Electric Melter Furnace 

NAIMA/U.S. EPA 

Emissions Test Report 

Prepared for: 

Guardian Fiberglass, Inc. 

Mineral Wells, Mississippi 

Mineral Wells Plant 

7046 State Line Road 

Mineral Wells, Mississippi 

BTEC Project No. 10-3990.05 

November 12, 2010 

BT Environmental Consulting, Inc. 

2615 Wolcott Street 

Ferndale, Michigan 48220 

(248) 548-8070 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

i

Executive Summary

U.S. EPA has agreed with the North American Insulation Manufacturer’s Association (NAIMA) 

and its members to a voluntary collection of residual risk-related data for the National Emission 

Standards for Hazardous Air Pollutants (NESHAP) for Mineral Wool Production1

 as well as for 

the NESHAP for Wool Fiberglass Manufacturing2. To assist in collecting the agreed upon data, 

BT Environmental Consulting, Inc. (BTEC) was retained by NAIMA to evaluate emission rates 

of the following pollutants from the one exhaust stack associated with the Electric Glass Melt 

Furnace process located at the Guardian Fiberglass, Inc. (Guardian) site in Mineral Wells, 

Mississippi: 

• Particulate matter (PM) and particulate matter less than 2.5 microns in diameter (PM2.5) 

• Antimony, arsenic, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and 

selenium 

• Mercury 

• Hexavalent chromium 

• Hydrogen fluoride and hydrogen chloride 

Reference test methods used and test program methodologies were agreed upon by U.S. EPA and 

NAIMA prior to initiating test program fieldwork. Table I on the following page summarizes the 

overall results of the emissions test program. 

 

1

 Codified at Title 40, Part 63, Subpart DDD of the Code of Federal Regulations (40 CFR 63, Subpart DDD) 2

 Codified at 40 CFR 63, Subpart NNN 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

ii

Table I 

Emissions Test Program Results Summary

Test Date(s) Pollutant Emission 

Rate 

(lbs/hr) 

Emission Rate 

(lbs/ton glass) 

Emission 

Rate 

(mg/dscm)

Filterable PM2.5 <7.6 x 10-3 <2.6 x 10-3 <3.5 x 10-1

Organic Condensible PM2.5 2.1 x 10-2 7.0 x 10-3 9.5 x 10-1

Inorganic Condensible PM2.5 5.7 x 10-2 1.9 x 10-2 2.6 Sept 21 & 22, 2010 

Total PM2.5 <8.5 x 10-2 <2.9 x 10-2 <3.9 

Filterable Particulate 0.04 0.01 2.0 

Antimony <3.9 x 10-6 <1.3 x 10-6 <1.9 x 10-4

Arsenic <3.9 x 10-6 <1.3 x 10-6 <1.9 x 10-4

Beryllium <9.8 x 10-7 <3.4 x 10-7 <4.7 x 10-5

Cadmium <1.1 x 10-6 <3.9 x 10-7 <5.6 x 10-5

Chromium 2.3 x 10-5 7.7 x 10-6 1.1 x 10-3

Cobalt <1.6 x 10-6 <5.4 x 10-7 <7.7 x 10-5

Lead 1.5 x 10-5 5.1 x 10-6 7.2 x 10-4

Manganese 8.7 x 10-6 3.0 x 10-6 4.2 x 10-4

Nickel 3.9 x 10-5 1.3 x 10-5 1.9 x 10-3

Sept 21 & 22, 2010 

Selenium 1.2 x 10-5 4.0 x 10-6 5.6 x 10-4

Sept 22, 2010 Mercury 8.4 x 10-4 2.9 x 10-4 4.0 x 10-2

Sept 22 & 23, 2010 Hexavalent Chromium 6.6 x 10-6 2.2 x 10-6 3.2 x 10-4

Hydrogen Chloride <3.4 x 10-3 <1.2 x 10-3 <1.6 x 10-1

Sept 22 & 23, 2010 Hydrogen Fluoride <3.4 x 10-3 <1.2 x 10-3 <1.6 x 10-1

Notes: (1) Pollutant emission rates in terms of mg/dscm were not corrected to 7% O2 because exhaust from the 

process is essentially ambient (i.e., approximately 20.9% O2). 

(2) The “less than” symbol (<) included in the table indicates that the emission rate was calculated using the method 

detection limit (MDL) value instead of zero because the analytical result was below the MDL for one or more of the 

sample fractions.
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

iii

TABLE OF CONTENTS

1.0 INTRODUCTION............................................................................................................... 1

2.0 PROCESS DESCRIPTION ............................................................................................... 1

2.1 PROCESS MONITORING ....................................................................................................... 2 

3.0 SAMPLING AND ANALYTICAL METHODOLOGIES.............................................. 2

3.1 EXHAUST GAS VELOCITY, MOLECULAR WEIGHT, AND MOISTURE CONTENT .................... 2 

3.2 PM AND PM2.5 CONCENTRATIONS AND EMISSION RATES................................................... 3 

3.3 TOTAL SELECTED METALS CONCENTRATIONS AND EMISSION RATES................................ 3 

3.4 HG CONCENTRATIONS AND EMISSION RATES..................................................................... 4 

3.5 HEXAVALENT CHROMIUM CONCENTRATIONS AND EMISSION RATES................................. 4 

3.6 HF AND HCL CONCENTRATIONS AND EMISSION RATES..................................................... 4 

4.0 TEST RESULTS ................................................................................................................. 4

TABLES

Table 1 – Test Personnel 

Table 2 - Emissions Test Program Summary 

FIGURES

Figure 1 – Exhaust Stack Traverse Point Diagram 

Figure 2 – Method 3 Sampling Train Schematic Drawing 

Figure 3 – OTM 27/OTM 28 Sampling Train Schematic Drawing 

Figure 4 – Method 29 Sampling Train Schematic Drawing 

Figure 5 – Method 30B Sampling Train Schematic Drawing 

Figure 6 – Method 0061 Sampling Train Schematic Drawing 

Figure 7 – Method 26A Sampling Train Schematic Drawing 

APPENDICES

Appendix A – Detailed Test Run Results 

Appendix B – Production Data 

Appendix C – Field and Computer-Generated Data Sheets and Notes 

Appendix D – Equipment Calibration Documents 

Appendix E – Laboratory Analytical Reports 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

1

1.0 Introduction 

U.S. EPA has agreed with the North American Insulation Manufacturer’s Association (NAIMA) 

and its members to a voluntary collection of residual risk-related data for the National Emission 

Standards for Hazardous Air Pollutants (NESHAP) for Mineral Wool Production3

 as well as for 

the NESHAP for Wool Fiberglass Manufacturing4. To assist in collecting the agreed upon data, 

BT Environmental Consulting, Inc. (BTEC) was retained by NAIMA to evaluate emission rates 

of the following pollutants from one exhaust stack associated with the Electric Glass Melt 

Furnace process located at the Guardian Fiberglass, Inc. (Guardian) site in Mineral Wells, 

Mississippi: 

• Particulate matter (PM) and particulate matter less than 2.5 microns in diameter (PM2.5) 

• Antimony, arsenic, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and 

selenium 

• Mercury 

• Hexavalent chromium 

• Hydrogen fluoride and hydrogen chloride 

Reference test methods used and test program methodologies were agreed upon by U.S. EPA and 

NAIMA prior to initiating test program fieldwork. The emissions test program was conducted on 

September 21, 22, and 23, 2010. The test program consisted of triplicate emission tests for each 

parameter. The field sampling portion of the emissions test program was conducted by METCO 

Environmental of Carrollton, Texas and included the personnel summarized by Table 1. 

Table 1 

Emissions Test Program Personnel

Personnel Affiliation 

Jason LaCroix METCO Environmental 

Jerry McDonald METCO Environmental 

Chris Maxwell METCO Environmental 

Bobby Pineda METCO Environmental 

Michael Meadows METCO Environmental 

Grover Thomas Guardian Fiberglass 

Joey Bronc Guardian Fiberglass 

2.0 Process Description

The Guardian facility in Mineral Wells includes a refractory-lined electric melt furnace 

controlled by an externally vented baghouse. Mixed batch is fed to the electric melter furnace 

and melted to be formed into fiberglass. The emissions test program will evaluate air pollutant 

emission rates from the single exhaust stack exhausting emissions from the electric melt furnace. 

 

3

 Codified at Title 40, Part 63, Subpart DDD of the Code of Federal Regulations (40 CFR 63, Subpart DDD) 4

 Codified at 40 CFR 63, Subpart NNN 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

2

The stack serving the electric melt furnace (AB-005) is round and 29 inches in diameter at the 

test location. The stack is equipped with four emissions test ports, each four inches in diameter. 

Testing was conducted from a stack platform located approximately fifty feet above the plant 

floor. The Guardian facility in Mineral Wells is located at 7046 State Line Road in Mineral 

Wells, Mississippi. 

2.1 Process Monitoring 

During the emissions test program, the electric melt furnace was operated under maximum 

conditions. In addition to total production for each test run, process operating data recorded (at 

15-minute intervals) during the emissions test program included (1) baghouse pressure drop, (2) 

baghouse operating temperature, and (3) bag leak detector reading. Process production data is 

available in Appendix B. Control equipment data will be available to U.S. EPA on request. 

3.0 Sampling and Analytical Methodologies 

Sampling and analytical methodologies for the emissions test program can be separated into six 

categories as follows: 

(1) Measurement of exhaust gas velocity, molecular weight, and moisture content; 

(2) Measurement of exhaust gas PM and PM2.5 concentrations and emission rates; 

(3) Measurement of exhaust gas total selected metals concentrations and emission rates; 

(4) Measurement of exhaust gas Hg concentrations and emission rates; 

(5) Measurement of exhaust gas hexavalent chromium concentrations and emission rates; 

(6) Measurement of exhaust gas HF and HCl concentrations and emission rates; 

Descriptions of sampling and analytical methodologies by category are summarized by Sections 

3.1 through 3.6, respectively. 

3.1 Exhaust Gas Velocity, Molecular Weight, and Moisture Content 

Measurement of exhaust gas velocity, molecular weight, and moisture content was conducted 

using the following reference test methods codified at Title 40, Part 60, Appendix A of the Code 

of Federal Regulations (40 CFR 60, Appendix A): 

• Method 1 - “Location of the Sampling Site and Sampling Points” 

• Method 2 - “Determination of Stack Gas Velocity and Volumetric Flowrate” 

• Method 3A - “Determination of Oxygen and Carbon Dioxide Concentrations in 

Emissions from Stationary Sources”(Instrumental Analyzer Procedure)

• Method 4 - “Determination of Moisture Content in Stack Gases”

These test methods were used to evaluate exhaust gas flowrates either in conjunction with the 

isokinetic sampling methodologies used to evaluate some pollutant emission rates or as separate, 

discrete measurements conducted in support of the non-isokinetic sampling methodologies. 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

3

Stack gas velocity traverses were conducted in accordance with the procedures outlined in 

Method 1 and Method 2 (see Figure 1 for a traverse location drawing). An S-type pitot tube with 

a thermocouple assembly, calibrated in accordance with Method 2, Section 4.1.1, was used to 

measure exhaust gas velocity pressures (using a manometer) and temperatures at each location 

during testing. The S-type pitot tube dimensions will be within specified limits, therefore, a 

baseline pitot tube coefficient of 0.84 (dimensionless) will be assigned. 

Molecular weight was determined according to USEPA Method 3. The O2 content of the 

exhaust gas was measured via integrated bag sampling followed by Method 3 Orsat gas analysis. 

A schematic drawing of the sampling system is provided as Figure 2. 

Exhaust gas moisture content was evaluated using Method 4. Exhaust gas moisture content was 

be determined volumetrically (liquid impingers) and gravimetrically (silica gel impinger). 

3.2 PM and PM2.5 Concentrations and Emission Rates 

PM/PM2.5 concentrations and emission rates were measured using U.S. EPA Other Test 

Methods (OTM) 27 and OTM 28. PM, PM2.5, and CPM concentrations and emission rates were 

measured using BTEC’s Nutech® Model 2010 modular isokinetic stack sampling system. This 

system consisted of (1) a tapered nozzle, (2) a PM10 particle sizer cyclone followed by a PM2.5

particle sizer cyclone, (3) a glass or quartz fiber filter assembly and heated probe, (4) a glass 

recirculating ice water condenser system, (5) a set of four GS impingers, (6) a length of sample 

line, and (7) a Nutech® control case equipped with a pump, dry gas meter, and calibrated 

orifice. Prior to each test, the second and third impingers were filled with 100 ml of HPLC 

water, the first and fourth impingers were empty, and the fifth impinger contained 

approximately 300 g of silica gel desiccant. A schematic drawing of the PM2.5/CPM sample 

train is provided as Figure 3. The total filterable PM faction was collected on the front half of 

the M29 Metals sampling train as per the QAPP. 

3.3 Total Selected Metals Concentrations and Emission Rates

Total selected metals concentrations and emission rates were measured using the procedures of 

40 CFR 60, Appendix A, Method 29. Selected metals concentrations and emission rates were 

measured using BTEC’s Nutech® Model 2010 modular isokinetic stack sampling system. This 

system consisted of (1) a borosilicate glass or quartz nozzle, (2) a steel probe w/glass liner, (3) a 

heated quartz fiber filter assembly, (4) a set of six GS impingers, (5) a length of sample line, 

and (6) a Nutech® control case equipped with a pump, dry gas meter, and calibrated orifice. 

Prior to each test, the first two impingers were filled with 100 ml of a 5% nitric acid 

(HNO3)/10% hydrogen peroxide solution, the third impinger was empty, and the fourth 

contained approximately 300 g of silica gel desiccant. A schematic drawing of the metals 

sampling train is provided as Figure 4. 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

4

3.4 Hg Concentrations and Emission Rates 

Hg concentrations and emission rates were measured using the procedures of 40 CFR 60, 

Appendix A, Method 30B and using BTEC’s Nutech® Model 2010 modular isokinetic stack 

sampling system. This system consisted of (1) a sorbent trap, (2) a steel probe, (3) Teflon 

tubing, (4) three GS impingers, (5) a length of sample line, and (6) a Nutech® control case 

equipped with a pump, dry gas meter, and calibrated orifice. The first impinger was left empty 

as a water knockout, and the remaining two impingers contained approximately 300 g of silica 

gel desiccant. A schematic drawing of the Hg sampling train is provided as Figure 5. 

3.5 Hexavalent Chromium Concentrations and Emission Rates 

Hexavalent chromium concentrations and emission rates were measured using the procedures of 

Method 0061 with analysis by NCASI CI/WM-98.01. Hexavalent chromium concentrations and 

emission rates were measured using BTEC’s Nutech® Model 2010 modular isokinetic stack 

sampling system. This system consisted of (1) a glass nozzle, (2) a heated steel probe with a 

glass probe liner, (3) a Teflon tee with a recirculating pump, (4) five GS impingers, (5) a length 

of sample line, and (6) a Nutech® control case equipped with a pump, dry gas meter, and a 

calibrated orifice. Prior to each test, the first impinger was filled with 150 mL of 0.1N KOH, the 

next two were filled with 75 mL of 0.1 N KOH, the fourth was empty, and the last impinger 

contained approximately 300 g of silica gel desiccant. A schematic drawing of the Method 0061 

sampling train is provided as Figure 6. 

3.6 HF and HCl Concentrations and Emission Rates 

Measurement of hydrogen halide concentrations and emission rates were conducted using the 

procedures of 40 CFR 60, Appendix A, Method 26A. The Method 26A sampling train consisted 

of: (1) a heated borosilicate or quartz probe liner; (2) a heated borosilicate or quartz glass filter 

holder containing a pre-weighed 110-mm diameter washed quartz filter with Teflon filter 

support; (3) a set of three Greensburg-Smith (GS) impingers each containing 100 ml of 0.1 

Normal Sulfuric Acid (0.1 N H2SO4), (4) a modified GS impinger containing a known weight of 

silica gel desiccant; (5) a length of sample line, and (6) a Nutech control case equipped with a 

pump, dry gas meter, and calibrated orifice. Figure 7 provides an illustration of the Method 26A 

sample train. 

4.0 Test Results 

The overall results of the emissions test program are summarized by Table 2. 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

5

Table 2 

Emissions Test Program Results Summary

Test Date(s) Pollutant Emission 

Rate 

(lbs/hr) 

Emission Rate 

(lbs/ton glass) 

Emission 

Rate 

(mg/dscm)

Filterable PM2.5 <7.6 x 10-3 <2.6 x 10-3 <3.5 x 10-1

Organic Condensible PM2.5 2.1 x 10-2 7.0 x 10-3 9.5 x 10-1

Inorganic Condensible PM2.5 5.7 x 10-2 1.9 x 10-2 2.6 Sept 21 & 22, 2010 

Total PM2.5 <8.5 x 10-2 <2.9 x 10-2 <3.9 

Filterable Particulate 0.04 0.01 2.0 

Antimony <3.9 x 10-6 <1.3 x 10-6 <1.9 x 10-4

Arsenic <3.9 x 10-6 <1.3 x 10-6 <1.9 x 10-4

Beryllium <9.8 x 10-7 <3.4 x 10-7 <4.7 x 10-5

Cadmium <1.1 x 10-6 <3.9 x 10-7 <5.6 x 10-5

Chromium 2.3 x 10-5 7.7 x 10-6 1.1 x 10-3

Cobalt <1.6 x 10-6 <5.4 x 10-7 <7.7 x 10-5

Lead 1.5 x 10-5 5.1 x 10-6 7.2 x 10-4

Manganese 8.7 x 10-6 3.0 x 10-6 4.2 x 10-4

Nickel 3.9 x 10-5 1.3 x 10-5 1.9 x 10-3

Sept 21 & 22, 2010 

Selenium 1.2 x 10-5 4.0 x 10-6 5.6 x 10-4

Sept 22, 2010 Mercury 8.4 x 10-4 2.9 x 10-4 4.0 x 10-2

Sept 22 & 23, 2010 Hexavalent Chromium 6.6 x 10-6 2.2 x 10-6 3.2 x 10-4

Hydrogen Chloride <3.4 x 10-3 <1.2 x 10-3 <1.6 x 10-1

Sept 22 & 23, 2010 Hydrogen Fluoride <3.4 x 10-3 <1.2 x 10-3 <1.6 x 10-1

Notes: (1) Pollutant emission rates in terms of mg/dscm were not corrected to 7% O2 because exhaust from the 

process is essentially ambient (i.e., approximately 20.9% O2). 

(2) The “less than” symbol (<) included in the table indicates that the emission rate was calculated using the method 

detection limit (MDL) value instead of zero because the analytical result was below the MDL for one or more of the 

sample fractions. 

Detailed results for individual emission test run are summarized in Appendix A. Process 

production data is included in Appendix B. Field and computer-generated data sheets are 

included in Appendix C. Appendix D includes calibration documents and Appendix E includes 

laboratory analytical reports. 
Guardian Fiberglass, Inc. BTEC Project No. 10-3990.05 

NAIMA/U.S. EPA Emissions Test Report November 12, 2010 

6

Limitations

The information and opinions rendered in this report are exclusively for use by NAIMA and/or 

Guardian Fiberglass, Inc. BTEC will not distribute or publish this report without NAIMA’s 

consent except as required by law or court order. BTEC accepts responsibility for the competent 

performance of its duties in executing the assignment and preparing reports in accordance with 

the normal standards of the profession, but disclaims any responsibility for consequential 

damages. 

This report was prepared by: 

Brandon V. Chase 

Staff Environmental Engineer 

This report was reviewed by: 

Randal J. Tysar 

Senior Environmental Engineer 
diameter = 29"

Points Distance "

12 0.6

11 1.9

10 3.4

9 5.1

8 7.3

7 10.3

6 18.7

5 21.8

4 23.9

3 25.6

2 27.1

1 28.4

Figure 1

Site:

Guardian Fiberglass

Mineral Wells, Mississippi

Electric Melt Furnace

BT Environmental Consulting, 

Inc.

2615 Wolcott Street

Ferndale, Michigan

Not to Scale

> 14.5"

 > 58"
Bags Samples

to analyzer

Figure 2

Site:

USEPA Method 3

Guardian Fiberglass

Mineral Wells, Mississippi

Electric Melt Furnace

BT Environmental Consulting, 

Inc.

2615 Wolcott Street

Ferndale, Michigan

Orsat Absorbance 

Test Stand

pump

tedlar 

bag
Figure 3

Site:USEPA OTM27/28Guardian FiberglassMineral Wells, MississippiElectric Melt Furnace

BT Environmental Consult

2615 Wolcott Michigan

Silica gel

Heated Filter Box

S-Type Pitot w/ Thermocouple

Heated Probe w/ Glass Liner & Nozzle

Meter Rig

Temp.

ProbeFilter

On

Off

-

+

00:00

1 2 3 4 5

45mm Filter Housing

Verticle Condenser Filter Holder W/ Tef

Pot Belly Impinger 100 mL DI H2O
Figure 4

Site:USEPA Method 29Guardian FiberglassMineral Wells, Mississippi

BT Environmental Consult

2615 Wolcott Michigan 48220

Silica gel

100 mL 5% HNO3 / 10% H2O2 solution 

Heated Filter Box

S-Type Pitot w/ Thermocouple

Heated Probe w/ Glass Liner & Nozzle

Meter Rig

Temp.

ProbeFilter

On

Off

-

+

00:00

1 2 3 4 5
Figure 5

Site:USEPA Method 30B Sampling TrainGuardian FiberglassMineral Wells, MississippiElectric Melt Furnace

BT Environmental Cons2615 Wolcott Ferndale, Michigan 482

Knock out

Temperature sensor

Meter Rig

Temp.

ProbeFilter

On

Off

-

+

00:00

1 2 3 4 5

Sample Line

MercuryT rap

Probe
Figure 6

Site:USEPA Method 0061Guardian FiberglassMineral Wells, MississippiElectric Melt Furnace

BT Environmental Cons2615 WolcottFerndale, Michigan

Meter Rig

Temp.

ProbeFilter

On

Off

-

+

00:00

1 2 3 4 5

150 mL 0.1 N KOH Empty Silica Gel

Perastaltic pump

Teflon tee

75 mL 0.1 N KOH
Empty

Figure 7

Site:USEPA Method 26A Sampling TrainGuardian FiberglassMineral Wells, MississippiElectric Melt Furnace

BT Environmental Cons2615 Wolcott Michigan

Heated Filter Box

S-type pitot w/ thermocouple

Heated probe with glass liner

Meter Rig

Temp.

ProbeFilter

On

Off

-

+

00:00

1 2 3 4 5

Empty 15 mL 0.1N H2SO4 
APPENDIX A 

DETAILED TEST RUN RESULTS 
Plant Job #

Location OTM27/OTM 28 Testing Copyright by Walter Smith

Run Number 1 2 3 Average

Date Test Date 9/21/2010 9/21/2010 9/22/2010

Start Run Start Time 12:20:00 18:05:00 8:35:00

Run Finish Time 16:33:15 22:13:15 12:45:45

Net Traversing Points 12 12 12

Θ Net Run Time, minutes 226.06 226 239.41 230

DN Nozzle Diameter, inches 0.248 0.248 0.248 0.248

Cp Pitot Tube Coeficient 0.809 0.809 0.809 0.81

Y Dry Gas Meter Calibration Factor 1.009 1.009 1.009 1.009

PBr Barometric Pressure, inches of Mercury 29.82 29.82 29.89 29.84

ΔH Average orifice meter Differential, inches H2O 0.37 0.38 0.38 0.38

Vm Dry Gas Meter Volume Sampled, cubic feet 91.147 92.626 92.414 92.062

tm Average Dry Gas Meter Temperature, °F 107.42 103.17 95.71 102.10

Vmstd Dry Gas Meter Volume Sampled, dscf 85.370 87.413 88.590 87.124

Vlc Total Moisture Liquid collected, ml 72.5 69.5 75 72.3

Vwstd Volume of Water Vapor, standard cubic feet 3.41 3.27 3.53 3.40

% H2O Moisture Content of Stack Gas, % 3.8 3.6 3.8 3.8

Mfd Dry Mole Fraction 0.962 0.964 0.962 0.962

%CO2 Carbon Dioxide, % 0.4 0.6 0.4 0.5

%O2 Oxygen, % 20.8 20 20.8 20.5

% CO+ N2 Carbon Monoxide & Nitrogen, % 78.8 79.4 78.8 79.0

Md Dry Molecular Weight, lb/lb-Mole 28.90 28.90 28.90 28.90

Ms Wet Molecular weight, lb/lb-Mole 28.48 28.50 28.48 28.49

Pg Flue Gas Static Pressure, inches of H2O -0.2 -0.20 -0.20 -0.20

Ps Absolute Flue Gas Pressure, inches of Mercury 29.81 29.81 29.88 29.83

ts Average Stack Gas Temperature, °F 162 158 148 156

ΔPavg Average Velocity Head, inches of H2O 0.200 0.178 0.188 0.189

vs Average Stack Gas Velocity, feet/second 26.4 24.8 25.3 25.5

As Stack Crossectional Area, square feet 4.6 4.6 4.6 4.6

Qsd Dry Volumetric Flow Rate, dry scfm 5,605 5,907 5,803 5,772

Qaw Actual Wet Volumetric Flue Gas Flow Rate, acfm 6,830 7,259 6,960 7,016

%I Percent Isokinetic of Sampling Rate, % 87.8 94.4 85.1 89.1

Wp Production, tons glass per hour

W Filterable PM2.5 Catch Weight, mg 0.8 0.8 1.0 0.9

Cmg/dscm Filterable PM2.5 Concentration, mg/dscm 3.3E-01 3.2E-01 4.0E-01 3.5E-01

Cmg/dscm@7%O2 Filterable PM2.5 Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Filterable PM2.5 Emission Rate, pounds/hr 7.3E-03 6.8E-03 8.7E-03 7.6E-03

Elb/ton product Filterable PM2.5 Emission Rate, pounds/ton product

W Organic Condensible PM2.5 Catch Weight, mg 2.7 2.0 2.3 2.3

Cmg/dscm Organic Condensible PM2.5 Concentration, mg/dscm 1.1E+00 8.1E-01 9.2E-01 9.5E-01

Cmg/dscm@7%O2 Organic Condensible PM2.5 Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Organic Condensible PM2.5 Emission Rate, pounds/hr 2.5E-02 1.7E-02 2.0E-02 2.1E-02

Elb/ton product Organic Condensible PM2.5 Emission Rate, pounds/ton product

W Inorganic Condensible PM2.5 Catch Weight, mg 7.1 4.3 8.0 6.5

Cmg/dscm Inorganic Condensible PM2.5 Concentration, mg/dscm 2.9E+00 1.7E+00 3.2E+00 2.6E+00

Cmg/dscm@7%O2 Inorganic Condensible PM2.5 Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Inorganic Condensible PM2.5 Emission Rate, pounds/hr 6.5E-02 3.6E-02 6.9E-02 5.7E-02

Elb/ton product Inorganic Condensible PM2.5 Emission Rate, pounds/ton product

W Total PM2.5 Catch Weight, mg 10.6 7.1 11.3 9.7

Cmg/dscm Total PM2.5 Concentration, mg/dscm 4.4E+00 2.9E+00 4.5E+00 3.9E+00

Cmg/dscm@7%O2 Total PM2.5 Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Total PM2.5 Emission Rate, pounds/hr 9.7E-02 6.0E-02 9.8E-02 8.5E-02

Elb/ton product Total PM2.5 Emission Rate, pounds/ton product

Guardian Fiberglass 10-3990.05

Mineral Wells, MS

Address

Personnel -
Plant Job #

Location Method 29 Metals Copyright by Walter Smith

Run Number 1 2 3 Average

Date Test Date 9/21/2010 9/21/2010 9/22/2010

Start Run Start Time 12:20:00 18:05:00 8:35:00

Run Finish Time 16:33:00 22:09:00 12:50:00

Net Traversing Points 12 12 12

Θ Net Run Time, minutes 240 240 240 240

DN Nozzle Dianeter, inches 0.305 0.305 0.305 0.305

Cp Pitot Tube Coeficient 0.806 0.806 0.806 0.81

Y Dry Gas Meter Calibration Factor 0.990 0.990 0.990 0.990

PBr Barometric Pressure, inches of Mercury 29.82 29.78 29.88 29.83

ΔH Average orifice meter Differential, inches H2O 1.26 1.28 1.35 1.30

Vm Dry Gas Meter Volume Sampled, cubic feet 158.219 163.682 162.974 161.625

tm Average Dry Gas Meter Temperature, °F 111.55 107.10 101.52 106.73

Vmstd Dry Gas Meter Volume Sampled, dscf 144.665 150.641 152.013 149.106

Vlc Total Moisture Liquid collected, ml 119.5 115.9 126.7 120.7

Vwstd Volume of Water Vapor, standard cubic feet 5.62 5.46 5.96 5.68

% H2O Moisture Content of Stack Gas, % 3.7 3.5 3.8 3.7

Mfd Dry Mole Fraction 0.963 0.965 0.962 0.963

%CO2 Carbon Dioxide, % 0.4 0.6 0.4 0.5

%O2 Oxygen, % 20.8 20 20.8 20.5

% CO+ N2 Carbon Monoxide & Nitrogen, % 78.8 79.4 78.8 79.0

Md Dry Molecular Weight, lb/lb-Mole 28.90 28.90 28.90 28.90

Ms Wet Molecular weight, lb/lb-Mole 28.49 28.52 28.48 28.50

Pg Flue Gas Static Pressure, inches of H2O -0.20 -0.20 -0.20 -0.20

Ps Absolute Flue Gas Pressure, inches of Mercury 29.81 29.77 29.87 29.81

ts Average Stack Gas Temperature, °F 162 158 150 156

ΔPavg Average Velocity Head, inches of H2O 0.170 0.173 0.182 0.175

vs Average Stack Gas Velocity, feet/second 24.2 24.4 24.8 24.5

As Stack Crossectional Area, square feet 4.6 4.6 4.6 4.6

Qsd Dry Volumetric Flow Rate, dry scfm 5,519 5,433 5,671 5,541

Qaw Actual Wet Volumetric Flue Gas Flow Rate, acfm 6,725 6,669 6,822 6,739

%I Percent Isokinetic of Sampling Rate, % 100.5 102.9 101.0 101.5

Wp Production, tons glass per hour

W Particulate Method 5 Catch Weight, mg 10.0 10.4 5.2 8.5

Cmg/dscm Particulate Concentration, mg/dscm 2.4 2.4 1.2 2.0

Cmg/dscm@7%O2 Particulate Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Particulate Emission Rate, pounds/hr 0.05 0.05 0.03 0.04

Elb/ton product Particulate Emission Rate, pounds/ton product

W Antimony Catch Weight, μg 0.8 0.8 0.8 0.8

Cmg/dscm Antimony Concentration, mg/dscm 2.0E-04 1.9E-04 1.9E-04 1.9E-04

Cmg/dscm@7%O2 Antimony Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Antimony Emission Rate, pounds/hr 4.0E-06 3.9E-06 3.9E-06 3.9E-06

Elb/ton product Antimony Emission Rate, pounds/ton product

W Arsenic Catch Weight, μg 0.8 0.8 0.8 0.8

Cmg/dscm Arsenic Concentration, mg/dscm 2.0E-04 1.9E-04 1.9E-04 1.9E-04

Cmg/dscm@7%O2 Arsenic Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Arsenic Emission Rate, pounds/hr 4.0E-06 3.9E-06 3.9E-06 3.9E-06

Elb/ton product Arsenic Emission Rate, pounds/ton product

W Beryllium Catch Weight, μg 0.2 0.2 0.2 0.2

Cmg/dscm Beryllium Concentration, mg/dscm 4.9E-05 4.7E-05 4.6E-05 4.7E-05

Cmg/dscm@7%O2 Beryllium Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Beryllium Emission Rate, pounds/hr 9.9E-07 9.7E-07 9.9E-07 9.8E-07

Elb/ton product Beryllium Emission Rate, pounds/ton product

W Cadmium Catch Weight, μg 0.3 0.2 0.2 0.2

Cmg/dscm Cadmium Concentration, mg/dscm 7.3E-05 4.7E-05 4.6E-05 5.6E-05

Cmg/dscm@7%O2 Cadmium Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Cadmium Emission Rate, pounds/hr 1.5E-06 9.7E-07 9.9E-07 1.1E-06

Elb/ton product Cadmium Emission Rate, pounds/ton product

W Chromium Catch Weight, μg 8.8 2.2 2.7 4.6

Cmg/dscm Chromium Concentration, mg/dscm 2.1E-03 5.2E-04 6.3E-04 1.1E-03

Cmg/dscm@7%O2 Chromium Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Chromium Emission Rate, pounds/hr 4.4E-05 1.1E-05 1.3E-05 2.3E-05

Elb/ton product Chromium Emission Rate, pounds/ton product

W Cobalt Catch Weight, μg 0.5 0.3 0.2 0.3

Cmg/dscm Cobalt Concentration, mg/dscm 1.2E-04 6.1E-05 4.6E-05 7.7E-05

Cmg/dscm@7%O2 Cobalt Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Cobalt Emission Rate, pounds/hr 2.5E-06 1.3E-06 9.9E-07 1.6E-06

Elb/ton product Cobalt Emission Rate, pounds/ton product

W Lead Catch Weight, μg 6.6 0.6 1.8 3.0

Cmg/dscm Lead Concentration, mg/dscm 1.6E-03 1.4E-04 4.2E-04 7.2E-04

Cmg/dscm@7%O2 Lead Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Lead Emission Rate, pounds/hr 3.3E-05 2.9E-06 8.9E-06 1.5E-05

Elb/ton product Lead Emission Rate, pounds/ton product

W Manganese Catch Weight, μg 2.7 2.0 0.6 1.8

Cmg/dscm Manganese Concentration, mg/dscm 6.6E-04 4.7E-04 1.4E-04 4.2E-04

Cmg/dscm@7%O2 Manganese Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Manganese Emission Rate, pounds/hr 1.3E-05 9.7E-06 3.0E-06 8.7E-06

Elb/ton product Manganese Emission Rate, pounds/ton product

W Nickel Catch Weight, μg 18.7 1.2 3.9 7.9

Cmg/dscm Nickel Concentration, mg/dscm 4.6E-03 2.8E-04 9.1E-04 1.9E-03

Cmg/dscm@7%O2 Nickel Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Nickel Emission Rate, pounds/hr 9.3E-05 5.8E-06 1.9E-05 3.9E-05

Elb/ton product Nickel Emission Rate, pounds/ton product

W Selenium Catch Weight, μg 2.5 2.6 2.0 2.4

Cmg/dscm Selenium Concentration, mg/dscm 6.1E-04 6.1E-04 4.6E-04 5.6E-04

Cmg/dscm@7%O2 Selenium Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Selenium Emission Rate, pounds/hr 1.2E-05 1.3E-05 9.9E-06 1.2E-05

Elb/ton product Selenium Emission Rate, pounds/ton product

Guardian Fiberglass 10-3990.05

Mineral Wells, MS

Address

Personnel Maxwell
Company Name Plant Location City Plant Location State Source Name Source ID

Guardian Fiberglass Mineral Wells Mississippi Electric Melt Furnace Please note QA/QC documentation starting in Column "S"

Measured Value 

(mg/dscm)

Corrected 

Concentration 

(mg/dscm at 7% O2)

Basis (Wet or Dry) Test Method Used (EPA Method 30B) Data Flag (AD

BDL, DDL) 

1 9/22/2010 10:05 9/22/2010 12:05 4.42E-02 N/A Wet EPA Method 30B ADL 2 9/22/2010 14:05 9/22/2010 16:05 4.09E-02 N/A Wet EPA Method 30B ADL 3 9/23/2010 8:20 9/23/2010 10:20 3.47E-02 N/A Wet EPA Method 30B ADL 

Total Vapor Phase Mercury Emission 

Run Number Test Start Date Test Start Time Test End Date Test End Time

M30B - Guardian Mineral Wells Hg Emission Data-30B 
QA/QC Documentation

Calculated 

Emission Rate 

(lb/ton)

Trap ID Section 1 Mass (ng) Section 2 Mass (ng) Total Mass (ng) Initial Spike (ng) Total Non- Spike (ng) Sample Volume (dscm) Volume Difference (%) Volume Diff. Limit B

3.8 0.4 20.8 6,822 5,671 150 Flowrate data from M29, R3 R1, B 4940 0 4940 0 4940 0.11 1% 

3.5 0.4 20.7 6,786 5,551 162 Flowrate data from M0061, R1 R2, B 4507 2.8 4509.8 0 4509.8 0.11 1% 

3.3 0.2 20.8 6,751 5,617 153 Flowrate data from M0061, R2 R3, B 3920 6.3 3926.3 0 3926.3 0.11 1% 

Trap #1

≤20% of field 

recovery test

Flue Gas 

Temperature (F) Other Supporting Information

Flue Gas 

Moisture 

(%)

Flue Gas 

O2 (%)

Flue Gas 

CO2 (%)

Flue Gas 

Flow Rate 

(dscfm)

Flue Gas 

Flow Rate 

(acfm)

M30B - Guardian Mineral Wells Hg Emission Data-30B 
Section 1 

Mass

Section 2 

Mass

Total 

Mass

Initial 

Spike

Total NonSpike Sample Volume Volume Difference (%) Volume Diff. Limit Breaktrough (%) Breaktrough Limit Concentration (μg/dscm) Abs. diff. RD (%) Limit Crec R (%) by Run Ravg (%

4280.0 6.90 4286.90 20 4266.9 0.11 1% 0

37.8

6.3 8 -6.1607 -3476

8600.0 3.40 8603.40 20 8583.4 0.11 1% 0

77.4

36.5 31 36.6975 20346

8150.0 0.90 8150.90 20 8130.9 0.11 1% 0

71.4

36.7 35 36.8731 20984

Trap #2 Paired Trap Agreement (RD) Measured Spike Recovery ( 

≤20% of field 

recovery test

≤ 10% of Section 

1 Hg mass for 

Hg conc. >1 

μg/dscm: or ≤ 

20% of Section 1 

for Hg conc.≤1 

μg/dscm

≥10 % RD mass 

for Hg conc. >1 

μg/dscm: or 

≤20% RD or ≤0.2 

μg/dscm abs.diff. 

for Hg conc. ≤1

μg/dscm

12618

M30B - Guardian Mineral Wells Hg Emission Data-30B 
Plant Job #

Location Hex Chrome Testing Copyright by Walter Smith

Run Number 1 2 3 Average

Date Test Date 9/22/2010 9/23/2010 9/23/2010

Start Run Start Time 14:05:00 8:20:00 13:15:00

Run Finish Time 18:18:00 12:30:00 17:20:00

Net Traversing Points 12 12 12

Θ Net Run Time, minutes 240 240 240 240

DN Nozzle Dianeter, inches 0.308 0.308 0.308 0.308

Cp Pitot Tube Coeficient 0.809 0.809 0.809 0.81

Y Dry Gas Meter Calibration Factor 0.990 0.990 0.990 0.990

PBr Barometric Pressure, inches of Mercury 29.88 29.91 29.91 29.90

ΔH Average orifice meter Differential, inches H2O 1.31 1.31 1.23 1.28

Vm Dry Gas Meter Volume Sampled, cubic feet 162.296 160.692 159.123 160.704

tm Average Dry Gas Meter Temperature, °F 114.24 102.08 114.49 110.27

Vmstd Dry Gas Meter Volume Sampled, dscf 148.013 149.871 145.173 147.685

Vlc Total Moisture Liquid collected, ml 114.2 109.4 117.3 113.6

Vwstd Volume of Water Vapor, standard cubic feet 5.38 5.15 5.52 5.35

% H2O Moisture Content of Stack Gas, % 3.5 3.3 3.7 3.5

Mfd Dry Mole Fraction 0.965 0.967 0.963 0.965

%CO2 Carbon Dioxide, % 0.4 0.2 0.2 0.3

%O2 Oxygen, % 20.7 20.8 20.8 20.8

% CO+ N2 Carbon Monoxide & Nitrogen, % 78.9 79 79 79.0

Md Dry Molecular Weight, lb/lb-Mole 28.89 28.86 28.86 28.87

Ms Wet Molecular weight, lb/lb-Mole 28.51 28.50 28.47 28.49

Pg Flue Gas Static Pressure, inches of H2O -0.2 -0.20 -0.20 -0.20

Ps Absolute Flue Gas Pressure, inches of Mercury 29.87 29.90 29.90 29.89

ts Average Stack Gas Temperature, °F 162 153 162 159

ΔPavg Average Velocity Head, inches of H2O 0.175 0.176 0.166 0.172

vs Average Stack Gas Velocity, feet/second 24.7 24.5 24.0 24.4

As Stack Crossectional Area, square feet 4.6 4.6 4.6 4.6

Qsd Dry Volumetric Flow Rate, dry scfm 5,617 5,551 5,404 5,524

Qaw Actual Wet Volumetric Flue Gas Flow Rate, acfm 6,751 6,786 6,617 6,718

%I Percent Isokinetic of Sampling Rate, % 98.8 98.9 99.4 99.0

Wp Production, tons glass per hour

W Hexavalent Chromium Catch Weight, μg 1.5 2.0 0.5 1.3

Cmg/dscm Hexavalent Chromium Concentration, mg/dscm 3.6E-04 4.7E-04 1.2E-04 3.2E-04

Cmg/dscm@7%O2 Hexavalent Chromium Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr Hexavalent Chromium Emission Rate, pounds/hr 7.4E-06 9.9E-06 2.5E-06 6.6E-06

Elb/ton product Hexavalent Chromium Emission Rate, pounds/ton product

Guardian Fiberglass 10-3990.05

Mineral Wells, MS

Address

Personnel Maxwell
Plant Job #

Location HCl and HF Testing Copyright by Walter Smith

Run Number 1 2 3 Average

Date Test Date 9/22/2010 9/23/2010 9/23/2010

Start Run Start Time 15:25:00 9:40:00 14:35:00

Run Finish Time 16:48:00 11:00:00 15:54:00

Net Traversing Points 12 12 12

Θ Net Run Time, minutes 60 60 60 60

DN Nozzle Dianeter, inches 0.333 0.333 0.333 0.333

Cp Pitot Tube Coeficient 0.809 0.809 0.809 0.81

Y Dry Gas Meter Calibration Factor 1.009 1.009 1.009 1.009

PBr Barometric Pressure, inches of Mercury 29.89 29.91 29.91 29.90

ΔH Average orifice meter Differential, inches H2O 1.55 1.69 1.67 1.64

Vm Dry Gas Meter Volume Sampled, cubic feet 44.613 45.603 46.182 45.466

tm Average Dry Gas Meter Temperature, °F 110.13 95.29 110.25 105.22

Vmstd Dry Gas Meter Volume Sampled, dscf 41.806 43.919 43.308 43.011

Vlc Total Moisture Liquid collected, ml 35 41 36 37.3

Vwstd Volume of Water Vapor, standard cubic feet 1.65 1.93 1.69 1.76

% H2O Moisture Content of Stack Gas, % 3.8 4.2 3.8 3.9

Mfd Dry Mole Fraction 0.962 0.958 0.962 0.961

%CO2 Carbon Dioxide, % 0.4 0.2 0.2 0.3

%O2 Oxygen, % 20.7 20.8 20.8 20.8

% CO+ N2 Carbon Monoxide & Nitrogen, % 78.9 79 79 79.0

Md Dry Molecular Weight, lb/lb-Mole 28.89 28.86 28.86 28.87

Ms Wet Molecular weight, lb/lb-Mole 28.48 28.41 28.45 28.45

Pg Flue Gas Static Pressure, inches of H2O -0.2 -0.20 -0.20 -0.20

Ps Absolute Flue Gas Pressure, inches of Mercury 29.88 29.90 29.90 29.89

ts Average Stack Gas Temperature, °F 162 152 163 159

ΔPavg Average Velocity Head, inches of H2O 0.165 0.179 0.175 0.173

vs Average Stack Gas Velocity, feet/second 24.0 24.8 24.7 24.5

As Stack Crossectional Area, square feet 4.6 4.6 4.6 4.6

Qsd Dry Volumetric Flow Rate, dry scfm 5,639 5,379 5,544 5,521

Qaw Actual Wet Volumetric Flue Gas Flow Rate, acfm 6,827 6,598 6,805 6,743

%I Percent Isokinetic of Sampling Rate, % 98.3 98.5 98.9 98.6

Wp Production, tons glass per hour

W HCl Catch Weight, μg 200.0 200.0 200.0 200.0

Cmg/dscm HCl Concentration, mg/dscm 1.7E-01 1.6E-01 1.6E-01 1.6E-01

Cmg/dscm@7%O2 HCl Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr HCl Emission Rate, pounds/hr 3.4E-03 3.4E-03 3.4E-03 3.4E-03

Elb/ton product HCl Emission Rate, pounds/ton product

W HF Catch Weight, μg 200.0 200.0 200.0 200.0

Cmg/dscm HF Concentration, mg/dscm 1.7E-01 1.6E-01 1.6E-01 1.6E-01

Cmg/dscm@7%O2 HF Concentration, mg/dscm @ 7% O2 N/A N/A N/A

Elb/hr HF Emission Rate, pounds/hr 3.4E-03 3.4E-03 3.4E-03 3.4E-03

Elb/ton product HF Emission Rate, pounds/ton product

Guardian Fiberglass 10-3990.05

Mineral Wells, MS

Address

Personnel McDonald
APPENDIX B 

PROCESS DATA 
LINE 2 BAGHOUSE STACK - EP-5 (AB-005) - Sep 21, 2010 through Sep 22, 2010

Total

#1 #2 #3 #4 #5 #6 Pull Rate

EP-5 (AB-005) 9/21/2010 12:20 890 890 1122 1124 902 906

Run #1 12:35 898 901 1127 1126 905 901

12:50 900 898 1129 1128 900 901

13:05 906 900 1134 1127 906 902

13:20 900 901 1134 1127 906 903

13:35 906 961 1126 1125 902 898

13:50 900 903 1122 1124 901 902

14:05 906 893 1114 1122 894 900

14:20 900 896 1118 1124 897 904

14:35 898 906 1131 1117 912 904

14:50 904 902 1124 1127 899 899

15:05 904 905 1121 1130 904 898

15:20 899 898 1125 1128 903 901

15:35 901 903 1126 1128 901 905

15:50 905 901 1127 1127 900 899

16:05 901 904 1125 1125 904 898

16:20 902 900 1125 1125 906 900

16:33 908 905 1128 1124 900 907

AVG. 902 904 1125 1125 902 902 5860

EP-5 (AB-005) 9/21/2010 18:05 903 900 1126 1123 900 900

Run #2 18:20 901 899 1126 1122 900 899

18:35 901 900 1119 1123 895 897

18:50 924 895 1125 1126 904 900

19:05 902 902 1129 1125 901 907

19:20 899 903 1123 1127 900 902

19:35 901 899 1127 1126 898 900

19:50 905 904 1127 1128 892 900

20:05 902 900 1123 1122 903 900

20:20 924 896 1125 1127 904 900

20:35 939 905 1116 1124 903 895

20:50 940 897 1126 1121 900 900

21:05 952 900 1127 1124 894 902

21:20 894 898 1124 1123 900 904

21:35 955 896 1125 1099 901 901

21:50 903 899 1120 1122 903 907

22:05 898 897 1125 1127 899 904

22:15 903 901 1126 1124 902 904

AVG. 914 899 1124 1123 900 901 5862

EP-5 (AB-005) 9/22/2010 8:35 901 898 1126 1124 896 899

Run #3 8:50 902 902 1125 1124 896 898

9:05 902 900 1129 1141 897 898

9:20 900 901 1126 1123 901 902

9:35 898 899 1124 1125 899 908

9:50 901 902 1126 1125 900 901

10:05 900 904 1127 1125 904 902

10:20 902 897 1130 1127 902 904

10:35 884 896 1146 1124 897 892

10:50 905 904 1127 1126 905 900

11:05 905 897 1129 1125 898 897

11:20 904 900 1128 1125 900 901

11:35 899 900 1127 1124 901 898

11:50 900 900 1125 1125 904 903

12:05 908 900 1127 1125 900 900

12:20 900 906 1127 1126 901 897

12:35 904 906 1125 1126 898 906

12:50 913 903 1123 1125 900 904

AVG. 902 901 1128 1126 900 901 5856

Average of all 3 runs 906 901 1126 1125 901 901 5859

SPINNER PULLRATES (lbs/hour)

TEST ID DATE TIME

NON-RESINATED LINE #2
LINE 2 BAGHOUSE STACK - EP-5 (AB-005) - Sep 22, 2010 through Sep 23, 2010

Total

#1 #2 #3 #4 #5 #6 Pull Rate

EP-5 (AB-005) 9/22/2010 14:05 904 894 1130 1125 901 893

Run #1 14:20 896 905 1129 1128 902 899

14:35 910 902 1141 1125 898 1082

14:50 898 905 1137 1126 904 915

15:05 903 907 1150 1126 900 903

15:20 914 903 1163 1128 905 906

15:35 908 908 1178 1126 904 905

15:50 899 906 1184 1124 904 908

16:05 904 901 1186 1126 901 903

16:20 900 908 1188 1124 899 907

16:35 894 900 1188 1126 900 908

16:50 904 900 1178 1124 900 901

17:05 897 895 1168 1124 895 912

17:20 903 895 1159 1126 900 899

17:35 900 895 1158 1126 899 900

17:50 902 900 1158 1126 901 903

18:05 896 897 1165 1126 906 904

18:18 901 899 1166 1127 901 906

AVG. 902 901 1163 1126 901 914 5906

EP-5 (AB-005) 9/23/2010 8:20 965 888 1109 1119 889 895

Run #2 8:35 875 890 1124 1119 896 897

8:50 951 899 1120 1122 899 897

9:05 943 888 1095 1121 896 902

9:20 902 892 1120 1122 899 898

9:35 894 900 1126 1130 901 900

9:50 906 899 1129 1131 901 902

10:05 903 920 1152 1137 907 906

10:20 915 906 1145 1132 912 905

10:35 914 911 1158 1131 910 903

10:50 900 909 1179 1131 910 908

11:05 906 906 1202 1129 906 902

11:20 902 916 1230 1125 907 898

11:35 904 904 1238 1123 900 897

11:50 900 904 1244 1123 892 899

12:05 893 895 1158 1122 894 901

12:20 916 888 1123 1122 899 903

12:30 913 899 1089 1117 892 904

AVG. 911 901 1152 1125 901 901 5891

EP-5 (AB-005) 9/23/2010 13:15 891 904 1126 1124 901 893

Run #3 13:30 899 910 1124 1123 901 896

13:45 896 900 1132 1132 903 900

14:00 899 905 1126 1125 900 901

14:15 908 904 1134 1123 900 895

14:30 935 899 1121 1125 899 899

14:45 901 899 1124 1124 902 901

15:00 900 901 1127 1124 900 901

15:15 900 900 1126 1125 905 897

15:30 908 898 1128 1124 906 898

15:45 900 900 1130 1123 908 900

16:00 901 901 1127 1126 903 898

16:15 895 900 1125 1126 901 903

16:30 897 902 1125 1125 900 899

16:45 904 901 1125 1124 902 898

17:00 898 898 1125 1124 899 894

17:15 906 904 1130 1125 905 917

17:20 905 901 1126 1125 900 901

AVG. 902 902 1127 1125 902 900 5857

Average of all 3 runs 905 901 1147 1125 901 905 5885

SPINNER PULLRATES (lbs/hour)

TEST ID DATE TIME

NON-RESINATED LINE #2
APPENDIX C 

FIELD AND COMPUTER-GENERATED DATA 

SHEETS 
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # Pollutant PM2.5 Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-2 Method OTM27/28 Total Points 12

Location Mineral Wells, MSRate (cfm) Run # 1 Time/pt (min) 18.8

Source Glass Melt FurnacDelta ∆H@ 1 Date 21-Sep-10 Time/reading 18.8

Operator Bws (%) 3.84 # of Ports 2 Total Run 226.1

Filter Number Condensate Volume 56.3 Cp 0.809 Ps (in Hg) 29.81

Barometric 29.82 Silica Gel Weight Gain 16.2 DGM Y 1.009 Pm (in Hg) 29.82 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.248 O2 (%) 20.80 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00034 CO2 (%) 0.4 Md 28.90 Stack Area (sf) 4.59

Est.DH(in H2O) Ms 28.48 Act. Flow (cfm) 7,259 Must delete extra zeros in the Velocity column

Vmnstd 85.25 Preliminary dP (in H20) Total Vol.(cf) 0.0 Wet Ref Flow (cfm) 6,143

Moisture % 3.85 Preliminary Ts (oF) Est. Us (ft/s) 0.0 Dry Ref Flow (cfm) 5,907

Preliminary Tm (oF) Theor Dn (in) #DIV/0! Comments:

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 18.8 12:20 367.50 0.25 162 100 100 0.45 0.37 253 252 67 2

5 18.8 37.7 12:38 375.18 0.25 162 103 103 0.45 0.37 252 250 61 2

4 37.7 56.5 12:57 383.54 0.23 162 105 104 0.41 0.37 251 252 57 2

3 56.5 75.4 13:16 392.02 0.21 162 106 105 0.38 0.37 251 251 59 2

2 75.4 94.2 13:35 400.03 0.22 161 109 106 0.39 0.37 251 252 63 2

1 94.2 113.0 13:54 406.08 0.13 155 108 107 0.23 0.37 253 252 61 2

1 113.0 131.9 14:40 412.40 0.20 163 108 108 0.36 0.37 251 252 66 2

2 131.9 150.7 14:59 419.02 0.19 161 108 108 0.34 0.37 251 252 59 2

3 150.7 169.5 15:17 427.56 0.19 162 110 110 0.34 0.37 252 251 62 2

4 169.5 188.4 15:36 435.85 0.18 164 111 111 0.32 0.37 251 252 64 2

5 188.4 207.2 15:55 443.37 0.17 162 112 112 0.30 0.37 251 252 59 2

6 207.2 226.1 16:14 450.88 0.18 162 112 112 0.32 0.37 251 259 61 2

226.1 244.9 16:33 458.65

244.9 263.7

263.7 282.6

282.6 301.4

301.4 320.3

320.3 339.1

339.1 357.9

357.9 376.8

376.8 395.6

395.6 414.4

414.4 433.3

433.3 452.1

452.1 471.0

471.0 489.8

489.8 508.6

508.6 527.5

527.5 546.3

546.3 565.2

565.2 584.0

584.0 602.8

602.8 621.7

621.7 640.5

640.5 659.3

659.3 678.2

678.2 697.0

697.0 715.9

715.9 734.7

734.7 753.5

753.5 772.4

772.4 791.2

791.2 810.0

810.0 828.9

828.9 847.7

847.7 866.6

866.6 885.4

885.4 904.2

904.2 923.1

923.1 941.9

941.9 960.8

960.8 979.6

979.6 998.4

998.4 1017.3

1017.3 1036.1

1036.1 1054.9

1054.9 1073.8

1073.8 1092.6

1092.6 1111.5

1111.5 1130.3

1130.3 1149.1

1149.1 1168.0

1168.0 1186.8

1186.8 1205.7

1205.7 1224.5

1224.5 1243.3

1243.3 1262.2

1262.2 1281.0

1281.0 1299.8

1299.8 1318.7

1318.7 1337.5

1337.5 1356.4

1356.4 1375.2

1375.2 1394.0

1394.0 1412.9

1412.9 1431.7

1431.7 1450.6

1450.6 1469.4

1469.4 1488.2

1488.2 1507.1

1507.1 1525.9

1525.9 1544.7

1544.7 1563.6

1563.6 1582.4

1582.4 1601.3

1601.3 1620.1

1620.1 1638.9

1638.9 1657.8

1657.8 1676.6

1676.6 1695.5

1695.5 1714.3

1714.3 1733.1

1733.1 1752.0

1752.0 1770.8

1770.8 1789.6

1789.6 1808.5

1808.5 1827.3

1827.3 1846.2

1846.2 1865.0

1865.0 1883.8

1883.8 1902.7

1902.7 1921.5

1921.5 1940.3

1940.3 1959.2

1959.2 1978.0

1978.0 1996.9

1996.9 2015.7

2015.7 2034.5

2034.5 2053.4

2053.4 2072.2

2072.2 2091.1

2091.1 2109.9

2109.9 2128.7

2128.7 2147.6

2147.6 2166.4

2166.4 2185.2

2185.2 2204.1

2204.1 2222.9

2222.9 2241.8

2241.8 2260.6

Average: 91.15 0.20 161.5 107.7 107.2 0.36 0.37 252 252 61.5833333 2

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # Pollutant PM2.5 Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-2 Method OTM27-28 Total Points 12

Location Mineral Wells, MSRate (cfm) Run # 2 Time/pt (min) 18.8

Source Glass Melt FurnacDelta ∆H@ 1 Date 21-Sep-10 Time/reading 18.8

Operator Bws (%) 3.6 # of Ports 2 Total Run 226.0

Filter Number Condensate Volume 51.9 Cp 0.809 Ps (in Hg) 29.81

Barometric 29.82 Silica Gel Weight Gain 17.6 DGM Y 1.009 Pm (in Hg) 29.82 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.248 O2 (%) 20.00 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00034 CO2 (%) 0.6 Md 28.90 Stack Area (sf) 4.59

Est.DH(in H2O) Ms 28.50 Act. Flow (cfm) 6,830 Must delete extra zeros in the Velocity column

Vmnstd 87.29 Preliminary dP (in H20) Total Vol.(cf) 0.0 Wet Ref Flow (cfm) 5,815

Moisture % 3.61 Preliminary Ts (oF) Est. Us (ft/s) 0.0 Dry Ref Flow (cfm) 5,605

Preliminary Tm (oF) Theor Dn (in) #DIV/0! Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 18.8 18:05 459.10 0.18 165 107 108 0.32 0.38 250 252 67 2

5 18.8 37.7 18:23 466.51 0.19 164 108 108 0.34 0.38 251 252 65 2

4 37.7 56.5 18:42 473.67 0.18 162 108 108 0.32 0.38 251 251 63 2

3 56.5 75.3 19:01 481.15 0.17 161 108 107 0.31 0.38 250 251 62 2

2 75.3 94.2 19:20 488.76 0.17 160 107 107 0.31 0.38 250 251 62 2

1 94.2 113.0 19:39 496.24 0.18 159 105 106 0.32 0.38 251 250 64 2

1 113.0 131.8 20:20 503.09 0.20 157 101 103 0.36 0.38 250 252 66 2

2 131.8 150.7 20:39 512.76 0.22 160 100 103 0.40 0.38 250 251 56 2

3 150.7 169.5 20:57 521.35 0.18 159 102 100 0.32 0.38 256 252 56 2

4 169.5 188.3 21:16 529.60 0.16 155 97 99 0.29 0.38 252 252 56 2

5 188.3 207.2 21:35 537.72 0.15 150 96 97 0.27 0.38 251 251 58 2

6 207.2 226.0 21:54 545.49 0.15 142 95 96 0.27 0.38 252 253 62 2

226.0 244.8 22:13 551.73

244.8 263.7

263.7 282.5

282.5 301.3

301.3 320.2

320.2 339.0

339.0 357.8

357.8 376.7

376.7 395.5

395.5 414.3

414.3 433.2

433.2 452.0

452.0 470.8

470.8 489.7

489.7 508.5

508.5 527.3

527.3 546.2

546.2 565.0

565.0 583.8

583.8 602.7

602.7 621.5

621.5 640.3

640.3 659.2

659.2 678.0

678.0 696.8

696.8 715.7

715.7 734.5

734.5 753.3

753.3 772.2

772.2 791.0

791.0 809.8

809.8 828.7

828.7 847.5

847.5 866.3

866.3 885.2

885.2 904.0

904.0 922.8

922.8 941.7

941.7 960.5

960.5 979.3

979.3 998.2

998.2 1017.0

1017.0 1035.8

1035.8 1054.7

1054.7 1073.5

1073.5 1092.3

1092.3 1111.2

1111.2 1130.0

1130.0 1148.8

1148.8 1167.7

1167.7 1186.5

1186.5 1205.3

1205.3 1224.2

1224.2 1243.0

1243.0 1261.8

1261.8 1280.7

1280.7 1299.5

1299.5 1318.3

1318.3 1337.2

1337.2 1356.0

1356.0 1374.8

1374.8 1393.7

1393.7 1412.5

1412.5 1431.3

1431.3 1450.2

1450.2 1469.0

1469.0 1487.8

1487.8 1506.7

1506.7 1525.5

1525.5 1544.3

1544.3 1563.2

1563.2 1582.0

1582.0 1600.8

1600.8 1619.7

1619.7 1638.5

1638.5 1657.3

1657.3 1676.2

1676.2 1695.0

1695.0 1713.8

1713.8 1732.7

1732.7 1751.5

1751.5 1770.3

1770.3 1789.2

1789.2 1808.0

1808.0 1826.8

1826.8 1845.7

1845.7 1864.5

1864.5 1883.3

1883.3 1902.2

1902.2 1921.0

1921.0 1939.8

1939.8 1958.7

1958.7 1977.5

1977.5 1996.3

1996.3 2015.2

2015.2 2034.0

2034.0 2052.8

2052.8 2071.7

2071.7 2090.5

2090.5 2109.3

2109.3 2128.2

2128.2 2147.0

2147.0 2165.8

2165.8 2184.7

2184.7 2203.5

2203.5 2222.3

2222.3 2241.2

2241.2 2260.0

Average: 92.63 0.18 157.8 102.8 103.5 0.32 0.38 251.2 251.5 61.4 2

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # Pollutant PM2.5 Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-2 Method OTM27-28 Total Points 12

Location Mineral Wells, MSRate (cfm) Run # 3 Time/pt (min) 20.6

Source Glass Melt FurnacDelta ∆H@ 1 Date 22-Sep-10 Time/reading 20.6

Operator Bws (%) 3.8 # of Ports 2 Total Run 246.8

Filter Number Condensate Volume 58.3 Cp 0.809 Ps (in Hg) 29.88

Barometric 29.89 Silica Gel Weight Gain 16.7 DGM Y 1.009 Pm (in Hg) 29.89 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.248 O2 (%) 20.80 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00034 CO2 (%) 0.4 Md 28.90 Stack Area (sf) 4.59

Est.DH(in H2O) Ms 28.48 Act. Flow (cfm) 6,960 Must delete extra zeros in the Velocity column

Vmnstd 88.46 Preliminary dP (in H20) Total Vol.(cf) 0.0 Wet Ref Flow (cfm) 6,035

Moisture % 3.84 Preliminary Ts (oF) Est. Us (ft/s) 0.0 Dry Ref Flow (cfm) 5,803

Preliminary Tm (oF) Theor Dn (in) #DIV/0! Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 20.6 8:35 552.30 0.24 142 88 87 0.43 0.38 251 252 64 2

5 20.6 41.1 8:55 559.46 0.22 145 90 89 0.39 0.38 250 252 52 2

4 41.1 61.7 9:16 566.31 0.22 147 91 90 0.39 0.38 250 251 52 2

3 61.7 82.3 9:36 574.24 0.20 150 94 92 0.36 0.38 251 252 55 2

2 82.3 102.8 9:57 582.62 0.19 146 95 93 0.34 0.38 253 255 56 2

1 102.8 123.4 10:17 591.16 0.14 142 96 94 0.25 0.38 251 253 60 2

1 123.4 144.0 10:42 599.04 0.21 147 97 96 0.38 0.38 252 254 65 2

2 144.0 164.5 11:02 607.19 0.18 150 100 97 0.32 0.38 251 252 57 2

3 164.5 185.1 11:23 615.52 0.19 150 100 99 0.34 0.38 251 250 59 2

4 185.1 205.7 11:44 623.53 0.16 151 100 99 0.29 0.38 250 251 60 2

5 205.7 226.2 12:04 630.80 0.16 153 102 101 0.29 0.38 251 253 63 2

6 226.2 246.8 12:25 637.57 0.15 154 104 103 0.27 0.38 251 251 59 2

246.8 267.4 12:45 644.71

267.4 287.9

287.9 308.5

308.5 329.1

329.1 349.6

349.6 370.2

370.2 390.8

390.8 411.3

411.3 431.9

431.9 452.4

452.4 473.0

473.0 493.6

493.6 514.1

514.1 534.7

534.7 555.3

555.3 575.8

575.8 596.4

596.4 617.0

617.0 637.5

637.5 658.1

658.1 678.7

678.7 699.2

699.2 719.8

719.8 740.4

740.4 760.9

760.9 781.5

781.5 802.1

802.1 822.6

822.6 843.2

843.2 863.8

863.8 884.3

884.3 904.9

904.9 925.5

925.5 946.0

946.0 966.6

966.6 987.2

987.2 1007.7

1007.7 1028.3

1028.3 1048.9

1048.9 1069.4

1069.4 1090.0

1090.0 1110.6

1110.6 1131.1

1131.1 1151.7

1151.7 1172.3

1172.3 1192.8

1192.8 1213.4

1213.4 1234.0

1234.0 1254.5

1254.5 1275.1

1275.1 1295.6

1295.6 1316.2

1316.2 1336.8

1336.8 1357.3

1357.3 1377.9

1377.9 1398.5

1398.5 1419.0

1419.0 1439.6

1439.6 1460.2

1460.2 1480.7

1480.7 1501.3

1501.3 1521.9

1521.9 1542.4

1542.4 1563.0

1563.0 1583.6

1583.6 1604.1

1604.1 1624.7

1624.7 1645.3

1645.3 1665.8

1665.8 1686.4

1686.4 1707.0

1707.0 1727.5

1727.5 1748.1

1748.1 1768.7

1768.7 1789.2

1789.2 1809.8

1809.8 1830.4

1830.4 1850.9

1850.9 1871.5

1871.5 1892.1

1892.1 1912.6

1912.6 1933.2

1933.2 1953.8

1953.8 1974.3

1974.3 1994.9

1994.9 2015.5

2015.5 2036.0

2036.0 2056.6

2056.6 2077.1

2077.1 2097.7

2097.7 2118.3

2118.3 2138.8

2138.8 2159.4

2159.4 2180.0

2180.0 2200.5

2200.5 2221.1

2221.1 2241.7

2241.7 2262.2

2262.2 2282.8

2282.8 2303.4

2303.4 2323.9

2323.9 2344.5

2344.5 2365.1

2365.1 2385.6

2385.6 2406.2

2406.2 2426.8

2426.8 2447.3

2447.3 2467.9

Average: 92.41 0.19 148.1 96.4 95.0 0.34 0.38 251.0 252.2 58.5 2.0

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 51-3-1 Pollutant Metals/PM Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-1 Method M29 Total Points 12

Location Mineral Wells, MSRate (cfm) 0.602 Run # 1 Time/pt (min) 20.0

Source Furnace Stack Delta ∆H@ Date 21-Sep-10 Time/reading 5.0

Operator Maxwell Bws (%) 3.74 # of Ports 2 Total Run 240.0

Filter Number Condensate Volume 91 Cp 0.806 Ps (in Hg) 29.81

Barometric 29.82 Silica Gel Weight Gain 28.5 DGM Y 0.99 Pm (in Hg) 30.04 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.305 O2 (%) 20.8 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00051 CO2 (%) 0.4 Md 28.90 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.49 Act. Flow (cfm) 6,669 Must delete extra zeros in the Velocity column

Vmnstd 144.15 Preliminary dP (in H20) 0.36 Total Vol.(cf) 144.5 Wet Ref Flow (cfm) 5,644

Moisture % 3.76 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.3 Dry Ref Flow (cfm) 5,433

Preliminary Tm (oF) 85 Theor Dn (in) 0.2729 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

1 0.0 5.0 12:20 93.51 0.20 159.00 103.00 103.00 0.00 1.50 255.00 255.00 60.00 4.00

5.0 10.0 12:25 95.74 0.20 159.00 103.00 103.00 0.00 1.50 250.00 254.00 60.00 4.00

2 10.0 15.0 12:30 98.26 0.18 160.00 103.00 103.00 0.00 1.35 250.00 253.00 61.00 4.00

15.0 20.0 12:35 102.80 0.18 160.00 105.00 103.00 0.00 1.35 251.00 252.00 61.00 4.00

3 20.0 25.0 12:40 105.75 0.20 161.00 106.00 104.00 0.00 1.50 255.00 252.00 61.00 4.00

25.0 30.0 12:45 109.15 0.19 161.00 107.00 104.00 0.00 1.40 256.00 254.00 60.00 4.00

4 30.0 35.0 12:50 112.42 0.19 161.00 108.00 104.00 0.00 1.40 254.00 255.00 60.00 4.00

35.0 40.0 12:55 116.40 0.19 160.00 109.00 105.00 0.00 1.40 250.00 251.00 60.00 4.00

5 40.0 45.0 13:00 119.33 0.21 162.00 109.00 105.00 0.00 1.55 251.00 253.00 60.00 4.00

45.0 50.0 13:05 122.74 0.21 162.00 110.00 106.00 0.00 1.55 250.00 251.00 60.00 4.00

6 50.0 55.0 13:10 126.96 0.21 162.00 110.00 106.00 0.00 1.55 250.00 250.00 59.00 4.00

55.0 60.0 13:15 130.12 0.21 162.00 111.00 106.00 0.00 1.55 251.00 250.00 59.00 4.00

7 60.0 65.0 13:20 133.62 0.16 162.00 112.00 108.00 0.00 1.20 250.00 249.00 58.00 4.00

65.0 70.0 13:25 136.94 0.16 162.00 112.00 108.00 0.00 1.20 251.00 248.00 58.00 4.00

8 70.0 75.0 13:30 138.26 0.16 161.00 113.00 108.00 0.00 1.20 251.00 253.00 59.00 4.00

75.0 80.0 13:35 143.37 0.16 162.00 113.00 108.00 0.00 1.20 251.00 250.00 59.00 4.00

9 80.0 85.0 13:40 147.10 0.15 163.00 113.00 109.00 0.00 1.10 250.00 249.00 59.00 4.00

85.0 90.0 13:45 149.76 0.15 163.00 113.00 109.00 0.00 1.10 251.00 250.00 59.00 4.00

10 90.0 95.0 13:50 152.88 0.15 163.00 113.00 109.00 0.00 1.10 249.00 251.00 60.00 3.00

95.0 100.0 13:55 156.68 0.15 163.00 113.00 110.00 0.00 1.10 250.00 249.00 60.00 3.00

11 100.0 105.0 14:00 159.22 0.15 162.00 113.00 110.00 0.00 1.10 250.00 255.00 61.00 3.00

105.0 110.0 14:05 162.25 0.15 162.00 114.00 110.00 0.00 1.10 251.00 254.00 61.00 3.00

12 110.0 115.0 14:10 166.04 0.15 162.00 114.00 111.00 0.00 1.10 251.00 250.00 61.00 3.00

115.0 120.0 14:15 168.56 0.15 162.00 115.00 111.00 0.00 1.10 250.00 250.00 60.00 3.00

1 120.0 120.0 14:20 171.52

120.0 125.0 14:33 171.52 0.19 163.00 111.00 111.00 0.00 1.40 251.00 249.00 61.00 3.00

2 125.0 130.0 14:38 174.89 0.19 162.00 112.00 111.00 0.00 1.40 255.00 254.00 62.00 3.00

130.0 135.0 14:43 178.38 0.19 161.00 113.00 111.00 0.00 1.40 254.00 254.00 61.00 3.00

3 135.0 140.0 14:48 181.91 0.19 160.00 114.00 111.00 0.00 1.40 255.00 254.00 60.00 3.00

140.0 145.0 14:53 185.45 0.15 160.00 114.00 111.00 0.00 1.10 255.00 254.00 62.00 3.00

4 145.0 150.0 14:58 188.70 0.15 160.00 115.00 111.00 0.00 1.10 255.00 254.00 63.00 3.00

150.0 155.0 15:03 191.93 0.15 161.00 115.00 111.00 0.00 1.10 254.00 255.00 63.00 3.00

5 155.0 160.0 15:08 195.16 0.15 164.00 115.00 112.00 0.00 1.10 255.00 254.00 64.00 3.00

160.0 165.0 15:13 198.39 0.16 164.00 116.00 112.00 0.00 1.20 255.00 254.00 64.00 3.00

6 165.0 170.0 15:18 201.72 0.16 162.00 117.00 112.00 0.00 1.20 255.00 255.00 64.00 3.00

170.0 175.0 15:23 205.08 0.16 162.00 117.00 112.00 0.00 1.20 255.00 254.00 63.00 3.00

7 175.0 180.0 15:28 208.48 0.16 164.00 117.00 112.00 0.00 1.20 255.00 255.00 63.00 3.00

180.0 185.0 15:33 211.71 0.16 164.00 117.00 113.00 0.00 1.20 255.00 255.00 62.00 3.00

8 185.0 190.0 15:38 215.12 0.16 163.00 118.00 114.00 0.00 1.20 254.00 253.00 63.00 3.00

190.0 195.0 15:43 218.47 0.16 164.00 118.00 114.00 0.00 1.20 254.00 255.00 64.00 3.00

9 195.0 200.0 15:48 220.92 0.16 162.00 118.00 115.00 0.00 1.20 250.00 250.00 63.00 3.00

200.0 205.0 15:53 225.15 0.15 162.00 118.00 115.00 0.00 1.10 250.00 252.00 63.00 3.00

10 205.0 210.0 15:58 229.00 0.18 160.00 118.00 115.00 0.00 1.35 250.00 250.00 63.00 3.00

210.0 215.0 16:03 232.00 0.18 160.00 118.00 115.00 0.00 1.35 250.00 251.00 63.00 3.00

11 215.0 220.0 16:08 235.46 0.18 160.00 118.00 115.00 0.00 1.35 251.00 252.00 63.00 3.00

220.0 225.0 16:13 240.12 0.15 160.00 118.00 115.00 0.00 1.10 250.00 250.00 60.00 3.00

12 225.0 230.0 16:18 242.71 0.15 160.00 118.00 115.00 0.00 1.10 250.00 250.00 61.00 3.00

230.0 235.0 16:23 245.50 0.15 160.00 118.00 115.00 0.00 1.10 251.00 253.00 62.00 3.00

235.0 240.0 16:28 248.94 0.15 160.00 118.00 115.00 1.10 251.00 250.00 64.00 3.00

240.0 240.0 16:33 251.73

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 158.22 0.17 161.5 113.2 109.9 0.00 1.26 252 252 61.1875 3

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 51-3-1 Pollutant Metals/PM Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-1 Method M29 Total Points 12

Location Mineral Wells, MSRate (cfm) 0.602 Run # 2 Time/pt (min) 20.0

Source Furnace Stack Delta ∆H@ 0 Date 21-Sep-10 Time/reading 5.0

Operator Maxwell Bws (%) 3.5 # of Ports 2 Total Run 240.0

Filter Number 0 Condensate Volume 85.4 Cp 0.806 Ps (in Hg) 29.77

Barometric 29.78 Silica Gel Weight Gain 30.5 DGM Y 0.99 Pm (in Hg) 30.00 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.305 O2 (%) 20 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00051 CO2 (%) 0.6 Md 28.90 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.52 Act. Flow (cfm) 6,725 Must delete extra zeros in the Velocity column

Vmnstd 150.09 Preliminary dP (in H20) 0.36 Total Vol.(cf) 144.5 Wet Ref Flow (cfm) 5,719

Moisture % 3.51 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.3 Dry Ref Flow (cfm) 5,519

Preliminary Tm (oF) 85 Theor Dn (in) 0.2725 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

1 0.0 5.0 18:05 253.64 0.15 165.00 109.00 110.00 0.00 1.10 250.00 249.00 60.00 3.00

5.0 10.0 18:10 256.81 0.15 165.00 109.00 110.00 0.00 1.10 251.00 250.00 60.00 3.00

2 10.0 15.0 18:15 260.32 0.15 165.00 110.00 110.00 0.00 1.10 249.00 251.00 60.00 3.00

15.0 20.0 18:20 263.24 0.15 165.00 111.00 110.00 0.00 1.10 251.00 250.00 60.00 3.00

3 20.0 25.0 18:25 267.46 0.15 163.00 112.00 110.00 0.00 1.10 249.00 251.00 61.00 3.00

25.0 30.0 18:30 270.10 0.15 163.00 112.00 110.00 0.00 1.10 249.00 256.00 61.00 3.00

4 30.0 35.0 18:35 273.20 0.15 163.00 112.00 110.00 0.00 1.10 251.00 253.00 61.00 3.00

35.0 40.0 18:40 276.44 0.15 163.00 112.00 110.00 0.00 1.10 253.00 254.00 61.00 3.00

5 40.0 45.0 18:45 279.71 0.15 162.00 113.00 110.00 0.00 1.10 254.00 255.00 62.00 3.00

45.0 50.0 18:50 283.24 0.15 162.00 113.00 110.00 0.00 1.10 254.00 255.00 63.00 3.00

6 50.0 55.0 18:55 286.09 0.15 162.00 113.00 110.00 0.00 1.10 255.00 255.00 64.00 3.00

55.0 60.0 19:00 289.36 0.15 162.00 112.00 110.00 0.00 1.10 254.00 255.00 65.00 3.00

7 60.0 65.0 19:05 292.62 0.17 161.00 113.00 110.00 0.00 1.25 255.00 255.00 65.00 3.00

65.0 70.0 19:10 295.93 0.17 161.00 113.00 110.00 0.00 1.25 254.00 255.00 65.00 3.00

8 70.0 75.0 19:15 299.39 0.17 161.00 113.00 110.00 0.00 1.25 254.00 254.00 65.00 3.00

75.0 80.0 19:20 303.11 0.17 161.00 113.00 110.00 0.00 1.25 255.00 255.00 66.00 3.00

9 80.0 85.0 19:25 306.36 0.21 160.00 113.00 110.00 0.00 1.60 254.00 255.00 65.00 3.00

85.0 90.0 19:30 310.21 0.21 160.00 113.00 110.00 0.00 1.60 254.00 254.00 65.00 3.00

10 90.0 95.0 19:35 314.05 0.21 160.00 112.00 109.00 0.00 1.60 255.00 254.00 66.00 3.00

95.0 100.0 19:40 317.32 0.21 160.00 112.00 109.00 0.00 1.60 255.00 253.00 66.00 3.00

11 100.0 105.0 19:45 322.25 0.19 158.00 112.00 108.00 0.00 1.40 254.00 253.00 65.00 3.00

105.0 110.0 19:50 325.51 0.19 158.00 112.00 108.00 0.00 1.40 253.00 255.00 64.00 3.00

12 110.0 115.0 19:55 329.14 0.19 158.00 111.00 108.00 0.00 1.40 255.00 255.00 64.00 3.00

115.0 120.0 20:00 332.03 0.19 158.00 111.00 107.00 0.00 1.40 255.00 255.00 64.00 3.00

1 120.0 120.0 20:05 335.39

120.0 125.0 20:09 335.39 0.17 160.00 107.00 106.00 0.00 1.25 254.00 254.00 64.00 3.00

2 125.0 130.0 20:14 339.92 0.17 160.00 107.00 106.00 0.00 1.25 254.00 254.00 64.00 3.00

130.0 135.0 20:19 342.25 0.17 160.00 107.00 105.00 0.00 1.25 255.00 255.00 63.00 3.00

3 135.0 140.0 20:24 345.63 0.17 160.00 107.00 105.00 0.00 1.25 255.00 255.00 63.00 3.00

140.0 145.0 20:29 349.38 0.18 160.00 108.00 105.00 0.00 1.35 254.00 253.00 61.00 3.00

4 145.0 150.0 20:34 352.43 0.18 160.00 108.00 105.00 0.00 1.35 253.00 253.00 59.00 3.00

150.0 155.0 20:39 355.97 0.18 160.00 107.00 104.00 0.00 1.35 255.00 254.00 59.00 3.00

5 155.0 160.0 20:44 358.72 0.18 160.00 107.00 104.00 0.00 1.35 255.00 255.00 59.00 3.00

160.0 165.0 20:49 362.89 0.19 156.00 106.00 104.00 0.00 1.40 254.00 256.00 59.00 3.00

6 165.0 170.0 20:54 365.21 0.19 156.00 106.00 104.00 0.00 1.40 254.00 255.00 59.00 3.00

170.0 175.0 20:59 370.04 0.19 156.00 106.00 103.00 0.00 1.40 253.00 254.00 59.00 3.00

7 175.0 180.0 21:04 373.73 0.19 156.00 105.00 102.00 0.00 1.40 254.00 255.00 60.00 3.00

180.0 185.0 21:09 377.31 0.17 154.00 105.00 102.00 0.00 1.25 255.00 255.00 59.00 3.00

8 185.0 190.0 21:14 381.36 0.17 154.00 105.00 102.00 0.00 1.25 255.00 255.00 59.00 3.00

190.0 195.0 21:19 385.08 0.17 154.00 104.00 101.00 0.00 1.25 254.00 253.00 60.00 3.00

9 195.0 200.0 21:24 388.01 0.17 154.00 103.00 100.00 0.00 1.25 253.00 255.00 60.00 3.00

200.0 205.0 21:29 391.27 0.19 150.00 103.00 100.00 0.00 1.40 253.00 255.00 60.00 3.00

10 205.0 210.0 21:34 395.04 0.19 150.00 103.00 100.00 0.00 1.40 254.00 254.00 60.00 3.00

210.0 215.0 21:39 398.45 0.19 150.00 103.00 99.00 0.00 1.40 253.00 254.00 60.00 3.00

11 215.0 220.0 21:44 402.17 0.19 150.00 103.00 99.00 0.00 1.40 254.00 254.00 60.00 3.00

220.0 225.0 21:49 405.32 0.16 143.00 103.00 99.00 0.00 1.20 253.00 255.00 61.00 3.00

12 225.0 230.0 21:54 409.15 0.16 143.00 102.00 99.00 0.00 1.20 255.00 255.00 62.00 3.00

230.0 235.0 21:59 412.06 0.16 143.00 101.00 99.00 0.00 1.20 254.00 253.00 64.00 3.00

235.0 240.0 22:04 414.70 0.16 143.00 100.00 98.00 1.20 255.00 255.00 64.00 3.00

240.0 240.0 22:09 417.33

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 163.68 0.17 157.7 108.4 105.8 0.00 1.28 253.6 254.0 62.0 3

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 51-3-1 Pollutant Metals/PM Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-1 Method M29 Total Points 12

Location Mineral Wells, MSRate (cfm) 0.602 Run # 3 Time/pt (min) 20.0

Source Furnace Stack Delta ∆H@ Date 22-Sep-10 Time/reading 5.0

Operator Maxwell Bws (%) 3.8 # of Ports 2 Total Run 240.0

Filter Number Condensate Volume 95.8 Cp 0.806 Ps (in Hg) 29.87

Barometric 29.88 Silica Gel Weight Gain 30.9 DGM Y 0.99 Pm (in Hg) 30.10 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.305 O2 (%) 20.8 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00051 CO2 (%) 0.4 Md 28.90 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.48 Act. Flow (cfm) 6,822 Must delete extra zeros in the Velocity column

Vmnstd 151.44 Preliminary dP (in H20) 0.36 Total Vol.(cf) 144.5 Wet Ref Flow (cfm) 5,893

Moisture % 3.79 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.3 Dry Ref Flow (cfm) 5,671

Preliminary Tm (oF) 85 Theor Dn (in) 0.2731 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

1 0.0 5.0 8:35 417.64 0.20 145.00 90.00 90.00 0.00 1.50 249.00 251.00 72.00 3.00

5.0 10.0 8:40 421.11 0.20 145.00 90.00 90.00 0.00 1.50 251.00 252.00 67.00 3.00

2 10.0 15.0 8:45 425.10 0.20 145.00 93.00 91.00 0.00 1.50 250.00 249.00 59.00 3.00

15.0 20.0 8:50 429.26 0.20 145.00 94.00 91.00 0.00 1.50 251.00 249.00 59.00 3.00

3 20.0 25.0 8:55 433.64 0.18 147.00 95.00 92.00 0.00 1.35 250.00 248.00 59.00 3.00

25.0 30.0 9:00 435.67 0.18 148.00 96.00 93.00 0.00 1.35 251.00 252.00 60.00 3.00

4 30.0 35.0 9:05 438.23 0.18 148.00 96.00 93.00 0.00 1.35 251.00 253.00 60.00 3.00

35.0 40.0 9:10 441.76 0.18 148.00 97.00 93.00 0.00 1.35 252.00 258.00 61.00 3.00

5 40.0 45.0 9:15 445.16 0.20 148.00 98.00 94.00 0.00 1.50 251.00 259.00 61.00 3.00

45.0 50.0 9:20 449.10 0.20 148.00 99.00 95.00 0.00 1.50 252.00 250.00 61.00 3.00

6 50.0 55.0 9:25 451.61 0.20 148.00 100.00 96.00 0.00 1.50 250.00 249.00 61.00 3.00

55.0 60.0 9:30 455.60 0.20 148.00 101.00 97.00 0.00 1.50 250.00 251.00 61.00 3.00

7 60.0 65.0 9:35 460.11 0.14 148.00 101.00 97.00 0.00 1.05 251.00 252.00 61.00 3.00

65.0 70.0 9:40 463.20 0.14 149.00 102.00 97.00 0.00 1.05 250.00 251.00 61.00 3.00

8 70.0 75.0 9:45 465.10 0.14 149.00 102.00 97.00 0.00 1.05 250.00 250.00 61.00 3.00

75.0 80.0 9:50 468.12 0.14 149.00 102.00 97.00 0.00 1.05 251.00 250.00 61.00 3.00

9 80.0 85.0 9:55 471.75 0.15 149.00 102.00 97.00 0.00 1.10 250.00 249.00 61.00 3.00

85.0 90.0 10:00 474.70 0.15 149.00 102.00 97.00 0.00 1.10 251.00 250.00 61.00 3.00

10 90.0 95.0 10:05 478.22 0.15 149.00 103.00 98.00 0.00 1.10 249.00 252.00 56.00 3.00

95.0 100.0 10:10 481.00 0.15 149.00 104.00 99.00 0.00 1.10 251.00 251.00 56.00 3.00

11 100.0 105.0 10:15 485.20 0.15 149.00 104.00 99.00 0.00 1.10 250.00 252.00 57.00 3.00

105.0 110.0 10:20 487.30 0.15 149.00 104.00 99.00 0.00 1.10 251.00 255.00 58.00 3.00

12 110.0 115.0 10:25 490.39 0.15 149.00 104.00 99.00 0.00 1.10 251.00 253.00 59.00 3.00

115.0 120.0 10:30 493.90 0.15 149.00 105.00 100.00 0.00 1.10 252.00 250.00 59.00 3.00

1 120.0 120.0 10:35 496.84

120.0 125.0 10:50 496.84 0.23 151.00 100.00 100.00 0.00 1.70 251.00 256.00 69.00 3.00

2 125.0 130.0 10:55 499.60 0.23 153.00 104.00 100.00 0.00 1.70 250.00 254.00 68.00 3.00

130.0 135.0 11:00 504.33 0.23 151.00 104.00 100.00 0.00 1.70 250.00 255.00 56.00 3.00

3 135.0 140.0 11:05 508.60 0.23 151.00 104.00 100.00 0.00 1.70 252.00 250.00 56.00 3.00

140.0 145.0 11:10 512.00 0.21 153.00 105.00 101.00 0.00 1.55 254.00 251.00 56.00 3.00

4 145.0 150.0 11:15 515.62 0.21 153.00 106.00 101.00 0.00 1.55 250.00 256.00 56.00 3.00

150.0 155.0 11:20 519.40 0.21 153.00 106.00 102.00 0.00 1.55 251.00 252.00 57.00 3.00

5 155.0 160.0 11:25 522.45 0.21 153.00 107.00 102.00 0.00 1.55 250.00 254.00 58.00 3.00

160.0 165.0 11:30 521.63 0.21 153.00 107.00 102.00 0.00 1.55 251.00 250.00 58.00 3.00

6 165.0 170.0 11:35 529.92 0.21 153.00 107.00 103.00 0.00 1.55 250.00 251.00 59.00 3.00

170.0 175.0 11:40 533.10 0.21 153.00 107.00 103.00 0.00 1.55 251.00 250.00 60.00 3.00

7 175.0 180.0 11:45 537.28 0.21 153.00 108.00 104.00 0.00 1.55 251.00 251.00 60.00 3.00

180.0 185.0 11:50 540.67 0.20 152.00 108.00 104.00 0.00 1.50 250.00 252.00 60.00 3.00

8 185.0 190.0 11:55 544.97 0.20 152.00 108.00 104.00 0.00 1.50 251.00 250.00 60.00 3.00

190.0 195.0 12:00 547.45 0.20 152.00 108.00 104.00 0.00 1.50 250.00 251.00 60.00 3.00

9 195.0 200.0 12:05 550.62 0.20 152.00 110.00 105.00 0.00 1.50 251.00 250.00 61.00 3.00

200.0 205.0 12:10 555.52 0.17 152.00 110.00 105.00 0.00 1.25 250.00 250.00 60.00 3.00

10 205.0 210.0 12:15 558.95 0.17 152.00 110.00 105.00 0.00 1.25 250.00 250.00 60.00 3.00

210.0 215.0 12:20 562.01 0.17 152.00 110.00 106.00 0.00 1.25 250.00 250.00 60.00 3.00

11 215.0 220.0 12:25 564.40 0.17 152.00 110.00 106.00 0.00 1.25 250.00 258.00 61.00 3.00

220.0 225.0 12:30 568.10 0.14 152.00 111.00 107.00 0.00 1.05 250.00 253.00 61.00 3.00

12 225.0 230.0 12:35 571.40 0.14 152.00 112.00 107.00 0.00 1.05 250.00 251.00 61.00 3.00

230.0 235.0 12:40 574.96 0.14 152.00 112.00 107.00 0.00 1.05 250.00 251.00 61.00 3.00

235.0 240.0 12:45 578.72 0.14 152.00 112.00 107.00 0.00 1.05 250.00 253.00 61.00 3.00

240.0 240.0 12:50 580.61

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 162.97 0.18 150.1 103.5 99.5 0.00 1.35 250.6 251.8 60.2291667 3.0

Leak Check
BT Environmental Consulting

30B Run Sheet

Project No.: 10-286-D Probe # Pollutant Hg Points/Port 1Company Guardian FiberglassDGM # HG2 Method 30B Total Points 1

Location Mineral Wells, MS Rate (L/m) 1 L/min. Run # 1 Time/pt (min) 5.0

Source Furnace Stack Delta ∆H@ Date 22-Sep-10 Time/reading 5.0Operator Pineda Bws (%) # of Ports 1 Total Run 120.0

Filter Number Condensate Volume Cp Ps (in Hg) 29.88Barometric 29.89 Silica Gel Weight Gain DGM Y 0.991, 0.989 Pm (in Hg) 29.89 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) O2 (%) Ref Press 29.92Stack Dia (ft) 2.42 An (ft^2) 4.58800 CO2 (%) Md 28.00 Stack Area (sf) 4.59

Est.DH(in H2O) Ms 28.00 Act. Flow (cfm)

Preliminary dP (in H20) Total Vol.(cf) Wet Ref Flow (cfm)Preliminary Ts (oF) Est. Us (ft/s) Dry Ref Flow (cfm) 

Preliminary Tm (oF) Theor Dn (in)

Clock Time Sample Time Stack Temp

A B A B A B AB A B 

10:05:00 AM 0.0 253 253 1 1 4 4 0.00 0 93 9310:10:00 AM 5.0 249 249 1 1 4 4 4.86 4.8 95 9410:15:00 AM 10.0 250 250 1 1 4 4 9.79 9.75 95 9410:20:00 AM 15.0 247 247 1 1 4 4 14.65 14.55 96 9510:25:00 AM 20.0 248 248 1 1 4 5 18.75 18.21 97 9610:30:00 AM 25.0 248 248 1 1 4 5 24.47 24.39 97 9610:35:00 AM 30.0 248 248 1 1 5 6 29.79 29.51 98 9610:40:00 AM 35.0 248 248 1 1 5 6 36.47 35.51 98 9710:45:00 AM 40.0 249 249 1 1 4 6 40.06 39.71 98 9710:50:00 AM 45.0 248 248 1 1 4 6 44.75 43.49 99 9810:55:00 AM 50.0 249 249 1 1 4 6 49.89 48.58 99 9811:00:00 AM 55.0 248 248 1 1 4 6 54.79 54.23 100 9911:05:00 AM 60.0 248 248 1 1 5 6 60.45 59.79 100 9911:10:00 AM 65.0 248 248 1 1 5 6 65.22 64.79 100 10011:15:00 AM 70.0 250 250 1 1 5 6 70.04 69.51 100 10011:20:00 AM 75.0 248 248 1 1 4 6 74.79 74.44 100 10011:25:00 AM 80.0 249 249 1 1 4 6 79.28 78.86 101 10111:30:00 AM 85.0 249 249 1 1 4 6 84.59 85.02 102 10111:35:00 AM 90.0 248 248 1 1 4 6 89.15 89.55 101 10211:40:00 AM 95.0 248 248 1 1 4 6 95.27 94.78 102 10211:45:00 AM 100.0 248 248 1 1 4 6 100.31 100.71 103 10211:50:00 AM 105.0 248 248 1 1 4 6 105.62 104.29 103 10211:55:00 AM 110.0 248 248 1 1 4 6 110.55 109.77 103 10212:00:00 PM 115.0 248 248 1 1 4 6 115.64 114.53 103 10212:05:00 PM 120.0 120.725 119.797

Average 120.0 248.5 248.5 99.29166667 98.58333

Volume 120.725 119.797 

dscm 0.11 0.11 

Trap/ Probe Temp

15.0/000 10.0/0.000 

Leak Check Train "A" Unspiked

Rotameter Setting (LPM) Meter Vacuum ("Hg) Meter Reading (liters) Meter Temp (*F)

Pre Test Post Test 
BT Environmental Consulting

30B Run Sheet

Project No.: 10-286-D Probe # HG2 Pollutant Hg Points/Port 1Company Guardian FiberglassDGM # 1 L/min. Method 30B Total Points 2

Location Mineral Wells, MS Rate (L/m) Run # 2 Time/pt (min) 5.0

Source Furnace Stack Delta ∆H@ Date 22-Sep-10 Time/reading 5.0Operator Pineda Bws (%) # of Ports 2 Total Run 120.0

Filter Number Condensate Volume Cp Ps (in Hg) 29.88Barometric 29.89 Silica Gel Weight Gain DGM Y 0.991, 0.989 Pm (in Hg) 29.89 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) O2 (%) Ref Press 29.92Stack Dia (ft) 2.42 An (ft^2) 4.58800 CO2 (%) Md 28.00 Stack Area (sf) 4.59

Est.DH(in H2O) Ms 28.00 Act. Flow (cfm)

Preliminary dP (in H20) Total Vol.(cf) Wet Ref Flow (cfm)Preliminary Ts (oF) Est. Us (ft/s) Dry Ref Flow (cfm) 

Preliminary Tm (oF) Theor Dn (in)

Clock Time Sample Time Stack Temp

A B A B A B AB A B 

2:05:00 PM 0.0 249 249 1 1 6 7 0.00 0 106 1052:10:00 PM 5.0 252 252 1 1 5 8 4.88 4.78 107 1052:15:00 PM 10.0 250 250 1 1 5 8 9.89 9.8 107 1062:20:00 PM 15.0 247 247 1 1 5 8 14.79 14.89 108 1072:25:00 PM 20.0 248 248 1 1 5 8 19.04 19.88 108 1072:30:00 PM 25.0 249 249 1 1 5 8 25.13 25.44 108 1072:35:00 PM 30.0 249 249 1 1 5 8 30.14 30.22 108 1072:40:00 PM 35.0 248 248 1 1 5 8 35.35 34.76 109 1082:45:00 PM 40.0 249 249 1 1 5 8 40.25 40.13 109 1092:50:00 PM 45.0 248 248 1 1 5 8 45.29 44.99 109 1092:55:00 PM 50.0 249 249 1 1 5 8 50.03 50.01 110 1103:00:00 PM 55.0 250 250 1 1 5 8 55.41 55.22 110 1103:05:00 PM 60.0 250 250 1 1 5 8 60.22 60.3 110 1103:10:00 PM 65.0 249 249 1 1 5 8 65.42 64.93 111 1103:15:00 PM 70.0 249 249 1 1 5 8 69.68 69.81 111 1113:20:00 PM 75.0 248 248 1 1 5 8 75.05 75.22 112 1113:25:00 PM 80.0 248 248 1 1 5 8 80.15 80.29 112 1113:30:00 PM 85.0 249 249 1 1 5 8 84.89 85.14 113 1113:35:00 PM 90.0 248 248 1 1 5 8 90.00 89.74 111 1113:40:00 PM 95.0 248 248 1 1 5 8 95.22 94.66 111 1113:45:00 PM 100.0 248 248 1 1 5 8 11.02 100.56 112 1113:50:00 PM 105.0 249 249 1 1 5 8 106.08 105.74 112 1113:55:00 PM 110.0 248 248 1 1 5 8 110.99 110.39 112 1114:00:00 PM 115.0 248 248 1 1 5 8 115.780 115.5 112 1114:05:00 PM 120.0 120.897 120.332

Average 120.0 248.8 248.8 109.9166667 109.17

Volume 120.897 120.332 

dscm 0.11 0.11 

Leak Check Train "A" Unspiked

Rotameter Setting (LPM) Meter Vacuum ("Hg) Meter Reading (liters) Meter Temp (*F)

Pre Test Post Test 

15.0/0.000 10.0/0.000 

Trap/ Probe Temp
BT Environmental Consulting

30B Run Sheet

Project No.: 10-286-D Probe # HG2 Pollutant Hg Points/PortCompany Guardian FiberglassDGM # 1 L/min. Method 30B Total Points 0

Location Mineral Wells, MS Rate (L/m) Run # 3 Time/pt (min) N/A

Source Furnace Stack Delta ∆H@ Date 23-Sep-10 Time/readingOperator Pineda Bws (%) # of Ports 3 Total Run 120.0

Filter Number Condensate Volume Cp Ps (in Hg) 10.0/0.000

Barometric 29.91 Silica Gel Weight Gain DGM Y 0.991, 0.989 Pm (in Hg) 29.91 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) O2 (%) Ref Press 29.92Stack Dia (ft) 2.42 An (ft^2) 4.58800 CO2 (%) Md 28.00 Stack Area (sf) 4.59

Est.DH(in H2O) Ms 28.00 Act. Flow (cfm)

Preliminary dP (in H20) Total Vol.(cf) 0.0 Wet Ref Flow (cfm)

Preliminary Ts (oF) Est. Us (ft/s) Dry Ref Flow (cfm) Preliminary Tm (oF) Theor Dn (in)

Clock Time Sample Time Stack Temp

A B A B A B AB A B 

8:20:00 AM 0.0 250 250 1 1 4 9 0.00 0 93 928:25:00 AM 5.0 248 248 1 1 4 8 4.96 4.98 93 938:30:00 AM 10.0 248 248 1 1 4 8 10.08 10.21 94 938:35:00 AM 15.0 248 248 1 1 4 8 14.89 14.79 94 938:40:00 AM 20.0 248 248 1 1 4 8 20.84 19.25 94 948:45:00 AM 25.0 248 248 1 1 4 8 25.10 24.89 94 948:50:00 AM 30.0 248 248 1 1 4 8 30.22 30.23 95 948:55:00 AM 35.0 248 248 1 1 4 8 35.88 35.55 95 959:00:00 AM 40.0 248 248 1 1 4 8 41.02 40.47 95 959:05:00 AM 45.0 248 248 1 1 4 8 45.89 45.35 95 959:10:00 AM 50.0 247 247 1 1 4 8 50.15 50.17 95 969:15:00 AM 55.0 248 248 1 1 4 8 55.37 56.21 96 969:20:00 AM 60.0 248 248 1 1 4 8 60.21 61.18 96 969:25:00 AM 65.0 248 248 1 1 4 8 65.14 66.29 96 969:30:00 AM 70.0 248 248 1 1 4 8 70.19 70.84 96 969:35:00 AM 75.0 248 248 1 1 4 8 75.81 75.84 96 969:40:00 AM 80.0 248 248 1 1 4 8 80.13 80.71 96 969:45:00 AM 85.0 248 248 1 1 4 8 84.88 85.69 96 969:50:00 AM 90.0 248 248 1 1 4 8 89.96 90.51 96 969:55:00 AM 95.0 248 248 1 1 4 8 95.12 95.88 96 97

10:00:00 AM 100.0 248 248 1 1 4 8 100.25 100.23 96 9710:05:00 AM 105.0 248 248 1 1 4 8 105.17 105.66 97 9710:10:00 AM 110.0 248 248 1 1 4 8 110.83 110.91 97 9710:15:00 AM 115.0 248 248 1 1 4 8 115.41 115.78 97 9710:20:00 AM 120.0 120.837 120.221

Average 120.0 248.0 248.0 95.33333333 95.29

Volume 120.837 120.221 

dscm 0.11 0.11 

Trap/ Probe Temp

15.0/0.000 10.0/0.000 

Leak Check Train "A" Unspiked

Rotameter Setting (LPM) Meter Vacuum ("Hg) Meter Reading (liters) Meter Temp (*F)

Pre Test Post Test 
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 49-6-3 Pollutant Cr6 Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-1 Method 61 Total Points 12

Location Mineral Wells, MSRate (cfm) 0.617 Run # 1 Time/pt (min) 20.0

Source Furnace Stack Delta ∆H@ 1.5 Date 22-Sep-10 Time/reading 5.0

Operator Maxwell Bws (%) 3.50 # of Ports 2 Total Run 240.0

Filter Number Condensate Volume 79 Cp 0.809 Ps (in Hg) 29.87

Barometric 29.88 Silica Gel Weight Gain 35.2 DGM Y 0.99 Pm (in Hg) 30.10 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.308 O2 (%) 20.7 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00052 CO2 (%) 0.4 Md 28.89 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.51 Act. Flow (cfm) 6,786 Must delete extra zeros in the Velocity column

Vmnstd 147.47 Preliminary dP (in H20) 0.36 Total Vol.(cf) 148.1 Wet Ref Flow (cfm) 5,753

Moisture % 3.52 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.4 Dry Ref Flow (cfm) 5,551

Preliminary Tm (oF) 85 Theor Dn (in) 0.2722 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 5.0 14:05 581.19 0.20 162.00 107.00 107.00 1.30 1.50 117.00 120.00 69.00 3.00

6 5.0 10.0 14:10 584.59 0.20 162.00 107.00 107.00 1.30 1.50 117.00 120.00 60.00 3.00

6 10.0 15.0 14:15 588.70 0.20 162.00 110.00 107.00 1.30 1.50 117.00 120.00 60.00 3.00

6 15.0 20.0 14:20 591.60 0.20 162.00 110.00 108.00 1.30 1.50 117.00 120.00 60.00 3.00

5 20.0 25.0 14:25 595.50 0.20 162.00 110.00 108.00 1.30 1.50 117.00 120.00 60.00 3.00

5 25.0 30.0 14:30 598.22 0.20 163.00 111.00 110.00 1.30 1.50 117.00 120.00 61.00 3.00

5 30.0 35.0 14:35 601.90 0.20 163.00 114.00 110.00 1.30 1.50 117.00 120.00 61.00 3.00

5 35.0 40.0 14:40 604.61 0.20 163.00 115.00 111.00 1.30 1.50 117.00 120.00 63.00 3.00

4 40.0 45.0 14:45 608.41 0.16 164.00 115.00 111.00 1.04 1.20 118.00 115.00 60.00 3.00

4 45.0 50.0 14:50 612.30 0.16 164.00 116.00 111.00 1.04 1.20 118.00 115.00 61.00 3.00

4 50.0 55.0 14:55 615.50 0.16 164.00 116.00 112.00 1.04 1.20 118.00 115.00 61.00 3.00

4 55.0 60.0 15:00 618.35 0.16 164.00 117.00 112.00 1.04 1.20 118.00 115.00 61.00 3.00

3 60.0 65.0 15:05 622.62 0.17 163.00 117.00 113.00 1.10 1.25 118.00 115.00 61.00 3.00

3 65.0 70.0 15:10 625.74 0.17 163.00 117.00 113.00 1.10 1.25 118.00 115.00 62.00 3.00

3 70.0 75.0 15:15 629.46 0.17 163.00 118.00 114.00 1.10 1.25 118.00 115.00 62.00 3.00

3 75.0 80.0 15:20 633.90 0.17 163.00 118.00 114.00 1.10 1.25 118.00 115.00 62.00 3.00

2 80.0 85.0 15:25 635.90 0.17 162.00 117.00 114.00 1.10 1.25 118.00 115.00 62.00 3.00

2 85.0 90.0 15:30 638.63 0.17 162.00 117.00 114.00 1.10 1.25 118.00 115.00 62.00 3.00

2 90.0 95.0 15:35 642.70 0.17 162.00 117.00 114.00 1.10 1.25 118.00 115.00 61.00 3.00

2 95.0 100.0 15:40 645.45 0.17 162.00 118.00 114.00 1.10 1.25 104.00 115.00 61.00 3.00

1 100.0 105.0 15:45 649.45 0.17 162.00 118.00 114.00 1.10 1.25 104.00 115.00 61.00 3.00

1 105.0 110.0 15:50 652.41 0.17 162.00 118.00 114.00 1.10 1.25 104.00 115.00 61.00 3.00

1 110.0 115.0 15:55 655.72 0.17 162.00 118.00 114.00 1.10 1.25 104.00 115.00 61.00 3.00

1 115.0 120.0 16:00 659.11 0.17 162.00 118.00 114.00 1.11 1.25 104.00 115.00 61.00 3.00

STOP 120.0 16:05 662.62

1 120.0 125.0 16:18 662.62 0.20 163.00 114.00 114.00 1.30 1.50 103.00 123.00 61.00 3.00

1 125.0 130.0 16:23 665.32 0.20 163.00 117.00 114.00 1.30 1.50 103.00 120.00 61.00 3.00

1 130.0 135.0 16:28 668.40 0.20 163.00 117.00 114.00 1.30 1.50 103.00 120.00 61.00 3.00

1 135.0 140.0 16:33 673.70 0.20 163.00 117.00 114.00 1.30 1.50 103.00 120.00 61.00 3.00

2 140.0 145.0 16:38 676.74 0.21 162.00 117.00 114.00 1.36 1.55 103.00 121.00 62.00 3.00

2 145.0 150.0 16:43 680.96 0.21 162.00 117.00 114.00 1.36 1.55 103.00 121.00 62.00 3.00

2 150.0 155.0 16:48 684.39 0.21 162.00 117.00 114.00 1.36 1.55 103.00 121.00 62.00 3.00

2 155.0 160.0 16:53 687.35 0.21 162.00 117.00 114.00 1.36 1.55 101.00 121.00 62.00 3.00

3 160.0 165.0 16:58 691.31 0.20 162.00 118.00 114.00 1.30 1.50 101.00 121.00 61.00 3.00

3 165.0 170.0 17:03 695.26 0.20 162.00 118.00 114.00 1.30 1.50 101.00 121.00 61.00 3.00

3 170.0 175.0 17:08 698.21 0.20 162.00 118.00 114.00 1.30 1.50 101.00 121.00 61.00 3.00

3 175.0 180.0 17:13 701.80 0.20 162.00 118.00 114.00 1.30 1.50 101.00 120.00 61.00 3.00

4 180.0 185.0 17:18 705.50 0.14 161.00 116.00 114.00 0.91 1.05 101.00 120.00 61.00 3.00

4 185.0 190.0 17:23 709.10 0.14 161.00 116.00 113.00 0.91 1.05 101.00 120.00 61.00 3.00

4 190.0 195.0 17:28 712.06 0.14 161.00 116.00 113.00 0.91 1.05 101.00 120.00 61.00 3.00

4 195.0 200.0 17:33 715.00 0.14 161.00 116.00 113.00 0.91 1.05 101.00 120.00 61.00 3.00

5 200.0 205.0 17:38 718.62 0.14 159.00 116.00 113.00 0.91 1.05 101.00 120.00 61.00 3.00

5 205.0 210.0 17:43 723.14 0.14 159.00 116.00 113.00 0.91 1.05 101.00 120.00 61.00 3.00

5 210.0 215.0 17:48 725.06 0.14 159.00 116.00 114.00 0.91 1.05 101.00 120.00 61.00 3.00

5 215.0 220.0 17:53 728.33 0.14 159.00 116.00 114.00 0.91 1.05 101.00 120.00 61.00 3.00

6 220.0 225.0 17:58 730.61 0.14 158.00 116.00 114.00 0.91 1.05 101.00 120.00 62.00 3.00

6 225.0 230.0 18:03 734.21 0.14 158.00 116.00 114.00 0.91 1.05 101.00 120.00 63.00 3.00

6 230.0 235.0 18:08 737.64 0.14 158.00 116.00 114.00 0.91 1.05 101.00 120.00 64.00 3.00

6 235.0 240.0 18:13 740.72 0.14 158.00 116.00 114.00

STOP 240.0 245.0 18:18 743.48

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 162.30 0.18 161.7 115.8 112.7 1.14 1.31 108 119 61.4255319 3

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 49-6-3 Pollutant Cr6 Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-1 Method 61 Total Points 12

Location Mineral Wells, MSRate (cfm) 0.617 Run # 2 Time/pt (min) 20.0

Source Furnace Stack Delta ∆H@ 1.5 Date 23-Sep-10 Time/reading 5.0

Operator Maxwell Bws (%) 3.3 # of Ports 2 Total Run 240.0

Filter Number Condensate Volume 79.6 Cp 0.809 Ps (in Hg) 29.90

Barometric 29.91 Silica Gel Weight Gain 29.8 DGM Y 0.99 Pm (in Hg) 30.13 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.308 O2 (%) 20.8 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00052 CO2 (%) 0.2 Md 28.86 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.50 Act. Flow (cfm) 6,751 Must delete extra zeros in the Velocity column

Vmnstd 149.32 Preliminary dP (in H20) 0.36 Total Vol.(cf) 148.1 Wet Ref Flow (cfm) 5,810

Moisture % 3.33 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.4 Dry Ref Flow (cfm) 5,617

Preliminary Tm (oF) 85 Theor Dn (in) 0.2720 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 5.0 8:20 744.96 0.18 143.00 91.00 92.00 1.16 1.35 95.00 95.00 69.00 3.00

6 5.0 10.0 8:25 750.22 0.18 143.00 91.00 92.00 1.16 1.35 95.00 95.00 60.00 3.00

6 10.0 15.0 8:35 753.60 0.18 143.00 92.00 92.00 1.16 1.35 95.00 95.00 60.00 3.00

6 15.0 20.0 8:40 757.24 0.18 143.00 94.00 93.00 1.16 1.35 95.00 95.00 61.00 3.00

5 20.0 25.0 8:45 761.32 0.18 144.00 97.00 93.00 1.16 1.35 95.00 95.00 61.00 3.00

5 25.0 30.0 8:50 764.02 0.18 144.00 97.00 93.00 1.16 1.35 99.00 99.00 61.00 3.00

5 30.0 35.0 8:55 768.23 0.18 144.00 98.00 94.00 1.16 1.35 90.00 90.00 61.00 3.00

5 35.0 40.0 9:00 770.70 0.18 144.00 99.00 94.00 1.16 1.35 90.00 90.00 61.00 3.00

4 40.0 45.0 9:05 774.20 0.16 148.00 99.00 95.00 1.03 1.20 90.00 90.00 61.00 3.00

4 45.0 50.0 9:10 778.30 0.16 148.00 100.00 95.00 1.03 1.20 90.00 90.00 62.00 3.00

4 50.0 55.0 9:15 780.65 0.16 148.00 100.00 96.00 1.03 1.20 90.00 90.00 62.00 3.00

4 55.0 60.0 9:20 784.82 0.16 148.00 101.00 96.00 1.03 1.20 90.00 90.00 62.00 3.00

3 60.0 65.0 9:25 788.10 0.22 153.00 102.00 97.00 1.42 1.65 91.00 91.00 62.00 3.00

3 65.0 70.0 9:30 791.66 0.22 153.00 102.00 97.00 1.42 1.65 91.00 91.00 61.00 3.00

3 70.0 75.0 9:35 795.50 0.22 153.00 102.00 98.00 1.42 1.65 91.00 91.00 61.00 3.00

3 75.0 80.0 9:40 798.69 0.22 153.00 103.00 98.00 1.42 1.65 91.00 92.00 62.00 3.00

2 80.0 85.0 9:45 802.72 0.22 152.00 103.00 98.00 1.42 1.65 92.00 92.00 62.00 3.00

2 85.0 90.0 9:50 807.06 0.22 152.00 105.00 98.00 1.42 1.65 92.00 92.00 62.00 3.00

2 90.0 95.0 9:55 811.30 0.22 152.00 104.00 98.00 1.42 1.65 92.00 91.00 61.00 3.00

2 95.0 100.0 10:00 815.30 0.22 152.00 104.00 98.00 1.42 1.65 91.00 91.00 61.00 3.00

1 100.0 105.0 10:05 818.40 0.20 155.00 104.00 98.00 1.29 1.50 91.00 91.00 61.00 3.00

1 105.0 110.0 10:10 821.64 0.20 155.00 104.00 98.00 1.29 1.50 91.00 91.00 61.00 3.00

1 110.0 115.0 10:15 824.80 0.20 155.00 105.00 99.00 1.29 1.50 91.00 91.00 62.00 3.00

1 115.0 120.0 10:20 828.64 0.20 155.00 105.00 99.00 1.29 1.50 91.00 91.00 62.00 3.00

STOP 120.0 10:25 831.92

1 120.0 125.0 10:30 831.92 0.14 152.00 102.00 100.00 0.91 1.05 91.00 91.00 68.00 3.00

1 125.0 130.0 10:35 835.51 0.14 152.00 103.00 101.00 0.91 1.05 91.00 91.00 62.00 3.00

1 130.0 135.0 10:40 838.45 0.14 152.00 103.00 101.00 0.91 1.05 91.00 91.00 62.00 3.00

1 135.0 140.0 10:45 841.31 0.14 152.00 104.00 101.00 0.91 1.05 91.00 91.00 62.00 3.00

2 140.0 145.0 10:50 843.64 0.14 152.00 105.00 101.00 0.91 1.05 91.00 91.00 62.00 3.00

2 145.0 150.0 10:55 848.30 0.14 152.00 106.00 102.00 0.91 1.05 91.00 91.00 62.00 3.00

2 150.0 155.0 11:00 851.32 0.14 152.00 106.00 102.00 0.91 1.05 91.00 91.00 62.00 3.00

2 155.0 160.0 11:05 854.20 0.14 152.00 106.00 102.00 0.91 1.05 91.00 91.00 62.00 3.00

3 160.0 165.0 11:10 857.50 0.15 157.00 106.00 102.00 0.97 1.10 91.00 91.00 62.00 3.00

3 165.0 170.0 11:15 859.70 0.15 157.00 106.00 103.00 0.97 1.10 91.00 91.00 62.00 3.00

3 170.0 175.0 11:20 863.21 0.15 157.00 107.00 103.00 0.97 1.10 91.00 91.00 62.00 3.00

3 175.0 180.0 11:25 866.50 0.15 157.00 108.00 104.00 0.97 1.10 91.00 91.00 62.00 3.00

4 180.0 185.0 11:30 869.90 0.16 159.00 109.00 104.00 1.03 1.15 91.00 91.00 62.00 3.00

4 185.0 190.0 11:35 874.00 0.16 159.00 110.00 105.00 1.03 1.15 91.00 91.00 63.00 3.00

4 190.0 195.0 11:40 876.91 0.16 159.00 111.00 105.00 1.03 1.15 93.00 93.00 63.00 3.00

4 195.0 200.0 11:45 879.24 0.16 159.00 111.00 105.00 1.03 1.15 93.00 93.00 61.00 3.00

5 200.0 205.0 11:50 883.60 0.18 161.00 111.00 105.00 1.16 1.35 93.00 93.00 61.00 3.00

5 205.0 210.0 11:55 888.10 0.18 161.00 111.00 105.00 1.16 1.35 93.00 93.00 61.00 3.00

5 210.0 215.0 12:00 889.58 0.18 161.00 112.00 107.00 1.16 1.35 93.00 93.00 61.00 3.00

5 215.0 220.0 12:05 892.59 0.18 161.00 112.00 107.00 1.16 1.35 93.00 93.00 61.00 3.00

6 220.0 225.0 12:10 895.64 0.18 161.00 112.00 107.00 1.16 1.35 93.00 93.00 61.00 3.00

6 225.0 230.0 12:15 898.24 0.18 161.00 113.00 108.00 1.16 1.35 93.00 93.00 62.00 3.00

6 230.0 235.0 12:20 901.64 0.18 161.00 113.00 108.00 1.16 1.35 93.00 93.00 62.00 3.00

6 235.0 240.0 12:25 903.81 0.18 161.00 114.00 108.00 1.35 93.00 93.00 62.00 3.00

STOP 240.0 245.0 12:30 905.65

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 160.69 0.18 153.1 104.2 99.9 1.14 1.31 91.9 91.9 61.9 3

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 49-6-3 Pollutant Cr6 Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-1 Method 61 Total Points 12

Location Mineral Wells, MSRate (cfm) 0.617 Run # 3 Time/pt (min) 20.0

Source Furnace Stack Delta ∆H@ 1.5 Date 23-Sep-10 Time/reading 5.0

Operator Maxwell Bws (%) 3.7 # of Ports 2 Total Run 240.0

Filter Number Condensate Volume 68.9 Cp 0.809 Ps (in Hg) 29.90

Barometric 29.91 Silica Gel Weight Gain 48.4 DGM Y 0.99 Pm (in Hg) 30.13 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.308 O2 (%) 20.8 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00052 CO2 (%) 0.2 Md 28.86 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.47 Act. Flow (cfm) 6,617 Must delete extra zeros in the Velocity column

Vmnstd 144.66 Preliminary dP (in H20) 0.36 Total Vol.(cf) 148.1 Wet Ref Flow (cfm) 5,609

Moisture % 3.68 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.4 Dry Ref Flow (cfm) 5,404

Preliminary Tm (oF) 85 Theor Dn (in) 0.2724 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 5.0 13:15 906.72 0.19 156.00 107.00 108.00 1.23 1.40 110.00 111.00 69.00 5.00

6 5.0 10.0 13:20 909.87 0.19 156.00 107.00 108.00 1.23 1.40 110.00 111.00 60.00 5.00

6 10.0 15.0 13:25 912.47 0.19 156.00 108.00 109.00 1.23 1.40 110.00 111.00 60.00 5.00

6 15.0 20.0 13:30 917.64 0.19 156.00 109.00 109.00 1.23 1.40 110.00 111.00 60.00 5.00

5 20.0 25.0 13:35 920.83 0.19 163.00 113.00 109.00 1.23 1.40 110.00 111.00 60.00 5.00

5 25.0 30.0 13:40 924.22 0.19 163.00 114.00 110.00 1.23 1.40 110.00 112.00 60.00 5.00

5 30.0 35.0 13:45 927.43 0.19 163.00 114.00 110.00 1.23 1.40 110.00 111.00 61.00 5.00

5 35.0 40.0 13:50 931.60 0.19 163.00 115.00 110.00 1.23 1.40 111.00 111.00 61.00 5.00

4 40.0 45.0 13:55 934.72 0.16 164.00 115.00 110.00 1.04 1.20 116.00 111.00 61.00 5.00

4 45.0 50.0 14:00 937.62 0.16 164.00 116.00 112.00 1.04 1.20 116.00 112.00 61.00 5.00

4 50.0 55.0 14:05 941.70 0.16 164.00 116.00 112.00 1.04 1.20 116.00 112.00 61.00 5.00

4 55.0 60.0 14:10 944.92 0.16 164.00 117.00 113.00 1.04 1.20 114.00 112.00 61.00 5.00

3 60.0 65.0 14:15 948.09 0.14 162.00 117.00 113.00 0.91 1.05 114.00 112.00 61.00 5.00

3 65.0 70.0 14:20 951.66 0.14 162.00 117.00 114.00 0.91 1.05 114.00 112.00 62.00 5.00

3 70.0 75.0 14:25 954.92 0.14 162.00 117.00 114.00 0.91 1.05 114.00 112.00 62.00 5.00

3 75.0 80.0 14:30 958.74 0.14 162.00 117.00 114.00 0.91 1.05 114.00 112.00 63.00 5.00

2 80.0 85.0 14:35 961.40 0.16 163.00 117.00 114.00 1.04 1.20 114.00 112.00 60.00 5.00

2 85.0 90.0 14:40 964.76 0.16 163.00 117.00 114.00 1.04 1.20 114.00 112.00 60.00 5.00

2 90.0 95.0 14:45 968.11 0.16 163.00 117.00 114.00 1.04 1.20 114.00 112.00 60.00 5.00

2 95.0 100.0 14:50 971.55 0.16 163.00 117.00 114.00 1.04 1.20 114.00 111.00 60.00 5.00

1 100.0 105.0 14:55 974.32 0.14 162.00 117.00 114.00 0.91 1.05 114.00 111.00 61.00 5.00

1 105.0 110.0 15:00 977.40 0.14 162.00 118.00 114.00 0.91 1.05 114.00 111.00 61.00 5.00

1 110.0 115.0 15:05 980.01 0.14 162.00 118.00 114.00 0.91 1.05 114.00 111.00 61.00 5.00

1 115.0 120.0 15:10 982.24 0.14 162.00 118.00 114.00 0.91 1.05 114.00 111.00 61.00 5.00

STOP 120.0 15:15 986.77

1 120.0 125.0 15:20 986.77 0.15 163.00 116.00 115.00 0.97 1.10 114.00 111.00 68.00 5.00

1 125.0 130.0 15:25 988.91 0.15 163.00 116.00 115.00 0.97 1.10 114.00 111.00 68.00 5.00

1 130.0 135.0 15:30 992.60 0.15 163.00 116.00 115.00 0.97 1.10 114.00 111.00 60.00 5.00

1 135.0 140.0 15:35 995.14 0.15 163.00 117.00 115.00 0.97 1.10 114.00 111.00 60.00 5.00

2 140.0 145.0 15:40 998.90 0.19 165.00 118.00 115.00 1.23 1.40 114.00 111.00 60.00 5.00

2 145.0 150.0 15:45 1001.43 0.19 165.00 118.00 115.00 1.23 1.40 114.00 111.00 60.00 5.00

2 150.0 155.0 15:50 1006.02 0.19 165.00 118.00 115.00 1.23 1.40 114.00 111.00 59.00 5.00

2 155.0 160.0 15:55 1008.40 0.19 165.00 118.00 115.00 1.23 1.40 114.00 111.00 59.00 5.00

3 160.0 165.0 16:00 1009.40 0.19 164.00 118.00 115.00 1.23 1.40 114.00 111.00 59.00 5.00

3 165.0 170.0 16:05 1011.32 0.19 164.00 118.00 115.00 1.23 1.40 114.00 111.00 59.00 5.00

3 170.0 175.0 16:10 1016.24 0.19 164.00 118.00 115.00 1.23 1.40 114.00 111.00 59.00 5.00

3 175.0 180.0 16:15 1019.48 0.19 164.00 118.00 115.00 1.23 1.40 114.00 111.00 59.00 5.00

4 180.0 185.0 16:20 1026.36 0.18 164.00 118.00 114.00 1.17 1.35 114.00 111.00 59.00 5.00

4 185.0 190.0 16:25 1030.14 0.18 164.00 117.00 114.00 1.17 1.35 114.00 111.00 59.00 5.00

4 190.0 195.0 16:30 1032.95 0.18 164.00 116.00 114.00 1.17 1.35 114.00 111.00 59.00 5.00

4 195.0 200.0 16:35 1036.14 0.18 164.00 116.00 114.00 1.17 1.35 114.00 111.00 59.00 5.00

5 200.0 205.0 16:40 1040.31 0.15 161.00 116.00 114.00 0.97 1.10 114.00 111.00 59.00 5.00

5 205.0 210.0 16:45 1044.21 0.15 161.00 116.00 114.00 0.97 1.10 114.00 111.00 60.00 5.00

5 210.0 215.0 16:50 1046.72 0.15 161.00 115.00 114.00 0.97 1.10 114.00 111.00 60.00 5.00

5 215.0 220.0 16:55 1048.61 0.15 161.00 115.00 114.00 0.97 1.10 114.00 111.00 61.00 5.00

6 220.0 225.0 17:00 1051.28 0.15 161.00 115.00 114.00 0.97 1.10 114.00 111.00 61.00 5.00

6 225.0 230.0 17:05 1055.61 0.15 161.00 115.00 114.00 0.97 1.10 114.00 111.00 61.00 5.00

6 230.0 235.0 17:10 1059.01 0.15 161.00 115.00 114.00 0.97 1.10 114.00 111.00 61.00 5.00

6 235.0 240.0 17:15 1061.26 0.15 161.00 115.00 114.00 1.10 114.00 111.00 61.00 5.00

STOP 240.0 245.0 17:20 1065.84

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 159.12 0.17 162.3 115.8 113.2 1.08 1.23 113.5 111.2 60.7708333 5.0

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 50-3-3 Pollutant HCl Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # 0.697 Method M26A Total Points 12

Location Mineral Wells, MSRate (cfm) 1 Run # 1 Time/pt (min) 5.0

Source ectric Melt FurnaDelta ∆H@ 1.5 Date 22-Sep-10 Time/reading 5.0

Operator McDonald Bws (%) 3.79 # of Ports 2 Total Run 60.0

Filter Number Condensate Volume 25 Cp 0.809 Ps (in Hg) 29.88

Barometric 29.89 Silica Gel Weight Gain 10 DGM Y 1.009 Pm (in Hg) 30.11 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.333 O2 (%) 20.7 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00060 CO2 (%) 0.4 Md 28.89 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.48 Act. Flow (cfm) 6,598 Must delete extra zeros in the Velocity column

Vmnstd 41.63 Preliminary dP (in H20) 0.36 Total Vol.(cf) 60.0 Wet Ref Flow (cfm) 5,591

Moisture % 3.81 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.4 Dry Ref Flow (cfm) 5,379

Preliminary Tm (oF) 85 Theor Dn (in) 0.2726 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 5.0 15:25 645.14 0.16 161.00 108.00 109.00 1.40 1.50 252.00 251.00 66.00 3.00

5 5.0 10.0 15:30 648.75 0.20 162.00 109.00 108.00 1.75 1.90 251.00 250.00 53.00 3.00

4 10.0 15.0 15:35 653.10 0.20 162.00 109.00 109.00 1.75 1.90 250.00 251.00 52.00 3.00

3 15.0 20.0 15:40 656.86 0.16 164.00 110.00 109.00 1.40 1.50 252.00 253.00 54.00 3.00

2 20.0 25.0 15:45 660.53 0.14 163.00 111.00 109.00 1.23 1.30 251.00 252.00 55.00 3.00

1 25.0 30.0 15:50 663.87 0.14 163.00 112.00 110.00 1.23 1.30 250.00 252.00 57.00 3.00

STOP 30.0 15:55 667.36

6 30.0 35.0 16:18 667.36 0.19 161.00 110.00 110.00 1.66 1.80 251.00 250.00 67.00 3.00

5 35.0 40.0 16:23 671.28 0.18 162.00 111.00 110.00 1.58 1.70 253.00 253.00 60.00 3.00

4 40.0 45.0 16:28 675.31 0.16 161.00 111.00 110.00 1.40 1.50 253.00 252.00 57.00 3.00

3 45.0 50.0 16:33 678.84 0.16 161.00 112.00 110.00 1.40 1.50 252.00 252.00 58.00 3.00

2 50.0 55.0 16:38 682.64 0.15 163.00 113.00 110.00 1.31 1.40 251.00 251.00 59.00 3.00

1 55.0 60.0 16:48 686.22 0.14 162.00 113.00 110.00 1.23 1.30 251.00 252.00 62.00 3.00

60.0 16:48 689.75

65.0 70.0

70.0 75.0

75.0 80.0

80.0 85.0

85.0 90.0

90.0 95.0

95.0 100.0

100.0 105.0

105.0 110.0

110.0 115.0

115.0 120.0

120.0 125.0

125.0 130.0

130.0 135.0

135.0 140.0

140.0 145.0

145.0 150.0

150.0 155.0

155.0 160.0

160.0 165.0

165.0 170.0

170.0 175.0

175.0 180.0

180.0 185.0

185.0 190.0

190.0 195.0

195.0 200.0

200.0 205.0

205.0 210.0

210.0 215.0

215.0 220.0

220.0 225.0

225.0 230.0

230.0 235.0

235.0 240.0

240.0 245.0

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 44.61 0.17 162.1 110.8 109.5 1.45 1.55 251 252 58.3333333 3

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 50-3-3 Pollutant HCl Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-2 Method M26A Total Points 12

Location Mineral Wells, MSRate (cfm) 1 Run # 2 Time/pt (min) 5.0

Source ectric Melt FurnaDelta ∆H@ 1.5 Date 23-Sep-10 Time/reading 5.0

Operator McDonald Bws (%) 4.2 # of Ports 2 Total Run 60.0

Filter Number Condensate Volume 30.5 Cp 0.809 Ps (in Hg) 29.90

Barometric 29.91 Silica Gel Weight Gain 10.5 DGM Y 1.009 Pm (in Hg) 30.13 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.333 O2 (%) 20.8 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00060 CO2 (%) 0.2 Md 28.86 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.41 Act. Flow (cfm) 6,827 Must delete extra zeros in the Velocity column

Vmnstd 43.72 Preliminary dP (in H20) 0.36 Total Vol.(cf) 60.0 Wet Ref Flow (cfm) 5,887

Moisture % 4.23 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.4 Dry Ref Flow (cfm) 5,639

Preliminary Tm (oF) 85 Theor Dn (in) 0.2731 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 5.0 9:40 690.18 0.18 149.00 91.00 92.00 1.55 1.70 251.00 249.00 58.00 3.00

5 5.0 10.0 9:45 693.94 0.19 150.00 92.00 92.00 1.64 1.80 250.00 250.00 58.00 3.00

4 10.0 15.0 9:50 697.82 0.17 150.00 94.00 93.00 1.46 1.60 250.00 250.00 58.00 3.00

3 15.0 20.0 9:55 701.72 0.16 152.00 96.00 93.00 1.38 1.50 252.00 253.00 59.00 3.00

2 20.0 25.0 10:00 705.17 0.16 152.00 97.00 93.00 1.38 1.50 251.00 252.00 59.00 3.00

1 25.0 30.0 10:05 708.84 0.14 151.00 97.00 93.00 1.21 1.30 251.00 253.00 60.00 3.00

STOP 30.0 10:10 712.22

6 30.0 35.0 10:30 712.22 0.17 152.00 96.00 95.00 1.46 1.60 252.00 251.00 59.00 3.00

5 35.0 40.0 10:35 716.04 0.17 153.00 97.00 95.00 1.46 1.60 251.00 252.00 58.00 3.00

4 40.0 45.0 10:40 719.63 0.21 154.00 97.00 95.00 1.81 2.00 250.00 251.00 60.00 3.00

3 45.0 50.0 10:45 723.97 0.20 154.00 99.00 96.00 1.72 1.90 252.00 250.00 62.00 3.00

2 50.0 55.0 10:50 728.23 0.21 153.00 101.00 96.00 1.81 2.00 251.00 251.00 59.00 3.00

1 55.0 60.0 10:55 731.94 0.19 152.00 100.00 97.00 1.64 1.80 250.00 251.00 58.00 3.00

60.0 65.0 11:00 735.78

65.0 70.0

70.0 75.0

75.0 80.0

80.0 85.0

85.0 90.0

90.0 95.0

95.0 100.0

100.0 105.0

105.0 110.0

110.0 115.0

115.0 120.0

120.0 125.0

125.0 130.0

130.0 135.0

135.0 140.0

140.0 145.0

145.0 150.0

150.0 155.0

155.0 160.0

160.0 165.0

165.0 170.0

170.0 175.0

175.0 180.0

180.0 185.0

185.0 190.0

190.0 195.0

195.0 200.0

200.0 205.0

205.0 210.0

210.0 215.0

215.0 220.0

220.0 225.0

225.0 230.0

230.0 235.0

235.0 240.0

240.0 245.0

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 45.60 0.18 151.8 96.4 94.2 1.54 1.69 250.9 251.1 59.0 3

Leak Check
BT Environmental Consulting

Isokinetic Run Sheet

Project No.: 10-3990.05 Probe # 50-3-3 Pollutant HCl Points/Port 6 Start Finish Pre Post

Company Guardian Fibergla DGM # T3-2 Method M26A Total Points 12

Location Mineral Wells, MSRate (cfm) 1 Run # 3 Time/pt (min) 5.0

Source ectric Melt FurnaDelta ∆H@ 1.5 Date 23-Sep-10 Time/reading 5.0

Operator McDonald Bws (%) 3.8 # of Ports 2 Total Run 60.0

Filter Number Condensate Volume 24.5 Cp 0.809 Ps (in Hg) 29.90

Barometric 29.91 Silica Gel Weight Gain 11.5 DGM Y 1.009 Pm (in Hg) 30.13 Ref Temp 68

Static (in H2O) -0.2 Actual Dn (in) 0.333 O2 (%) 20.8 Ref Press 29.92

Stack Dia (ft) 2.42 An (ft^2) 0.00060 CO2 (%) 0.2 Md 28.86 Stack Area (sf) 4.59

Est.DH(in H2O) 3.00 Ms 28.45 Act. Flow (cfm) 6,805 Must delete extra zeros in the Velocity column

Vmnstd 43.11 Preliminary dP (in H20) 0.36 Total Vol.(cf) 60.0 Wet Ref Flow (cfm) 5,761

Moisture % 3.78 Preliminary Ts (oF) 125 Est. Us (ft/s) 34.4 Dry Ref Flow (cfm) 5,544

Preliminary Tm (oF) 85 Theor Dn (in) 0.2725 Comments: "Data Entry Cells" 

"Calculated Cells Do Not Touch"

PT # Start Time End Time

Clock Time 

(24hr) DGM Vol. Delta P Stack Temp Meter In Meter Out

Desired Delta 

H

Actual 

Delta H

Probe Temp. 

(*F)

Filter Temp 

(*F)

Imp temp. 

(*F) Pump Vac.

