCER COMMENT METH CODE NUM

111. 14. ITNA 78NAD 02 6. 0.2 IENA 77ROW 03

111. 7. ITNA 83GLA 01 6.03 0.23 5 IENA T T T">/*\ T T fW //ROW 04

111. 13.5 ITNA 75NAD 02 6.1 0.4 5

T TM A 1 1NA "7 7Dni T f\ /. I 1 KOW OA

112. 20. ITNA 7 £!.TtTI.T A

Ul 6.2 35 TTNA Olu L. 1 (J j 114. XRF 6.4 0.2 ITNA 7 ot An n9

115. 15. ITNA 73SHE 01 6.5 0.2 35 RTNA 1 Ou Lin U L 115. 10. ITNA 7 QT ATI o *> u z 6.72 0.35 TTNA J. 111 A 7*;wAn no

116. 10. ITNA 77rHA 01 6.72 0.35 TTNA 7QMAn p)

f) i oruiiJ u l 116. 10. D* ITNA 78RYA 01 6.9 ITNA 78WEA 01 117. 6. 35 IENA 80GLA 03 6.9 0.5 D* TTNA /OK.IA Ul 118. 7. 35 NAA Q 1 PI A U4 6.9 0.5 ITNA 7 7CHA 01 119. 7. 35 ITNA 81GLA 02 6.9 0.6 ITNA 750ND 01

120. 10. PAA 76CHA 01 6.9 0.6 ITNA 76RAG 01

120. 10. D* PAA 77CHA 01 6.9 0.3 ITNA 760ND 01 120. XRF 75KLE 01 7.

1 .2

TTIT u uQ AUTTM A 1

123. 9. 35 ITNA 81GLA 03 7. PAA 76KAT 03

124. 10. ITNA 7 3 ABE 01

7. 1.1 PAA 750ND 01

125. ITNA 7 QT.TC A O 1 7.1 0.5 NAA 7 7TFR 01 125. 4- EXRF 77NIE 01 7.1 0.5 D* PAA 77CHA 01 125. 10. ITNA 750ND 01 7.1 0.5 PAA 76CHA 01 126. 10. PAA 750ND 01 7.1 0.7 PAA 76KAT 02

130. 30. ITNA 7 AAWTl / OUNJJ 01U l 7 1 A

/ . 1* 0.50 PAA 74CHA 01 137. 4. * 14NAA 81WIL 01 7 .2 0.8 ITNA 73ABE 01 150. * DD 80HEN 01 7.2

7.2

0-.3 0.3

35

35

W A A 1NAA ITNAQ 1 /it A A A 0 1 (j Lh Uh

81GLA 02

(ppb) 7.3 0.3 FAA 78HAY 01

7.4 0.3 ITNA 7 8MA C 0

200. L* UU 80HEN 01 7.7

7.8

0.5 35 IENA ITNA

80G1A 03

75KLE 01 (ppm) 8.3 1.8 * 14NAA 81WIL 02

9.8 2.1 * ITNA 76WEW 01 30. L* OES 76WEW 01 12.08 0.86 * ITNA 7 3 SHE 01

4. 500.L*

L* EXRF UU

77GIA

80HEN

0101 Sc (ppm)

Ru (ppm) 20. * UU 80HEN 01 20. * ICPES 80FLO 01 30. L* OES 76WEW 01 20.7 2.1 * PAA 74CHA 01 0.5 L* UU 80HEN 01 23. 0.4 ITNA 76BL0 01 0.258 0.02 RTNA 7 7 NAD 02 23. 2.3 OES 76WEW 01

3. 2. EXRF 77GIA 01 24. 1. ITNA 76WEW 01 25.1 0.5 ITNA 78NAD 02

S (ppm) 25.1 0.5 ITNA 75NAD 02

25.5 2. D* ITNA 78RYA 01 2000. XRF 81C0H 02 25.5 2. ITNA 77CHA 01 3900. 400. D* TCGS 80AND 01 25.6 0.5 IENA 77R0W 04

3900. 400. TCGS 79FAI 01 26. 2. 35 IENA 80GLA 03

4000. 400. TCGS 7 9 AND 01 26.5 0.2 ITNA 83GLA 01 4400. 100. TCGS 77JUR 01 26.7 0.2 D* ITNA 77R0W 04

7800. XRF 78CAM 02 26.7 0.2 ITNA 77R0W 03

9000. 500. XRF 79SMI 01 26.8 0.2 ITNA 78MAC 01 26.9 0.3 ITNA 81 WAN 01 Sb (ppm) 26.9 1.4 ITNA 760ND 01

27 . 0.5 ITNA 78LAU 02

15. L* 14NAA 81WIL 01 27. 1. ITNA 7 3ABE 01

100. L* OES 76WEW 01 27. ITNA 78WEA 01

4. 3. * EXRF 77GIA 01 27. 2. PAA 76CHA 01

5. * ICPES 82NYG 01 27. 2. D* PAA 77CHA 01 5.9 0.3 ITNA 81WAN 01 27. 1. ITNA 750ND 01 5.9 0.5 5 IENA 77ROV) 04 27 . 0.6 ITNA 76RAG 01

5.9 0.5 5 ITNA 77R0W 04 27.5 2.4 ITNA 7 3 SHE 01 5.96 0.61 HAA 82NAD 01 28. 1. 35 ITNA 81GLA 02

142
TABLE X (cont)

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM CONC

28.3 0.7 35 ITNA 81GLA U<. gl (%) 29. 3. 14NAA 81WIL 02

29.1 ITNA 7 5MIL 01 16

30. 1. 35 ITNA 81GLA 03 1?

*

32 * ITNA 75KLE 01 41. 5. * 14NAA 81WIL 01 2Q

'

20.

Se (ppm) 20.4

20.9

21.

21.5

21.8

21.8

21.9

22.

22.4

22.4

22.6

22.8

23.

23.

23.5

24.5

Sm (ppm)

10.05

10.4

11. 11.4

11.8

12.1

12.1

12.1

12.1 12.1

12.4

12.4

12.4

12.8

13.

13.

13. 13.2

13.4

13.5

13.6

13.6

14.9

15. 15.8

20.

Sn (ppm)

3.

5.5.7 6.7

10.

i n TLi* ICPES 81CHU 01

3 .2 * HAA 74BYR 02

n 7 * ASV 76AND 01

DO J • H

* ITNA 81 WAN 01

ft 7 1 .8 ITNA 78MAC 01 8.76 0.48 HAA 82NAD 01 8.8 1.2 ITNA 7 3ABE 01 8.8 0.7 9 ITNA 80WAN 01

8.8 XRF 78CAM 02

8.9 1.2 XRF 79SMI 01

8.9 0.6 ITNA 80WAN 01

9. 1.4 ITNA 76RAG 01

q 2. 35 IENA 80GLA 03

9.9.1

ICPES 82NYG 01

0.2 ITNA 78NAD 02

9.1 1. RTNA 740RV 01

9.1 0.3 35 NAA 81GLA 04

9.1 0.2 ITNA 75NAD 02

9.1 0.2 ITNA 81 CAR 02

9.35 0.03 GCMES 74TAL 02

9.35 0.03 DCP 81 CAR 02

9.35 0.03 GCMES 75KLE 01 9.48 0.8 PAA 74CHA 01

9 s 0.8 D* PAA 77CHA 01 9.5 0.8 PAA 76CHA 01 9.6 3.1 ITNA 76BL0 01 9.7 COLOR 74BYR 02

9.8 1

.

D* ITNA 78RYA 01

9 .8 0.5 6 PAA 82SEG 01

9. ft ITNA 78WEA 01 9.8 1

.

ITNA 77CHA 01

1 A10

.

A C QO ROVftp ft 1

10

.

0-9 6 PAA

1 A

10 • A t TTM A I LNA 7QT ATT ft O

1 ft 1U • Z • TTNA X Inn 760ND / DU VtLf 01\J I UU 80HEN 01 10. 0.9 PAA 80SEG 01

10. 0.6 RTNA 80KNA 01 10.1 2.2 ITNA 76WEW 01 10.2 HAA 80WAL 01 10.2 1.4 ITNA 750ND 01 10.2 1.4 D* NAA 740ND 01 10.3 0.7 RTNA 81 GAL 01

10.3 0.7 RTNA 81GAL 02

10.6 1.3 ITNA 77R0W 04

10.6 1. ITNA 78LAU 02

10.8 0.8 D* IENA 77ROW 04

10.8 0.8 IENA 77ROW 03

11. 3. ITNA 76KUC 01 11. 1. EXRF 77GIA 01 12.7 1.8 * ITNA 73SHE 01 35. 13. * 14 NAA 81WIL 01

35. 13. * 14NAA 81WIL 02

TABLE X (cont)

ANAL REF REF UNCER COMMENT METH CODE NUM

* OES 78SUG 01

3.4 * OES 76WEW 01 *35 TCGS 78GLA 04

1.6 PAA 76CHA 01 1.6 D* PAA 77CHA 01 ICPES 80NAD 01

UU 80HEN 01

2. PAA 750ND 01

1.4 XRF 79SMI 01

0.3 TCGS 79FAI 01 0.3 TCGS 80AND 01 XRF 78CAM 02

1. 35 AA 81GLA 03

1.6 14NAA 81WIL 02

0.3 ICPES 8 ONAD 01 AA 79SIL 01 0.8 14NAA 81WIL 01

1. EXRF 77NIE 01

6. 14NAA 76BL0 01 0.5 35 IENA 80GLA 03

1.1 TCGS 7 9 AND 01

in Li \JCiO m\j i

ft Eg TUNA TXT A ~1 1 CUE1 A 1 U 1 0.9 IENA 77ROW 0£

ii TTNA 78MAC 01

1 .6 TDM A IENA 76STE A C 05

1 .0 IENA / 7RDW A 1 03

0.4 D* TCGS 80AND 01

1. D* ITNA 78RYA 01 0.4 TCGS 79FAI 01

1.4 ITNA 77ROW 04

1

.

ITNA 77CHA 01 0*5 ITNA 7 3ABE 01

0 .V ITNA 7 50ND A 1 01 TTMA ITNA ~T QT.T17 A A 1 Ul

D ft TTNA x inn 7p\UFU TTNA X inn OJUU\ Ul

0.3 TCGS 7 9AND 01

0.7 ITNA 76RAG 01 ITNA 82GLA 02

0.7 ITNA 760ND 01

0.5 ITNA 78LAU 02

0.88 ITNA 75NAD 02

0.9 ITNA 78NAD 02

1. 35 ITNA 81GLA 03 ITNA 75KLE 01 0.3 * ICPES 81CHU 01

3. * SSMS 78SUG 02

UU 80HEN 01

2- EXRF 77GIA 01 0.6 NM 81IMU 01

1.4 XRF 79SMI 01

5. OES 76WEW 01

143
TABLE X (cont) TABLE X (cont)

ANAL REP R£F ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

10.2 1.4 D* ITNA 78RYA 01 Ta (ppm)

10.2 1.4 ITNA 77CHA 01

12. 1. PAA 76CHA 01 22. EXRF 77GIA 01 12. 1. D* PAA 77CHA 01 1.6 * ITNA 7 SIC T F n 1 12.5 1.2 PAA 74CHA 01 1.74 0.12 35 NAA 81GLA 04

12.7 0.82 HAA 82NAD 01 1.74 0.1 35 ITNA 81GLA 02 740. 210. * ITNA 73SHE 01 1.8

1.8 0.2 35 ITNA IENA 78WEA 01 80GLA 03

S03 (ppm) 1.8 0.3 ITNA 760ND 01 1.8 0.3 ITNA 750ND 01

100. L* UU 80HEN 01 1 .81 1.9

0.08

0.25 D*

ITNA

ITNA 83GLA 01 78RYA 01 S04 (%) 1.9

1.9

0.25

0.2 35

ITNA

ITNA

77CHA 01 81GLA 03

0.98 UU 80HEN 01 1.9

2.

0.1 0.2ITNA

ITNA

78LAU 02

76RAG 01 Sr (ppm) 2.2.

0.06 IENA UU

77R0W 03

80HEN 01 126. * EXRF 78WEG 01 2. 0.1 ITNA 78MAC 01 869. 33. * ITNA 73SHE 01 2. 0.06 D* IENA 77ROW 04

1200. 300. ITNA 76STE 05 2.01 0.14 ITNA 77R0W 04

1244. 6. PAA 76KAT 02 2.04 0.03 ITNA 75NAD 02

1244. 9. PAA 76KAT 03 2.04 0.03 ITNA 78NAD 02

1250. 230. ITNA 76RAG 01 2.1 0.2 ITNA 81WAN 01 1256. 37. LXKr / Or CjLj Ul 2.2 * ITNA 75MIL 01 1260. 35 T CM A Ql pi a no o 1 b Ln U J 2.74 0.25 * ITNA 7 3 SHE 01 1260. 30. 5 I ENA

OAP OUbLAT a mUj 3.5 0.3 * ITNA 73ABE 01 1300. 200. ITNA / OUNU Ul 1300. 35 IENA 0 1 f T A fl/i Tb (ppm)

1301. XRF 7 WT 1? n 1

1310. 60. 14NAA OITTTl ftO OlWlL UZ 100. L* 0ES 76WEW 01 1310. 50. i ANA A ftl OX UT1 WIL 01U 1 0.22 0.04 * ITNA 73SHE 01 1340. 100. ITNA 7 QUA r* D 1 1.2 0.2 ITNA 78MAC 01 1340. AA 79S1L Ul 1.5 0.4 ITNA 760ND 01 1342. 20. EXRF 77GIA 01 1.5 0.3 ITNA 81WAN 01 1360. 110. 5 IENA 76STE 05 1.53 0.11 ITNA 83GLA 01 1370. 120. PAA 76CHA 01 1.8 ITNA 75MIL 01 1370. 120. D* PAA 77CHA 01 1.87 0.15 ITNA 76RAG 01 1373. 95. PAA 74CHA 01 1.9 0.1 ITNA 78LAU 02

1375. 28. ICPES 81CHU 01 1.9 0.3 ITNA 750ND 01 1390. ITNA 75MIL 01 1.99 0.16 ITNA 77R0W 04

1390. XRF 78CAM 02 2. 0.3 ITNA 73ABE 01 1406. 80. ITNA 75NAD 02 2. 0.25 ITNA 77CHA 01 1406. 80. ITNA 78NAD 02 2. 0.1 35 NAA 81GLA 04

1410. 400. 14NAA 77VAN 01 2. 0.1 35 IENA 80GLA 03

1430. 30. XRF 79 SMI 01 2. 0.25 D* ITNA 78RYA 01

14 30. 60. 5 IENA 76STE 05 2.01 0.06 D* IENA 77R0W 04

1480. 60. ITNA 77R0W 04 2.01 0.06 IENA 77ROW 03

1480. 60. IENA 77R0W 03 3.12 0.02 * ITNA 75NAD 02

1480. 50. ITNA 77MAE 01 3.12 0.02 * ITNA 78NAD 02

1500. 180. ITNA 77CHA 01 3.3 0.5 * SSMS 78SUG 02

1500. UU 80HEN 01 1500. 200. ITNA 78LAU 02 Te (ppm)

1500. 1510.

180. 60.

D*

5

ITNA IENA 78RYA 01 80GLA 03 0.5 L* UU 80HEN 01

1520. 35. IENA 77ROW 04 5. L* EXRF 77GIA 01

1541. 188. ITNA 81WAN 01 0.92 0.05 HAA 82NAD 01

1600. 100. 9 ITNA 78LAU 02 2.3 0.3 D* PAA 77CHA 01

1620. * ICPES 80FL0 01 2.3 0.3 PAA 76CHA 01

1700. 300. * ITNA 750ND 01 2.32 0.2 PAA 74CHA 01

1900. 200. * ITNA 7 3 ABE 01 9.9 1.1 *35 RTNA 75GLA 01 2300. 1100. * 0ES 76WEW 01 8000. * XRF 76WEW 01

144
TABLE X (cont) TABLE X (cont)

CONC

Th (ppm)

UNCER COMMENT

ANAL REF REF METH CODE NUM

20. * UU 80HEN 01 21. 3. EXRF 77GIA 01 22.8 0.5 ITNA 76BL0 01 23.6 0.8 ITNA 76RAG 01 23.8 0.4 ITNA 77R0W OA

24. 0.8 ITNA 81 WAN 01

24. 2. ITNA 760ND 01

24. 1

.

35 ITNA 81GLA 03

24. 1. ITNA 78LAU 02

24. 1. 35 IENA 80GLA 03

24. 0.5 I ENA 77R0W 03

24. 2. 35 RTNA 78GLA 02

24. 0.5 D* IENA 77R0W 04

24 .4 2.2 ITNA 750ND 01 24.5 0.4 ITNA 83G1A 01

25

.

2. ITNA 73SHE 01 25. 1

.

35 ITNA 81GLA 02

25. 0.9 35 NAA 81GLA 04

lb . DNA 75MIL 0 1 26. ITNA 75MIL 01 2d . ITNA 7 5KLE 0

1

26.2 1.3 GAMMA 7 3 ABE 01 26.2 1.3 GAMMA 750ND 01

28. 2. ITNA 73ABE 01 32.2 0.2 * ITNA 7 8 NAD 02

32.2 0.2 * ITNA 75NAD 02

Th-228 (PCi)

2.23 0.05 D* NM 81 CAS 01 2.23 0.05 NM 80CAS 01

Th-230 (PCi)

3.74 0.17 D* NM 81 CAS 01 3.74 0.17 NM 80CAS 01

Th-232 (PCi)

D* MM 8 1 CAS U

1

n no mmNM U 1

Ti ( DDm)

3000. * XRF 76WEW 01 6000. * UU 80HEN 0 1 6000. 400. * ITNA 78MAC 01 6100. 200. * ITNA 75NAD 02

6100. 200. * ITNA 78NAD 02

6100. * OES 78SUG 01 6420. ITNA 75KLE 01 6800. AA 79SIL 01 6800. 1100. ITNA 760ND 01 6960. 35 TCGS 78GLA 04

7000. 700. ITNA 76WEW 01 7000. 300. ITNA 77R0W 03

7000. 300. ITNA 76STE 05

7000. 100. 35 IENA 80GLA 03 7070. 180. ICPES 81CHU 01

7100. 100. ICPES 80NAD 01

CONC

7150.

7200.

7200.

7200.

7200.

7210.

7230.

7250.

7250.

7300.

7300.

7300.

7300.

7300.

7330.

7360.

7400.

7400.

7400.

7400.

7500.

7500.

7500.

7600.

7600.

7660.

7660.

7700.

8200.

8600.

8700.

8900.

Tl (ppm)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

l onn ITNA 76RAG 01 200

.

J J NAA olGLA 03

200

.

r»* TCGS 80AND 01 200

.

1 Cbo /9FAI 01

l Aon OES 76WEW 01 05 TCGS 79AND 01

/. nn PAA 74CHA 01 360. PAA 76CHA 01 360. D* PAA 77CHA 01 150. 14 NAA 81WIL 01

280. D* ITNA 78RYA 01 400. PAA 750ND 01 XRF 78CAM 02

280. ITNA 77CHA 01 ICPES 80FL0 01 344

.

EXRF 78PEL 01 ITNA 78WEA 01 inn ITNA 78LAU 02 AA 760ND 01 300

.

T Til A 750ND 01 ICPES 80NAD 01 EXRF 78WEG 01 500. 35 ITNA 81GLA 02

800. ITNA 73ABE 01 200. 14 NAA 81WIL 02

100. PAA 76KAT 03

70. PAA 76KAT 02

300. XRF 79SMI 01 1100. * ITNA 81 WAN 01 1100. * EXRF 77GIA 01

* AA 76WEW 01 752. * ITNA 73SHE 01

30. L* OES 76WEW 01

2. UU 80HEN 01 3.5 0.5 6 PAA 82SEG 01 3.5 0.5 PAA 80SEG 01 3.64 0.34 PAA 74CHA 01 3.7 0.4 PAA 76CHA 01 3.7 0.4 D* PAA 77CHA 01 3.8 0.27 8 SSMS 80K0P 01 3.8 0.5 6 PAA 82SEG 01

5. * AA 76WEW 01 5.3 * POT 82CHR 01

18. 6. * 14NAA 81WIL 02

18. 6. * 14 NAA 81WIL 01

(ppm)

30. OES 76WEW 01

1.3 0.3 SSMS 78SUG 02

1.3 ITNA 75MIL 01

(ppm)

8.4 0.56 * ITNA 73SHE 01 8.6 1. *35 FLUOR 78GLA 01

9. 6. * EXRF 77GIA 01 10.5 1. ITNA 76RAG 01 10.6 ITNA 81WAN 01

145
TABLE X (cont) TABLE X (cont)

ANAL UF REF ANAL REF REF CONC UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

10.6 0.6 35 I ENA 78GLA 01 219. ICPES BONAD 0

11. 0.4 6 PAA 82SEG 01 220. 15. 1 INA 1 O A TIC f\ 1 / 3 ABE 01 11.1 1.7 ITNA 760ND 01 220. 15. TTNA 7 7 nu A fYl

1 1 .3 0.3 ITNA 78NAD 02 220

20. 35 ITNA OlU Lmt\ U J 11.3 0.3 ITNA 75NAD 02 220. 15. D* TTNA / OKI A U 1 11.3 0.3 35 DNA 78GLA 01 221. TTMA L INA 7 Q I .TP A ftl /owe* A Ul 11.5 0.5 35 DNA 81GLA 03 223. 10. T TH A 1 1NA 1 Q M A T\ A O /oNAD 02

11.5 0.5 35 IENA 80GLA 03 223. 9.9 TTM A 1 INA / 3NAD \Jl 11.7 DNA 75MIL 01 224. 6.7 T CUC C olCHU 01 11.7 2. IDMS 78CAR 02 225. 20. T TWA 7/OWLW AT.nr u a i Ul 11.8 IDMS 75KLE 01 226. TTA r /aaA 7 op itt n i / ObUl U 1 11.9 0.6 PAA 80SEG 01 230. 10.6 TTMA i in/A / j on H U

11.9 0.4 6 PAA 82SEG 01 230. 12. OES 7 f,UF u n 1 12. 0.5 GAMMA 7 3 ABE 01 230. 30. 35 IENA Rdr.i OUy LmtXa n ^ \J J 12. ITNA 7 8 WEA 01 230. 10. 35 ITNA 81GLA 02

12. 0.5 D* NAA 740ND 01 230. 10. ITNA 78LAU 02

12. 0.5 GAMMA 750ND 01 233. ICPES 80FL0 01 12.1 0.8 13 PAA 81SEG 01 o o /. Z34. 34

ITNA 81 WAN 01 12.1 2. 35 RTNA 75GLA 01 2 35

13. D* NAA 740ND 01 12.2 0.6 IENA 77R0W 04 235

15. ITNA 7 smsm ni 12.2 1

13 PAA 81SEG 01 237 . 20. ITNA 77R0W 03

12.4 0.6 IENA 77R0W 03 237

20. ITNA 76STE 05

12.7 0.5 IENA 76STE 05 237. 9. ITNA 7 7MAE 01 12 .8 ITNA 80EDD 01 240. T *PM A ITNA 7 5KLE 0

13.5 1.2 ITNA 76STE 05 270. 60. T Ttl A ITNA 7 60ND 01 13.8 * ITNA 7 SMIL 01 271. 6

C CMC o ono

"7 Of1 TTT A 1 /oOUl Ul 15. * UU 80HEN 01 290. 80. * TTH UNAA /ORAL* Ul

295. 156. * EXRF 77CTA 01 34 (PCi) 410. * AA 7 fiWEW 0

4.07 0.12 NM 8 OCAS 01 w (ppm)

4.07 0.12 D* NM 81 CAS 01

19

L* EXRF 77CITA 01 35 (PCI) 3 .8 0.7 ITNA ftO 11 UAWAINM 01\J I 3.9 0.4 T I7M A IENA //RUW U4

0.179 0.012 NM 80CAS 01 4. 0.4 TFNA l&NA 7 7 DAI.T A T

/ / tuJW U J 0.179 0.012 D* NM 81 CAS 01 4.2 0.4 IENA 76STE 05

4.5 1. D* ITNA 78RYA 01

:38 (PCI) 4.5 1. TTHA 1 "7 /"TJ A A 1 / /CHA Ul

4.6 T TXT A 1 INA T Ol TT? A 1 /owEA 01 4.01 0.04 NM 80CAS 01 4.6 1.6 TTMA 1 INA 7 RAKiT\ A 1 / jUND U

4.01 0.04 D* NM 81 CAS 01 4.8 1.5 TTMA 1 INA 7£.AXTA Al / OUINU U 1 4.9 0.7 35 RENA ft 1 fT A n ^ ppm) 5. UU 80HEN 01

5. 1

35 IENA 80GLA 03

200. L* XRF 81C0H 02 5.2 0.3 35 RTNA 78GLA 02

151

*6 SSMS 78GUI 01 j.j s s 1X.Js ITNA 76RAG 01

17455. XRF ~tCk CUT A 1 /ysMi ui 5.8 U. J

s jj NAA 81GLA 04

inn 182 - vt>r /oLArl UZ £O .

il

ITNA 78MAC 01

1 ft A C A50. 1 CGfe fyrAL Ul 19 7 i

i i • i ITNA 7 3 SHE 01

1 ft A 190C A50. D* TCGS oUAND Ul

196. 10. ITNA 78MAC 01 V fnmnl

200. UU 80HEN 01

iU . 200. 34. EXRF 78PEL 01 It UU 80HEN 01 201. 6. FAA 760WE 01 44

4.2 OES 76WEW 01 204. 15. ITNA 76BL0 01 60. 8. PAA 77CHA 01 208. 12. PAA 74CHA 01 60. 5. EXRF 77GIA 01 210. OES 78SUG 01 62. 10. PAA 750ND 01

210. 12. D* PAA 77CHA 01 65. ICPES 80FLO 01

210. 12. PAA 76CHA 01 66.. XRF 78CAM 02

216. AA 78GUI 01 66. 2. PAA 76KAT 03

216. EXRF 78WEG 01 67. 1. PAA 76KAT 02

146
TABLE X (cont) TABLE X (cont)

ANAL KEF KEF CONC " UNCER COMMENT METH i CODE NUM

68. 16. SSMS 78SUG 02

68. 1 . XRF 1 A OUT A

1

79SMI Ul 150. 15. * 14NAA 81WIL 02

150. 7. * 14NAA 81WIL 01

( n rani

A 7 o a ITNA

A R U .0 TTNA x xha / DWLH U

1

c c

-> - J U.J TTNA 7ftT AIT ft? j • j 1 .4 ITNA 78NAD 02

5.53 0.14 ITNA 75NAD 02

5.7 0.56 OES 76WEW 01 5.7 0.6 ITNA 760ND 01

5.9 0.3 IENA 77R0W 04

5.9 0.3 ITNA 76RAG 01

6.1 0.18 ICPES 81CHU 01

6.2 3.4 ITNA 7 3 SHE 01

6.2 0.2 5 ITNA 77R0W 04

6.6 0.4 D* ITNA 77R0W 04

ft A 0.4 ITNA 77R0W 03

A ft 0 • o TTNA 1 XWA 7^MTT ftl

/ . TPTJF c

7/ • o

3 • TTNA 1 IMA 7 ^ftun ft

i

7.2 2.1 D* ITNA 78RYA 01 7.2 2.1 ITNA 77CHA 01

8. 0.5 35 ITNA 81GLA 03

8.

A

0.6 ITNA 81 WAN 01 8.9 0.9 * ITNA 7 3ABE 01

9. 1.4 * SSMS 78SUG 02

(ppm)

420. L* 14NAA 81WIL 01

300. L* 14NAA 81WIL 02

1 80 7 A. * AA 74GAL 01 71£. 3 . RTNA 740RV 01

1 Q ft AAAA 7RCITT 01 zuu

.

F YUTT l. Ar\.r 7ftUFfi 01

7 aa ZUU • If 11 ftftHFN 01

7 a. a zuu

.

7ft zu TTNA X XWA 77CHA 01 LUU e QO . IENA 77ROW 04

200

.

10. EXRF 78PEL 01 200. 20. ITNA 78LA0 02

200. 20. D* ITNA 78RYA 01

200. 10. 9 ITNA 78LAU 02

200.5 4. RTNA 74GAL 01

201

.

6. ITNA 77ROW 03

201

.

8. AA 760ND 01

20 1

.

6

.

D* ITNA 77R0W 04

201

.

ISP i »p 77TJI7T ni 202

.

AW 1 OL»ATl \M. OA A 204 . 1Z . 3J FAA r AA

204. 13. 5 IENA 80GLA 03

70S XUin . u PAA 82SEG 01 205. 20. PAA 80SEG 01

206. 73 ITNA 81 WAN 01 207. ITNA 78WEA 01 208. 9.5 AA 80ST0 02

208. XRF 75KLE 01 208.1 24. ITNA 74GAL 01

208.2 3.6 AA 77MIT 01

210. 36. OES 76WEW 01

ANAL KEF KEF CONC tUMMLPi 1 i"h^ :i h i CODE NUM

210. OES 78SUG 01

210. ICPES 80NAD 01 211. ICPES ouLro u J 7 1 7 1

A

TTNA X xnA 7ftNAH A7

Z 1Z a

1

A

UNA 1 CUAA AO Oil Z 12 • ICPES 80FL0 01 Oil Z 1Z • Oft ZU • FAA T ^ Aim rt i 760WE 01

Z 1Z . 7 AK_r *?0 CUT fi . / V brll U

1

1i « AIU 7APAT ftl 214. AA 7ftGET. 01 214. 2. AF 75EPS 01 214. 16. PAA 74CHA 01 214. 2. AA 75EPS 01 215. 20. NAA 77JER 01 215. 20. PAA 76CHA 01 215. 20. D* PAA 77CHA 01 216. FAA ftOUAT 0

1

7 1

A

£ XO . 7 1* n* NANAAA 7Aftwn /HUNU ftl Ul

7 1 A Z ID » <)C I J . TJ A A rAA /DUNU Ul

7 1A 2 XO • 14 . EXRF 77GIA 01

Z xo

.

Z .4 AA T A T> A T A » 74RAI 0

1

7 10 / X7 • 4 • / y Lr o U

1

770 101U . £D PAA IT AA fto^F/: ftl 220

.

5. ITNA 7nftisin ni 220. 130. ITNA 76BL0 01 221. 16. 5 IENA 80GLA 03

221. AA 79SIL 01 221. 16. 35 NAA 81GIA 04

228. 6.9 ICPES 81CHU 01

230. 40. ITNA 76RAG 01

234. AA 7f.WFR 01 250. * AA 76WEW 01 270. *6 SSMS 78GUI 01 270. 30. * ITNA 78MAC 01 283. *6 SSMS 78GUI 01

loft is * TTNA X XPl A 7nn 77H TTMA X INA

2r CoDm)

160. 34. * OES 76WEW 01 182. 76. ITNA 76RAG 01 200. UU 80HEN 01 223. 6.7 ICPES 81CHU 01 286. 8. 35 IENA 81GLA 04

288. ICPES 80FL0 01 290. 20

.

5 IENA

7Q0 A7 VJ . 7 Ej Atvr 77TTA ftl / iKjIA U

1

70Z70.ft xu

.

TJ A A rAA / OKA! (J J Z77Q ftO . c0 . DA A

/ ONAl U Z 70 XI" JrAA PAA 77PHA ftl 300. 20

.

PAA 7fifHA 01 301

.

22. PAA 74CHA 01 301. 20. PAA 750ND 01

305. XRF 78CAM 02

310. 20. ITNA 77CHA 01 310. 20. 9 ITNA 78LAU 02

310. 70. D* IENA 77R0W 04

310. 20. D* ITNA 78RYA 01 310. 70. IENA 77R0W 03

311. 8. XRF 79SMI 01

340. 50. 5 IENA 80GLA 03

380. 20. 14NAA 81WIL 02

147
TABLE Y

TABLE X (cont)

CONC UNCER

20.

140.

COMMENT

ANAL

METH

REF CODE

KEF NUM

ITNA 77R0W 04

14NAA 81WIL 01 ITNA 75MIL 01 ITNA 7 3 SHE 01

NBS SRM 1633A—COLLECTED DATA

CONC

Ag (ppb)

Al (Z)

13.8

14.

14. 14.2

14.2

14.2

14.5

14.7

14.81

15.

UNCER

600.

1100.

COMMENT

L*

0.32

0.2

0.2

0.3

0.3

0.4

0.12

0.7

0.2

0.43

D*

35

35

ANAL

METH

IENA

ITNA

ITNA

TCGS

TCGS ITNA ITNA

ITNA AA

ITNA ICPES

CPXRF

HEF CODEREF NUM

80GLA 03

82SUZ 02

820BR 01 80AND 01 79FAI 01

81G1A 02

80GAR 01 81G1A 04

82NAD 02

82SUZ 02

82 NAD 02

80KIR 01

As (ppm)

97. 141.

142.

143.

145.

145.

145.

145.3

148.

18.

8.

8.6.

11.8.1

3.

35

35

CPXRF

AE+AF

ITNA RTNA

VV

ITNA

IENA

ITNA IENA

80KIR 01 82MAT 01 81SL0 01 81SL0 01 81GLA 04

82SUZ 02

82GLA 02

820BR 01 80GLA 03

B (ppm)

39

3939

3941

I.3.0.7

0.7

2.

35

D*

ICPES

TCGS

TCGS

TCGS

TCGS

820WE 01 81GLA 04

79FAI 01

80AND 01

83GLA 03

Ba (ppm)

1060.

1100.

1210.

1240.

1400.

1440.

1450.

1490.

1500.

1500.

1500.

1520.

1600.

1760.

Br (ppm)

100.

50.

200.

20.

36. 110.

80.

100.

90.

200.

20.

300.

S

55

35

35

5

ITNA

ITNA

ITNA

IENA

IENA

ITNA NAA

ITNA

CPXRF ITNA

ITNA

IENA ICPES IENA

82GLA 02

82SUZ 02

82SUZ 02

80GLA 03

80GLA 03

820BR 01 81GLA 04

83GLA 01 80KIR 01 80GAR 01 81GLA 02

80GLA 03

82NAD 02

80GLA 03

2.2

2.4

10.0.3

0.1

L*

5

IENA ITNA IENA

80GLA 03

82SUZ 02

80GLA 03

148
TABLE Y (cont) TABLE Y (cont)

CONC

Ca (%)

UNCER COMMENT

ANAL

METH

REF KEF CODE NUM

1.05 0.16 35 ITNA 81GLA 02 1.09 0.01 AA 82NAD 02

1.1 0.3 35 IENA 80GLA 03

1 .1 0 .

1

is ITNA ftl OlutilLinA DA

1.11 0.076 ITNA 820BR 01 1.11 0.03 ICPES 82 NAD 02 1.12 0.08 ITNA 80GAR 01 1.14 0.04 AA 82GLA 02

1.16 0.21 ITNA 82SUZ 02

I • Z u • uo nnv TD Ct 1 U 1

1

1 • 9QZ7 Ui 11 A 7QPAT U 1

1

\ »Z79Q U . 1 1 n*U" OUAW1J U 1

(.ppm;

1 A T TW A Q9 CTI

7

UZ

1.07 0.05 TCGS 79FAI 01 1.07 0.05 D* TCGS 80AND 01

(ppm)

163. 6. ITNA 82GLA 02

167. 8. ITNA 82SUZ 02

170. 6. 35 ITNA 81GLA 02

1 7 A cJ - 1 Z 1 1NA Q*> CTI7 lOU • cJ . \t A A NAA

18 5 .

1 O ITNA 80GAR 01 loo. 35 IENA 80GLA 03

1)0. /. c HD . CPXRF 80KIR 01

. . ( ppm)

69. L* ITNA 82SUZ 02

(ppm)

37

.

3. 35 IENA 80GLA 03

38

.

13. CPXRF 80KIR 01 40. ITNA 82GLA 02 44. 1

.

ITNA 82SUZ 02 44. 1

.

35 ITNA 81GLA 02 44.8 0.8 ITNA 83GLA 01

A A 9 i ft x *o ITNA

47. 4. 35 NAA 81GLA 04

(ppm)

185. 7

.

ITNA 82SUZ 02

186. 8. 35 ITNA 81GLA 02

191 . 13. ITNA 82GLA 02

192. ICPES 81WAL 01

194. 6. 12 ITNA 82SUZ 02

195. 7. ITNA 83GLA 01 197. 18. 35 ITNA 81GLA 04

197. 13. ITNA 80GAR 01 200. 11. CPXRF 80KIR 01

(ppm)

9.3 0.5 ITNA 82GLA 02 9.7 0.6 35 ITNA 81GU 02

CONC

9.9

10.1 10.2

10.5

10.6

Cu (ppm)

120.

Dy (ppm)

14.3

14.5

15. 16.6

16.8

Eu (ppm)

2.2.98

3.19

3.6 3.64

3.7

3.7

3.7

Fe (%)

8.84

8.88

9.21

9.23

9.36

9.4

9.4 9.49

9.5

9.5

9.7 9.7

9.7

Ga (ppm)

51.

55. 55.7

56.

59.

Gd (ppm)

15.3

23.5

H20-T (%)

0.35

UNCER

0.9 0.2

0.2 0.3

1.1

350.

5.2

0.2

3.3

1.3 0.3

2.0.33

0.08

0.1 0.25

0.2

0.2 0.3

0.07

0.1 0.09

0.49 0.3

0.1

0.1 0.3 0.3

0.2

0.2 0.2

5.4.6

4.5

1.

COMMENT

35

35

L*

35

35

35

35

ANAL

METH

ITNA IENA ITNA NAA

ITNA

*35

35

35

3535

12

5

D*

REF REF CODE NUM

83GLA 01 80GLA 03

82SUZ 02

81GLA 04 80GAR 01

ITNA CPXRF

ITNA

ITNA ITNA ITNA

ITNA

IENA

ITNA

ITNA ITNA

ITNA ITNA

ITNA

ITNA

AAAA

ICPES

ITNA NAA

ITNA IENA ITNA

ITNA

ITNA

IENA TCGS

TCGS

ITNA

CPXRF ITNA

IENA

IENA

TCGS TCGS

FD

82SUZ 02 80KIR 01

81GLA 02 81GLA 04

820BR 01 80GAR 01 82SUZ 02

80G1A 03

80GAR 01 81GLA 02

83GLA 01 820BR 01 82GLA 02 81GLA 04 82SUZ 02

82GLA 02 82NAD 02

82 NAD 02

81GLA 02 81GLA 04

82SUZ 02 80GLA 03

83GLA 01 80GAR 01 82SUZ 02

80GLA 03

79FAI 01 80AND 01

82SUZ 02 80KIR 01 820BR 01 81GLA 04

80GLA 03

79FAI 01 80AND 01

80KHA 02

149
TABLE Y (cont) TABLE Y (cont)

CONC

Hf (ppm)

UNCER COMMENT

ANAL

METH

KEF EEF CODE NUM CONC UNCER COMMENT

ANAL

METH

REF CODEREF NUM

6.3

6.6

7.2

7.2

7.4

7.6

7.78

7.8

Hg (ppm)

150.

151.

I (ppm)

In (ppb)

151.

160.

K (%)

1.8

1 .82

1 .84 1.86

1 .86

1 .88 1.88

1.93

1 .96 1.97

1.97

1.99

La (ppm)

62.

79.

81

83.

84.

84.

87.9

100.

Lu (ppm)

0.93

0.97

1 .44

0.7

0.3

0.8

0.4

0.2

0.85

0.2

0.63

0.42

10.

12.

5.

16. 30.

0.07

0.14

0.089

0.12

0.1

0.04

.03

.02

.04 .04

.03

1. 4.

2.

6.

7. 23.

0.09

0.25

0.12

9

35

35

35

L*

L*

L*

35

D*

35

35

35

*

ITNA ITNA

ITNA ITNA

ITNA

NAA

ITNA

IENA

ITNA

ITNA CVAA

CVAA

ITNA

ITNA

ITNA

CPXRF ITNA

ITNA

ITNA

ITNA ITNA

ICPES

AA

AA

TCGS

TCGS IENA

ITNA ITNA

ITNA

ITNA ITNA

IENA

ITNA

ITNA

ITNA ITNA

ITNA

82SUZ 02

82GLA 02

81GLA 02

82SUZ 02

83GLA 01 81GLA 04

80GAR 01 80GLA 03

82SUZ 02

82SUZ 02

82GLA 02

82D00 01

82SUZ 02

82SUZ 02

820BR 01

80KIR 01 83GLA 01 80GAR 01 820BR 01 82SUZ 02

81GLA 04

82 NAD 02

82NAD 02

82GLA 02

79FAI 01 80AND 01

80GLA 03

82SUZ 02

83GLA 01 82GLA 02

81GLA 04

82GRA 01 80GLA 03

820BR 01 80GAR 01

80GAR 01 82GLA 02

82SUZ 02

Mg (ppm)

3800. 700. CPXRF 80KIR 01 4200. AA 82GLA 02

jUU • TTNA p.rir at? 4590. 30. AA 82NAD 02

4600 .. 70. ICPES 82NAD A 1 8000 1300 - K ITNA Bz SUZ A 1

Mn (ppm)

170. 24. ITNA 82SUZ 02

182. 3. 35 ITNA 81GLA 02

IOC 185. 11

ITNA A ^ Ann 820BR 01 190. 15. TCGS 79FAI 01

190. 15. D* TCGS 80AND 01 191. 4. ITNA 80GAR 01 195. 15. CPXRF 80KIR 01 210. 50. 35 ITNA 81GLA 04

230. ICPES 82NAD 02

260. 20. 35 IENA 80GLA 03

277. 7ITNA 83GLA 01

Mo (ppm)

27. 6. ITNA 82SUZ 02

30. 4.2 CPXRF 80KIR 01 36. 1. 35 IENA 80GLA 03

Na (ppm)

1560. 70. AA 82NAD 02

1680. 90. ITNA 820BR 01 1700. 70. ICPES 82NAD 02

1720. 50. ITNA 80GAR 01

17 30. 10. ITNA 83GLA 01 1740. 100. 35 ITNA 81GLA 04

17 50. 50. ITNA 82SUZ 02

1760. ITNA 82GLA 02

1800. 100. 35 ITNA 81GLA 02

2020. 400. ITNA 82SCH 05

2100. 600. * TCGS 79FAI 01

2100. 600. D* TCGS 80AND 01

o *>aa zzuu Ann * CPXRF 80KIR 01

Nd (ppm)

65.6 5.4 TCGS 79FAI 01 66. 5. TCGS 80AND A 1 0

71

3. 35 IENA 80GLA A O 03

1 13. 7. ITNA O O CTT *7 oz bUz A O Uz 122. 13. *12 ITNA 82SUZ 02

Ni (ppm)

112. 4.8 CPXRF 80KIR 01 117. 6. 35 IENA 80GLA 03

128. 6. ITNA 82SUZ 02

139. 7. 12 ITNA 82SUZ 02

150
TABLE Y (cont) TABLE Y (cont)

CONC

0 (Z)

47.66

P (ppm)

1700.

1800.

2000.

Pb (ppm)

65.

Pr (ppm)

17.9

18.9

Rb (ppm)

124.

130.

134.

134.

138.

147.

150.

163.

S (ppm)

2700.

27 00.

Sb (ppm)

6.3

6.6

6.95

7.3

7.7 7.8

Sc (ppm)

34. 34.

36.

39. 40.

40.6

41.

43.

Se (ppm)

7.8

8.8

9.4

9.4

UNCER COMMENT

ANAL

METH

KEF KEF CODE NUM CONC UNCER

0.36

300.

5.7

1.7

1.1

4. 26.

16.

8.8.

8. 12.

2.

114000.

200.

200.

0.2

0.22

0.2

0.5

1.5

2.1 0.4

0.5

0.3

34

12

35

1235

35

L*

D*

35

35

35

35

35

9

35

14NAA 80KHA 02

XRF

ICPES

AA

ITNA

ITOA

ITNA ITNA NAA

ITNA ITNA

ITNA CPXRF

IENA

ITNA TCGS

TCGS

ITNA

ITNA

ITNA RTNA

IENA

ITNA

CPXRF ITNA ITNA

ITNA

ITNA ITNA

ITNA IENA

CPXRF

ITNA RTNA

RTNA

81TUR 01 82NAD 02

82NAD 02

CPXRF 80KIR 01

82SUZ 02

82SUZ 02

82SUZ 02

80GAR 01 81GLA 04

83GLA 01 82SUZ 02

81GLA 02

80KIR 01

80GIA 03

82SUZ 02

79FAI 01

80AND 01

82SUZ 02

82GLA 02

81GLA 02

81SL0 01 80GLA 03

80GAR 01

80KIR 01 82SUZ 02

82GLA

83GLA

81GLA 02

80GAR 01 81GIA

02

01

04

80GLA 03

80KIR 01 82SUZ 02

81SL0 01 81GLA 01

10. 10.2

10.7

Si (%)

18.

22,

22,

23.37

23.9

23.9

24.2

Sm (ppm)

14.!

16- 16.

16

16

4

7 18.8

19.4

20.

Sr (ppm)

740.

770.

813.

815.

819.

825.

840.

840.

850.

Ta (ppm)

1.71

1.8 1.8

1.8 1.94

2.2.1

Tb (ppm)

2.1

2.1 2.3

2.8

2.9

Te (ppm)

2.0.6

0.8

0.93

0.4

0.4

0.23

0.5

0.5

0.8

COMMENT

35

ANAL

METH

REF CODE

REF NUM

0.6

0.7

4.4

20.

70.

7. 54.

40. 40.

30. 70.

0.05

0.2

0.1

0.12

0.5

0.2

0.1

0.2

0.7

0.5

0.1

6.6

35

D*

35

35

D*

*5

35

12

5

35

35

35

35

35

L*

IENA ITNA NAA

CPXRF

TCGS

TCGS

ICPES

AA

IENA AA

ITNA

TCGS

TCGS ITNA

ITNA

ITNA

ITNA

ITNA

IENA IENA

ITNA IENA

ITNA

CPXRF ITNA

IENA

ITNA

ITNA NAA

ITNA ITNA

ITNA

ITNA

IENA

ITNA ITNA

ITNA NAA

IENA

ITNA

80GLA 03

82SUZ 02

81GLA 04

80KIR 01 79FAI 01 80AND 01

82NAD 02

82GLA 02

80GLA 03

82 NAD 02

81GLA 04

79FAI 01 80AND 01 82GLA 02

83GLA 01 820BR 01 82SUZ 02

80GAR 01

80G1A 03

81GLA 04

820BR 01 83GLA 01 80GAR 01 80KIR 01 82SUZ 02

80CLA 03

82SUZ 02

82SUZ 02

81GLA 04

83GLA 01 81GIA 02

82GLA 02

80GAR 01

80G1A 03

82SUZ 02

83GLA 01 80GAR 01 81GLA 04

80GLA 03

82SUZ 02

151
TABLE Y (cont) TABLE Y (cont)

ftriAL AM A I UF REF ANAL REF REF UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

(ppm) W (ppm)

11 .4 TTHA 1 IMA 82GLA 02 5.4 0.4 35 IENA 80GLA 03

24.3 3.8 ITNA OZ 5.4 0.8 ITNA 820BR 01

n Q jj MA A 81GLA 04 «; A 0.4 D* NAA 81GLA 04

1 . 1 35 ITNA 81GLA 02 j . 7 U • 4 ITNA 82SUZ 02

24 .8 1 .6 80GAR 01 c a 0.5 1 .2 RENA 82GLA 02

24.8 0.5 ITNA 83GLA 01 25. 1. 35 IENA 80GLA 03 Yb (ppm)

26. 1.3 12 ITNA 82SUZ 02

28. 8.3 * CPXRF 80KIR 01 6.9

7.5

0.3

0.5 ITNA

ITNA 82SUZ 02

82GLA 02

(ppm) 8.2 35 ITNA 81GLA 04

10. 1.8 ITNA 80GAR 01 7800. 300. ITNA 82SUZ 02

7880. 540. ITNA 820BR 01 Zn (ppm)

8000. 600. 35 NAA 81GLA 04

8000. 800. CPXRF 80KIR 01 2 18

18

CPXRF 80KIR 01 8060. 370. ITNA 80GAR 01 220. 50. ITNA 80GAR 01 8200. 700. 35 ITNA 81GLA 02 222. 7. 5 IENA 80GLA 03

8300. ITNA 83G1A 01 230. AA 82GLA 02

o/. fin inn 1UU

3D T CM A 80GIA 03 250. it ITNA 82SUZ 02

8400. 100. TCGS 79FAI 01 250. 30. ITNA 82SUZ 02

8400. 60. ICPES 82 NAD 02 256. 12. 5 IENA 80GIA 03

8400. 100. D* TCGS 80AND 01 9000. * AA 82NAD 02 Zr (ppm)

(ppm) 300.

370.

30. 50.

5

5

IENA

IENA

80GLA 03

80GLA 03

4.4 1.3 CPXRF 80KIR 01 400.

410.

50.

40.

12 ITNA ITNA

82SUZ 02

82SUZ 02 U (ppm)

9.83 0.9 * IENA 820BR 01 10.2 0.3 DMA 82GLA 02

10.2 0.1 35 IENA 80GLA 03

10.2 0.2 DNA 80GAR 01 10.3 0.4 ITNA 82SUZ 02

10.4 0.3 17 DNA 82C0N 01

10.4 0.8 DNA 83GLA 01

10.47 0.09 35 DNA 80GLA 01

10.6 0.4 35 NAA 81GLA 04

10.7 0.3 17 DNA 82 CON 01 11. 2.7 * CPXRF 80KIR 01

>pm)

280. ICPES 81 UAL 01

280. 18. CPXRF 80KIR 01

288. 20. ITNA 820BR 01 290. 20. 35 IENA 80GLA 03

290. 20. ITNA 82SUZ 02

292. 16. 35 ITNA 81GLA 02

294. 28. 35 ITNA 81GLA 04

301. 8. ITNA 80GAR 01 360. 40. * TCGS 79FAI 01 360. 40. D* TCGS 80 AND 01

c

152
TABLE Z

NBS SRM 1634—COLLECTED DATA TABLE Z (cont)

CONC UNCER COMMENT

ANAL

METH

KEF CODE

REF NUM

As (ppb)

400. EXRF 79GIA 01 56. ITNA 77FIL 01 63. 3. ITNA 78BER 02 70. ITNA 78WEA 01

95. RTNA 740RV 01

120. ITNA 81SHA 01

Au (ppb)

24. ITNA 73SHE 01

Br (ppb)

39. ITNA 77FIL 01 39.1 5.3 UU 77PAC 01 AO. ITNA 78WEA 01

A 1 . ITNA 78BER 02 240. 70. * ITNA 7 3 SHE 01

Ca (ppm)

15

.

2. ITNA 7 3 SHE 01

Cd (ppb)

10. L* RTNA 740RV 01 5. FAA 74RAI 01

CI (ppm)

7.8 0.5 UU 77PAC 01

ao

.

T TTvl A 1 LviA 7 QLTTT A / OWEiA A 1 U 1 8.4 0.5 ITNA 78BER 02

18. 0.7 * ITNA 73SHE 01

Co (ppb)

in T TM A 1 IPiA 7 o cup U 1 301. ITNA 77FIL 01 Jul .

1 A TTIT UU 7 7D a r* A 1 U 1 310. 15. ITNA 78BER 02

400. ITNA 78WEA 01

Cr (ppb)

6000. L* EXRF 79GIA 01 80. ITNA 81SHA 01 93. ITNA 77FIL 01 100. ITNA 78WEA 01 116. 35. ITNA 7 3 SHE 01

Cu (ppm)

800. L* EXRF 79GIA 01 220. 20. ITNA 7 3 SHE 01

CONC

Fe (ppm)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

10 .8 3.3 EXRF 78KUB 01 12.3 POL 74MAI 01 12.4 1.6 ITNA 73SHE 01 12.5 2.2 UU 77PAC 01 13. ICPES 79MER 01 13.5 1 .2 ITNA 81 SHA 01

14

.

1 .5 EXRF 79GIA 01

14 .

1

AA 74RAI ni 14.2 1.5 ITNA 78BER 02

14.4 1.7 32 EXRF 78KUB 01 15.1 2.4 32 EXRF 78KUB 01 16.2 2.8 32 EXRF 78KUB 01 16.9 2.5 32 EXRF 78KUB 01 20. ITNA 77FIL 01

25. * ITNA 78WEA 01

Da / ri nL \

10

.

