Dolan Chemical Laboratory 4001 Bixby Road Groveport, OH 43125 T: 614-836-4221, Audinet 210-4221 F: 614-836-4168, Audinet 210-4168 http://aepenv/labs 

### Water Analysis Form REP-703 Rev. 0, 4/2012



### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-001Date Collected:10/02/2013Date Received:10/2/2013 

### CPS Influent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 39.3 0.05DPC EPA 200.8 0.01 10/04/2013 10:43 ug/L Arsenic, As 339 0.1 DPC EPA 200.8 0.03 10/04/2013 10:43 ug/L Barium, Ba 4540 0.1 DPC EPA 200.8 0.02 10/04/2013 10:43 ug/L Beryllium, Be < 20 50 DAM EPA 200.7 20 10/11/2013 10:48 U ug/L Cadmium, Cd 262 0.05DPC EPA 200.8 0.01 10/04/2013 10:43 ug/L Chromium, Cr 1920 0.2 DPC EPA 200.8 0.04 10/04/2013 10:43 ug/L Cobalt, Co 407 0.02 DPC EPA 200.8 0.004 10/04/2013 10:43 ug/L Copper, Cu 774 0.05DPC EPA 200.8 0.01 10/04/2013 10:43 ug/L Lead, Pb 456 0.01 DPC EPA 200.8 0.002 10/04/2013 10:43 ng/L Mercury, Hg 235000 5000TLT EPA 1631E 2000 10/07/2013 ug/L Molybdenum, Mo 636 0.05DPC EPA 200.8 0.01 10/04/2013 10:43 ug/L Nickel, Ni 2640 0.2 DPC EPA 200.8 0.05 10/04/2013 10:43 ug/L Selenium, Se 1470 0.5 DPC EPA 200.8 0.2 10/04/2013 10:43 ug/L Silver, Ag 2.01 0.01 DPC EPA 200.8 0.002 10/04/2013 10:43 ug/L Thallium, Tl 22.2 0.05DPC EPA 200.8 0.002 10/04/2013 10:43 ug/L Tin, Sn < 200 500 DAM EPA 200.7 200 10/11/2013 10:48 U ug/L Titanium, Ti 879 100 DAM EPA 200.7 20 10/11/2013 10:48 ug/L Zinc, Zn 6840 0.5 DPC EPA 200.8 0.1 10/04/2013 10:43 mg/L Aluminum, Al 296 0.001DPC EPA 200.8 0.0003 10/04/2013 10:43 mg/L Boron, B 387 1 DAM EPA 200.7 0.2 10/11/2013 10:48 mg/L Calcium, Ca 3030 1 DAM EPA 200.7 0.2 10/11/2013 10:48 mg/L Iron, Fe 563 2 DAM EPA 200.7 0.5 10/11/2013 10:48 mg/L Magnesium, Mg 4460 0.5 DAM EPA 200.7 0.1 10/11/2013 10:48 mg/L Manganese, Mn 91.3 0.02DAM EPA 200.7 0.005 10/11/2013 10:48 mg/L Potassium, K 147 2 DAM EPA 200.7 0.4 10/11/2013 10:47 mg/L Sodium, Na 330 2 DAM EPA 200.7 0.4 10/11/2013 10:47 mg/L Strontium, Sr 21.1 0.05DAM EPA 200.7 0.02 10/11/2013 10:47 mg/L Ammonia, NH3, as N 3.49 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N11.3 5 DMM EPA 351.2 1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N34.4 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013

Mountaineer Plant, 133995 Page 1 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-001ADate Collected:10/02/2013Date Received:10/2/2013 

### CPS Influent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.77 0.05DPC EPA 200.8 0.01 10/04/2013 10:48 ug/L Arsenic, As 2.39 0.1 DPC EPA 200.8 0.03 10/04/2013 10:48 ug/L Barium, Ba 49.5 0.1 DPC EPA 200.8 0.02 10/04/2013 10:48 ug/L Beryllium, Be < 20 50 DAM EPA 200.7 20 10/11/2013 10:52 U ug/L Cadmium, Cd 146 0.05DPC EPA 200.8 0.01 10/04/2013 10:48 ug/L Chromium, Cr 0.3 0.2 DPC EPA 200.8 0.04 10/04/2013 10:48 ug/L Cobalt, Co 219 0.02DPC EPA 200.8 0.004 10/04/2013 10:48 ug/L Copper, Cu 4.75 0.05DPC EPA 200.8 0.01 10/04/2013 10:48 ug/L Lead, Pb 0.126 0.01 DPC EPA 200.8 0.002 10/04/2013 10:48 ng/L Mercury, Hg 68.2 10 TLT EPA 1631E 4 10/07/2013 ug/L Molybdenum, Mo 151 0.05DPC EPA 200.8 0.01 10/04/2013 10:48 ug/L Nickel, Ni 1270 0.2 DPC EPA 200.8 0.05 10/04/2013 10:48 ug/L Selenium, Se 261 0.5 DPC EPA 200.8 0.2 10/04/2013 10:48 ug/L Selenite, Se+4 (Hydride) 207 20 TLT AEP Method 4 10/10/2013 ug/L Silver, Ag 0.007 0.01 DPC EPA 200.8 0.002 10/04/2013 10:48 J ug/L Thallium, Tl 7.87 0.05DPC EPA 200.8 0.002 10/04/2013 10:48 ug/L Tin, Sn < 200 500 DAM EPA 200.7 200 10/11/2013 10:52 U ug/L Titanium, Ti < 20 100 DAM EPA 200.7 20 10/11/2013 10:52 U ug/L Zinc, Zn 507 0.5 DPC EPA 200.8 0.1 10/04/2013 10:48 mg/L Aluminum, Al 0.0872 0.001DPC EPA 200.8 0.0003 10/04/2013 10:48 mg/L Boron, B 395 1 DAM EPA 200.7 0.2 10/11/2013 10:52 mg/L Calcium, Ca 691 1 DAM EPA 200.7 0.2 10/11/2013 10:52 mg/L Iron, Fe < 0.5 2 DAM EPA 200.7 0.5 10/11/2013 10:52 U mg/L Magnesium, Mg 4110 0.5 DAM EPA 200.7 0.1 10/11/2013 10:52 mg/L Manganese, Mn 86.1 0.02DAM EPA 200.7 0.005 10/11/2013 10:52 mg/L Potassium, K 58.4 2 DAM EPA 200.7 0.4 10/11/2013 10:51 mg/L Sodium, Na 325 2 DAM EPA 200.7 0.4 10/11/2013 10:51 mg/L Strontium, Sr 10.1 0.05DAM EPA 200.7 0.02 10/11/2013 10:51

Mountaineer Plant, 133995 Page 2 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-002Date Collected:10/02/2013Date Received:10/2/2013 

### Primary Clarifier Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.14 0.05DPC EPA 200.8 0.01 10/04/2013 10:53 ug/L Arsenic, As 4.47 0.1 DPC EPA 200.8 0.03 10/04/2013 10:53 ug/L Barium, Ba 74.3 0.1 DPC EPA 200.8 0.02 10/04/2013 10:53 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 10:56 U ug/L Cadmium, Cd 45.1 0.05DPC EPA 200.8 0.01 10/04/2013 10:53 ug/L Chromium, Cr 13.0 0.2 DPC EPA 200.8 0.04 10/04/2013 10:53 ug/L Cobalt, Co 50.0 0.02DPC EPA 200.8 0.004 10/04/2013 10:53 ug/L Copper, Cu 6.15 0.05DPC EPA 200.8 0.01 10/04/2013 10:53 ug/L Lead, Pb 2.45 0.01 DPC EPA 200.8 0.002 10/04/2013 10:53 ng/L Mercury, Hg 1100 50 TLT EPA 1631E 20 10/07/2013 ug/L Molybdenum, Mo 186 0.05DPC EPA 200.8 0.01 10/04/2013 10:53 ug/L Nickel, Ni 307 0.2 DPC EPA 200.8 0.05 10/04/2013 10:53 ug/L Selenium, Se 397 0.5 DPC EPA 200.8 0.2 10/04/2013 10:53 ug/L Silver, Ag 0.024 0.01 DPC EPA 200.8 0.002 10/04/2013 10:53 ug/L Thallium, Tl 6.50 0.05DPC EPA 200.8 0.002 10/04/2013 10:53 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 10:56 U ug/L Titanium, Ti 10 20 DAM EPA 200.7 3 10/11/2013 10:56 J ug/L Zinc, Zn 40.8 0.5 DPC EPA 200.8 0.1 10/04/2013 10:53 mg/L Aluminum, Al 1.98 0.001DPC EPA 200.8 0.0003 10/04/2013 10:53 mg/L Boron, B 318 0.2 DAM EPA 200.7 0.04 10/11/2013 10:56 mg/L Calcium, Ca 735 0.2 DAM EPA 200.7 0.04 10/11/2013 10:56 mg/L Iron, Fe 2.79 0.5 DAM EPA 200.7 0.1 10/11/2013 10:56 mg/L Magnesium, Mg 3440 0.1 DAM EPA 200.7 0.02 10/11/2013 10:56 mg/L Manganese, Mn 46.8 0.005DAM EPA 200.7 0.001 10/11/2013 10:56 mg/L Potassium, K 54.8 0.5 DAM EPA 200.7 0.07 10/11/2013 10:55 mg/L Sodium, Na 280 0.3 DAM EPA 200.7 0.08 10/11/2013 10:55 mg/L Strontium, Sr 8.63 0.01 DAM EPA 200.7 0.003 10/11/2013 10:55 mg/L Ammonia, NH3, as N 2.47 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.73 0.5 DMM EPA 351.2 0.1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N32.2 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013

Mountaineer Plant, 133995 Page 3 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-002ADate Collected:10/02/2013Date Received:10/2/2013 

