GREAT OAK ENERGY, INC. February 28, 2011 Dept. of Environmental Protection Bureau of Waste Management 400 Waterfront Drive Pittsburgh, PA 15222 To Whom

It May Concern:

....., c::::::» ::£ :Dot :::::0 I - -o :X - .. 0 N Enclosed please find Great Oak Energy, Inc.'s Form 26R

, Chemical Analysis of Residual Waste Generated, for our Export Fuel #1 Marcellus well.
If you need any additional information
or have any questions, please feel free to contact Ed Klammer
at our office, as indicated on the report. Sincerely, Donna T. Hogue Enclosure

637 ALLEGHENY AVENUE P.O. BOX445 OAKMONT, PA 15139-0445 PHONE

: 412-828-2900 FAX

: 412-828

- 8942

(.() 0 c: **~** :I: **~0** 1"'"1" **(/1~** ---1"""0 7.l ["f1 (;) ,-.. • .7 ·- ?"2540-PM-BWM0347 'Rev. **~/2011** g **~~~~~~!~.!!..** COMMONWEALTH

OF PENNSYLVANIA DEPARTMENT
OF ENVIRONMENTAL PROTECTION BUREAU OF WASTE MANAGEMENT FORM 26R CHEMICAL ANALYSIS OF RESIDUAL WASTE ANNUAL REPORT BY THE GENERATOR This form must be fully and accurately completed.
All required Information must be typed or legibly printed
In the spaces provided.

If additional space Is necessary, identify each attached sheet as Form 26R, reference the Item number and Identify the date prepared. The date on attached sheets needs to match the date noted below. General Reference 287.54 Date Prepared/Revised 02/24/11 c. Physical Appearance

- 1 -

EPA
ID#2540-PM-BWM0347Rev.1/2011anpollutioncontrolprocessesproducingthewaste,asspecifiedIntheInstructions,isattached.b.Acontrolprocessesproducingthewaste,NoasspecifiedIntheInstructions,Isattached.c.arethe substantiationforN/Aaclaim,asdescribedIntheInstructions,Isattached.a.b.c.SolidwastepermitnuPA0091472FacilityNameAddressLine1AddressLine1AddressCityStateZIPMunicipalityTitlePhoneNameConemaughTownshipIndianaEmailAddressd.Volumeofwasteshippedtoprocessingordisposalyear.DcuydDgalDlbDton(checkone)a.Solidwastepermitnumber(s)forprocessingordisposalfacilityb.FacilityNameAddressLine1AddressLine1AddressCityStateZIPMunicipality.C.TitlePhoneNamentytoprocessingordisposalfacilityInthepreviousyear.DcuydDgalDlbDton(checkone)Dton(checkone)-2-2540-PM-BWM0347
Rev. 1/2011 I certify, under penalty of law, that

I have personally examined and

· am familiar with the Information submitted

in this Annual Report and all attached documents and that based upon my inquiry of those Individuals Immediately responsible for obtaining the Information,

I verify that the submitted Information

Is true, accurate and complete
to the best of my knowledge.

I understand that the submission
of false Information herein
Is made subject to the penalties of 18 Pa. C.S. §4904, relating to unsworn falsification

to authorities, which include fine and imprisonment. Check the following,

If applicable: 0

I certify the Information required

In Section B-1, General Properties was supplied to the Department for the year __ and has not changed. Form Submitted:

0 0 Date Submitted:
Form 26R Other (specify) 0

I certify the information required
in Section B-2, Chemical Analysis was supplied to the Department for the year _and has not changed. Form Submitted:

0 Form 26R 0 Other (specify) Date Submitted: 0

I certify the information required
In Section B-3, Process Description and Schematic, was supplied to the Department for the year __ and has not changed. Form Submitted:

0 Form 26R Date Submitted: Name of Responsible Official Edward A. Klammer Signature

0 Other (specify)

Title Vice President Date 2/24/11 -3
-Form 26R Chemical Analysis of Residual Waste Annual Report by the Generator Attachment

to Great Oak Energy Report Dated February 24, 2011 SECTION

B. WASTE DESCRIPTION Item 2. Chemical Analysis Attachments a. Two waste streams have been generated
by the Export Fuel #1 and the waste was segregated prior to disposal. The first waste stream was used frac fluid. The analysis of the sample drawn by McCutcheon Enterprises
on May 13, 2010,
is included. The second waster stream
is production brine.
A detailed analysis of waste drawn on May 27, 2010,
is included. b . Frac fluid samples were drawn by McCutcheon Enterprises. Great Oak Energy, Inc

. does not have details of the sampling method. Brine samples were drawn from the tank battery at the well location by Great Oak Energy, Inc. personnel. The samples were collected

in clean, apparently un-used containers provided by Environmental Service Labs (ESL) and according
to instructions provided by ESL. The samples were delivered
to ESL the same day as collected. c . Environmental Service Laboratories, Inc. (ESL) is accredited
by the Pennsylvania Department

of Environmental Protection.

A letter indicating their accreditation

is included. The Report of Analysis

in Section B.2.a. indicates the test methods employed

in the analysis.

### ~ame;



# Form 26R

• Section
B. Item 2.a. Attachment
to Great Oak Energy Report dated February 24, 2011 Production Brine

- RWC 802 Page

1 of 7 

# Report of Analysis -----

· -- · . ..



# . 

# ·· -----------

· - . DEP Cortiticlll.ion

Us 

# 32-00382 

# SampJeiD#: 

# Sample Type; 

# SaiQple Soarce: 

# Sampler; Client Sample lD: 10 15713 

# Waste Water 

# Grab CLIENT (Client) 

# Export Fuel # 

# 1 Oeta QuB/mers: 0:: The reported value
is from dilution.

E ,. Estimated value.



# S ,. Surrogate out of 

# <lOnttollimits

. R 

# = Sample received 

# out of holding time.


# H "' Sample analyzed 

# out 

# of holding time.



# C 

# = Sample received

in incorrect 

# container. 

# 8 

# = Analyte was 

# detected
in 

# both sample and meti\Qd$ blank

.


# x .. user defined data 

# qualifier.



# Page
1 ct3

# ENVJ SERVICE LABORATORIES. 

# INC. lal1 **~st.** 

## lndiCinQ. PA 15701 

# (724) 

# 463·TEST **(724}~** 

## Form 26R

• Section
B. Item 2.a. Attachment

to Great Oak Energy Report dated February 24, 

## 2011 Production Brine- RWC 802 

## Page
2 of 

# 7 

# Report of Analysis · · ----- ---· - ·· ----

· .. 

# ··· ----- **~ame:** 

## DEP Certitication

lis 

## 32.00382 

# ___ _ .. . 

# · -----..

.



# · ----
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# Grab Sampkl Souree: Sampler: 

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# Export Fuel #I ...



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S 

# = Sun"Ogate 

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## limits

. R .. Sample received out of holding time

. H '" Sample **an~ly)!ed** 

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C 

# = Sample received

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### containet

. B 

## = Anatyte was detected

In both sample and methods 

### blank.

X .. 

### uaer defined data qualifier.



## Page 2 of3**~lame:** 

## Great Oak 

## Energy, Inc:. Atul: 

## Mr. Ed **Klanun~:tr** 

### Form 26R

• Section B. Item 2.a. Attachment

to Great Oak Energy Report dated February 24, 2011 Production Brine- RWC 802 Page
3 of 7 

# Report of Analysis 

# --- Sample 

## II»: sample Typo: 637 

## AlleJ}!eny Avenue



## I p0 

## Box 

## 44S Oalanont, PA 1Sl39..0445



## Sample Source: Sampler: 

## »ample Sblrt **DJ~~te:** 

### S/2712010


## Il :30 AM

Client Sample ID: leccdpt Date: S/2712010 2:23 PM 

## leport Date: 6121/20 10

10 15713 

## Waste Water Grab 

### CLIENT (Client) 

## Sxport Fuel #I 

# -::~~~iii'::~~;


# Ail 

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# __ **--:~~~~:~-~-~i~J** 0 .. ! • • **·,,.,~·.** r,: 

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### 32-00382 

## ·-··--· ,_...

. 

## · · · · ---- Data Qualifiers:

D =The reported value I& from dilution.

E .. Estimated value.

S .. Surrogata out of 1;0ntrollimits. R = S01mple received out of holding 

### time.
H .. S41mple analyzed 

### out of holding time.

C • Sample received

In Jneorrect container. B • Analyte wa$ detected

in both sample and methods blank.