L* ITNA 81 SHA LI I

Li TTTJA L LriA 77FT1 U 1 7Anpv U 1 22. 15. ITNA 7 3 SHE 01

K (ppm)

315. ITNA 77FIL 01

Mn (ppb)

Trppc 7QMC D ft 1

Li Ej AK-T 7QTT A / V\3 Art U 1

1 10

.

in ITNA / ODL rv VJ L 190. ITNA 73SHE 01 200. ITNA 81 SHA 01 320. ITNA 78WEA 01

Mn ( nnS

lav \yyuj

A7H Qf. OU • T *HM A I 1 W A

Via \ JJ pUl }

11.2 ITNA 77FIL 01 11.2 0.7 UU llSkC 01

12. ITNA 78WEA 01 13.2 1.5 ITNA 78BER 02

Nl (ppm)

31.1 2.1 AA 74RAI 01

32. 2. 32 EXRF 78KUB 01 32. 1.6 EXRF 79GIA 01 32. 1. 32 EXRF 78KUB 01 33. 1. 32 EXRF 78KUB 01 35. 2. 32 EXRF 78KUB 01

153
TABLE Z (cont) TABLE Z (cont)

ANAL REF REF CONC LUMMtn 1 Mt | n

rnt\r fern in CODE NUM

JJ •/ DAT 1AJO •

i 10JZ 7/OP.UD ftVTIft niUl

36 .7 ICPES /VMER Ul

Z

TX TWA inn 7ARFR D? 37.4 I TOA 77FIL 01 37.4 1.5 UU 77PAC 01 38.1 6 IDMS 74MOO 01

38.1 6 IDMS 74M00 01

id o Jo • Z

£.D IDMS 7*»nUU Ul

1Q Z • ZD TUNA TM A 71CUP A1 /Jbnb Ul

Pb (ppb)

500. * ICPES 79MER 01 1500. EXRF 79GIA 01 41. POL 74MAT fil JU • f An 7APAT C\ 1

S (%)

2 . 0.1 TITR 80MCC 01

2

0.2 MECA 80MCC 01

2 .04 0.39 ITOA 73SHE 01 2.05 0.4 UU 77PAC 01 2.154 0.009 IC 80MCC 01 2.17 XRF 80MCC 01 2.24 0.05 ICPES 81WAL 02

9 94 TTNA L IDA fll QUA ni

2 .3 0.3 ITOA 7RRFR (19

Sb (ppb)

10. ITOA 77FIL 01

10. ITOA 78WEA 01

14. 3. ITOA 73SHE 01

Se (ppb)

138. 60. * RTOA 740RV 01 170. ITOA 77FIL 01

19030

ITOA 73SHE 01 Odd TTMA 1 1NA /OWE. A Ul

V ( Ttnm\

-

266. 18

ITOA 73SHF 01

9R 1 1 9 7QrT A m

jUU • TTMA R 1 GUA n

Ol OHA U 1 JO J

1 oId . 3Z EXRF /oKUB 01 310. ITOA 78WEA 01 310. 5. 32 EXRF 78KUB 01 311

7

32 EXRF 78KUB 01 312

16 .4 UU 77PAC 01 314

ICPES 79MER 01 317. 6. GC 81DIL 01

318. 15. ITOA 78BER 02

323. 9. 32 EXRF 78KUB 01 325. 11. 32 EXRF 78KUB 01 326. 6.8 AA 74RAI 01

CONC

Zn (ppb)

170.

300.

480.

ANAL REF REF UNCER COMMENT METH CODE NUM

1000. L* ITOA 81SHA 01 600. * ICPES 79MER 01

600. L* EXRF 79GIA 01 20. RTOA 740RV 01 ITOA 78WEA 01 120. ITOA 7 3 SHE 01

s

154
TABLE AA

NBS SRM 1635—COLLECTED DATA

TABLE AA (cont)

CONC

Ag (ppm)

Al (ppm)

3000.

3000.

3400.

3400.

3400.

As (ppb)

280.

320.

330.

400.

440.

700.

700.

Ash (X)

4.8

B (ppm)

104.5

105. 105.

135.

Ba (ppm)

67.

70. 72.

77. 81.

Bi (ppm)

Br (ppm)

1.07

1.6 1.9

3.

UNCER COMMENT

2.5

0.038

300.

300.

400.

400.

400.

20.

50. 50.

400.

2.6

3.

3. 11.

2800.

20.

9.

17. 24.

C (%)

59.

59.

59. 66.23

170.

0.17

0.3

0.2

3.3.

3.0.06

L*

D*

*34

34

D*

L*

9

5

34

L*

L*

534

D*

D*

ANAL

METH

WXRF

ITNA

ITNA

ITNA

TCGS

TCGS

TCGS

HAA

FAA AF

ITNA RTNA

ITNA WXRF

CB

TCGS

TCGS

TCGS

ITNA

ITNA

ITNA ITNA ITNA

ITNA WXRF

WXRF

ITNA ITNA

ITNA

ITNA WXRF

TCGS

TCGS

TCGS

CB

REF CODE

REF NUM

82MIL 01 82SUZ 02

80GER 01 82SUZ 02

80GER 01 79FAI 01

80AND 01

82NAD 01

82WIL 01 82WIL 01

82SUZ 02

78GAL 01

80GER 01 82MIL 01

82MIL 01

79FAI 01 80GER 01

80AND 01

82SCH 05

80TOU 01 82SUZ 02

80GER 01 80T0U 01

82SUZ 02

82MIL 01

82MIL 01

80T0U 01

82SUZ 02

80GER 01 80T0U 01

82MIL 01

80GER 01 79FAI 01

80ANT) 01

80SCH 02

CONC

Ca (ppm)

5400.

5400.

5400.

5500.

5700.

Cd (ppb)

29.

Ce (ppm)

3.3

3.4

3.5

8.

CI (ppm)

26.

26. 26.

26.

36.

Co (ppm)

0.62

0.7

0.59

Cr (ppm)

2.2.3

2.48

2.5

2.6

Cs (ppb)

46.

53.

Cu (ppm)

3.3.56

Dy (ppb)

310.

UNCER

200.

200.

200.

900.

700.

3000.

380.

3.

0.2

0.2

0.5

30.

2.

2.4.

2.

0.06

0.06

0.2

0.08

0.2

0.3

500.

5.6.

46.

0.18

740.

2000.

40.

COMMENT

ANAL

METH

REF REF CODE NUM

D*

D*

L*

12

*34

L*

D*

D*

34

34

34

12

L*

34

L*

L*

TCGS

TCGS

TCGS ITNA

ITNA

WXRF

ITNA RTNA

ITNA

ITNA

ITNA WXRF

ITNA TCGS

TCGS

ITNA

TCGS

WXRF

ITNA WXRF

ITNA

WXRF ITNA

RTNA

ITNA

ITNA

WXRF

ITNA

ITNA

ITNA WXRF RTNA

ITNA WXRF

ITNA

79FAI 01 80GER 01 80AND 01 82SUZ 02

80GER 01

82MIL 01

82SUZ 02

78GAL 01

82SUZ 02

82SUZ 02

80GER 01 82MIL 01

82SUZ 02

80GER 01 79FAI 01 SOGER 01 80AND 01 82MIL 01

82SUZ 02

82MIL 01

80GER 01

82MIL 01 80GER 01 78GAL 01 82SUZ 02

82SUZ 02

82MIL 01 80GER 01 82SUZ 02

82SUZ 02

82MIL 01

78GAL 01

82SUZ 02

82MIL 01 80GER 01

155
TABLE AA (cont) TABLE AA (cont)

ANAL REP REF UNCER COMMENT METH CODE NUM

Eu (ppb)

59. 61.

F (ppm)

20.

Fe (ppm)

2200.

2200.

2200.

2300.

2330.

2340.

Ga (ppm)

1 .1

Gd (ppb)

230.

350.

Ge (ppm)

0.5

H (%)

3.96

3.96

3.96

4.18

H20-T (%)

14.

Hf (ppb)

240.

270.

290.

Hg (ppb)

2000.

1000.

2.

7.

100.

100.

100.

200.

240.

140.

1500.

10. 20.

0.03

0.03

0.03

0.14

5. 35.

2000.

40.

40.

20.

1500.

56.

15.

11.

L* WXRF 82MIL 01

L*

D*

D*

12

12

L*

34

L*

34

D*

D*

L*

9

L*

L*R*

12

WXRF

ITOA

ITOA

ISE

TCGS

TCGS

TCGS

I TOA

I TOA

ITOA

ITOA WXRF

WXRF

TCGS

TCGS

WXRF

TCGS

TCGS

TCGS

CB

FD

WXRF

ITOA

ITOA

ITOA

WXRF

ITOA

CVAA

ITOA

82MIL 01

82SUZ 02

80GER 01

83KNA 01

80GER 01 79FAI 01 80AND 01

80GER 01 82SUZ 02

82SUZ 02

82SUZ 02

82MIL 01

82MIL 01

79FAI 01 80AND 01

82MIL 01

79FAI 01 80AND 01

80GER 01 80SCH 02

80KHA 02

82MIL 01 82SUZ 02

80GER 01 82SUZ 02

82MIL 01 82SUZ 02

82DOO 01 82SUZ 02

CONC

Ho (ppm)

I (ppb)

600.

In (ppb)

5.

K (ppm)

90.

97.

97.

97.

120.

La (ppm)

1.38

2.2.1

Lu (ppb)

27.

36.

Mg (ppm)

940.

1000.

Mn (ppm)

19. 22.

23.

24.

24.

24.

Mo (ppb)

270.

N (%)

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

1 . 1.

1 . 1.52

1 .5

1300.

860.

300.

1000.

31.

2.

90.

6.

6.

6. 10.

0.07

0.3

2000.

4.

7.

190.

200.

1000.

100.

0.1

0.1

0.1

0.02

L*

L*

L*

L*L*

D*D*

34

L*

34

D*D*

L*

D*

D*

WXRF

WXRF

ITOA

ITOA

WXRF

ITOA

ITOA

ITOA

TCGS

TCGS

TCGS

ITOA

ITOA

WXRF

ITOA

WXRF

ITOA

ITOA

ITOA

ITOA

ITOA

ITOA

WXRF

TCGS

TCGS

TCGS

WXRF

ITOA

TCGS

TCGS

TCGS

CB

82MIL 01

82MIL 01 82SUZ 02

80GER 01

82MIL 01 82SUZ 02

80GER 01

82SUZ 02

79FAI 01

80GER 01 80AND 01

80GER 01

82SUZ 02

82MIL 01

80GER 01

82MIL 01

80GER 01 82SUZ 02

82SUZ 02

80GER 01

82SUZ 02

80GER 01 82MIL 01

79FAI 01 80AND 01

80GER 01

82MIL 01

82SUZ 02

79FAI 01

80AND 01

80GER 01 80SCH 02

156
TABLE AA (cont) TABLE AA (cont)

ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE MUM CONC ' UNCER COMMENT METH CODE HUM

Na (ppm) R ( ntvm^

—

2200. 160. ITNA 82SCH 05 19000. L* TTNA Linn R7QTI7 07

2400. 200. ITNA 80GER 01 JZUU •

1 A A 100. TCGS ^ A T. A T A 1 79FAI 01 2400. 200. ITNA 82SUZ 02 *i oaa JZUU

.

100. D* TCGS 80GER 01 2420. 34 WAKf Q 0 UTT 01 3200. 100. D* TCGS 80AND 01 2700. 50. 7QT?AT / 7ffU 01

2700. 50. D* OUuLK 01 2700. ^ a30 . DK Q A AMR ft i 0

1

1000. L* WXRF 82MIL 01 Nb ( nDnl 120. 10. RTNA 78GAL 01

130 10. HAA 82NAD 01

1 . L* WXRF 82MIL 01 140. 10. ITNA SOGER 01 160. 30. ITNA 82SUZ 02 no vppmj 170. 40. 5 ITNA 80TOU 01

1 .8 L* ITNA ol buz. 02 Sc f onh

** u VFr°/

1.6 L* ITNA 82SUZ 02

1

.

L* WXRF 82MIL 01 1200. L* ITNA 80TOU 01

1 .4 0.2 ITNA 80GER 01 QUA C A50. ITNA 82SUZ 02

07u • 7ft TTMA 1 1NA oubfcK Ul

^ft. c3 TTMA 1 1NA Q ATATT A 1 OUIUU Ul AAA 7UU. 34 WXRF 82MIL 01

1 .72 0.32 ITNA 82SUZ 02 - 1 .83 0.23 12 ITNA 82SUZ 02 Se (ppm)

3. 34 WXRF 82MIL 01

0 (%)

AU • 7QfJ ftU.U/ft7 UA A HAA D O XT A A AT 0 ft ft 7 Kl NA OUIVNA OAVMA AlUl

a qo U .oZ A A A 0.04 OTM A KINA / ObAL U

1

20 .79 ft 1 o ^A 1 A M A A 14NAA ft7 uz 0 .9 AF O 1 T tt T A 1 oZWIL Ul

33. 1 .6 14NAA 80NAD 01 0.9 FAA O^f ITT At 82WIL 01

J** .77 0.32 35 14NAA 8 OKHA 02 0.94 0.11 ITNA 82SUZ 02

0.98 0.09 ITNA 80GER 01

P (ppm) 0.99 0.11 9 ITNA 82SUZ 02

1 .2 *34 WXRF 82MIL 01 oi. 34 Q7MT1 A 1 0 1 Si (ppm)

5200 • 200. TCGS 79FA1 Ul

1 .48 0.21 HAA 82NAD 01 DZUU . 7ftft n*u

QAflTp AT 2.6 34 WXRF 82MIL 01 S900 200. D* TCGS ft HAND 01 5600. 700. 14NAA 80GER 01 Pb-210 (PCi)

A nAi 0.001 NM ft 1 nKJ . (17 U / A AA 1 0 .001 n*DK NM 81 CAS ft i U i OQ ftftft X) uUU . T * L TTMA 1 1NA OUIUU QATA1T A 1 Ul

1000. L* WXRF BzMTL 01 Pr (ppm) 250. 10

.

TCGS 79FAI 01 250. 10. D* TCGS 80GER 01 4.3 L* ITNA 82SUZ 02 250. 10. D* TCGS 80AND 01

1

.

L* WXRF 82MIL 01 270. 10. 5 ITNA 80T0U 01

4.4 L* ITNA 82SUZ 02 300. 40. ITNA 80GER 01 340. 30. ITNA 82SUZ 02

Rb (ppm)

Sn (ppm)

0.3 L* WXRF 82MII. 01 0.76 0.09 ITNA 82SUZ 02 0.6 L* WXRF 82MIL 01 0.83 0.08 12 ITNA 82SUZ 02

157
TABLE AA (cont) TABLE AA (cont)

ANAL REF REF ANAL REF KEF CONC UNCER COMMENT METH CODE MUM CONC UNCER COMMENT METH CODE HVM

St (ppm) U (ppb)

118. 127.

129.

140.

Ta (ppb)

44.

46.

Tb (ppb)

35.

8. 24.

14.

1000.

6.9.

2000.

3.

12

34

L*

L*

ITNA

ITNA ITNA

WXRF

WXRF

ITNA ITNA

WXRF

ITNA

82SUZ 02 82SUZ 02

80GER 01 82MIL 01

82 MIL 01 82SUZ 02

80GER 01

82MIL 01 82SUZ 02

2 3000. L* ITNA 80TOU 01 1000. L* WXRF 82MIL 01 200. 50. ITNA 80GER 01 240. 30. ITNA 82SUZ 02

320. 40. 5 ITNA 80T0U 01

U-234 (FCi)

71.9 4.4 NM 80CAS 01 71.9 4.4 D* NM 81 CAS 01

U-235 (FCi)

4.9 0.3 NM 80CAS 01 4.9 0.3 D* NM 81 CAS 01

Te (ppb) U-2 38 (PCi)

290. L* ITNA 82SUZ 02 0.073 0.004 NM 80CAS 01 600. 34 WXRF 82MIL 01 0.073 0.004 D* NM 81 CAS 01

Th (ppb) V (ppm)

1000. L* WXRF 82 MIL 01 4. 34 WXRF 82MIL 01 580. 40. ITNA 82SUZ 02 4.3 0.3 ITOA 82SUZ 02

610. 70. 12 ITNA 82SUZ 02 4.5 0.05 ITNA 80GER 01 640. 50. 5 ITNA 80TOU 01 640. 60. ITNA 80GER 01 W (ppm)

Th-228 (FCi)

1. L* WXRF 82MIL 01

64.8 4.1 D* NM 81 CAS 01 0.173 0.051 ITNA 82SUZ 02

64.8 4.1 NM 80CAS 01 Y (ppm)

Th-230 (FCi) 1 .9 34 WXRF 82 MIL 01

76.5 7.9 D* NM 81 CAS 01 Yb (ppb)

76.5 7.9 NM 80CAS 01 2000. L* WXRF 82MIL 01

Th-232 (FCi) 140. 20. ITNA 80GER 01 170. 60. 5 ITNA 80T0U 01

61.9 7.7 D* NM 81 CAS 01 175. 12. ITNA 82SUZ 02

61.9 7.7 NM 80CAS 01 Zn (ppm)

Ti (ppm)

5.6 34 WXRF 82MIL 01 190. 20. TCGS 79FAI 01 6.6 1.4 12 ITNA 82SUZ 02

190. 20. D* TCGS 80AND 01 7.5 2.2 ITNA 80GER 01 190. 20. D* TCGS 80GER 01 7.8 1.2 ITNA 82SUZ 02

200. 34 WXRF 82MIL 01 Zr (ppm) 210. 20. ITNA 80GER 01 210. 50. ITNA 82SUZ 02

15. 34 WXRF 82MIL 01 Tl (ppm) 15.7 4.3 12 ITNA 82SUZ 02

16. 3. ITNA 80GER 01

1 . L* WXRF 82MIL 01 19.4 3.3 * ITNA 82SUZ 02

Tm (ppm)

L* WXRF 82MIL 01

158
TABLE BB TABLE DD

NBS SRM 1641—COLLECTED DATA NBS SRM 1643—COLLECTED DATA

ANAL REF REF CONC ONCER COMMENT METH CODE NUM

Hg (ppm)

1 .47 0.17 CVAA 82G1A 02

CONC

Al (ppb)

50. 77.1

82.1

83.

83.

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

5.7

1.4

2.

2. D*

ITNA AE+AF FAA

DCP

DCP

81HAB 01 78EPS 01 78EPS 01 79REE 01 81 REE 01

CONC

TABLE CC

NBS SRM 1642A—COLLECTED DATA

ANAL REF REF UNCER COMMENT METH CODE NUM

Hg (ppb)

1.3 CVAA 82GLA 02

As (ppb)

71 . 75.7

78.

79.

Ba (ppb)

17.3

18.

18. 18.7

19.7 21.5

1.3

1.8

0.7

1.1.2

13

13

14

*14

ICPES HAA

ASV

ASV

AE+AF

FAA FAA

FAA AE+AF

FAA

82NYG 01 80YAN 01

8 2 LEU 01

8 2 LEU 01

79EPS 03

78BEA 01 79EPS 03

78EPS 01 78EPS 01 79EPS 03

Be (ppb)

18.8

21.3

Ca (ppm)

23.9

Cd (ppb)

0.4

5.5

15. L*

FAA AE+AF

ITNA

XRF

78EPS 01 78EPS 01

81HAB 01

80BER 02

Co (ppb)

20.

Cu (ppb)

14. 16.2

17.

2.

0.3

1.8

1

XRF

FAA

AE+AF

XRF

80BER 02

78EPS 01 78EPS 01 80BER 02

Fe (ppb)

76.

76. 82.

2.

2.

3.

D* DCP DCP

XRF

81 REE 01 79REE 01 80BER 02

Hg (ppb)

L* XRF 80BER 02

Mg (ppm)

5.7 ITNA 81HAB 01

159
TABLE EE

TABLE DD (cont) NBS SRM 1643A—COLLECTED DATA

CONC

Mn (ppb)

20.

26. 27.5

28.

29.

29.

Mo (ppb)

104.

110.

Na (ppm)

8.8

Ni (ppb)

48.

48. 49.8

50. 51.3

Pb (ppb)

23.

Se (ppb)

10.

12.

Sn (ppb)

V (ppb)

40. 50.

50.

Zn (ppb)

61 . 61.

63.

UNCER COMMENT

ANAL

METH

REP REF CODE NUM

3.0.7

2.5

3.

3.

3.5.

4.

4.0.8

3.4.2

20.

D*

D*

L*

D*

D*

ITNA XRF

FAA AE+AF

DCP DCP

FAA AE+AF

ITNA

DCP DCP

FAA XRF AE+AF

XRF

ICPES HAA

XRF

ITNA

DCP DCP

DCP DCP

XRF

81HAB 01 80BER 02 78EPS

78EPS

81 REE 01 79REE 01

0101

78EPS 01 78EPS 01

81HAB 01

81REE 01 79REE 01 78EPS 01 80BER 02

78EPS 01

80BER 02

82NYG 01 81C0X 01

80BER 02

81HAB 01

81 REE 01 79REE 01

81 REE 01 79REE 01 80BER 02

CONC

Ag (ppb)

2.7

2.8

Al (ppb)

57.

As (ppb)

70.

76.

Ba (ppb)

45.

48.

Ca (ppm)

26.9

30.

Cd (ppb)

5. 11. 12.

Cr (ppb)

17.5

20.

Cu (ppb)

10.

16. 19.

Fe (ppb)

23.

88. 100.

K (ppm)

1.5 1.62

Mg (ppm)

ANAL

UNCER COMMENT METH

0.1

6.

0.8

4.

0.3

1.

1.

0.04

FAA FAA

FAA

FAA

FAA

FAA

FAA

AA

FAA

FAA

FAA

FAA

FAA

FAA

FAA

FAA FAA

FAA

FAA

FAA

FAA AA

REF REF CODE NUM

82CLA 02

83G1A 01

82 JEN 02

83GLA 01 82GLA 02

83GLA 01 82GLA 02

83GLA 01 82GLA 02

82 JEN 02

83GLA 01 82G1A 02

83GLA 01 82GLA 02

82JEN 02

82G1A 02 83GLA 01

82 JEN 02

83GLA 01 82GLA 02

82GLA 02

83GLA 01

7.8

79

0.4

0 3

AA

FAA

83GIA 01 82GLA 02

Mn (ppb)

10. 32.

FAA FAA

82 JEN 02

83GLA 01

160
TABLE FF

NBS SRM 1645—COLLECTED DATA

CONC

Na (ppm)

9.

9.

Ni (ppb)

57.

N03 (ppm)

1.

Pb (ppb)

26.

28. 41.

Se (ppb)

10.

Sr (ppb)

236.

Zn (ppb)

57. 66.

76.

TABLE EE (cont)

ANAL REF REF UNCER COMMENT METH CODE NUM

0.2

0.2

FAA AA

FAA

ISE

FAA

FAA

FAA

FAA

FAA

FAA

FAA FAA

82GLA 02 83GLA 01

82GLA 02

83GLA 01

82GLA 02

83GLA 01 82 JEN 02

83GLA 01

83GLA 01

82JEN 02

83GLA 01 82GIA 02

CONC

Al (Z)

2.37

2.42

3.9

As (ppm)

62.6

65.

66.

66. 66.4

67.

68.

70. 71.

72.

87.

B (ppm)

29.9

Ba (ppm)

178. 340. 400.

Be (ppm)

1

Bi (ppm)

Ca (%)

2.33

2.73

2.9 2.93

3.106

4.2

Cd (ppm)

8.9

9.1 9.2

10. 10.2

10.8

11- 11.4

UNCER COMMENT

0.04

0.12

2.1

1.5.

15. 50.

0.1

0.15

0.13

0.01

0.4 0.3

0.5

0.4

2.

4.3

35

*35

L*

635

ANAL

METH

REF REF CODE NUM

I TOA

AA

ICPES

RTNA

FAE IENA HAA

ICPES

ICPES IENA RTNA

ICPES

I TOA PAA

TCGS

PAA

I TOA

ICPES

FAA

XRF ITNA AAPAA

XRF

ICPES

RTNA

IDMS FAA

ICPES RTNA

ICPES PAA

AE+AF

81GLA 02

81 FAR 01 80FL0 01

82ELS 02

80DSI 01 82GLA 02

80AGE 03

81G0U 01 82NYG 01 83G1A 01

81 SL 01 80FLO 01 81SL0 01 80BER 01

83GLA 03

8 OKAT 01 81GLA 02

80FL0 01

ICPES 80FL0 01

82MAT 02

78TAK 01 81GLA 02

81 FAR 01 80KAT 01 78TAK 01 80FL0 01

80VAL 01 80ROS 01

81 FAR 01 80FL0 01 79DER 01 82SCH 04 80BER 01 82GOL 01

Ce (ppm)

20.

28.

0.6 PAA

PAA

80KAT 01 80BER 01

161
TABLE FF (cont) TABLE FF (cont)

ANAL UF REF CONC ' UNCER rnuurkrr V. \Jrn Mtr< 1 utni Mt 1 n CODE NUM

Co (ppm)

8. 0.2 35 ITNA 81GLA 02

8.4 0.7 RTNA 77MEL 01

8.5 0.3 PAA 80K.AT 01 9.96 0.12 RTNA 79DER 01

11. ICPES 80FL0 01

24. * PAA 80BER 01

Cr (Z)

2.29 0.08 * PAA 80KAT 01 2.5 0.4 * RTNA 77MEL 01 2.91 0.24 ICPES 82SCH 04

2.97 0.125 11 RTNA 76STE 01 2.98 PAA 80BER 01 2.99 0.13 35 ITNA 81GLA 02 3.02 ICPES tJUr LU n i 3.15 0.147 1

RTNA 76STE 01 3.16 0.152 11 RTNA 76STE 0

3.18 0.08 AA 81 FAR 01 3.19 0.038 6 XRF 80IWA 02

3.25 0.152 1

RTNA 7 tCTr / Dj 1 a 0W 11 3.25 0.049 6 XRF 80IWA 02

3.27 0.155 ITNA 7 tCTl? fl 1 U I 3.4 0. 148 *1

RTNA 76STE 01 3.52 *6 XRF 78TAK 01

Cs (ppm)

2.32 0.13 35 ITNA 81GLA 02 3.3 0.2 RTNA 77MEL 01

Cu (ppm)

78. *6 XRF 78TAK 01

96. 14

ASV 8 1 DOG 0 1 100. 20. AA 77YAN 01

105. 14. ICPES ft? oi Don QfH U H 106. PAA 80BER 01 108. 6 XRF 78TAK 01

111. 7. FAA 81 FAR 01

1 1 1 1 1 J • 0YUT? 78TAK 01

119. ICPES 80FL0 01 123. 6

RTNA 79DER 01 125.2 8.2 RTNA 80VAL 01

Eu (ppm)

0.7 ICPES 80FL0 01

0.31 0.03 35 ITNA 81GLA 02

r (.ppm;

1740. 60. ISE 83KNA 01

Fe (%)

8.372 *6 XRF 78TAK 01 8.5 0.5 * RTNA 77MEL 01

9-89 6 XRF 78TAK 01 10.4 6 XRF 78TAK 01

CONC

10.5

10.51

10.6

11.4 11.5

Ga (ppm)

38.

Hf (ppm)

1.39

Hg (ppm)

0.85

1 .1 1.11

1.3

1 .3

K (%)

0.893

1 .24

La (ppm)

15.

Mg (%)

0.684

0.75

4.1

Mn (ppm)

746.

750.

750.

762.

768.

780.

1460.

3321.

Mo (ppm)

25.

Na (ppm)

5450.

5600.

Nb (ppm)

1.4

UNCER COMMENT

0.3

0.18

0.3

1.3

0.07

0.036

0.1

0.26

0.2

0.01

0.02

130.

18.

9. 85.

90.

110. 200.

35

35

35

*6*6

ANAL

METH

ITNA PAA

AA

ICPES

ICPES

REF REF CODE NUM

81GLA 02

8 OKAT 01

81 FAR 01 82SCH 04

80FL0 01

ICPES 80FLO 01

ITNA

CVAA RTNA

CVAA PAA

RTNA

XRF

XRF

35

0.07

PAA AA

ICPES

AE+AF PAA

ICPES

ITNA ICPES

AA

XRF XRF

PAA

PAA

ITNA

PAA

81GLA 02

80NAD 01 77MEL 01 80WHI 01 80BER 01 80VAL 01

78TAK 01 78TAK 01

ICPES 80FLO 01

80KAT 01

81 FAR 01 80FLO 01

82G0L 01 80KAT 01 80FL0 01 81GLA 02

82SCH 04

81 FAR 01 78TAK 01 78TAK 01

80BER 01

80KAT 01 81GLA 02

80KAT 01

162
TABLE FF (cont) TABLE FF (cont)

CONC

Ni (ppm)

UNCER COMMENT

ANAL

METH

KEF CODER£F NUM

28. 6 XRF * 78TAK 01

30. 6 XRF 78TAK 01 33. 6 XRF 78TAK 01 37.6 6.4 AE+AF 82GOL 01 45. ICPES 80FL0 01 46.1 2.5 ICPES 82SCH 04 46.6 4.6 PAA 78MAS 01

47. 3. PAA 80KAT 01 48. PAA 80BER 01 48. PAA 78KAT 01 55. 3. RTNA 77MEL 01

Pb (ppm)

680.

683.

695.

717.

719. 721.

724.

725. 771.

1019.

Pr (ppm)

14.

Rb (ppm)

38.

39. 40. 41.4

50.

Sb (ppm)

21.7

22.6

25. 28.3

31. 33.2

33.6

36. 38. 40.

52.

Sc (ppm)

2.13

3.1

Se (ppm)

0.85

1 .

20.

29. 45.

20.

231.

2.0.5

7.

1.2

4.

2.2

0.07

0.5

**6

*35

35

*

35

AA

FAA

ASV

XRF

XRF ICPES PAA

ICPES AE+AF

XRF

XRF

XRF PAA

RTNA

ITNA

RTNA RTNA HAA

FAA

ITNA RTNA

RTNA

ITNA

ICPES

ITNA PAA

ITNA RTNA

RTNA

ICPES

77YAN 01

81 FAR 01 81D0G 01 78TAK 01 78TAK 01 82SCH 04 80BER 01 80FL0 01 82G0L 01 78TAK 01

ICPES 80FL0 01

78TAK 01 78TAK 01

8 OKAT 01 77MEL 01 81GLA 02

81NIS 01 81KIB 01

81 YAM 01 82MAT 02

81 HAM 01 81SL0 01 82ELS 02

81SL0 01 82NYG 01 81GLA 02 SOBER 01

81GLA 02 77MEL 01

81SLO 01 81G0U 01

ANAL R£F REF CONC ' UNCER COMMENT METH CODE NUM

1.3 0.2 RTNA 77MEL 01

1 .5 0.1 35 RTNA 81GLA 01

5. * ICPES 80FL0 01

8. * ICPES 82NYG 01

SI (%)

30.6 1.2 AA 81 FAR C

Sn (ppm)

313. 9. FAA 82MAT 02

Sr (ppm)

851. 13. PAA 80KAT 01 862. PAA 80BER 01 870. 6 XRF 78TAK 01 1033. 6 XRF 78TAK 01 1200. * ICPES 80FLO 01

Ta (ppb)

220. 20. 35 ITNA 81GLA 02

Th (ppm)

1 .8 PAA SOBER 01

Tl (ppm)

1000. L* ITNA 81GLA 02 258. 6 XRF 78TAK 01 490. 6 XRF

642. 13. PAA 8 OKAT 01 700. AA ft? OlIMAT in i. OA\J * 825. PAA 80BER 01

Tl (ppm)

1 .9 PAA 80BER 01

U (ppm)

0.8 0.02 RTNA 78DER 01

1 .16 DNA 83GLA 01

1 .4 PAA 80BER 01

V (ppm)

24.1 6 .5 ICPES

25. ICPES 80FLO 01 29

£u . 3D TTMA

Y (ppm)

7. ICPES 80FLO 01 7.4 0.3 PAA 8 OKAT 01

Yb (ppb)

600. ICPES 80FL0 01

163
TABLE FF (cont)

CONC

Zn (ppm)

1414.

1480.

1540.

1587.

1610.

1640.

1640.

1713.

1720.

1730.

1794.

1806.

Zr (ppm)

55.

71.

UNCER

84.

67.

40.

40.

145. 361.

37.

COMMENT

ANAL

METH

REF REF CODE NVIM

RTNA

XRF PAA

ICPES

AA

AA

XRF ICPES

AE+AF

PAA

XRF RTNA

PAA

PAA

77MEL 01 78TAK 01 80KAT 01 80FLO 01 77YAN 01

81 FAR 01 78TAK 01 82SCH 04

82G0L 01

80BER 01 78TAK 01 79DER 01

80KAT 01 80BER 01

TABLE GG

NBS SRM 1646—COLLECTED DATA

ANAL REF REF CONC UNCER COMMENT METH CODE HUM

B (ppm)

83.

Cs (ppm)

3.6

Sb (ppm)

0.85

Sc (ppm)

10.4

U (ppm)

3.

2.

0.4

0.2

TCGS 83GLA 03

ITNA 83GLA 01

ITNA 83GLA 01

ITNA 83G1A 01

DNA 83GIA 01

164
TABLE HH

TABLE HH (cont) NBS SRM 1648—COLLECTED DATA

Be

C

ANAL REF REF ANAL REF REF CONC UNCER COMMENT METH CODE NVJM CONC UNCER COMMENT METH CODE NUM

; (ppm) 5.6 0.4 AA 83GLA 02 5.8 0.5 ITNA 79GRE 01 5.8 0.9 IENA 83GLA 02 6.1 0.04 EXRF 78PEL 01

6. 1

XRF 77GIA 02 6.18 0.23 AA 81 FAR 01

6. 1D* XRF 79GIA 03 6.3 0.3 ITNA 83GLA 02 6.4 0.5 ITNA 79GRE 01 Cd (ppm)

(*) 64. 7. AA 82GLA 02

3-05 0.03 AA 81FRA 01 69. 4. FAA 81 FAR 01 3.1 0-1 ITNA 83GLA 02 70. 2. XRF 77GIA 02 3.12 0.2 35 ITNA 81GLA 03 70. 2. D* XRF 79GIA 03

3.3 ICPES 80FL0 01 70. 6. ITNA 79GRE 01 3.3 0.45 AA 81 FAR 01 73. ICPES 80FL0 01 3.5 0.1 ITNA 79GRE 01 75. 7. AA 83GLA 02

105. 9. * AA 81FRA 01

i (ppm)

Ce (ppm)

112. ICPES 80FLO 01 117. Tr'Dtr c lLrtio OOMV h OZNl b 01 52. 5. IENA 83GLA 02

117. 5. ITNA 83GLA 02 53. 2. ITNA 83GLA 02

117. 5. ITNA 79GRE 01 ITNA 79GRE 01 119. 35 NAA 81GLA 03 61. ICPES 80FL0 01

119. 2. IENA 83GLA 02

CI (ppm)

(ppm)

500. 60. *35 ITNA 81GLA 03

158. 8. TCGS 83GLA 03 4500. 200. ITNA 79GRE 01 6000. 170. * UU 81FRA 01 4890. 80. ITNA 83GLA 02

(ppm) Co (ppm)

740. 60. ITNA 79GRE 01 15.2 0.9 AA 81FRA 01

757. 35. XRF 77GIA 02 17.2 0.6 ITNA 83GLA 02

757. 35. D* XRF 79GIA 03 17.6 0.5 ITNA 79GRE 01 774. ICPES 80FLO 01 18. 1. IENA 83GIA 02 800. 10. 5 ITNA 83GLA 02 28. ICPES 80FLO 01 840. 40. IENA 83GLA 02 42. 7. *35 ITNA 81GLA 03

980. 100. 5* ITNA 83GLA 02

Cr (ppm)

! (ppm)

173. 27. * FAA 81 FAR 01

3. ICPES 80FLO 01 380. 40. AA 83GLA 02

38 3. AA 82GIA 02

(ppm) 398. ICPES 80FLO 01 402. 10. ITNA 79GRE 01 460. 15. 5 83GLA 02 410. 50. 35 ITNA 81GLA 03

500. 30. ITNA 79GRE 01 410. 8. ITNA 83GLA 02

504. 14. 5 IENA 83GLA 02 417. 16. AA 81FRA 01 517. 14. XRF 77GIA 02 440. 10. EXRF 78PEL 01 517. 14. D* XRF 79GIA 03 1 1

UU 81FRA 01 526. 24. 35 ITNA 81GLA 03 580. 50. * UU 81FRA 01

25

ITNA 83GLA 02

Cs (ppm)

(%)

j • j

fi. U 9• Z ItNA 83GLA 02

14.7 0.3 CB 83GLA 02 3.4 0.2 ITNA 79GRE 01 15.27 0.15 UU 81FRA 01 3.73 0.29 ITNA 83GLA 02

i «) Cu (ppm)

5.4 0.3 IENA 83GLA 02 570. 44. UU 81FRA 01 5.5 0.4 AA 82GLA 02 581. 16. XRF 77GIA 02

165
TABLE HH (cont) TABLE HH (cont)

APi AfcJAl AL REF HEF ANAL REF REF CONC UNCER y. \juc. pium CONC UNCER COMMENT METH CODE NUM

1 .04 0.02 EXRF 78PEL 01 586. 22

FAA Q 1 U' A D A 1 0 1 r AK U

1 .07 0.02 I ENA 83GLA 02

589. 12. AA 81FRA 01 1.11 0.08 35 ITNA 81GLA 03

596. 24. AA 82GLA 02

598. ICPES oUrLO Ul La (ppm)

600. 30. AA 8JGLA 02 610. 18. UU 81FRA 01 35. ICPES 80FL0 01 640. 60. * EXRF 81KIN 01 38. 3. 35 ITNA 81GLA 03

700. 100. * EXRF 78PEL 01 40. 2. ITNA 83GLA 02

42. 2. ITNA 79GRE 01 (ppm) 42

5

I ENA 83GLA 02

0.77 0.03 T TM A I 1NA oJOLA Uz Lu (ppb)

0.79 U . Uo T TM A 1 1NA 7 Q PD T? A 1 /yOKti Ul

1

ICPES o An A A 1 34

3

ITNA 83GLA 02

! (%) Mg (ppm)

3.4 3 0.05 AA Q 1 CD A A 1 ol rKA Ul 7 Tnfi /ZUO. 600. AA 82GLA 02

3 .7 AA 82GLA 02 7 500. Ann 4UU . A A Art ojOLA UZ

3 .8 0.5 35 ITNA 81GLA 0 3 7600. 400

rtA A A ft i v ft p ni 01 r AK U

3. 84 0.08 ITNA 79GRE 01 8000. i ^n AAA A o 1 rKA U

3 .86 0.06 ITNA 83GLA 02 8300. p.nn T TWA 7 o fT? tt n 1 /yijKn. Ul 3.9 0.

I ENA 83GLA 02 yuuu. ICPES oOFLO 01

3 .96 0.037 EXRF 78PEL 01

4 m 0.1 EXRF 81KIN 01 Mn ( ppm)

4.05 0.

XRF 77GIA 02

4 .U5 n i U. 1 D7* AKr 7Q C T A A 740. 30. IENA 83GLA 02

4 .

I CPE S

O A PI /"\ A 1 747. 10. ITNA 83GLA 02

4 . z nU • A4 A A O JVj U\ \J L 790. 20

ITNA 79GRE 01 4.5 n 7 i U • Z J A" A A Art O 1 TT AD A 1 790. 80. AA 83GLA 02

Jt4J 0 37 * UU 8 1 FR A 01 o\JD 4 . A A Art ol rKA U

5.65 n i /. *^ nil UU Q 1 T7D A A 1 (5 1 rKA U 1 q i n Ol U

40. 35 ITNA 81GLA 03

810. 60. AA 81 FAR 01

i (ppm) 840. 85. UU 81FRA 01 851. ICPES 80FLO 01 8.3 0.4 I ENA 83GLA 02 860. 20. EXRF 81KIN 01 72. ICPES 80FLO 01 870. ^n 7 QTJTTT A 1 / or t-L U 1

(%)

nan OoU o nOU

A A Q O i°T A AO ozGLA Uz

b on ooU. 19

UU O 1 I'M » A 1 81FRA 01 961 . 34. * XRF 77GIA 02

2.23 0.04 CB 83GLA 02 961

34D* XRF 79GIA 03

(ppm) Mo (ppm)

4.2 n 7 0 . J ITNA 7 0 rn it A l / y LiK fc. U 1 17 . 2

XRF 77GIA 02

/. A 7 n m T TM A 1 1NA O-lfl A AO OJOljA UZ 2 . IENA oiGLA Uz

C 0 3 . Z nU A• 4 T FN A QO,/-»t a AO O JuLft U Z

(ppm)

3.25 0.04 CB 83GLA 02

16. 2. XRF 77GIA 02

16. 2. D* XRF 79GIA 03 Na (ppm)

20

ITNA 79GRE 01 4000. 200. ITNA 79GRE 01

i (ppb) 4220. 120. 5 ITNA 83GLA 02 4600. 200. 5 ITNA 83GLA 02 980. 70. ITNA 79GRE 01 5500. 1500. 35 ITNA 81GLA 03

(%) Nb (ppm)

0.96 0.12 ITNA 83GLA 02 22. 3. XRF 77GIA 02

0.99 0.11 ITNA 79GRE 01

166
TABLE HH (cont) TABLE HH (cont)

CONC

Ni (ppm)

72-

75. 83.

85.

99.

100.

105.

Pb (ppm)

6100.

6200.

6210.

6300.

6300.

6400.

6780.

6900.

7000.

Pr (ppm)

8.

Rb (ppm)

52. 53.

55.

58.

S (%)

5.21

Sb (ppm)

41.

44.

44.

44.

45.

47.

Sc (ppm)

6.6

6.6

6.8

6.8

Se (ppm)

4. 23.1

25.

25.

26.

27.

UNCER

15.

4.

4.

13.

7. 21.

200.

810.

85.

300.

100.

45.

60. 200.

COMMENT

ANAL METH

REF HEF CODE NVIM

9.

5.

6.

2.

0.06

0.2

0.6

0.3

0.2

4.

4.

35

D*

35

35

D*

AA

IENA

EXRF

ICPES

XRF UU

AA

AA

UU

FAA AA

XRF AA

EXRF EXRF

ICPES

I TOA

I TOA

I TOA

I ENA

UU

ICPES XRF

ITOA XRF ITOA

ITOA

ITOA

ITOA

ITOA

ITOA

ICPES RTNA

XRF

XRF ICPES

ITOA

82GLA 02

83GIA 02

78PEL 01 80FL0 01 77GIA 02

81FRA 01 81FRA 01

82GLA 02

81FRA 01

81 FAR 01 83GLA 02

77GIA 02

81FRA 01 78PEL 01

81KIN 01 80FLO 01

ICPES 80FL0 01

79GRE 01 83GLA 02

81GLA 03

83GLA 02

81FRA 01

82NYG 01

77GIA 02

83GLA 01 79GIA 03

79GRE 01 83GLA 02

79GRE 01 83GLA 01 81GLA 03

83GLA 02

80FLO 01 81GLA 01 77GIA 02

79GIA 03

82NYG 01

79GRE 01

Sm (ppm)

4.4.2

4.4

Sn (ppm)

147.

Sr (ppm)

190.

211.

220.

450.

Ta (ppm)

6.76

7.2

Th (ppm)

7.4

7.5

7.8

Ti (ppm)

3800.

3900.

4000.

4000.

4000.

4100.

4100.

4260.

4500.

9700.

U (ppm)

5.42

5.6

5.9

V (ppm)

106.

116.

116.

UNCER

2.0.47

1.1

2.0.3

1.

0.4

0.4

0.3

COMMENT

10.6.

10.

0.17

0.4

0.3

0.5

0.4

200.

800.

200.

200.

400.

300.

30. 400.

0.2

0.05

19.

4.

35

**35

35

ANAL

METH

AA

AA

I ENA AA

EXRF AA

ITOA

ITOA

ITOA

XRF

EXRF

XRF IENA

ICPES

ITOA IENA

ITOA

ITOA

IENA

EXRF AA

ICPES

ITOA

ITOA AA

AAEXRF

IENA NAA

DNA

IENA DNA

ICPES

ITOA

ITOA

REF REF CODE NUM

82GLA 02

81FRA 01 83GLA 02

83GLA 02

78PEL 01

81 FAR 01

79GRE 01 81GLA 03

83GLA 02

77GIA 02

78PEL 01 77GIA 02

83G1A 02

80FLO 01

83GLA 02

83GLA 02

79GRE 01 83GLA 02

83GLA 02

81KTN 01 81FRA 01 80FLO 01 79GRE 01 83GLA 02

82GLA 02

83GLA 02

78PEL 01

83GLA 02

81GLA 03

83GLA 02

83GLA 02

83GLA 01

80FLO 01 81GLA 03

83GLA 02

167
TABLE II

TABLE HH (cont) NBS SRM I A—COLLECTED DATA

ANAL REF REF ANAL REF REF

' UNCER COMMENT METH CODE NUM CONC UNCER COMMENT METH CODE NUM

123. 12. 1ENA 83GLA 02 Al (*) 130. 7. I TOA 79GRE 01 2.1 OES 62JOE 01 W (ppm) 2.23 OES 78KNO 01 2.27 DCP 7 3KAR 01 3.5 35 RENA 81GLA 03 2.29 TITR 5 8 WAT 01 4.4 2.8 IENA 83GLA 02 2.36 RR 73KAR 01 4.8 0.6 ITNA 79GRE 01 B (ppm) Y (ppm)

on80. 3 OES 6JCLA 01

J - ICPES 80FLO 01 1UU.

id ^ppm; Ba (ppm)

2. ICPES 80FLO 01 OUUt Li UEjD

Zn (ppm) C (a)

4 300. 550. * UU 81FRA 01 9.73 CB 78TER 01 4400. 60. UU 81FRA 01 4580. 160. AA 81 FAR 01 Ca (%)

4650. 150. EXRF 7 8PEL 01 4700. 200. ITNA 79GRE 01 28 .6 OES 62JOE 01 4700. ICPES 80FL0 01 29.5 RR 73KAR 01 4740. 130. IENA 83GLA 02 29.6 XRF 78KNO 01 4740. 30. AA 80EPS 01 29.7 DCP 73KAR 01 4750. 50. ITNA 83GLA 02 4800. AA 82GLA 02 Co (ppm)

4800. 100. EXRF 81KIN 01 4800. 300. AA 83GLA 02 10. L* OES 63CLA 01 4800. 60. AA 81FRA 01 3.9 1 .4 RTNA 61TUR 01 4850. 240. 35 ITNA 81GLA 03

4890. 130. XRF 77GIA 02 Cr (ppm)

4890. 130. D* XRF 79GIA 03

23. RTNA 61TUR 01 Zr (ppm) 30. OES 63CLA 01

169. 8. XRF 77GIA 02 Cu (ppm)

3. OES 63CLA 01

Fe (%)

0.855 OES 6 2 JOE 01

1 .08 OES 78KNO 01 1.08 DCP 73KAR 01

1 .1 COLOR DyKXfL Ul

1 .13 RR "J IV AC A 1 / JK.AK Ul 1.15 TITR 69WIC 01

Ga (ppm)

4. OES 63CLA 01

Hg (ppb)

44. FAA 75HEI 01 71.4 2.16 FAA 8 2 FLA 01

168
TABLE II (cont) TABLE II (cont)

CONC

K (ppm)

6900.

La (ppm)

100.

Mg (%)

1 .29

1 .3 1.37

1 .39

Mn (ppm)

320.

500.

500.

Mo (ppm)

Na (ppm)

2300.

2700.

Ni (ppm)

10.

P (ppm)

650.

1500.

Pb (ppm)

17.2

20.

21.

S (ppm)

2700.

2800.

2800.

2800.

3000.

3020.

3073.

Sc (ppm)

15.

UNCER COMMENT

L*

90.

ANAL

METH

RR

OES

OES

OES RR

DCP

OES

OES

OES

OES

RR

DCP

OES

WXRF OES

FAA

OES

FAA

CB

OES

CB

uuTURB

CB

CB

OES

KEF KEF CODE HUM

73KAR 01

63CLA 01

78KN0 01 62J0E 01 73KAR 01 73KAR 01

78KN0 01 63CLA 01 63CLA 01

63CLA 01

73KAR 01

7 3KAR 01

63CLA 01

71 FAB 01 78KN0 01

75CAM 02

63CLA 01 79HEI 03

55C0L 01 78KNO 01 74RUN 01 72BOU 01

73SHA 01 77LAN 01 78TER 01

63CLA 01

CONC

Si (Z)

6.53

6.54

6.58

6.63

6.72

Sn (ppm)

1.68

Sr (ppm)

1700.

1940.

2000.

2000.

3000.

Ti (ppm)

900.

900.

960.

1000.

1500.

2500.

V (ppm)

30.

W (ppm)

10.

Zn (ppm)

17. 23.3

Zr (ppm)

60.

UNCER COMMENT

ANAL

METH

KEF KEF CODE NUM

3

*3

61

3*3

XRF OES

RR

COLOR

DCP

AA

OES

OES

OES

RTNA

OES

RR

DCP

RTNA

OES

OES

OES

OES

OES

XRF RTNA

OES

78KNO 01 62J0E 01 73KAR 01 74SHA 01 73KAR 01

82TER 01

75TH0 01 58GRA 01 63CLA 01 61TUR 01 63CLA 01

73KAR 01

7 3KAR 01 65WAH 01 78KN0 01 63CLA 01 63CLA 01

63CLA 01

63CLA 01

65BAL 01 65BAL 01

63CLA 01

169
TABLE JJ

NBS SRM IB—COLLECTED DATA TABLE JJ (cont)

CONC

Ag (ppm)

Al (ppm)

5660.

5800.

As (ppm)

Au (ppm)

Ba (ppm)

86.

Be (ppb)

420.

Bi (ppm)

Ca (Z)

35.93

36.8

Cd (ppb)

52.

Ce (ppm)

Co (ppm)

4.1

Cr (ppm)

15.7

Cu (ppm)

5.5

Eu (ppm)

1 .7

Fe (ppm)

5000.

5460.

ANAL REF REF UNCER COMMENT METH CODE HUM

5.

200.

3.

1.7

50.

25.

1.19

2000.

15.

1.2

140.

L* ICPES 81CHU 01

ICPES 81CHU 01 OES 73BES 01

L* ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01 OES 73BES 01

L* ICPES 81CHU 01 IDMS 74ROS 02

L* ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

OES 73BES 01 ICPES 81CHU 01

CONC

Gd (ppm)

Hg (ppb)

15.7

K (ppm)

2000.

La (ppm)

Li (ppm)

Mg (ppm)

2040.

2400.

Mn (ppm)

1430.

1510.

Mo (ppm)

Na (ppm)

260.

Nd (ppm)

Nl (ppm)

11.

P (ppm)

370.

Pb (ppm)

2.

17.

S (ppm)

100.

Sb (ppm)

ANAL REF REF UNCER COMMENT METH CODE NUM

0.9

50.

60.

45.

15.

20.

1

0.4

2.

10.

L* ICPES 81CHU 01

FAA 82FLA 01

ICPES 81CHU 01

L* ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01 OES 73BES 01

OES 73BES 01 ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

FAA 75CAM 02 ICPES 81CHU 01

CB 77LAN 01

L* ICPES 81CHU 01

170
TABLE KK

TABLE JJ (cont) NBS SRM 278—COLLECTED DATA

CONC

ANAL UF UF

UNCER COMMENT METH CODE NUM

Se (ppm)

Si (%)

2.28

2.32

Sm (ppm)

Sn (ppm)

Sr (ppm)

1200.

1208.

Th (ppm)

Ti (ppm)

292.

300.

U (ppm)

V (ppm)

30.1

Yb (ppm)

2.1

Zn (ppm)

40.7

Zr (ppm)

16.

30.

0.05

5.

24.

25.

30.

1.4

0.1

2.

1

L* ICPES 81CHU 01

COLOR 81F0N 01 0ES 73BES 01

L* ICPES 81CHU 01

L* ICPES 81CHU 01

0ES 75TH0 01 ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01 OES 73BES 01

L* ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

CONC

Al (%)

7.43

7.8

As (ppm)

4.68

5.06

5.1

Au (ppb)

1 .6 2.64

B (ppm)

24.9

25.2

25.3

Ba (ppm)

885.

1060. 1080.

Br (ppm)

2.61

2.65

2.99

Ca (ppm)

6000.

7300.

7500.

Ce (ppm)

56.5

56.5

59.4

66.5

CI (ppm)

640.

Co (ppm)

1 .85 1.89

2.04

UNCER

0.57

0.2

0.13

1.29 0.88

0.8 0.52

COMMENT

ANAL REF REF METH CODE NUM

0.5

0.4

1.

54.

40.

58.

0.62

0.2 1.01

1000.

300. 1200.

1.9 2.9 6.8

9.3

90.

0.18

0.31

0.22

ITNA

TCGS

ITNA

ITNA

ITNA

ITNA ITNA

TCGS TCGS

TCGS

ITNA ITNA

ITNA

ITNA

ITNA ITNA

TCGS

TCGS

ITNA

ITNA

ITNA

ITNA

ITNA

TCGS

ITNA ITNA

ITNA

82GRA 01 82GRA 01

81AHM 01 82GRA 01 82V0G 01

82GRA 01 82V0G 01

82V0G 01 82GRA 01 83GLA 03

81AHM 01 82V0G 01 82GRA 01

82GRA 01 81AHM 01 82VOG 01

82GRA 01 82V0G 01 82GRA 01

81AHM 01 80AHM 01 82GRA 01 82VOG 01

82GRA 01

82GRA 01 82V0G 01 81AHM 01

Cr (ppm)

6.34

6.42

6.79

0.93

0.28

0.44

ITNA

ITNA ITNA

82GRA 01 82V0G 01 81AHM 01

171
TABLE KK (cont) TABLE KK (cont)

CONC

Cs (ppm)

4.92

5.12

5.3

5.3

Eu (ppb)

764.

796.

820.

820.