### Primary Clarifier Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.63 0.05DPC EPA 200.8 0.01 10/04/2013 10:58 ug/L Arsenic, As 2.47 0.1 DPC EPA 200.8 0.03 10/04/2013 10:58 ug/L Barium, Ba 57.1 0.1 DPC EPA 200.8 0.02 10/04/2013 10:58 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 11:05 U ug/L Cadmium, Cd 38.4 0.05DPC EPA 200.8 0.01 10/04/2013 10:58 ug/L Chromium, Cr 2.7 0.2 DPC EPA 200.8 0.04 10/04/2013 10:58 ug/L Cobalt, Co 41.7 0.02DPC EPA 200.8 0.004 10/04/2013 10:58 ug/L Copper, Cu 2.09 0.05DPC EPA 200.8 0.01 10/04/2013 10:58 ug/L Lead, Pb 0.017 0.01 DPC EPA 200.8 0.002 10/04/2013 10:58 ng/L Mercury, Hg 22.9 5 TLT EPA 1631E 2 10/07/2013 ug/L Molybdenum, Mo 176 0.05DPC EPA 200.8 0.01 10/04/2013 10:58 ug/L Nickel, Ni 243 0.2 DPC EPA 200.8 0.05 10/04/2013 10:58 ug/L Selenium, Se 348 0.5 DPC EPA 200.8 0.2 10/04/2013 10:58 ug/L Selenite, Se+4 (Hydride) 306 20 TLT AEP Method 4 10/10/2013 ug/L Silver, Ag 0.004 0.01 DPC EPA 200.8 0.002 10/04/2013 10:58 J ug/L Thallium, Tl 6.46 0.05DPC EPA 200.8 0.002 10/04/2013 10:58 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 11:05 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 11:05 U ug/L Zinc, Zn 9.4 0.5 DPC EPA 200.8 0.1 10/04/2013 10:58 mg/L Aluminum, Al 0.0257 0.001DPC EPA 200.8 0.0003 10/04/2013 10:58 mg/L Boron, B 318 0.2 DAM EPA 200.7 0.04 10/11/2013 11:05 mg/L Calcium, Ca 734 0.2 DAM EPA 200.7 0.04 10/11/2013 11:05 mg/L Iron, Fe 0.2 0.5 DAM EPA 200.7 0.1 10/11/2013 11:05 J mg/L Magnesium, Mg 3480 0.1 DAM EPA 200.7 0.02 10/11/2013 11:05 mg/L Manganese, Mn 46.7 0.005DAM EPA 200.7 0.001 10/11/2013 11:05 mg/L Potassium, K 54.4 0.5 DAM EPA 200.7 0.07 10/11/2013 11:04 mg/L Sodium, Na 281 0.3 DAM EPA 200.7 0.08 10/11/2013 11:04 mg/L Strontium, Sr 8.71 0.01 DAM EPA 200.7 0.003 10/11/2013 11:04

Mountaineer Plant, 133995 Page 4 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-003Date Collected:10/02/2013Date Received:10/2/2013 

### CPS Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.28 0.05DPC EPA 200.8 0.01 10/04/2013 11:02 ug/L Arsenic, As 4.32 0.1 DPC EPA 200.8 0.03 10/04/2013 11:02 ug/L Barium, Ba 74.5 0.1 DPC EPA 200.8 0.02 10/04/2013 11:02 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 11:25 U ug/L Cadmium, Cd 16.8 0.05DPC EPA 200.8 0.01 10/04/2013 11:02 ug/L Chromium, Cr 7.7 0.2 DPC EPA 200.8 0.04 10/04/2013 11:02 ug/L Cobalt, Co 13.2 0.02DPC EPA 200.8 0.004 10/04/2013 11:02 ug/L Copper, Cu 2.41 0.05DPC EPA 200.8 0.01 10/04/2013 11:02 ug/L Lead, Pb 1.39 0.01 DPC EPA 200.8 0.002 10/04/2013 11:02 ng/L Mercury, Hg 726 20 TLT EPA 1631E 8 10/07/2013 ug/L Molybdenum, Mo 535 0.05DPC EPA 200.8 0.01 10/04/2013 11:02 ug/L Nickel, Ni 113 0.2 DPC EPA 200.8 0.05 10/04/2013 11:02 ug/L Selenium, Se 339 0.5 DPC EPA 200.8 0.2 10/04/2013 11:02 ug/L Silver, Ag 0.004 0.01 DPC EPA 200.8 0.002 10/04/2013 11:02 J ug/L Thallium, Tl 4.58 0.05DPC EPA 200.8 0.002 10/04/2013 11:02 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 11:26 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 11:25 U ug/L Zinc, Zn 27.8 0.5 DPC EPA 200.8 0.1 10/04/2013 11:02 mg/L Aluminum, Al 1.01 0.001DPC EPA 200.8 0.0003 10/04/2013 11:02 mg/L Boron, B 306 0.2 DAM EPA 200.7 0.04 10/11/2013 11:25 mg/L Calcium, Ca 724 0.2 DAM EPA 200.7 0.04 10/11/2013 11:25 mg/L Iron, Fe 1.51 0.5 DAM EPA 200.7 0.1 10/11/2013 11:26 mg/L Magnesium, Mg 3140 0.1 DAM EPA 200.7 0.02 10/11/2013 11:25 mg/L Manganese, Mn 44.5 0.005DAM EPA 200.7 0.001 10/11/2013 11:25 mg/L Potassium, K 56.6 0.5 DAM EPA 200.7 0.07 10/11/2013 11:24 mg/L Sodium, Na 357 0.3 DAM EPA 200.7 0.08 10/11/2013 11:24 mg/L Strontium, Sr 8.39 0.01 DAM EPA 200.7 0.003 10/11/2013 11:24 mg/L Ammonia, NH3, as N 2.10 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N2.98 0.5 DMM EPA 351.2 0.1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N22.6 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013

Mountaineer Plant, 133995 Page 5 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-003ADate Collected:10/02/2013Date Received:10/2/2013 