X = 

### User defined 

### data qualifier.



### Page 3 of3. r 

# 'lame; **=~;;;~....**



### ...: . **-~:......** 

# .............. **..;._~~~**

**-- ~**  

# Great Oak 

# Ener&Y, Jno. Attn: Mr. nc!Klammer Form 26R

• Section
B. Item 2.a. Attachment
to Great Oak Energy

' Report dated February 24, 2011 Production Brine

- RWC 802 Page
4 of 7 

# Report of Analysis 

# ----- SsmpleiD#: Sample Type: 

# 637 **All~eny** 

# Avenue

I 

# PO Box 44:5 Oalanont, PA 15139..()445
Sample Soaree: Sampler: 

# )ample Start Dato: S/27/2010 11:30 AM



# Client Sample ID: lUcoipt Date:

. 5/27/2010 2:23PM 

# !teportl)ato:

· 6/2212010

10 1S714 Waste War 

# Grab CUENT (Client) 

# Export Fuel Nl Rads E . .. th · 

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# Metrohm·Peak. ISO# 10001397QM08 

# Radiologicats done by 

# Benchmark Analytical. PADBP Lab ID: 39-00401

**·----**

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H 

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C "' Sample receivect

ln inc:orrect container. 8 "' 

## Analyte wa& 

## detected

in both sample 

## and 

## methods blank.

X "' 

## User defined data **qualif~er**

**.**



## Page

1 of 1

# . 

# LAB ID: 39w00401 st:ND OAT" TO: 

# NAME: Mike Moy8r 

# BENCHMARK 

# ANAL YTICS. 

# INC. . 4777

. Saucon Creek Road 

# Center Valley; PA 18034--9004 PHONE (610) 974-8100 FAX (610) 974-8104 COMPANY: Environmental 

# Service Laboratories,
Inc ADDRESS:

· 1803 Philadelphia


# St 1018714 

# Indiana, PA 15701 

# (724) 483-8378 . (724) 

# 465-4209 RECEtyED FOR LAB BY: 

# MAK 

# TEST REPORT DATE: 0610212010 9:45 Form 26R

• Section
B. Item 2.a. Attachment

to Great Oak Energy Report dated February 24, 2011 Production Brine- RWC 802 Page
5 of 7 

# Work 

# Order: 10060203 WOit. 10060203 PAGE:

· 1 of1 

# Pat: OAS06012010 

# PWSII»

Page


# 1 ofl 

# .. , **E;** 

# . to 11'114 " eAW'LED BY: David 

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# Lab 10: 1001020S-(101A

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# --- REMARKS:



# MtlbGsl EPAS04.0 

# .MQL 

# &IJWS Stilt 

# ADIII!N l!!nd 

# ADI.IliiC 06116110 9:00 06118110 NI.&-CV 

# . 

# ~ **~ ·~**  method has been perfotmed 

# under 

# NElAP certification, the 

# .,..~ys~a hal 

# met an of the requirements

of 

# · the 

# NEI.:AC standard unless 

# olhenNise 

# noted on the 

# Analytical **~** 

# * CV **Benchmaf1c;** 

# Analytlcs. Inc::. 

# Center Valley, PA; $A= **~** 

# Anrdytica, Inc. Seyre, 

# PA 

# MANAGER .. :•.

' t1" --

... 

# -----

· ---- DAl"E; __ 611 __ 112_0_1_0 __

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# 38-40401 LAB 10: 

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.
;


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# . . .... 

# Benchmark 

# Analytics,

Inc. 47Tl Saucon Creek Road Center Valley, PA 18034 Phone: (610) 974-8100 Fax: (610) 974-8104

Form 26R

• Section
B. Item 2.a

. Attachment

to Great Oak Energy Report dated February 24, 2011 Production Brine- RWC 802 Page
6 of 7 

# Work Order: 10060203 W()l;; 

# 10060203 

# NAME: Mike Moyer 

# OOJ4pANY: Environmental Service Laboratorll$,


# lno **AO~SS:** 

# 1803 Philldefphia


# st
. .

. **l~lane,** 

# PA 1!701

PAGE:

1 of1 

# PHONE: 

# F. AX:. 

# 10 1Ji'f4

' **-~1· ··;~**  **;'-~** 

# .• . - 

# (724) 48$8378 

# (724> 466-4209 **REC~D** 

# FOR lAB BY: MAK SAttFU!:


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# TEST REPORT DATE: **~108:46** 

# La6r ID: 

# 1CJ08G203.0018 SalrtJllel'lln« 05127120'10 U:30 

# Billa 1111111111 c 

# 0.0825 mgiL



# - EPA200.8 

# < 62.50 

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# JRA-CV DATE: 6/JJIJ(J/0

# ENVIRONMENTAL SERVICE LABORATORIES
.. INC. SAMPLE REQUEST 

# & CHAIN 

# OF CUSTODY PAG'E OF HEAOQUARlERS: 11103 Phlladelpbla 

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# Indiana. PA 15701**(12.4}~63-** 

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# ---- ---- nEI.INDERSI3!iB:I PUROHABER HEREBY loGREm 'ltl 

# PAY SERYICECKARGES ON 

# '-COO'JNTS OIIER:11 W.VB OLD. 1. 111BS£ SERYICE ato.RGEB VIILLACCRUEA.T l1iJ!. 

# RATE OF 1 1m! PER MOHJK 

# {111% PER ANNUM OR THE ti.AXIWJP.IAU.OWED 11'1' lAW.l 2. 

# tHe UNDERSIGNED PURa-t•.seR I.GREBI 

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# 1 7L /71,**/~ 5-~7-<.~**  \S'-""a Ma1rlx II of Contalners


# ww 1 

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# (2) 1000 ml 

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# J**Dale~** 

# lime 

# PRESERVAT10.r((:Y) N CONTAINERlvY N TEMP

# :s~c(fY)f NINA ContmnerType Pnla-1\'· 

# Plastic. Lilar none 

# PlasUc 

# liter 

# nooe Plastic Liter 

# HNO, 

# Plastic Liter 

# K.zSOc Plaslic Liter HNOt 

# Amber Glass L HCI 

# Amber Glass 

# l H,S0 4 

# Amber VOA Vials 1101\e 

# Amber VOA 

# Vlllls KCI 

# AmberVOA VIBls HCI PtoJec:l 

# NOtes:

Company/Name:
Address:

Contact Peraon: 

# Phone: Fax: 

# Form 2SR. 

# Section B. \tern 2.a. " · · • Attachment to Great Oak Energy.

Report dated February 24, 2011 

# Production Brine - RWC 802 Pa

_ ge 7 of 7
Analyst& Requested

# -~-~~: SU!rate,**AJ~, ,B~Ide** 

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# GREAT OAK ENERGY 637 Allegheny Ave.l 

# PO Box 445 Oakmont, PA 15139 

# Mr. Ed Klamm&r 

# 412-.828-2900 /412-828-8942

. (724] 349-5323 

# I

I



# i '



# I '

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# I I

I



# l I IName:SampleDate:ReceiptDate:ReportDate:SampleSite:AnalyteArsenic-ICPBarium-ICPCadmium-ICPChromium-ICPCopper-ICPLead-ICPMercuryNickei-ICPSelenium-ICPSilver-ICPZinc-ICP1)Benzene-37)Ethylbenzcne47)Toluene58)m+p-Xylene60)o-XyleneForm26R-SectionB.Item2.a.AttachmenttoGreatOakEnergyReportdatedFebruary24,2011UsedFracFluid-RWC804ReportofAnalysisMcCutcheonEnterprises,Inc.Attn:Mr.TimDobroskySampleiD#:SampleType:250ParkRoadSampleSource:Apollo,PA15613Sampler:1013983WaterGrab5/13/20108:00AM5/13/20103:14PM05117/2010ClientSampleID:MF(Client)GreatOakEnergyPO026676-07AnalystDateSampleUnitsMethodMDLAnalyzedResultDRM5/14/2010NDmgll200.7/60100DRM5/14/2010734.9mg!l200.7/60100DRM5/14/2010NDmg!l200.7/60100DRM5/14/2010NDmg!l200.7/60100DRM5/14/20100.50000000mgll200.7/60100DRM5/14/20100.90000000mg!l200.7/60100DRM5/14/2010NDmgll245.10DRM5/14/2010NDmgll200.7/60100DRM5/14/2010NDmg!l200.7/60100DRM5/14/2010NDmgll200.7/60100DRM5/14/20100.75000000mg/1200.7/60100CL5/13/2010NDug/L624/8260810CL5!13/2010NDug/L624/8260B10CL5/13/2010NDug/L624/8260B10CL5/13/2010NDug!L624/8260B20CL5/1312010NDug!L624/8260B10ND=NotDetectedDEPCertification#s32-0038232-03566Form 26R- Section
B. Item 2.c. Attachment

to Great Oak Energy Report dated February 24, 2011 11:: N- -\II Pn!\11\JI-= -N-T a 1 ...

.. .. **,~.** ..........

.. ·- SERVICE LABORATORIES, INC. 1803 Philadelphia
St., Indiana, PA 15701 (724) 463-TEST FAX (724) 465-4209 Great Oak Energy, Inc. Mr. Ed Klammer P.O. B0x445 Oakmont, PA 15139-0445 November

4, 201 0 Dear Mr. Klammer

,

- **'"~i?Qrf**

f' . '

- .... Environmental Service Laboratories, Inc. (ESL)
is accredited

in accordance with the Pennsylvania Department

of Environmental Protection (PADEP) State Environmental Laboratory Accreditation Program. State accreditation

is based upon compliance with Pennsylvania Code, Title 25, Part

I, Subpart
D, Article VI, Chapter 252 "Environmental Laboratory Accreditation" which specifies
all state mandated Quality ControVQuality Assurance policies and procedures. ESL, Inc. is certified to perform all analysis as outlined on the laboratories Scope of Accreditation and utilizes methods promulgated through 40 CFR. Our laboratory prides itself on the ability to provide our customers with top quality and legally defensible data. We value your company as a customer and appreciate your business. Thank you for using ESL for all your environmental testing requirements. Please do not hesitate
to contact our laboratory

if you have any questions
or concerns. Sincerely, Anngela

. Cha an Director
of Operations/Quality Assurance

**nr~r:--** . ',

Form 26R Chemical Analysis of Residual Waste Annual Report by the Generator Attachment

to Great Oak Energy Report Dated February 24, 2011 SECTION

B. WASTE DESCRIPTION Item 3. Process Description

& Schematic Frac Flow Back During the hydraulic fracturing process treated water and sand are pumped into the well under pressure. Once the treatment

is completed

a controlled flow back is used to allow the frac fluid to return to the surface. The flow back is monitored for sand returns, chlorides, natural gas, and liquid hydrocarbons. The flow back begins at the wellhead. The fluid then passes through

a choke to an oil, gas, and water separator. Flow backwater

is directed
to a lined pit. In order to reclaim the location the water will be transported from the pit to an approved treatment facility for proper disposal.

If liquid hydrocarbons had returned they would have been directed
to steel storage tanks for subsequent sales.
In the case of natural gas,
it is initially directed
to a flare stack. Once the volume and pressure are sufficient the natural gas is directed
to a sales pipeline. When the water volume diminishes

to less than 20 barrels per day the flow back phase
is completed and normal production operations begin. Flair stack Separator

Sales Meter Wellhead

Lined Pit

Steel TankForm26RChemicalAnalysisofResidualWasteAnnualReportbytheGeneratorAttachmenttoGreatOakEnergyReportDatedFebruary24,2011SECTIONB.WASTEDESCRIPTIONItem3.ProcessDescription&SchematicProductionBrineBrinewaterisgeneratedduringthecourseofnormalnaturalgasproduction.Normalproductionprocessesbeginwhenthewellbeginsproducinglessthan20barrelsofwaterperday.Althoughthewellbegantheproductionphaseproducingapproximately20barrelsperday,thedailyvolumeofwaterdiminishestoapproximately2barrelsperdayintenmonths.Theproductionphasebeginsatthewellhead.Naturalgasandtheassociatedproductionbrinethenflowtoagasandwaterseparator.Naturalgasisdirectedtothesalesmeter.Theproductionwaterflowstoatankbatteryoftwo210barrelsteeltanks.Thetanksarelocatedinsideadike.Thetanksaremonitoreddailybytelemetryandperiodicallybythewelltenderinperson.Whenthetanksreach75%capacitythewaterishauledtowatertreatmentfacilityforproperdisposal.WellheadEBSalesMeterSeparatorDikedTankBattery2 x210barrels