### 13339 Hagers Ferry Road Huntersville, NC 28078-7929 McGuire Nuclear Complex - MG03A2 Phone: 980-875-5245 Fax: 980-875-4349 

# Order Summary Report Analytical Laboratory

Order Number: J10120192

Lab Contact: Jason C Perkins 

## Date: 12/30/2010 Customer Address: 253 Plant Allen Road Customer Name(s): Don Scruggs, Robbin Jolly, Ray Lidke, Bill Kennedy

Belmont, NC 28012

Phone: 980-875-5348 Report Authorized By: (Signature)


### Program Comments: Allen Test Burn #2 - 12/7 Data Flags & Calculations: Any analytical tests or individual analytes within a test flagged with an "X" or "1" indicate a deviation from the method quality system or quality control requirement. All results are reported on a dry weight basis unless otherwise noted. Data Package: This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows: Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC) Certification: The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina (DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods.

# Sample ID's & Descriptions:

Sample ID Plant/Station Collection Date and Time Collected By Sample Description 2010013325 ALLEN 07-Dec-10 12:35 PM Chris Williams FGD Purge Eff 2010013326 ALLEN 07-Dec-10 8:30 AM Chris Williams EQ Tank Eff 2010013327 ALLEN 07-Dec-10 8:36 AM Chris Williams BioReactor 1 Inf 2010013328 ALLEN 07-Dec-10 8:38 AM Chris Williams BioReactor 2 Inf 2010013329 ALLEN 07-Dec-10 8:33 AM Chris Williams BioReactor 2 Eff 2010013330 ALLEN 22-Nov-10 1:45 PM L. Davis TRIP BLANK 2010013331 ALLEN 07-Dec-10 8:25 AM Chris Williams Filter Blk 7 Total Samples

### COC and .pdf report are in agreement with sample totals

and analyses (compliance programs and procedures). All Results are less than the laboratory reporting limits. All laboratory QA/QC requirements are acceptable. The Vendor Laboratories have been qualified by the Analytical Laboratory Yes No



# Technical Validation Review Checklist:

Yes No
Yes No



# Report Sections Included:

Job Summary Report Sub-contracted Laboratory Results Sample Identification Customer Specific Data Sheets, Reports, & Documentation Technical Validation of Data Package Customer Database Entries Analytical Laboratory Certificate of Analysis Test Case Narratives Analytical Laboratory QC Report Chain of Custody

Reviewed By:

### DataBase Administrator Date:

### 12/30/2010Yes

Electronic Data Deliverable (EDD) Sent Separately

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J10120192

2010013325 Collection Date: 07-Dec-10 12:35 PM 

## Site:FGD Purge Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst MERCURY (COLD VAPOR) IN WATER Mercury (Hg) 31.2 ug/L EPA 245.1 10-Dec-10 11:04 2.5 TLINN TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 84.8 mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Barium (Ba) 1.08 mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Beryllium (Be) < 0.05mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Boron (B) 184 mg/L EPA 200.7 16-Dec-10 10:35 0.5 DJSULL1 Calcium (Ca) 2520mg/L EPA 200.7 16-Dec-10 10:35 0.1 DJSULL1 Cobalt (Co) 0.136mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Iron (Fe) 124 mg/L EPA 200.7 16-Dec-10 10:35 0.1 DJSULL1 Magnesium (Mg) 997 mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Manganese (Mn) 8.77 mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Molybdenum (Mo) < 0.05mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 Sodium (Na) 49.1 mg/L EPA 200.7 16-Dec-10 10:35 0.5 DJSULL1 Tin (Sn) < 0.5mg/L EPA 200.7 16-Dec-10 10:35 0.5 DJSULL1 Titanium (Ti) 1.82 mg/L EPA 200.7 16-Dec-10 10:35 0.05 DJSULL1 DISSOLVED METALS BY ICP-MS Selenium (Se) 243 ug/L EPA 200.8 27-Dec-10 14:07 10 KRICHAR TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) 11.0 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Arsenic (As) 233 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Cadmium (Cd) < 10ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Chromium (Cr) 241 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Copper (Cu) 251 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Lead (Pb) 151 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Nickel (Ni) 400 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Selenium (Se) 1940ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Silver (Ag) < 10ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Thallium (Tl) < 10ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Vanadium (V) 198 ug/L EPA 200.8 21-Dec-10 12:10 10 KRICHAR Zinc (Zn) 488 ug/L EPA 200.8 21-Dec-10 12:10 20 KRICHAR TOTAL DISSOLVED SOLIDS Vendor Parameter Complete V_PRISM 