6 0.0 5.0 14:35 736.10 0.19 162.00 108.00 109.00 1.66 1.80 251.00 254.00 62.00 3.00

5 5.0 10.0 14:40 740.03 0.21 162.00 109.00 109.00 1.84 2.00 250.00 253.00 53.00 3.00

4 10.0 15.0 14:45 744.20 0.21 163.00 110.00 109.00 1.84 2.00 250.00 251.00 54.00 3.00

3 15.0 20.0 14:50 748.36 0.18 164.00 111.00 109.00 1.57 1.80 252.00 251.00 55.00 3.00

2 20.0 25.0 14:55 752.39 0.17 163.00 112.00 109.00 1.49 1.60 253.00 252.00 57.00 3.00

1 25.0 30.0 15:00 756.28 0.18 163.00 112.00 109.00 1.57 1.80 251.00 251.00 58.00 3.00

STOP 30.0 15:05 760.29

6 30.0 35.0 15:24 760.29 0.17 163.00 110.00 110.00 1.49 1.60 251.00 250.00 67.00 3.00

5 35.0 40.0 15:29 764.03 0.16 164.00 110.00 110.00 1.40 1.50 250.00 249.00 58.00 3.00

4 40.0 45.0 15:34 767.74 0.16 164.00 111.00 110.00 1.40 1.50 252.00 251.00 59.00 3.00

3 45.0 50.0 15:39 771.52 0.17 163.00 112.00 111.00 1.49 1.60 252.00 252.00 61.00 3.00

2 50.0 55.0 15:44 774.71 0.15 164.00 112.00 111.00 1.31 1.40 253.00 250.00 62.00 3.00

1 55.0 60.0 15:49 778.80 0.15 163.00 112.00 111.00 1.31 1.40 253.00 251.00 64.00 3.00

60.0 65.0 15:54 782.28

65.0 70.0

70.0 75.0

75.0 80.0

80.0 85.0

85.0 90.0

90.0 95.0

95.0 100.0

100.0 105.0

105.0 110.0

110.0 115.0

115.0 120.0

120.0 125.0

125.0 130.0

130.0 135.0

135.0 140.0

140.0 145.0

145.0 150.0

150.0 155.0

155.0 160.0

160.0 165.0

165.0 170.0

170.0 175.0

175.0 180.0

180.0 185.0

185.0 190.0

190.0 195.0

195.0 200.0

200.0 205.0

205.0 210.0

210.0 215.0

215.0 220.0

220.0 225.0

225.0 230.0

230.0 235.0

235.0 240.0

240.0 245.0

245.0 250.0

250.0 255.0

255.0 260.0

260.0 265.0

265.0 270.0

270.0 275.0

275.0 280.0

280.0 285.0

285.0 290.0

290.0 295.0

295.0 300.0

300.0 305.0

305.0 310.0

310.0 315.0

315.0 320.0

320.0 325.0

325.0 330.0

330.0 335.0

335.0 340.0

340.0 345.0

345.0 350.0

350.0 355.0

355.0 360.0

360.0 365.0

365.0 370.0

370.0 375.0

375.0 380.0

380.0 385.0

385.0 390.0

390.0 395.0

395.0 400.0

400.0 405.0

405.0 410.0

410.0 415.0

415.0 420.0

420.0 425.0

425.0 430.0

430.0 435.0

435.0 440.0

440.0 445.0

445.0 450.0

450.0 455.0

455.0 460.0

460.0 465.0

465.0 470.0

470.0 475.0

475.0 480.0

480.0 485.0

485.0 490.0

490.0 495.0

495.0 500.0

500.0 505.0

505.0 510.0

510.0 515.0

515.0 520.0

520.0 525.0

525.0 530.0

530.0 535.0

535.0 540.0

540.0 545.0

545.0 550.0

550.0 555.0

555.0 560.0

560.0 565.0

565.0 570.0

570.0 575.0

575.0 580.0

580.0 585.0

585.0 590.0

590.0 595.0

Average: 46.18 0.18 163.2 110.8 109.8 1.53 1.67 251.5 251.3 59.1666667 3.0

Leak Check



































































APPENDIX D 

EQUIPMENT CALIBRATION DOCUMENTS 

































APPENDIX E 

LABORATORY ANALYTICAL REPORTS 
Acetone 

Rinse 

Volume 

(mL)

Particulate 

Weight in 

Acetone 

(mg)

Particulate 

Weight on 

Filter 

(mg)

Organic 

(mg)

Inorganic 

(mg)

Acetone 

(mg)

Filterable 

PM2.5 Catch 

Weight (mg)

O

PM2

Wei

Run 1 35 ND ND 2.7 9.1 ND 0.80 Run 2 41 ND 0.30 2 6.3 ND 0.80 Run 3 45 ND 0.50 2.3 10 ND 1.00 

Blank: 96 ND ND ND 2.30

RDL: 0.5 0.30

*Filterable PM2.5 catch weight is the sum of the detection limit for the acetone rinse (0.5 mg) plus the maximum of the de

for the filter.

Correct

OTM 27/28 PM2.5 Lab Results Blank Correction

Guardian Fiberglass

Mineral Wells, Mississippi

10-3990.05

Sampling Dates: September 21 and 22, 2010

OTM27 OTM28
Acetone 

Rinse 

Volume 

(mL)

Particulate 

Weight in 

Acetone 

Rinse (mg)

Particulate 

Weight on 

Filter (mg)

Particulate 

Weight in 

Acetone 

Rinse (mg)

Combined 

Particulate 

Weight (mg)

Run 1 90 6.5 3.5 6.5 10.0

Run 2 99 6.1 4.3 6.1 10.4

Run 3 99 3.8 1.4 3.8 5.2

Blank 96 0.00 1.10

Method 5 PM Lab Results

Corrected

Sampling Dates: September 21 and 22, 2010

10-3990.05

Mineral Wells, Mississippi

Guardian Fiberglass
Compound/Fraction

Blank 

Result

(μg)

Blank

Detection 

Limit

(μg)

Run 1 

Result

(μg)

Run 2 

Result

(μg)

Run 3 

Result

(μg)

Test Run 

Detection 

Limit

(μg)

Run 1

(μg)

Run 2

(μg)

Run 3

(μg)

Antimony ND 0.40 ND ND ND 0.80 0.80 0.80 0.80 Value reported as equal to the detection limit as per USEPA instru

Arsenic 0.92 0.40 1.00 0.83 0.81 0.80 0.80 0.80 0.80 Value reported as equal to the detection limit because the correc

Berylium ND 0.10 ND ND ND 0.20 0.20 0.20 0.20 Value reported as equal to the detection limit as per USEPA instru

Cadmium ND 0.10 0.29 0.24 ND 0.20 0.29 0.24 0.20 Value for Run 3 reported as equal to the detection limit as per US

Chromium 1.71 0.30 10.5 3.90 4.43 0.60 8.79 2.19 2.72 Values blank corrected as per Method 29

Cobalt ND 0.10 0.51 0.26 ND 0.20 0.51 0.26 0.20 Value for Run 3 reported as equal to the detection limit as per US

Lead 2.98 0.20 9.53 3.60 4.79 0.40 6.55 0.62 1.81 Values blank corrected as per Method 29

Manganese 0.89 0.75 3.6 2.9 1.5 1.5 2.71 2.01 0.61 Values blank corrected as per Method 29

Nickel 0.57 0.50 19.3 1.8 4.5 1.0 18.73 1.23 3.93 Values blank corrected as per Method 29

Selenium ND 1.0 2.5 2.6 ND 2.0 2.50 2.60 2.00 Value for Run 3 reported as equal to the detection limit as per US

Notes

Method 29 Lab Results

Guardian Fiberglass

Mineral Wells, Mississippi

10-3990.05

Sampling Dates: September 21 and 22, 2010

Corrected
Corrected

Total Volume 

(ml)

Impinger KOH 

(ml)

Hexavalent 

Chromium, 

Cr6+ [μg]

Hexavalent 

Chromium, 

Cr6+ [μg]

Run 1 670 300 2.0 1.50

Run 2 620 300 2.5 2.00

Run 3 660 300 1.0 0.50

Blank H2O 300 ND

Blank KOH 310 0.50

*The Run 1 mass was blank corrected as per Method 0061. For Runs 2 and 3, the blankcorrected result would be negative. Therefore, the run detection limit of 0.4 μg was used

Method 0061 Lab Results

Sampling Dates: September 22 and 23, 2010

10-3990.05

Mineral Wells, Mississippi

Guardian Fiberglass
Your Project #: 10-3990.05 

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Your C.O.C. #: 0698

Attention: Barry Boulianne

BT Environmental Consulting

2615 Wolcott St.

Ferndale, MI

USA 48220

Report Date: 2010/10/20

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B0D8224

Received: 2010/09/30, 12:00

Sample Matrix: Stack Sampling Train

# Samples Received: 8

Date Date Method

Analyses Quantity Extracted Analyzed Laboratory Method Reference

Organic Condensable PM (OTM28) (1 ) 4 2010/10/13 2010/10/13 BRL SOP-00120 EPA OTM 28 

Inorganic Condensable PM (OTM28) (1 ) 4 2010/10/15 2010/10/15 BRL SOP-00120 EPA OTM 28 

2.5 um Particulates on Filter (OTM-027) (2 ) 4 N/A 2010/10/13 BRL SOP-00109 EPA OTM - 027 

<2.5um Particulates in Rinse(OTM-027) (2 ) 3 2010/10/07 2010/10/13 BRL SOP-00109 EPA OTM - 027 

Particulates/Acetone Rinse (M5/315/M201) (2 ) 1 2010/10/07 2010/10/14 BRL SOP-00109 EPA 5/315 

Final Volume of Acetone Probe Rinse 4 N/A 2010/10/13 

Weight of DCM Received 4 N/A 2010/10/13 

Weight of Water from Impingers 4 N/A 2010/10/13 

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This is a non-accredited test.

(2) This test was performed in Maxxam Mississauga under Maxxam Burlington SCC Accreditation

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

LINA BARRETO, Project Manager

Email: LBarreto@maxxam.ca

Phone# (905) 817-5700

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section

5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 1 of 7
BT Environmental Consulting

Maxxam Job #: B0D8224 Client Project #: 10-3990.05

Report Date: 2010/10/20 Project name: METCO-GUARDIAN MINERAL WELLS,MS

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID H I 8 7 9 7 H I 8 7 9 9 H I 8 8 0 0

Sampling Date 2010/09/22 2010/09/21 2010/09/21

11:15 20:35 00:00

COC Number 0698 0698 0698

 U n i t s TRAIN R1-OTM28 R2-OTM28 RDL QC Batch

BLANK-OTM28

Weight g 210 190 200 0.1 2295472

DCM Weight g 210 190 240 0.1 2295471

Inorganic Condensible PM mg 2.3 9.1 6.3 0.50 2298277

Organic Condensible PM mg ND 2.7 2.0 1.0 2295467

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID H I 8 8 0 1 H I 8 8 0 3 H I 8 8 0 4

Sampling Date 2010/09/22 2010/09/22 2010/09/21

16:30 17:53 17:35

COC Number 0698

 U n i t s R3-OTM28 BLANK-OTM27 R1-OTM27 RDL QC Batch

< 2.5 Particulate Weight in Acetone Rinse mg ND 0.5 2291839

Acetone Rinse Particulate Weight in Acetone Rinse mg ND 0.5 2291838

< 2.5 Particulate Weight on Filter mg ND ND 0.30 2291837

Acetone Rinse Volume ml 96 1 2291840

Acetone Rinse Volume (2.5) ml 35 1 2291840

Weight g 180 0.1 2295472

DCM Weight g 200 0.1 2295471

Inorganic Condensible PM mg 10 0.50 2298277

Organic Condensible PM mg 2.3 1.0 2295467

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 2 of 7
BT Environmental Consulting

Maxxam Job #: B0D8224 Client Project #: 10-3990.05

Report Date: 2010/10/20 Project name: METCO-GUARDIAN MINERAL WELLS,MS

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID H I 8 8 0 5 H I 8 8 0 6

Sampling Date 2010/09/21 2010/09/22

23:41 15:25

COC Number

 U n i t s R2-OTM27 R3-OTM27 RDL QC Batch

< 2.5 Particulate Weight in Acetone Rinse mg ND ND 0.5 2291839

< 2.5 Particulate Weight on Filter mg 0.30 0.50 0.30 2291837

Acetone Rinse Volume (2.5) ml 41 45 1 2291840

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 3 of 7
BT Environmental Consulting

Maxxam Job #: B0D8224 Client Project #: 10-3990.05

Report Date: 2010/10/20 Project name: METCO-GUARDIAN MINERAL WELLS,MS

Test Summary

Maxxam ID HI8797 Collected 2010/09/22

Sample ID TRAIN BLANK-OTM28 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Organic Condensable PM (OTM28) 2295467 2010/10/13 2010/10/13 MGE

Inorganic Condensable PM (OTM28) 2298277 2010/10/15 2010/10/15 FMO

Weight of DCM Received 2295471 N/A 2010/10/13 

Weight of Water from Impingers 2295472 N/A 2010/10/13 FMO

Maxxam ID HI8799 Collected 2010/09/21

Sample ID R1-OTM28 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Organic Condensable PM (OTM28) 2295467 2010/10/13 2010/10/13 MGE

Inorganic Condensable PM (OTM28) 2298277 2010/10/15 2010/10/15 FMO

Weight of DCM Received 2295471 N/A 2010/10/13 

Weight of Water from Impingers 2295472 N/A 2010/10/13 FMO

Maxxam ID HI8800 Collected 2010/09/21

Sample ID R2-OTM28 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Organic Condensable PM (OTM28) 2295467 2010/10/13 2010/10/13 MGE

Inorganic Condensable PM (OTM28) 2298277 2010/10/15 2010/10/15 FMO

Weight of DCM Received 2295471 N/A 2010/10/13 

Weight of Water from Impingers 2295472 N/A 2010/10/13 FMO

Maxxam ID HI8801 Collected 2010/09/22

Sample ID R3-OTM28 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Organic Condensable PM (OTM28) 2295467 2010/10/13 2010/10/13 MGE

Inorganic Condensable PM (OTM28) 2298277 2010/10/15 2010/10/15 FMO

Weight of DCM Received 2295471 N/A 2010/10/13 

Weight of Water from Impingers 2295472 N/A 2010/10/13 FMO

Maxxam ID HI8803 Collected 2010/09/22

Sample ID BLANK-OTM27 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

2.5 um Particulates on Filter (OTM-027) BAL 2291837 N/A 2010/10/13 BLM

Particulates/Acetone Rinse (M5/315/M201) BAL 2291838 2010/10/07 2010/10/14 NUA

Final Volume of Acetone Probe Rinse 2291840 N/A 2010/10/13 BLM

Page 4 of 7
BT Environmental Consulting

Maxxam Job #: B0D8224 Client Project #: 10-3990.05

Report Date: 2010/10/20 Project name: METCO-GUARDIAN MINERAL WELLS,MS

Test Summary

Maxxam ID HI8804 Collected 2010/09/21

Sample ID R1-OTM27 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

2.5 um Particulates on Filter (OTM-027) BAL 2291837 N/A 2010/10/13 BLM

<2.5um Particulates in Rinse(OTM-027) BAL 2291839 2010/10/07 2010/10/13 NUA

Final Volume of Acetone Probe Rinse 2291840 N/A 2010/10/13 BLM

Maxxam ID HI8805 Collected 2010/09/21

Sample ID R2-OTM27 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

2.5 um Particulates on Filter (OTM-027) BAL 2291837 N/A 2010/10/13 BLM

<2.5um Particulates in Rinse(OTM-027) BAL 2291839 2010/10/07 2010/10/13 NUA

Final Volume of Acetone Probe Rinse 2291840 N/A 2010/10/13 BLM

Maxxam ID HI8806 Collected 2010/09/22

Sample ID R3-OTM27 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

2.5 um Particulates on Filter (OTM-027) BAL 2291837 N/A 2010/10/13 BLM

<2.5um Particulates in Rinse(OTM-027) BAL 2291839 2010/10/07 2010/10/13 NUA

Final Volume of Acetone Probe Rinse 2291840 N/A 2010/10/13 BLM

Page 5 of 7
BT Environmental Consulting

Maxxam Job #: B0D8224 Client Project #: 10-3990.05

Report Date: 2010/10/20 Project name: METCO-GUARDIAN MINERAL WELLS,MS

GENERAL COMMENTS

Sample HI8799-01: ORGANIC EXTRACTION : Yellowish white residue found in vial.

INORGANIC EXTRACTION : Whitish residue found in aluminum dish.

Sample HI8800-01: ORGANIC EXTRACTION : Yellowish white residue found in vial.

INORGANIC EXTRACTION : Whitish residue found in aluminum dish.

Sample HI8801-01: ORGANIC EXTRACTION : Yellowish white residue found in vial.

INORGANIC EXTRACTION : Whitish residue found in aluminum dish.

Results relate only to the items tested.

Page 6 of 7
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 10-3990.05

P.O. #:

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Quality Assurance Report

Maxxam Job Number: GB0D8224

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2291838 NUA Method Blank Acetone Rinse Particulate Weight in Acetone 2010/10/14 ND, RDL=0.5 mg

2291839 NUA Method Blank < 2.5 Particulate Weight in Acetone Rinse 2010/10/13 ND, RDL=0.5 mg

2295467 MGE Spiked Blank Organic Condensible PM 2010/10/13 94 % 70 - 130

Spiked Blank DUP Organic Condensible PM 2010/10/13 93 % 70 - 130

RPD Organic Condensible PM 2010/10/13 1.1 % 20

Method Blank Organic Condensible PM 2010/10/13 ND, RDL=1.0 mg

2298277 MGE Method Blank Inorganic Condensible PM 2010/10/15 ND, RDL=0.50 mg

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.

Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.

Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

Page 7 of 7
Your Project #: 10-3990.05 

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Attention: Barry Boulianne

BT Environmental Consulting

2615 Wolcott St.

Ferndale, MI

USA 48220

Report Date: 2010/10/14

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B0D8184

Received: 2010/09/30, 12:00

Sample Matrix: Stack Sampling Train

# Samples Received: 4

Date Date Method

Analyses Quantity Extracted Analyzed Laboratory Method Reference

Metals in Combined Train (6020) (1 ) 4 2010/10/13 2010/10/13 BRL SOP-00103/ BRL EPA 6020 / M29 

SOP-00102

Particulates/Acetone Rinse (M5/315/M201) (1 ) 4 2010/10/05 2010/10/08 BRL SOP-00109 EPA 5/315 

Particulates/Filter (M5/315/NJATM1/M201) (1 ) 4 N/A 2010/10/07 BRL SOP-00109 EPA 5/315/NJATM1 

Final Volume of Acetone Probe Rinse 4 N/A 2010/10/08 

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed in Maxxam Mississauga under Maxxam Burlington SCC Accreditation

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

LINA BARRETO, Project Manager

Email: LBarreto@maxxam.ca

Phone# (905) 817-5700

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section

5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 1 of 8
BT Environmental Consulting

Maxxam Job #: B0D8184 Client Project #: 10-3990.05

Report Date: 2010/10/14 Project name: METCO-GUARDIAN MINERAL WELLS,MS

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID H I 8 6 1 9 H I 8 6 2 0 H I 8 6 2 1

Sampling Date 2010/09/22 2010/09/21 2010/09/21

09:30 19:40 23:15

 U n i t s BLANK-M5/29 RUN 1-M5/29 RUN 2-M5/29 RDL QC Batch

Acetone Rinse Particulate Weight in Acetone Rinse mg ND 6.5 6.1 0.5 2288968

Front Half Particulate Weight on Filter mg 0.40 3.50 4.30 0.30 2288967

Acetone Rinse Volume ml 96 90 99 1 2291082

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID H I 8 6 2 2

Sampling Date 2010/09/22

14:35

 U n i t s RUN 3-M5/29 RDL QC Batch

Acetone Rinse Particulate Weight in Acetone Rinse mg 3.8 0.5 2288968

Front Half Particulate Weight on Filter mg 1.40 0.30 2288967

Acetone Rinse Volume ml 99 1 2291082

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 2 of 8
BT Environmental Consulting

Maxxam Job #: B0D8184 Client Project #: 10-3990.05

Report Date: 2010/10/14 Project name: METCO-GUARDIAN MINERAL WELLS,MS

ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN)

Maxxam ID H I 8 6 1 9 H I 8 6 2 0 H I 8 6 2 0 H I 8 6 2 1

Sampling Date 2010/09/22 2010/09/21 2010/09/21 2010/09/21

09:50 19:30 19:30 23:05

 U n i t s BLANK-M5/29 RDL RUN 1-M5/29 RUN RUN 2-M5/29 RDL QC Batch

1-M5/29 Lab-Dup

Total Antimony (Sb) ug ND 0.40 ND ND ND 0.80 2295780

Total Arsenic (As) ug 0.92 0.40 1.00 0.92 0.83 0.80 2295780

Total Beryllium (Be) ug ND 0.10 ND ND ND 0.20 2295780

Total Cadmium (Cd) ug ND 0.10 0.29 0.29 0.24 0.20 2295780

Total Chromium (Cr) ug 1.71 0.30 10.5 10.4 3.90 0.60 2295780

Total Cobalt (Co) ug ND 0.10 0.51 0.52 0.26 0.20 2295780

Total Lead (Pb) ug 2.98 0.20 9.53 9.44 3.60 0.40 2295780

Total Manganese (Mn) ug 0.89 0.75 3.6 3.4 2.9 1.5 2295780

Total Nickel (Ni) ug 0.57 0.50 19.3 19.0 1.8 1.0 2295780

Total Selenium (Se) ug ND 1.0 2.5 2.7 2.6 2.0 2295780

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID H I 8 6 2 2

Sampling Date 2010/09/22

14:30

 U n i t s RUN 3-M5/29 RDL QC Batch

Total Antimony (Sb) ug ND 0.80 2295780

Total Arsenic (As) ug 0.81 0.80 2295780

Total Beryllium (Be) ug ND 0.20 2295780

Total Cadmium (Cd) ug ND 0.20 2295780

Total Chromium (Cr) ug 4.43 0.60 2295780

Total Cobalt (Co) ug ND 0.20 2295780

Total Lead (Pb) ug 4.79 0.40 2295780

Total Manganese (Mn) ug 1.5 1.5 2295780

Total Nickel (Ni) ug 4.5 1.0 2295780

Total Selenium (Se) ug ND 2.0 2295780

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 3 of 8
BT Environmental Consulting

Maxxam Job #: B0D8184 Client Project #: 10-3990.05

Report Date: 2010/10/14 Project name: METCO-GUARDIAN MINERAL WELLS,MS

Test Summary

Maxxam ID HI8619 Collected 2010/09/22

Sample ID BLANK-M5/29 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals in Combined Train (6020) ICP1/MS 2295780 2010/10/13 2010/10/13 N_R

Particulates/Acetone Rinse (M5/315/M201) BAL 2288968 2010/10/05 2010/10/08 NUA

Particulates/Filter (M5/315/NJATM1/M201) BAL 2288967 N/A 2010/10/07 BLM

Final Volume of Acetone Probe Rinse 2291082 N/A 2010/10/08 NUA

Maxxam ID HI8620 Collected 2010/09/21

Sample ID RUN 1-M5/29 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals in Combined Train (6020) ICP1/MS 2295780 2010/10/13 2010/10/13 N_R

Particulates/Acetone Rinse (M5/315/M201) BAL 2288968 2010/10/05 2010/10/08 NUA

Particulates/Filter (M5/315/NJATM1/M201) BAL 2288967 N/A 2010/10/07 BLM

Final Volume of Acetone Probe Rinse 2291082 N/A 2010/10/08 NUA

Maxxam ID HI8620 D u p Collected 2010/09/21

Sample ID RUN 1-M5/29 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals in Combined Train (6020) ICP1/MS 2295780 2010/10/14 2010/10/13 N_R

Maxxam ID HI8621 Collected 2010/09/21

Sample ID RUN 2-M5/29 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals in Combined Train (6020) ICP1/MS 2295780 2010/10/13 2010/10/13 N_R

Particulates/Acetone Rinse (M5/315/M201) BAL 2288968 2010/10/05 2010/10/08 NUA

Particulates/Filter (M5/315/NJATM1/M201) BAL 2288967 N/A 2010/10/07 BLM

Final Volume of Acetone Probe Rinse 2291082 N/A 2010/10/08 NUA

Maxxam ID HI8622 Collected 2010/09/22

Sample ID RUN 3-M5/29 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Metals in Combined Train (6020) ICP1/MS 2295780 2010/10/13 2010/10/13 N_R

Particulates/Acetone Rinse (M5/315/M201) BAL 2288968 2010/10/05 2010/10/08 NUA

Particulates/Filter (M5/315/NJATM1/M201) BAL 2288967 N/A 2010/10/07 BLM

Final Volume of Acetone Probe Rinse 2291082 N/A 2010/10/08 NUA

Page 4 of 8
BT Environmental Consulting

Maxxam Job #: B0D8184 Client Project #: 10-3990.05

Report Date: 2010/10/14 Project name: METCO-GUARDIAN MINERAL WELLS,MS

ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN)

Metals in Combined Train (6020): Extra 2x dilution was required for all samples except HI8619, due to the matrix.

Post digestion duplicate and spike was done on sample HI8620.

Trace level As was observed in the Processed Blank.

Results relate only to the items tested.

Page 5 of 8
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 10-3990.05

P.O. #:

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Quality Assurance Report

Maxxam Job Number: GB0D8184

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2288968 NUA Method Blank Acetone Rinse Particulate Weight in Acetone 2010/10/08 ND, RDL=0.5 mg

2295780 N_R Matrix Spike

(HI8620) Total Antimony (Sb) 2010/10/13 98 % 70 - 130

Matrix Spike DUP

(HI8620) Total Antimony (Sb) 2010/10/13 98 % 70 - 130

MS/MSD RPD Total Antimony (Sb) 2010/10/13 0 % 20

Matrix Spike

(HI8620) Total Arsenic (As) 2010/10/13 95 % 70 - 130

Matrix Spike DUP

(HI8620) Total Arsenic (As) 2010/10/13 96 % 70 - 130

MS/MSD RPD Total Arsenic (As) 2010/10/13 1.0 % 20

Matrix Spike

(HI8620) Total Beryllium (Be) 2010/10/13 91 % 70 - 130

Matrix Spike DUP

(HI8620) Total Beryllium (Be) 2010/10/13 92 % 70 - 130

MS/MSD RPD Total Beryllium (Be) 2010/10/13 1.1 % 20

Matrix Spike

(HI8620) Total Cadmium (Cd) 2010/10/13 94 % 70 - 130

Matrix Spike DUP

(HI8620) Total Cadmium (Cd) 2010/10/13 96 % 70 - 130

MS/MSD RPD Total Cadmium (Cd) 2010/10/13 2.1 % 20

Matrix Spike

(HI8620) Total Chromium (Cr) 2010/10/13 99 % 70 - 130

Matrix Spike DUP

(HI8620) Total Chromium (Cr) 2010/10/13 100 % 70 - 130

MS/MSD RPD Total Chromium (Cr) 2010/10/13 1.0 % 20

Matrix Spike

(HI8620) Total Cobalt (Co) 2010/10/13 97 % 70 - 130

Matrix Spike DUP

(HI8620) Total Cobalt (Co) 2010/10/13 99 % 70 - 130

MS/MSD RPD Total Cobalt (Co) 2010/10/13 2.0 % 20

Matrix Spike

(HI8620) Total Lead (Pb) 2010/10/13 101 % 70 - 130

Matrix Spike DUP

(HI8620) Total Lead (Pb) 2010/10/13 102 % 70 - 130

MS/MSD RPD Total Lead (Pb) 2010/10/13 1 % 20

Matrix Spike

(HI8620) Total Manganese (Mn) 2010/10/13 99 % 70 - 130

Matrix Spike DUP

(HI8620) Total Manganese (Mn) 2010/10/13 100 % 70 - 130

MS/MSD RPD Total Manganese (Mn) 2010/10/13 1.0 % 20

Matrix Spike

(HI8620) Total Nickel (Ni) 2010/10/13 96 % 70 - 130

Matrix Spike DUP

(HI8620) Total Nickel (Ni) 2010/10/13 97 % 70 - 130

MS/MSD RPD Total Nickel (Ni) 2010/10/13 1.0 % 20

Matrix Spike

(HI8620) Total Selenium (Se) 2010/10/13 94 % 70 - 130

Matrix Spike DUP

(HI8620) Total Selenium (Se) 2010/10/13 95 % 70 - 130

MS/MSD RPD Total Selenium (Se) 2010/10/13 1.1 % 20

Spiked Blank Total Antimony (Sb) 2010/10/13 100 % 85 - 115

Spiked Blank DUP Total Antimony (Sb) 2010/10/13 99 % 85 - 115

RPD Total Antimony (Sb) 2010/10/13 1.1 % 20

Spiked Blank Total Arsenic (As) 2010/10/13 101 % 85 - 115

Page 6 of 8
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 10-3990.05

P.O. #:

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Quality Assurance Report (Continued)

Maxxam Job Number: GB0D8184

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2295780 N_R Spiked Blank DUP Total Arsenic (As) 2010/10/13 101 % 85 - 115

RPD Total Arsenic (As) 2010/10/13 0.7 % 20

Spiked Blank Total Beryllium (Be) 2010/10/13 96 % 85 - 115

Spiked Blank DUP Total Beryllium (Be) 2010/10/13 97 % 85 - 115

RPD Total Beryllium (Be) 2010/10/13 1.0 % 20

Spiked Blank Total Cadmium (Cd) 2010/10/13 96 % 85 - 115

Spiked Blank DUP Total Cadmium (Cd) 2010/10/13 94 % 85 - 115

RPD Total Cadmium (Cd) 2010/10/13 1.1 % 20

Spiked Blank Total Chromium (Cr) 2010/10/13 101 % 85 - 115

Spiked Blank DUP Total Chromium (Cr) 2010/10/13 99 % 85 - 115

RPD Total Chromium (Cr) 2010/10/13 1.3 % 20

Spiked Blank Total Cobalt (Co) 2010/10/13 101 % 85 - 115

Spiked Blank DUP Total Cobalt (Co) 2010/10/13 100 % 85 - 115

RPD Total Cobalt (Co) 2010/10/13 1.2 % 20

Spiked Blank Total Lead (Pb) 2010/10/13 98 % 85 - 115

Spiked Blank DUP Total Lead (Pb) 2010/10/13 96 % 85 - 115

RPD Total Lead (Pb) 2010/10/13 2.3 % 20

Spiked Blank Total Manganese (Mn) 2010/10/13 101 % 85 - 115

Spiked Blank DUP Total Manganese (Mn) 2010/10/13 102 % 85 - 115

RPD Total Manganese (Mn) 2010/10/13 0.7 % 20

Spiked Blank Total Nickel (Ni) 2010/10/13 99 % 85 - 115

Spiked Blank DUP Total Nickel (Ni) 2010/10/13 99 % 85 - 115

RPD Total Nickel (Ni) 2010/10/13 0.06 % 20

Spiked Blank Total Selenium (Se) 2010/10/13 100 % 85 - 115

Spiked Blank DUP Total Selenium (Se) 2010/10/13 100 % 85 - 115

RPD Total Selenium (Se) 2010/10/13 0.7 % 20

Method Blank Total Antimony (Sb) 2010/10/13 ND, RDL=0.40 ug

Method Blank DUP Total Antimony (Sb) 2010/10/13 ND, RDL=0.40 ug

RPD Total Antimony (Sb) 2010/10/13 NC % 20

Method Blank Total Arsenic (As) 2010/10/13 0.71, RDL=0.40 ug

Method Blank DUP Total Arsenic (As) 2010/10/13 0.71, RDL=0.40 ug

RPD Total Arsenic (As) 2010/10/13 NC % 20

Method Blank Total Beryllium (Be) 2010/10/13 ND, RDL=0.10 ug

Method Blank DUP Total Beryllium (Be) 2010/10/13 ND, RDL=0.10 ug

RPD Total Beryllium (Be) 2010/10/13 NC % 20

Method Blank Total Cadmium (Cd) 2010/10/13 ND, RDL=0.10 ug

Method Blank DUP Total Cadmium (Cd) 2010/10/13 ND, RDL=0.10 ug

RPD Total Cadmium (Cd) 2010/10/13 NC % 20

Method Blank Total Chromium (Cr) 2010/10/13 ND, RDL=0.30 ug

Method Blank DUP Total Chromium (Cr) 2010/10/13 ND, RDL=0.30 ug

RPD Total Chromium (Cr) 2010/10/13 NC % 20

Method Blank Total Cobalt (Co) 2010/10/13 ND, RDL=0.10 ug

Method Blank DUP Total Cobalt (Co) 2010/10/13 ND, RDL=0.10 ug

RPD Total Cobalt (Co) 2010/10/13 NC % 20

Method Blank Total Lead (Pb) 2010/10/13 ND, RDL=0.20 ug

Method Blank DUP Total Lead (Pb) 2010/10/13 ND, RDL=0.20 ug

RPD Total Lead (Pb) 2010/10/13 NC % 20

Method Blank Total Manganese (Mn) 2010/10/13 ND, RDL=0.75 ug

Method Blank DUP Total Manganese (Mn) 2010/10/13 ND, RDL=0.75 ug

RPD Total Manganese (Mn) 2010/10/13 NC % 20

Method Blank Total Nickel (Ni) 2010/10/13 ND, RDL=0.50 ug

Method Blank DUP Total Nickel (Ni) 2010/10/13 ND, RDL=0.50 ug

RPD Total Nickel (Ni) 2010/10/13 NC % 20

Method Blank Total Selenium (Se) 2010/10/13 ND, RDL=1.0 ug

Method Blank DUP Total Selenium (Se) 2010/10/13 ND, RDL=1.0 ug

Page 7 of 8
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 10-3990.05

P.O. #:

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Quality Assurance Report (Continued)

Maxxam Job Number: GB0D8184

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2295780 N_R RPD Total Selenium (Se) 2010/10/13 NC % 20

RPD -

Sample/Sample

Dup Total Antimony (Sb) 2010/10/13 NC % 20

Total Arsenic (As) 2010/10/13 NC % 20

Total Beryllium (Be) 2010/10/13 NC % 20

Total Cadmium (Cd) 2010/10/13 NC % 20

Total Chromium (Cr) 2010/10/13 0.9 % 20

Total Cobalt (Co) 2010/10/13 NC % 20

Total Lead (Pb) 2010/10/13 0.9 % 20

Total Manganese (Mn) 2010/10/13 NC % 20

Total Nickel (Ni) 2010/10/13 1.6 % 20

Total Selenium (Se) 2010/10/13 NC % 20

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.

Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.

Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a

reliable calculation.

Page 8 of 8
Your Project #: 10-3990.05 

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Attention: Barry Boulianne

BT Environmental Consulting

2615 Wolcott St.

Ferndale, MI

USA 48220

Report Date: 2010/10/15

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B0D7712

Received: 2010/09/30, 12:00

Sample Matrix: Stack Sampling Train

# Samples Received: 5

Date Date Method

Analyses Quantity Extracted Analyzed Laboratory Method Reference

Hexavalent Chromium (M0061) 5 2010/10/01 2010/10/11 BRL SOP-00106 EPA 7199 (M0061) 

Final Volume of KOH Impinger 5 N/A 2010/10/11 

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

LINA BARRETO, Project Manager

Email: LBarreto@maxxam.ca

Phone# (905) 817-5700

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section

5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 1 of 5
BT Environmental Consulting

Maxxam Job #: B0D7712 Client Project #: 10-3990.05

Report Date: 2010/10/15 Project name: METCO-GUARDIAN MINERAL WELLS,MS

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID H I 6 2 9 1 H I 6 2 9 2 H I 6 2 9 4

Sampling Date 2010/09/23 2010/09/23 2010/09/22

14:30 14:26 20:00

 U n i t s R.BLANK-H2O-M0061 RDL R.BLANK-.5N RDL RUN 1-M0061 RDL QC Batch

KOH-M0061

Volume ml 300 1 310 1 670 1 2287483

Hexavalent Chromium (Cr 6+) ug ND 0.1 0.5 0.2 2.0 0.3 2285683

ND = Not detected

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID H I 6 2 9 4 H I 6 2 9 5 H I 6 2 9 6

Sampling Date 2010/09/22 2010/09/23 2010/09/23

20:00 13:50 18:45

 U n i t s RUN 1-M0061 RUN 2-M0061 RUN 3-M0061 RDL QC Batch

Lab-Dup

Volume ml 620 660 1 2287483

Hexavalent Chromium (Cr 6+) ug 2.1 2.5 1.0 0.3 2285683

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 2 of 5
BT Environmental Consulting

Maxxam Job #: B0D7712 Client Project #: 10-3990.05

Report Date: 2010/10/15 Project name: METCO-GUARDIAN MINERAL WELLS,MS

Test Summary

Maxxam ID HI6291 Collected 2010/09/23

Sample ID R.BLANK-H2O-M0061 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2285683 2010/10/01 2010/10/11 LLE

Final Volume of KOH Impinger 2287483 N/A 2010/10/11 FMO

Maxxam ID HI6292 Collected 2010/09/23

Sample ID R.BLANK-.5N KOH-M0061 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2285683 2010/10/01 2010/10/11 LLE

Final Volume of KOH Impinger 2287483 N/A 2010/10/11 FMO

Maxxam ID HI6294 Collected 2010/09/22

Sample ID RUN 1-M0061 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2285683 2010/10/01 2010/10/11 LLE

Final Volume of KOH Impinger 2287483 N/A 2010/10/11 FMO

Maxxam ID HI6294 D u p Collected 2010/09/22

Sample ID RUN 1-M0061 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2285683 2010/10/01 2010/10/11 LLE

Maxxam ID HI6295 Collected 2010/09/23

Sample ID RUN 2-M0061 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2285683 2010/10/01 2010/10/11 LLE

Final Volume of KOH Impinger 2287483 N/A 2010/10/11 FMO

Maxxam ID HI6296 Collected 2010/09/23

Sample ID RUN 3-M0061 Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hexavalent Chromium (M0061) IC/SPEC 2285683 2010/10/01 2010/10/11 LLE

Final Volume of KOH Impinger 2287483 N/A 2010/10/11 FMO

Page 3 of 5
BT Environmental Consulting

Maxxam Job #: B0D7712 Client Project #: 10-3990.05

Report Date: 2010/10/15 Project name: METCO-GUARDIAN MINERAL WELLS,MS

GENERAL COMMENTS

Samples received above 6°C.

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Hexavalent Chromium (M0061): Samples were initially analyzed within hold-time (2010-10-01) however data was not considered acceptable.

Samples were re-analzyed on 2010-10-11.

Results relate only to the items tested.

Page 4 of 5
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 10-3990.05

P.O. #:

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Quality Assurance Report

Maxxam Job Number: GB0D7712

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2285683 LLE Matrix Spike

(HI6294) Hexavalent Chromium (Cr 6+) 2010/10/11 101 % 80 - 120

Spiked Blank Hexavalent Chromium (Cr 6+) 2010/10/11 98 % 90 - 110

Method Blank Hexavalent Chromium (Cr 6+) 2010/10/11 ND, RDL=0.1 ug

RPD -

Sample/Sample

Dup Hexavalent Chromium (Cr 6+) 2010/10/11 2.0 % 20

Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.

Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

Page 5 of 5
Your Project #: 10-3990.05 

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Your C.O.C. #: N/A

Attention: Barry Boulianne

BT Environmental Consulting

2615 Wolcott St.

Ferndale, MI

USA 48220

Report Date: 2010/10/16

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B0D8178

Received: 2010/09/30, 12:00

Sample Matrix: Stack Sampling Train

# Samples Received: 5

Date Date Method

Analyses Quantity Extracted Analyzed Laboratory Method Reference

Hydrogen Halides in H2SO4 Imp. (1 ) 5 2010/10/14 2010/10/14 BRL SOP-00108 EPA Method 26A 

Volume of Sulfuric Acid Impinger 5 N/A 2010/10/14 

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed in Maxxam Mississauga under Maxxam Burlington SCC Accreditation

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

LINA BARRETO, Project Manager

Email: LBarreto@maxxam.ca

Phone# (905) 817-5700

====================================================================

Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section

5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Page 1 of 5
BT Environmental Consulting

Maxxam Job #: B0D8178 Client Project #: 10-3990.05

Report Date: 2010/10/16 Project name: METCO-GUARDIAN MINERAL WELLS,MS

RESULTS OF ANALYSES OF STACK SAMPLING TRAIN

Maxxam ID H I 8 5 8 8 H I 8 5 8 9 H I 8 5 9 0 H I 8 5 9 0 H I 8 5 9 1

Sampling Date 2010/09/23 2010/09/23 2010/09/22 2010/09/22 2010/09/23

19:00 18:57 17:30 17:30 11:45

COC Number N/A N/A N/A N/A N/A

 U n i t s R.BLANK-H2O-M26A R.BLANK-.1N RUN RUN RUN RDL QC Batch

H2SO4-M26A 1-H2SO4-M26A 1-H2SO4-M26A 2-H2SO4-M26A

Lab-Dup

Volume ml 190 200 300 290 1 2297977

Hydrochloric Acid ug ND ND ND ND ND 200 2298035

Hydrofluoric Acid ug ND ND ND ND ND 200 2298035

ND = Not detected

N/A = Not Applicable

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Maxxam ID H I 8 5 9 2

Sampling Date 2010/09/23

16:19

COC Number N/A

 U n i t s RUN RDL QC Batch

3-H2SO4-M26A

Volume ml 280 1 2297977

Hydrochloric Acid ug ND 200 2298035

Hydrofluoric Acid ug ND 200 2298035

ND = Not detected

N/A = Not Applicable

RDL = Reportable Detection Limit

QC Batch = Quality Control Batch

Page 2 of 5
BT Environmental Consulting

Maxxam Job #: B0D8178 Client Project #: 10-3990.05

Report Date: 2010/10/16 Project name: METCO-GUARDIAN MINERAL WELLS,MS

Test Summary

Maxxam ID HI8588 Collected 2010/09/23

Sample ID R.BLANK-H2O-M26A Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hydrogen Halides in H2SO4 Imp. IC/SPEC 2298035 2010/10/14 2010/10/14 A_S

Volume of Sulfuric Acid Impinger 2297977 N/A 2010/10/14 A_S

Maxxam ID HI8589 Collected 2010/09/23

Sample ID R.BLANK-.1N H2SO4-M26A Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hydrogen Halides in H2SO4 Imp. IC/SPEC 2298035 2010/10/14 2010/10/14 A_S

Volume of Sulfuric Acid Impinger 2297977 N/A 2010/10/14 A_S

Maxxam ID HI8590 Collected 2010/09/22

Sample ID RUN 1-H2SO4-M26A Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hydrogen Halides in H2SO4 Imp. IC/SPEC 2298035 2010/10/14 2010/10/14 A_S

Volume of Sulfuric Acid Impinger 2297977 N/A 2010/10/14 A_S

Maxxam ID HI8590 D u p Collected 2010/09/22

Sample ID RUN 1-H2SO4-M26A Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hydrogen Halides in H2SO4 Imp. IC/SPEC 2298035 2010/10/14 2010/10/14 A_S

Maxxam ID HI8591 Collected 2010/09/23

Sample ID RUN 2-H2SO4-M26A Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hydrogen Halides in H2SO4 Imp. IC/SPEC 2298035 2010/10/14 2010/10/14 A_S

Volume of Sulfuric Acid Impinger 2297977 N/A 2010/10/14 A_S

Maxxam ID HI8592 Collected 2010/09/23

Sample ID RUN 3-H2SO4-M26A Shipped

Matrix Stack Sampling Train Received 2010/09/30

Test Description Instrumentation Batch Extracted Analyzed Analyst

Hydrogen Halides in H2SO4 Imp. IC/SPEC 2298035 2010/10/14 2010/10/14 A_S

Volume of Sulfuric Acid Impinger 2297977 N/A 2010/10/14 A_S

Page 3 of 5
BT Environmental Consulting

Maxxam Job #: B0D8178 Client Project #: 10-3990.05

Report Date: 2010/10/16 Project name: METCO-GUARDIAN MINERAL WELLS,MS

GENERAL COMMENTS

Results relate only to the items tested.

Page 4 of 5
BT Environmental Consulting

Attention: Barry Boulianne 

Client Project #: 10-3990.05

P.O. #:

Site Location: METCO-GUARDIAN MINERAL WELLS,MS

Quality Assurance Report

Maxxam Job Number: GB0D8178

QA/QC Date

Batch Analyzed

Num Init QC Type Parameter yyyy/mm/dd Value %Recovery Units QC Limits

2298035 A_S Matrix Spike

(HI8590) Hydrochloric Acid 2010/10/14 99 % 80 - 120

Hydrofluoric Acid 2010/10/14 101 % 80 - 120

Spiked Blank Hydrochloric Acid 2010/10/14 100 % 90 - 110

Hydrofluoric Acid 2010/10/14 100 % 90 - 110

Method Blank Hydrochloric Acid 2010/10/14 ND, RDL=200 ug

Hydrofluoric Acid 2010/10/14 ND, RDL=200 ug

RPD -

Sample/Sample

Dup Hydrochloric Acid 2010/10/14 NC % 20

Hydrofluoric Acid 2010/10/14 NC % 20

Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.

Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.

Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a

reliable calculation.

Page 5 of 5
Ohio Lumex Co., Inc.

9263 Ravenna Rd., Unit A-3

Twinsburg, OH 44087

Phone: (330) 405-0837

Fax: (330) 405-0847

www.ohiolumex.com

Other

Client Name BT Environmental Consulting, Inc. Report Number BTEnvironmental100610 Report 1

Date

Contact Name Phone (248)-548-8072 (972)-931-7127

Trap I.D. Test Location Date Analyzed Scientist

 Mass ng 

Sect.1

 Mass ng 

Sect.2

Spike 

Level 

% Spike 

Recovery

Date(s) in 

Stack Comments

70866 Glassmelt Furnace 10/1/2010 Matt Carhart 4280 6.9 20 9/22/2010 Run 1, Trap A

80265 Glassmelt Furnace 10/4/2010 Matt Carhart 4940 0 9/22/2010 Run 1, Trap B

70854 Glassmelt Furnace 10/4/2010 Matt Carhart 8600 3.4 20 9/22/2010 Run 2, Trap A

80269 Glassmelt Furnace 10/1/2010 Matt Carhart 4507 2.8 9/22/2010 Run 2, Trap B

70862 Glassmelt Furnace 10/4/2010 Matt Carhart 8150 0.9 20 9/23/2010 Run 3, Trap A

80284 Glassmelt Furnace 10/4/2010 Matt Carhart 3920 6.3 9/23/2010 Run 3, Trap B

Variability +- 10%

Calibration Report Available

Turn - Around Time

Standard

48 hour rush

Less than .031 ng is considered "< LDL." Which is less 

than the lowest detection limit.

Plant/Source Guardian (Mineral Wells, MS) 

Sorbent Trap Analysis Report

10/6/2010

Barry Boulianne bboulianne@sbcglobal.net Matthew 

Smith msmith@btecinc.com