Fe (%)

1 .14 1.32

1.52

1.54

1 .55

Ga (ppm)

10. 12.47

Gd (ppm)

52834 37.74

37.74

H (%)

0.089

Hf (ppm)

6.41

8.82

8.86

In (ppb)

43.6

K (%)

3.42

3.44

3.58

4.23

La (ppm)

27.59

27.6

35.4

35.8

UNCER

0.34

0.44

0.25

0.7

56.

9. 30.

30.

0.23

0.17

0.05

0.01

0.06

3.2.53

0.06

0.08

1.5 1.5

0.012

0.24

0.73

0.73

2.7

0.34

0.08

0.7 0.13

0.38

0.4 2.5

1.5

COMMENT

ANAL HEF METH CODE

KEF NUM

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

TCGS ITNA ITNA

TCGS

ITNA

ITNA

ITNA

TCGS

TCGS ITNA

ITNA

TCGS

ITNA

ITNA ITNA

ITNA

ITNA

TCGS

TCGS

ITNA

ITNA ITNA

ITNA ITNA

82GRA 01 81AHM 01 82VOG 01 83GLA 01

82GRA 01 82V0G 01 81AHM 01 80AHM 01

81AHM 01 82GRA 01 82GRA 01 82V0G 01 82V0G 01

82GRA 01 82VOG 01

82GRA 01 82V0G 01 82GRA 01 81AHM 01 80AHM 01

82VOG 01

81AHM 01 82GRA 01 82VOG 01

81AHM 01

82GRA 01 82GRA 01 82V0G 01 81AHM 01

81AHM 01 80AHM 01 82GRA 01 82V0G 01

CONC

Lu (ppb)

740.

745.

820.

836.

Mn (ppm)

367.

400.

409. 430.

Mo (ppm)

3.73

3.73

Na (%)

2.6

3.3 3.46

3.9

Nd (ppm)

28.2

Rb (ppm)

130.

138. 143.17

Sb (ppm)

1 .59 1.61

1.7 1.9

Sc (ppm)

4.16

5.5.24

5.31

Si (%)

33.2

36.6

Sm (ppm)

5.61 5.66

5.69

5.7

UNCER

50.

310.

39. 50.

15. 50.

15. 70.

0.52

0.52

0.2

0.4 0.26

0.23

1.

12.

10.2.63

0.05

0.13

0.4

0.21

0.1 0.14

0.05

0.7

1.3

0.05

0.1 0.62

0.7

COMMENT

ANAL REF HEF METH CODE NUM

ITNA ITNA

ITNA ITNA

ITNA ITNA ITNA

TCGS

ITNA

ITNA

TCGS ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA ITNA

ITNA

TCGS

TCGS

TCGS TCGS ITNA

ITNA

80AHM 01 81AHM 01 82V0G 01 82GRA 01

82V0G 01 82GRA 01 81AHM 01 82GRA 01

82VOG 01 82GRA 01

82GRA 01 82VOG 01 82GRA 01 81AHM 01

82GRA 01

82GRA 01 82V0G 01

81 AHM 01

82V0G 01 82GRA 01

81 AHM 01 83GLA 01

81 AHM 01 83GLA 01 82GRA 01 82VOG 01

82V0G 01 82GRA 01

82V0G 01 82GRA 01 82GRA 01 82VOG 01

172
TABLE LL

TABLE KK (cont) NBS SRM 4350—COLLECTED DATA

CONC UNCER COMMENT

ANAL

METH

REF REF CODE NUM

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

Ta (ppm)

Cs-137 (PCi

1.23 0.19 ITNA 82GRA 01

1 .23 0.16 ITNA 82V0G 01 2.5

1 .32 \J . I o ITNA 81 AHM 01

I (ppb)

Tb (ppm) 5400.

1.12 0.22 ITNA 82V0G 01 1-129 (FCi)

1 . 14 0.1 ITNA 82GRA 01 1.23 0.03 ITNA 81 AHM 01 1.23 0.08 ITNA 80AHM 01 Pu-239 (PCi)

Th (ppm) 0.033

12 .27 0.77 ITNA 81 AHM 01 12.27 0.77 ITNA 80CHA 02

1 1 O 1 z .o U.J T TMA 1 1NA 13.1 0.2 ITNA 82VOG 01

Ti (ppm)

1450. 90. TCGS 82GRA 01 NBS

1500. 40. TCGS 82 V0G 01

Tm1 i n r>m i 111 \ L/ pui /

0.301 0.02 ITNA 81 AHM U

1

CONC

U (ppm) Am-241 (PCi)

4.204 0.284 ITNA 81 AHM 01 0.005

4 .58 DNA 83GLA 01 4.82 0.35 ITNA 82GRA 01 Co-o (.PCi;

4.96 0.33 ITNA 82 VOG 01 0.13

Yb (ppm)

pB_ 1 *17 ( T>C\ \ i ji \ r\j± ) 3.58 0.25 ITNA 81 AHM 01 3.58 0.25 ITNA 80AHM 01 0.85

4.54 0.86 ITNA 82GRA 01 5.09 0.95 ITNA 82 VOG 01 Pu-238 (FCi)

Zn (ppm) 0.2

54. 2.5 ITNA 82GRA 01 Pu-239 (FCi)

57.4 3.6 ITNA 8 2 VOG 01

Zr (ppm)

11.6

Th-230 (PCi)

285. 16. ITNA 82GRA 01 311. 50. ITNA 82 VOG 01 0.8

0.35

5000.

GAMMA 83GLA 01

RTNA 79BRA 01

0.001 AS 81 CAR 01

TABLE MM

ANAL REF REF

0.01

0.08

0.8

2.5

AS 83GLA 01

GAMMA 82 JEN 03

GAMMA 83GLA 01

AS 83GLA 01

AS 83GLA 01

AS 83GLA 01

173
TABLE NN

NBS SRM 4353—COLLECTED DATA

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

TABLE OO

NBS SRM 610—COLLECTED DATA

Am-241 (PCi)

0.042

Cs-137 (PCi)

0.52

Pu-238 (FCi)

3.5

Pu-239 (PCi)

0.202

Th-230 (PCi)

1.2

0.008

0.06

1.9

0.039

AS 83GLA 01

GAMMA 83GLA 01

AS 83GLA 01

AS 83GLA 01

AS 83GLA 01

CONC

Ag (ppm)

180.

As (ppm)

305.

Au (ppm)

20.

B (ppm)

368.

Ba (ppm)

638.

Be (ppm)

450.

Bi (ppm)

405.

Ca (%)

7.64

Cd (ppm)

187.

Ce (ppm)

318.

Co (ppm)

135. 375.

Cr (ppm)

371.

Ga (ppm)

481.

Ge (ppm)

496.

Hf (ppm)

220.

ANAL REF REF UNCER COMMENT METH CODE NUM

80.

20.

2.

12.

24.

50.

18.

0.002

21.

14.

14.

12.

15.

10.

10.

14.

ITNA 7 3 SHE 01

SSMS 74BER 01

ITNA 7 3 SHE 01

ICPES 820WE 01

SSMS 74BER 01

CPAA 82LAS 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

ITNA

SSMS

7 3 SHE 01 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

174
TABLE OO (com) TABLE OO (cont)

CONC

In (ppm)

319-

Li (ppm)

354.

Mg (ppm)

472.

Mn (ppm)

391.

Mo (ppm)

307.

Ni (ppm)

431.

Pb (ppm)

392.

Sb (ppm)

387.

Ta (ppm)

206.

Te (ppm)

259.

Th (ppm)

469.

Ti (ppm)

361.

Tl (ppm)

52.

U (ppm)

413.

430.

470.

471.

U-235 (a%)

0.251

ANAL KEF KEF UNCER COMMENT METH CODE NUM

11.

27.

22.

19.

10.

11.

18.

9.

21.

7.

18.

35.

18.

90.

28.

0.009

SSMS 74BER 01

CPAA 82 LAS 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

SSMS 74BER 01

17

17

SSMS DNA

DMA DNA

74BER 01 83GLA 01 8200N 01 82CON 01

CONC

V (ppm)

206.

ANAL KEF KEF UNCER COMMENT METH CODE NUM

10. SSMS 74BER 01

RTNA 83GLA 01

175
TABLE PP

NBS SRM 612—COLLECTED DATA

TABLE QQ

NBS SRM 614—COLLECTED DATA

CONC

Ag (ppm)

31.

Au (ppm)

5.

B (ppm)

AO.

Be (ppm)

31.

Ce (ppm)

37.

Co (ppm)

31.

Eu (ppm)

26.

La (ppm)

35.

Li (ppm)

44.

Pb (ppm)

38.56

Th (ppm)

31.

U (ppm)

35.74

36.3

37.66

39. 40.

U-235 (a%)

0.229

ANAL REF REF UNCER COMMENT METH CODE HUM

ANAL REF REF CONC UNCER COMMENT METH CODE HUM

2.

1.

15.

0.11

7.2 0.08

4.9

0.011

ITNA 73SHE 01

ITNA 7 3 SHE 01

ICPES 820WE 01

CPAA 82LAS 01

ITNA 73SHE 01

ITNA 73SHE 01

ITNA 73SHE 01

ITNA 7 3 SHE 01

CPAA 82LAS 01

IDMS 77GUL 01

ITNA 7 3 SHE 01

17

17

NT

DMA

IDMS DMA

DMA

80VIR 01 82CON 01 77GUL 01 82CON 01 83GLA 01

Ag (ppm)

0.471 0.06

0.57 0.07

Au (ppm)

0. 28 0.14

1 . 0.8

Co (ppm)

0.59 0.1

Cu (ppm)

1.61 0.32

Eu (ppm)

1.1 0.6

La (ppm)

2.

Sb (ppm)

1.1 0.1

Sc (ppm)

0.68 0.23

Th (ppm)

0.58 0.15

Tl (ppm)

0.29 0.05

U (ppm)

0.74

FAA 82 JEN 02 ITNA 7 3 SHE 01

FAA 82 JEN 02 ITNA 7 3 SHE 01

ITNA 7 3 SHE 01

FAA 82 JEN 02

ITNA 7 3 SHE 01

ITNA 7 3 SHE 01

ITNA 7 3 SHE 01

ITNA 73SHE 01

ITNA 7 3 SHE 01

RTNA 82C0H 01

NT 80VIR 01

RTNA 83GLA 01

176
TABLE RR TABLE SS

NBS SRM 616—COLLECTED DATA NBS SRM 688—COLLECTED DATA

CONC

Sb (ppb)

12.

Sc (ppb)

20.

Th (ppb)

18.

ANAL REF REF UNCER COMMENT METH CODE NUM

20.

2.

ITNA 73SHE 01

ITNA 7 3 SHE 01

ITNA 7 3 SHE 01

CONC

Al (%)

8.54

9.3

As (ppm)

2.68

Au (ppb)

0.9

B (ppm)

0.88

1.3

Ba (ppm)

197. 210.

Ca (%)

7.9 8.2

ANAL REF REF UNCER COMMENT METH CODE NUM

0.39

0.2

0.54

0.4

0.14

0.2

33.

30.

0.2

0.6

ITNA

TCGS

ITNA

ITNA

TCGS

TCGS

ITNA

ITNA

TCGS

ITNA

82GRA 01 82GRA 01

82GRA 01

82GRA 01

82GRA 01 83GLA 03

82GRA 01 83GLA 01

82GRA 01 82GRA 01

Ce (ppm)

10.1

Co (ppm)

47.5

55.6

Cr (ppm)

328.

330.

Cs (ppb)

210.

Eu (ppm)

0.919

1 .01

3.9

1.5 1.2

15. 10.

110.

0.048

0.05

ITNA

ITNA ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

82GRA 01

82GRA 01 83GLA 01

82GRA 01 83GLA 01

83GLA 01

82GRA 01 83GLA 01

Fe (%)

7.1 7.23

7.23

0.06

0.19

0.17

ITNA

ITNA

TCGS

83GLA 01 82GRA 01 82GRA 01

Ga (ppm)

57. 10. ITNA 82GRA 01

177
TABLE SS (cont) TABLE SS (cont)

CONC

Gd (ppm)

2.5

2.82

Hf (ppm)

1 .46 1.58

K (ppm)

1700.

La (ppm)

5.9 7.54

Lu (ppb)

342.

Mg (%)

3.9 5.7

Mn (ppm)

1120.

1180.

1290.

Na (%)

1.05

1.39

1.61

Nd (ppm)

9.95

Ni (ppm)

123.

Sb (ppb)

420.

466.

Sc (ppm)

36.1 36.3

Si (%)

24.6

ANAL UF R£F UNCER COMMENT METH CODE NUM

0.08

0.13

0.14

100.

0.2 0.93

57.

0.8

0.4

60.

70.

60.

0.07

0.12

0.01

1.08

29.

207.

0.9

0.5

0.6

ITNA

TCGS

ITNA

ITNA

TCGS

ITNA ITNA

ITNA

ITNA

TCGS

TCGS

ITNA

ITNA

TCGS ITNA

ITNA"

ITNA

ITNA

ITNA

ITNA

ITNA ITNA

TCGS

82GRA 01 82GRA 01

83GLA 01 82GRA 01

82GRA 01

83GLA 01 82GRA 01

82GRA 01

82GRA 01 82GRA 01

82GRA 01 82GRA 01 83GLA 01

82GRA 01 82GRA 01 83GLA 01

82GRA 01

82GRA 01

83GLA 01 82GRA 01

82GRA 01 83GLA 01

82GRA 01

CONC

Sm (ppm)

2.09

2.31

2.54

Sr (ppm)

179.

Ta (ppb)

246.

380.

Tb (ppb)

462.

520.

Th (ppb)

460.

Ti (ppm)

7000.

7200.

U (ppb)

280.

340.

V (ppm)

235.

Yb (ppm)

1.86

Zr (ppm)

58.6

ANAL KEF REF UNCER COMMENT METH CODE NUM

0.22

0.08

0.07

14.

58.

70.

25.

60.

130.

700. 200.

80.

25.

0.27

8.7

ITNA TCGS

ITNA

IENA

ITNA

ITNA

ITNA

ITNA

ITNA

ITNA

TCGS

DNA

ITNA

ITNA

ITNA

ITNA

82GRA 01 82GRA 01 83GLA 01

83GLA 01

82GRA 01 83GLA 01

82GRA 01 83GLA 01

83GLA 01

82GRA 01 82GRA 01

83GLA 01 82GRA 01

82GRA 01

82GRA 01

82GRA 01

178
TABLE TT

NBS SRM 70—COLLECTED DATA TABLE TT (cont)

CONC

Ba (ppm)

380.

Ce (ppm)

Co (ppb)

100.

Cr (ppm)

Cs (ppm)

6.6

Eu (ppb)

400.

Fe (ppm)

300.

Hf (ppb)

Hg (ppb)

98.

La (ppm)

Lu (ppb)

Nd (ppm)

Rb (ppm)

A70.

Sb (ppb)

Sc (ppb)

AO.

ANAL REF REF UNCER COMMENT METH CODE NUM

17.

2.

0.19

10.

200.

5.95

AO.

26.

500.

3.

ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

ITNA 7 7 FLA 01

ITNA 77FLA 01

L* ITNA 77FLA 01

FAA 82 FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

CONC

Sm (ppb)

Ta (ppb)

Tb (ppb)

Th (ppb)

Yb (ppb)

Zn (ppm)

6.7.3

7.5

Zr (ppm)

ANAL REF REF UNCER COMMENT METH CODE NUM

500.

200.

200.

A00.

300.

0.71

L* ITNA 77FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA RTNA

XRF

77FLA 01 65BAL 01 65BAL 01

75. L* ITNA 77FLA 01

179
TABLE UU

NBS SRM 70A—COLLECTED DATA

TABLE UU (cont)

CONC

Ba (ppm)

120. 121.9

C (ppm)

50.

Ca (ppm)

640.

Cd (ppb)

8.7

Ce (ppm)

Co (ppb)

200.

Cr (ppm)

Cs (ppm)

9.28

10.

Eu (ppb)

570.

Fe (ppm)

490.

600.

Hf (ppb)

Hg (ppb)

15.

K (%)

9.71

9.71

9.79

La (ppm)

ANAL REF REF UNCER COMMENT METH CODE NUM

5.

0.15

10.

300.

1.03

ITNA

IDMS

CB

ITNA AA

ITNA

AA

ITNA

FAA

ISE

FEAA

77FLA 01 69LAE 01

78TER 01

AA 7 3 RAM 01

IDMS 74ROS 02

L* ITNA 77FLA 01

ITNA 77FLA 01

L* ITNA 77FLA 01

77FLA 01 72ALL 01

77FLA 01

73RAM 01 77FLA 01

L* ITNA 77FLA 01

82 FLA 01

75PUF 01 75PUF 01 73RAM 01

CONC

Lu (ppb)

Na (%)

1.8

1 .87 1.9

Nd (ppm)

Rb (ppm)

519.1

523.4

524.2

529.8

529 .9 530.

540.

S (ppm)

3.

Sb (ppb)

Sc (ppb)

110.

Se (ppm)

66.1

Sm (ppb)

Sn (ppm)

0.75

Sr (ppm)

64. 65.1

65.5

66.4

Sr 87/86

1.202

1.1978

UNCER COMMENT

ANAL REF METH CODE

REF NUM

100.

1.5

1 .6

1

15.

400.

0.2

200.

0.4

0.1

L*

L*

L*

ITNA

IDMS

ISE AA

FE

ITNA

IDMS

IDMS

IDMS IDMS XRF ITNA AA

0.001

0.0033

CB

ITNA

ITNA

XRF

ITNA

AA

IDMS

IDMS IDMS

IDMS

IDMS

IDMS

77FLA 01 76MCC 03

75PUF 01 73RAM 01 75PUF 01

77FLA 01

82KRA 01 70LAE 01 74COR 01 69COM 01 69COM 01 77FLA 01 72ALL 01

78TER 01

77FLA 01

77FLA 01

69COM 01

77FLA 01

82TER 01

74COR 01 69COM 01 82KRA 01 70LAE 01

69COM 01 74COR 01 L* ITNA 77FLA 01

180
TABLE UU (cont)

TABLE VV

NBS SRM 76—COLLECTED DATA

ANAL REF REF CONC ' UNCER COMMENT METH CODE NUM

Ta (ppb)

150.

Tb (ppb)

Th (ppb)

300.

Tl (ppm)

Yb (ppb)

Zn (ppm)

Zr (ppm)

8.

200.

500.

90.

ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

2.715 0.217 7 ASV 82CAL 01 2.906 0.25 7 ASV 82CAL 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

CONC

Al (%)

20.05

Ca (ppm)

1600.

Fe (%)

1 .47 1.59

K (%)

1 .29

Mg (ppm)

2800.

Mn (ppm)

230.

Si (%)

25.76

Sr (ppm)

85.

Ti (%)

1 .34

ANAL REF REF UNCER COMMENT METH CODE NUM

0.01

WXRF 67KOD 01

WXRF 67K0D 01

COLOR WXRF

59C0L 01 67K0D 01

WXRF 67K0D 01

WXRF 67KOD 01

WXRF 67KOD 01

WXRF 67KOD 01

WXRF 67K0D 01

WXRF 67K0D 01

181
TABLE WW TABLE XX

NBS SRM 77—COLLECTED DATA NBS SRM 88—COLLECTED DATA

CONC

ANAL REF REF UNC ESt COMMENT METH CODE NUM CONC

ANAL REF REF UNCER COMMENT METH CODE NUM

Al (Z) Ca (Z)

30.63 WXRF 67KOD 01 21.81 0.03 TITR 80HIT 02

31.4 XRF 72ASH 01 Co (ppm)

Ca (ppm)

0.7 0.6 RTNA 61T0R 01 1400. WXRF 67KOD 01 Cr (ppm) Fe (ppm)

3.9 RTNA 61TUR 01 WAKr 0 /K.UD A 1 U 1 Fe (ppm) 5700. 100. COLOR 59 COL 01

K (%) 580. 10. COLOR 59 COL 01

1 70 WAKr UCi 11 S (ppm)

Mg (ppm) LI u. 290.

ItJ) CBJ J UJ L

7 7 LAN

U i 01

2 200. WXRF 67K0D 01 inn TI1B 1 UtvDR 7 1CWA nU 11

Mn (ppm) Sr (ppm)

80. WXRF 67K0D 01

55. 60.OES

RTNA

58GRA

61TUR

0101 Si (%) Ti (ppm)

15.3

15.34 XRF WXRF

72ASH

67KOD

0101 24. 340.

4. RTNA

COLOR

65WAH

63K0R

01

01 Sr (ppm)

1200. WXRF 67KOD 01

Ti (%)

1 .82 WXRF 67K0D 01

182
TABLE YY

NBS SRM 88A—COLLECTED DATA TABLE YY (cont)

CONC

Ag (ppm)

Al (ppm)

300.

900.

As (ppm)

Au (ppm)

Ba (ppm)

13.

Be (ppb)

180.

Bi (ppm)

C (%)

12.83

Ca (%)

20.96

22.5

Cd (ppm)

Ce (ppm)

Co (ppm)

3.

Cr (ppm)

11.7

Cu (ppm)

2 .5

Eu (ppm)

1 .2

ANAL REF REF UNCER COMMENT METH CODE NUM

30.

0.26

20.

25.

0.69

15.

1.

L* ICPES 81CHU 01

EXRF 80DAL 01 ICPES 81CHU 01

L* ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01

ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01 EXRF 80DAL 01

I* ICPES 81CHU 01

L* ICPES 81CHU 01

0.6

ICPES 81CHU 01

ICPES 81CHU 01

CONC

Fe (ppm)

2050.

2200.

Gd (ppm)

3.4

Hg (ppb)

28.2

K (ppm)

700.

1000.

La (ppm)

Li (ppm)

Mg (%)

13. 13.06

ANAL REF REF UNCER COMMENT METH CODE NUM

CB 78TER 01 Mn (PP»0

150. 210.

Mo (ppm)

Na (ppm)

104.

Nd (ppm)

ICPES 81CHU 01 Ni ( PPn )

ICPES 81CHU 01 p <PPm)

70. 220.

Pb (ppm)

27.

40.

0.35

0.68

25.

5.

2.

0.4

6.3

7.

20.

3.

ICPES 81CHU 01 EXRF 80DAL 01

ICPES 81CHU 01

FAA 82FLA 01

EXRF 80DAL 01 ICPES 81CHU 01

L* ICPES 81CHU 01

L* ICPES 81CHU 01

EXRF 80DAL 01 ICPES 81CHU 01

EXRF 80DAL 01 ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01

L* ICPES 81CHU 01

L* ICPES 81CHU 01

ICPES 81CHU 01 EXRF 80DAL 01

ICPES 81CHU 01

183
TABLE ZZ

TABLE YY (cont) NBS SRM 91—COLLECTED DATA

CONC ' UNCEB COMMENT

ANAL UF KEF METH CODE NUM CONC ' UNCEB COMMENT

ANAL

METH

REF REF CODE NUM

S (ppra) Al (Z)

4. CB 78TER 01 3.21 35 TCGS 78GLA 04

21. CB / /LAN 01 B (ppm)

Sb (ppm)

302. 0ES 64FIL 01

10. L* ICPES 81 CHI) 01

Ba (ppm)

Se (ppm)

79. 0ES 72AVN 01

30. L* ICPES 81CHU 01

(»a (7,) Si (ppm)

7.54 35 TCGS 78GU I 4100. EXRF 80DAL 01 Co (ppm)

Sm (ppm)

4.5 0ES 72AVN 01

5. L* ICPES 81CHU 01 Cr (ppm)

Sn (ppm)

26. OES 64FIL 01

3. L* ICPES 81CHU 01 26. 0ES 72AVN 01

Sr (ppm) Cu (ppm)

41. 0.8 ICPES 81CHU 01 16. OES 72AVN 01

96. 0ES 75TH0 01 F (Z>

Th (ppm)

5.1 * IC 82WIL 02

25. L* ICPES 81CHU 01 5.16

5.6

*35

0.16 11

I ENA

ISE

79GLA 03

77H0P 01 Ti (ppm) 5.62 0.08 NAA 80NOR 01 5.68 0.15 ISE 77TRO 01 66. 180.

2. ICPES EXRF

81CHU 01

80DAL 01

5.7 5.72

5.75

11

0.003

ISE

ISE

ISE

77H0P 01 70ING 01

71 PET 01

1! ( nDin^ Fe (ppm)

25. L* ICPES 81CHU 01 430. OES 64FIL 01

V (ppm) 600.

4000.

35

35

I ENA

TCGS

79GLA 03

78GLA 04

9. 1. ICPES 81CHU 01 5200. 100. COLOR 59COL 01

Yb (ppm) Cln ( TtrnrtS

1.2 0.04 ICPES 81CHU 01 12. OES 72AVN 01

Zn (ppm) K (Z)

4.1 1. ICPES 81CHU 01 2.68 35 TCGS 78GLA 04

Zr (ppm) Mg (ppm)

1. L* ICPES 81CHU 01 60. 35 TCGS 78GLA 04

184
TABLE AAA

TABLE ZZ (cont) NBS SRM 950A—COLLECTED DATA

CONC

Mn (pptn)

39. 63.

Na (%)

6.23

6.32

Ni (ppm)

0.79

6.

0 (X)

49.

Pb (ppm)

17. 1150.

Si (%)

31.5

32.1 32.2

Sr (ppm)

39.

Ti (ppm)

110. 140.

156.

U (ppb)

540.

V (ppm)

43.

Zr (ppm)

47.

ANAL REF REF UNCER COMMENT METH CODE MUM

0.6

1.21

350.

35

35

35

0ES

0ES

IENA

TCGS

IENA 0ES

35

35

L*

35

0ES

OES

AA

TCGS IENA

OES

IENA

TCGS OES

OES

DNA

OES

64FIL 01 72AVN 01

79GLA 03

78GLA 04

79GIA 03

72AVN 01

14NAA 80N0R 01

64FIL 01 72AVN 01

82KIS 01 78GLA 04 79GLA 03

72AVN 01

79GLA 03

78GLA 04

72AVN 01 64FIL 01

66HAM 01

72AVN 01

CONC

U2 36/235

UNCER COMMENT

137.55

138.889

137.9

138.

0.29

4761.

0.2

0.4

U234/238

0.00005672

U2 35/238

727.65

ANAL

METH

IDMS

MSIDMS

IDMS

IDMS

IDMS

REF REF CODE NUM

79UNR 01 82SMI 01

81 CHE 02

81 CHE 01

80RIL 01

80RIL 01

OES 64FIL 01

185
TABLE BBB

NBS SRM 97—COLLECTED DATA TABLE BBB (cont)

CONC

Al (2)

20.47

20.51

B (ppm)

57.

71 .3

Ba (ppm)

110.

141. 270.

Be (ppm)

1.3

C (ppm)

3200.

Ce (ppm)

57. 60.7

Co (ppm)

3.3 3.46

4.4

Cr (ppm)

486.

500.

540. 576.

581

.

639.

Cs (ppm)

2.4

Cu (ppm)

11. 18.5

20.

22.

Dy (ppm)

4.28

UNCER COMMENT

21.

29.

0.06

14.4

0.08

ANAL

METH

COLOR

CHEW

0ES

OES

OES

OES

ITNA

OES

CB

ITNA

OES

ITNA

OES RTNA

OES

COLOR

CHEM

ITNA RTNA AA

ITNA

OES

OES

CHEM COLOR

OES

REF MF

CODE NUM

57SHI 01 57SHI 01

64FIL 01 77FLA 01

77FLA 01 58GRA 01 77FLA 01

77FLA 01

78TER 01

77FLA 01 77FLA 01

77FLA 01 77FLA 01 61TUR 01

77FLA 01

57 SHI 01

57 SHI 01 77FLA 01 61TUR 01 80D0N 01

77FLA 01

64FIL 01 77FLA 01 57SHI 01

57 SHI 01

77FLA 01

CONC

Eu (ppm)

1 .24 1.56

Fe (ppm)

6500.

6600.

6600.

6800.

Ga (ppm)

45.1

Hf (ppm)

39.5

Hg (ppb)

68.

159.2

La (ppm)

34.

Li (ppm)

1074.

Lu (ppm)

0.96

Mg (%)

0.13

0.16

Mn (ppm)

16.

35. 99.7

Mo (ppm)

2.

Nb (ppm)

35.6

Nd (ppm)

19.

ANAL REF REF UNCER COMMENT METH CODE NUM

0.03

100.

100.

1.19

6.22

14.7 0.71

0.02

L*

ITNA 77FLA 01 OES 7 7FLA 01

COLOR 59 COL 01 ITNA 77FLA 01 COLOR 57 SHI 01 CHEM 57SHI 01

OES

FAA

FAA

OES

ITNA

CHEM OES

OES

CHEM

OES

ITNA

77FLA 01

ITNA 77FLA 01

75HEI 01 82FLA 01

7 7 FLA 01 77FLA 01

OES 77FLA 01

ITNA 77FLA 01

COLOR 5 7 SHI 01 CHEM 57SHI 01

57 SHI 01 64FIL 01 77FLA 01

57SHI 01

77FLA 01

77FLA 01

186
TABLE BBB (cont) TABLE BBB (cont)

CONC

Ni (ppm)

32. 36.8

Pb (ppm)

34.3

35.

Rb (ppm)

24.

S (ppm)

158. 170. 200.

Sb (ppm)

1.4

Sc (ppm)

12.1 20.7

Si (%)

20.

ANAL REF REF UNCER COMMENT METH CODE NUM

1.6

0.11

0.17

OES

0ES

OES FAA

ITNA

CB

CB

TURB

ITNA

OES

ITNA

64FIL 01 77FLA 01

77FLA 01 79HEI 03

77FLA 01

78TER 01 55C0L 01 73SHA 01

77FLA 01

77FLA 01 77FLA 01

CONC

Ti (%)

1 .3 1.43

V (ppm)

148. 205.

234. 362.

Y (ppm)

33. 37.6

Yb (ppm)

6.8 7.47

Zn (ppm)

81 . 103.

Zr (ppm)

1390.

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

0.17

3.15

34.8

COLOR

CHEM

OES

COLOR

CHEM OES

OES

OES

ITNA OES

XRF ITNA

ITNA

57SHI 01

57 SHI 01

64FIL 01

57 SHI 01

57 SHI 01 77FLA 01

64FIL 01 77FLA 01

77FLA 01 77FLA 01

65BAL 01 77FLA 01

77FLA 01

TITR 770HL 01

Sm (ppm)

4.64 L* OES 77FLA 01 5.8 0.08 ITNA 77FLA 01

Sn (ppm)

7. OES 64FIL 01 10.1 OES 77FLA 01

Sr (ppm)

30. RTNA 61TUR 01

88. OES 58GRA 01 101. OES 77FLA 01

Ta (ppm)

4.2 0.09 ITNA 77FLA 01

Tb (ppm)

1.27 0.02 ITNA 77FLA 01

Th (ppm)

37. 0.48 ITNA 77FLA 01

187
TABLE CCC

NBS SRM 97A—COLLECTED DATA TABLE CCC (cont)

CONC

B (ppm)

69.4

Ba (ppm)

660.

Be (ppm)

3.55

C (ppm)

600.

Ce (ppm)

124. 203.

Co (ppm)

4.1 4.64

Cr (ppm)

180. 203.

Cs (ppm)

1.6

Cu (ppm)

24.9

Dy (ppm)

8.89

Eu (ppm)

3.66

3.81

Fe (ppm)

3000.

Ga (ppm)

31.6

Hf (ppm)

11.3

15.4

ANAL REF REF UNCER COMMENT METH CODE NUM

20.6

3.51

0.08

4.1

0.6

0.02

30.

0ES 77FLA 01

ITNA 77FLA 01

0ES 77FLA 01

CB 78TER 01

0ES

ITNA

ITNA OES

ITNA OES

OES

ITNA

0.39

OES

ITNA RTNA

77FLA 01 77FLA 01

77FLA 01 77FLA 01

77FLA 01 77FLA 01

ITNA 77FLA 01

OES 7 7 FLA 01

OES 77FLA 01

77FLA 01 77FLA 01

ITNA 77FLA 01

CONC

Hg (ppb)

387.5

La (ppm)

43.7

103.

Li (ppm)

439.

Lu (ppm)

0.98

Mn (ppm)

5.24

Nb (ppm)

39.

Nd (ppm)

88.

Nl (ppm)

81.

Pb (ppm)

41.7

Rb (ppm)

S (ppm)

308.

Sb (ppb)

800.

Sc (ppm)

21.3

31.3

ANAL KEF REF UNCER COMMENT METH CODE HUM

77FLA 01 Sm <'PP"0

6.88

21.3

22.5

1 .83

0.04

3.7

20.

100.

0.75

0.69

FAA 82 FLA 01

OES

ITNA

7 7 FLA 01 77FLA 01

OES 77FLA 01

ITNA 77FLA 01

OES 7 7 FLA 01

OES 77FLA 01

ITNA 7 7 FLA 01

OES 77FLA 01

OES 77FLA 01

L* ITNA 77FLA 01

CB 78TER 01

ITNA 7 7FLA 01

OES ITNA

OES

ITNA

77FLA 01 77FLA 01

7 7 FLA 01

7 7 FLA 01 77FLA 01 76GAN 01

188
TABLE DDD

TABLE CCC (cont) NBS SRM 98—COLLECTED DATA

CONC

Sn (ppm)

6.16

6.53

Sr (ppm)

860.

Ta (ppm)

3.21

Tb (ppm)

2.77

Th (ppm)

31.1

U (ppm)

6.58

V (ppm)

362.

Y (ppm)

121.

Yb (ppm)

7.7

10.1

Zn (ppm)

Zr (ppm)

465.

580.

ANAL REF BJEF WNCER COMMENT METH CODE NUM

AA 82TER 01 OES 77FLA 01

0.06

0.08

0.37

OES

ITNA

ITNA

ITNA

0.23

20.

19. 21.

L* ITNA

RTNA

ITNA

77FLA 01

77FLA 01

77FLA 01

77FLA 01

RTNA 76GAN 01

OES 77FLA 01

OES 77FLA 01

ITNA 77FLA 01 OES 77FLA 01

77FLA 01

76GAN 01

7 7 FLA 01

CONC

Al (X)

13.48

13.5

13.5

13.51

13.65

B (ppm)

68. 78.5

150. 250.

Ba (ppm)

570.

670. 800.

Be (ppm)

4.1

C (ppm)

4000.

Ca (ppm)

1500. 1500.

1600.

Ce (ppm)

119. 135.

Co (ppm)

13.8

15. 16.5

16.9

17.

Cr (ppm)

113. 119.

130.

136. 143. 144.

150.

170. 250.

1400. 1600.

UNCER ANAL REF REF COMMENT METH CODE NUM

TITR

CHEM OES

CHEM COLOR

OES

OES OES

OES

10.8

1.32

0.1

2.33

CHEM

OES TITR

OES

ITNA

ITNA OES

RTNA

OES OES

58WAT 01 62JOE 01 62JOE 01 57SHI 01 57SHI 01

64FIL 01 77FLA 01 63CLA 01 63CLA 01

OES 58GRA 01 ITNA 77FLA 01 OES 63CLA 01

OES 77FLA 01

CB 78TER 01

62JOE 01 62JOE 01 80HIT 02

77FLA 01 77FLA 01

77FLA 01 63CLA 01 61TUR 01 77FLA 01 64FIL 01

ITNA 77FLA 01 OES 64FIL 01 RTNA 61TUR 01 OES 77FLA 01 AA 80DON 01 CHEM 5 7 SHI 01

3 OES 63CLA 01 COLOR 57SHI 01

3 OES 63CLA 01

* CHEM 62JOE 01

* OES 62JOE 01

189
TABLE DDD (cont) TABLE DDD (cont)

CONC

Cs (ppm)

10.7

Cu (ppm)

33.7

39. 70.

70.

72. 100.

Dy (ppm)

7.07

Eu (ppm)

1 .74 2.07

Fe (%)

1.12

1 .17

1 .38 1.4 1.4

1 .43

Ga (ppm)

24.1

80.

Hf (ppm)

7.

Hg (ppb)

462.6

La (ppm)

55.2

79.

150.

Li (ppm)

144.

Lu (ppb)

650.

UNCER COMMENT

ANAL

METH UF REF CODE NUM

0.17

0.02

0.01

0.05

100. L*

3

0.42

12.1

1.7

ITNA

OES OES

COLOR

OES

CHEM

OES

OES

ITNA

OES

CHEM OES

COLOR

ITNA COLOR

CHEM

OES OES

OES

ITNA

FAA

OES

ITNA OES

OES

ITNA

77FLA 01

7 7 FLA 01 64FIL 01 57SHI 01 63CLA 01 57SHI 01 63CLA 01

77FLA 01

77FLA 01 77FLA 01

62J0E

62J0E

59COL 01 77FLA 01

5 7 SHI

57 SHI

01

01

0101

63CLA 01

7 7 FLA 01 63CLA 01

7 7 FLA 01

82 FLA 01

77FLA 01 77FLA 01 63CLA 01

77FLA 01

77FLA 01

CONC

Mg (ppm)

4100.

4 200.

4 300.

4 300. 4600.

Mn (ppm)

39. 39. 40.

96.5

100.

100.

Mo (ppm)

1.

Nd (ppm)

49.

Ni (ppm)

39. 40.

52.8

P (ppm)

350.

390.

Pb (ppm)

40. 47.5

Rb (ppm)

154.

S (ppm)

250.

270.

300.

Sb (ppm)

1.3

Sc (ppm)

22.1

22.9

30.

UNCER COMMENT

ANAL

METH

REF REF CODE NUM

80.

1

0.58

L*

L*

1111

1.12

0.12

0.06

TITR

OES

CHEM CHEM

COLOR

OES

OES

CHEM

CHEM

OES

OES

OES

OES CHEM

ITNA

OES

OES

OES

COLOR

COLOR

OES

OES

ITNA

CB

CB

TURB

ITNA

OES

ITNA OES

80HIT 02

62J0E 01 62JOE 01 57SHI 01 57SHI 01

62J0E 01 64FIL 01

57 SHI 01 62JOE 01 77FLA 01 63CLA 01 63CLA 01

63CLA 01 57SHI- 01

77FLA 01

64FIL 01 63CLA 01 77FLA 01

76WHI 01 76WHI 01

63CLA 01 77FLA 01

77FLA 01

78TER 01 55C0L 01 73SHA 01

77FLA 01

77FLA 01 77FLA 01 63CLA 01

190
TABLE DDD (cont) TABLE DDD (cont)

ANAL KEF KEF CONC UNCER COMMENT METH CODE NUM CONC

Se (ppm) Y (ppm)

1 .04 0.08 FLUOR 74CRE 01 28.

1 .2 UU 74WAH 01 40.

1.37 UU 6 5WEL 01 46.7

Si (%) Yb (ppm)

*)7 CO TITR 770HL 01 27.6 CHEM 62J0E 01 6.8

27 .6 0ES 62J0E 01 21.2

Cm t \ Zn (ppm)

O.J Arc 77F1 lie LtAA U 1 125. U.Hi ITNA 7lit7T?1UAA

Sn (ppm) ^ppm;

6.47 0ES 77FLA 01 ion 270.

Sr (ppm) { 300. 300. 205. RTNA 61TUR 01 340.

377. 230. OES 58GRA 01 300. 0ES 63CLA 01 326. OES 77FLA 01 390. OES 75THO 01

Ta (ppm)

2.22 0.03 ITNA 77FLA 01

Tb (ppm)

1.35 0.02 ITNA 77FLA 01

Th (ppm)

U.Z 1 ITNA 77FLA 01

Ti (ppm)

8400. CHEM 62JOE 01 8600. CHEM 57 SHI 01 8690. OES 62JOE 01 9000. 3 OES 63CLA 01 9300. COLOR 5 7 SHI 01 10000. 3 OES 63CLA 01

V (ppm)

106. OES 64FIL 01

120. OES 62JOE 01 140. CHEM 62JOE 01 140. CHEM 57SHI 01 161. COLOR 57 SHI 01 200. 3 OES 63CLA 01 300. 3 OES 63CLA 01 310. OES 7 7 FLA 01

UNCER COMMENT

0.1

2.1

19.6

ANAL

METH

OES

OES

OES

ITNA OES

OES

ITNA

OES

OES

CHEM OES

ITNA OES

KEF KEF CODE NUM

64FIL 01 63CLA 01 77FLA 01

77FLA 01 77FLA 01 77FLA 01

77FLA 01

64FIL 01

62 JOE 01 62 JOE 01 63CLA 01 77FLA 01 77FLA 01

191
TABLE EEE

NBS SRM 98A—COLLECTED DATA TABLE EEE (cont)

CONC

B (ppm)

120.

Ba (ppm)

168. 480.

Be (ppm)

5.93

C (ppm)

8100.

Ce (ppm)

180. 219.

Co (ppm)

11.5

14.4

Cr (ppm)

212.

234.

Cs (ppm)

6.2

Cu (ppm)

121.

Dy (ppm)

17.5

Eu (ppm)

3.18

3.52

Fe (ppm)

8800.

Ga (ppm)

23.3

Hf (ppm)

7.3

ANAL REF UF

UNCER COMMENT METH CODE NUM

20.

0.29

0.06

4.8

0.06

0.02

30.

0ES 77FLA 01

OES

I TOA

OES

I TOA

I TOA OES

I TOA

OES

I TOA OES

77FLA 01 77FLA 01

OES 77FLA 01

CB 78TER 01

77FLA 01 77FLA 01

77FLA 01 77FLA 01

77FLA 01 77FLA 01

I TOA 77FLA 01

OES 77FLA 01

OES 77FLA 01

77FLA 01 77FLA 01

0.14

ITOA 77FLA 01

OES 77FLA 01

ITOA 77FLA 01

CONC

Hg (ppb)

39.3

La (ppm)

91.7

162.

Li (ppm)

291

Lu (ppm)

1 .15

Mn (ppm)

41.4

Nb (ppm)

39.9

Nd (ppm)

98.

Ni (ppm)

162.

Pb (ppm)

69.2

Rb (ppm)

35.

S (ppm)

1300.

Sb (ppm)

2.3

Sc (ppm)

28.8

34.8

Sm (ppm)

9.18

15.

ANAL REF REF UNCER COMMENT METH CODE NUM

4.8

2.99

0.06

2.6

2.3

0.1

0.21

2.4

FAA 82 FLA 01

OES

ITOA

77FLA 01 77FLA 01

OES 77FLA 01

ITOA 77FLA 01

OES 77FLA 01

OES 77FLA 01

ITOA 77FLA 01

OES 77FLA 01

OES 77FLA 01

ITOA 77FLA 01

CB 78TER 01

ITOA 77FLA 01

OES

ITOA

OES

ITOA

77FLA 01 77FLA 01

77FLA 01 77FLA 01

192
TABLE FFF

TABLE EEE (cont) NBS SRM 99—COLLECTED DATA

ANAL REF KEF CONC " UNCER COMMENT METH CODE HUM

Sn (ppm)

4.88

5.25

Sr (ppm)

438.

Ta (ppm)

2.46 0.03

Tb (ppm)

2.92 0.06

Th (ppm)

23.9

Tl (ppb)

351.

V (ppm)

554.

Y (ppm)

176.

Yb (ppm)

9.3

10.3

Zn (ppm)

Zr (ppm)

740.

0.11

40.

0.29

23.

32.

OES 77FLA 01 AA 82TER 01

OES 77FLA 01

ITNA 77FLA 01

ITNA 77FLA 01

ITNA 77FLA 01

7 ASV 82CAL 01

OES 77FLA 01

OES 77FLA 01

ITNA 77FLA 01 OES 7 7 FLA 01

L* ITNA 7 7 FLA 01

ITNA 77FLA 01

CONC

Al (%)

10.07

B (ppm)

10.

Ba (ppm)

Ce (ppm)

8.

Co (ppb)

700.

780.

Cr (ppm)

3.3

5.3

13.

Cs (ppb)

700.

Cu (ppm)

20. 22.

Eu (ppb)

350.

Fe (ppm)

500.

Ga (ppm)

30.

Hf (ppb)

900.

La (ppm)

ANAL REF REF UNCER COMMENT METH CODE NUM

130. 800.

0.6

10000.

30. 120.

20.0.16

100.

60.

100.

8.

L*

L*

L*

L*

TITR 58WAT 01

OES 63CLA 01

ITNA OES

OES

ITNA RTNA

OES

ITNA

RTNA OES

OES

OES

77FLA 01 63CLA 01

ITNA 77FLA 01

63CLA 01

7 7 FLA 01 61TUR 01

63CLA 01 77FLA 01 61TUR 01 64FIL 01

ITNA 77FLA 01

63CLA 01 64FIL 01

ITNA 77FLA 01

ITNA 77FLA 01

OES 63CLA 01

ITNA 77FLA 01

L*

L*

OES ITNA63CLA 01 77FLA 01

193
TABLE FFF (cont) TABLE FFF (cont)

CONC

ANAL B£F KEF UNCER COMMENT METH CODE HUM

Lu (ppb)

Mn (ppm)

12. 50.

Nd (ppm)

Ni (ppm)

15.

P (ppm)

567.

Pb (ppm)

62.

150.

Rb (ppm)

23.

Sb (ppb)

500.

Sc (ppb)

830.

Si (%)

32.05

32.05

Sm (ppm)

Sr (ppm)

120. 130. 400.

Ta (ppm)

1.9

Tb (ppb)

280.

200.

1.6

60.

10000.

10.

0.01

0.02

6-

L* ITNA 77FLA 01

L*

OES

OES

OES

OES

OES ITNA

RTNA

OES

OES

64FIL 01 63CLA 01

L* ITNA 77FLA 01

OES 63CLA 01

OES 64FIL 01

64FIL 01 63CLA 01

ITNA 77FLA 01

ITNA 77FLA 01

63CLA 01 77FLA 01

TITR 770HL 01 COLOR 82SAR 01

L* ITNA 77FLA 01

61TUR 01 75TH0 01 63CLA 01

ITNA 77FLA 01

ITNA 77FLA 01

CONC

Th (ppm)

1.6

Ti (ppm)

61 . 150.

200.

560.

U (ppm)

1.09

V (ppm)

Y (ppm)

10.

Yb (ppm)

1.

Zn (ppm)

14.6

15.

18.

Zr (ppm)

11. 40.

ANAL REF R£F UNCER COMMENT METH CODE NUM

0.03

10.

0.06

0.82

100.

ITNA 7 7 FLA 01

OES 64FIL 01

3 OES 63CLA 01

3 OES 63CLA 01 COLOR 63K0R 01

DNA 66HAM 01

L* OES 63CLA 01

OES 63CLA 01

ITNA 77FLA 01

L*

RTNA XRF

ITNA

ITNA OES

OES

65BAL 01 65BAL 01 77FLA 01

77FLA 01 64FIL 01 63CLA 01

194
TABLE OOG

NBS SRM 99A—COLLECTED DATA TABLE GGG (cont)

CONC

Ba (ppm)

2570.

C (ppm)

300.

Ca (Z)

1.51

Ce (ppm)

5.

Co (ppb)

100.

Cr (ppm)

Cs (ppm)

0.5

9.

Eu (ppb)

820.

Fe (ppm)

450.

500.

Hf (ppb)

300.

Hg (ppb)

164.6

K (%)

4.2

4.2

4.4

La (ppm)

22.

Lu (ppb)

Mg (ppm)

130.

ANAL KEF REF UNCER COMMENT METH CODE NUM CONC

ANAL REF REF UNCER COMMENT METH CODE NUM

38.6

0.29

3.

0.03

30.

7.35

0.13

1.9

100.

ITNA 77FLA 01

AA 7 3 RAM 01

ITNA 77FLA 01

ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA AA77FLA 01 72ALL 01

ITNA 77FLA 01

AA

ITNA

73RAM 01 77FLA 01

ITNA 77FLA 01

FAA 82 FLA 01

ISE

FEAA

75PUF 01 75PUF 01

7 3 RAM 01

ITNA 77FLA 01

L* ITNA 77FLA 01

AA 73RAM 01

Na (%)

4.45

4.6

4.6

CB 78TER 01 Nd (ppm)

Rb (ppm)

100.

109.

S (ppm)

19.

Sb (ppb)

Sc (ppb)

230.

Si (%)

30.42

Sm (ppb)

500.

Sn (ppm)

0.45

Ta (ppb)

Tb (ppb)

Th (ppb)

500.

Yb (ppb)

Zn (ppm)

Zr (ppm)

70.

0.1

4.

1.2

300.

0.4

70.

200.

200.

300.

AA

FEISE

73RAM 01 75PUF 01 75PUF 01

L* ITNA 77FLA 01

AA

ITNA

72ALL 01 77FLA 01

CB 78TER 01

L* ITNA 77FLA 01

ITNA 77FLA 01

AA 82KIS 01

ITNA 77FLA 01

AA 82TER 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

L* ITNA 77FLA 01

L* ITNA 77FLA 01

ITNA 77FLA 01

195
TABLE hHH: REFERENCES FOR NBS SRM COLLECTED DATA

CODE N DESCRIPTION

55COL 01 M. E. COLLER AND R. K. LEININCER ( 1955) DETERMINATION OF TOTAL SULFUR CONTENT OF SEDIMENTARY ROCKS

BY A COMBUSTION METHOD, ANALYTICAL CHEMISTRY, 27: 949-951.

57SHI 01 N.F. SHIHP, J. CONNOR, A.L. PRINCE, F.E. BEAR (1957) SPECTROCHEMICAL ANALYSIS OF SOILS AND BIOLOGICAL MATERIALS

SOIL SCIENCE, 83: 51-64.

58GRA 01 R. J. GRABOWSKI AND R. C. UNICE (1958) QUANTITATIVE SPECTRO CHEMICAL DETERMINATION OF BARIUM AND

STRONTIUM, ANALYTICAL CHEMISTRY, 30: 1374-1379.

58UAT 01 H. L. WATTS ( 1958) VOLUMETRIC DETERMINATION OF ALUMINIUM IN PRESENCE OF IRON, TITANIUM, CALCIUM, SILICON, AND OTHER IMPURITIES, ANALYTICAL CHEMISTRY, 30: 967-970.

59C0L 01 P. F. COLLINS, H. DIEHL, AND C. F. SMITH (1959) DETERMINATION OF IRON IN LIMESTONE, SILICATES, AND

REFRACTORIES, ANALYTICAL CHEMISTRY , 31: 1862-1867.

61TUR 01 K. K. TUREKIAN AND M. H. CARR (1961) CHROMIUM, COBALT AND STRONTIUM IN SOME BUREAU OF STANDARDS

ROCK REFERENCE SAMPLES, GEOCHIMICA ET COSMOCHIMICA ACTA,

24: 1-9.

62J0E 01 0. I. JOENSUU AND N. H . SUHR ( 1962) SPECTROCHEMICAL ANALYSIS OF ROCKS, MINERALS , AND RELATED

MATERIALS, APPLIED SPECTROSCOPY, 16: 101-104.

63CLA 01 M. C. CLARK AND D.J. SWAINE ( 1963) TRACE-ELEMENT CONTENTS OF THE NATIONAL BUREAU OF STANDARDS

REFERENCE SAMPLES NUMBERS 1A, 98 AND 99, GEOCHIMICA ET COSMOCHIMICA ACTA, 27 : 1 139-1 142.

63KOR 01 J. KORKISCH, G. ARRHENIUS AND D. P. KHARKAR ( 1963) SPECTROPHOTOMETRIC DETERMINATION OF TITANIUM AFTER

SEPARATION BY ANION EXCHANGE , ANALYTICA CHIMICA ACTA,

28: 270-277.

64FIL 01 R. H. FILBY ( 1964) THE CONTENTS OF SEVERAL TRACE ELEMENTS IN SOME STANDARD ROCK SAMPLES, GEOCHIMICA ET COSMOCHIMICA ACTA, 28: 265-269.

65BAL 01 T. K. BALL AND R. H. FILBY ( 1965) THE ZINC CONTENTS OF SOME GEOCHEMICAL STANDARDS BY NEUTRON ACTIVATION AND X-RAY FLUORESCENCE ANALYSIS, GEOCHIMICA ET COSMOCHIMICA ACTA, 29 : 737-740.

65MTA 01 PROCEEDINGS OF THE 1965 INTERNATIONAL CONFERENCE ON MODERN TRENDS IN ACTIVATION ANALYSIS , COLLEGE STATION, TEXAS , APRIL 19-22.

65WAH 01 W. H. WAHL, V. J. MOLINSKI , AND H. ARINO (1965) RAPID RADIOCHEMICAL SEPARATION PROCEDURES FOR ACTIVATION ANALYSIS INDICATORS, IN 65MTA 01, PP. 44-47.

65WEL 01 N. WELLS (1965) SELENIUM CONTENT OF SOIL-FORMING ROCKS, NEW ZEALAND JOURNAL

OF GEOLOGY AND GEOPHYSICS, 10: 198-208; TAKEN FROM 74CRE 01.

66HAM 01 E. I. HAMILTON (1966) THE URANIUM CONTENT OF SOME INTERNATIONAL STANDARDS, EARTH

AND PLANETARY SCIENCE LETTERS, 1: 317-318.

67KOD 01 H. KODAMA, J. E. BRYDON , AND B. C. STONE (1967) X-RAY SPECTROCHEMICAL ANALYSIS OF SILICATES USING SYNTHETIC

STANDARDS WITH A CORRECTION OF I NTERELEMENTAL EFFECTS BY A

COMPUTER METHOD, GEOCHIMICA ET COSMOCHIMICA ACTA,

31: 649-659.

69COM 01 W. COMPSTON, B.W. CHAPPELL, P.A. ARRIENS, M.J. VERNON (1969) ON THE FEASIBILITY OF NBS 70A K-FELDSPAR AS A RB-SR AGE REFERENCE SAMPLE, GEOCHIMICA ET COSMOCHIMICA ACTA, 33: 753-757.

6 9 EDM 01 C. R. EDMOND (1969) DIRECT DETERMINATION OF FLUORIDE IN PHOSPHATE ROCK SAMPLES USING THE SPECIFIC ION ELECTRODE, ANALYTICAL CHEMISTRY,

41: 1327-1328.

CODE N DESCRIPTION

69LAE 01 J. R. DE LAETER, I. D. ABERCROMBIE, AND R. DATE ( 1969) MASS SPECTROMETRIC ISOTOPE DILUTION ANALYSES OF BARIUM IN STANDARD ROCKS, EARTH AND PLANETARY SCIENCE LETTERS,

7: 64-66.

69THI 01 G. THIELICKE ( 1969) TITRIMETRISCHE BESTIMMUNG DES ALUMINIUMS IN SI LICATGESTEINEN MIT POTENT! OMETRISCHER INDICATION, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 246: 118-122.

69WIC 01 R. WICKBOLD ( 1969) EXTRACTION DES EISENS MIT METHYLISOBUTYLKETON UND SEINE TITRATION IM EXTRACT MIT ADTA, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 244 : 372-375.

70ING 01 B. L. INGRAM (1970) DETERMINATION OF FLUORIDE IN SILICATE ROCKS WITHOUT

SEPARATION OF ALUMINIUM USING A SPECIFIC ION ELECTRODE

ANALYTICAL CHEMISTRY, 4 2: 1825-1827.

70LAE 01 J. R. DE LAETER AND I. D. ABERCROMBIE ( 1970) MASS SPECTROMETRIC ISOTOPE DILUTION ANALYSES OF RUBIDIUM AND

STRONTIUM IN STANDARD ROCKS , EARTH AND PLANETARY SCIENCE

LETTERS, 9: 327-330.

71 FAB 01 B. P. FABBI (1971) RAPID X-RAY FLUORESCENCE DETERMINATION OF PHOSPHORUS IN GEOLOGICAL SAMPLES, APPLIED SPECTROSCOPY, 25: 4 1-4 3.

71PET 01 M. A. PETERS AND D. M. LADD (1971) DETERMINATION OF FLUORIDE IN OXIDES WITH THE FLUORIDE-ION

ACTIVITY ELECTRODE, TALANTA, 18 : 655-664.

72ALL 01 W. J. F. ALLEN (1972) THE DETERMINATION OF RUBIDIUM AND CAESIUM IN GEOLOGICAL MATERIALS BY ATOMIC EMISSION SPECTROPHOTOMETRY WITH A NITROUS OXI DE -ACETYLENE FLAME , ANALYTICA CHIMICA ACTA,

59: 111-117.

72ASH 01 D. G. ASHLEY AND K. W. ANDREWS (1972) ANALYSIS OF ALUMINOSILICATE MATERIALS BY X-RAY FLUORESCENCE

SPECTROMETRY , ANALYST, 97: 84 1-845.

72AVN 01 R. AVNI, A. HAREL , AND I. B. BRENNER ( 1972) A NEW APPROACH TO THE SPECTROCHEMICAL ANALYSIS OF SILICATE

ROCKS AND MINERALS, APPLIED SPECTROSCOPY, 26: 641-645.

72BEC 03 D. A. BECKER AND P. D. LAFLEUR ( 1972) DETERMINATION OF TRACE QUANTITIES OF URANIUM IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS USING A RAPID

RADIOCHEMICAL SEPARATION, ANALYTICAL CHEMISTRY , 44: 1508-1511.

72B0U 01 J. L. BOUVIER, J. G. SEN GUPTA, AND S. ABBEY (1972) TITLE UNKNOWN, GEOLOGICAL SURVEY OF CANADA PAPER 72-31,

P. 22; TAKEN FROM 77LAN 01.

72BOW 01 H. J. M. BOWEN (1972) THE DETERMINATION OF TIN IN BIOLOGICAL MATERIAL BY USING NEUTRON-ACTIVATION ANALYSIS, ANALYST, 97: 1003-1005.

72BYR 01 A. R. BYRNE (1972) THE TOLUENE EXTRACTION OF SOME ELEMENTS AS IODIDES FROM H2S04-KI MEDIA. APPLICATION TO NEUTRON ACTIVATION ANALYSIS, ANALYTICA CHIMICA ACTA, 59: 91-99.

72DAM 01 E. DAMSGAARD, K. HEYDORN, AND B. RIETZ (1972) DETERMINATION OF VANADIUM IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS, NUCLEAR ACTIVATION TECHNIQUES IN THE LIFE SCIENCES: 1972, IAEA, VIENNA, PP. 119-130, IN 72IAE 01.

72GIB 01 D. GIBBONS, M. PERKINS, T.W. SANDERS, (1972) DETERMINATION OF LEAD IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS, PP. 131-138, IN 72IAE 01.

72HEI 01 M. W. BEITZMAN AND R. E. SIMPSON (1972) NEUTRON ACTIVATION ANALYSIS OF MERCURY IN FISH, FLOUR, AND

STANDARD REFERENCE ORCHARD LEAVES BY ELECTRO DEPOSITION RAD- IOCHEMISTRY , JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL

CHEMISTS, 55: 960-965.

196
CODE N DESCRIPTION CODE N DESCRIPTION

72IAE 01 NUCLEAR ACTIVATION TECHNIQUES IN THE LIFE SCIENCES ( 1972) PROCEEDINGS OF A SYMPOSIUM ON NUCLEAR ACTIVATION TECHNIQUES

IN THE LIFE SCIENCES HELD BY THE IAEA IN BLED, YUGOSLAVIA,

APRIL, 1972, STI/PUB/310.

72LEV 01 M. LEVSTEK AND L. KOSTA, M. DERKELJ , AND A. R. BYRNE (1972) VANADIUM DETERMINATION IN BIOLOGICAL MATERIALS BY THE USE OF PRECONCENTRAIION, NUCLEAR ACTIVATION TECHNIQUES IN THE LIFE

SCIENCES, IAEA, VIENNA, PP. 111-116, IN 72IAE 01.

72LYO 01 H. 8. LYON, L. C. BATE, J.P. EMERY (1972) ENVIRONMENTAL POLLUTION: USE OF NEUTRON ACTIVATION ANALYSIS TO DETERMINE THE FATE OF TRACE ELEMENTS FROM FOSSIL FUEL COMBUSTION IN THE ECOLOGICAL CYCLE, PP. 253-261 , IN 72IAE 01.

72MAG 01 C. W. MAGEE, D. L. DONOHUR , AND W. W. HARRISON (1972) ADVANTAGES OF DUAL ELECTRODE MOUNTS IN SPARK SOURCE MASS SPECTROMETRY USING ELECTRICAL DETECTION, ANALYTICAL CHEMISTRY, 44: 2413-2415.

72MAI 01 E. J. MAIENTHAL (1972) ANALYSIS OF BOTANICAL STANDARD REFERENCE MATERIALS BY CATHODE RAY POLAROGRAPHY , JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 55: 1109-1113.

72MOR 03 G. H. MORRISON AND N. M. POTTER (1972) MULTIELEMENT NEUTRON ACTIVATION ANALYSIS OF BIOLOGICAL MATERIAL USING CHEMICAL GROUP SEPARATIONS AND HIGH RESOLUTION GAMMA SPECTROMETRY, ANALYTICAL CHEMISTRY,

44 : 839-842.

72RAI 01 T. C. RAINS AND 0. MENIS ( 1972) DETERMINATION OF SUBMICROGRAM AMOUNTS OF MERCURY IN STANDARD REFERENCE MATERIALS BY FLAMELESS ATOMIC ABSORPTION

SPECTROMETRY, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 55: 1339-1344.

72ROO 01 H. L. ROOK, P. D. LAFLEUR, AND T. E. GILLS (1972) MERCURY IN COAL: A NEW STANDARD REFERENCE MATERIAL

ENVIRONMENTAL LETTERS, 2: 195-204.

72ROO 02 H. L. ROOK, T. E. GILLS, AND P. D. LAFLEUR (1972) METHOD FOR DETERMINATION OF MERCURY IN BIOLOGICAL MATERIALS

BY NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY,

44: 1114-1117.

72ROO 03 H. L. ROOK (1972) RAPID, QUANTITATIVE SEPARATION FOR THE DETERMINATION OF SELENIUM USING NEUTRON ACTIVATION, ANALYTICAL CHEMISTRY

44: 1276-1278.

72SAN 01 P. M. SANTOLIQUIDO AND R. R. RUCH (1972) RAPID RADIOCHEMICAL SEPARATION AND DETERMINATION OF GALLIUM

IN COAL ASH, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS,

12: 71-76.

72SEI 01 W. R. SEITZ AND D. M. HERCULES (1972) DETERMINATION OF TRACE AMOUNTS OF IRON(II) USING

CH EMI LUMINESCENCE ANALYSIS, ANALYTICAL CHEMISTRY,

44: 2143-2148.

72SIN 01 I. SINKO AND L. KOSTA (1972) DETERMINATION OF LEAD, CADMIUM, COPPER, AND ZINC IN BIOLOGICAL MATERIALS BY ANODIC STRIPPING POLAROGRAPHY

INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY,

2: 167-178.

73ABE 01 K. R. ABEL AND L. A. RANCITELLI (1973) MAJOR, MINOR, AND TRACE ELEMENT COMPOSITION OF COAL AND

FLY ASH, AS DETEIWINED BY INSTRUMENTAL NEUTRON ACTIVATION

ANALYSIS, IN 73BAB 01, PP. 118-138.

73BAB 01 S. P. BABU (EDITOR) (1973) TRACE ELEMENTS IN FUEL, ADVANCES IN CHEMISTRY SERIES 141, AMERICAN CHEMICAL SOCIETY, WASHINGTON, D.C.

73BES 01 Y. BESNUS AND R. ROUAULT (1973) UNE METHODE D' ANALYSE DES ROCHES AU SPECTROMETRE D'ARC A

LECTURE DIRECTE PAR UN DISPOSITIF D'ELECTRODE ROTATIVE, ANALUSIS, 2: 111-116.

73BLA 01 M. S. BLACK AND R. E. SIEVERS (1973) ENVIRONMENTAL ANALYSIS PROBLEMS CREATED BY UNEXPECTED

VOLATILE BERYLLIUM COMPOUNDS IN VARIOUS SAMPLES, ANALYTICAL CHEMISTRY, 45: 1773-1775.

73BLO 02 A. J. BLOTCKY, L. J. ARSENAULT, AND E. P. RACK (1973) OPTIMUM PROCEDURE FOR THE DETERMINATION OF SELENIUM IN BIOLOGICAL SPECIMENS USING SE-77M NEUTRON ACTIVATION, ANALYTICAL CHEMISTRY, 45: 1056-1060.

73CAR 01 J.A. CARTER, D.R. MATTHEWS, R.L. WALKER, J.R. WALTON (1973) MEASUREMENT OF NITROGEN AND NITROGEN ISOTOPIC RATIOS USING REDUCTION PYROLYSIS COUPLED WITH MASS SPECTROMETRY

ANALYTICAL LETTERS, 6: 951-960.

73COR 01 R. CORNELIS, A. SFEECKE AND J. HOSTE (1973) A MULTI-ELEMENT SERUM STANDARD FOR NEUTRON ACTIVATION

ANALYSIS, ANALYTICA CHIMICA ACTA, 68: 1-10.

73GIA 01 R. D. GIAUQUE, F. S. GOULDING , J. M. JAKLEVIC, AND

R. H. FEHL (1973), TRACE ELEMENT DETERMINATION WITH

SEMICONDUCTOR DETECTOR X-RAY SPECTROMETERS, ANALYTICAL CHEMISTRY, 45: 671-681.

73HEM 01 D.D. HEMPHILL (EDITOR) (19 73) PROCEEDINGS OF THE SEVENTH ANNUAL CONFERENCE ON TRACE SUBSTANCES IN ENVIRONMENTAL HEALTH, UNIVERSITY OF MISSOURI, COLUMBIA, MISSOURI.

73HEY 01 K. HEYDORN AND E. DAMSCAARD (1973) SIMULTANEOUS DETERMINATION OF ARSENIC, MANGANESE, AND

SELENIUM IN BIOLOGICAL MATERIALS BY NEUTRON-ACTIVATION

ANALYSIS, TALANTA, 20: 1-11.

73KAR 01 S. S. KARACKI AND F. L. CORCORAN { 1973) COAL ASH ANALYSIS WITH AN ARGON PLASMA EMISSION EXCITATION

SOURCE, APPLIED SPECTROSCOPY, 27: 41-4 2.

73LEB 01 P. J. LEBLANC AND A. L. JACKSON (1973)

DRY ASHING TECHNIQUE FOR THE DETERMINATION OF ARSENIC IN MARINE FISH, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 56 : 383-38 6.

73LO 01 F.-C. 10 AND B. BUSH (1973) MODIFIED PROCEDURE FOR DETERMINING HG IN COAL BY COLD VAPOR

ATOMIC ABSORPTION SPECTROPHOTOMETRY, JOURNAL OF THE ASSOCIA- TION OF OFFICIAL ANALYTICAL CHEMISTS, 56: 1509-1510.

73LOO 01 J. C. VAN LOON, J. LICHUA, AND D. RUTTAN ( 1973) A STUDY OF THE DETERMINATION AND DISTRIBUTION OF CADMIUM IN

SAMPLES COLLECTED IN A HEAVILY INDUSTRIALIZED AND URBANIZED

REGION (METROPOLITAN TORONTO), INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 3: 147-160.

73L00 03 J. C. VAN LOON AND J. LICHWA (1973) A STUDY OF THE ATOMIC ABSORPTION DETERMINATION OF SOME IMPORTANT HEAVY METALS IN FERTILIZERS AND DOMESTIC SEWAGE PLANT SLUDGES, ENVIRONMENTAL LETTERS, 4: 1-8.

7 3NAD 01 R. A. NADKARNI AND G. H. MORRISON (1973) MULTIELEMENT INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF BIOLXICAL MATERIALS, ANALYTICAL CHEMISTRY, 4 5: 1957-1960.

73PIE 01 J. 0. PIERCE, A. ABU-SAHRA, D. FEHLAUER, T. CLEVENGER, AND

J. VOGT (1973), IN TRACE ELEMENTS IN RELATION TO CARDIOVASCULAR DISEASES, IAEA, VIENNA, P. 103, FROM REF 80HEY 01

73RAM 01 E. R. RAMBALDI (1973) VARIATION IN THE COMPOSITION OF PLAGIOCLASE AND EPIDOTE IN

SOME METAMORPHIC ROCKS NEAR BANCROFT, ONTARIO, CANADIAN JOURNAL OF EARTH SCIENCES, 10: 852-868.

73SEG 01 D. A. SEGAR AND J. L. GILIO (1973) THE DETERMINATION OF TRACE TRANSITION ELEMENTS IN BIOLOGICAL

TISSUES USING FLAMELESS ATOM RESERVOIR ATOMIC ABSORPTION, INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY,

2: 291-301.

73SHA 01 L. SHAPIRO (1973) RAPID DETERMINATION OF SULFUR IN ROCKS, JOURNAL OF RESEARCH

OF THE U. S. GEOLOGICAL SURVEY, 1: 81-64.

73SHE 01 D. W. SHEIBLEY (1973) TRACE ELEMENTS IN INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS

FOR POLLUTION MONITORING, IN 73BAB 01, PP. 98-117.

73SPA 01 C. J. SPARKS , JR. , O.B. CAVIN, L.A. HARRIS, J.C. OGLE (1973)

SIMPLE, QUANTITATIVE X-RAY FLUORESCENT ANALYSIS FOR TRACE ELEMENTS, PP. 361-368, IN 73HEM 01.

197
00 DC H ASCRIPTION

core n DESCRIPTION

73STE 01 E. STEINNES (1973) IN TRACE ELEMENTS IN RELATION TO CARDIOVASCULAR DISEASES, IAEA TECHNICAL REPORT 157, VIENNA, P. 149; FROM 78BYR 01.

73TAL 01 Y. TALMI AND R. CROSMUN (1973) APPLICABILITY OF THE RF-FUKNACE TECHNIQUE FOR AA AND AE ANALYSES OF TRACE ELEMENTS IN ENVIRONMENTAL SAMPLES,

PP. 379-383, IN 73HEM 01.

73TH0 01 A. D. THOMAS AND L. E. SMYTHE ( 1973) RAPID DESTRUCTION OF PLANT MATERIAL WITH CONCENTRATED

NITRIC ACID VAPOUR (VAPOUR PHASE OXIDATION), TALANTA,

20: 469-475.

73TJI 01 P. S. TJIOE, J. J. M. DE GOEIJ, AND J. P. W. HOUTMAN ( 1973) AUTOMATED CHEMICAL SEPARATIONS IN ROUTINE ACTIVATION

ANALYSIS , JOURNAL OF RAD IOANALYTI CAL CHEMISTRY, 16: 153-164.

74ALV 01 R. ALVAREZ (19 74) SUB-MICROGRAM PER GRAM CONCENTRATIONS OF MERCURY IN ORCHARD

LEAVES DETERMINED BY ISOTOPE DILUTION AND SPARK- SOURCE MASS

SPECTROMETRY, ANALYTICA CHIMICA ACTA, 73: 33-38.

7 4 AND 01 L. W. ANDERSON AND L. ACS (1974) SELENIUM IN NORTH AMERICAN PAPER PULPS , ENVIRONMENTAL

SCIENCE AND TECHNOLOGY, 8: 462-464.

74BEC 01 R.R. BECKER, A. VEGLIA, E.R. SCHMID (1974) INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF STANDARD

BIOLOGICAL MATERIALS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 19: 34 3-354.

74BER 01 J. BERGHOLZ, J. LUCK, P. HOLLER, AND VI. SZACKI ( 1974) PUNKENQUELLEN-MASSENSPEKTROMETRI SCHE ANALYSE DES NBS-SRM 610 (3 MM) STANDARDS, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 269: 121.

74B0P 01 B. BOPPEL (19 74) BLEIGEHALTE VON LEBENSMITTELN. ZUR ANALYTIK DER BLEIBESTIMMUNG IN LEBENSMITTELN, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 268: 114-119.

74BRA 03 D. V. BRADY, J. G. MONTALVO, J. JUNG, AND R. CURRAN ( 19 74 ) DIRECT DETERMINATION OF LEAD IN PLANT LEAVES VIA GRAPHITE

FURNACE ATOMIC ABSORPTION, ATOMIC ABSORPTION NEWSLETTER,

13: 118-119.

74 BUS 02 K. W. BUSCH, N. C. HOWELL, AND G. H. MORRISON (1974) ELIMINATION OF INTERFERENCES IN FLAME SPECTROMETRY USING SPECTRAL STRIPPING, ANALYTICAL CHEMISTRY, 46: 2074-2079.

74BYR 01 A. R. BYRNE (1974) NEUTRON ACTIVATION ANALYSIS OF TIN IN BIOLOGICAL MATERIALS

AND THEIR ASH USING SN-123 AND SN-125, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 20: 627-637.

74BYR 02 F. P. BYRNE ( 1974) THE ANALYST AND ACCURACY, IN 74LAF 01, PP. 123-125.

74BYR 03 A. R. BYRNE AND L. KOSTA (1974) SIMULTANEOUS NEUTRON-ACTIVATION DETERMINATION OF SELENIUM AND MERCURY IN BIOLOGICAL SAMPLES BY VOLATILIZATION,

TALANTA, 21: 1083-1090.

74CAR 01 B. S. CARPENTER AND P. D. LAFLEUR (1974) NITROGEN DETERMINATION IN BIOLOGICAL MATERIALS BY THE NUCLEAR TRACK TECHNIQUE, ANALYTICAL CHEMISTRY,

46: 1112-1113.

74 CAR 02 B. S. CARPENTER ( 19 74) LITHIUM DETERMINATIONS BY THE NUCLEAR TRACK TECHNIQUE, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 19: 233-234.

74 CAR 03 V. CARAMELLA-CRESPI, U. PISANI, M. T. GANZERLI-VALENTINI

S. MELONI , AND V. MAXIA (1974), DETERMINATION OF SOME NOBLE METALS AND COPPER BY DESTRUCTIVE NEUTRON ACTIVATION ANALYSIS

OF DIFFERENT MATRICES, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

23: 23-31.

74CAR 05 B. S. CARPENTER AND G. M. REIMER (1974) HOMOGENEITY CONSIDERATIONS IN TRACE ANALYSES USING THE NUCLEAR TRACK TECHNIQUE, IN 74LAF 01, PP. 457-4 59.

74CHA 01 A. CHATTOPADHYAY AND R. E. JERVIS ( 19 74) MULTIELEMENT DETERMINATION IN MARKET-GARDEN SOILS BY INSTRUMENTAL PHOTON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY, 46: 1630-1639.

74CHO 02 T. J. CHOW , C. C. PATTERSON, D. SETTLE ( 19 74) OCCURRENCE OF LEAD IN TUNA, NATURE, 251: 159-161.

74CHU 01 M. R. CHURCH AND W. H. ROBISON (19 74 ) A RAPID, ROUTINE ATOMIC ABSORPTION SPECTROMETRY METHOD FOR THE DETERMINATION OF SELENIUM AT SUB-MICROGRAM LEVELS IN ANIMAL TISSUE, INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 3: 323-331.

74CHU 03 D. A. CHURCH, T. HADEISHI , L. LEONG, R. D. MCLAUGHLIN, AND

B. D. ZAK (1974), TWO-CHAMBER FURNACE FOR FLAMELESS ATOMIC ABSORPTION SPECTROMETRY, ANALYTICAL CHEMISTRY

46: 1352-1355.

74COP 01 T. R. COPELAND, R. A. OYSTERYOUNG , AND R. K. SKOGERBOE (1974 ELIMINATION OF COPPER-ZINC INTERMETALLIC INTERFERENCES IN ANODIC STRIPPING VOLTAMMETRY, ANALYTICAL CHEMISTRY,

46: 2093-2097.

74COR 01 R. F. CORMIER ( 19 74) RADIOMETRIC AGE OF THE KEPPOCH FORMATION, BROWNS MOUNTAIN

GROUP, NORTHERN MAINLAND OF NOVA SCOTIA, CANADIAN JOURNAL

OF EARTH SCIENCES, 11: 1325-1329.

74CRE 01 G. L. CRENSHAW AND R. W. LAKIN ( 1974) A SENSITIVE AND RAPID METHOD FOR THE DETERMINATION OF TRACE AMOUNTS OF SELENIUM IN GEOLOGICAL MATERIALS, JOURNAL OF RESEARCH OF THE U. S. GEOLOGICAL SURVEY, 2: 483-487.

74DAU 01 E.H. DAUGHTREY, JR. AND W.W. HARRISON (1974) ANALYSIS FOR TRACE LEVELS OF BORON BY ION-EXCHANGE-HOLLOW

CATHODE EMISSION, ANALYTICA CHIMICA ACTA, 72: 225-230.

74DON 01 I. Y. DONEV AND L. M. MARICHKOVA (1974) DETERMINATION OF ELEMENTS IN STANDARD MATERIAL (BOVINE LIVER

SRM 1577), IN 74LAF 01, PP. 1293-130 3.

74ERD 01 G. ERDTMANN AND 0. ABOULWAFA (1974) SELECTIVE CHEMICAL SEPARATION PROCEDURES FOR ACTIVATION

ANALYSIS: II. SEPARATION OF ARSENIC BY COLUMN EXTRACTION WITH TINUDETHYLXANTHATE. DETERMINATION IN TITANIUM

DIOXIDE OF HIGH ANTIMONY CONTENT AND IN BIOLOGICAL MATERIAL, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 272: 105-114.

74FEL 01 C. FELDMAN (1974) PERCHLORIC ACID PROCEDURE FOR WET-ASHING ORGANICS FOR THE DETERMINATION OF MERCURY (AND OTHER METALS), ANALYTICAL CHEMISTRY, 46: 1606-1609.

74FIT 01 W. F. FITZGERALD, W. B. LYONS, AND C. D. HUNT ( 19 74) COLD-TRAP PRECONCENTRATION METHOD FOR THE DETERMINATION OF MERCURY IN SEA WATER AND IN OTHER NATURAL MATERIALS, ANALYTICAL CHEMISTRY, 46: 1882-1885.

74FLO 01 T. M. FLORENCE, Y. J. FARRAR, L. DALE, AND G. BATLEY (19 74) BERYLLIUM CONTENT OF NBS STANDARD REFERENCE ORCHARD LEAVES, ANALYTICAL CHEMISTRY, 46: 1874-1876.

74FRI 01 M. H. FRIEDMAN, E. MILLER, J. T. TANNER (1974) INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS FOR MERCURY IN DOGS ADMINISTERED METHYLME RCURY CHLORIDE: USE OF A LOW ENERGY

PHOTON DETECTOR, ANALYTICAL CHEMISTRY, 46: 236-239.

74 GAL 01 M. GALLORINI AND E. ORVINI (1974) DETERMINATION OF ZINC IN ENVIRONMENTAL MATRICES: A

COMPARISON OF RESULTS OBTAINED BY INDEPENDENT METHODS, IN 74LAF 01, PP. 239-245.

74GOE 01 J.J.M. DE GOEIJ, V.P. GUINN, D.R. YOUNG, A.J. MEARNS (1974) NEUTRON ACTIVATION ANALYSIS TRACE-ELEMENT STUDIES OF DOVER

SOLE LIVER AND MARINE SEDIMENTS, IN COMPARATIVE STUDIES OF FOOD AND ENVIRONMENTAL CONTAMINATION, PROCEEDINGS SERIES,

IAEA, VIENNA, 1974, PP. 193-196.

74GRO 01 S. B. GROSS AND E. S. PARKINSON (1974) ANALYSES OF METALS IN HUMAN TISSUES USING BASE (TMAH) DIGESTS AND GRAPHITE FURNACE ATOMIC ABSORPTION

SPECTROPHOTOMETRY, ATOMIC ABSORPTION NEWSLETTER, 13: 107-108.

198
CODE N DESCRIPTION

CODE N DESCRIPTION

74GUI 01 V. P. GUINN, R. KISHORE (1974) RESULTS FROM MULTI-TRACE-ELEMENT NEUTRON ACTIVATION ANALYSES

OF MARINE BIOLOGICAL SPECIMENS, JOURNAL OF RAD10ANALYTICAL

CHEMISTRY, 19 : 367-371.

74 HEM 01 D.D. HEMPHILL (EDITOR) (1974) PROCEEDINGS OF THE EIGHTH ANNUAL CONFERENCE ON TRACE SUB- STANCES IN ENVIRONMENTAL HEALTH, UNIVERSITY OF MISSOURI,

COLUMBIA, MISSOURI.

74 HEN 01 T. E. HENZLER, R. J. KORDA, P. A. HELMKE, M. R. ANDERSON,

M. M. JIMENEZ, AND L. A. RASKIN (19 74), AN ACCURATE PROCEDURE FOR MULTIELEMENT NEUTRON ACTIVATION ANALYSIS OF TRACE ELEMENTS IN BIOLOGICAL MATERIALS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 20 : 649-6 63.

74HEY 01 K. HEYDORN (1974) DETECTION OF SYSTEMATIC ERRORS BY THE ANALYSIS OF PRECISION, IN 74LAF 01, PP. 127-134.

74HIC 01 J. E. HICKS, J. E. FLEENOR AND H. SMITH (1974) THE RAPID DETERMINATION OF SULFUR IN COAL, ANALYTICA CHIMICA

ACTA, 68: 480-483.

74HOF 01 G. L. HOFFMAN, P. R. WALSH, AND M. P. DOYLE (19 74) DETERMINATION OF A GEOMETRY AND DEAD TIME CORRECTION FACTOR

FOR NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY,

46: 492-496.

74IHN 01 M. IHNAT AND R. J. WESTERBY (1974) APPLICATION OF FLAMELESS ATOMIZATION TO THE ATOMIC ABSORPTION DETERMINATION OF SELENIUM IN BIOLOGICAL SAMPLES, ANALYTICAL LETTERS, 7: 257-265.

74 LAP 01 P. D. LAFLEUR (EDITOR) (19 74) ACCURACY IN TRACE ANALYSIS: SAMPLING , SAMPLE HANDLING , AND

ANALYSIS, PROCEEDINGS OF THE SEVENTH IMR SYMPOSIUM, NATIONAL

BUREAU OF STANDARDS SPECIAL PUBLICATION 4 22.

74LEI 01 0. W. LEISURE AND 0. E. OLSON (1974) USE OF THE AOAC FLUOROMETRIC METHOD FOR SELENIUM IN PLANTS

FOR THE ANALYSIS OF PAPERS AND TOBACCOS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 57: 658-661.

74LI 01 R. T. LI AND D. M. HERCULES (1974) DETERMINATION OF CHROMIUM IN BIOLOGICAL SAMPLES USING

CH EMI LUMINESCENCE, ANALYTICAL CHEMISTRY, 46: 916-919.

74LIN 01 R. VAN DER LINDEN, F. DE CORTE, AND J. HOSTE (19 74) ACTIVATION ANALYSIS OF BIOLOCICAL MATERIAL WITH RUTHENIUM

AS A MULTI-ISOTOPIC COMPARATOR, ANALYTICA CHIMICA ACTA,

71 : 263-275.

74LO0 01 J. C. VAN LOON AND E. J. BROOKER (1974) A SIMPLIFIED METHOD FOR DETERMINING ARSENIC AND ANTIMONY BY THE HYDRIDE EVOLUTION-ATOMIC ABSORPTION METHOD, ANALYTICAL LETTERS, 7: 505-513.

74LUT 01 G. J. LUTZ (1974) THE ANALYSIS OF BIOLOGICAL AND ENVIRONMENTAL SAMPLES FOR LEAD BY PHOTON ACTIVATION, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 19 : 239-244.

74MAI 01 E. J. MAIENTHAL (1974) THE APPLICATION OF LINEAR SWEEP VOLTAMMETRY TO THE DETERMIN- ATION OF TRACE ELEMENTS IN BIOLOGICAL AND ENVIRONMENTAL

MATERIALS, PP. 24 3-246, IN 74 HEM 01.

74MAS 01 R. MASIRONI (1974) TRACE ELEMENTS IN RELATION TO CARDIOVASCULAR DISEASES, WHO

STATUS REPORT, WHO OFFSET PUBLICATION NO. 5.

74MCC 01 L. T. MCCLENDON (1974) SELECTIVE DETERMINATION OF CHROMIUM IN BIOLOGICAL AND

ENVIRONMENTAL MATRICES, PP. 255-257, IN 74 HEM 01.

74M00 01 L. J. MOORE, L. A. MACHIAN, W. R. SHIELDS, AND E. L. GARNER

(1974), INTERNAL NORMALIZATION TECHNIQUES FOR HIGH ACCURACY

ISOTOPE DILUTION ANALYSES - APPLICATION TO MOLYBDENUM AND

NICKEL IN STANDARD REFERENCE MATERIALS, ANALYTICAL CHEMISTRY 46: 1082-1089.

74NAD 02 R. A. NADKARNI ( 1974) RE-EVALUATION OF ARSENIC CONCENTRATION IN THE BIOLOGICAL

STANDARDS, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS,

19 : 127-134 .

740ND 01 J. M. ONDOV, W. H. ZOLLER, I. OLMEZ, N. K. ARAS, G. GORDON,

L. A. RANCITELLI, K. H. ABEL, R. H. FILBY, K. R. SHAH, AND

R. C. RAGAINI ( 19 74), FOUR- LABORATORY COMPARATIVE

INSTRUMENTAL NUCLEAR ANALYSIS OF THE NBS COAL AND FLY ASH

STANDARD REFERENCE MATERIALS, IN 74LAF 01, PP. 211-218.

740RV 01 E. ORVINI, T. E. GILLS, AND P. D. LAFLEUR ( 19 74 ) METHOD FOR DETERMINATION OF SELENIUM, ARSENIC, ZINC, CADMIUM, AND MERCURY IN ENVIRONMENTAL MATRICES BY NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY, 46: 1294-1297.

74RAI 01 T. C. RAINS AND 0. MENIS ( 19 74) AN INTERCOMPARISON OF FLAME AND NONFLAME SYSTEMS IN ATOMIC ABSORPTION SPECTROMETRY, IN 74LAF 01, PP. 1045-1051.

74RAI 02 T. C. RAINS, M. S. EPSTEIN, AND 0. MENIS ( 19 74) AUTOMATIC CORRECTION SYSTEM FOR LIGHT SCATTER IN ATOMIC

FLUORESCENCE SPECTROMETRY , ANALYTICAL CHEMISTRY,

46: 207-210.

74RAN 02 L.A. RANCITELLI, J.A. COOPER, R.W. PERKINS ( 19 74) MULTI-ELEMENT CHARACTERIZATION OF ATMOSPHERIC AEROSOLS BY NEUTRON ACTIVATION AND DIRECT GAMMA-RAY ANALYSIS , AND X-RAY

FLUORESCENCE ANALYSIS, IN COMPARATIVE STUDIES OF FOOD AND

ENVIRONMENTAL CONTAMINATION, PROCEEDINGS SERIES, IAEA, VIENNA, 1974 , PP. 440-444.

74RAV 01 V. RAVNTK, M. DERMELJ , AND L. KOSTA (1974) A HIGHLY SELECTIVE DIETHYLDITHIOCARBAMATE EXTRACTION SYSTEM IN ACTIVATION ANALYSIS OF COPPER, INDIUM, MANGANESE, AND

ZINC: APPLICATION TO THE ANALYSIS OF STANDARD REFERENCE

MATERIALS, JOURNAL OF RADIOANALYTICAL CHEMISTRY

20: 44 3-4 53.

74REU 01 F. W. REUTER AND W. L. RAYNOLDS ( 1974) TITLE UNKNOWN, IN PROTEIN-METAL INTERACTIONS, M. FRIEDMAN,

EDITOR, PLENUM PRESS, NEW YORK, P. 621; TAKEN FROM 78DAH 01.

74RIC 01 E. RICCI, T. H. HANDLEY, AND F. F. DYER ( 1974) ANALYSIS OR TRACES AT ORNL'S NEW HIGH-FLUX NEUTRON

ACTIVATION LABORATORY , JOURNAL OF RADIOANALYTICAL CHEMISTRY,

19: 141-148.

74ROO 01 H.L. ROOK, P.D. LA FLEUR, J.E. SU DDUETH ( 1974 ) TRACE ELEMENT DETERMINATION USING A HIGH YIELD ELECTROMAGNETIC ISOTOPE SEPARATOR AND NEUTRON ACTIVATION-THE DETERMINATION OF CADMIUM, NUCLEAR INSTRUMENTS AND METHODS, 116: 579-586.

74ROS 02 K. J. R. ROSMAN AND J. R. DE LAETER ( 19 74) MASS SPECTROMETRIC ISOTOPE DILUTION ANALYSES OF CADMIUM IN STANDARD ROCKS , CHEMICAL GEOLOGY, 13: 69-74 .

74RUN 01 L.M. RUNDLE ( 19 74) A COMBUSTION METHOD FOR THE DETERMINATION OF TOTAL SULPHUR

IN LIMESTONES, ANALYST, 99: 163-165.

74SCH 03 R. SCHELENZ AND J.-F. DIEHL (19 74) A STUDY INTO THE ACCURACY OF A REMOTE-CONTROLLED SYSTEM FOR MULTIELEMENT DETERMINATION IN FOODSTUFFS USING NAA, IN 74LAF 01, PP. 1173-1180.

74SHA 01 L. SHAPIRO (1974) SPECTROPHOTOMETRIC DETERMINATION OF SILICA AT HIGH CONCENTRATIONS USING FLUORIDE AS A DEPOLYMERIZER, JOURNAL OF RESEARCH OF THE U.S. GEOLOGICAL SURVEY, 2: 357.

74SIE 02 D. SIEMER AND R. WOODRIFF (19 74 ) APPLICATION OF THE CARBON ROD ATOMIZER TO THE DETERMINATION

OF MERCURY IN THE GASEOUS PRODUCTS OF OXYGEN COMBUSTION OF SOLID SAMPLES, ANALYTICAL CHEMISTRY, 46: 597-598.

74SLE 01 G. SLEGERS AND A. CLAEYS (19 74) SPECTROPHOTOMETRIC DETERMINATION OF MAGNESIUM IN TOBACCO LEAVES WITH ERIOCHROME BLACK B, ANALYST, 99: 471-475.

74TAL 02 Y. TALMI AND A. W. ANDREN (1974) DETERMINATION OF SELENIUM IN ENVIRONMENTAL SAMPLES USING GAS CHROMATOGRAPHY WITH A MICROWAVE EMISSION SPECTROMETRIC DETECTION SYSTEM, ANALYTICAL CHEMISTRY, 46: 2122-2126.

199
CODE N INSCRIPTION

CODE N DESCRIPTION 74TAM 01 N. TAMURA (1974) ACCURACY IN THE NONDESTRUCTIVE NEUTRON ACTIVATION ANALYSIS

OF COAL AND BERYLLIUM FOR MINOR AND TRACE ELEMENTS USING COBALT AS A FLUX DETERMINANT, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 18: 135-14 2.

74THO 01 J. THOMAS AND H. J. GLUSKOTER ( 19 74) DETERMINATION OF FLUORIDE IN COAL WITH THE FLUORIDE ION-SELECTIVE ELECTRODE, ANALYTICAL CHEMISTRY

,

46! 1321-1323.

74ULL 01 P. A. OLLUCCI AND J. Y. HWANG (1974) DETERMINATION OF CADMIUM IN BIOLOGICAL MATERIALS BY ATOMIC ABSORPTION, TALANTA, 21: 745-750.

74WAH 01 J. S. WAHLBERG (1974) UNPUBLISHED DATA; QUOTED IN 74CRE 01.

74VEA 01 J. N. WEAVER (19 74) RAPID, INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS FOR THE

DETERMINATION OF URANIUM IN ENVIRONMENTAL MATRICES, ANALYTICAL CHEMISTRY, 46: 1292-1294.

74WES 01 H. WESCH AND A. BINDL (1974) ANALYSIS OF 11 ELEMENTS IN BIOLOGICAL MATERIAL: COMPARISON

OF NEUTRON ACTIVATION ANALYSIS AND ATOMIC ABSORPTION

ANALYSIS, IN 74LAF 01, PP. 231-235.

74WOL 01 W. R. WOLF AND F. E. GREENE ( 19 74) PREPARATION OF BIOLOGICAL MATERIALS FOR CHROMIUM ANALYSIS,

IN 74LAF 01, PP. 605-610.

75ABU 01 A. ABU-SAMA, J. S. MORRIS, AND S. R. KOIRTYOHANN ( 1975) WET ASHING OF SOME BIOLOGICAL SAMPLES IN A MICROWAVE OVEN

,

ANALYTICAL CHEMISTRY, 47: 1475-1477.

75AND01 R. W. ANDREWS AND D. C. JOHNSON (1975) VOLTAMMETRIC DEPOSITION AND STRIPPING OF SELENIUM(IV) AT A ROTATING GOLD-DISK ELECTRODE IN 0.1 M PERCHLORIC ACID, ANALYTICAL CHEMISTRY, 47: 294-299.

75BEH 01 D. BEHNE, P. BRATTER, AND W. WOLTERS (1975) BESTIMMUNC VON BLEI IN BIOLOGISCHEN MATERIAL IEN MIT HILFE DER FLAMMENLOSEN ATOMABSORPTIONSSPEKTROMETRIE, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 277: 355-358.

75BLO 01 E. R. BLOOD AND G. C. GRANT (1975) DETERMINATION OF CADMIUM IN FISH TISSUE BY FLAMELESS ATOMIC ABSORPTION WITH A TANTALUM RIBBON, ANALYTICAL CHEMISTRY

,

47: 1438-1441.

75BOL 01 B. A. BOLTON AND P. K. HOPKE ( 1975) THE USE OF INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS FOR THE DETERMINATION OF ARSENIC CONCENTRATIONS IN POULTRY, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 25: 299-302.

75BOL 02 H. J. BOLLINGBERG (1975) GEOCHEMICAL PROSPECTING USING SEAWEED, SHELLFISH AND FISH, GEOCHIMICA ET COSMOCHIMICA ACTA, 39: 1567-1570.

75CAM 01 J. L. CAMPBELL, B. H. ORR, A. W. HERMAN, L. A. MCNELLES,

J. A. THOMPSON, AND W. B. COOK (1975), TRACE ELEMENT

ANALYSIS OF FLUIDS BY PROTON-INDUCED X-RAY FLUORESCENCE

SPECTROMETRY , ANALYTICAL CHEMISTRY, 47: 1542-1553.

75EPS 01 M. S. EPSTEIN, T. C. RAINS AND 0. MENIS (1975) DETERMINATION OF CADMIUM AND ZINC IN STANDARD REFERENCE MATERIALS BY ATOMIC FLUORESCENCE SPECTROMETRY WITH AUTOMATIC

SCATTER CORRECTION, CANADIAN JOURNAL OF SPECTROSCOPY,

20: 22-26.

75GLA 01 E. S. GLADNEY AND H. L. ROOK (1975) SIMULTANEOUS DETERMINATION OF TELLURIUM AND URANIUM BY

NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY,

47: 1554-1557.

75GUI 01 V. P. GUINN, M. A. PURCELL, AND W. W. WADMAN (1975) INTERNATIONAL SYMPOSIUM ON DEVELOPMENT OP NUCLEAR BASED TECHNIQUES FOR MEASUREMENT, DETECTION, AND CONTROL OF ENVIRONMENTAL POLLUTANTS, VIENNA, IAEA-SM-206, PAPER 30.

7 SHAG 01 L. HACEMAN, L. TORMA AND B. GINTHER (1975) ANALYSIS OF FEED GRAINS AND FORAGES FOR TRACES OF COBALT BY FLAMELESS ATOMIC ABSORPTION SPECTROSCOPY, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 58: 990-994 .

7 5HAL 01 C. HALVORSEN AND E. 8TEINNES (1975) SIMPLE AND PRECISE DETERMINATION OF ZN AND CD IN HUMAN LIVER

BY NEUTRON ACTIVAIION ANALYSIS, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 274: 199-202.

75HEI 01 H. HEIHRICHS (1975) DETERMINATION OF MERCURY IN WATER, ROCKS, COAL, AND

PETROLEUM WITH FLAMELESS ATOMIC ABSORPTION SPECTROPHOTOMETRY

ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 273: 197-201.

75HIN 01 T. A. HINNERS (1975) ATOMIC ABSORPTION ANALYSIS OF LIVER WITHOUT ASHING, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 277: 377-378.

75ISA 01 R. A. ISAAC AND W. C. JOHNSON (1975) COLLABORATIVE STUDY OF WET AND DRY ASHING TECHNIQUES FOR THE

ELEMENTAL ANALYSIS OF PLANT TISSUE BY ATOMIC ABSORPTION

SPECTROPHOTOMETRY, JOURNAL OF THE ASSOCIATION OF OFFICIAL

ANALYTICAL CHEMISTS, 58: 4 36-440.

7 5JON 01 J. B. JONES (1975) COLLABORATIVE STUDY OF THE ELEMENTAL ANALYSIS OF PLANT

TISSUE BY DIRECT READING EMISSION SPECROSCOPY, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 58: 764-769 LABORATORY 1.

7 5JON 02 IBID., LABORATORY 2.

7 5JON 03 IBID., LABORATORY 3.

7 5JON 04 IBID., LABORATORY 4.

7 5JON 05 IBID., LABORATORY 5.

7 5JON 06 IBID., LABORATORY 6.

75JON 07 IBID., LABORATORY 7.

7 5JON 08 IBID., LABORATORY 8.

7 5JON 09 IBID., LABORATORY 9.

75JON 10 IBID., LABORATORY 10.

7 5JON 11 IBID., LABORATORY 11.

75KLE 01 D. H. KLEIN, A. W. ANDREN, J. A. CARTER, J. F. EMERY,

C. FELDMAN, W. FULKERSON, W. S. LYON, J. C. OGLE, Y. TALMI

,

R. I. VAN HOOK, AND N. BOLTON (1975) PATHWAYS OF THIRTY-SEVEN TRACE ELEMENTS THROUGH COAL-FIRED POWER PLANT, ENVIRONMNETAL SCIENCE AND TECHNOLOGY,

9: 973-978.

75KOI 01 H. KOIZUMI AND K. YASUDA (1975) NEW ZEEMAN METHOD FOR ATOMIC ABSORPTION SPECTROPHOTOMETRY, ANALYTICAL CHEMISTRY, 47: 1679-1682.

75LIE 01 P. LIEVENS, R. CORNELIS, AND J. HOSTE ( 1975) A SEPARATION SCHEME FOR THE DETERMINATION OF TRACE ELEMENTS

IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS, ANALYTICA CHIMICA ACTA, 80: 97-108.

75LIT 01 R. LITMAN, H. L. FINSTON, AND E. T. WILLIAMS (1975) EVALUATION OF SAMPLE PRETREATMENTS FOR MERCURY DETERMINATION ANALYTICAL CHEMISTRY, 47: 2364-2369.

75MAN 01 D. C. MANNING (1975) ASPIRATING SMALL VOLUME SAMPLES IN FLAME ATOMIC ABSORPTION

SPECTROSCOPY, ATOMIC ABSORPTION NEWSLETTER, 14: 99-102.

75MAZ 01 B. MAZIERE, J. GROS, AND D. COMAR (1975) POSSIB1LITES ET LIMITES DE L ' ANALYSE D'ECHANTILLONS BIOLOGIQUES PAR ACTIVATION NEUTRONIQUE DERRIERE ECRAN DE CADMIUM, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 24 : 27 9-29 3.

75MCG 01 J. R. MCGINLEY AND E. A. SCHWEIKERT (1975) DETERMINATION OF LITHIUM, BORON, AND CARBON BY QUASI-PROMPT CHARGED PARTICLE ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY,

47: 2403-2407.

200
CODE N DESCRIPTION CODE N DESCRIPTION

75MIL 01 H. T. MILLARD AND V. W. SWANSON (1975) NEUTRON ACTIVATION ANALYSIS OF COALS USING INSTRUMENTAL

TECHNIQUES, TRANSACTIONS OF THE AMERICAN NUCLEAR SOCIETY,

21: 108-109.

7 5MUR 01 J. MURPHY ( 1975) DETERMINATION OF MERCURY IN COALS BY PEROXIDE DICESTION AND COLD VAPOR ATOMIC ABSORPTION SPECTROPHOTOMETRY

ATOMIC ABSORPTION NEWSLETTER, 14: 151-152.

7 5NAD 02 R. A. NADRARNI ( 19 75) MULTIELEMENT ANALYSIS OF COAL AND COAL FLY ASH STANDARDS BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND

RADIOANALYTICAL LETTERS, 21: 161-176.

750LS 01 0. E. OLSON, I. S. PALMER, AND E. E. CARY (1975) MODIFICATION OF THE OFFICIAL FLUOROMETRIC METHOD FOR

SELENIUM IN PLANTS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 58: 117-121.

75OND01 J. M. ONDOV, W. H. ZOLLER, I. OLMEZ, N. K. ARAS,

G. E. GORDON, L. A. RANCITELLI , K. H. ABEL, R. H. FILBY,

K. R. SHAH, AND R. C. RAGAINI (1975) ELEMENTAL CONCENTRATIONS IN THE NATIONAL BUREAU OF STANDARDS ENVIRONMENTAL COAL AND FLY ASH STANDARD REFERENCE MATERIALS, ANALYTICAL CHEMISTRY, 47: 1102-1109.

750WE 01 J. W. OWENS AND E. S. GLADNEY ( 1975) DETERMINATION OF BERYLLIUM IN ENVIRONMENTAL MATERIALS BY FLAMELESS ATOMIC ABSORPTION SPECTROSCOPY, ATOMIC ABSORPTION

NEWSLETTER, 14 : 76-77.

7 5PEC 01 E. S. PECK ( 1975) SPECTROGRAPHIC DETERMINATION OF MERCURY IN ROCKS AND COAL

ANALYTICA CHIMICA ACTA, 80: 75-83.

75PIC 01 C. J. PICKFORD AND G. ROSSI ( 1975) DETERMINATION OF SOME TRACE ELEMENTS IN NBS (SRM-1577) BOVINE LIVER USING FLAMELESS ATOMIC ABSORPTION AND SOLID

SAMPLING, ATOMIC ABSORPTION NEWSLETTER, 14: 78-80.

75PIE 01 R. PIETRA, E. SABBIONI AND F . GIRARD1 (1975) DETERMINATION OF CA, MG, NI AND SI IN BIOLOGICAL MATERIALS

BY NEUTRON ACTIVATION AND CERENKOV COUNTING , RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 22: 24 3-250.

75PUF 01 J. H. PUFFER AND R. S. COHEN ( 1975) FIELD DETERMINATION OF SODIUM AND POTASSIUM IN FELDSPARS BY ION-SELECTIVE ELECTRODES, CHEMICAL GEOLOCY, 15: 217-222.

75REU 01 F. W. REUTER III ( 1975) NUMERICAL MATRIX CORRECTION TECHNIQUE FOR THE MEASUREMENT OF TRACE ELEMENTS IN PLANT MATERIALS BY X-RAY FLUORESCENCE

SPECTROMETRY, ANALYTICAL CHEMISTRY, 47 : 1763-1766.

75RIC 01 E. RICCI ( 1975) METHODOLOGY FOR HIGH-FLUX ABSOLUTE MULTIELEMENT NEUTRON ACTIVATION ANALYSIS-ENVIRONMENTAL BASELINES BY ANALYSIS OF TREE RINGS , ANALYTICA CHIMICA ACTA, 79: 109-124.

75RUC 01 R. R. RUCH, R. A. CAHILL, J. K. FROST, L. R. CAMP AND

H. J. GLUSKOTER ( 1975), TRACE ELEMENTS IN COALS OF THE UNITED STATES DETERMINED BY ACTIVATION ANALYSIS AND OTHER

TECHNIQUES, TRANSACTIONS OF THE AMERICAN NUCLEAR SOCIETY,

21: 107-108.

75SIE 01 D. D. SIEMER AND L. HAGEMANN ( 1975) AN IMPROVED HYDRIDE GENERATION-ATOMIC ABSORPTION APPARATUS

FOR SELENIUM DETERMINATION, ANALYTICAL LETTERS , 8 : 3 2 3- 3 37.

7 5 SLA 01 S. SLAVIN, G. E. PETERSON, AND P. C. LINDAHL ( 1975) DETERMINATION OF HEAVY METALS IN MEATS BY ATOMIC ABSORPTION

SPECTROSCOPY, ATOMIC ABSORPTION NEWSLETTER, 14: 57-59.

75SME 01 J. SMEYERS-VEBEDE, G. SEGEBARTH, AND D. L. MASSART (1975) THE DETERMINATION OF COPPER AND MANGANESE IN SMALL BIOLOGICAL SAMPLES WITH GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY, ATOMIC ABSORPTION NEWSLETTER,

14: 153-154.

7 5STE 02 E. STEINNES ( 19 75) A TWO-GROUP SEPARATION SCHEME FOR THE DETERMINATION OF 11 TRACE ELEMENTS IN BIOLOGICAL MATERIAL BY NEUTRON ACTIVATION

ANALYSIS, ANALYTICA CHIMICA ACTA, 78: 307-315.

75TAL 01 Y. TALMI AND V. E. NORVELL (1975) DETERMINATION OF ARSENIC AND ANTIMONY IN ENVIRONMENTAL

SAMPLES USING GAS CHROMATOGRAPHY WITH A MICROWAVE

EMISSION SPECTROMETRIC SYSTEM, ANALYTICAL CHEMISTRY,

47: 1510-1516.

75THO 01 C. P. THOMAS (1975)

AN INTEGRATED-INTENSITY METHOD FOR EMISSION SPECTROGRAPHIC

COMPUTER ANALYSIS, JOURNAL OF RESEARCH OF THE U.S. GEOLOGICAL SURVEY , 3: 181-185.

75WEL 02 R. M. WELCH, AND E. E. CARY (1975) TITLE UNKNOWN, IN JOURNAL OF AGRICULTURE AND FOOD CHEMISTRY.

23: TAKEN FROM 78BYR 01.

7 5WIM 01 J. W. W1MBERLEY ( 19 75) THE DETERMINATION OF TOTAL MERCURY AT THE PART PER BILLION

LEVEL IN SOILS, ORES, AND ORGANIC MATERIALS, ANALYTICA CHIMICA ACTA, 76 : 337- 34 3.

7 5WOR 01 G. J. WORRELL, T. J. VICKERS AND F. D. WILLIAMS ( 1975) A SOLVENT EXTRACTION-ATOMIC FLUORESCENCE SYSTEM FOR THE

DETERMINATION OF CADMIUM IN COMPLEX SAMPLES, ANALYTICA

CHIMICA ACTA, 75: 4 53-4 56.

76AGG 01 J. AGGETT AND A.C. ASPELL (1976) THE DETERMINATION OF ARSENIC(III) AND TOTAL ARSENIC

BY ATOMIC-ABSORPTION SPECTROSCOPY, ANALYST, 101: 34 1-347.

76AND 01 R. W. ANDREWS AND D. C. JOHNSON (1976) DETERMINATION OF SELENIUM(IV) BY ANODIC STRIPPING VOLTAMMETRY IN FLOW SYSTEM WITH ION EXCHANGE SEPARATION, ANALYTICAL CHEMISTRY , 48: 1056-1060.

76BAT 01 L. C. BATE, S. E. LINDBERG , AND A. W. ANDERN ( 1976) ELEMENTAL ANALYSIS OF WATER AND AIR SOLIDS BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

32: 125-135.

76BLO 01 C. BLOCK, R. DAMS, AND J. HOSTE (1976) CHEMICAL COMPOSITION OF COAL AND FLY ASH, IN 76IAE 01,

PP. 101-110.

76CAV 01 P. CAVALLI AND G. ROSSI ( 1976) DETERMINATION OF SUBMICROGRAM AMOUNTS OF MERCURY IN VARIOUS MATRICES BY FLAMELESS ATOMIC-FLUORESCENCE

SPECTROMETRY , ANALYST, 101: 272-277.

7 6CHA 01 A. CHATTOPADHYAY (19 76) MULTIELEMENT INSTRUMENTAL PHOTON ACTTVATION ANALYSIS OF DIGESTED SEWAGE SLUDGES, IN 76IAE 01, PP. 383-403.

76DER 01 M. DERMELJ, V. RAVNIK, AND L. KOSTA (1976) A FAST ISOLATION AND DETERMINATION OF CD IN SOME FUNGI, OTHER BIOLOGICAL MATERIALS, SOIL AND ZN METAL BY NAA, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS 24 : 91-102.

76DTK 01 M. DKSIC AND M.O. MC CRADY (1976) FAST DETERMINATION OF SELENIUM IN BIOLOGICAL MATERIALS BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND

RADIOANALYTICAL LETTERS, 26: 89-94.

76DOG 01 S. DOGAN AND W. RAERDI (1976)

SOME APPLICATIONS OF RAPID SEPARATION OF MERCURY ON METALLIC

COPPER TO ENVIRONMENTAL SAMPLES WITH DETERMINATION BY FLAME- LESS ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA ACTA,

84 : 89-96.

76EPS 01 M. S. EPSTEIN, T. C. RAINS, AND T. C. 0' HAVER ( 1976) WAVELENGTH MODULATION FOR BACKGROUND CORRECTION IN GRAPHITE FURNACE ATOMIC EMISSION SPECTROMETRY, APPLIED SPECTROSCOPY, 30: 324-329.

76EPS 02 M. S. EPSTEIN (1976) PRIVATE COMMUNICATION, NATIONAL BUREAU OF STANDARDS; TAKEN FROM 76ZAN 01.

76FIO 01 J. A. FIORINO, J. W. JONES, AND S. G. CAPAR (1976) SEQUENTIAL DETERMINATION OF ARSENIC, SELENIUM, ANTIMONY,AND

TELLURIUM IN FOODS VIA RAPID HYDRIDE EVOLUTION AND ATOMIC ABSORPTION SPECTROMETRY , ANALYTICAL CHEMISTRY, 48: 120-125.

76FUK 01 M. FUKAMI, S. TODA, AND K. FUWA (1976) DEVELOPMENT OF A NEW TYPE LOW TEMPERATURE ASHER FOR SMALL AMOUNT OF BIOLOGICAL SAMPLE, BUNSEKI KAGAKU, 25: 282-284.

201
CODE N DESCRIPTION

76CAL 01 M. GALLORINI , H. DI CASA, R. STELLA, N. GENOVA, AND E. ORVINI

(1976), MULTIELEMENT TRACE ANALYSIS BY ATOMIC ABSORPTION

SPECTROMETRY AND NEUTRON ACTIVATION ANALYSIS IN BIOLOGICAL

MATRICES, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 32: 17-23.

76CAN 01 R. GANAPATHY , G. M. PAPIA, AND L. GROSSMAN ( 1976) THE ABUNDANCES OF ZIRCONIUM AND HAFNIUM IN THE SOLAR SYSTEM, EARTH AND PLANETARY SCIENCE LETTERS, 29: 302-308.

76GAU 01 A. CAD DRY, B. HAZIERE, D. COMAR, AND D. NAU (1976) MULTI-ELEMENT ANALYSIS OF BIOLOGICAL SAMPLES AFTER INTENSE NEUTRON IRRADIATION AND FAST CHEMICAL SEPARATION, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 29: 77-87.

76GLA 01 E. S. GLADNEY , E. T. JURNEY, AND D. B. CURTIS (1976) NONDESTRUCTIVE DETERMINATION OF BORON AND CADMIUM IN ENVIRONMENTAL MATERIALS BY THERMAL NEUTRON-PROMPT GAMMA-RAY

SPECTROMETRY, ANALYTICAL CHEMISTRY, 48: 2139-2142.

7 6C LA 02 E. S. GLADNEY AND J. W. OWENS ( 1976) BERYLLIUM EMISSIONS FOR A COAL-FIRED POWER PLANT, JORUNAL OF ENVIRONMENTAL SCIENCE AND HEALTH, All: 29 7-311.

76CUI 01 V. P. GUINN, M. A. FUR CELL, AND W. W. WADMAN (1976) MEASUREMENT OF VANADIUM IN OCEANOGRAPHIC/ENVIRONMENTAL

SAMPLES BY NEUTRON ACTIVATION ANALYSIS WITH PRE- IRRADIATION

SEPARATION, IN 76IAE 01, PP. 407-412.

76GUZ 01 G. GUZZI, R. PIETRA, AND E. SABBI0N1 (1976) DETERMINATION OF 25 ELEMENTS IN BIOLOGICAL STANDARD

REFERENCE MATERIALS BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 34: 35-57.

76HAD 01 T. HADE1SHI AND R. D. MCLAUGHLIN ( 1976) ZEEMAN ATOMIC ABSORPTION DETERMINATION OF LEAD WITH A DUAL CHAMBER FURNACE, ANALYTICAL CHEMISTRY , 48: 1009-1011.

76HAN 01 R. G. V. HANCOCK (1976)

LOW FLUX MULTIELEMENT INSTRUMENTAL NEUTRON ACTIVATION

ANALYSIS IN ARCHAEOMETRY, ANALYTICAL CHEMISTRY,

48: 1443-1445.

76HOW 01 N. G. HOWELL, J. D. GANJEI , AND G. H. MORRISON ( 1976) INTERNAL- STANDARDIZATION IN FLAME ANALYSES USING A VIDICON

SPECTROMETER, ANALYTICAL CHEMISTRY, 48: 319-326.

76IAE 01 INTERNATIONAL ATOMIC ENERGY AGENCY (1976) PROCEEDINGS OF AN INTERNATIONAL SYMPOSIUM ON THE DEVELOP- MENT OF NUCLEAR-BASED TECHNIQUES FOR THE MEASUREMENT,

DETECTION, AND CONTROL OF ENVIRONMENTAL POLLUTANTS, VIENNA.

76IHN 01 M. IHNAT (1976) ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF SELENIUM WITH CARBON FURNACE ATOMIZATION, ANALYTICA CHIMICA ACTA,

82, 293-309.

76KAT 02 T. RATO, K. MASUMOTO, N. SATO, AND N. SUZUKI (1976) THE YIELDS OF PHOTONUCLEAR REACTIONS FOR MULTIELEMENT

PHOTON-ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 32: 51-70.

76KAT 03 T. KATO, N. SATO, AND N. SUZUKI (1976) NON- DESTRUCTIVE MULTI -ELEMENT PHOTOACTIVATION ANALYSIS

OF ENVIRONMENTAL MATERIALS , TALANTA, 23: 517-524.

76KAT 04 T. KATO, N. SATO AND N. SUZUKI (1976) MULTIELEMENT PHOTON ACTIVATION ANALYSIS OF BIOLOGICAL

MATERIALS, ANALYTICA CHIMICA ACTA, 81: 337-347.

76KOI 01 H. KOIZUMI AND K. YASUDA (1976) DETERMINATION OF LEAD, CADMIUM, AND ZINC USING THE ZEEMAN

EFFECT IN ATOMIC ABSORPTION SPECTROMETRY

,

ANALYTICAL CHEMISTRY, 48: 1178-1182.

76KRI 03 K. V. KRISHNAMURTY, E. SHPIRT, AND M. M. REDDY (1976) TRACE METAL EXTRACTION OF SOILS AND SEDIMENTS BY NITRIC ACID-HYDROGEN PEROXIDE, ATOMIC ABSORPTION NEWSLETTER,

15: 68-70.

76KUC 01 E. T. KUCERA AND R. R. HEINRICH (1976) MULTIELEMENT TRACE ANALYSIS OF COALS , ASHES, AND RELATED

MATERIALS FROM COAL-TREATMENT FACILITIES BY INSTRUMENTAL NEUTRON ACITVAIION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY. 32: 117-1 50.

CODE N DESCRIPTION

76LAN 01 F. J. LANGMYHR AND J. AAMODT ( 1976) ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF SOME TRACE METALS IN FISH MEAL AND BOVINE LIVER BY THE SOLID SAMPLING TECHNIQUE, ANALYTICA CHIMICA ACTA, 87: 483-486.

76MCC 03 M. T. MCCULLOCH, J. R. DE LAETER, AND K. J. R. ROSMAN ( 1976) THE ISOTOPIC COMPOSITION AND ELEMENTAL ABUNDANCE OF LUTETIUM IN METEORITES AND TERRESTRIAL SAMPLES AND THE LU-176

COSMOCHRONOMETER, EARTH AND PLANETARY SCIENCE LETTERS,

28: 308-322.

76MEL 01 S. MELON! , V. CARAMELLA-CRESPI , M. T. GANZERLI-VALENTINI

,

AND P. BORRONI (1976), ACCURATE DETERMINATION OF ARSENIC AND MERCURY IN REFERENCE MATERIALS BY DESTRUCTIVE NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 25: 117-128.

76MEL 03 S. MEL ONI , V. CARAMELLA-CRESPI, AND C. FASSI ( 1976) DETERMINATION OF SOME BIOELEMENTS IN RICE GRAINS BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 34: 113-119.

76MIL 02 D. A. MILLER AND V. P. GUINN ( 1976) PRECISION HIGH-SPEED NEUTRON ACTIVATION ANALYSIS VIA VERY SHORT-LIVED ACTIVITIES, JOURNAL OF RADIOANALYTICAL CHEMISTRY

32: 179-188.

760ND 01 J. M. ONDOV, R. C. RAGAINI, R. E. HEFT, G. L. FISHER,

D. SILBERMAN, AND B. A. PRENTICE ( 19 76), INTERLABORATORY COMPARISON OF NEUTRON ACTIVATION AND ATOMIC ABSORPTION ANALYSES OF SIZE-CLASSIFIED STACK FLY ASH, IN METHODS AND

STANDARDS FOR ENVIRONMENTAL MEASUREMENT, PROCEEDINGS OF THE

8TH TMR SYMPOSIUM, GAITHERSBURG , MARYLAND, NATIONAL BUREAU

OF STANDARDS SPECIAL PUBLICATION 4 64 , PP. 565-569.

760WE 01 J. W. OWENS AND E. S. GLADNEY (1976) LITHIUM METABORATE FUSION AND THE DETERMINATION OF TRACE METALS IN FLY ASH BY FLAMELESS ATOMIC ABSORPTION, ATOMIC ABSORPTION NEWSLETTER, 15: 95-97.

76PIE 01 J. 0. PIERCE , F. E. LICHTE, C. R. H. VOGT, A. ABU-SAMRA,

T. R. RYAN, S. R. KOIRTYOHANN, AND J. R. VOGT (1976) COMPARISON OF CHROMIUM DETERMINATIONS IN ENVIRONMENTAL AND

BIOLOGICAL SAMPLES BY NEUTRON ACTIVATION ANALYSIS, ATOMIC ABSORPTION AND GAS CHROMATOGRAPHY , IN 76IAE, PP. 357-368.

76RAG 01 R. C. RAGAINI, R. E. HEFT, AND D. GARVIS (1976) NEUTRON ACTIVATION ANALYSIS AT THE LIVERMORE POOL-TYPE

REACTOR FOR THE ENVIRONMENTAL RESEARCH PROGRAM, LAWRENCE LIVERMORE LABORATORY REPORT UCRL-52092.

76SIE 01 D. D. SIEMER, P. KOTEEL , AND V . JAPJWALA (1976) OPTIMIZATION OF ARSINE GENERATION IN ATOMIC ABSORPTION

ARSENIC DETERMINATIONS, ANALYTICAL CHEMISTRY, 48: 836-840.

76STE 01 R. STELLA, N. GENOVA, M. DI CASA, M. GALLORINI, AND E. ORVINI

(1976), COMPARATIVE INVESTIGATION OF DIFFERENT RADIOCHEMICAL METHODS FOR CHROMIUM DETERMINATION IN BIOLOGICAL AND

ENVIRONMENTAL MATRICES, JOURNAL OF RADIOANALYTICAL CHEMISTRY

34 : 59-63.

76STE 05 E. STEINNES ( 1976) INSTRUMENTAL ACTIVATION ANALYSIS OF COAL AND FLY ASH WITH

THERMAL AND EPITHERMAL NEUTRONS AND SHORT-LIVED NUCLIDES, ANALYTICA CHIMICA ACTA, 87: 4 51-462.

76URE 01 A.M. URE AND M.C. MITCHELL (1976) THE DETERMINATION OF CADMIUM IN PLANT MATERIAL AND SOIL EX- TRACTS BY SOLVENT EXTRACTION AND ATOMIC ABSORPTION WITH A

CARBON-ROD ATOMIZER, ANALYTICA CHIMICA ACTA, 87: 283-290.

76VIJ 01 P. N. V1JAN AND G. R. WOOD (1976) SEMI-AUTOMATED DETERMINATION OF LEAD BY HYDRIDE GENERATION AND ATOMIC-ABSORPTION SPECTROPHOTOMETRY,

ANALYST, 101: 966-973.

76VIJ 02 P. N. VIJAN, A. C. RAYNER, D. STURGIS, AND G. R. WOOD (1976) A SEMI-AUTOMATED METHOD FOR THE DETERMINATION OF ARSENIC IN

SOIL AND VEGETATION BY GAS-PHASE SAMPLING & ATOMIC ABSORP- TION SPECTROMETRY , ANALYTICA CHIMICA ACTA, 82 : 329 -336.

202
CODE N DESCRIPTION

CODE N DESCRIPTION

76WAU 01 R. D. WAUCHOPE (1976) ATOMIC ABSORPTION DETERMINATION OF TRACE QUANTITIES OF ARSENIC: APPLICATION OF A RAPID ARSINE GENERATION TECHNIQUE

TO SOIL, HATER, AND PLANT SAMPLES, ATOMIC ABSORPTION

NEWSLETTER, 15: 64-67.

7 6WEW 01 E. M. KEVERKA (1976) TRACE ELEMENT CHARACTERIZATION AND REMOVAL/RECOVERY FROM

COAL AND COAL WASTES, LOS ALAMOS SCIENTIFIC LABORATORY

REPORT, LA-6498-PR.

76WHI 01 D. WHITEHEAD AND S. A. MALIK (1976) AUTOMATED COLORIMETRIC DETERMINATION OF PHOSPHORUS IN SILICATE ROCKS IN THE PRESENCE OF SILICON, ANALYST,

101: 485-490.

76WIL 01 D.R. WILLIAMS AND J.S. HISLOP ( 1976) DETERMINATION OF COPPER AND ZINC IN BONE ASH USING ACCELERATOR PRODUCED GAMMA PHOTONS, PROC. ANALYT. DTV. CHEM. SOC. (LONDON), 13: 202-204.

76WOL 01 W. R. WOLF (1976) COUPLED GAS CHROMATOGRAPHY - ATOMIC ABSORPTION SPECTROMETRY FOR THE NANOGRAM DETERMINATION OF CHROMIUM, ANALYTICAL CHEMISTRY, 48: 1717-1720.

76ZAN 01 A. T. ZANDER, T. C. 0' RAVER AND P. N. KELIRER (1976) CONTINUUM SOURCE ATOMIC ABSORPTION SPECTROMETRY WITH HIGH RESOLUTION AND WAVELENGTH MODULATION, ANALYTICAL CHEMISTRY,

48: 1166-1175.

76ZAN 02 A. T. ZANDER AND T. C. O'HAVER (1976) IMPROVED ACCURACY IN BACKGROUND CORRECTED ATOMIC ABSORPTION

SPECTROMETRY, IN METHODS AND STANDARDS FOR ENVIRONMENTAL

MEASUREMENT, PROCEEDINGS OF THE 8TH IMR SYMPOSIUM, GAITHERSBURG, MARYLAND, NATIONAL BUREAU OF STANDARDS SPECIAL PUBLICATION 4 64 , PP. 53-59.

76ZEI 01 R. ZEISLER, J. B. CROSS, AND E. A. SCHWEIKERT ( 1976) TRACE ELEMENTAL ANALYSIS BY HEAVY ION INDUCED X-RAY EMISSION ANALYTICAL CHEMISTRY, 48: 2124-2129.

77AND 01 W. L. ANDERSON AND K. E. SMITH ( 1977) DYNAMICS OF MERCURY AT COAL-FIRED POWER PLANT AND ADJACENT

COOLING LAKE, ENVIRONMENTAL SCIENCE AND TECHNOLOGY,

11: 75-80.

77ARU 01 P. ARUSCAVAGE (1977) DETERMINATION OF ARSENIC, ANTIMONY, AND SELENIUM IN COAL BY ATOMIC ABSORPTION SPECTROMETRY WITH A GRAPHITE TUBE ATOMIZER

JOURNAL OF RESEARCH OF THE UNITED STATES GEOLOGICAL SURVEY

5 : 4 0 5-4 08.

77BAJ 02 S. BAJO AND A. WYTTEN BACH (1977) LIQUID-LIQUID EXTRACTION OF CADMIUM WITH

DIETHYLDITHIOCARBAMIC ACID, ANALYTICAL CHEMISTRY,

49: 158-161.

77BAN 03 S. BAN DO AND T. IMAHASHI (1977) DETERMINATION OF ARSENIC , MERCURY, AND SELENIUM IN BIOLOGICAL STANDARD REFERENCE MATERIALS BY NEUTRON ACTIVATION

ANALYSIS, BUNSEK1 KACAKU, 26: 138-140.

77BUO 01 J. A. BUONO, J. C. BUONO, AND J. L. FASCHING (1977) SIMULTANEOUS DETERMINATION OF AL, V, MN, AND CU FROM NEUTRON-ACTIVATED SALINE MATRICES BY PRECIPITATION WITH

POLY-5-VINYL-8-HYDROXYQUINOLINE, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 36: 353-358.

77BUR 01 R. W. BURKE AND B. I. DIAMONDSTONE (1977) PROCEDURES FOR THE DETERMINATION OF ARSENIC, COPPER, AND

NICKEL BY MOLECULAR ABSORPTION SPECTROMETRY, IN 77MAV 01,

PP. 73-84.

77BYR 01 A. R. BYRNE (1977) ACTIVATION ANALYSIS OF TIN AT NANOGRAM LEVEL BY LIQUID

SCINTILLATION COUNTING OF SN-121, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 37: 591-597.

77CAH 01 R. A. CAHILL (1977) TAKEN FROM 77GLU 01.

77CAM 01 J. L. CAMPBELL (1977) SPECIMEN PREPARATION IN PIXE ANALYSIS, NUCLEAR INSTRUMENTS AND METHODS, 142: 263-273.

77CHA 01 A. CHATTOPADHYAY (1977) OPTIMAL USE OP INSTRUMENTAL NEUTRON AND PHOTON ACTIVATION ANALYSES FOR MULTIELEMENT DETERMINATIONS IN SEWAGE SLUDGES, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 37: 785-799.

77CRO 01 J. B. CROSS, R. ZEISLER AND E. A. SCHWEIKERT ( 1977) HIGH ENERGY HEAVY-ION INDUCED X-RAY EMISSION ANALYSIS

NUCLEAR INSTRUMENTS AND METHODS, 142: 111-119.

77DER 01 M. DERMELJ , V. RAVNIK, AND L. KOSTA (1977) SIMULTANEOUS DETERMINATION OF TRACE ELEMENTS CADMIUM, COPPER, AND ZINC IN DIFFERENT ENVIRONMENTAL SAMPLES BY NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 28 : 231-240.

77DIK 01 M. DUtSIC AND T. F. COLE ( 1977) FAST DETERMINATION OF MOLYBDENUM AND TELLURIUM BY NEUTRON ACTIVATION ANALYSIS, ANALYTICA CHIMICA ACTA, 93: 261-266.

77DON 01 D. L. DONOHUE, J. A. CARTER, AND J. C. FRANKLIN (1977) SEPARATED ISOTOPES AS INTERNAL STANDARDS IN SPARK SOURCE MASS SPECTROMETRY, ANALYTICAL LETTERS, 10: 371-379.

77EGA 01 A. EGAN, S. A. KERR, AND M. J. MINSKI (1977) DETERMINATION OF SELENIUM IN BIOLOGICAL MATERIALS USING

SE-77M (T-17.5 SEC) AND CYCLIC ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 28: 369-378.

77FEL 01 C. FELDMAN (1977) DETERMINATION OF TRACES OF ARSENIC IN SILICEOUS MATERIALS, ANALYTICAL CHEMISTRY, 49: 825-828.

77FIL 01 R. H. FILBY, K. R. SHAH , AND C. A. SAUTTER (1977) A STUDY OF TRACE ELEMENT DISTRIBUTION IN THE SOLVENT REFINED

COAL (SRC) PROCESS USING NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37: 693-704.

77FLA 01 F. J. FLANAGAN, L. J. SCHWARZ, J. J. ROWE, AND A. DORRZAPF

(1977), AVAILABLE CLAY AND FELDSPAR REFERENCE SAMPLES AS STANDARDS FOR ARCHAEOLOGICAL POTTERY STUDIES, GEOSTANDARDS

NEWSLETTER, 1: 61-66.

77FLO 01 T. FLORKOWSKI, T. KUC, AND S. PIOREK (1977) DETERMINATION OF TRACE ELEMENTS IN PLANTS BY THE X-RAY FLUORESCENCE ANALYSIS FOR ENVIRONMENTAL POLLUTION

INVESTIGATIONS, INTERNATIONAL JOURNAL OF APPLIED RADIATION AND ISOTOPES, 28: 679-686.

77FRI 01 M. T. FRIEND, C. A. SMITH, AND D. WIS HART (1977) ASHING AND WET OXIDATION PROCEDURES FOR THE DETERMINATION OF SOME VOLATILE TRACE METALS IN FOODSTUFFS AND BIOLOGICAL MATERIALS BY AAS, ATOMIC ABSORPTION NEWSLETTER, 16: 46-49.

77FRY 01 R. C. FRY AND M. B. DENTON (1977) HIGH SOLIDS SAMPLE INTRODUCTION FOR FLAME ATOMIC ABSORPTION ANALYSIS, ANALYTICAL CHEMISTRY, 49: 1413-1417.

77FUJ 01 K. FUJIWARA, Y. UMEZAWA, U. NUMATA, K. FUWA, AND S. FUJIWARA,

(1977), CARBON ROD ATOMIC ABSORPTION FOR INTACT CELL SYSTEMS AND BIOLOGICAL TISSUES, BUNSEKI KAGAKU, 26: 735-737.

77GAN 03 S. GANGADHARAN , M. SANKAR DAS, AND S. YEGNASUBRAMANIAN ( 1977) MEASUREMENT OF ANNIHILATION RADIATION IN ACTIVATION ANALYSIS ENHANCEMENT OF SPECIFICITY THROUGH TRIPLE COINCIDENCE, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37: 181-187.

77GIA 01 R. D. GIAUQUE , R. B. GARRETT, AND L. Y. GODA (1977) DETERMINATION OF FORTY ELEMENTS IN GEOCHEMICAL SAMPLES AND COAL FLY ASH BY X-RAY FLUORESCENCE SPECTROMETRY, ANALYTICAL CHEMISTRY, 49: 1012-1017.

77GIA 02 R. D. GIAUQUE (1977) PRIVATE COMMUNICATION, LAWRENCE BERKELEY LABORATORY.

77GIL 01 T. E. GILLS AND L. T. MCCLENDON (1977) ROLE OF NEUTRON ACTIVATION ANALYSIS IN THE EVALUATION OF SAMPLING, STORAGE, AND ANALYSIS OF SAMPLES FOR THE NATIONAL

ENVIRONMENTAL BANKING SYSTEM , JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 39 : 28 5-291.

77GIL 03 T. E. GILLS, M. GALLORIN1, AND R. GREENBERG (1977) THE DETERMINATION OF SELECTED TOXIC ELEMENTS IN BIOLOGICAL MATRICES USING RADIOCHEMICAL ACTIVATION ANALYSIS,

PP. 597-609. IN 77VOG 01.

203
CODE N DESCRIPTION CODE N DESCRIPTION

77CLA 01 E. S. CLADNEY (1977) COPPER DETERMINATION IN STANDARD MATERIALS BY NEUTRON ACTIVATION AND S RAFT ON NMRR AN ION-EXCHANGE RESIN, ANALYTICA CHIMICA ACTA, 91 : 353-356.

77CLA 02 E. S. CLADNEY (1977) DIRECT DETERMINATION OF BERYLLIUM IN NBS SRM 16 32 COAL BY FLAMELESS ATOMIC ABSORPTION, ATOMIC ABSORPTION NEWSLETTER,

16: 4 2-4 3.

77GLA 03 E. S. CLADNEY AND J. W. OWENS ( 1977) DETERMINATION OF MERCURY BY CARRIER-FREE COMBUSTION SEPARA- TION AND FLAMELESS ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA

CHIMICA ACTA, 90: 271-274

77GLU 01 H. J. GLUSKOTER, R. R. RUCH, W. G. MILLER, R. A. CAHILL,

C. B. DREHER, AND J. R. KURN (19 77), TRACE ELEMENTS IN

COAL: OCCURRENCE AND DISTRIBUTION, ILLINOIS STATE GEOLOGICAL SURVEY, CIRCULAR 499.

77GOO 01 C.C. COODE, J. HERRINGTON, AND P.C. GODDARD (1977) NEUTRON ACTIVATION ANALYSIS FOR ALUMINUM IN BONE AND TISSUE

SAMPLES, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS,

31: 87-94.

77GUI 02 V. P. GUINN AND D. A. MILLER ( 1977) RECENT INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS STUDIES UTILIZING VERY SHORT-LIVED ACTIVITIES, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37 : 3 1 3- 324 .

77GUI 03 V. P. CUINN, E. R. CHRISTENSEN, K. DE LANCEY ( 1977) NEUTRON ACTIVATION ANALYSIS TRACE-ELEMENT STUDIES IN CONNECTION WITH THE OFFSHORE DRILLING FOR OIL, PP. 303-311, IN 77VOG 01.

77GUL 01 B. L. CULSON (1977) ISOTOPIC AND GEOCHEMICAL STUDIES ON CRUSTAL EFFECTS IN THE GENESIS OF THE WOODLAWN PB-ZN-CU DEPOSIT, CONTRIBUTIONS TO MINERALOGY AND PETROLOGY, 65: 227-242.

77GUZ 01 G. GUZZI, A. COLOMBO, F. GIRARDI, R. PIETRA, G. ROSSI, AND

N. TOUSSAINT (1977), COMPARISON OF VARIOUS ANALYTICAL TECHNIQUES FOR HOMOGENEITY TEST OF CANDIDATE STANDARD REFERENCE MATERIALS , JOURNAL OF RADIOANALYTICAL CHEMISTRY,

39 : 263-276.

77HAM 01 H. HAMACUCHI, Y. NUMATA, S. IWATA, M. KOYAMA, K. SASAJIMA,

Y. KATAYAMA, T. TAKEUCHI, M. SHINOGI, T. MAMURO, Y. KUSAKA,

H. TSUJI, T. TAMARI, T. SAGAWA, S. OHMORI, S. NAGATSUKA,

Y. TANIZAKI, T. SUSUKI, K. TOMURS, Y. HASHIMOTO, S. BANDO, AND T. IMAHASHI ( 1977) PRECISION OF NEUTRON ACTIVATION ANALYSIS FOR ENVIRONMENTAL BIOLOGICAL MATERIALS, BUNSEKI KAGAKU, 26: T23-T28.

77HAM 04 L. G. HAMBLETON (1977) SEMIAUTOMATED METHOD FOR SIMULTANEOUS DETERMINATION OF PHOSPHORUS, CALCIUM, AND CRUDE PROTEIN IN ANIMAL FEEDS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS,

60 : 845-852.

77HEY 01 K. HEYDORN, P. Z. SKANBORG, R. GOWZDZ, J. 0. SCHMIDT, AND

M. E. WACKS ( 1977), DETERMINATION OF LITHIUM BY INSTRUMENTAL

NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 37: 155-168.

77HOP 01 D. M. HOPKINS ( 1977) AN IMPROVED ION-SELECTIVE ELECTRODE METHOD FOR THE RAPID

DETERMINATION OF FLUORINE IN ROCKS AND SOILS, JOURNAL OF RESEARCH OF THE UNITED STATES GEOLOGICAL SURVEY , 5: 589-593.

77JER 01 R. E. JERVIS, B. TIEFENBACH, AND A. CHATTOPADHYAY (1977)

SCALP HAIR AS A MONITOR OF POPULATION EXPOSURE TO ENVIRONMENTAL POLLUTANTS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 37 : 751-760.

77JUR 01 E. T. JURNEY, D. B. CURTIS, AND E. S. CLADNEY (1977) DETERMINATION OF SULFUR IN ENVIRONMENTAL MATERIALS BY THERMAL NEUTRON CAPTURE PROMPT GAMMA- RAY SPECTROMETRY, ANALYTICAL CHEMISTRY, 49 : 1741-1743.

7 7JUR 02 H. JURGENSEN AND D. BEHNE ( 19 77) VARIATIONS IN TRACE ELEMENT CONCENTRATIONS IN HUMAM BLOOD

SERUM IN THE NORMAL STATE INVESTIGATED BY INSTRUMENTAL

NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 37 : 37 5-382.

77KON 01 N. K. KONANUR AND C. W. VAN LOON (1977) DETERMINATION OF LEAD AND ANTIMONY IN FIREARM DISCHARGE RES- IDUES ON HANDS BY ANODIC STRIPPING VOLTAMMETRY .TALANTA,

24 : 184-187

77KUS 01 Y. KUSAKA, H. TSUJI , Y. TAMARI, T. SAGAWA, S. OHMORI,

S. IMAI, AND T. OZAKI (1977), NEUTRON ACTIVATION ANALYSIS OF BIOLOGICALLY ESSENTIAL TRACE ELEMENTS IN ENVIRONMENTAL

SPECIMENS USING PYRROLIDINEDITHIOCARBAMATE EXTRACTION, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37 : 917-926.

7 7LAD 01 W. LADRACH AND J. D. VAN DER LAARSE ( 1977) THE DETERMINATION OF TOTAL SULPHUR IN COAL BY A SEMI-MICRO TUBE-COMBUSTION METHOD, ANALYTICA CHIMICA ACTA, 94: 213-216.

77LAN 01 J. LANGE AND H.-J. BRUMS ACK (1977) TOTAL SULPHUR ANALYSIS IN GEOLOCICAL AND BIOLOGICAL MATERIAL

BY COULOMETRIC TITRATION FOLLOWING COMBUSTION, ZEITSCHRIFT

FUR ANALYTISCHE CHEMIE, 286: 361-366.

77LAU 01 J. C. LAUL AND L. A. RANCITELLI (1977) MULTIELEMENT ANALYSIS BY SEQUENTIAL INSTRUMENTAL AND

RADIOCHEMICAL NEUTRON ACTIVATION, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 38 : 461-4 7 5.

77LAU 02 J. C. LAUL, K. K. NIELSON AND N. A. WOGMAN (1977) TRACE RARE EARTH ANALYSIS BY NEUTRON ACTIVATION AND GAMMARAY/ X-RAY SPECTROMETRY, PP. 198-209, IN 77VOG 01.

77LIE 01 P. LIEVENS, J. VERSIECK, R. CORNELIS, AND J. HOSTE ( 1977) THE DISTRIBUTION OF TRACE ELEMENTS IN NORMAL HUMAN LIVER

DETERMINED BY SEMI-AUTOMATED RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

37 : 483-496.

77LOR 01 D. A. LORD, J. W. MCLAREN , AND R. C. WHEELER (1977) DETERMINATION OF TRACE METALS IN FRESH WATER MUSSELS BY ATOMIC ABSORPTION SPECTROMETRY WITH DIRECT SOLID SAMPLE

INJECTION, ANALYTICAL CHEMISTRY, 49: 257-261.

77MAE 01 W. MAENHAUT AND W. H. ZOLLER (1977) DETERMINATION OF THE CHEMICAL COMPOSITION OF THE SOUTH POLE

AEROSOL BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS

,

JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37: 637-650.

77MA1 01 E. J. MAIENTHAL (1977) ANALYSIS OF BOTANICAL STANDARD REFERENCE MATERIALS BY CATHODE RAY POLAROGRAPHY , IN 77MAV 01, PP. 91-105.

77MAV 01 R. MAVRODINEANU (EDITOR) (1977) PROCEDURES USED AT THE NATIONAL BUREAU OF STANDARDS TO DETERMINE SELECTED TRACE ELEMENTS IN BIOLOGICAL AND

BOTANICAL MATERIALS, NBS SPECIAL PUBLICATION 492.

77IHN 01 M. IHNAT AND H. J. MILLER ( 1977) 77MEL 01 S. MELONI, M.T. GANZERLI-VALENTINI (1977) ACID DIGESTION, RYDRIDE EVOLUTION ATOMIC ABSORPTION SPECTRO- NEW IMPROVED CHEMICAL PROCEDURES IN THE NEUTRON ACTIVATION

PHOTOMETRIC METHOD FOR DETERMINING ARSENIC AND SELENIUM IN ANALYSIS OF ENVIRONMENTAL SAMPLES, PP. 161-169, IN 77VOG 01. FOODS: COLLABORATIVE STUDY. PART I., JOURNAL OF THE ASSOCIATION

OF OFFICIAL ANALYTICAL CHEMISTS, 60: 1414-1433. 77MIN 01 M. J. MINSKI, C. A. GIRLING , AND P. J. PETERSON (1977) DETERMINATION OF GOLD AND ARSENIC IN PLANT MATERIAL BY

77IHN 03 M. IHNAT AND H. J. MILLER (1977) NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYANALYSIS OF FOODS FOR ARSENIC AND SELENIUM BY ACID DIGESTION TICAL LETTERS, 30: 179-186. HYDRIDE EVOLUTION ATOMIC ABSORPTION SPECTROPHOTOMETRY, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 77MIT 01 J. W. MITCHELL, L. D. BLITZER, T. Y. KOMETANI, T. GILLS, AND

60: 813-825. I. CLARK (1977), HOMOGENEOUSLY DOPED SILICA MATRICES FOR TRACE ELEMENT STANDARDS IN NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 39 : 3 3 5-342.

204
CODE N DESCRIPTION CODE N DESCRIPTION

77MYR 01 D. R. MYRON, S. H. GIVAND, AND P. H. NIELSEN (1977) VANADIUM CONTENT OF SELECTED FOODS AS DETERMINED BY FLAMELESS ATOMIC ABSORPTION SPECTROSCOPY, JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY , 25: 297-300.

77NAD 01 R. A. NADKARNI AND C. H. MORRISON (1977) NEUTRON ACTIVATION DETERMINATION OF NOBLE METALS USING A SELECTIVE GROUP SEPARATION SCHEME, JOURNAL OF RADIGANALYTI CAL CHEMISTRY , 38 : 4 35-449.

77NAD 02 R. A. NADKARNI (1977) MULTIELEMENT ANALYSIS OF BIOLOGICAL STANDARDS BY NEUTRON

ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 30: 329-340.

77NIE 01 K. K. NIELSON (1977) MATRIX CORRECTIONS FOR ENERGY DISPERSIVE X-RAY FLUORESCENCE

ANALYSIS OF ENVIRONMENTAL SAMPLES WITH CO HERENT/ INCOHERENT

SCATTERED X-RAYS, ANALYTICAL CHEMISTRY, 49: 641-648.

770HL 01 0. A. OHLWEILER AND J. 0. MEDITSCH ( 1977) DETERMINATION OF SILICA IN SILICATES BY FORMATION OF 12-MOLYBDOSILICIC A CI D AND REDOX TITRATION OF MOLYBDENUM(III), TALANTA, 24 : 6 52- 654.

770M1 01 J. OMI AND Y. HASHIMOTO (1977) POST-IRRADIATION CHEMISTRY OF SELENIUM IN NEUTRON ACTIVATION

ANALYSIS, BUNSEKI KAGAKU, 26: 419-421.

770SB 01 T. W. OSBORN AND W. B. BROERING ( 1977) NEUTRON ACTIVATION ANALYSIS IN AN INDUSTRIAL LABORATORY

USING AN OFF-SITE NUCLEAR REACTOR, PP. 185-197, IN 77VOG 01.

77PAC 01 PETROL. ASSOC. CONSERV. CAN. ENVIR. (1977)

PACE REPORT NO. 77-5; TAKEN FROM 78BER 02.

77PAR 01 R. M. PARR (1977) PROBLEMS OF CHROMIUM ANALYSIS IN BIOLOGICAL MATERIALS: AN INTERNATIONAL PERSPECTIVE WITH SPECIAL REFERENCE TO RESULTS

FOR ANALYTICAL QUALITY CONTROL SAMPLES, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 39 : 421-4 33.

77PAU 01 P. J. PAULSEN (1977) SPARK SOURCE MASS SPECTRDMETRIC ISOTOPE DILUTION DETERMINATION OF CADMIUM , COPPER, IRON, LEAD, MERCURY, MOLYBDENUM, NICKEL , SELENIUM, SILVER, TELLURIUM, THALLIUM, AND ZINC , IN 77MAV 01, PP. 33-48.

77PIL 01 A. PILATE, P. GELADI, AND F. ADAMS (1977) DETERMINATION OF ALUMINUM IN AEROSOLS BY FLAMELESS ATOMIC- ABSORPTION SPECTROMETRY, TALANTA, 24, 512-514.

77POO 01 C. F. POOLE, N. J. EVANS, AND D. G. WIBBERLEY (1977) DETERMINATION OF SELENIUM IN BIOLOGICAL SAMPLES BY GAS-LIQUID CHROMATOGRAPHY WITH ELECTRON CAPTURE DETECTION, JOURNAL OF CHROMATOGRAPHY , 136: 73-83.

77RAI 01 R. M. RAIE, AND H. SMITH ( 1977) THE DETERMINATION OF SELENIUM IN BIOLOGICAL MATERIAL BY THERMAL NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND

RADIOANALYTICAL LETTERS, 28: 215-220.

77RIN 01 H. A. VAN RINSVELT, R. D. LEAR, AND W. R. ADAMS ( 1977) HUMAN DISEASES AND TRACE ELEMENTS: INVESTIGATIONS BY PROTON INDUCED X-RAY EMISSION, NUCLEAR INSTRUMENTS AND METHODS,

142: 171-180.

77ROO 01 H. L. ROOK (1977) THE DETERMINATION OF IODINE IN BIOLOGICAL AND ENVIRONMENTAL

STANDARD REFERENCE MATERIALS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 39: 351-358.

77RDW 03 J. J. ROWE AND E. STEINNES (1977) INSTRUMENTAL ACTIVATION ANALYSIS OF COAL AND FLY ASH WITH

THERMAL AND EPITHERMAL NEUTRONS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 37: 849-856.

77ROW 04 J. J. ROWE AND E. STEINNES (1977) DETERMINATION OF 30 ELEMENTS IN COAL AND FLY ASH BY THERMAL AND EPITHERMAL NEUTRON-ACTIVATION ANALYSIS, TALANTA, 24: 4 33-4 39.

77SEG 01 C. S EGE BADE (1977) SIMULTANE BESTIMMUNG VON N, MG, SI, P, UND K IN

P FLANZENMATERIAL DURCH 14 MEV-NEUTRONENAKTIVIERUNGS ANALYSE, ZEITSCHR1FT FUR ANALYTISCHE CHEMIE, 284 : 23-29.

77SHE 02 D. A. SHEARER, R. 0. C10UTIER, AND M. HIDIROGLOU ( 1977) CHELATE EXTRACTION AND FLAME ATOMIC ABSORPTION SPECTRDMETRIC DETERMINATION OF NANOGRAM AMOUNTS OF MANGANESE IN BLOOD AND

ANIMAL TISSUE, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALY- TICAL CHEMISTS, 60: 155-159.

77SHU 01 G. T.C. SHUM, H. C. FREEMAN AND J. F. UTHE ( 1977) FLAMELESS ATOMIC ABSORPTION SPECTROPHOTOMETRY OF SELENIUM IN FISH AND FOOD PRODUCTS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 60: 1010-1014.

77SIE 01 D. D. SIEMER, R. K. V1TEK, P. KOTEEL , AND W. C. HOUSER ( 1977) DETERMINATION OF ARSENIC IN BEVERAGES AND FOODS BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY, ANALYTICAL LETTERS, 10: 357-369.

77SMI 01 R. G. SMITH, J. C. VAN LOON, J. R. KNECHTEL, J. L. FRASER,

A. E. PITTS, AND A. E. HODGES ( 1977), A SIMPLE AND RAPID

HYDRIDE GENERATION-ATOMIC ABSORPTION METHOD FOR THE DETERMINATION OF ARSENIC IN BIOLOGICAL, ENVIRONMENTAL, AND GEOLOGICAL SAMPLES, ANALYTICA CHIMICA ACTA, 93: 61-67.

77SMI 04 J. SMITS AND R. VAN GRIEKEN ( 1977) OPTIMIZATION OF A SIMPLE SPOTTING PROCEDURE FOR X-RAY

FLUORESCENCE ANALYSIS OF WATERS, ANALYTICA CHIMICA ACTA,

88: 97-107.

77311 05 F. SMITH, JR, A. MCMURTRIE, AND H. GALBRAITH ( 1977) ION CHROMATOGRAPHIC DETERMINATION OF SULFUR AND CHLORINE USING MILLIGRAM AND SUBMILLIGRAM SAMPLE WEIGHTS, MICROCHEMICAL JOURNAL, 22: 4 5-49.

77SMY 01 W. R. SMYTHE (1977) PRIVATE COMMUNICATION, UNIVERSITY OF COLORADO; TAKEN FROM 77RIN 01.

77STE 02 R. STELLA, N. GENOVA, M. DI CASA (1977) HALOGENS DETERMINATION IN VEGETABLE NBS STANDARD REFERENCE

MATERIALS: FLUORINE BY ISOTOPE DILUTION; CHLORINE, BROMINE, IODINE BY NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND

RADIOANALYTICAL LETTERS, 30 : 65- 74.

77TAG 01 M. TAGUCHI , K. YASUDA, Y. DOKIYA, M. SHIMIZU, AND S. TODA (1977) MERCURY DETERMINATION IN FISH SAMPLES BY FLAMELESS ATOMIC ABSORPTION SPECTROMETRY; SAMPLING AND WET DIGESTION, BUNSEKI KAGAKU , 26: 4 38-441.

77TAM 01 K. H. TAM AND H. B. S. CONACHER ( 1977) THE SUITABILITY OF THE DRY ASHING PROCEDURE FOR DETERMINATION OF ARSENIC IN MARINE SAMPLES, JOURNAL OF ENVIRONMENTAL SCIENCE AND HEALTH, B12: 213-227.

77TTL 01 J. H. TILLMAN ( 1977) A COMBUSTIMETRIC METHOD FOR DETERMINING THE TOTAL CARBON CONTENT OF GEOLOGICAL MATERIALS, JOURNAL OF RESEARCH OF THE UNITED STATES GEOLOGICAL SURVEY, 5: 583-587.

77TJI 01 P. S. TJIOE, J. J. M. DE GOEIJ, AND J. P. W. HOUTMAN (1977) EXTENDED AUTOMATED SEPARATION TECHNIQUES IN DESTRUCTIVE NEUTRON ACTIVATION ANALYSIS: APPLICATION TO VARIOUS

BIOLOGICAL MATERIALS, INCLUDING HUMAN TISSUES AND BLOOD, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37 : 511-522.

77TRO 01 G. TROLL, A. FARZANEH, AND K. CAMMANN (1977) RAPID DETERMINATION OF FLUORIDE IN MINERAL AND ROCK SAMPLES USING AN ION-SELECTIVE ELECTRODE, CHEMICAL GEOLOGY,

20: 295-305.

77TSU 01 K. TSUNODA, K. FUJIWARA, AND K. FUWA (1977) SUBNANOGRAM FLUORINE DETERMINATION BY ALUMINIUM MONOFLUORI DE MOLECULAR ABSORPTION SPECTROMETRY, ANALYTICAL CHEMISTRY,

49: 2035-2039.

77UCH 02 T. UCHIDA, I. KOJIMA AND C. IIDA ( 1977) "ONE-DROP METHOD" IN FLAME ATOMIC ABSORPTION SPECTROMETRY, BUNSEKI KAGAKU, 26: T44-T47.

205
CODE M DESCRIPTION CODE N DESCRIPTION

7 7VAN 01 C. VANDECASTEELE, R. KIEFFER, AND J. HOSTE ( 1977) ACTIVATION ANALYSIS WITH CYCLOTRON-PRODUCED PAST NEUTRONS APPLICATION TO INSTRUMENTAL MULTI-ELEMENT ANALYSIS AND TO THE RADIOCHEMICAL DETERMINATION OF FLUORINE, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 37: 255-265.

77V0B 01 M. VOBECZKY, L. PAVLLK, AND J. BENES (1977) NON- DESTRUCTIVE NEUTRON ACTIVATION ASSAY OF SUBM1CROGRAM QUANTITIES OF SELENIUM , RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 29: 159-164.

77VOC 01 J.R. VOCT (EDITOR) (1977) PROCEEDINGS OF THE THIRD INTERNATIONAL CONFERENCE ON NUCLEAR METHODS IN ENVIRONMENTAL AND ENERGY RESEARCH,

COLUMBIA, MISSOURI , OCTOBER 1977, CONF-771072.

77WIC 01 W. A. WICKS AND R. W. BURKE (1977) DETERMINATION OF BERYLLIUM BY FLUORESCENCE SPECTROMETRY

,

IN 77MAV 01, PP. 85-89.

77WIL 01 D. R. WILLIAMS AND J. S. HISLOP (1977) THE NON DESTRUCTIVE DETERMINATION OF IODINE IN SOILS AND

BIOLOGICAL MATERIALS BY HIGH ENERGY GAMMA-PHOTON ACTIVATION, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 39: 359-373.

77W1L 02 R. D. WILLIS AND R. L. WALTER ( 1977) COMPUTER ANALYSIS OF PROTON INDUCED X-RAY EMISSION SPECTRA, NUCLEAR INSTRUMENTS AND METHODS, 142: 231-242.

77WIL 03 R. D. WILLIS, R. L. WALTER, R. W. SHAW, AND W. F. GUTKNECHT

( 1977), PROTON-INDUCED X-RAY EMISSION ANALYSIS OF THICK AND

THIN TARGETS, NUCLEAR INSTRUMENTS AND METHODS , 142: 67-77.

77YAN 01 Y. YANO, N. ODAKA, S. TAKEI , AND K. NAGASHIMA ( 1977) DETERMINATION OF TRACE HEAVY METALS IN ENVIRONMENTAL SAMPLES WITH SPECIAL REFERENCE TO LEAD IN PLANTS, BUNSEKI KAGAKU,

26: T25-T29.

77YAS 01 K. YASUDA, M. TAGUCHI , S. TAMURA, AND S. TODA ( 1977) DETERMINATION OF SELENIUM IN BIOLOGICAL SAMPLES BY SOLVENT EXTRACTION-GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY,

BUNSEKI KAGAKU, 26 : 44 2-44 5.

77YAS 02 A. YASUI AND C. TSUTSUM1 ( 1977) ADAPTABILITY OF WET DECOMPOSITION METHOD TO FOOD SAMPLES

FOR THE DETERMINATION OF ARSENIC BY ARSINE GENERATION-ATOMIC

ABSORPTION SPECTROPHOTOMETRY, BUNSEKI KAGAKU, 26: 809-814.

77ZIK 01 I. ZIKOVSKY AND E. A. SCHWEIKERT ( 1977) COMPARISON OF NONDESTRUCTIVE PROTON AND NEUTRON ACTIVATION: THE CASE OF BIOLOGICAL SAMPLES, JOURNAL OF RADIOANALYTICAL

CHEMISTRY , 37: 571-580.

7 BALL 04 R. 0. ALLEN AND E. STEINNES (1978) DETERMINATION OF VANADIUM IN BIOLOGICAL MATERIALS BY RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS, ANALYTICAL

CHEMISTRY, 50: 1553-1555.

78BEA 01 R. D. BEATY ANDM. M. COOKSEY ( 1978) THE INFLUENCE OF FURNACE CONDITIONS ON MATRIX EFFECTS IN GRAPHITE FURNACE ATOMIC ABSORPTION, ATOMIC ABSORPTION

NEWSLETTER, 17: 53-58.

78BEH 01 D. BEHNE AND H. JURGENSEN (1978) DETERMINATION OF TRACE ELEMENTS IN HUMAN BLOOD SERUM AND IN THE STANDARD REFERENCE MATERIAL "BOVINE LIVER" BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 4 2: 447-4 53.

78BER 01 C. BERGERIOUX AND L. ZIKOVSKY (1978) INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF BREWER'S YEAST, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 47: 17 3-179.

78BER 02 C. BERGERIOUX AND L. ZIKOVSKY (19 78) DETERMINATION OF 18 TRACE ELEMENTS IN PETROLEUM AND ITS DERIVATIVES BY NEUTRON ACTIVATION WITH A SMALL NUCLEAR

REACTOR, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 46: 277-284.

78BYR 01 A. R. BYRNE AND L. KOSTA (1978) DETERMINATION OF VANADIUM IN BIOLOGICAL MATERIALS AT NANO- GRAM LEVEL BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 44: 247-264.

78CAM 02 J. A. CAMPBELL, J. C. LAUL, K. K. NIELSON, AND R. D. SMITH (1978) SEPARATION AND CHEMICAL CHARACTERIZATION OF FINELY-SIZED

FLY-ASH PARTICLES, ANALYTICAL CHEMISTRY, 50: 1032-1040.

78CAP 01 S. C. CAFAR, J. T. TANNER, M. H. FRIEDMAN, AND K. W. BOYER

(1978), MULTIELEMENT ANALYSIS OF ANIMAL FEED, ANIMAL WASTES, AND SEWAGE SLUDGE, ENVIRONMETAL SCIENCE AND TECHNOLOGY,

12: 785-790.

78CAR 01 M. B. CARVALHO AND D. M. HERCULES (1978) TRACE ARSENIC DETERMINATION BY VOLATILIZATION AND X-RAY

PHOTOELECT RON SPECTROSCOPY, ANALYTICAL CHEMISTRY,

50: 2030-2034.

78CAR 02 J.A. CARTER, D.L. DONOHUE, J.C. FRANKLIN, AND R.L. WALKER ( 1978) TRACE IMPURITIES IN COAL AND FLY ASH BY ISOTOPE DILUTION MASS SPECTROMETRY , PP. 4 03-4 20, IN 78KAR 01.

78CAR 03 B. S. CARPENTER, M. D. D'AGOSTINO, AND H. P. YULE (EDITORS) (1978) COMPUTERS IN ACTIVATION ANALYSIS AND GAMMA-RAY SPECTROSCOPY, PROCEDURES OF THE AMERICAN NUCLEAR SOCIETY, MAYAGUEZ, PUERTO

RICO, MAY 1978, CONF-780421.

78DAH 01 R. L. DAHLQUIST AND J. W. KNOLL (1978) INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY: ANALYSIS OF BIOLOGICAL MATERIALS AND SOILS FOR MAJOR, TRACE, AND ULTRA-TRACE ELEMENTS, APPLIED SPECTROSCOPY, 32: 1-29.

78DAV 01 P. H. DAVIS, G. R. DULUDE, R. M. GRIFFIN, W. R. MATSON, AND E. W. ZINK (1978) DETERMINATION OF TOTAL ARSENIC AT THE NANOGRAM LEVEL BY HIGH-SPEED ANODIC STRIPPING VOLTAMMETRY, ANALYTICAL

CHEMISTRY, 50: 137-143.

78DER 01 M. DERMELJ , J. NOVAK, V. RAVNIK, AND L. KOSTA ( 1978) RAPID DETERMINATION OF URANIUM AT THE NANOGRAM LEVEL IN GEOLOGICAL AMD BIOLOGICAL MATERIALS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 44 : 271-277.

78EDI 01 R. D. EDIGER, A. R. KNOTT, G. E. PETERSON, AND R. D. BEATY

(1978), THE DETERMINATION OF PHOSPHORUS BY ATOMIC ABSORPTION

USING THE GRAPHITE FURNACE, ATOMIC ABSORPTION NEWSLETTER,

17: 28-32.

78EGA 01 E. EGAAS AND K. JULSHAMN (1978)

A METHOD FOR THE DETERMINATION OF SELENIUM AND MERCURY IN FISH PRODUCTS USING THE SAME DIGESTION PROCEDURE, ATOMIC ABSORPTION NEWSLETTER, 17: 135-138.

78EPS 01 M. S. EPSTEIN, T. C. RAINS, T. J. BRADY, J. R. MOORE, AND

1. L. BARNES ( 1978), DETERMINATION OF SEVERAL TRACE METALS

IN SIMULATED FRESH WATER BY GRAPHITE FURNACE ATOMIC EMISSION

SPECTROMETRY, ANALYTICAL CHEMISTRY, 50: 874-880.

78EVA 01 W. H. EVANS, J. I. READ, AND B. E. LUCAS (1978) EVALUATION OF A METHOD FOR THE DETERMINATION OF TOTAL

CADMIUM, LEAD AND NICKEL IN FOODSTUFFS USING MEASUREMENT

BY FLAME ATOMIC-ABSORPTION SPECTROPHOTOMETRY,

ANALYST, 103: 580-591.

78FLA 01 J. FLANJAK (1978) ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF ARSENIC AND

SELENIUM IN OFFAL AND FISH BY HYDRIDE GENERATION, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 61: 1299-1303.

78FUD 01 N. FUDAGAWA AND A. KAWASE ( 1978) DETERMINATION OF NICKEL BY GRAPHITE TUBE FURNACE ATOMIC AB- SORPTION SPECTROMETRY; APPLICATION TO NICKEL DETERMINATION

IN PLANT MATERIALS, BUNSEKI KAGAKU, 27: 37-42.

78FUR 01 A. K. FURR, B. A. ROSCOE, AND T. F. PARKINSON (1978) VAT-69, A SOFTWARE SYSTEM FOR GAMMA SPECTROSCOPY

PP. 352-366, IN 78CAS 03.

78GAI 01 T. POWELL GAINES AND G. ALLEN MITCHELL (1978) SAMPLE PREPARATION BY COLUMN ELUTION FOR ELEMENTAL ANALYSIS

OF PLANT TISSUE, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 61: 1179-1181.

7 8 GAL 01 M. GALLORI NT , R. R. GREEN BE RG , AND T. E. GILLS (1978) SIMULTANEOUS DETERMINATION OF ARSENIC, ANTIMONY, CADMIUM, CHROMIUM, COPPER, AND SELENIUM IN ENVIRONMENTAL MATERIALS

BY RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS, ANALYTICAL

CHEMISTRY, 50: 1479-1481.

206
CODE N DESCRIPTION CODE N DESCRIPTION

78GAN 01 S. GANGADHARAN AND S. YEGNASUBRAMAN IAN ( 1978) ELEMENTAL CHARACTERIZATION THROUGH INSTRUMENTAL NEUTRON ACTIVATION, JOURNAL OF RADIOANALYTICAL CHEMISTRY

42: 455-462.

78GEL 01 R. GELADI AND F. ADAMS (1978) THE DETERMINATION OF CADMIUM, COPPER, IRON, LEAD AND ZINC IN AEROSOLS BY ATOMIC-ABSORPTION SPECTROMETRY , ANALYTICA

CHIMICA ACTA, 96: 229-241.

78GIL 01 T. E. GILLS, M. GAL LORI NT , AND H. L. ROOK ( 1978) THE DETERMINATION OF TRACE ELEMENTS IN NEW FOOD GRAIN SRM'S USING NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 46: 21-25.

78GLA 01 E. S. GLADNEY, W. K. HENSLEY, AND M. M. MINOR ( 1978) COMPARISON OF THREE TECHNIQUES FOR THE MEASUREMENT OF DEPLETED URANIUM IN SOILS, ANALYTICAL CHEMISTRY,

50: 652-653.

78GLA 02 E. S. GLADNEY ( 1978) DETERMINATION OF ARSENIC, ANTIMONY, MOLYBDENUM, THORIUM, AND

TUNGSTEN IN SILICATES BY THERMAL NEUTRON ACTIVATION AND

INORGANIC ION EXCHANGE , ANALYTICAL LETTERS, All: 429-4 35.

78GLA 04 E. S. GLADNEY, D. B. CURTIS, AND E. T. JURNEY ( 1978) MULTIELEMENT ANALYSIS OF MAJOR AND MINOR ELEMENTS BY THERMAL NEUTRON INDUCED CAPTURE GAMMA-RAY SPECTROMETRY, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 46: 299-308.

78G0E 01 J.J.M. DE GOEIJ, K.J. VOLKERS , P.S. TJIOE, AND J.J. KROON (1978)

NBS SRM 1569 BREWER'S YEAST: IS IT AN ADEQUATE STANDARD REFERENCE MATERIAL FOR TESTING A CHROMIUM DETERMINATION IN BIOLOGICAL MATERIALS? , RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 35: 139-146.

f8G0R 01 D. T. GORDON (1978) ATOMIC ABSORPTION SPECTROMETRIC AND COLORIMETRIC DETERMINATION OF IRON IN SEAFOODS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 61: 715-719.

78GRO 01 Z. GROBENSKI, M. MELCHER, AND B. WELZ (1978) RICHTIGKEIT BE I DER BESTIMMUNG VON SPURENELEMENTEN IN LEBENSMITTELN MIT DER GRAPH ITROHRTECHNIK AAS, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 290: 144-145.

78GUI 01 R. J. GUIDOBONI (1978) SPARK SOURCE MASS SPECTROMETRY AND ATOMIC ABSORPTION SPEC- TROMETRY FOR THE DETERMINATION OF TRACE ELEMENTS IN COAL,

PP. 421-4 34 , IN 78KAR 01.

78HAY 01 B. W. HAYNES (1978) ELECTROTHERMAL ATOMIC ABSORPTION DETERMINATION OF ARSENIC AND ANTIMONY IN COMBUSTABLE MUNICIPAL SOLID WASTE, ATOMIC ABSORPTION NEWSLETTER, 17: 49-52.

78HIR 01 S. HIRAI, S. SUZUKI, AND M. OKAMOTO (1978) DETERMINATION OF SELENIUM IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS USING SE-77M, BUNSEKI KAGAKU, 27 : 4 35-4 39.

78HIS 01 J.S. HISLOP (1978) GAMMA ACTIVATION ANALYSIS : AN APPRAISAL , PROCEEDINGS OF THE

ANALYTICAL DIVISION OF THE CHEMICAL SOCIETY (LONDON), 15: 193-205.

78JAC 01 C.J. JACKSON, D.G. PORTER, A.L. DENNIS AND P.B. STOCKWELL

(1978) AUTOMATED DIGESTION AND EXTRACTION APPARATUS FOR USE

IN THE DETERMINATION OF TRACE METALS IN FOODSTUFFS

ANALYST, 103: 317-331.

78JOL 01 R. K. JOLLY, J. R. KANE, D. C. BUCKLE , G. RANDERS-PEHRSON

W. TEOH, AND H. ACETO (1978), A TARGET CHAMBER FOR PIXE

ANALYSIS USING MICROAMPERE BEAMS OF 4 MEV PROTONS

NUCLEAR INSTRUMENTS AND METHODS, 151: 183-188.

78KAR 01 C. KARR, JR. (EDITOR) (19 78) ANALYTICAL METHODS FOR COAL AND COAL PRODUCTS, VOLUME 1, ACADEMIC PRESS, NEW YORK.

78KAT 01 K. KATO (1978) UNPUBLISHED DATA, QUOTED IN 78MAS 01.

78KEL 02 M. T. KELLEY, J. E. RILEY, JR. AND G. GLEASON (1978) NAALSQ: A PROGRAM FOR NEUTRON ACTIVATION ANALYSIS WITH LEAST

SQUARES DECONVOLUTION OF THE GAMMA SPECTRA ON A MINICOMPUTER

PP. 4 56-464, IN 78CAR 03.

78KNO 01 A. C. KNOTT, J. C. MILLS AND C. B. BELCHER (1978) SYNTHETIC CALIBRATION STANDARDS FOR OPTICAL EMISSION AND

X-RAY SPECTROMETRY, CANADIAN JOURNAL OF SPECTROSCOPY, 23: 105-111.

78KOB 01 K. KOBAYASHI AND K. KUDO (1978) DETERMINATION OF INDIUM, COPPER, AND NICKEL IN GLASSMAKING MATERIALS AND NBS STANDARD REFERENCE MATERIALS BY SUBSTOICHIOMETRIC RADIOACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 46: 265-276.

78KOR 01 G. A. KORBA AND E. S. YEUNG ( 1978) APPLICATION OF FABRY-PEROT INTERFEROMETRY IN MULTI-ELEMENT

FLAME EMISSION ANALYSIS, ANALYTICA CHIMICA ACTA, 99: 209-216.

78KUB 01 H. KUBO, R. BERNTHAL, AND T. R. WILDEMAN ( 19 78) ENERGY DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRIC

DETERMINATION OF TRACE ELEMENTS IN OIL SAMPLES, ANALYTICAL CHEMISTRY, 50: 899-903.

78KUB 02 T. KUBOTA AND T. UEDA (1978) ATOMIC ABSORPTION SPECTROPHOTOMETRIC DETERMINATION OF ANTI- MONY WITH USE OF BOROHY ERI DE SOLUTION AS REDUCTANT, BUNSEKI KAGAKU, 27: 692-696.

78LAU 02 J.C. LAUL, C.L. WILKERSON, ANDV.L. CROW (1978) COMPUTER METHODOLOCY AND ITS APPLICATIONS TO GEOLOGICAL AND

ENVIRONMENTAL MATRICES, PP. 84 0-856, IN 78CAR 03.

78LIN 01 H. R. LINDER, H. D. SELTNER, AND B. SCHREIBER ( 1978) USE OF DIBENZYLDITHIOC ARBAMI NATE AS COPRECIPITANT IN THE ROUTINE DETERMINATION OF 12 HEAVY METALS IN PHARMACEUTICALS

BY X-RAY FLUORESCENCE SPECTROSCOPY, ANALYTICAL CHEMISTRY,

50: 896-899.

78MAC 01 K. W. MACHURDO AND W. W. BOWMAN ( 1978) AUTOMATED ABSOLUTE ACTIVATION ANALYSIS WITH CALIFORNIUM-252

SOURCES, REPORT DP-14 57, SAVANNAH RIVER LABORATORY, E. I. DUPONT DE NEMOURS AND COMPANY.

78MAS 01 K. MASUMOTO AND N. SUZUKI (1978) SELECTIVE COINCIDENCE SPECTROMETRY IN THE NONDESTRUCTIVE

DETERMINATION OF NICKEL IN GEOLOGICAL MATERIALS WITH HIGH ENERGY PHOTON ACTIVATION, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 46: 121-135.

78MAT 01 M. MATTHES, R. FLUCHT, AND M. STOEPPLER ( 1978)

BE I TRACE ZUR AUTOMATISIERTEN SPURENANALYSE, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 291 : 20-26.

78MCC 01 L. T. MCCLENDON (1978) DETERMINATION OF CHROMIUM IN BIOLOGICAL MATRICES BY NEUTRON

ACTIVATION: APPLICATION TO STANDARD REFERENCE MATERIALS, JOURNAL OF RADIOANALYTICAL CHEMISTRY ,4 2 : 85-91 .

78MCG 01 J. R. MCGINLEY, G. J. STOCK, E. A. SCHWEIKERT, J. B. CROSS,

R. ZEISLER, AND L. ZIKOVSKY (1978), NUCLEAR AND ATOMIC ACTIVATION WITH HEAVY ION BEAMS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 43: 559-573.

78MCK 01 D. M. MCKOWN AND J. S. MORRIS (1978) RAPID MEASUREMENT OF SELENIUM IN BIOLOGICAL SAMPLES USING INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 4 3: 411-4 20.

78M0R 01 A. E. MORGAN AND H. W. WERNER (19 78) SEMIQUANTITATIVE ANALYSES BY SECONDARY ION MASS SPECTROMETRY

USING ONE FITTING PARAMETER, MIKROCHIMICA ACTA (WIEN), 1978 II: 31-50.

78NAD 01 R. A. NADKARNI AND G. H. MORRISON (1978) DETERMINATION OF MOLYBDENUM BY NEUTRON ACTIVATION AND

SRAFION NMRR ION EXCHANGE RESIN SEPARATION, ANALYTICAL CHEMISTRY, 50: 294-296.

78NAD 02 R. A. NADKARNI AND G. H. MORRISON ( 1978) USE OF STANDARD REFERENCE MATERIALS AS MULTIELEMENT

IRRADIATION STANDARDS IN NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 4 3: 347-369.

207
CODE N DESCRIPTION

CODE N DESCRIPTION

78NAK 01 R. NAKASHIMA (19 78) UHF-PLASMA TORCH EMISSION SPECTROMETRY FOR CADMIUM, LEAD AND

ZINC BY VAPORIZATION INTRODUCTION, BUNSEK1 KAGAKU, 27: 199-203.

78PEL 01 P. A. PELLA, K. E. LORBER, AND K. F. J. REINRICH ( 1978) ENERGY- DISPERSIVE X-RAY SPECTROMETRIC ANALYSIS OF ENVIRONMENTAL SAMPLES AFTER BORATE FUSION, ANALYTICAL

CHEMISTRY, 50i 1268-1271.

7BPIE 01 Z. PIETRZAK-FL IS , G. L. REHNBERC, M. J. FAVOR, D. F. C AH ILL, AND J. W. LASKEY (1978), CHRONIC INGESTION OF CADMIUM AND/OR TRITIUM IN RATS I. ACCUMULATION AND DISTRIBUTION OF CADMIUM

IN TWO GENERATIONS, ENVIRONMENTAL RESEARCH , 16 1 9-17.

7BRIT 01 C. J. RITTER, S. C. BERGMAN, C. R. COTHERN , AND E. E. ZAM1ER0WSKI (1978), COMPARISON OF SAMPLE PREPARATION

TECHNIQUES FOR ATOMIC ABSORPTION ANALYSIS OF SEWAGE SLUDGE AND SOIL, ATOMIC ABSORPTION NEWSLETTER, 17 : 70-72.

78RYA 01 D. E. RYAN , D. C. STUART, AND A. CHATTOPADHYAY (1978) RAPID MULTIELEMENT NEUTRON ACTIVATION ANALYSIS WITH A SLOWPOKE REACTOR, ANALYTICA CHIMICA ACTA, 100: 87-93.

78SIE 01 D. D. SIEMER AND H. WEI (1978) DETERMINATION OF LEAD IN ROCKS AND GLASSES BY TEMPERATURE

CONTROLLED GRAPHITE CUP ATOMIC ABSORPTION SPECTROMETRY, ANALYTICAL CHEMISTRY, 50: 147-151.

78SMI 01 R. G. SMITH (1978) SOURCES OF COPPER AND CADMIUM CONTAMINATION IN SMALL BIOLOGICAL SAMPLES, TALANTA, 25: 173-175.

78SUD 01 R. F. SU DDENDORF AND R. W. BOYER (1978) NEBULIZER FOR ANALYSIS OF HIGH SALT CONTENT SAMPLES WITH

INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 50: 1769-1771.

78SUG 01 A. SUCIMAE AND R. K. SKOGERBOE (1978)

DUAL APPROACH TO THE EMISSION SPECTROGRAPHIC DETERMINATION

OF ELEMENTS IN AIRBORNE PARTICULATE MATTER, ANALYTICA

CHIMICA ACTA, 97: 1-11.

78SUG 02 A. SUGIMAE ( 1978) DETERMINATION OF TRACE AMOUNTS OF RARE EARTH ELEMENTS IN VARIOUS ENVIRONMENTAL SAMPLES BY SPARK SOURCE MASS SPECTROGRAPHY, BUNSEKI KAGAKU, 27: 169-174.

78SZY 01 F. J. SZYDLOWSKI (1978) USE OF BRANCH CAPILLARY FOR IONIZATION BUFFER ADDITION IN FLAME ATOMIC ABSORPTION SPECTROMETRI C DETERMINATION OF SODIUM AND POTASSIUM IN FOOD PRODUCTS, ATOMIC ABSORPTION

NEWSLETTER, 17 : 65-69.

78TAK 01 T. TAKAMATSU (1978) MULTI-ELEMENT ANALYSES OF ROCK AND SEDIMENT SAMPLES BY NON- DISPERSIVE X-RAY FLUORESCENCE, BUNSEKI KAGAKU, 27: 193-198.

78TER 01 S. TERASHIMA (1978) RAPID DETERMINATION OF TOTAL CARBON AND SULFUR IN GEOLOGICAL MATERIALS BY COMBUSTION AND INFRARED ABSORPTION

PHOTOMETRY, ANALYTICA CHIMICA ACTA, 101: 25-31.

78TSU 01 K. TSUNODA, K. FUJIWARA, AND K. FUWA (1978) DETERMINATION OF CHLORINE AND BROMINE BY MOLECULAR

ABSORPTION OF ALUMINIUM MONOHALIDES AT HIGH TEMPERATURE, ANALYTICAL CHEMISTRY, 50: 861-865.

78UEM 01 Y.J. UEMURA, Y. KUNO, H. KOYAMA, T. YAMAZAKI , AND P. KIENLE (19 A NEW WAY OF DETERMINING CONCENTRATIONS IN P.I.X.E. TRACE ELEMENT ANALYSIS, NUCLEAR INSTRUMENTS AND METHODS, 153: 573-579.

78URE 01 A. M. URE AND J. R. BACON (1978) SCANDIUM, YTTRIUM, AND RARE EARTH CONTENT OF WATER LILY

,

GEOCHIMICA ET COSMOCHIMICA ACTA, 42: 651-652.

7 SURE 02 A. M. URE, M. P. HERNANDEZ-ARTIGA, AND M. C. MITCHELL (1978) A CARBON-ROD ATOMIZER FOR THE DETERMINATION OF CADMIUM AND

LEAD IN PLANT MATERIALS AND SOIL EXTRACTS, ANALYTICA CHIMICA

ACTA, 96: 37-4 3.

78VAL 01 I. VALENTE, M. J. MINSKI, AND H. J. M. BOWEN ( 1978) RAPID DETERMINATION OF ANTIMONY IN BIOLOGICAL AND ENVIRON- MENTAL SAMPLES USING INSTRUMENTAL NEUTRON ACTIVATION

ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 45: 4 17-421.

78VIS 01 R. D. VIS, K. J. WIEDERSPAHN, AND H. VERHEUL ( 1978) THE DETERMINATION OF THE ELEMENTAL COMPOSITION OF GLASSES

FOR FORENSIC APPLICATION USING A COMBINATION OF PROTON

INDUCED X-RAY EMISSION AND INELASTIC PROTON SCATTERING, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 4 5: 4 07-416.

78WAN 01 L. E. WANGEN AND E. S. GLADNEY ( 1978)

IE TERMINATION OF ARSENIC AND GALLIUM IN STANDARD MATERIALS

BY INSTRUMENTAL EPITHERMAL NEUTRON ACTIVATION ANALYSIS, ANALYTICA CHIMICA ACTA, 96: 271-277.

78WEA 01 J. N. WEAVER ( 19 78) NEUTRON ACTIVATION ANALYSIS OF TRACE ELEMENTS IN COAL, FLY

ASH, AND FUEL OILS, PP. 377-401 , IN 78KAR 01.

78WEE 01 C. A. WEERS, K. HOEDE, AND H. A. DAS (1978) APPLICATION OF SELECTIVE EVAPORATION IN THE DETERMINATION OF ARSENIC AND BROMINE IN DRY BIOLOGICAL MATERIAL BY THERMAL

NEUTRON ACTIVATION ANALYSIS , JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 42: 113-119.

78WEC 01 W. WEGSCHEIDER, K. E. LORBER, AND K. MULLER ( 1978) QUANTITATIVE INTERMETHOD COMPARISON OF ENERGY DISPERSIVE X-RAY FLUORESCENCE AND ATOMIC ABSORPTION SPECTROMETRY FOR

THE ANALYSIS OF URBAN DUSTS AND FLY ASH, INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 5: 171-187.

78WEL 01 B. WELZ AND M. MELCHER (1978) BESTIMMUNG VON ARSEN UND SELEN IN KORPERFLUSSIGKEITEN UND

GEWEBEN MIT DER HY DRI D-METHODE , FRESEN IUS ZEITSCRHIFT FUR ANALYTISCHE CHEMIE, 290: 106-107.

79ABE 01 F. N. ABERCROMBIE, M. D. SILVESTER, AND R. B. CRUZ (1979) SIMULTANEOUS MULTIELEMENT ANALYSIS OF BIOLOGICALLY RELATED

SAMPLES WITH RF-ICP, PP 10-25, IN 79RIS 01.

79ABO 01 M. D. K. ABO-RADY (1979) SCHWERMETALLBESTIMMUNG IN ZWEI BIOLOGISCHEN UND ZWEI GEOLOGISCHEN STANDARDS MIT HILFE DER ATOM-ABSORPTIONS

SPECTROSKOPIE, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE,

296: 380-382.

79ABU 01 J. ABUKAWA, H. HIGUCHI, K. SATO, S. BAN DO, AND H. HAMAGUCHI (1979) A COMPARISON OF VARIOUS METHODS FOR DETERMINATION OF COBALT

IN MARINE BIOLOGICAL MATERIALS, BUBSEKI KAGAKU, 28: 506-508.

79AHM 01 S. AHMAD, M. S. CHAUDHRY, AND I. H. QURESHI ( 1979) DETERMINATION OF TOXIC ELEMENTS IN TOBACCO PRODUCTS BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 54 : 331-341.

79AND 01 D.L. ANDERSON, M.P. FAILEY, W.H. ZOLLER, ETAL (1979) NEUTRON-CAPTURE PROMPT GAMMA-RAY ACTIVATION ANALYSIS: MULTI-ELEMENT MEASUREMENTS ON VARIOUS MATERIALS, PP. 546-

548, IN 79CHR 01.

79BAR 03 R. M. BARNES (EDITOR) (1979) APPLICATIONS OF PLASMA EMISSION SPECTROCHEMISTRY, HEY DEN

,

PHILADELPHIA.

79BEN 01 G. E. BENTLEY, L. MARKOWITZ, AND R. MEGLEN (1979) ANALYSIS OF MOLYBDENUM IN BIOLOGICAL MATERIALS, PP 35-39, IN 79RIS 01.

79BLO 01 A. J. BLOTCKY, C. FALCONE , V. A. MEDINA, E. P. RACK, AND

D. W. HOBSON (1979) DETERMINATION OF TRACE-LEVEL VANADIUM IN MARINE BIOLOGICAL

SAMPLES BY CHEMICAL NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY, 51: 178-182.

79BOG 01 S. L. BOGDANSKI, I. SHAKIR, W. E. STEPHEN, AND A. TOWNSHEND

( 19 79), DETERMINATION OF TRACE AMOUNTS OF SULPHATE BY MOLECULAR EMISSION CAVITY ANALYSIS USING A VAPORISATION

SYSTEM , ANALYST, 104: 886-890.

79BRA 01 F. P. BRAUER AND R. S. STREBIN (1979)

IN NUCLEAR ACTIVATION TECHNIQUES IN THE LIFE SCIENCES, IAEA, VIENNA, P. 27; TAKEN FROM 80GVA 01.

208
CODE N DESCRIPTION CODE N DESCRIPTION

79BRE 01 J. J. LA BRECQUE (1979) INTERFERENCES IN THE DETERMINATION OF TITANIUM IN SILICATE

ROCKS AND VENEZUELAN LATERITES BY ATOMIC ABSORPTION

SPECTROSCOPY, APPLIED SPECTROSCOPY, 33: 389-393.

79BRE 02 J. J. LA BRECQUE (1979) DECOMPOSITION AND DETERMINATION OF ALUMINIUM AND SILICON IN VENEZUELAN LATERITES BY ATOMIC ABSORPTION SPECTROSCOPY, CHEMICAL GEOLOGY, 26: 321-329.

79BRI 02 C. BR I HAYE ( 19 79) ANALYSE DE TRACES PAR LA METHODE ELECT ROCHIMIQUE UTILISANT

UNE ELECTRODE DISQUE-ANNEAU , DOCTORAL THESIS, UNIVERSITY OF LIEGE, BELGIUM.

79BYR 01 A. R. BYRNE (1979) EXTRACTION OF SOME TRACE ELEMENTS AS IODIDES WITH METHYLISOBUTYL KETONE AND ITS APPLICATION IN NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 40: 1-16.

79CAH 01 R. A. CAH ILL (1979) PRIVATE COMMUNICATION , ILLINOIS STATE GEOLOGICAL SURVEY.

79CHA 02 A. CH ATTOPADHYAY , K. M. ELLIS, AND K. N. DE SILVA (1979)

IN NUCLEAR ACTIVATION TECHNIQUES IN THE LIFE SCIENCES,

IAEA, VIENNA, PP. 667-682, IN 79IAE 01.

79CHA 04 A. CHATTOPADHYAY AND K. N. DE SILVA ( 1979) PSEUDO-CYCLIC NEUTRON ACTIVATION ANALYSIS OF AG, F, RB,

SC, AND SE IN BIOLOGICAL SAMPLES, TRANSACTIONS OF THE

AMERICAN NUCLEAR SOCIETY, 32: 185-186.

79CHR 01 R. E. CHRIEN AND W. R. KANE (EDITORS) (1979) NEUTRON CAPTURE GAMMA RAY SPECTROSCOPY, PLENUM PRESS, NEW YORK.

79COO 01 M. COOKSEY AND W. B. BARNETT ( 1979) SEQUENTIAL MULTIELEMENT ATOMIC ABSORPTION ANALYSIS OF AGRICULTURAL SAMPLES, ATOMIC ABSORPTION NEWSLETTER, 18: 1-4.

79COR 01 R. CORNELIS, L. MEES, J. HOSTE, J. RYCKENBUSCH, J. VERSIECK, AND F. BARBIER ( 19 79), IN NUCLEAR TECHNIQUES IN THE LIFE SCIENCES 1978, IAEA, VIENNA, P. 165, FROM REF 80HEY 01.

79CRO 01 J. D. CROSS AND H. SMITH ( 1979) THE DETERMINATION OF BROMINE IN BIOLOGICAL MATERIAL BY THERMAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 48: 191-196. 79MB 01 R. W. DABEKA, A. D. MCKENZIE, AND H. CONACHER ( 1979) MICRODIFFUSION AND FLUORIDE-SPECIFIC ELECTRODE DETERMINATION OF FLUORIDE IN FOODS , JOURNAL OF THE

ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 62: 1065-1068.

79DAB 02 R. W. DABEKA ( 1979) GRAPHITE-FURNACE ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF LEAD AND CADMIUM IN FOODS AFTER SOLVENT

EXTRACTION AND STRIPPING , ANALYTICAL CHEMISTRY, 51 : 902-907.

79 DAL 01 L. S. DALE (1979) THE EMISSION SPECTROCRAPHIC DETERMINATION OF BORON IN SILICATE MATERIALS, APPLIED SPECTROSCOPY, 33: 404-406.

79DAS 01 H. A. DAS, A. FAANHOF, AND H. A. VAN DER SLOOT ( 1979) ERRORS IN INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS:

I. DETERMINATION OF THE PEAK AREA, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 54: 289-301.

79DER 01 M. DERMELJ, A. VAKSELJ, V. RAVNTK, MD B. SMODIS (1979) APPLICABILITY OF CARBAMATE EXTRACTION TO RADIOCHEMICAL

SEPARATION AND DETERMINATION OF CADMIUM, COBALT, COPPER, AND ZINC IN VARIOUS BIOSPHERE SAMPLES, RADIOCHEMICAL AND

RADIOANALYTICAL LETTERS, 41: 149-160.

79DES 01 H. B. DESAI , R. K. IYER, AND S. R. KAYASTH (1979) PRECIPITATION OF MERCURY AS ZINC MERCURO THIOCYANATE, APPLICATION TO ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 41: 299-306.

79DOG 01 S. DOCAN AND W. HAERDI (1979) RAPID SEPARATION ON COPPER POWDER OF TOTAL MERCURY IN BLOOD AND DETERMINATION OF MERCURY BY FLAMELESS ATOMIC ABSORPTION, INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY,

6: 327-T14.

79ED1 01 R. D. EDIGER AND D. L. WILSON (1979) THE PERFORMANCE OF AN INDUCTIVELY COUPLED PLASMA ON THE

MODEL 5000 ATOMIC ABSORPTION SPECTROPHOTOMETER, ATOMIC ABSORPTION NEWSLETTER, 18: 41-4 5.

79EPS 01 M. S. EPSTEIN, S. NIK DEL, N. OHENETTO; R. REEVES,

J. BRADSHAW, AND J. D. WINEFORDNER (1979) INDUCTrVKLY-COUPLED ARGON PLASMA AS AN EXCITATION SOURCE FOR FLAME ATOMIC FLUORESCENCE SPECTROMETRY, ANALYTICAL CHEMISRTY , 51: 2071-2077.

79EPS 03 M. S. EPSTEIN AND A. T. ZANDER (1979) DIRECT DETERMINATION OF BARIUM IN SEA AND ESTUARINE WATER BY GRAPHITE FURNACE ATOMIC SPECTROMETRY, ANALYTICAL CHEMISTRY

51: 915-918.

79EVA 01 W. H. EVANS, F. J. JACKSON, AND D. DELLAR (1979) EVALUATION OF A METHOD FOR DETERMINATION OF TOTAL ANTIMONY, ARSENIC AND TIN IN FOODSTUFFS USING MEASUREMENT BY ATOMIC- ABSORPTION SPECTROPHOTOMETRY WITH ATOMISATION IN A SILICA

TUBE USING THE HYDRIDE GENERATION TECHNIQUE, ANALYST,

104: 16-30.

79FAA 01 A. FAANHOF AND H. A. DAS (1979) ANALYSIS OF TOBACCO BY INSTRUMENTAL EPITHERMAL NEUTRON ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 41: 367-374.

79FAI 01 M. P. FAILEY, D. L. ANDERSON, W. H. ZOLLER, G. E. GORDON, AND R. M. LINDSTROM (1979) NEUTRON-CAPTURE PROMPT GAMMA-RAY ACTIVATION ANALYSIS FOR MULTIELEMENT DETERMINATION IN COMPLEX SAMPLES, ANALYTICAL CHEMISTRY, 51: 2209-2221.

79FEL 01 C. FELDMAN ( 1979) IMPROVEMENTS IN THE ARSINE ACCUMULATION-HELIUM GLOW

DETECTOR PROCEDURE FOR DETERMINING TRACES OF ARSENIC, ANALYTICAL CHEMISTRY, 51: 664-669.

79FLA 02 J. FLANJAK AND H. Y. LEE (1979) TRACE METAL CONTENT OF LIVERS AND KIDNEYS OF CATTLE, JOURNAL OF SCIENCE AND FOOD AGRICULTURE, 30: 503-507.

79GEL 01 P. GELADI AND F. ADAMS ( 1979) THE DETERMINATION OF BERYLLIUM AND MANGANESE IN AEROSOLS BY ATOMIC ABSORPTION SPECTROMETRY WITH ELECTROTHERMAL

ATOMIZATION, ANALYTICA CHIHICA ACTA, 105: 219-231.

79GIA 01 R. D. CIAUQUE, R. B. GARRETT, AND L. Y. GODA (1979) DETERMINATION OF TRACE ELEMENTS IN LIGHT ELEMENT MATRICES

BY X-RAY FLUORESCENCE SPECTROMETRY WITH INCOHERENT SCATTERED RADIATION AS AN INTERNAL STANDARD, ANALYTICAL CHEMISTRY, 51: 511-516.

79GIA 03 R. D. CIAUQUE (1979) PRIVATE COMMUNICATION, LAWRENCE BERKELEY LABORATORY.

79GLA 02 E. S. GLADNEY AND D. R. PERRIN (1979) DETERMINATION OF BROMINE IN BIOLOGICAL, SOIL, AND GEOLOGICAL STANDARD REFERENCE MATERIALS BY INSTRUMENTAL EPITHERMAL

NEUTRON ACTIVATION, ANALYTICAL CHEMISTRY, 51: 2015-2018.

79GLA 03 E. S. GLADNEY AND D. R. PERRIN (1979) QUANTITATIVE ANALYSIS OF SILICATES BY INSTRUMENTAL EPITHERMAL NEUTRON ACTIVATION USING (N,P) REACTIONS, ANALYTICAL CHEMISTRY, 51: 2297-2300.

79GLA 04 E. S. GLADNEY, D. B. CURTIS, AND E. T. JURNEY (1979) SIMULTANEOUS DETERMINATION OF NITROGEN, CARBON, AND HYDROGEN

BY THERMAL NEUTRON PROMPT GAMMA-RAY SPECTROMETRY, ANALYTICA CHIMICA ACTA, 110 : 339-34 3.

79GRE 01 R. R. GREENBERG (1979) TRACE ELEMENT CHARACTERIZATION OF THE NBS URBAN PARTICULATE MATTER STANDARD REFERENCE MATERIAL BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY, 51: 2004-2006.

79HEC 01 M. M. HECKMAN (1979) ANALYSIS OF FOODS FOR IODINE: INTERLABORATORY STUDY, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS,

62: 1045-1048.

209
CODE N DESCRIPTION

79HE1 01 H. HEI rJRICHS ( 1979) DETERMINATION OF BISMUTH, CADMIUM. AND THALLIUM IN 33 INTERNATIONAL STANDARD REFERENCE ROCKS BY FRACTIONAL

DISTILLATION COMBINED WITH FLAMELESS ATOMIC ABSORPTION

SPECTROMETRY, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE,

294: 34 5-351.

79HEI 03 H. HE1NRICHS (1979) DETERMINATION OF LEAD IN GEOLOGICAL AND BIOLOGICAL MATERIALS

BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 295: 355-361.

79HER 01 J. L. HERN (1979) ELEMENTAL ANALYSIS IN AGRICULTURE USING INDUCTIVELY COUPLED

PLASMA-ATOMIC EMISSION SPECTROSCOPY, IN 79BAR 03.

79HIL 01 E. P. HILL1ARD AND J. D. SMITH (1979) MINIMUM SAMPLE PREPARATION FOR THE DETERMINATION OF TEN ELE- MENTS IN PIG FAECES AND FEEDS BY ATOMIC-ABSORPTION SPECTRO- PHOTOMETRY AND A SPECTROPHOTOMETRIC PROCEDURE FOR TOTAL PHOSPHORUS , ANALYST, 104: 313-322

79HOE 01 D. HOEDE AND H. A. VAN DER SLOOT (1979) APPLICATION OF HYDRIDE GENERATION FOR THE DETERMINATION OF ANTIMONY AND ARSENIC IN BIOLOGICAL MATERIAL BY NEUTRON ACTIVATION ANALYSIS, ANALYTICA CHIMICA ACTA, 111: 321-325.

79HOE 02 M. HOENIC, P. VAN HOEYVEGHEN ET J. LIBOTON (1979) EVALUATION A L'AIDE D'ETALONS INTERNATIONAUX DE DEUX

ME THODES DE MINERALISATION DES VEGETAUX , ANALUSIS, 7: 104-106.

79IAE 01 PROCEEDINGS OF AN INTERNATIONAL SYMPOSIUM ON NUCLEAR

ACTIVATION TECHNIQUES IN THE LIFE SCIENCES HELD BY THE IAEA IN VIENNA, MAY 1978, STI/PUB/492, ISBN 92-0-010079-1.

79IMA 01 A. IMAHORI, I. FUKUSHIMA, S. SHIOBARA, Y. YANACIDA, AND

K. TOMURA (1979) MULTIELEMENT NEUTRON ACTIVATION ANALYSIS OF HUMAN SCALP HAIR A LOCAL POPULATION SURVEY IN THE TOKYO METROPOLITAN

AREA, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 52: 167-180.

79IMA 03 A. IMAHORI, I. FUKUSHIMA, S. SHIOBARA, K. TOMURA,

M. SUZUKI-YASUMOTO, M. YUKAWA, M. TERAI (1979) A STUDY OF TRACE ELEMENT CONCENTRATIONS IN HUMAN HAIR OF SOME LOCAL POPULATIONS IN JAPAN, PP. 563-571, IN 79IAE 01.

79INU 01 T. INUI, N. FU DAGAWA , AND A. KAWASE (1979) EXTRACTION AND ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION

OF BISMUTH WITH ELECTROTHERMAL ATOMIZATION, FRESENIUS

ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 299: 190-193.

79JER 01 R. E. JERVIS, AND B. TIEFENBACH (1979) ARSENIC ACCUMULATION IN PEOPLE WORKING WITH AND LIVING NEAR A GOLD SMELTER, PP. 627-642, IN 79IAE 01.

79JON 01 J. D. JONES, P. B. KAUFMAN, AND W. L. RIGOT (1979) METHOD FOR DETERMINATION OF SILICON IN PLANT MATERIALS

BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 50: 261-275.

79KAN 02 Y. KAN DA AND N. SUZUKI (1979) REDOX SUBSTOICHIOMETRIC DETERMINATION OF ARSENIC IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 54: 7-14.

79KNE 01 J. R. KNECHTEL AND J. L. FRASER (1979) WET DIGESTION METHOD FOR THE DETERMINATION OF MERCURY IN BIOLOGICAL AND ENVIRONMENTAL SAMPLES, ANALYTICAL CHEMISTRY,

51: 315-317.

79KOB 01 K. KOBAYASHI AND K. KUDO (1979) RAPID DETERMINATION OF INDIUM, NICKEL, AND COPPER IN NBS STANDARD REFERENCE MATERIAL BY SUBSTOICHIOMETRIC RADIO- ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

54 : 49 -58.

79KOB 03 R. KOBAYASHI AND K. KUDO (1979) DETERMINATION OF MULTIELEMENT IN OPTICAL WAVEGUIDE AND

STANDARD REFERENCE MATERIALS BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

53 : 233-246.

CODE N DESCRIPTION

79KRA 01 J. A. KRASOWSKI AND T. R. COPELAND ( 1979) MATRIX INTERFERENCES IN FURNACE ATOMIC ABSORPTION

SPECTROMETRY , ANALYTICAL CHEMISTRY, 51: 184 3-1849.

79KUC 01 J. KUCERA (1979) EPITHERMAL NEUTRON ACTIVATION ANALYSIS OF TRACE ELEMENTS IN BIOLOGICAL MATERIALS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 38 : 2 29 -24 6.

79KUE 01 E. C. KUEHNER AND P. A. PELLA (19 79) ENERGY- DISPERSIVE X-RAY SPECTROMETRIC ANALYSIS OF NBS STANDARD REFERENCE MATERIAL 1571 ORCHARD LEAVES AFTER OXIDATION AND BORATE FUSION, APPLIED SPECTROSCOPY,

33: 632-634.

79LAK 01 E.-L. LAKOMAA AND P. EKLUND (1979) TRACE ELEMENT ANALYSIS OF HUMAN CATARACTOUS LENSES BY NEUTRON ACTIVATION ANALYSIS AND ATOMIC ABSORPTION SPECTRO- METRY, PP. 333-343, IN 79IAE 01.

79LDC 01 W. LTKUSSAR ( 19 79) UNTERSUCHUNGEN UBER DAS MORPHOLIN-N- DITHI O-CARBONSAURE MOR- PHOLINIUM (MDCM) ALS REAGENS IN DER QUANTITATIVEN ANALYTIK X MIKROCHIMICA ACTA (WIEN), 1979,11: 43-52.

79LOC 01 J. LOCKE ( 1979) THE DETERMINATION OF EIGHT ELEMENTS IN HUMAN LIVER TISSUE BY FLAME ATOMIC ABSORPTION SPECTROMETRY IN SULPHURIC ACID

SOLUTION, ANALYTICA CHIMICA ACTA, 104: 225-231.

79LPI 01 LUNAR AND PLANETARY INSTITUTE ( 1979) PROCEEDINGS OF THE TENTH LUNAR AND PLANETARY SCIENCE

CONFERENCE, HOUSTON, TEXAS , MARCH 19-23, 1979: GEOCHIMICA

ET COSMOCHIMICA ACTA SUPPLEMENT 11.

79MAN 01 N. F. MANGELSON, M. W. HILL, K. K. NEILSON, D. J. EATOUGH

J. J. CHR1STENSEN , R. M. IZATT, AND D. 0. RICHARDS ( 1979) PROTON INDUCED X-RAY EMISSION ANALYSIS OF PIMA INDIAN AUTOPSY TISSUES, ANALYTICAL CHEMISTRY, 51: 1187-1194.

79MAT 01 K. MATSUMOTO AND K. FUWA (1979) MAJOR AND TRACE ELEMENTS DETERMINATION IN GEOLOGICAL AND

BIOLOGICAL SAMPLES BY ENERGY- DISPERSIVE X-RAY FLUORESCENCE

SPECTROMETRY , ANALYTICAL CHEMISTRY, 51 : 2355-2358.

79MAT 02 T. D. MATHEWS , J. V. BOYNE, R. A. DAVIS, AND D. R. SIMMONS

( 1979), THE DISTRIBUTION OF COPPER AND IRON IN SOUTH CAROLINA OYSTERS, JOURNAL OF ENVIRONMENTAL SCIENCE AND

HEALTH, A14 : 683-694

79MAY 01 S. MAY AND D. PICCOT (19 79) DOSAGE DE TRACES D'ELEMENTS TOXIQUES (AS, CD, HG, SB, SE) DANS LES PROTEINES SYNTHETIQUES , PAR RADIOACTIVATION

NEUTRONIQUE , ANALUSIS, 7: 133-137.

79MCQ 01 N. R. MCqUAKER, P. D. KLUCKNER, AND G. N. CHANG (1979) CALIBRATION OF AN INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETER FOR THE ANALYSIS OF ENVIRONMENTAL

HATERIALS, ANALYTICAL CHEMISTRY, 51: 888-895.

79MCQ 02 N. R. MCQUAKER, D. F. BROWN, AND P. D. KLUCKNER (1979) DIGESTION OF ENVIRONMENTAL MATERIALS FOR ANALYSIS BY INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 51: 1082-1084.

79MEN 01 E. MENDELOVICI, J. J. LABRECQUE, AND R. E. VILLALBA (1979) CALCIUM AND MAGNESIUM DETERMINATION IN SILICATES AND

VENEZUELAN LATERITES BY ATOMIC ABSORPTION SPECTROSCOPY: INTERFERENCE STUDIES IN THE FLUOROBORIC - BORIC ACID MATRIX, CHEMICAL GEOLOGY, 24: 199-209.

79HER 01 R. N. MERRYTIELD AND R. C. LOYD (1979) SIMULTANEOUS DETERMINATION OF METALS IN OIL BY INDUCTIVELY COUPLED PLASMA EMISSION SPECTROMETRY , ANALYTICAL CHEMISTRY,

51: 1965-1968.

79MIL 01 R. J. MILLER AND D. J. INGLE (1979) UNPUBLISHED DATA; TAKEN FROM 81MAR 01.

79MIZ 01 A. MIZUIKE AND A. UNO (19 79) COATING OF BOROSILICATE GLASS CONTAINERS FOR PREVENTING CONTAMINATION IN TRACE ELEMENT ANALYSIS, ANALYTICA CHIMICA ACTA, 111: 251-256.

210
CODE N DESCRIPTION CODE N DESCRIPTION

79MON 01 J. R. MONTGOMERY AND M. T. PRICE ( 1979) RELEASE OF TRACE METALS BY SEWAGE SLUDGE AND THE SUBSEQUENT

UPTAKE BY MEMBERS OF A TURTLE GRASS MANGROVE ECO SYSTEM

ENVIRONMENTAL SCIENCE AND TECHNOLOGY, 13: 546-549.

79NAR 01 8. NARASAKI (1979) DETERMINATION OF CADMIUM IN POLISHED RICE BY LOW-TEMPERATURE ASHING AND ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA

ACTA, 104 : 393-39 5.

79NIC 01 L. W. NICHOLSON AND K. RENGAN (1979) DETERMINATION OF ARSENIC IN SOME LAKE MICHIGAN FISH USING NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 54: 355-360.

790RV 01 E. ORVINI AND R. DELFANTI (1979) DETERMINATION OF ARSENIC AT NANOGRAM LEVEL IN BIOLOGICAL

TISSUES BY RADIOCHEMICAL ACTIVATION ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 37: 199-206.

79PAV 02 L. PAVLDC, J. KALOUSKOVA, M. VOBECKY, J. DEDINA,

J. BENES, J. PARIZEK (19 79), SELENIUM LEVELS IN THE KIDNEYS

OF MALE AND FEMALE RATS, PP. 213-223, IN 79IAE 01.

79PEA 01 S. PEATS (1979) DETERMINATION OF ARSENIC IN SEAWEED AND RELATED PRODUCTS BY ATOMIC ABSORPTION SPECTROPHOTOMETRY USING THE MHS-10 HYDRIDE GENERATION SYSTEM , ATOMIC ABSORPTION NEWSLETTER, 18: 118-120

79PLA 01 L.-O. PLANTIN (19 79) TRACE ELEMENTS IN CARDIOVASCULAR DISEASES, PP. 321-330, IN 79IAE 01.

79RAI 01 R. M. RAIE AND H. SMITH (1979) THE DETERMINATION OF SELENIUM IN BIOLOGICAL MATERIALS BY THERMAL NEUTRON ACTIVATION ANALYSIS AND ATOMIC ABSORPTION

SPECTROMETRY , JOURNAL OF RADIOANALYTICAL CHEMISTRY,

48: 185-190.

79REE 01 J. REEDNICK (1979) A UNIQUE APPROACH TO ATOMIC SPECTROSCOPY-HIGH ENERGY PLASMA EXCITATION AND HIGH RESOLUTION SPECTROMETRY, AMERICAN LAB- ORATORY, 11: 53-62.

79REI 01 J. E. O'REILLY AND D. G. HICKS ( 1979) SLURRY- INJECTION ATOMIC ABSORPTION SPECTROMETRY FOR ANALYSIS OF WHOLE COAL, ANALYTICAL CHEMISTRY, 51: 1905-1915.

79REN 01 K. RENGAN, J. P. HAUSHALTER, AND J. D. JONES ( 1979) SIMULTANEOUS DETERMINATION OF ARSENIC AND ANTIMONY IN ENVIRONMENTAL SAMPLES BY RADIOCHEMICAL NEUTRON ACTIVATION

ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 54 : 347-3 5 3.

79REN 02 M. J. RENAN (1979) THE DETERMINATION OF ELEMENTS NOT PREVIOUSLY CERTIFIED IN INTERNATIONAL BIOLOGICAL REFERENCE MATERIALS, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 40: 87-102.

79REN 03 M.J. RENAN, B.D. DRENNAN, R.J. KEDDY, J. SELLSCHOP ( 1979) OESOPHAGEAL CANCER IN THE TRANSKEI- DETERMINATION OF TRACE ELEMENT CONCENTRATIONS IN SELECTED PLANT MATERIAL BY INAA, PP. 479-494, IN 79IAE 01.

79RIS 01 T. H. RISBY (EDITOR) (1979) ULTRATRACE METAL ANALYSIS IN BIOLOGICAL SCIENCES AND ENVIRONMENT, ADVANCES IN CHEMISTRY SERIES, AMERICAN CHEMICAL SOCIETY, WASHINGTON, D.C.

79ROB 01 W. B. ROBBINS, J. A. CARUSO, AND F. L. FRICKE (1979) DETERMINATION OF GERMANIUM, ARSENIC, SELENIUM, TIN, AND ANTIMONY

IN COMPLEX SAMPLES BY HYDRIDE GENERATION - MICROWAVE- INDUCE

PLASMA ATOMIC-EMISSION SPECTROMETRY, ANALYST, 104 : 34-40.

79ROS 02 R. J. ROSENBERG (1979) RADIOCHEMICAL ACTIVATION ANALYSIS OF ARSENIC , SELENIUM, AND ANTIMONY IN BIOLOGICAL SAMPLES, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 50: 109-114.

79ROS 03 G. ROSSI AND A. COLOMBO (1979) REFERENCE MATERIALS FOR CHEMICAL ANALYSIS : HIGHLIGHTS ON THE ACTIVITY OF JRC-ISPRA LABORATORIES, FRESENIUS ZEITSCHRIFT

FUR ANALYTISCHE CHEMIE, 297: 13-17.

21

79SAT 01 T. SATO AND T. KATO (1979) DETERMINATION OF TRACE ELEMENTS IN VARIOUS ORGANS OF RATS

BY THERMAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 53: 181-190.

79SCH 02 B. SCHORIN (1979) QUANTITATIVE DETERMINATION OF SI, AL, TI , AND FE IN LATERITE AND BAUXITES BY X-RAY FLUORESCENCE USING A COMPUTER FOR CORRECTION OF INTERELEMENT EFFECTS, APPLIED SPECTROSCOPY,

33: 634-637.

79SIL 01 D. SILBERMAN AND G. L. FISHER (1979) ROOM- TEMPERATURE DISSOLUTION OF COAL FLY ASR FOR TRACE METAL ANALYSIS BY ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA ACTA, 106: 299-307.

79SMI 01 R. D. SMITH, J. A. CAMPBELL, AND K. K. NIELSON (1979) CONCENTRATION DEPENDENCE UPON PARTICLE SIZE OF VOLATILIZED

ELEMENTS IN FLY ASH, ENVIRONMENTAL SCIENCE AND TECHNOLOGY,

13: 553-560.

79STO 01 M. STOEPPLER, P. VALENTA, AND H. W. NURNBERG (1979) APPLICATION OF INDEPENDENT METHODS AND STANDARD MATERIALS:

AN EFFECTIVE APPROACH TO RELIABLE TRACE AND ULTRATRACE

ANALYSIS OF METALS AND METALLOIDS IN ENVIRONMENTS AND

BIOLOGICAL MATRICES, FRESENIUS ZEITSCHRIFT FIR ANALYTISCHE

CHEMIE, 297 : 22-34.

79SZY 01 F. J. SZYDLOWSKI (1979) . BORON IN NATURAL WATERS BY ATOMIC ABSORPTION SPECTROMETRY WITH ELECTROTHERMAL ATOMIZATION, ANALYTICA CHIMICA ACTA,

106: 121-125.

79TAG 01 M. TAGUCHI, K. YASUDA, M. HASHIMOTO, AND S. TODA (1979) SOME IMPROVEMENTS FOR MERCURY DETERMINATION IN MARINE

ORGANISMS BY ATOMIC ABSORPTION SPECTROMETRY , BUNSEKI KAGAKU,

28: T33-T38.

79TAM 01 Y. TAMARI , K. HIRAKI, AND Y. NISHIKAWA (1979) FLUOROMETRIC DETERMINATION OF SELENIUM IN SEDIMENTS WITH

2 ,3-DIAMINONAPHTHALENE, BUNSEKI KAGAKU , 28: 164-169.

79ULL 01 A. H. ULLMAN, B. D. POLLARD, G. D. BOUTILLIER, R. P. BATEH,

P. HANLEY, AND J. D. W1NEFORDNER (1979) COMPUTER-CONTROLLED MULTIELEMENT ATOMIC

EMISSION/ FLUORESCENCE SPECTROMETER SYSTEM, ANALYTICAL CHEMISTRY, 51 : 2 382- 238 7.

79UNR 01 D. M. UNRUH, R. HUTCHISON, ANDM. TAT SUMO TO ( 1979) U-TH-PB AGE OF THE BARWELL CHONDRITE: ANATOMY OF A

"DISCORDANT" METEORITE, IN 79LPI 01, PP. 1011-1030.

79VEI 01 C. VEILLON, W. R. WOLF, AND B. E. GUTHRIE (1979) DETERMINATION OF CHROMIUM IN BIOLOGICAL MATERIALS BY STABLE ISOTOPE DILUTION, ANALYTICAL CHEMISTRY,

51: 1022-1024.

79VER 01 J. VERSIECK, J. HOSTE, J. DE RUDDER, F . BARBIER, AND

L. VANBALLENBERGHE (1979), DETERMINATION OF CHRCMIUM IN BOWEN'S KALE, NBS BOVINE LIVER, AND BREWERS YEAST, BEFORE AND AFTER DRY ASHING, ANALYTICAL LETTERS, 12: 555-562.

79VIJ 01 P. N. VIJAN (1979) DETERMINATION OF ANTIMONY IN ENVIRONMENTAL SAMPLES BY AA, AMERICAN LABORATORY, 11: 32-4 3

79VOB 01 M. VOBECKY, J. DEDINA, L. PAVLIK, AND J. VALASEK ( 1979) GAMMA-RAY INTERFERENCES IN THE DETERMINATION OF SELENIUM BY THE INAA METHOD, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS,

38: 19 7-204.

79WAR 01 N. I. WARD, R. STEPHENS, AND D. E. RYAN (1979) COMPARISON OF THREE ANALYTICAL METHODS FOR THE DETERMINATION

OF TRACE ELEMENTS IN WHOLE BLOOD, ANALYTICA CHIMICA ACTA,

110: 9-19.

79WAR 02 N. I. WARD AND D. E. RYAN (1979) MULTI-ELEMENT ANALYSIS OF BLOOD FOR TRACE METALS BY NEUTRON ACTIVATION ANALYSIS , ANALYTICA CHIMICA ACTA, 105: 185-197.