## 2010013326 Collection Date: 07-Dec-10 8:30 AM 

## Site:EQ Tank Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J10120192

2010013326 Collection Date: 07-Dec-10 8:30 AM 

## Site:EQ Tank Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst MERCURY (COLD VAPOR) IN WATER Mercury (Hg) 43.4 ug/L EPA 245.1 10-Dec-10 11:06 2.5 TLINN TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 82.7 mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Barium (Ba) 1.07 mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Beryllium (Be) < 0.05mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Boron (B) 149 mg/L EPA 200.7 16-Dec-10 10:39 0.5 DJSULL1 Calcium (Ca) 2390mg/L EPA 200.7 16-Dec-10 10:39 0.1 DJSULL1 Cobalt (Co) 0.123mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Iron (Fe) 118 mg/L EPA 200.7 16-Dec-10 10:39 0.1 DJSULL1 Magnesium (Mg) 874 mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Manganese (Mn) 6.70 mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Molybdenum (Mo) < 0.05mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 Sodium (Na) 46.3 mg/L EPA 200.7 16-Dec-10 10:39 0.5 DJSULL1 Tin (Sn) < 0.5mg/L EPA 200.7 16-Dec-10 10:39 0.5 DJSULL1 Titanium (Ti) 1.94 mg/L EPA 200.7 16-Dec-10 10:39 0.05 DJSULL1 DISSOLVED METALS BY ICP-MS Selenium (Se) 127 ug/L EPA 200.8 27-Dec-10 14:11 10 KRICHAR TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) 12.2 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Arsenic (As) 229 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Cadmium (Cd) < 10ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Chromium (Cr) 216 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Copper (Cu) 240 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Lead (Pb) 142 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Nickel (Ni) 380 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Selenium (Se) 1620ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Silver (Ag) < 10ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Thallium (Tl) < 10ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Vanadium (V) 196 ug/L EPA 200.8 21-Dec-10 12:05 10 KRICHAR Zinc (Zn) 434 ug/L EPA 200.8 21-Dec-10 12:05 20 KRICHAR 

## 2010013327 Collection Date: 07-Dec-10 8:36 AM 

## Site:BioReactor 1 Inf Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 0.826mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 Barium (Ba) 0.172mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 Beryllium (Be) < 0.05mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J10120192

2010013327 Collection Date: 07-Dec-10 8:36 AM 

## Site:BioReactor 1 Inf Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Boron (B) 126 mg/L EPA 200.7 16-Dec-10 10:43 0.5 DJSULL1 Calcium (Ca) 1940mg/L EPA 200.7 16-Dec-10 10:43 0.1 DJSULL1 Cobalt (Co) < 0.05mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 Iron (Fe) < 0.1mg/L EPA 200.7 16-Dec-10 10:43 0.1 DJSULL1 Magnesium (Mg) 787 mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 Manganese (Mn) 0.915mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 Molybdenum (Mo) < 0.05mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 Sodium (Na) 44.8 mg/L EPA 200.7 16-Dec-10 10:43 0.5 DJSULL1 Tin (Sn) < 0.5mg/L EPA 200.7 16-Dec-10 10:43 0.5 DJSULL1 Titanium (Ti) < 0.05mg/L EPA 200.7 16-Dec-10 10:43 0.05 DJSULL1 DISSOLVED METALS BY ICP-MS Selenium (Se) 104 ug/L EPA 200.8 27-Dec-10 14:15 10 KRICHAR TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Arsenic (As) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Cadmium (Cd) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Chromium (Cr) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Copper (Cu) 10.8 ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Lead (Pb) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Nickel (Ni) 30.5 ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Selenium (Se) 83.4 ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Silver (Ag) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Thallium (Tl) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Vanadium (V) < 10ug/L EPA 200.8 21-Dec-10 12:00 10 KRICHAR Zinc (Zn) < 20ug/L EPA 200.8 21-Dec-10 12:00 20 KRICHAR 

## 2010013328 Collection Date: 07-Dec-10 8:38 AM 

## Site:BioReactor 2 Inf Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 1.57 mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 Barium (Ba) 0.204mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 Beryllium (Be) < 0.05mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 Boron (B) 96.9 mg/L EPA 200.7 16-Dec-10 10:47 0.5 DJSULL1 Calcium (Ca) 2020mg/L EPA 200.7 16-Dec-10 10:47 0.1 DJSULL1 Cobalt (Co) < 0.05mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 Iron (Fe) 2.53 mg/L EPA 200.7 16-Dec-10 10:47 0.1 DJSULL1 Magnesium (Mg) 736 mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J10120192

2010013328 Collection Date: 07-Dec-10 8:38 AM 

## Site:BioReactor 2 Inf Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Manganese (Mn) 1.41 mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 Molybdenum (Mo) < 0.05mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 Sodium (Na) 44.2 mg/L EPA 200.7 16-Dec-10 10:47 0.5 DJSULL1 Tin (Sn) < 0.5mg/L EPA 200.7 16-Dec-10 10:47 0.5 DJSULL1 Titanium (Ti) < 0.05mg/L EPA 200.7 16-Dec-10 10:47 0.05 DJSULL1 TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Arsenic (As) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Cadmium (Cd) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Chromium (Cr) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Copper (Cu) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Lead (Pb) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Nickel (Ni) 48.0 ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Selenium (Se) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Silver (Ag) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Thallium (Tl) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Vanadium (V) < 10ug/L EPA 200.8 21-Dec-10 11:54 10 KRICHAR Zinc (Zn) < 20ug/L EPA 200.8 21-Dec-10 11:54 20 KRICHAR 

## 2010013329 Collection Date: 07-Dec-10 8:33 AM 

## Site:BioReactor 2 Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst MERCURY (COLD VAPOR) IN WATER Mercury (Hg) < 1 ug/L EPA 245.1 10-Dec-10 11:09 1 TLINN TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) 0.913mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Barium (Ba) 0.184mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Beryllium (Be) < 0.05mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Boron (B) 77.0 mg/L EPA 200.7 16-Dec-10 10:10 0.5 DJSULL1 Calcium (Ca) 2220mg/L EPA 200.7 16-Dec-10 10:10 0.1 DJSULL1 Cobalt (Co) < 0.05mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Iron (Fe) 0.176mg/L EPA 200.7 16-Dec-10 10:10 0.1 DJSULL1 Magnesium (Mg) 690 mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Manganese (Mn) 1.27 mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Molybdenum (Mo) 0.107mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1 Sodium (Na) 44.0 mg/L EPA 200.7 16-Dec-10 10:10 0.5 DJSULL1 Tin (Sn) < 0.5mg/L EPA 200.7 16-Dec-10 10:10 0.5 DJSULL1 Titanium (Ti) < 0.05mg/L EPA 200.7 16-Dec-10 10:10 0.05 DJSULL1

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J10120192

2010013329 Collection Date: 07-Dec-10 8:33 AM 

## Site:BioReactor 2 Eff Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Arsenic (As) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Cadmium (Cd) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Chromium (Cr) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Copper (Cu) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Lead (Pb) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Nickel (Ni) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Selenium (Se) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Silver (Ag) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Thallium (Tl) < 5 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Vanadium (V) 5.20 ug/L EPA 200.8 21-Dec-10 12:16 5 KRICHAR Zinc (Zn) < 10ug/L EPA 200.8 21-Dec-10 12:16 10 KRICHAR 

## 2010013330 Collection Date: 22-Nov-10 1:45 PM 

## Site:TRIP BLANK Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP Aluminum (Al) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Barium (Ba) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Beryllium (Be) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Boron (B) < 0.05mg/L EPA 200.7 16-Dec-10 10:31 0.05 DJSULL1 Calcium (Ca) 0.020mg/L EPA 200.7 16-Dec-10 10:31 0.01 DJSULL1 Cobalt (Co) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Iron (Fe) < 0.01mg/L EPA 200.7 16-Dec-10 10:31 0.01 DJSULL1 Magnesium (Mg) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Manganese (Mn) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Molybdenum (Mo) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 Sodium (Na) < 0.05mg/L EPA 200.7 16-Dec-10 10:31 0.05 DJSULL1 Tin (Sn) < 0.05mg/L EPA 200.7 16-Dec-10 10:31 0.05 DJSULL1 Titanium (Ti) < 0.005mg/L EPA 200.7 16-Dec-10 10:31 0.005 DJSULL1 TOTAL RECOVERABLE METALS BY ICP-MS Antimony (Sb) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Arsenic (As) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Cadmium (Cd) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Chromium (Cr) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Copper (Cu) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Lead (Pb) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Nickel (Ni) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Selenium (Se) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR

# Certificate of Laboratory Analysis This report shall not be reproduced, except in full.



## Order # J10120192

2010013330 Collection Date: 22-Nov-10 1:45 PM 

## Site:TRIP BLANK Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst TOTAL RECOVERABLE METALS BY ICP-MS Silver (Ag) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Thallium (Tl) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Vanadium (V) < 1 ug/L EPA 200.8 21-Dec-10 11:49 1 KRICHAR Zinc (Zn) < 2 ug/L EPA 200.8 21-Dec-10 11:49 2 KRICHAR 

## 2010013331 Collection Date: 07-Dec-10 8:25 AM 

## Site:Filter Blk Matrix: OTHER

Analyte Analysis Date/Time Method Units Qualifiers RDL Result 

## Sample #:

Analyst DISSOLVED METALS BY ICP-MS Selenium (Se) < 2 ug/L EPA 200.8 27-Dec-10 14:19 2 KRICHAR

### This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 SC Certification No. 99012 NC Drinking Water Cert No. 37735 

# Case Narrative 12/20/2010

Duke Energy Corporation Jay Perkins 13339 Hagers Ferry Road Huntersville, NC 28078 Project: Allen - FGD Alternative Fuels Test Burn #2 Daily Project No.: J10120192 Lab Submittal Date: 12/09/2010 Prism Work Order: 0120271

Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC.



### VP Laboratory Services Reviewed By

Data Qualifiers Key Reference:



### Method Detection Limit MDLBelow Reporting Limit BRLRelative Percent Difference RPD


## *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J.

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 1 of 5

# Sample Receipt Summary 12/20/2010 

## Prism Work Order: 0120271 Client Sample ID Matrix Lab Sample ID Date SampledDate Received 

### 0120271-01 12/07/10 2010013325/FGD PURGE EFF 12/09/10 Water Samples received in good condition at 2.9 degrees C unless otherwise noted.

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 2 of 5

# Laboratory Report 12/20/2010

Result Parameter Batch ID Report Limit Analysis Date/Time Method Dilution Factor Units MDL Analyst 

### 13339 Hagers Ferry Road Project No.: J10120192 Project: Allen - FGD Alternative Fuels Test Burn #2 Daily Duke Energy Corporation
Huntersville, NC 28078 Attn: Jay Perkins Sample Matrix: Water Client Sample ID: 2010013325/FGD PURGE Prism Sample ID: 0120271-01 Prism Work Order: 0120271 Time Collected: 12/07/10 12:35 Time Submitted: 12/09/10 08:20

General Chemistry Parameters 10000 *SM2540 C P0L0288 1 50 12/14/10 14:00JAB mg/L 8.7 Total Dissolved Solids

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 3 of 5

### 12/20/10 

## Level II QC Report

13339 Hagers Ferry Road Project No: J10120192 Project: Allen - FGD Alternative Fuels Test Burn #2 Daily Duke Energy Corporation
Huntersville, NC 28078 Attn: Jay Perkins Prism Work Order: 0120271 Time Submitted: 12/9/10 8:20:00AM

Result Limit

ReportingUnitsLevel SpikeResult

Source%REC%REC LimitsRPDRPD LimitNotes Analyte General Chemistry Parameters - Quality Control



### Batch P0L0288 - NO PREP Blank (P0L0288-BLK1) 

### Prepared & Analyzed: 12/14/10 Total Dissolved Solids mg/L BRL 50 LCS (P0L0288-BS1) 

### Prepared & Analyzed: 12/14/10 Total Dissolved Solids mg/L 998 50 1000 90-110 100


### Sample Extraction Data
NO PREP Lab Number Batch Date Initial Final P0L0288 0120271-01 12/14/10 50 50 mL mL

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.

449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 

## Page 4 of 5Page 5 of 5