### CPS Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 1.90 0.05DPC EPA 200.8 0.01 10/04/2013 11:41 ug/L Arsenic, As 3.13 0.1 DPC EPA 200.8 0.03 10/04/2013 11:41 ug/L Barium, Ba 57.3 0.1 DPC EPA 200.8 0.02 10/04/2013 11:41 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 11:34 U ug/L Cadmium, Cd 0.95 0.05DPC EPA 200.8 0.01 10/04/2013 11:41 ug/L Chromium, Cr 2.0 0.2 DPC EPA 200.8 0.04 10/04/2013 11:41 ug/L Cobalt, Co 4.04 0.02DPC EPA 200.8 0.004 10/04/2013 11:41 ug/L Copper, Cu 0.26 0.05DPC EPA 200.8 0.01 10/04/2013 11:41 ug/L Lead, Pb 0.013 0.01 DPC EPA 200.8 0.002 10/04/2013 11:41 ng/L Mercury, Hg 3.8 2 TLT EPA 1631E 0.8 10/07/2013 ug/L Molybdenum, Mo 468 0.05DPC EPA 200.8 0.01 10/04/2013 11:41 ug/L Nickel, Ni 57.0 0.2 DPC EPA 200.8 0.05 10/04/2013 11:41 ug/L Selenium, Se 303 0.5 DPC EPA 200.8 0.2 10/04/2013 11:41 ug/L Selenite, Se+4 (Hydride) 273 20 TLT AEP Method 4 10/10/2013 ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 11:41 J ug/L Thallium, Tl 3.29 0.05DPC EPA 200.8 0.002 10/04/2013 11:41 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 11:35 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 11:34 U ug/L Zinc, Zn 7.1 0.5 DPC EPA 200.8 0.1 10/04/2013 11:41 mg/L Aluminum, Al 0.0173 0.001DPC EPA 200.8 0.0003 10/04/2013 11:41 mg/L Boron, B 307 0.2 DAM EPA 200.7 0.04 10/11/2013 11:34 mg/L Calcium, Ca 725 0.2 DAM EPA 200.7 0.04 10/11/2013 11:34 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 10/11/2013 11:35 U mg/L Magnesium, Mg 3160 0.1 DAM EPA 200.7 0.02 10/11/2013 11:34 mg/L Manganese, Mn 44.4 0.005DAM EPA 200.7 0.001 10/11/2013 11:34 mg/L Potassium, K 56.1 0.5 DAM EPA 200.7 0.07 10/11/2013 11:33 mg/L Sodium, Na 357 0.3 DAM EPA 200.7 0.08 10/11/2013 11:33 mg/L Strontium, Sr 8.41 0.01 DAM EPA 200.7 0.003 10/11/2013 11:33

Mountaineer Plant, 133995 Page 6 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-004Date Collected:10/02/2013Date Received:10/2/2013 

### Landfill Leachate

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 11.9 0.05DPC EPA 200.8 0.01 10/04/2013 11:46 ug/L Arsenic, As 40.1 0.1 DPC EPA 200.8 0.03 10/04/2013 11:46 ug/L Barium, Ba 28.6 0.1 DPC EPA 200.8 0.02 10/04/2013 11:46 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 11:43 U ug/L Cadmium, Cd 0.89 0.05DPC EPA 200.8 0.01 10/04/2013 11:46 ug/L Chromium, Cr 0.5 0.2 DPC EPA 200.8 0.04 10/04/2013 11:46 ug/L Cobalt, Co 2.44 0.02DPC EPA 200.8 0.004 10/04/2013 11:46 ug/L Copper, Cu 0.36 0.05DPC EPA 200.8 0.01 10/04/2013 11:46 ug/L Lead, Pb 0.022 0.01 DPC EPA 200.8 0.002 10/04/2013 11:46 ng/L Mercury, Hg 57.2 10 TLT EPA 1631E 4 10/07/2013 ug/L Molybdenum, Mo 7870 0.05DPC EPA 200.8 0.01 10/04/2013 11:46 ug/L Nickel, Ni 8.03 0.2 DPC EPA 200.8 0.05 10/04/2013 11:46 ug/L Selenium, Se 258 0.5 DPC EPA 200.8 0.2 10/04/2013 11:46 ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 11:46 U ug/L Thallium, Tl 3.45 0.05DPC EPA 200.8 0.002 10/04/2013 11:46 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 11:44 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 11:43 U ug/L Zinc, Zn 2.2 0.5 DPC EPA 200.8 0.1 10/04/2013 11:46 mg/L Aluminum, Al 0.0246 0.001DPC EPA 200.8 0.0003 10/04/2013 11:46 mg/L Boron, B 62.1 0.2 DAM EPA 200.7 0.04 10/11/2013 11:43 mg/L Calcium, Ca 495 0.2 DAM EPA 200.7 0.04 10/11/2013 11:43 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 10/11/2013 11:44 U mg/L Magnesium, Mg 463 0.1 DAM EPA 200.7 0.02 10/11/2013 11:43 mg/L Manganese, Mn 1.24 0.005DAM EPA 200.7 0.001 10/11/2013 11:44 mg/L Potassium, K 125 0.5 DAM EPA 200.7 0.07 10/11/2013 11:42 mg/L Sodium, Na 2070 0.3 DAM EPA 200.7 0.08 10/11/2013 11:42 mg/L Strontium, Sr 6.56 0.01 DAM EPA 200.7 0.003 10/11/2013 11:42 mg/L Ammonia, NH3, as N 0.32 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N0.83 0.5 DMM EPA 351.2 0.1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N7.27 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013

Mountaineer Plant, 133995 Page 7 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-004ADate Collected:10/02/2013Date Received:10/2/2013 

### Landfill Leachate Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 11.2 0.05DPC EPA 200.8 0.01 10/04/2013 11:50 ug/L Arsenic, As 36.6 0.1 DPC EPA 200.8 0.03 10/04/2013 11:50 ug/L Barium, Ba 25.8 0.1 DPC EPA 200.8 0.02 10/04/2013 11:50 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 11:47 U ug/L Cadmium, Cd 0.98 0.05DPC EPA 200.8 0.01 10/04/2013 11:50 ug/L Chromium, Cr 0.4 0.2 DPC EPA 200.8 0.04 10/04/2013 11:50 ug/L Cobalt, Co 1.92 0.02DPC EPA 200.8 0.004 10/04/2013 11:50 ug/L Copper, Cu 0.28 0.05DPC EPA 200.8 0.01 10/04/2013 11:50 ug/L Lead, Pb 0.110 0.01 DPC EPA 200.8 0.002 10/04/2013 11:50 ng/L Mercury, Hg 7.3 2 TLT EPA 1631E 0.8 10/07/2013 ug/L Molybdenum, Mo 7320 0.05DPC EPA 200.8 0.01 10/04/2013 11:50 ug/L Nickel, Ni 7.01 0.2 DPC EPA 200.8 0.05 10/04/2013 11:50 ug/L Selenium, Se 244 0.5 DPC EPA 200.8 0.2 10/04/2013 11:50 ug/L Selenite, Se+4 (Hydride) 153 20 TLT AEP Method 4 10/10/2013 ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 11:50 U ug/L Thallium, Tl 3.21 0.05DPC EPA 200.8 0.002 10/04/2013 11:50 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 11:48 U ug/L Titanium, Ti 7 20 DAM EPA 200.7 3 10/11/2013 11:47 J ug/L Zinc, Zn 2.7 0.5 DPC EPA 200.8 0.1 10/04/2013 11:50 mg/L Aluminum, Al 0.0076 0.001DPC EPA 200.8 0.0003 10/04/2013 11:50 mg/L Boron, B 65.8 0.2 DAM EPA 200.7 0.04 10/11/2013 11:47 mg/L Calcium, Ca 524 0.2 DAM EPA 200.7 0.04 10/11/2013 11:47 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 10/11/2013 11:48 U mg/L Magnesium, Mg 492 0.1 DAM EPA 200.7 0.02 10/11/2013 11:47 mg/L Manganese, Mn 1.11 0.005DAM EPA 200.7 0.001 10/11/2013 11:48 mg/L Potassium, K 133 0.5 DAM EPA 200.7 0.07 10/11/2013 11:46 mg/L Sodium, Na 2230 0.3 DAM EPA 200.7 0.08 10/11/2013 11:46 mg/L Strontium, Sr 6.95 0.01 DAM EPA 200.7 0.003 10/11/2013 11:46

Mountaineer Plant, 133995 Page 8 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-005Date Collected:10/02/2013Date Received:10/2/2013 

### 1st Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 5.78 0.05DPC EPA 200.8 0.01 10/04/2013 11:55 ug/L Arsenic, As 17.4 0.1 DPC EPA 200.8 0.03 10/04/2013 11:55 ug/L Barium, Ba 56.5 0.1 DPC EPA 200.8 0.02 10/04/2013 11:55 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 12:45 U ug/L Cadmium, Cd 12.2 0.05DPC EPA 200.8 0.01 10/04/2013 11:55 ug/L Chromium, Cr 6.1 0.2 DPC EPA 200.8 0.04 10/04/2013 11:55 ug/L Cobalt, Co 13.6 0.02DPC EPA 200.8 0.004 10/04/2013 11:55 ug/L Copper, Cu 2.27 0.05DPC EPA 200.8 0.01 10/04/2013 11:55 ug/L Lead, Pb 1.01 0.01 DPC EPA 200.8 0.002 10/04/2013 11:55 ng/L Mercury, Hg 457 10 TLT EPA 1631E 4 10/07/2013 ug/L Molybdenum, Mo 3120 0.05DPC EPA 200.8 0.01 10/04/2013 11:55 ug/L Nickel, Ni 88.6 0.2 DPC EPA 200.8 0.05 10/04/2013 11:55 ug/L Selenium, Se 305 0.5 DPC EPA 200.8 0.2 10/04/2013 11:55 ug/L Silver, Ag 0.011 0.01 DPC EPA 200.8 0.002 10/04/2013 11:55 ug/L Thallium, Tl 3.69 0.05DPC EPA 200.8 0.002 10/04/2013 11:55 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 12:45 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 12:45 U ug/L Zinc, Zn 21.1 0.5 DPC EPA 200.8 0.1 10/04/2013 11:55 mg/L Aluminum, Al 0.815 0.001DPC EPA 200.8 0.0003 10/04/2013 11:55 mg/L Boron, B 218 0.2 DAM EPA 200.7 0.04 10/11/2013 12:45 mg/L Calcium, Ca 645 0.2 DAM EPA 200.7 0.04 10/11/2013 12:45 mg/L Iron, Fe 1.40 0.5 DAM EPA 200.7 0.1 10/11/2013 12:45 mg/L Magnesium, Mg 2160 0.1 DAM EPA 200.7 0.02 10/11/2013 12:45 mg/L Manganese, Mn 28.6 0.005DAM EPA 200.7 0.001 10/11/2013 12:45 mg/L Potassium, K 85.5 0.5 DAM EPA 200.7 0.07 10/11/2013 12:44 mg/L Sodium, Na 1040 0.3 DAM EPA 200.7 0.08 10/11/2013 12:44 mg/L Strontium, Sr 7.80 0.01 DAM EPA 200.7 0.003 10/11/2013 12:44 mg/L Ammonia, NH3, as N 1.39 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N2.10 0.5 DMM EPA 351.2 0.1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N18.3 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013

Mountaineer Plant, 133995 Page 9 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-005ADate Collected:10/02/2013Date Received:10/2/2013 

### 1st Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 5.79 0.05DPC EPA 200.8 0.01 10/04/2013 12:00 ug/L Arsenic, As 13.9 0.1 DPC EPA 200.8 0.03 10/04/2013 12:00 ug/L Barium, Ba 47.7 0.1 DPC EPA 200.8 0.02 10/04/2013 12:00 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 12:49 U ug/L Cadmium, Cd 1.39 0.05DPC EPA 200.8 0.01 10/04/2013 12:00 ug/L Chromium, Cr 1.4 0.2 DPC EPA 200.8 0.04 10/04/2013 12:00 ug/L Cobalt, Co 3.64 0.02DPC EPA 200.8 0.004 10/04/2013 12:00 ug/L Copper, Cu 0.36 0.05DPC EPA 200.8 0.01 10/04/2013 12:00 ug/L Lead, Pb 0.027 0.01 DPC EPA 200.8 0.002 10/04/2013 12:00 ng/L Mercury, Hg 5.4 2 TLT EPA 1631E 0.8 10/07/2013 ug/L Molybdenum, Mo 3150 0.05DPC EPA 200.8 0.01 10/04/2013 12:00 ug/L Nickel, Ni 42.8 0.2 DPC EPA 200.8 0.05 10/04/2013 12:00 ug/L Selenium, Se 298 0.5 DPC EPA 200.8 0.2 10/04/2013 12:00 ug/L Selenite, Se+4 (Hydride) 227 20 TLT AEP Method 4 10/10/2013 ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 12:00 U ug/L Thallium, Tl 3.33 0.05DPC EPA 200.8 0.002 10/04/2013 12:00 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 12:49 U ug/L Titanium, Ti 4 20 DAM EPA 200.7 3 10/11/2013 12:49 J ug/L Zinc, Zn 6.1 0.5 DPC EPA 200.8 0.1 10/04/2013 12:00 mg/L Aluminum, Al 0.0134 0.001DPC EPA 200.8 0.0003 10/04/2013 12:00 mg/L Boron, B 218 0.2 DAM EPA 200.7 0.04 10/11/2013 12:49 mg/L Calcium, Ca 642 0.2 DAM EPA 200.7 0.04 10/11/2013 12:49 mg/L Iron, Fe < 0.1 0.5 DAM EPA 200.7 0.1 10/11/2013 12:49 U mg/L Magnesium, Mg 2160 0.1 DAM EPA 200.7 0.02 10/11/2013 12:49 mg/L Manganese, Mn 28.3 0.005DAM EPA 200.7 0.001 10/11/2013 12:49 mg/L Potassium, K 84.8 0.5 DAM EPA 200.7 0.07 10/11/2013 12:48 mg/L Sodium, Na 1050 0.3 DAM EPA 200.7 0.08 10/11/2013 12:48 mg/L Strontium, Sr 7.86 0.01 DAM EPA 200.7 0.003 10/11/2013 12:48

Mountaineer Plant, 133995 Page 10 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-006Date Collected:10/02/2013Date Received:10/2/2013 

### 2nd Stage Feed

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.82 0.05DPC EPA 200.8 0.01 10/04/2013 12:05 ug/L Arsenic, As 9.71 0.1 DPC EPA 200.8 0.03 10/04/2013 12:05 ug/L Barium, Ba 33.5 0.1 DPC EPA 200.8 0.02 10/04/2013 12:05 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 12:10 U ug/L Cadmium, Cd 0.48 0.05DPC EPA 200.8 0.01 10/04/2013 12:05 ug/L Chromium, Cr 0.7 0.2 DPC EPA 200.8 0.04 10/04/2013 12:05 ug/L Cobalt, Co 3.75 0.02DPC EPA 200.8 0.004 10/04/2013 12:05 ug/L Copper, Cu 0.10 0.05DPC EPA 200.8 0.01 10/04/2013 12:05 ug/L Lead, Pb 0.014 0.01 DPC EPA 200.8 0.002 10/04/2013 12:05 ng/L Mercury, Hg 7.1 2 TLT EPA 1631E 0.8 10/07/2013 ug/L Molybdenum, Mo 4680 0.05DPC EPA 200.8 0.01 10/04/2013 12:05 ug/L Nickel, Ni 32.6 0.2 DPC EPA 200.8 0.05 10/04/2013 12:05 ug/L Selenium, Se 16.1 0.5 DPC EPA 200.8 0.2 10/04/2013 12:05 ug/L Silver, Ag 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 12:05 J ug/L Thallium, Tl 0.54 0.05DPC EPA 200.8 0.002 10/04/2013 12:05 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 12:10 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 12:10 U ug/L Zinc, Zn 1.0 0.5 DPC EPA 200.8 0.1 10/04/2013 12:05 mg/L Aluminum, Al 0.320 0.001DPC EPA 200.8 0.0003 10/04/2013 12:05 mg/L Boron, B 148 0.2 DAM EPA 200.7 0.04 10/11/2013 12:10 mg/L Calcium, Ca 419 0.2 DAM EPA 200.7 0.04 10/11/2013 12:10 mg/L Iron, Fe 0.746 0.5 DAM EPA 200.7 0.1 10/11/2013 12:10 mg/L Magnesium, Mg 776 0.1 DAM EPA 200.7 0.02 10/11/2013 12:10 mg/L Manganese, Mn 13.3 0.005DAM EPA 200.7 0.001 10/11/2013 12:10 mg/L Potassium, K 115 0.5 DAM EPA 200.7 0.07 10/11/2013 12:08 mg/L Sodium, Na 1870 0.3 DAM EPA 200.7 0.08 10/11/2013 12:08 mg/L Strontium, Sr 5.34 0.01 DAM EPA 200.7 0.003 10/11/2013 12:08 mg/L Ammonia, NH3, as N 2.16 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N3.84 0.5 DMM EPA 351.2 0.1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N< 0.02 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013 U

Mountaineer Plant, 133995 Page 11 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-006ADate Collected:10/02/2013Date Received:10/2/2013 

### 2nd Stage Feed Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 2.65 0.05DPC EPA 200.8 0.01 10/04/2013 12:10 ug/L Arsenic, As 9.21 0.1 DPC EPA 200.8 0.03 10/04/2013 12:10 ug/L Barium, Ba 33.1 0.1 DPC EPA 200.8 0.02 10/04/2013 12:10 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 12:14 U ug/L Cadmium, Cd 0.53 0.05DPC EPA 200.8 0.01 10/04/2013 12:10 ug/L Chromium, Cr 0.6 0.2 DPC EPA 200.8 0.04 10/04/2013 12:10 ug/L Cobalt, Co 3.57 0.02DPC EPA 200.8 0.004 10/04/2013 12:10 ug/L Copper, Cu 0.05 0.05DPC EPA 200.8 0.01 10/04/2013 12:10 ug/L Lead, Pb 0.016 0.01 DPC EPA 200.8 0.002 10/04/2013 12:10 ng/L Mercury, Hg 2.7 1 TLT EPA 1631E 0.4 10/07/2013 ug/L Molybdenum, Mo 4540 0.05DPC EPA 200.8 0.01 10/04/2013 12:10 ug/L Nickel, Ni 31.3 0.2 DPC EPA 200.8 0.05 10/04/2013 12:10 ug/L Selenium, Se 11.3 0.5 DPC EPA 200.8 0.2 10/04/2013 12:10 ug/L Selenite, Se+4 (Hydride) 7.7 2 TLT AEP Method 0.4 11/01/2013 ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 12:10 U ug/L Thallium, Tl 0.47 0.05DPC EPA 200.8 0.002 10/04/2013 12:10 ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 00:51 U ug/L Titanium, Ti 10 20 DAM EPA 200.7 3 10/11/2013 12:14 J ug/L Zinc, Zn 2.5 0.5 DPC EPA 200.8 0.1 10/04/2013 12:10 mg/L Aluminum, Al 0.317 0.001DPC EPA 200.8 0.0003 10/04/2013 12:10 mg/L Boron, B 147 0.2 DAM EPA 200.7 0.04 10/11/2013 12:14 mg/L Calcium, Ca 416 0.2 DAM EPA 200.7 0.04 10/11/2013 12:14 mg/L Iron, Fe 0.710 0.5 DAM EPA 200.7 0.1 10/11/2013 00:51 mg/L Magnesium, Mg 771 0.1 DAM EPA 200.7 0.02 10/11/2013 12:14 mg/L Manganese, Mn 13.2 0.005DAM EPA 200.7 0.001 10/11/2013 12:14 mg/L Potassium, K 115 0.5 DAM EPA 200.7 0.07 10/11/2013 12:12 mg/L Sodium, Na 1860 0.3 DAM EPA 200.7 0.08 10/11/2013 12:12 mg/L Strontium, Sr 5.32 0.01 DAM EPA 200.7 0.003 10/11/2013 12:12

Mountaineer Plant, 133995 Page 12 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-007Date Collected:10/02/2013Date Received:10/2/2013 

### Bioreactor Effluent

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.07 0.05DPC EPA 200.8 0.01 10/04/2013 12:14 ug/L Arsenic, As 0.88 0.1 DPC EPA 200.8 0.03 10/04/2013 12:14 ug/L Barium, Ba 52.5 0.1 DPC EPA 200.8 0.02 10/04/2013 12:14 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 12:18 U ug/L Cadmium, Cd < 0.01 0.05DPC EPA 200.8 0.01 10/04/2013 12:14 U ug/L Chromium, Cr 0.7 0.2 DPC EPA 200.8 0.04 10/04/2013 12:14 ug/L Cobalt, Co 0.092 0.02DPC EPA 200.8 0.004 10/04/2013 12:14 ug/L Copper, Cu 0.06 0.05DPC EPA 200.8 0.01 10/04/2013 12:14 ug/L Lead, Pb 0.011 0.01 DPC EPA 200.8 0.002 10/04/2013 12:14 ng/L Mercury, Hg 1.9 1 TLT EPA 1631E 0.4 10/07/2013 ug/L Molybdenum, Mo 9.28 0.05DPC EPA 200.8 0.01 10/04/2013 12:14 ug/L Nickel, Ni 2.03 0.2 DPC EPA 200.8 0.05 10/04/2013 12:14 ug/L Selenium, Se 1.5 0.5 DPC EPA 200.8 0.2 10/04/2013 12:14 ug/L Silver, Ag < 0.002 0.01 DPC EPA 200.8 0.002 10/04/2013 12:14 U ug/L Thallium, Tl 0.03 0.05DPC EPA 200.8 0.002 10/04/2013 12:14 J ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 12:18 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 12:18 U ug/L Zinc, Zn 0.7 0.5 DPC EPA 200.8 0.1 10/04/2013 12:14 mg/L Aluminum, Al 1.95 0.001DPC EPA 200.8 0.0003 10/04/2013 12:14 mg/L Boron, B 179 0.2 DAM EPA 200.7 0.04 10/11/2013 12:18 mg/L Calcium, Ca 588 0.2 DAM EPA 200.7 0.04 10/11/2013 12:18 mg/L Iron, Fe 1.42 0.5 DAM EPA 200.7 0.1 10/11/2013 12:18 mg/L Magnesium, Mg 1760 0.1 DAM EPA 200.7 0.02 10/11/2013 12:18 mg/L Manganese, Mn 27.0 0.005DAM EPA 200.7 0.001 10/11/2013 12:18 mg/L Potassium, K 87.0 0.5 DAM EPA 200.7 0.07 10/11/2013 12:16 mg/L Sodium, Na 1130 0.3 DAM EPA 200.7 0.08 10/11/2013 12:16 mg/L Strontium, Sr 6.85 0.01 DAM EPA 200.7 0.003 10/11/2013 12:16 mg/L Ammonia, NH3, as N 2.21 0.05DMM EPA 350.1 0.02 10/04/2013 mg/L Total Kjeldahl Nitrogen, TKN as N5.60 0.5 DMM EPA 351.2 0.1 10/05/2013 mg/L Nitrate-Nitrite, NO3-NO2, as N0.46 0.1 DMM SM20 4500NO3 H 0.02 10/08/2013

Mountaineer Plant, 133995 Page 13 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

Sample Number:133995-007ADate Collected:10/02/2013Date Received:10/2/2013 

### Bioreactor Effluent Dissolved

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ug/L Antimony, Sb 0.06 0.05DPC EPA 200.8 0.01 10/04/2013 12:19 ug/L Arsenic, As 0.82 0.1 DPC EPA 200.8 0.03 10/04/2013 12:19 ug/L Barium, Ba 46.5 0.1 DPC EPA 200.8 0.02 10/04/2013 12:19 ug/L Beryllium, Be < 3 10 DAM EPA 200.7 3 10/11/2013 12:22 U ug/L Cadmium, Cd < 0.01 0.05DPC EPA 200.8 0.01 10/04/2013 12:19 U ug/L Chromium, Cr 0.5 0.2 DPC EPA 200.8 0.04 10/04/2013 12:19 ug/L Cobalt, Co 0.064 0.02DPC EPA 200.8 0.004 10/04/2013 12:19 ug/L Copper, Cu 0.04 0.05DPC EPA 200.8 0.01 10/04/2013 12:19 J ug/L Lead, Pb 0.021 0.01 DPC EPA 200.8 0.002 10/04/2013 12:19 ng/L Mercury, Hg 1.5 0.5 TLT EPA 1631E 0.2 10/07/2013 ug/L Molybdenum, Mo 5.69 0.05DPC EPA 200.8 0.01 10/04/2013 12:19 ug/L Nickel, Ni 1.82 0.2 DPC EPA 200.8 0.05 10/04/2013 12:19 ug/L Selenium, Se 1.1 0.5 DPC EPA 200.8 0.2 10/04/2013 12:19 ug/L Selenite, Se+4 (Hydride)< 0.08 0.4 TLT AEP Method 0.08 11/01/2013 U ug/L Silver, Ag 0.003 0.01 DPC EPA 200.8 0.002 10/04/2013 12:19 J ug/L Thallium, Tl 0.01 0.05DPC EPA 200.8 0.002 10/04/2013 12:19 J ug/L Tin, Sn < 30 100 DAM EPA 200.7 30 10/11/2013 12:22 U ug/L Titanium, Ti < 3 20 DAM EPA 200.7 3 10/11/2013 12:22 U ug/L Zinc, Zn 4.1 0.5 DPC EPA 200.8 0.1 10/04/2013 12:19 mg/L Aluminum, Al 1.70 0.001DPC EPA 200.8 0.0003 10/04/2013 12:19 mg/L Boron, B 178 0.2 DAM EPA 200.7 0.04 10/11/2013 12:22 mg/L Calcium, Ca 584 0.2 DAM EPA 200.7 0.04 10/11/2013 12:22 mg/L Iron, Fe 1.38 0.5 DAM EPA 200.7 0.1 10/11/2013 12:22 mg/L Magnesium, Mg 1750 0.1 DAM EPA 200.7 0.02 10/11/2013 12:22 mg/L Manganese, Mn 26.9 0.005DAM EPA 200.7 0.001 10/11/2013 12:22 mg/L Potassium, K 86.9 0.5 DAM EPA 200.7 0.07 10/11/2013 12:20 mg/L Sodium, Na 1130 0.3 DAM EPA 200.7 0.08 10/11/2013 12:20 mg/L Strontium, Sr 6.89 0.01 DAM EPA 200.7 0.003 10/11/2013 12:20



### Sample Number:133995-008Date Collected:10/02/2013Date Received:10/2/2013 

### Field Blank

Units Parameter Result RLAnalysis ByAnalysis Date/TimeMethod MDL Data Qual ng/L Mercury, Hg < 0.2 0.5 TLT EPA 1631E 0.2 10/07/2013 U

Mountaineer Plant, 133995 Page 14 of 15

### Location: Mountaineer Plant Report Date: 11/4/2013

THIS TEST REPORT RELATES ONLY TO THE ITEMS TESTED AND SHALL NOT BE REPRODUCED EXCEPT IN FULL WITHOUT WRITTEN APPROVAL OF THE LABORATORY. ALL TEST RESULTS MEET ALL OF THE REQUIREMENTS OF THE ACCREDITING AUTHORITY, UNLESS OTHERWISE NOTED. U: Analyte was analyzed and not detected at or above adjusted Method Detection Limit J: Analyte was positively identified, though the quantitation was below Reporting Limit.

Brian Snyder, Chemist II Email bssnyder@aep.comTel. 614-836-4224

Fax 614-836-4168Audinet 210-4224

Mountaineer Plant, 133995 Page 15 of 15