79WAT 02 J. H. WATKINSON (1979) SEMI-AUTOMATED FLUORIMETRIC DETERMINATION OF NANOGRAM

QUANTITIES OF SELENIUM IN BIOLOGICAL MATERIAL, ANALYTICA CHIMICA ACTA, 105: 319-325.
cose n DESCRIPTION core n DESCRIPTION

79WEG 01 W. WECSCHEIDER, G. KNAPF, AND H. SPITZY ( 1979) SEQUENTIAL TESTING AS AN EFFICIENT SCREENING METHOD FOR INTERFERENCES IN ROUTINE ANALYSIS AS APPLIED TO ATOMIC- ABSORPTION SPECTROMETRY WITH FLAME AND GRAPHITE FURNACE ATOHIZATION, TALANTA, 26: 25-31.

79VES 01 M. B. SBST, J. F. MOLINA, C. L. YUAN AND D. G. DAVIS (19 79) DETERMINATION OF METALS IN WATERS AND ORGANIC MATERIALS BY FLAMELESS ATOMIC ABSORPTION SPECTROMETRY WITH A WIRE LOOP ATOMIZER, ANALYTICAL CHEMISTRY, 51: 2370-2375.

79IAN 01 M. H. YANG, C. L. TSENG, AND G. TOLG (1979) DETERMINATION OF SMALL AMOUNTS OF BORON BY RADIATION

DECOMPOSITION OF CHLOROACETIC ACID SOLUTION, TALANTA,

26: 705-711.

79TAS 01 K. YASUDA, S. TODA, C. IGARASRI , AND S. TAMUR A (1979) EXTRACTION SYSTEM FOR SOLVENT EXTRACTION-GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY, ANALYTICAL CHEMISTRY,

51: 161-163.

79ZEI 01 R. ZEISLER, F. LUX, H. SEI DENBERGER, H. SCHONENBERGER, AND

W. BECK (1979), STUDIES ON THE DISTRIBUTION OF PLATINUM IN TUMOR-BEARING RATS AFTER THE ADMINISTRATION OF PLATINUM

CO-ORDINATION COMPLEXES USED IN CANCER CHEMOTHERAPY,

PP. 467-476, IN 79IAE 01.

80AGE 01 H. AGEMIAN, D. P. STURTEVANT, AND K. D. AUSTEN (1980) SIMULTANEOUS ACID EXTRACTION OF SIX TRACE METALS FROM FISH

TISSUE BY ROT-BLOCK DIGESTION AND DETERMINATION BY ATOMIC

ABSORPTION SPECTROMETRY , ANALYST, 105: 125-130.

80AGE 02 H. AGEMIAN AND R. THOMSON (1980) SIMPLE SEMI-AUTOMATED ATOMIC-ABSORPTION SPECTROMETRIC METHOD FOR THE DETERMINATION OF ARSENIC AND SELENIUM IN

FISH TISSUE, ANALYST, 105: 902-907.

80AGE 03 H. AGEMIAN AND E. BEDEK (1980) A SEMI-AUTOMATED METHOD FOR THE DETERMINATION OF TOTAL

ARSENIC AND SELENIUM IN SOILS AND SEDIMENTS, ANALYTICA

CHIMICA ACTA, 119 : 3 2 3-330.

80AHM 01 S. AHMAD, M. S. CHAUBHARY, AND I. H. QURESHI (1980) DETERMINATION OF RARE EARTHS IN LOW GRADE URANIUM ORES AND SRM-ROCK BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 57: 185-193.

80AND 01 D. L. ANDERSON, M. P. FAILEY, G. E. GORDON, AND

W. H. ZOLLER (1980) INSTRUMENTAL PROMPT GAMMA ACTIVATION ANALYSIS OF ENERGY

RELATED SAMPLES AND STANDARDS, 4TH INTERNATIONAL

CONFERENCE ON NUCLEAR METHODS IN ENVIRONMENTAL AND ENERGY

RESEARCH, UNIVERSITY OF MISSOURI , APRIL 14-17,1980,

PREPRINT.

80ARO 01 H. S. ARORA, C. E. PUGH, L. R. HOSSNER, AND J. B. DIXON

(1980), FORMS OF SULFUR IN EAST TEXAS LIGNITIC COAL, JOURNAL OF ENVIRONMENTAL QUALITY, 9 : 383-386.

80AUG 01 J. H. AUGUSTSON, J. W. HAYNES, AND T. W. SANDERS (1980) THE DETERMINATION OF URANIUM IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS USING THE FISSION PRODUCT 1-134, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 60: 37 3-383.

SOBER 01 C. BERTHELOT, G. CARRARO, AND V. VERDINGH (1980) NON- DESTRUCTIVE MULTI-ELEMENT PHOTON ACTIVATION ANALYSIS OF RIVER SEDIMENTS, JOURNAL OF RADIOANALYTICAL CHEMISTRY

60: 443-4 51.

SOBER 02 C. BERGERIOUX AND W. HAERDI (1980) COPRECIPITATION OF DISSOLVED TRACE ELEMENTS WITH COMBINED

ORGANIC PRECIPITATING REAGENTS FOR USE IN X-RAY FLUORESCENCE

ANALYSIS. I.-l ,10-FHENANTHROLIN AND TETRAPHENYL BORON, ANALUSIS, 8: 169-173.

80BRE 01 I. B. BRENNER, A. E. WATSON, G. M. RUSSELL, AND

M. GONCALVES (1980) A NEW APPROACH TO THE DETERMINATION OF THE MAJOR AND MINOR

CONSTITUENTS IN SILICATE AND PHOSPHATE ROCKS, CHEMICAL GEOLOGY, 28 : 321-330.

80BUA 01 P. BUAT-MENARD, C. E. LAMBERT, M. ARNOLD, AND R. CHESSELET

(1980), MULTI-ELEMENT NEUTRON ACTIVATION ANALYSIS TOWARDS

THE GEOCHEMISTRY OF PARTICULATE MATTER EXCHANGE BETWEEN CONTINENT - ATMOSPHERE - OCEAN, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 55: 445-452.

80CAN 01 C. E. CANN AND S. G. PRUSSIN (1980) RADIOCHEMICAL DETERMINATION OF SHORT-LIVED RADIONUCLIDES

IN NEUTRON-ACTIVATED BIOLOGICAL SAMPLES, INTERNATIONAL JOURNAL OF APPLIED RADIATION AND ISOTOPES, 31: 446-447.

SOCAS 01 V. R. CASELLA, C. T. BISHOP, A. A. GLOSBY, AND C.A. PHILLIPS

(1980), RADIOCHEMICAL DETERMINATION OF URANIUM, THORIUM, AND

LEAD-210 IN COAL AND COAL ASH, RADIOELEMENT ANALYSIS

PROGRESS AND PROBLEMS, PROCEEDINGS OF THE TWENTY-THIRD

CONFERENCE ON ANALYTICAL CHEMISTRY IN ENERGY TECHNOLOGY,

V. 8. LYON (ED.), ANN ARBOR SCIENCE PUBLISHERS, ANN ARBOR, MICHIGAN, PP. 271-277.

80CHA 01 S. S. CHAD AND E. E. PICKETT (1980) TRACE CHROMIUM DETERMINATION BY FURNACE ATOMIC ABSORPTION

SPECTROMETRY FOLLOWING ENRICHMENT BY EXTRACTION, ANALYTICAL CHEMISTRY, 52: 335-339.

80CHR 01 J. D. CHRISTENSEN AND L. KRYGER (1980) REDUCTIVE POTENTIOMETRIC STRIPPING ANALYSIS, ANALYTICA CHIMICA ACTA, 118: 53-64.

80CLA 01 P. J. CLARK, R. A. ZINGARO, K. J. IRGOLIC AND A. N. MCGINLEY

(1980), ARSENIC AND SELENIUM IN TEXAS LIGNITE, INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 7: 295-314 .

80CRE 01 E. A. CRECELIUS, E. A. LEPPEL, J. C. LAUL, L. A. RANCITELLI AND R. L. MCKEEVER (1980), BACKGROUND AIR PARTICULATE

CHEMISTRY NEAR COLSTRIP, MONTANA, ENVIRONMENTAL SCIENCE AND

TECHNOLOGY, 14 : 4 2 2-4 28.

80DAL 01 P. DALHEIM (1980) APPLICATION OF THE FUNDAMENTAL PARAMETER MODEL TO ENERGY

DISPERSIVE X-RAY FLUORESCENCE ANALYSIS OF COMPLEX SILICATES, ADVANCES IN X-RAY ANALYSIS, NEW YORK, PLENUM PRESS,

23: 71-76.

80DON 01 E. M. DONALDSON (1980) DETERMINATION OF CHROMIUM IN ORES, ROCKS AND RELATED

MATERIALS, IRON, STEEL AND NON-FERROUS ALLOYS BY ATOMIC ABSORPTION SPECTROPHOTOMETRY AFTER SEPARATION BY TRIBENZYLAM1NE-CHLOROFORM EXTRACTION, TALANTA, 27: 779-786.

80DOR 01 A. DORNEMANN AND H. KLEIST (1980) BESTIMMUNG VON NANOSPUREN NICKEL IN BIOLOGISCHEM MATRIX, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 300: 197-199.

80DSI 01 A. P. D'SILVA, G. W. RICE, AND V. A. FASSEL (1980) ATMOSPHERIC PRESSURE ACTIVE NITROGEN (APAN) - A NEW SOURCE

FOR ANALYTICAL SPECTROSCOPY, APPLIED SPECTROSCOPY,

34 : 578-584.

BODUM 01 R. DUMAREY , R. HEINDRYCKX , AND R. DAMS (1980) DETERMINATION OF MERCURY IN ENVIRONMENTAL STANDARD REFERENCE

MATERIALS BY PYROLYSIS, ANALYTICA CHIMICA ACTA, 118: 381-383.

80DUP 01 S. DUPIRE ET M. HOENIG (1980) INFLUENCE DES MATRICES COMPLEXES SUR LA DETERMINATION DES ELEMENTS EN TRACE, ANALUSIS, 8: 153-158.

80DYC 01 P. M. VAN DYCK AND R. W. VAN GRIEKEN (1980) ABSORPTION CORRECTION VIA SCATTERED RADIATION IN ENERGY

DISPERSIVE X-RAY FLUORESCENCE ANALYSIS FOR SAMPLES OF VARIABLE COMPOSITION AND THICKNESS, ANALYTICAL CHEMISTRY,

52: 18 59-1864.

80EDD 01 B. T. EDDY, J. I. W. WATTERSON, AND C. S. ERASMUS (1980) PREPARATION OF SYNTHETIC STANDARDS FOR USE IN INSTRUMENTAL

NEUTRON ACTIVATION ANALYSIS, GE0STAN DARDS NEWSLETTER,

4 : 229-237.

80EPS 01 M. S. EPSTEIN AND J. D. WINEFORDNER (1980) PRECISION AND LINEARITY OF DETERMINATIONS AT HIGH CONCENTRATIONS IN ATOMIC ABSROPTION SPECTROMETRY WITH

HORIZONTAL ROTATION OF THE BURNER, TALANTA, 27: 177-180.

80EPS 02 M. S. EPSTEIN, J. BRADSHAW, S. BAYER, J. BOWER, E. VOIGTMAN, AND J. D. WINEFORDNER (1980), APPLICATION OF LASER-EXCITED

ATOMIC FLUORESCENCE SPECTROMETRY TO THE DETERMINATION OF NICKEL AND TIN, APPLIED SPECTROSCOPY, 34 : 372-37 6.

80EPS 03 M. S. EPSTEIN, N. OMENETTO, S. NIKDEL, J. BRADSHAW, AND

J. D. WINEFORDNER (1980), INDUCTIVELY COUPLED PLASMA AS AN EXCITATION SOURCE FOR FLAME ATOMIC FLUORESCENCE SPECTROMETRY ANALYTICAL CHEMISTRY. 52: 2R4-?R7-

212
CODE N DESCRIPTION

CODE N DESCRIPTION

80EVA 01 W. H. EVANS, D. DELLAR, B. E. LUCAS, F. J. JACKSON, AND J. I. READ (1980) OBSERVATIONS OF THE DETERMINATION OF TOTAL COPPER, IRON, MANGANESE AND ZINC IN FOODSTUFFS BY FLAKE ATOMIC ABSORPTION

SPECTROPHOTOMETRY, ANALYST, 105: 529-54 3.

60FAA 01 A. FAANHOF, H. A. DAS, AND J. ZONDERHUIS (1980) POSSIBILITIES OF THE ELEMENTAL ANALYSIS OF DRY BIOLOGICAL MATERIAL BY FAST NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 56: 173-184.

80FLO 01 M. A. FLOYD, V. A. FASSEL , AND A. P. D'SILVA (1980) COMPUTER-CONTROLLED SCANNING MONOCHROMATOR FOR THE

DETERMINATION OF 50 ELEMENTS IN GEOCHEMICAL AND

ENVIRONMENTAL SAMPLES BY INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 52: 2168-2173.

80FUD 01 N. FUDAGAWA AND A. RAVASE (1980) DETERMINATION OF COBALT IN PLANT MATERIALS BY GRAPHITE FUR- NACE ATOMIC ABSORPTION SPECTROMETRY AFTER SOLVENT EXTRACTION

BUNSEKI KAGAKU, 29: 6-11.

80GAR 01 S. R. GARCIA, W. K. HENSLEY, M. M. MINOR, M. M. DENTON,

M. A. FUKA (1980), AN AUTOMATED MULTI DETECTOR SYSTEM FOR

INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF GEOLOGICAL AND ENVIRONMENTAL MATERIALS, PRESENTED AT THE NOV 1980 AMERICAN NUCLEAR SOCIETY MEETING , PUERTO RICO.

SOGER 01 M. S. GERMANI, I. GORMEN, A. C. SIGLEO, G. S. KOWALCZYK

I. OLMEZ , A. M. SMALL, D. L. ANDERSON, M. P. FAILEY,

M. C. GULOVALI, C. E. CHOQUETTE, E. A. LEPEL, G. E. GORDON

AND W. H. ZOLLER (1980) CONCENTRATIONS OF ELEMENTS IN THE NATIONAL BUREAU OF STANDARDS' BITUMINOUS AND SUBBITUMINOUS COAL STANDARD REFERENCE MATERIALS, ANALYTICAL CHEMISTRY, 52: 240-245.

80GIN 01 J. H. VAN GINKEL AND J. SINNAEVE (1980) DETERMINATION OF TOTAL NITROCEN IN PLANT MATERIAL WITH

NESSLER'S REAGENT BY CONTINUOUS-FLOW ANALYSIS, ANALYST,

105: 1199-1203.

80GLA 01 E.S. GLADNEY, D.R. PERRIN, W.K. HENSLEY AND

M.E. BUNKER (1980) URANIUM CONTENT OF 25 SILICATE REFERENCE MATERIALS,

GEOSTAN DARDS NEWSLETTER, 4: 24 3-246.

80GLA 03 E. S. GLADNEY , D. R. PERRIN, J. P. BALAGNA, AND C. L. WARNER

(1980), EVALUATION OF A BORON-FILTERED EPITHERMAL NEUTRON

IRRADIATION FACILITY, ANALYTICAL CHEMISTRY , 52: 2128-2132.

80GLA 04 E. S. GLADNEY , D. R. PERRIN, AND W. K. HENSLEY (1980) DETERMINATION OF URANIUM IN NBS BIOLOGICAL STANDARD

REFERENCE MATERIALS BY DELAYED NEUTRON ASSAY, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 59: 249-251.

8 OGRE 01 R. R. GREENBERG (1980) SIMULTANEOUS DETERMINATION OF MERCURY AND CADMIUM IN BIOLOGICAL MATERIALS BY RADIOCHEMICAL NEUTRON ACTIVATION

ANALYSIS, ANALYTICAL CHEMISTRY, 52: 676-679.

80GVA 01 I. GVARDJANCIC, L. KOSTA, AND M. DERMEU (1980) DETERMINATION OF IODINE IN REFERENCE MATERIALS BY ACTIVATION

ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 58: 359-365.

80HAA 01 W. J. HAAS AND V. A. FASSEL (1980) INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROSCOPY, ELEMENTAL ANALYSIS OF BIOLOGICAL MATERIALS, IAEA TECHNICAL

REPORT SERIES NO. 197, PP. 167-199.

BOHAN 01 R. HANNINEN, J. RAISANEN, AND A. ANTTILA (1980) ELEMENTAL ANALYSIS OF LI AND B WITH PROTON INDUCED

GAMMA-RAY REACTIONS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 44: 201-206.

8 OHEN 01 W. M. HENRY AND K. T. KNAPP (1980) COMPOUND FORMS OF FOSSIL FUEL FLY ASR EMISSIONS, ENVIRONMENTAL SCIENCE AND TECHNOLOGY, 14: 4 50-4 56.

80HEY 01 K. HEYDORN , E. DAMSGAARD, AND B. REITZ (1980) SYSTEMATIC DIFFERENCES IN THE DETERMINATION OF VANADIUM

IN STANDARD REFERENCE MATERIAL 1571 ORCHARD LEAVES, ANALYTICAL CHEMISTRY, 52: 104 5-1049.

80HIT 02 A. HITCHEN AND G. ZECHANOWITSCH (1980) CHELATOMETRIC DETERMINATION OF CALCIUM AND MAGNESIUM IN IRON ORES, SLAGS, ANORTHOSITE, LIMESTONE, COPPER-NICKELLEAD-ZINC ORES AND DIVERSE MATERIALS, TALANTA, 27: 269-275.

80H0E 01 D. HOEDE, J. ZONDERHUIS, AND H. A. DAS (1980) THE DETERMINATION OF BROMINE IN DRY BIOLOGICAL MATERIAL BY INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 56: 199-202.

80H0N 01 P. K. HON, 0. W. LAU , W. C. CHEUNG, AND M. C. WONG (1980) ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF ARSENIC, BISMUTH, LEAD, ANTIMONY, SELENIUM , AND TIN WITH A

FLAME-HEATED SILICA T-TUBE AFTER HYDRIDE GENERATION, ANALYTICA CHIMICA ACTA, 115: 355-359.

80IID 01 C. IIDA, T. UCHIDA, AND I. KOJIMA (1980) DECOMPOSITION OF BOVINE LIVER IN A SEALED TEFLON VESSEL FOR

DETERMINATION OF METALS BY ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA ACTA, 113: 365-368.

80IWA 01 Y. IWATA, K. MATSUMOTO, AND K. FUWA (1980) DETERMINATION OF CHROMIUM IN ROCKS AND SEDIMENTS BY ENERGY

DISPERSIVE X-RAY FLUORESCENCE SPECTROMETRY; EVALUATION OF THE EFFECTIVENESS OF INTERNAL STANDARDS AND BRIQUETTING

SAMPLES, BUNSEKI KAGAKU, 29 : 640-644 .

80JAC 01 F. J. JACKSON, J. I. READ, AND B. E. LUCAS (1980) DETERMINATION OF TOTAL CHROMIUM , COBALT, AND SILVER IN FOODSTUFFS BY FLAME ATOMIC ABSORPTION SPECTROPHOTOMETRY,

ANALYST, 105: 359-370.

80JAR 01 J. 0. JARVISALO, J. KILPIO, N.-E. L. SARIS (1980) TOXICITY OF CADMIUM TO RENAL MITOCHONDRIA WHEN ADMINISTERED

IN VIVO AND IN VITRO, ENVIRONMENTAL RESEARCH , 22: 217-223.

80KAT 01 T. KATO AND M. KATO (1980) MULTIELEMENT DETERMINATION IN FLOOR SEDIMENTS OF THE JAPAN

SEA BY NONDESTRUCTIVE PHOTON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 57: 105-112.

80KHA 02 S. R. KHALIL, D. W. KOPPENAAL , AND W. D. EHMANN ( 1980) OXYGEN CONCENTRATIONS IN COAL AND FLY ASH STANDARDS, ANALYTICAL LETTERS, 13: 1063-1071.

80KIR 01 S. J. KIRCHNER, H. OONA, S. J. PERRON, Q. FERNANDO, J. LEE, AND H. ZEITLIN (1980), PROTON-INDUCED X-RAY EMISSION

ANALYSIS OF DEEP-SEA FERROMANGANESE NODULES, ANALYTICAL CHEMISTRY, 52: 2195-2201 .

80KNA 01 D. KNAB AND E. S. GLADNEY (1980) DETERMINATION OF SELENIUM IN ENVIRONMENTAL MATERIALS BY NEUTRON ACTIVATION AND INORCANIC ION EXCHANGE , ANALYTICAL

CHEMISTRY, 52: 825-828.

80KOH 01 T.-S. KOH (1980) MICROWAVE DRYING OF BIOLOGICAL TISSUES FOR TRACE DETERMINATION, ANALYTICAL CHEMISTRY, 52: 1978-1979.

80KOP 01 D. W. KOPPENAAL, R. G. LETT, F. R. BROWN, AND S. E. MANAHAN

(1980), DETERMINATION OF NICKEL , COPPER, SELENIUM, CADMIUM

THALLIUM, AND LEAD IN COAL GASIFICATION PRODUCTS BY ISOTOPE DILUTION SPARK SOURCE MASS SPECTROMETRY, ANALYTICAL CHEMISTRY , 52: 44-49.

80KOR 01 V. KORUNOVA AND J. DEDINA (1980) DETERMINATION OF TRACE CONCENTRATIONS OF MERCURY IN BIOLOGICAL MATERIALS AFTER DIGESTION UNDER PRESSURE IN NITRIC ACID CATALYZED BY VANADIUM PENTOXIDE, ANALYST,

105: 48-51.

80KOS 02 L. KOSTA (1980) REFERENCE SAMPLES FOR TRACE ELEMENTS IN BIOLOGICAL MATERIALS

AND ASSOCIATED ANALYTICAL PROBLEMS , ELEMENTAL ANALYSIS OF BIOLOGICAL MATERIALS: CURRENT PROBLEMS AND TECHNIQUES WITH

SPECIAL REFERENCE TO TRACE ELEMENTS, IAEA TECHNICAL REPORT

SERIES NO. 197, VIENNA, PP. 3 17 - 34 5.

80KUL 01 A. I. KULATHILAKE AND A. CHATT (1980) DETERMINATION OF MOLYBDENUM IN SEA AND ESTUARINE WATER WITH BETA-NAPHTHOIN OXIME AND NEUTRON ACTIVATION, ANALYTICAL CHEMISTRY, 52: 828-833.

213
CODE N DESCRIPTION

80KUM 01 J. KUMPULAINEN (1980)

EE TERMINATION OF CHROMIUM IN HUMAN MILK AND URINE BY GRAPHITE-FURNACE ATOMIC ABSORPTION SPECTROMETRY

ANALTTICA CHIMICA ACTA, 113: 355-359.

BOLAB 03 J. J. LAHRECQUE AND B. SCHORIN (1980) ANALYSIS OF THE MAJOR CONSTITUENTS IN VENEZUELAN LATERITES

A COMPARESI ON OF ATOMIC ABSORPTION, X-RAY FLUORESCENCE , AND

CLASSICAL METHODS, APPLIED SPECTROSCOPY, 34: 39-4 3.

SOLAN 01 T. J. LANGMYHR AND U. AADALEN ( 1980) DIRECT ATOMIC ABSORPTION DETERMINATION OF COPPER, NICKEL, AND VANADIUM IN COAL AND PETROLEUM COKE, ANALYTICA CHIMICA ACTA, 115: 365-368.

80LAU 01 O.W. LAU AND S.F. CHAM (1980) SPECTROPHOTOMETRIC DETERMINATION OF CALCIUM WITH CHLORINDAZON C, MIKROCHIMICA ACTA (WIEN) , 19801: 465-4 74.

80LF.C 01 P. A. LEGOTTE, W. C. ROSA, AND D. C. SUTTON (1980) DETERMINATION OF CADMIUM AND LEAD IN URINE AND OTHER

BIOLOGICAL SAMPLES BY GRAPHITE-FURNACE ATOMIC ABSORPTION

SPECTROMETRY , TALANTA, 27: 39-44.

80MAE 01 W. MAENHAUT , L. DE REU , H. A. VAN RINSVELT, J. CAFMEYER, AND

P. VAN ESPEN (1980), PARTICLE- INDUCED X-RAY EMISSION (PIXE) ANALYSIS OF BIOLOGICAL MATERIALS: PRECISION, ACCURACY, AND

APPLICATION TO CANCER TISSUES, NUCLEAR INSTRUMENTS AND

METHODS, 168: 557-562.

80MCC 01 J. MCCORMICK (1980) DETERMINATION OF TOTAL SULPHUR IN FUEL OILS BY ION CHROMATOGRAPHY, ANALYTICA CHIMICA ACTA, 121: 233-238.

80NAD 01 R. A. NADKARNI (1980) MULTI TECHNIQUE MULTIELEMENT ANALYSIS OF COAL AND FLY ASH, ANALYTICAL CHEMISTRY , 52: 929-935.

80NAK 01 S. NAKAMURA, N. FUDAGAWA AND A. KAWASE (1980) DETERMINATION OF ANTIMONY IN PLANT MATERIALS BY ZEEMAN

ATOMIC ABSORPTION SPECTROMETRY AFTER COPRECIPITATION WITH

MANGANESE DIOXIDE, BUNSEKI KAGAKU, 29: 477-482.

80NEV 01 J. NEVE, M. HANOCQ, AND L. MOLLE (1980) CRITICAL STUDY OF SOME WET DIGESTION METHODS FOR DECOMPOSI- TION OF BIOLOGICAL MATERIALS FOR THE DETERMINATION OF TOTAL

SELENIUM AND SELENIUM (VI), MIKROCHIMICA ACTA (WIEN), 19801, 259-269.

80N0R 01 L. DE NORRE, J. OP DE BEECK, AND J. HOSTE (1980) DETERMINATION OF FLUORINE IN ZINC ORES USING AN ISOTOPE NEUTRON SOURCE BASED AUTOMATED NEUTRON ACTIVATION ANALYSIS

SYSTEM, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 59: 4 53-466.

80P0L 01 J. E. POLDOSKI (1980) DETERMINATION OF LEAD AND CADMIUM IN FISH AND CLAM TISSUE

BY ATOMIC ABSORPTION SPECTROMETRY WITH A MOLYBDENUM AND

LANTHANUM TREATED PYROLYTIC GRAPHITE ATOMIZER, ANALYTICAL CHEMISTRY, 52: 1147-1151.

60PRF 01 J.R. FREER, H.S. SEKHON, B.R. STEPHENS, AND M.S. COLLINS (1980) FACTORS AFFECTINC HEAVY METAL CONTENT OF GARDEN VEGETABLES, ENVIRONMENTAL POLLUTION, 1: 95-104

80RAP 01 S. E. RAPTIS, W. WEGSCHEI DER, G. KNAPP, AND G. TOLG (1980) X-RAY FLUORESCENCE DETERMINATION OF TRACE SELENIUM IN ORGANIC AND BIOLOGICAL MATRICES, ANALYTICAL CHEMISTRY,

52: 1292-1296.

80RAP 02 S. RAPTIS, G. KNAPP, A. MEYER, AND G. TOLG (1980) SYSTEMATISCHE FEHLER BEI DER SELENBESTIMMUNG IN NG/G—BE REICH

IN BIOLOGISCHEN MATRICES NACH DEM HYDRID-AAS-VERFAHREN,

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 300: 18-21.

80RAP 03 S. RAPTIS, W. WEGSCHEI DER, G. KNAPP, AND G. TOLG (1980) X-RAY FLUORESCENCE DETERMINATION OF TRACES OF SELENIUM IN ORGANIC AND BIOLOGICAL MATRICES, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 301: 103.

COX N DESCRIPTION

80R1L 01 G. H. RILEY ANDM. J. KORSCR ( 1980) NATURAL REACTOR STUDIES, IN PROCEEDINGS OF THE INTERNATIONAL URANIUM SYMPOSIUM ON THE PINE CREEK GEOSYNCLINE, IAEA, VIENNA, PP. 4 07-416.

80RIL 02 G. H. RILEY, R. A. BINNS , AND S. J. CRAVEN (1980) RB-SR CHRONOLOGY OF MICAS AT JABILUKA, IN PROCEEDINGS OF THE INTERNATIONAL URNAIUM SYMPOSIUM ON THE PINE CREEK GEOSYNCLINE , IAEA, VIENNA, PP. 4 57-468.

SOROS 01 K. J. t. ROSMAN AND J.R. DE LAETER (1980) MASS SPECTROMETRIC ISOTOPE DILUTION DETERMINATION OF CADMIUM IN GEOCHEMICAL REFERENCE SAMPLES, CEOSTANDARDS NEWSLETTER, 4: 1-3.

80SAT 01 T. SATO AND T. RATO (1980) DETERMINATION OF TRACE ELEMENTS IN SUBCELLULAR FRACTIONS OF LIVER AND KIDNEY FROM MONKEY BY THERMAL NEUTRON ACITVATION

ANALYSIS, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 42 : 227-234.

SOSCH 02 T. G. SCHOFIELD, E. S. GLADNEY, F. H1ERA, AND P. TRUJILLO

(1980), COMPARATIVE DETERMINATION OF CARBON, NITROGEN, AND

HYDROGEN IN ENVIRONMENTAL STANDARD REFERENCE MATERIALS BY INSTRUMENTAL COMBUSTION ANALYSIS AND THERMAL NEUTRON CAPTURE GAMMA-RAY SPECTROMETRY, ANALYTICAL LETTERS, 13: 75-83.

SOSCH 05 P. S CARAMEL , A. WOLF, R. SEIF, AND B.-J. KLOSE (1980)

EI NE NEUE APPARATUR ZUR DRUCKVERASCHUNG VON BIOLOGISCHEM

MATERIAL, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE,

302: 62-64.

80SEG 01 C. SECEBADE, H.-U. FUSBAN, AND H.-P. WEISE (1980) ANALYSIS OF SOME TOXIC COMPONENTS OF ENVIRONMENTAL SAMPLES

BY HIGH ENERGY PHOTON ACTIVATION, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 59 : 399-4 05.

80SH1 01 T. SHIGEMATSU AND K. KUDO (1980) SUBSTOICHIOMETRIC EXTRACTION OF CHROMIUM, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 59: 63-73.

80SLO 01 H. A. VAN DER SLOOT, G. D. WALS, C. A. WEERS, AND H. A. DAS (1980) SIMULTANEOUS ELIMINATION OF SODIUM-24 , POTASSIUM-4 2 , BROMINE-82, AND PHOSPHORUS-32 IN THE DETERMINATION OF TRACE ELEMENTS IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION

ANALYSIS, ANALYTICAL CHEMISTRY, 52: 112-117.

80SMI 01 G. R. SMITH (1980) RAPID DETERMINATION OF TOTAL SULFUR IN PLANTS AND SOILS

BY COMBUSTION SULFUR ANALYSIS, ANALYTICAL LETTERS,

A13: 465-471.

80STO 02 T. R. STOLZENBURG AND A. W. ANDREN (1980) A SIMPLE ACID DIGESTION METHOD FOR THE DETERMINATION OF TEN ELEMENTS IN AMBIENT AEROSOLS BY FLAME ATOMIC ABSORPTION

SPECTROMETRY, ANALYTICA CHIMICA ACTA, 118: 377-380.

80STU 01 0. STULZAFT , B. MAZIERE, AND S. LY (1980) GALLIUM DETERMINATION IN BIOLOGICAL SAMPLES, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 55: 291-29 5.

80SUZ 01 N. SUZUKI , S. NAKAMURA, AND H. IMURA (1980) SUBSTOICHIOMETRIC ISOTOPE DILUTION ANALYSIS OF IRON IN BIOLOGICAL MATERIALS BY THE 8-QUIN0LIN0L EXTRACTION, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 57: 37-46.

80SUZ 02 M. SUZUKI, Y. DAK1YA, S. YAMAZAK2 , AND S. TODA (19fc0) A NEW TYPE OF BIOLOGICAL REFERENCE MATERIAL FOR MULTI- ELEMENT ANALYSIS-THE FUNGUS PENICILLIUM OCHRO-CHLORON

ATCC 36741, ANALYST, 105 : 944- 949.

80SZY 01 F.J. SZYDLOWSKI, K.L. MONTI , S.P. MICHALAK, AND D.L. DUNMIRE (1980) A PRACTICAL VOLTAMMETRIC METHOD FOR THE ANALYSIS OF LEAD

IN CEREAL AND FEED PRODUCTS USING A TUBULAR MERCURY THIN

FILM ELECTRODE, ANALYTICAL LETTERS, A13 : 529-542.

SOTAM 01 G. K. H. TAM AND G. LACR01X (1980) DETERMINATION OF ARSENIC IN URINE AND FECES BY DRY ASHING, ATOMIC ABSORPTION SPECTROMETRY, INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 8: 28 3-290.

80TON 01 S. L. TONG, W.-K. LEOW (1980) STATIONARY COLD-VAPOR ATOMIC ABSORPTION SPECTROMETRIC ATTACHMENT FOR DETERMINATION OF TOTAL MERCURY IN UNDIGESTED

FISH SAMPLFS 4NM.VTTr«T CHFMT9TRY. 5J : 581-583.

214
CODE N DESCRIPTION

80UCH 01 T. UCHIDA, I. KOJIMA, AND C. IIDA ( 1980) DETERMINATION OF METALS IN SMALL SAMPLES BY ATOMIC

ABSORPTION AND EMISSION SPECTROMETRY WITH DISCRETE

NEBULIZATION, ANALYTICA CHIMICA ACTA, 116: 205-210.

80URE 01 A. M. URE, C. J. EWEN, AND M. C. MITCHELL (1980)

A THREE-CHANNEL FLAME ATOMIC ABSORPTION/EMISSION

SPECTROMETER FOR THE RAPID, ROUTINE DETERMINATION OF MAJOR

CATIONS IN SOIL EXTRACTS AND PLANT ASH SOLUTIONS

,

ANALYTICA CHIMICA ACTA, 118: 1-9.

8 OVAL 01 M. T. G. VALENTINI , N. GENOVA, R. STELLA (1980) DETERMINATION OF CADMIUM , COPPER AND MERCURY IN ENVIRONMENTAL MATRICES BY DESTRUCTIVE NEUTRON ACTIVATION

ANALYSIS , RADIOCHEMICAL AND RADIOANALYTICAL LETTERS,

44: 359-368.

80VIJ 01 P. N. VIJAN AND D. LEUNG (1980) REDUCTION OF CHEMICAL INTERFERENCE AND SPECIATION STUDIES IN THE HYDRIDE GENERATION-ATOMIC ABSORPTION METHOD FOR

SELENIUM, ANALYTICA CHIMICA ACTA, 120: 141-146.

80VIR 01 H. S. VIRK (1980) INTERCALTBRATION OF GLASS DOSIMETERS FOR NEUTRON FLUENCE

DETERMINATION, INTERNATIONAL JOURNAL OF APPLIED RADIATION AND ISOTOPES, 31: 649-651.

8 OVAL 01 W. J. WALKER AND R. H. DOWDY (1980) ELEMENTAL COMPOSITION OF BARLEY AND RYEGRASS GROWN ON ACID

SOILS AMENDED WITH SCRUBBER SLUDGE, JOURNAL OF ENVIRONMENTAL

QUALITY, 9: 27-30.

80WAN 01 L. E. WANGEN , E. S. GLADNEY, AND W. K. HENSLEY (1980) DETERMINATION OF SELENIUM IN ENVIRONMENTAL STANDARD

REFERENCE MATERIALS BY A GAMMA-GAMMA COINCIDENCE METHOD

USING GE(I.I) DETECTORS , ANALYTICAL CHEMISTRY, 52: 765-767.

80WH1 01 L. E . WHITE AND M. H. CARTER (1980) DETERMINATION OF MERCURY IN ROCKS, SEDIMENTS, AND SOILS BY FLAMELESS ATOMIC ABSORPTION, OAK RIDGE Y-12 PLANT REPORT

Y/DK-254 , OAK RIDGE, TN. , 22 MAY 1980.

80YAM 01 M. YAMASHITA AND N. SUZUKI (1980) PHOTON ACTIVATION ANALYSIS OF TRACE METALS IN BIOLOGICAL MATERIALS VIA COLLECTION OF METAL TROPOLONE- 5- SULFONATE

COMPLEXES ONTO ANION-EXCHANGE RESIN, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 60: 73-85.

SOYAN 01 K. YANAGI (1980)

A NEW PROCEDURE FOR DETERMINING ARSENIC IN NATURAL WATERS

BY MEANS OF ATOMIC ABSORPTION SPECTROPHOTOMETRY COMBINED WITH THE TECHNIQUES OF ARSINE EVOLUTION BY SODIUM BORO- HYDRIDE AND OF ITS COLLECTION IN A TRAP OF LIQUID NITROGEN,

BUNSEKI KAGAKU , 29: 194-198.

81AHM 01 S. AHMAD, M. S. CHAUDHARY, AND I. H. QURESHI (1981) INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF OBSIDIAN ROCK, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 67: 119-125.

81 ALL 01 M. ALLEGRINI , K. W. BOYER, J. T. TANNER (1981) NEUTRON ACTIVATION ANALYSIS OF TOTAL DIET FOOD COMPOSITES

FOR IODINE, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 64: 1111-1115.

81ARA 01 N. M. ARAFAT AND W. A. CLOOSCHENKO (1981) METHOD FOR THE SIMULTANEOUS DETERMINATION OF ARSENIC, ALUM- INUM, IRON, ZINC, CHROMIUM AND COPPER IN PLANT TISSUE WITHOUT

THE USE OF PERCHLORIC ACID, ANALYST, 106: 1174-1178.

81BIS 01 K. M. BISGARD, J. LAURSEN, AND B. S. NIELSEN (1981) ENERGY- DISPERSIVE XRF SPECTROMETRY USING SECONDARY RADIATION IN A CARTESIAN GEOMETRY, X-RAY SPECTROMETRY, 10: 17-19.

81BLA 01 M. S. BLACK AND R. F. BROWNER (1981) VOLATILE METAL-CHELATE SAMPLE INTRODUCTION FOR INDUCTIVELY

COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 53: 249-253.

CODE N DESCRIPTION

81BLA 02 M. S. BLACK, M. B. THOMAS, AND R. F. BROWNER (1981) DETERMINATION OF METAL CHELATES BY INDUCTIVELY COUPLED

PLASMA ATOMIC EMISSION SPECTROMETRY AND APPLICATIONS TO BIOLOGICAL MATERIALS, ANALYTICAL CHEMISTRY, 53: 2224-2228.

81BLA 03 M. BLANUSA AND D. BRESKI (1981) COMPARISON OF DRY AND WET ASHING PROCEDURES FOR CADMIUM AND

IRON DETERMINATION IN BIOLOCICAL MATERIAL BY ATOMIC ABSORPTION SPECTROPHOTOMETRY, TALANTA, 28: 681-684.

81BRO 01 P. J. BROOKE AND W. H. EVANS (1981) DETERMINATION OF TOTAL INORGANIC ARSENIC IN FISH, SHELLFISH AND FISH PRODUCTS, ANALYST, 106: 514-520.

81BYR 01 A.R. BYRNE (1981) DETERMINATION OF PALLADIUM IN BIOLOCICAL SAMPLES BY NEUTRON- ACTIVATION ANALYSIS, MIKROCHIMICA ACTA (W1EN) , 19811: 323-329.

81 CAR 01 R. CARPENTER AND T. M. BEASLEY (1981) PLUTONIUM AND AMERICIUM IN ANOXIC MARINE SEDIMENTS : EVIDENCE AGAINST REMOBILIZATION, GEOCHIMICA ET COSMOCHIMICA ACTA, 45: 1917-1930.

81CAR 02 J.W. CARNAHAN, K.J. MULLIGAN AND J.A. CARUSO (1981) ELEMENT- SELECTIVE DETECTION FOR CHROMATOGRAPHY BY PLASMA EMISSION SPECTROMETRY, ANALYTICA CHIMICA ACTA, 130: 227-241 .

81CAS 01 V. R. CAS ELLA, C. T. BISHOP, A. A. GLOSBY , AND C.A. PHILLIPS

(1981), ANION EXCHANGE HETHOD FOR THE SEQUENTIAL DETERMINATION OF URANIUM, THORIUM, AND LEAD-2 10 IN COAL AND COAL ASH

,

JOURNAL OF RADIOANALYTICAL CHEMISTRY , 62: 257-266.

8 1 CHA 01 C. L. CHAKRABARTI, C. C. WAN, H. A. HAMED, AND P. C. BERTELS

(1981), MATRIX INTERFERENCES IN GRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY BY CAPAC1TIVE DISCHARGE HEATING, ANALYTICAL CHEMISTRY, 53: 444-4 50.

81 CHE 01 J. H. CHEN AND G. J. WASSERBURG (1981) THE ISOTOPIC COMPOSITION OF URANIUM AND LEAD IN ALLENDE

INCLUSIONS AND METEORITIC PHOSPHATES, EARTH AND PLANETARY

SCIENCE LETTERS, 52: 1-15.

81CHE 02 J. H. CHEN AND G. J. WASSERBURG (1981) ISOTOPIC DETERMINATION OF URANIUM IN PICOMOLE AND SUBPICOMOLE QUANTITIES, ANALYTICAL CHEMISTRY, 53: 2060-2067.

81CHR 01 L. H. CHRISTENSEN AND A. AGERBO (1981) DETERMINATION OF SULFUR AND HEAVY METALS IN CRUDE OIL AND

PETROLEUM PRODUCTS BY ENERGY-DISPERSIVE X-RAY FLUORESCENCE

SPECTROMETRY AND FUNDAMENTAL PARAMETER APPROACH, ANALYTICAL CHEMISTRY, 53: 1788-1792.

81CHU 01 S. E. CHURCH (1981) MULTI-ELEMENT ANALYSIS OF FIFTY-FOUR GEOCHEMICAL REFERENCE

SAMPLES USING INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION

SPECTROMETRY , GEOSTANDARDS NEWSLETTER, 5: 133-160.

81 CLE 01 M. S. CLEGG, C. L. KEEN, B. LONNERDAL AND L. S. HURLEY (1981) INFLUENCE OF ASHING TECHNIQUES ON THE ANALYSIS OF TRACE ELEMENTS IN ANIMAL TISSUE. I. WET ASHING, BIOLOGICAL TRACE ELEMENT RESEARCH, 3: 107-115

81CLF. 02 M. S. CLEGG, C. L. KEEN, BO LONNERDAL AND L. S. HURLEY (1981) INFLUENCE OF ASHING TECHNIQUES ON THE ANALYSIS OF TRACE ELEMENTS IN BIOLOGICAL SAMPLES. II. DRY ASHING, BIOLOGICAL

TRACE ELEMENT RESEARCH, 3 : 237-244

81COH 02 S. COHEN, S.-G. CHANG, S. S. MARKOWITZ , AND T. NOVAKOV( 1981

)

ROLE OF FLY ASH IN CATALYTIC OXIDATION OF S(IV) SLURRIES, ENVIRONMENTAL SCIENCE AND TECHNOLOGY, 15: 1498-1502.

81COR 01 R. CORNELIS, J. VERSIECK, A. DESMET, L. MEES, AND

L. VANBALLENBERGHE (1981), NEUTRON ACTIVATION ANALYSIS OF THE TRACE ELEMENT MOLYBDENUM IN URINE OF HEALTHY PERSONS, BULLETIN DES SOCIETES CHIMIQUES BELGES, 90: 289-295.

8100R 02 R. CORNELIS, J. VERSIECK, L. MEES, J. HOSTE, AND F. BARBIER (1981) THE ULTRATRACE ELEMENT VANADIUM IN HUMAN SERUM, BIOLOCICAL

TRACE ELEMENT RESEARCH, 3: 257-263

81COX 01 D. H. COX AND A. E. BIBB (1981) HYDROCEN SELENIDE EVOLUTION-ELECTROTHERMAL ATOMIC ABSORPTION METHOD FOR DETERMINING NANOGRAM LEVELS OF TOTAL SELENIUM, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS,

64 : 265-">B

215
CODE DESCRIPTION CODE N DESCRIPTION

81 DAN 01 L.-C. DANIELSSON, D. JACNER, M. JOSEFSON, AND S. WE STERLUND

(1981), COMPUTERIZED POTENTIOMETRIC STRIPPING ANALYSIS FOR THE DETERMINATION OF CADMIUM, LEAD, COPPER, AND ZINC IN BIOLOGICAL MATERIALS, ANALYTICA CHIMICA ACTA, 1 27 1 147-156.

81DIL 01 S. DILLI (1981) DETERMINATION OF VANADIUM IN PETROLEUM CRUDES AND FUEL OILS

BY GAS CHROMATOGRAPHY, ANALYTICA CHIMICA ACTA, 1 28

109-119.

81 DOG 01 8. DOGAN, G. NEMBRINI AND W. HAERDI (1981) A NOVEL APPROACH FOR DETERMINATION OF TIN, LEAD AND COPPER

IN BIOLOCICAL SAMPLES AND SEDIMENTS BY ALTERNATING CURRENT

ANODIC STRIPPING VOLTAMMETRY, ANALYTICA CHIMICA ACTA, 130:

38 5-390.

81EBD 01 La EBDON, J. R. WILKINSON AND K. W. JACKSON (1981) DETERMINATION OF SUB-NANOGRAM AMOUNTS OF MERCURY BY COLD- VAPOUR ATOMIC FLUORESCENCE SPECTROMETRY WITH AN IMPROVED

GAS- SHEATHED ATOM CELL, ANALYTICA CHIMICA ACTA, 128: 4 5-55.

81 PAR 01 J. G. FARMER AND M. J. GIBSON (1981) DIRECT DETERMINATION OF CADMIUM , CHROMIUM, COPPER, AND LEAD

IN SILICEOUS STANDARD REFERENCE MATERIALS FROM A FLUOROBORIC ACID MATRIX BY GRAPHITE FURNACE ATOMIC ABSORPTION

SPECTROMETRY , ATOMIC SPECTROSCOPY, 2: 176-178.

81FON 01 H. A. FONER AND I. GAL (1981) ACCURATE SPECTROPHOTOMETRIC METHOD FOR THE DETERMINATION

OF SILICA IN ROCKS, MINERALS AND RELATED MATERIALS,

ANALYST, 106: 521-528.

81FRA 01 G. FRAUERWIESER (1981) PRIVATE COMMUNICATION, TECHNICAL UNIVERSITY OF VIENNA

AUSTRIA.

81 GAL 01 M. GALLORINI, E. ORVINI, A. ROLLA, AND M . BURDISSO (1981) DESTRUCTIVE NEUTRON-ACTIVATION ANALYSIS OF TOXIC ELEMENTS

IN SUSPENDED MATERIALS RELEASED FROM REFUSE INCINERATORS,

ANALYST, 106 : 328 - 334.

81 GAL 02 M. GALLORINI, E. ORVINI, A. ROLLA, AND M. BURDISSO (1981) RADIOCHEMICAL NEUTRON-ACTIVATION ANALYSIS OF TRACE ELEMENTS

IN SUSPENDED MATERIALS RELEASED FROM REFUSE INCINERATORS, ANALYTICAL PROCEEDINGS PUBLISHED BY THE ROYAL SOCIETY OF CHEMISTRY (LONDON) , 18: 199-201.

81GLA 01 E. S. GLADNEY AND D. KNAB (1981) DETERMINATION OF SELENIUM IN TWENTY GEOLOGICAL REFERENCE

MATERIALS BY NEUTRON ACTIVATION AND INORGANIC ION EXCHANGE, GEOSTANDARDS NEWSLETTER, 5: 67-69.

81GLA 02 E. S. GLADNEY AND D. R. FERRIN (1981) INSTRUMENTAL THERMAL NEUTRON ACTIVATION DETERMINATION OF 20 ELEMENTS IN NINETEEN SILICATE REFERENCE MATERIALS, GEOSTANDARDS NEWSLETTER, 5: 113-124.

B1GLA 03 E. S. GLADNEY, J. W. OWENS, T. C. GUNDERSON, AND W. E. GOODE

(1981), QUALITY ASSURANCE FOR ENVIRONMENTAL ANALYTICAL

CHEMISTRY: 1976-1979, LOS ALAMOS SCIENTIFIC LABORATORY REPORT LA-8730-MS, PP. 113-118.

81GLA 04 E. S. GLADNEY, U. E. GOODE, D. R. PERRIN, AND C. E. JURNS

(1981), QUALITY ASSURANCE FOR ENVIRONMENTAL ANALYTICAL

CHEMISTRY: 1980, LOS ALAMOS NATIONAL LABORATORY REPORT

LA- 8966-MS, PP. 108-114.

81GOU 01 P. D. GOULDEN, D. H. J. ANTHONY, AND K. D. AUSTEN (1981) DETERMINATION OF ARSENIC AND SELENIUM IN WATER, FISH, AND

SEDIMENTS BY INDUCTIVELY COUPLED ARGON PLASMA EMISSION

SPECTROMETRY, ANALYTICAL CHEMISTRY, 53: 2027-2029.

81HAB 01 S. HABIB AND M. J. MINSK! (1981) NEUTRON ACTIVATION TECHNIQUE FOR THE ANALYSIS OF THE

SOLUBLE AND PARTICULATE FRACTIONS OF RIVER WATER, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 63: 379-39 5.

81HAH 01 M. H. HAHA, R. W. KUENNEN, J. A. CARUSO, AND F. L. FICKE

(1981), TITLE UNKNOWN, JOURNAL OF AGRICULTURAL AND FOOD

CHEMISTRY, IN PRESS.

81HAM 01 H. HAMAGUCHI (1981) PRIVATE COMMUNICATION, IN 81YAM 01.

81HAN 01 H.-B. HAN, G. KAISER AND G. TOLG (1981) DECOMPOSITION OF BIOLOCICAL MATERIALS , ROCKS, AND SOILS

IN PURE OXYGEN UNDER DYNAMIC CONDITIONS FOR THE DETERMINATION OF SELENIUM AT TRACE LEVELS, ANALYTICA CHIMICA

ACTA, 128: 9-21.

81HIN 01 E. J. HINDERBERGER, M. L. KAISER, AND S. R. KOIRTYOHANN

(1981), FURNACE ATOMIC ABSORPTION ANALYSIS OF BIOLOGICAL SAMPLES USINC THE L'VOV PLATFORM AND MATRIX MODIFICATION

ATOMIC SPECTROSCOPY, 2: 1-7.

81HOR 01 J. J. HORVATH, J. D. BRADSHAW, J. N. BOWER, M. S. EPSTEIN, iS?TM„ I)~W1NEF0RDNER C 1981 ) , COMPARISON OF NEBULIZER- BURNER SYSTEMS FOR LASER-EXCITED ATOMIC FLUORESCENCE FLAME SPECTROMETRY , ANALYTICAL CHEMISTRY, 53: 6-9.

81IMU 01 H. IMURA AND N. SUZUKI (1981) SUBSTOICHIOMETRIC ISOTOPE DILUTION ANALYSIS FOR TIN WITH

SALICYLIDENEAMINO-2-THIOPHENOL COMPLEXATION IN NON- AQUEOUS MEDIUM, TALANTA, 28: 73-79.

81INU 01 T. INUI, S. TERADA, AND H. TAMURA (1981) DETERMINATION OF ARSENIC BY ARSINE GENERATION WITH REDUCING

TUBE FOLLOWED BY GRAPHITE FURNACE ATOMIC ABSORPTION

SPECTROMETRY, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE

305: 189-192.

81JAC 01 K. W. JACKSON, L. EBDON, D. C. WEBB AND A. G. COX (1981) DETERMINATION OF LEAD IN VEGETATION BY A RAPID MICROSAMPLING

CUP ATOMIC ABSORPTION PROCEDURE WITH SOLID SAMPLE INTRODUCTION, ANALYTICA CHIMICA ACTA, 128 : 67- 74 .

81JIN 01 S. JINGXIN, T. SHUDE, W. YUQI, C. BINGRU, Q. QINFANG, AND

Z. SHEN (1981), DETERMINATION OF 28 TRACE ELEMENTS IN SOILS

FROM MOUNT QOMOLANGMA RECION BY INAA, TAKEN FROM 81MTA 01.

81KIB 01 T. KIBA (1981) PRIVATE COMMUNICATION, IN 81 YAM 01.

81KIN 01 H. KINGSTON AND P. A. PELLA (1981) PRECONCENTRATION OF TRACE METALS IN ENVIRONMENTAL AND

BIOLOCICAL SAMPLES BY CATION EXCHANGE RESIN FILTERS FOR X-RAY SPECTROMETRY , ANALYTICAL CHEMISTRY, 53: 223-227.

81KNA 01 G. KNAPP, S. RAPTIS, G. KAISER, G. TOLG, P. SCHRAMEL, AND

B. SCHREIBER (1981), A PARTIALLY MECHANIZED SYSTEM FOR THE COMBUSTION OF ORGANIC SAMPLES IN A STREAM OF OXYCEN WITH

QUANTITATIVE RECOVERY OF THE TRACE ELEMENTS, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 308: 97-103.

81KOS 01 K. KOSTADINOV AND R. DJINGOVA (1981) TRACE ELEMENT ANALYSIS OF BIOLOGICAL MATERIALS BY THERMAL AND EPITHERMAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 63: 5-12.

81KRI 01 V. KRIVAN, H. GEIGER, AND H. E. FRANZ (1981)

BE STIMMUNG VON FE , CO, CU, ZN, SE, RB, UND CS IN NBS-OCHSEN- LEBER BLUTPLASMA UND ERYTHROCYTEN DURCH INAA UND AAS

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 305 : 399-404.

81KUC 01 J. KUCERA, AND J. J. M. DE GOEIJ (1981)

A COMPARISON OF TWO SEPARATION TECHNIQUES USING NAI(TL) AND

CE(LI) SPECTROMETRY FOR TRACE ELEMENT DETERMINATION IN BIOLOGICAL MATERIALS BY NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 63: 23-40.

81KUL 01 I. KULEFF, R. DJINGOVA, K. KOSTADINOV, AND D. TODOROVSKY

(1981), INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF TRACE ELEMENTS IN QUARTZ, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

62: 187-194

81KUL 02 I. KULEFF AND K. KOSTADINOV (1981) EPITHERMAL NEUTRON ACTIVATION ANALYSIS OF URANIUM BY NEPTUNIUM-2 39 USING HIGH RESOLUTION GAMMA- SPECTROMETRY

JOURNAL OF RADIOANALYTICAL CHEMISTRY, 63 : 397-404.

B1LAN 01 F.J. LANGMYHR AND I. M. DAHL (1981) ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF PHOSPHORUS

IN BIOLOGICAL MATERIALS, ANALYTICA CHIMICA ACTA, 131: 303-306

81 LEE 01 S. W. LEE AND J. C. MERANGER (1981) DETERMINATION OF TOTAL ARSENIC SPECIES BY ANODIC STRIPPING

VOLTAMMETRY, ANALYTICAL CHEMISTRY, 53: 130-131.

216
CODE N DESCRIPTION

CODE N DESCRIPTION 81MAR 01 D. F. MARINO AND J. D. INGLE (1981)

ION EXCHANGE SEPARATION OF COBALT FROM ALKALINE EARTH AND

SELECTED TRANSITION METALS WITH LOPHINE CHEMILUMINESCENCE

DETECTION, ANALYTICAL CHEMISTRY , 53: 292-294.

81MEY 01 A. MEYER, C. HOFER, G. KNAPP, AND G. TOLG (1981) SELENBESTIMMUNG IN UG/G AND NG/G BE REICH IN ANORGANISCHEN DND ORGANISCHEN MATRICES NACH VERDAMP FUNGS ANALYSE IM DYNAMISCHEN SYSTEM DURCH AAS, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 305: 1-10.

81MIZ 01 A. MIZUIKE AND A. UNO (1981) SURFACE TREATMENT OF BOROSILICATE GLASS BEAKERS FOR PREVENTION OF SODIUM CONTAMINATION, ANALYTICA CHIMICA ACTA,

124: 427-4 30.

81MOH 01 N. MOHAMED AND R. C. FRY (1981) SLURRY ATOMIZATION DIRECT ATOMIC SPECTRO CHEMICAL ANALYSIS OF ANIMAL TISSUE , ANALYTICAL CHEMISTRY, 53: 4 50-4 55.

81M0L 01 A. MOLOKH1A AND A. DYER (1981) SIMULTANEOUS DETERMINATION OF EIGHT TRACE ELEMENTS IN HUMAN SKIN BY INSTRUMENTAL NEUTRON-ACTIVATION ANALYSIS, ANALYST,

106: 1168-1173.

81MTA 01 MODERN TRENDS IN ACTIVATION ANALYSIS, SIXTH INTERNATIONAL

CONFERENCE, UNIVERSITY OF TORONTO, TORONTO, CANADA

JUNE 1981 ; ABSTRACTS.

81 NAD 01 R.A. NADKARNI (1981) DETERMINATION OF VOLATILE ELEMENTS IN COAL AND OTHER ORGANIC MATERIALS BY OXYGEN BOMB COMBUSTION, AMERICAN LABORATORY

,

13(8): 22-29.

81NAR 01 H. NARASAKI (1981) DETERMINATION OF TRACE MERCURY IN MILK PRODUCTS AND PLASTICS BY COMBUSTION IN AN OXYGEN BOMB AND COLD-VAPOUR

ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA ACTA,

125: 187-191.

81NEU 01 D. R. NEUMAN AND F. F. MUNSHOWER (1981) RAPID DETERMINATION OF MOLYBDENUM IN BOTANICAL MATERIAL BY ELECTROTHERMAL ATOMIC ABSORPTION SPECTROMETRY , ANALYTICA

CHIMICA ACTA, 123: 325-328.

81NIS 01 Y. NISHIKAWA (1981) PRIVATE COMMUNICATION, IN 81 YAM 01.

81NON 01 N. NONAKA, H. HIGUCHI, H. HAMAGUCHI, K. TOMURA (1981) LOSSES OF THE ELEMENTS DURINC DRY ASHING OF PLANT MATERIALS

,

BUNSEKI KAGAKU, 30: 599-604.

810GU 01 K. OGUMA AND R. KURODA (1981) DRY-COLUMN CHROMATOGRAPHY OF URANIUM. APPLICATION TO CHEMICAL ANALYSIS OF MONAZITE AND PHOSPHATE ROCK FOR URANIUM

MIKROCHIMICA ACTA (WIEN) 1981II: 57-67.

810WE 01 J. W. OWENS (1981) PRIVATE COMMUNICATION, ENVIRONMENTAL SURVEILLANCE GROUP, LOS ALAMOS NATIONAL LABORATORY, LOS ALAMOS, NEW MEXICO.

81PAII 01 B. PAHLANANPOUR, M. THOMPSON, AND L. THORNE (1981) SIMULTANEOUS DETERMINATION OF TRACE AMOUNTS OF ARSENIC, ANTIMONY AND BISMUTH IN HERBAGE BY HYDRIDE GENERATION AND INDUCTIVELY COUPLED PLASMA ATOMIC-EMISSION

SPECTROMETRY, ANALYST, 106: 467-471.

81PAR 01 P.P. PAREKH (1981) ENERGY-DISPERSIVE X-RAY FLUORESCENCE ANALYSIS OF ORGANICRICH SOILS AND SEDIMENTS, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 50: 1-14.

81PIC 01 C. J. PICKFORD (1981) DETERMINATION OF ARSENIC BY EMISSION SPECTROMETRY USING AN INDUCTIVELY COUPLED PLASMA SOURCE AND THE SYRINGE HYDRIDE

TECHNIQUE, ANALYST, 106: 464-467.

81PIH 01 B. PIHLAR, P. VALENTA, AND H. W. NURNBERG (1981) NEW HIGH-PERFORMANCE ANALYTICAL PROCEDURE FOR THE

VOLTAMMETRI C DETERMINATION OF NICKEL IN ROUTINE ANALYSIS OF WATERS, BIOLOCICAL MATERIALS, AND FOOD, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 307 : 337 - 346.

81P0S 01 R. S. POSEY AND R. W. ANDREWS (1981) DETERMINATION OF SELENIUM(IV) BY ANODIC STRIPPING VOLTAMMETRY WITH AN IN SITU GOLD-PLATED ROTATING GLASSY CARBON DISK ELECTRODE, ANALYTICAL CHIMICA ACTA, 124 : 107-112.

81 RAP 01 S. E. RAPTIS, W. WEGSCHEI DER, AND G. KNAPP (1981) THE DETERMINATION OF ARSENIC AT NG/G AND PPM LEVELS IN ORGANIC AND BIOLOGICAL MATRICES, HIKROCHIMICA ACTA (WIEN)

,

19811: 93-97

81REA 01 D. C. REAMER AND C. VEILLON (1981) PREPARATION OF BIOLOGICAL MATERIALS FOR DETERMINATION OF SELENIUM BY HYDRIDE GENERATION - ATOMIC ABSORPTION

SPECTROMETRY, ANALYTICAL CHEMISTRY, 53: 1192-1195.

81REA 02 D. C. REAMER AND C. VEILLON (1981) DETERMINATION OF SELENIUM IN BIOLOGICAL MATERIALS BY STABLE ISOTOPE DILUTION GAS CROMATOGRAPHY — MASS SPECTROMETRY, ANALYTICAL CHEMISTRY, 53: 2166-2169.

81 REE 01 J. REEDNICK (1981) SPECTROSCOPY ATOMIQUE: EXCITATION D'UN PLASMA DE HAUTE

ENERGIE ET SPECTROME TRIE DE RESOLUTION ELEVEE, ANALUSIS,

9: 14-20.

81REL 01 R. E. RELM AND D. D. HAVN (1981) DETERMINATION OF TOTAL SULFUR IN HYDROCARBONS BY REDUCTIVE

PYROLYSIS WITH POLAROGRAPHIC DETECTION, ANALYTICAL

CHEMISTRY, 53: 1088-1093.

81R0B 02 G. ROBAYE, G. WEBER, J. DELBROUCK, I. ROELANDTS, P. BARTSCH, AND A. COLLIGNON (1981), ATTEMPTS TO IMPROVE PIXE QUANTITATIVE TRACE ELEMENT ANALYSIS OF BIOMEDICAL MATERIALS, NUCLEAR INSTRUMENTS AND METHODS, 181 : 59-62.

81SAS 01 C. S. SASTRI, R. CALETKA, AND V. KRI VAN (1981) SIMULTANEOUS DETERMINATION OF BORON AND LITHIUM BY CHARGED

PARTICLE ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY,

53: 765-770.

81SAS 02 C. S. SASTRI, R. CALETKA, AND V. KRIVAN (1981) ANALYSIS OF REFRACTORY METALS FOR LITHIUM, BORON, AND

NITROGEN BY CHARGED PARTICLE ACTIVATION YIELDING BE-7 AS THE INDICATOR RADIONUCLIX, TAKEN FROM 81MTA 01.

81SEG 01 CH. SEGEBADE AND H.-U. FUSBAN (1981) URANIUM ANALYSIS BY ACTIVATION WITH 30 MEV-BREMSSTRAHLUNG

,

RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 48: 311-328.

81SHA 01 P. G. SHAW, D. MCKOWN, AND S. E. MANAHAN (1981) TRACE ELEMENT DETERMINATIONS IN SHALE OIL PRODUCTS BY NEUTRON ACTIVATION, ANALYTICA CHIMICA ACTA, 123: 65-74.

81SHI 01 T. SHIGEMATSU AND K. KUDO (1981) SUBSTOICHIOMETRIC DETERMINATION OF PHOSPHORUS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 67: 307-319

81SLO 01 H. A. VAN DER SLOOT, D. HOEDE, T. J. L. KLINKERS, AND

H. A. DAS (1981), THE DETERMINATION OF ARSENIC , SELENIUM, AND ANTIMONY IN ROCKS, SEDIMENTS, FLY ASH, AND SLAG, PROCEEDINGS OF THE SIXTH MODERN TRENDS IN ACTIVATION

ANALYSIS CONFERENCE , TORONTO, CANADA.

81STR 01 W. B. STROUBE, W. C. CUNNINGHAM, AND M. ALLEGRINI (1981) ACTIVATION ANALYSIS PROGRAM OF THE FOOD AND DRUG ADMINISTRATION AT THE NBSR, IN NBS REACTOR: SUMMARY OF ACTIVITIES JULY 1979 TO JUNE 1980, NBS TECHNICAL NOTE 1142, PP. 186-188.

81SUZ 01 S. SUZUKI, S. HIRAI AND K. NODA (1981) DETERMINATION OF SELENIUM IN HERB PLANTS BY NEUTRON ACTIVATION ANALYSIS USING A COINCIDENCE COUNTING METHOD, BUNSEKI

KAGAKU, 31: 67-71.

81SZY 01 P. J. SZYDLOWSKI, D. L. DUNMIRE, E. E. FECK, R. L. EGGERS, AND W. R. MATSON (1981), SIMULTANEOUS DETERMINATION OF IRON(II), IRON(III), AND TOTAL IRON IN SPHAGNUM MOSS PEAT

BY PROGRAMMABLE VOLTAMMETRY ON A GRAPHITE TUBULAR ELECTRODE, ANALYTICAL CHEMISTRY, 53: 193-196.

81TAN 01 K. TANABE, K. CHIBA, H. RARAGUCHI, AND K. FUWA (1981) DETERMINATION OF MERCURY AT THE ULTRA! RACE LEVEL BY ATMOSPHERIC PRESSURE HELIUM MICROWAVE-INDUCED PLASMA

EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 53: 1450-1453.

217
CODE N DESCRIPTION CODE N DESCRIPTION

81TOE 01 K. TOEI AND Y. SHIMOISHI (1981) DETERMINATION OF ULTRAMICRO AMOUNTS OF SELENIUM BY GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE DETECTION, TALANTA,

28: 967-972

81TUR 01 K. E. TURNER < 1981

PRIVATE COMMUNICATION, BHP. CENTRAL RESEARCH LABORATORIES, SHORTLAND, AUSTRALIA*

81UCH 01 T. UCHIDA, I. KOJIHA AND C. IIDA (1981) APPLICATION OF AN AUTOMATICALLY TRIGGERED DIGITAL INTEGRATOR

TO FLAME ATOMIC-ABSORPTION SPECTROMETRY OF COPPER USING A DISCRETE NEBULISATION TECHNIQUE , ANALYST, 106: 206-212.

81UCH 02 H. UCHIDA, Y. SHIMOISHI AND K. TOEI (1981) RAPID DETERMINATION OF TRACE AMOUNTS OF SELENIUM IN BIOLOGICAL SAMPLES BY GAS CHROMATOGRAPHY WITH ELECTRON-CAPTURE

DETECTION, ANALYST, 106: 757-762

81UTH 01 E. 0. UTKUS, M. E. COLLINGS, V. E. CORNATZER, AND

F. H. NIELSEN (1981), DETERMINATION OF TOTAL ARSENIC IN

BIOLOGICAL SAMPLES BY ARSINE GENERATION AND ATOMIC

ABSORPTION SPECTROMETRY, ANALYTICAL CHEMISTRY , 53: 2221-2224.

81VER 02 A. VERBUEKEN, E. MICHIELS, AND R. VAN GRIEKEN (1981) TOTAL ANALYSIS OF PLANT MATERIAL AND BIOLOGICAL TISSUE BY SPARK SOURCE MASS SPECTROMETRY, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEM1E, 309 : 300-304.

81WAL 01 G. F. WALLACE (1981) APPLICATION OF A SEQUENTIAL SCANNING ICP TO THE ANALYSIS OF GEOLOGICAL MATERIALS, ATOMIC SPECTROSCOPY, 2: 87-90.

81 UAL 02 G. F. WALLACE AND R. D. EDIGER (1981) OPTIMIZATION OF ICP OPERATING CONDITIONS FOR THE DETERMINATION OF SULFUR IN OILS, ATOMIC SPECTROSCOPY,

2: 169-172.

81WAN 01 L. E. WANGEN (1981) RELATIONSHIPS BETWEEN THE ELEMENTAL CONPOSITION AND PARTICLE

SIZES OF AEROSOLS WITH AND WITHOUT IMPACT FROM A COAL-FIRED

POWER PLANT, LOS ALAMOS SCIENTIFIC LABORATORY REPORT

LA-8759-MS.

81WEI 01 A. D. WEISS, R. N. SAVAGE AND G. M. HIEFTJE (1981) DEVELOPMENT AND CHARACTERIZATION OF A 9-MM INDUCTIVELYCOUPLED ARGON PLASMA SOURCE FOR ATOMIC EMISSION

SPECTROMETRY , ANALYTICA CHIMICA ACTA, 124 : 245-258.

81UIL 01 R. E. WILLIAMS, P. K. HOPKE, AND R. A. MEYER (1981) TRACE MULTIELEMENT ANALYSIS USING HIGH-FLUX FAST-NEUTRON

ACTIVATION, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

63: 187-199.

81UIL 02 R. E. WILLIAMS (1981) GAMMA-RAY SPECTROSCOPY FOLLOWING HIGH-FLUX 14-MEV NEUTRON

ACTIVATION, PH.D. THESIS, UNIVERSITY OF ILLINOIS, AND

UCRL-53208, LAWRENCE LIVERMORY LABORATORY REPORT.

81W0L 01 K. A. WOLNIK, F. L. FRICKE, H. H. HAHN, AND J. A. CARUSO

(1981), SAMPLE INTRODUCTION SYSTEM FOR SIMULTANEOUS DETERMINATION OF VOLATILE ELEMENTAL HYDRIDES AND OTHER

ELEMENTS IN FOODS BY INDUCTIVELY COULPED ARGON PLASMA

EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY , 53: 1030-1035.

81 YAM 01 M. YAMAMOTO, T. SHOHJII, T. KUMAMARU, AND Y. YAMAMOTO (1981) MASKING EFFECT OF POTASSIUM IODIDE ON THE INTERFERENCES IN

THE ATOMIC ABSORPTION SPECTROMETRIC DETERMINATION OF ANTIMONY UTILIZING STI BINE GENERATION BY SODIUM BOROHYDRIDE TABLET REDUCTION, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE

CHEMIE, 305: 11-14.

81YAN 01 K. YANAGI AND M. AMBE (1981) DETERMINATION OF ARSENIC IN BIOLOGICAL, ENVIRONMENTAL AND

GEOLOGICAL MATERIALS BY ARSINE EVOLUTION-FLAMELESS ATOMIC ABSORPTION SPECTROPHOTOMETRY, BUNSEKI KAGAKU , 30: 209-214.

81YAS 01 A. YASUI, H. KOIZUMI, AND C.TSUTSUMI (1981) DETERMINATION OF CALCIUM IN FOOD SAMPLES; APPLICATION OF ADDING INTERFERENCE SUPPRESSING REAGENT-ATOMIC ABSORPTION

SPECTROPHOTOMETRIC METHOD, BUNSEKI KAGAKU, 30: T65-T71.

B1YUZ 01 M. YUZAWA AND N. SUZUKI (1981) SUBSTOICHIOMETRIC ISOTOPE DILUTION ANALYSIS OF CALCIUM IN BIOLOGICAL MATERIAL, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

62: 115-124.

81ZAU 01 G.-P. ZAUKE (1981) CADMIUM IN GAMMARI DAE (AMPHIPODA: CRUSTACEA) OF THE RIVERS WERRA AND VESER: GEOGRAPHICAL VARIATION AND CORRELATION TO CADMIUM IN SEDIMENTS, ENVIRONMENTAL POLLUTION, 2: 465-4 74 .

82AKA 01 J. AKASH1, I. FUKUSHIMA, A. IHAHORI , S. SHIOBARA, Y. TAKAHASHI , AND K. TOMURA (1982), MULTIELEMENT ANALYSIS OF THE HAIR OF MIN- ING INDUSTRY WORKERS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 68: 59-65.

82BAR 01 U. BARTELS AND T. T. PHAM (1982) SPECTROPHOTOMETRIC DETERMINATION OF SULPHUR IN PLANTS USING SCHONIGER COMBUSTION AND DIME THYLSULPHONAZO III, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE , 310: 13-15.

82 BEN 01 H. BENARD AND M. PI NTA (1982) DETERMINATION OF ARSENIC IN ATMOSPHERIC AEROSOLS BY ATOMIC

ABSORPTION WITH ELECTROTHERMAL ATOMIZATION , ATOMIC

SPECTROSCOPY, 3: 8-12.

82BYR 01 A.R. BYRNE (1982) SIMULTANEOUS RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS OF VANADIUM, MOLYBDENUM AND ARSENIC IN BIOLOGICAL SAMPLES, RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 52: 99-1 10.

82CAL 01 G. CALDERONI AND T. FERRI (1982) DETERMINATION OF THALLIUM AT SUBTRACE LEVEL IN ROCKS AND MINERALS BY COUPLING DIFFERENTIAL PULSE ANODIC- STRIPPING VOLTAMMETRY WITH SUITABLE ENRICHMENT METHODS, TALANTA, 29: 371-37 5.

82CHA 01 J. F. CHAPMAN AND L. S. DALE (1982) THE USE OF ALKALINE PERMANGANATE IN THE PREPARATION OF BIO- LOGICAL MATERIALS FOR THE DETERMINATION OF MERCURY BY ATOMIC ABSORPTION SPECTROMETRY , ANALYTICA CHIMICA ACTA, 134 : 379-382.

82CHR 01 J. K. CHRISTEN SEN , L. KRYCER AND N. PIND (1982) THE DETERMINATION OF TRACES OF CADMIUM, LEAD AND THALLIUM IN FLY ASH BY POTENTIOMETRIC STRIPPING ANALYSIS, ANALYTICA

CHIMICA ACTA, 141: 131-146.

82 CLE 01 M.S. CLEGG, C.L. KEEN, B. LONNERDAL, AND L.S. HURLEY ( 1982) ANALYSIS OF TRACE ELEMENTS IN ANIMAL TISSUES. DETERMINATION

OF MANGANESE BY GRAPHITE FURNACE ATOMIC ABSORPTION SPECTRO- PHOTOMETRY, BIOLOGICAL TRACE ELEMENT RESEARCH, 4: 145-156.

8200H 01 I.M. COHEN, S.M. RESNIZKY, G.B. BARO (1982) ACTIVATION ANALYSIS OF THALLIUM BY TL-203(N,2N)TL-202 REACTION

IN NUCLEAR REACTORS , JOURNAL OF RADIOANALYTICAL CHEMISTRY , 72: 451-461.

8200N 01 C. P. CONRAD, M. W. ROWE, AND E. S. GLADNEY (1982) COMPARATIVE DETERMINATION OF URANIUM IN SILICATES BY DELAYED NEUTRON ACTIVATION ANALYSIS, GEOSTAN DARDS NEWSLETTER,

6: 1-4.

8200R 01 E. CORTES, N. GRAS, L. MUNOZ , AND V. CASSORLA (1982) A STUDY OF SOME TRACE ELEMENTS IN INFANT FOODS, JOURNAL

OF RADIOANALYTICAL CHEMISTRY, 69: 4 01-415.

82CR0 01 J. G. CROCK AND F. E. LICHTE (1982) DETERMINATION OF RARE EARTH ELEMENTS IN GEOLOGICAL MATERIALS

BY INDUCTIVELY COUPLED ARGON PLASMA/ATOMIC EMISSION

SPECTROMETRY, ANALYTICAL CHEMISTRY , 54: 1329-1332.

82CUR 01 D. B. CURTIS (1982) PRIVATE COMMUNICATION, GROUP INC-7, LOS ALAMOS NATIONAL

LABORATORY.

8 2 DAK 01 T. DAKUBU AND M.D. SWAINE ( 1982) CALCIUM AND POTASSIUM LEVELS IN LEAVES MEASURED BY X-RAY FLUORESCENCE ANALYSIS, INTERNATIONAL JOURNAL OF APPLIED RADIATION ISOTOPES, 33: 193-196.

82DAM 01 E. DAMSGAARD, K. OSTERGAARD, AND K. HEYDORN (1982) CONCENTRATIONS OF SELENIUM AND ZINC IN HUMAN KIDNEYS, JOURNAL OF RADIOANALYTICAL CHEMISTRY , 70: 67-76.

218
CODE N DESCRIPTION CODE N DESCRIPTION

82DOO 01 K.J. DOOLAN (1982) THE DETERMINATION OF TRACES OF MERCURY IN SOLID FUELS BY HIGH-TEMPERATURE COMBUSTION AND COLD-VAPOUR ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA ACTA, 140: 187-195.

82EBD 01 L. EBDON, J.R. WILKINSON AND K.W. JACKSON (1982)

IETERMINATION OF MERCURY IN COAL BY NON-OX1DATIVE PYROLYSIS AND COLD VAPOUR ATOMIC-FLUORESCENCE SPECTROMETRY , ANALYST,

107: 269-275.

B2EBD 02 L. EBDON AND W.C. PEARCE (1982) DIRECT DETERMINATION OF ARSENIC IN COAL BY ATOMIC-ABSORPTION

SPECTROSCOPY USING SOLID SAMPLING AND ELECTROTHERMAL ATOMISATION, ANALYST, 107: 94 2-950.

82EHM 01 W.D. EHMANN, W.R. MARKESBERY, T.I.M. HOSSAIN, M. ALAUDDIN, AND

D. T. GOODIN (1982), TRACE ELEMENTS IN HUMAN BRAIN TISSUE BY

1NAA, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 70: 57-65.

82ELS 02 CM. ELSON, J. KILLEY AND A. CHATT (1982) DETERMINATION OF ARSENIC AND ANTIMONY IN GEOLOGICAL MATERIAL AND NATURAL WATERS BY COPRECIPITATION WITH SELENIUM AND

NEUTR04 ACTIVATION-GAMMA SPECTROMETRY, ANALYTICA CHIMICA

ACTA, 14 2: 269-275

82FLA 01 F. J. FLANAGAN, R. MOORE, AND P. J. ARUSCAVAGE (1982) MERCURY IN GEOLOCIC REFERENCE SAMPLES, GEOSTAN DARDS NEWSLETTER, 6: 25-46.

82GAJ 01 R.J. GAJAN, S.G. CAPAR, C.A. SUBJOC, AND M. SANDERS (1982) DETERMINATION OF LEAD AND CADMIUM IN FOODS BY ANODIC STRIPPING VOLTAMMETRY: I. DEVELOPMENT OF METHOD, JOURNAL OF THE

ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 65: 970-975.

82CLA 02 E. S. GLADNEY, D. R. PERRIN, C. E. BURNS, R. ROBINSON (1982) QUALITY ASSURANCE FOR ENVIRONMENTAL ANALYTICAL CHEMISTRY:

1981, LOS ALAMOS NATIONAL LABORATORY REPORT, LA-9579-MS,

PP. 100-105.

82GOL 01 J. GOLDBERG AND R. SACKS ( 1982) DIRECT DETERMINATION OF METALLIC ELEMENTS IN SOLID, POWDER

SAMPLES WITH ELECTRICALLY VAPORIZED THIN FILM ATOMIC EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 54 : 2 179-2 186.

82GRA 01 C. C. GRAHAM, M. D. GLASCOCK, J. J. CARNI, J. R. VOGT, AND

T. G. SPALDING (1982), DETERMINATION OF ELEMENTS IN NATIONAL

BUREAU OF STANDARDS' GEOLOGICAL STANDARD REFERENCE MATERIALS

BY NEUTRON ACTIVATION ANALYSIS, ANALYTICAL CHEMISTRY,

54: 1623-1627.

82GRI 01 A. P. GRI MAM IS , G.D. KAN IAS ( 1982) RAPID DETERMINATION OF MERCURY IN BIOLOGICAL MATERIALS BY RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIO- ANALYTICAL CHEMISTRY, 72: 587-595.

82GRO 01 Z. GROBENSKI, R. LEHMANN, R. TAMM, AND B. WELZ (1982) IMPROVEMENTS IN GRAPHITE FURNACE ATOMIC ABSORPTION

MICROANALYSIS WITH SOLID SAMPLING , MIKROCHIMICA ACTA (WIEN)

1982 I: 115-125.

82GUP 02 J. G. SEN GUPTA (1982) FLAME AND GRAPHITE FURNACE ATOMIC ABSORPTION AND OPTICAL

EMISSION SPECTROSCOPIC DETERMINATION OF YTTRIUM AND THE RARE-EARTH CONTENTS OF SIXTEEN INTERNATIONAL REFERENCE

SAMPLES OF ROCKS AND COAL, GEOSTAN DARDS NEWSLETTER,

6 : 241-248.

8 2 HAD 01 I. HADZISTELIOS AND C. PAPADOPOULOU (1982) RADIOCHEMICAL DETERMINATION OF MOLYBDENUM IN BIOLOGICAL

TISSUES BY ION EXCHANGE, JOURNAL OF RADIOANALYTICAL CHEMISTRY

72: 597-607

82 HAH 01 M. H. HAHN, K. A. WOLNIK, F. L. FRICKE, AND J. CARUSO (1982) HYDRIDE GENERATION/CONDENSATION SYSTEM WITH AN INDUCTIVELY COUPLED ARGON PLASMA POLYCHROMATOR FOR DETERMINATION OF ARSENIC, BISMUTH, GERMANIUM, ANTIMONY , SELENIUM, AND TIN

IN FOODS, ANALYTICAL CHEMISTRY, 54: 1048-1052.

82HEI 01 H. HE1NRICHS AND H. KELTSCH (1982) DETERMINATION OF ARSENIC, BISMUTH, CADMIUM, SELENIUM, AND

THALLIUM BY ATOMIC ABSORPTION WITH A VOLATILIZATION

TECHNIQUE , ANALYTICAL CHEMISTRY, 54: 1211-1214.

82HOE 01 M. HOENIG, C. LIMA ET S. DUPIRE (19B2) VALIDITE DES DETERMINATIONS PAR SPECTROMETR1 E D'ABSORPTION ATOMIQUE AVEC ATOMISAIION ELECTROTHERMIQUE DU CADMIUM

COBALT, CHROME, NICKEL ET PLOMB, ANALUSIS, 10: 132-139.

82H0E 02 M. HOENIG ET P. VAN HOEYWEGHEN (1982) APPLICATION DE LA SAA ELECTROTHERMIQUE A L' ANALYSE DES MATRICES COMPLEXES: CAS DE L' ARSENIC DAUS LES VEGETAUX, SPECTROCHIMICA ACTA, 37B: 817-828.

82INU 01 T. INUI, S.TERADA, H. TAMURA AND N. ICHINOSE (1982) DETERMINATION OF SELENIUM BY HYDRIDE GENERATION WITH REDUCING TUBE FOLLOWED BY GRAPHITE FURNACE ATOMIC ABSORPTION

SPECTROMETRY , FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE,

311: 492-495.

82JAG 01 D. JAGNER AND K. AREN (1982) PLOW POTENTIOMETRIC STRIPPING ANALYSIS FOR MERCURY(II) IN URINE, SEDIMENT AND ACID DIGEST OF BIOLOGICAL MATERIAL ANALYTICA CHIMICA ACTA, 14 1: 157-162.

82JEN 01 D. R. JENKE AND P. E. DIEBOLD (1982) CHARACTERIZATION OF PHOSPHORITE ORES, ANALYTICAL CHEMISTRY,

54: 1008-1011.

8 2JEN 02 D.R. JENKE AND R. WOODRIFF (1982) APPLICATION OP THE WOODRIFF CONSTANT TEMPERATURE GRAPHITE

FURNACE ATOMIZER TO ATOMIC SPECTROSCOPY, AMERICAN

LABORATORY, 14(8): 14-26.

82 JEN 03 CD. JENNINGS AND T.M. BEASLEY (1982) RADIOCHEMICAL DETERMINATION OF COBALT-60 IN ENVIRONMENTAL

SAMPLES, TALANTA, 29: 871-873.

82J0N 01 J. W. JONES, S. G. CAPAR, AND T. C. O'HAVER (1982) CRITICAL EVALUATION OP A MULTI-ELEMENT SCHEME USING PLASMA EMISSION AND HYDRIDE EVOLUTION ATOMIC-ABSORPTION

SPECTROMETRY FOR THE ANALYSIS OF PLANT AND ANIMAL TISSUES, ANALYST (LONDON), 107: 353-377.

82KEE 01 J. A. KEENAN AND D. HOLMES (1982) QUANTITATIVE TRACE ANALYSIS BY X-RAY FLUORESCENCE USING THE

COMPUTER PROGRAM NRLXRF, APPLIED SPECTROSCOPY, 36: 19-22.

82KIM 01 T. KIMURA, T. ISHIMORI , AND T. HAMADA (1982) REMOVAL OF SODIUM-24 BY A CHROMATOGRAPHIC EXTRACTION WITH A KIESELGUHR COLUMN AND A CROWN ETHER SOLUTION, ANALYTICAL

CHEMISTRY, 54: 1129-1131.

82KIR 01 T. KIRIYAMA AND R. KURODA (1982) COMBINED ION EXCHANGE-SPECTROPHOTOMETRIC METHOD FOR THE SI- MULTANEOUS DETERMINATION OF VANADIUM AND COBALT IN BIOLOGICAL MATERIALS , ANALYST, 107: 505-510.

82KIS 01 E. KISS (1982) DETERMINATION OF SILICA IN GEOLOGICAL MATERIALS BY ATOMIC ABSORPTION SPECTROMETRY, ANALYTICA CHIMICA ACTA, 140: 197-204.

82K0I 01 S.R. KOIRTYORANN, M.L. KAISER AND E.J. HINDERBERGER (1982) FOOD ANALYSIS FOR LEAD USING FURNACE ATOMIC ABSORPTION AND A L'VOV PLATFORM, JOURNAL OF THE ASSOCIATION OF OFFICIAL

ANALYTICAL CHEMISTS, 65: 999-1003.

82KRA 01 M. KRALTK (1982) RB-SR AGE DETERMINATIONS OF PRECAMBRIAN CARBONATE ROCKS OF THE CARFENTARIAN MCARTHUR BASIN, NORTHERN TERRITORIES, AUSTRALIA, PRECAMBRIAN RESEARCH, 18: 157-170.

82KRI 01 V. KRIVAN UND M. LANG (1982) RADIOTRACERS NTERSUCHUNJGEN ZUR DTREKTEN BESTIMMUNG VON KUPFER

IN BIOLOGISCHEN MATRICES DURCH FLAMMENLOSE AAS, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 312: 324-330

82KUE 01 R. W. KUENNEN, D. A. WOLNIK, F. FRICKE, AND J. CARUSO (1982) PRESSURE DISSOLUTION AND REAL SAMPLE MATRlf CALIBRATION FOR MULTIELEMENT ANALYSIS OP RAW AGRICULTURAL CROPS BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION SPECTROMETRY, ANALYTICAL CHEMISTRY, 54: 2146-2150.

82KUE 03 R. W. KUENNEN, M. H. HAHN, F. L. FRICKE, AND K. A. WOLNIK (1982) HYDRIDE GENERATION AND CONDENSATION FLAME ATOMIC ABSORPTION

SPECTROSCOPIC DETERMINATION OF ANTIMONY IN RAW COFFEE BEANS AND PROCESSED COFFEE, JOURNAL OP THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS. 65: 1146-I14B.

219
CODE N DESCRIPTION CODE N DESCRIPTION

82LAS 01 B. D. LASS, N. C. ROCHE, AND A. 0. SANNI , E. A. SCHWEIKERT, AND

J. ?. OJO (1982), HEAVY ION ACTIVATION ANALYSIS, JOURNAL OF RADIQANALYTICAL CHEMISTRY, 70: 251-272.

82LAU 01 J. C. LADL, E. A. LEPEL , W. C. WEIMER, AND N. WOGMAN ( 1982) PRECISE TRACE RARE EARTH ANALYSIS BY RADIOCHEMICAL NEUTRON ACTIVATION, JOURNAL OF RADIOANALYTICAL CHEMISTRY,

69: 181-196.

82LEU 01 P. C. LEUNG, K. S. SUBRAMANIAN, AND J. ME RANGER (1982) DETERMINATION OF ARSENIC IN POLLDTED WATERS BY DIFFERENTIAL

PULSE ANODIC-STRIPPING VOLTAKMETRY , TALANTA, 29: 515-518.

82LIA 01 C. F.-H. LIAO (1982) TELLURIUM AS CATALYST IN SEMIMICRO KJELDAHL METHOD FOR TOTAL NITROGEN DETERMINATION, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 65: 786-790.

82L0 01 J. M. LO, J. C. WEI, M, H. YANG, AND S. J. YEH (1982)

PRECONCENTRATION OF MERCURY WITH LEAD DIETHYLDITHIOCARBAMATE

FOR NEUTRON ACTIVATION ANALYSIS OF BIOLOGICAL AND ENVIRON- MENTAL SAMPLES, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 72: 571-585.

82LYO 01 D. J. LYONS AND R. L. ROOFAYEL (1982) DETERMINATION OF MOLYBDENUM IN PLANT MATERIAL USING INDUC- TIVELY COUPLED PLASMA EMISSION SPECTROSCOPY, ANALYST, 107: 331-334

82MAT 01 R. HATSUMOTO AND K. FUVA (1982) MOLECULAR EMISSION SPECTROMETRY WITH HYDRIDE GENERATION FOR DETERMINATION OF SUBNANOGRAM AMOUNTS OF ARSENIC, ANALYTICAL

CHEMISTRY, 54: 2012-2015.

82MAY 01 T. W. MAY (1982) RECOVERY OF ENDOGENOUS SELENIUM FROM FISH TISSUES BY OPEN SYSTEM DRY ASHING, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 65: 1140-1145.

82M1L 01 J. C. MILLS , I. E. TURNER, P. W. ROLLER, AND C. B. BELCHER (198 DIRECT DETERMINATION OF TRACE ELEMENTS IN COAL: WAVELENGTHDISPERSIVE X-RAY SPECTROMETRY WITH MATRIX CORRECTION USING COMPTON SCATTERED RADIATION, X-RAY SPECTROMETRY, 10: 131-137.

82M0R 01 J. MORTATTI, F. J. KRUG, L. C. R. PESSENDA, AND E. ZAGATTO (198 DETERMINATION OF IRON IN NATURAL WATERS AND PLANT MATERIAL

WITH 1 , 10-PHENANTHROLINE BY FLOW INJECTION ANALYSIS,

ANALYST, 107: 659-663.

82M0R 02 J. S. MORRIS, M. F. SMITH, R. E. MORROW , E. D. H EIMANN,

J.C. HANCOCK, AND T. GALL (1982) INAA DETERMINATION OF SELENIUM VIA SE-77M IN PLASMA, SEMEN AND HAIR SAMPLES FROM BEEF AND DAIRY BULLS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 69: 473-494.

82NAD 01 R. A. NADKARNI (1982) APPLICATIONS OF HYDRIDE GENERATION-ATOMIC ABSORPTION

SPECTROMETRY TO COAL ANALYSIS, ANALYTICA CHIMICA ACTA,

135: 363-368.

82NAD 02 R. A. NADKARNI, R. I. BOTTO, AND S. E. SMITH (1982) COMPARISON OF TWO ATOMIC SPECTROSCOPIC METHODS FOR ELEMENTAL ANALYSIS OF GEOLOGICAL MATERIALS, ATOMIC SPECTROSCOPY,

3: 180-184.

82NYG 01 D. D. NYGAARD AND J. H. LOVRY (1982) SAMPLE DIGESTION PROCEDURES FOR SIMULTANEOUS DETERMINATION

OF ARSENIC, ANTIMONY, AND SELENIUM BY INDUCTIVELY COUPLED

ARGON PLASMA EMISSION SPECTROMETRY WITH HYDRIDE GENERATION, ANALYTICAL CHEMISTRY, 54 : 8 0 3-807.

820BR 01 I. OBRUSNTJC AND S. POSTA (1982) INSTRUMENTAL NEUTRON ACTIVATION ANALYSIS OF NBS 1633A FLY ASH AND 1632A BITUMINOUS COAL REFERENCE SAMPLES WITH THE USE OF SHORT IRRADIATION, GEOSTANDARDS NEWSLETTER, IN PRESS.

820HA 01 M. OMAR AND H. J. M. BOWEN (1982) FRE-CONCENTRATION OF ENVIRONMENTAL TIN AND ITS DETERMINATION

USING CATECHOL VIOLET, ANALYST, 107: 654-658.

820WE 01 J. W. OWENS, E. S. GLADNEY , AND D. KNAB (1982) DETERMINATION OF BORON IN GEOLOGICAL MATERIALS BY INDUCTIVELY-COUPLED PLASMA EMISSION SPECTROMETRY

ANALYTIC* CHIMICA ACTA. 135: 169-172.

82POL 01 H. POLKOWSKA-MOTRENKO , M. DERMELJ , A. R. BYRNE , A. FAJGEU

P. STECNAR, AND L. KOSTA (1982) RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS OF SELENIUM USING CARBAMATE EXTRACTION, RADIOCHEMICAL AND RADIOANALYTICAL

LETTERS, 53 : 319 -328.

82PRE 01 J. R. FREER, B. R. STEPHENS, AND C. W. BLAND ( 1982) SAMPLE PREPARATION IN DETERMINATION OF LEAD IN GARDEN VEGE- TABLES BY FLAME ATOMIC ABSORPTION SPECTROPHOTOMETRY

JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS,

65: 1010-1014.

82QUR 01 I. H. QURESHI , M. S. CHAUDHARY.AND S. AHMAD ( 1982) TRACE ELEMENT CONCENTRATION IN HEAD HAIR OF THE INHABITANS OF THE RAWALPINDI- ISLAMABAD AREA, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 68: 209-218.

82RAI 01 T.C. RAINS, T.A. RUSH, AND T.A. BUTLER ( 1982) INNOVATIONS IN ATOMIC ABSORPTION SPECTROPHOTOMETRY WITH

ELECTROTHERMAL ATOMIZATION FOR DETERMINING LEAD IN FOODS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS,

65: 994-999.

82RIT 01 C. J. RITTER (1982) THE DRY-ASHING METHOD OF PREPARINC SEWAGE SLUDGE FOR CD AND

PB DETERMINATIONS BY AAS, AMERICAN LABORATORY

14(6):72-73.

82ROE 01 K. K. ROE, W. C. BURNETT, K. H. KIM, AND M. J. BEERS (1982) EXCESS PROTACTINIUM IN PHOSPHATE NODULES FROM A COASTAL UP- WELLING ZONE, EARTH AND PLANETARY SCIENCE LETTERS, 60: 39-4 6.

82R0E 02 I. ROELANDTS, G. ROBAYE, G. WEBER, J.H. DELBROUCK

P. BARTSCH, A. COLLIGNON, J. YUJIE (1982) NON-DESTRUCTIVE DETERMINATION OF BROMINE IN BLOOD SERUM SAMPLES USING PROTON INDUCED X-RAY EMISSION SPECTROMETRY

RADIOCHEMICAL AND RADIOANALYTICAL LETTERS, 50: 319-332.

82SAR 01 R. C. SARKAR AND M. S. DAS ( 1982) DIFFERENTIAL SPECTROPHOTOMETRIC DETERMINATION OF SILICA IN ROCKS AS ALPHA-MOLYBDOSILICIC ACID IN PRESENCE OF PHOSPHATE

AND OTHER INTERFERENCES, ANALYTICA CHIMICA ACTA, 134 : 4 01-4 05.

82SAT 01 T. SATO AND T. KATO ( 1982) ESTIMATES OF IODINE IN BIOLOGICAL MATERIALS BY EPITHERMAL

NEUTRON ACTIVATION ANALYSIS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 68: 175-180.

82SAT 02 R. D. SATZGER, C. S. CLOW , E. BONNIN, AND F. L. FRICKE ( 1982) DETERMINATION OF BACKGROUND LEVELS OF LEAD AND CADMIUM IN

RAW AGRICULTURAL CROPS BY USING DIFFERENTIAL PULSE ANODIC STRIPPING VOLTAMME TRY , JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS, 65: 987-991.

82SCH 01 P. SCHRAMEL AND XU LI-QIANG (1982) DETERMINATION OF BERYLLIUM IN THE PARTS-PER-BILLION RANGE IN THREE STANDARD REFERENCE MATERIALS BY INDUCTIVELY COUPLED

PLASMA ATOMIC EMISSION SPECTROMETRY , ANALYTICAL CHEMISTRY,

54: 1333-1336.

82SCH 03 A. A. SCHILT AND M. R. DI TUSA (1982) SPECTROPHOTOMETRIC DETERMINATION OF IRON AND REDUCING AGENTS WITH PPTS, A NEW WATER-SOLUBLE FERROIN-TYPE CHROMOGEN OF SUPERIOR SENSITIVITY, TALANTA, 29: 129-132.

82SCH 04 P. SCHRAMEL, XU LI-QIANG, A. WOLF, AND S. HASSE (1982) ICP-EMISSIONSPEKTROSKOPIE: EIN ANALYTISCHES VERFAHREN ZUR KLARSCHLAMM UND BODENUBERWACHUNG IN DER ROUTINE, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 313: 213-216.

82SCH 05 J.O. SCHMIDT, L. PALGAARD, J. WESTERMANN, AND M. E. MCCLAIN (1982) DETERMINATION OF BORON BY FAST INSTRUMENTAL NEUTRON ACTIVATION

ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 72 : 4 2 5-4 36.

82SEG 01 C. SEGEBADE, M. KUHL, B. F. SCHMITT, AND R. NEIDER (1982)

SOME REMARKS ON THE STATE OF PHOTON ACTIVATION ANALYSIS AND

THE USE OF INTERNAL STANDARDS, JOURNAL OF RADIOANALYTICAL

CHEMISTRY, 72: 665-696.

82SMI 01 D. H. SMITH, J. R. WALTON, H. S. MCKOWN, R. L.WALKER, AND J. A. CARTER (1982), A MOBILE MASS SPECTROMETRY LABORA- TORY FOR ISOTOPIC RATIO MEASUREMENTS OF URANIUM AND PLUTONIUM, ANALYTICA CHIMICA ACTA, 142: 355-359.

220
CODE H INSCRIPTION

CODE N DESCRIPTION

8 2 SUB 01 K.S. SUBRAMANIAN AND J.C. ME RANGER (1962) RAPID HYDRIDE EVOLUTION-ELECTRO THERMAL ATOMISATION ATOMIC- ABSORPTION SPECTROPHOTOMETRIC METHOD FOR DETERMINING ARSENIC AND SELENIUM IN HUMAN KIDNEY AND LIVER, ANALYST, 107 : 157-162.

82SUZ 01 M. SUZUKI AND K. OHTA (1982) REDUCTION OF INTERFERENCES WITH THIOUREA IN THE DETERMINA- TION OF CADMIUM BY ELECTROTHERMAL ATOMIC ABSORPTION SPECTROMETRY, ANALYTICAL CHEMISTRY , 54: 1686-1689.

82SUZ 02 S. SUZUKI AND S. BIRAI (1982) DETERMINATION OF TRACE ELEMENTS IN COAL AND FLY ASH BY NEU- TRON ACTIVATION ANALYSIS, BUNSEKI KAGAKU , 31: 44 3-449.

82SUZ 03 M. SUZUKI AND K. OHTA (1982) DETERMINATION OF STRONTIUM IN BIOLOGICAL SAMPLES BY ATOMIC EMISSION SPECTROMETRY WITH ELECTROTHERMAL ATOMIZATION, FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 313: 34-37.

82TAM 01 G. K. H. TAM AND G. LA CROIX (1982)

DRY ASHING, HYDRIDE GENERATION ATOMIC ABSORPTION SPECTRO- METRIC DETERMINATION OF ARSENIC AND SELENIUM IN FOODS, JOURNAL OF THE ASSOCIATION OF OFFICIAL ANALYTICAL CHEMISTS,

65: 647-651.

82TER 01 S. TERASHIMA (1982) DETERMINATION OF TRACE AMOUNTS OF TIN IN SEVENTY-THREE GEOCHEMICAL REFERENCE SAMPLES BY ATOMIC ABSORPTION

SPECTROMETRY, GEOSTANDARDS NEWSLETTER, 6: 77-81.

82TH0 02 J. THOMSON (1982) A TOTAL DISSOLUTION METHOD FOR DETERMINATION OF THE ALPHA- EMITTING ISOTOPES OF URANIUM AND THORIUM IN DEEP-SEA SEDIMENTS, ANALYTICA CHIMICA ACTA, 142: 259-268.

82TIN 01 B.T.G. TING, J. PAGOUNES, M. JANGHORBANI, AND V. R. YOUNG (1982 RADIOCHEMICAL NEUTRON ACTIVATION ANALYSIS OF STABLE ISOTOPES

IN RELATION TO HUMAN MINERAL NUTRITION, JOURNAL OF RADIO- ANALYTICAL CHEMISTRY, 70: 133-144.

82UCH 02 H. UCHIKAWA, R. FURUTA, AND Y. MI KARA (1982) THE DETERMINATION OF TRACE MERCURY IN SOLID FUEL BY ATOMIC ABSORPTION SPECTROPHOTOMETRY, BUNSEKI KAGAKU, 31: 367-372.

82VAN 01 C. VANOETEREN, R. CORNELIS, J. VERSIECK, J. HOSTE, AND

J. DE ROOSE (1982), TRACE ELEMENT PATTERNS IN HUMAN LUNG TISSUES, JOURNAL OF RADIO/ANALYTICAL CHEMISTRY, 70 : 219-238.

82VER 03 M. VERLINDEN (1982)

ON THE ACID DECOMPOSITION OF HUMAN BLOOD AND PLASMA FOR THE DETERMINATION OF SELENIUM, TALANTA, 29: 875-882.

82VIS 01 P. VISWANADHAM, D. R. SMICK, F. F. PISNEY, AND W. DILWORTH

(1982) , COMPARISON OF ION CHROMATOGRAPHY AND TITRIMETRY FOR DETERMINATION OF SULFUR IN FUEL OILS, ANALYTICAL CHEMISTRY,

54 : 24 31-24 33.

82VOG 01 J. R. VOGT, C. C. GRAHAM, M. D. GLASCOCK, R. H. COBEAN (1982) A STUDY OF ME SOAMERICAN OBSIDIAN SOURCES USING ACTIVATION

ANALYSIS, JOURNAL OF RADIOANALYTICAL CHEMISTRY, 69: 271-289.

82WE1 01 A. WEITZ, G. FUCHS UND K. BACHMANN (1982) AAS-BESTIMMUNG VON CADMIUM UND BLEI IN BIOLOCISCHEN PROBEN UND BODENPROBEN NACH AST RENNUNC DURCH VERFLUCHTIGUNG

FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 313 : 38-42.

82WIL 01 J. R. WILKINSON, L. EBDON, AND K. W. JACKSON (1982) DETERMINATION OF VOLATILE TRACE METALS IN COAL BY ANALYTICAL

ATOMIC SPECTROSCOPY, ANALYTICAL PROCEEDINGS PUBLISHED BY THE

ROYAL SOCIETY OF CHEMISTRY (LONDON) , 19: 305-307.

82WIL 02 S. A. WILSON AND C. A. GENT (1982) THE DETERMINATION OF FLUORIDE IN GEOLOGIC SAMPLES BY ION CHROMATOGRAPHY, ANALYTICAL LETTERS, 15: 851-864.

83GLA 01 E. S. G1ADNEY, C. E. BURNS, D. R. PERRIN, R. D. ROBINSON, AND D. KNAB (1983), QUALITY ASSURANCE FOR ENVIRONMENTAL ANALYTICAL CHEMISTRY: 1982, LOS ALAMOS NATIONAL LABORATORY

REPORT, IN PRESS.

83GLA 02 E. S. GLADNEY, D. R. PERRIN, R. D. ROBINSON, AND P. TRUJILLO

(1983) , EVALUATION OF NBS URBAN AIR PARTICULATE STANDARD

REFERENCE MATERIAL FOR QUALITY ASSURANCE PROGRAMS

IN PREPARATION.

221

83GLA 03 E. S. GLADNEY (1983) UNPUBLISHED DATA, LOS ALAMOS NATIONAL LABORATORY.

83KNA 01 D. KNAB (1963) AN INVESTIGATION OF THE ANALYSIS OF ENVIRONMENTAL SAMPLES

FOR FLUORIDE, SUBMITTED TO ANALYTICAL CHEMISTRY.
NBS-114A (REV. 2-8C)

11U.j.C P1CDT U t r f~* P" C (") KA KA | , U r \J iWIIVI 1 PIIRI ITATION OR A-y « Pprfnrm 1 CI 1 KJ 1 1 1 1 in1 1 1 o£ Hro^n 1 Kali. RI \ PHftrf CpUl L MnMUi 3. Publ ication Date

BIBLIOGRAPHIC DATA

REPORT NO.

March 1984 SHEET (See instructions) NBS SP 260-88

4. title and su btitle standard Reference Materials:

1982 Compilation of Elemental Concentration Data for NBS Biological, Geological,

and Environmental Standard Reference Materials

5. author(S) Ernest a Gladney, Colleen E. Burns, Daniel R. Perrin, Iwan Roelandts,

Thomas E. Gills

6. PERFORMING ORGANIZATION (If joint or other than NBS. see instructions)

NATIONAL BUREAU OF STANDARDS

DEPARTMENT OF COMMERCE

WASHINGTON, D.C 20234

7. Contract/Grant No.

8. Type of Report & Period Covered

Final

9. SPONSORING ORGANIZATION NAME AND COMPLETE ADDRESS (Street, City. State, ZIP)

Los Alamos National Laboratory National Bureau of Standards

Los Alamos, New Mexico 87545 * Washington, DC 20234

Uni versi te de Liege

B-4000 Sart-Tilman Par Liege 1, Belgium

10. SUPPLEMENTARY NOTES

Library of Congress Catalog Card Number: 84-601009

] Document describes a computer program; SF-185, FlPS Software Summary, is attached.

11. ABSTRACT (A 200-word or less factual summary of most significant information. If document includes a significant

bibliography or literature survey, mention it here)

Concentration data on 88 constituents in 75 NBS Standard Reference Materials have

been collected from over 850 journal articles and technical reports. These data

are summarized into mean values with uncertainties expressed as +/- one standard

deviation and compared with available certification data from NBS. Data are

presented on the analytical procedures employed and all raw data are given in the

Appendices

.

12. KEY WORDS (Six to twelve entries; alphabetical order- capitalize only proper names; and separate key words by semicolons)

Analytical methods; biological; certified; compilation; environmental; geological;

information values; literature values; mean values; Standard Reference Materials

13. AVAILABILITY

£X] Unlimited

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| For Official Distribution. Do Not Release to NTIS

5<LOrder From Superintendent of Documents, U.S. Government Printing Office, Washington, D.C.

20402.

Order From National Technical Information Service (NTIS), Springfield, VA. 22161

14. NO. OF

PRINTED PAGES

231

15. Price

<r U.S. GOVERNMENT PRINTING OFFICE: 1984-421-997:31 USCOMM-DC 6043-P80
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