### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Please fill in the EIA Facility Code, Facility Name, and Boiler ID using the drop

- down boxes provided on the Fuels Sample Results worksheet. 7. Provide the Sample Number and Sample date on the Fuels Sample Results worksheet. You must provide a minimum of 9 samples, but you are not limited to that number if you have collected more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. boxes provided on the Fuels

7. Provide the Sample Number and Sample date on the Fuels Sample Results worksheet. You must provide a minimum of

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date

8219 Ray

D Nixon 1Fuel Type 1 Fuel Type 2 Fuel Type 3

subbituminousOther Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte

8219 Ray

D Nixon 1 As Received Higher Heating Value 8219 Ray

D Nixon 1 As Received % Moisture 8219 Ray

D Nixon 1 As Received % Ash 8219 Ray

D Nixon 1 As Received % Sulfur 8219 Ray

D Nixon 1 Dry basis Higher Heating Value 8219 Ray

D Nixon 1 Dry basis % Moisture 8219 Ray

D Nixon 1 Dry basis % Ash 8219 Ray

D Nixon 1 Dry basis % Sulfur 8219 Ray

D Nixon 1 Dry basis Antim ony 8219 Ray

D Nixon 1 Dry basis Arsenic 8219 Ray

D Nixon 1 Dry basis Beryllium 8219 Ray

D Nixon 1 Dry basis Cadmium 8219 Ray

D Nixon 1 Dry basis Chlorine 8219 Ray

D Nixon 1 Dry basis Chromium 8219 Ray

D Nixon 1 Dry basis Cobalt 8219 Ray

D Nixon 1 Dry basis Fluorine 8219 Ray

D Nixon 1 Dry basis Lead 8219 Ray

D Nixon 1 Dry basis Manganese 8219 Ray

D Nixon 1 Dry basis Mercury 8219 Ray

D Nixon 1 Dry basis Nickel 8219 Ray

D Nixon 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D 5865 ASTM D 3173 ASTM D 3174 ASTM D 4239 ASTM D 5865 ASTM D 3173 ASTM D 3174 ASTM D 4239 SW 846-6010b SW 846-7062 SW 846-6010b SW 846-7130 ASTM D 2361 SW 846-7190 SW 846-7200 ASTM D 3761 SW 846-7420 SW 846-7460 SW 846-7471a SW 846-7520 SW 846-7742EIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 8219 Ray

D Nixon 1 M23

Sample Number (minimum of 9 samples) Sample Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Run 1 5/25/2010 8955.00 Btu/lb 26.68 Run 2 5/26/2010 8649.00 Btu/lb 28.03 Run 3 5/27/2010 8637.00 Btu/lb 28.65 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 5.11 0.235 12214 Btu/lb 10.91 6.97 0.321 6.84 0.234 12017 Btu/lb 11.67 9.50 0.325 5.15 0.226 12104 Btu/lb 11.00 7.22 0.317Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 0.017 % 0.18 mg /Kg 0.23 mg /Kg <0.3 mg /Kg 0.1 0.104 % 0.21 mg /Kg 0.42 mg /Kg <0.5 mg /Kg 0.2 0.046 % 0.22 mg /Kg 0.32 mg /Kg <0.4 mg /Kg 0.1Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units mg /Kg 3 mg /Kg 2.1 mg /Kg 9 mg /Kg 3.1 mg /Kg mg /Kg 6 mg /Kg 3 mg /Kg 10 mg /Kg 4.4 mg /Kg mg /Kg 6 mg /Kg 4.5 mg /Kg 8.7 mg /Kg 3.6 mg /KgSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 0.61 mg /Kg 0.007 % 2.4 mg /Kg 0.44 mg /Kg 0.006 % 3.6 mg /Kg 0.35 mg /Kg 0.005 % 2.6 mg /KgEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 8219 Ray

D Nixon 1

Sample Number (minimum of 9 samples) Sample Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 8219 Ray

D Nixon 1

Sample Number (minimum of 9 samples) Sample Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 8219 Ray

D Nixon 1

Sample Number (minimum of 9 samples) Sample Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm