Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. 

to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific 

This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were 

tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted 

yellow are required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fi

automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865-04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If 

of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, ora

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results works

6. Please fill in the EIA Facility Code, Facility Name, and Boiler ID using the drop-down boxes provided on the Fu

Sample Results worksheet.

7. Provide the Sample Number and Sample date on the Fuels Sample Results worksheet. You must provide a mi

9 samples, but you are not limited to that number if you have collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the uni

measure.
Information

nformation about chemical analyses of fuels 

, chlorine, fluorine, and metals, such as 

nd selenium. This spreadsheet is intended 

p to 4) fuel analyses at that specific boiler. 

esting for all 4 HAP surrogates were being 

Fields that are highlighted in 

down boxes, included. Gray fields are 

_Testing.xls).

ler on the Boiler Information worksheet.

fuel column of the Boiler Information 

 the Other Fuel Description column.

ethods worksheet. For example: "ASTM 

 Picklist worksheet (orange tab). If the units

le, please fill them in the blank, orange 

e in the Fuels Sample Results worksheet.

boxes provided on the Fuels 

s worksheet. You must provide a minimum of 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Test Date

8219 Ray D Nixon 1
Fuel Type 1 Fuel Type 2 Fuel Type 3

subbituminous
Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

8219 Ray D Nixon 1 As Received Higher Heating Value

8219 Ray D Nixon 1 As Received % Moisture

8219 Ray D Nixon 1 As Received % Ash

8219 Ray D Nixon 1 As Received % Sulfur

8219 Ray D Nixon 1 Dry basis Higher Heating Value

8219 Ray D Nixon 1 Dry basis % Moisture

8219 Ray D Nixon 1 Dry basis % Ash

8219 Ray D Nixon 1 Dry basis % Sulfur

8219 Ray D Nixon 1 Dry basis Antimony

8219 Ray D Nixon 1 Dry basis Arsenic

8219 Ray D Nixon 1 Dry basis Beryllium

8219 Ray D Nixon 1 Dry basis Cadmium

8219 Ray D Nixon 1 Dry basis Chlorine

8219 Ray D Nixon 1 Dry basis Chromium

8219 Ray D Nixon 1 Dry basis Cobalt

8219 Ray D Nixon 1 Dry basis Fluorine

8219 Ray D Nixon 1 Dry basis Lead

8219 Ray D Nixon 1 Dry basis Manganese

8219 Ray D Nixon 1 Dry basis Mercury

8219 Ray D Nixon 1 Dry basis Nickel

8219 Ray D Nixon 1 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D 5865

ASTM D 3173

ASTM D 3174

ASTM D 4239

ASTM D 5865

ASTM D 3173

ASTM D 3174

ASTM D 4239

SW846-6010b

SW846-7062

SW846-6010b

SW846-7130

ASTM D 2361

SW846-7190

SW846-7200

ASTM D 3761

SW846-7420

SW846-7460

SW846-7471a

SW846-7520

SW846-7742
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

8219 Ray D Nixon 1 M23

Sample Number 

(minimum of 9 

samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

Run 1 5/25/2010 8955.00 Btu/lb 26.68

Run 2 5/26/2010 8649.00 Btu/lb 28.03

Run 3 5/27/2010 8637.00 Btu/lb 28.65

 Fuel Testing Results
% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

5.11 0.235 12214 Btu/lb 10.91 6.97 0.321

6.84 0.234 12017 Btu/lb 11.67 9.50 0.325

5.15 0.226 12104 Btu/lb 11.00 7.22 0.317
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.017 % 0.18 mg/Kg 0.23 mg/Kg <0.3 mg/Kg 0.1

0.104 % 0.21 mg/Kg 0.42 mg/Kg <0.5 mg/Kg 0.2

0.046 % 0.22 mg/Kg 0.32 mg/Kg <0.4 mg/Kg 0.1
Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/Kg 3 mg/Kg 2.1 mg/Kg 9 mg/Kg 3.1 mg/Kg

mg/Kg 6 mg/Kg 3 mg/Kg 10 mg/Kg 4.4 mg/Kg

mg/Kg 6 mg/Kg 4.5 mg/Kg 8.7 mg/Kg 3.6 mg/Kg
Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

0.61 mg/Kg 0.007 % 2.4 mg/Kg

0.44 mg/Kg 0.006 % 3.6 mg/Kg

0.35 mg/Kg 0.005 % 2.6 mg/Kg
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

8219 Ray D Nixon 1

Sample Number 

(minimum of 9 

samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results
% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)
Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units
Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

8219 Ray D Nixon 1

Sample Number 

(minimum of 9 

samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results
% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)
Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units
Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units
EIA Facility Code Facility Name Boiler ID

Emissions test 

method(s) conducted 

at time of fuel sample 

collection (e.g., 

M30B, M26A, M0031 

with SW-846 

M6260B)

8219 Ray D Nixon 1

Sample Number 

(minimum of 9 

samples)

Sample Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

% Moisture

(as received)

 Fuel Testing Results
% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)
Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Arsenic (Dry

Basis) Arsenic Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)
Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units
Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units
Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

 unit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm