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AIR &RADIATION ~.

MAN.~GEMENT ADMINISTRATION

SOURCE TESTING REPORT

LEIDGH CE:MENT COMPANY

UNION BRIDGE FACILITY

UNION BRIDGE, MARYLAND

Testing Dates: August 20 & September 10 through 13, 2002

Prepared for:

Lehigh Cement Company

Union Bridge Facility

675 Quaker Hill Road

Union Bridge, Maryland 21791

Prepared by:

Air/Compliance Consultants, Inc.

1050 William Pitt Way

Pittsburgh, Pennsylvania 15238

Project No. 02-046B

Air/Compliance

Consultants,Inc.
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2.

3.

4.

5.

6.

7.

CONTENTS

Page

INTRODUCTION 1

TESTING PERSONNE-L 1

PROCESS DESCRIPTION 1

TESTIN'G METHODS 2

4.1. TRAVERSE POIN'T SELECTION 2

4.2. GAS VELOCITY 2

4.3. STACK GAS MOLECULAR WEIGHT 2

4.4. STACK GAS MOISTURE CONTENT 2

4.5. DIOXIN AND FUR.AN DETERMINATIONS 3

4.6. PARTICULATE MATIER DETERMINATIONS 3

4.7. OPACITY DETERMINATIONS 3

4.8. CARBON MONOXIDE AND TOTAL HYDROCARBON DETERMINATIONS 4

TESTIN'G LOCATION : 4

TESTIN'G SUMMARY 4

CONCLUSION 5

TABLES

1. Dioxin and Furan Test Results, Main Kiln Stack, Raw Mill O~ September 11 & 12, 2002

2. Dioxin and Furan Test Results, Main Kiln Stack, Raw Mill Off, September 10 & 13, 2002

3. Particulate Matter Test Results, Main Kiln Stack, Raw Mill O~ September 11 & 12, 2002

4. Particulate Matter Test Resul~, Main Kiln Stack, Raw Mill Off, September 10 & 13,2002

5. Particulate Matter Test Results, Clinker Cooler, August 20,2002

6. Carbon Monoxide and Total Hydrocarbon Test Results, M~ Kiln Exhaust, September 11,2002

7. Opacity Test Results, Main Kiln Exhaust, September 11,2002

8. Opacity Test Results, Clinker Cooler Exhaust, August 20, 2002

FIGURES

1. Kiln Stack Sampling Diagram

2. Clinker Cooler Exhaust Sampling Diagram
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CONTENTS CONT.

APPENDICES

A. Testing Protocol

B. ComputeriZed & Field Data Sheets

C. Plant Process Data

D. Laboratory Data

E. Equipment Calibrations and Certification Data

F. Sample Calculations
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1. INTRODUCTION

SOURCE TESTING REPORT

LEIDGH CEMENT COMPANY

UNION BRIDGE FACILITY

UNION BRIDGE, MARYLAND

Air/Compliance Consultants, Inc. (ACC!) was contracted by Lehigh Cement Company (Lehigh),

to conduct a compliance-testing program on the Main Cement Kiln, and Clinker Cooler exhausts

at the facility located in Union Bridge, Maryland. Testing was conducted to comply with the

requirements of.the Construction Permit 06-6-0256R, Prevention of Significant Deterioration

(PSD) Approval Number PSD-97-01R, New Source Review (NSR) Approval Number NSR-97-

02, and 40 Code ofFederal Regulations (CFR) 63, Subpart LLL requirements.

2. TESTING PERSONNEL

( Compliance testing was conducted on August 20, 2002 for the Clinker Cooler exhaust, and

September 10 through 13,2002 for the Main Kiln exhaust. ACCI testing personnel consisted of

Mr. James Phillippi, Senior Project Manager; Mr. Michael Matvey, Scientist; Mr. William

Cowell, Project Engineer; and Mr. Patrick Walters, Technician. Mr. Steve Lang ofthe Maryland

Department ofthe Environment (MDEP) observed the testing.

3. PROCESS DESCRIPTION

Lehigh operates one Portland Cement Kiln at their Union Bridge facility located in Union

Bridge, Maryland. The pyroprocessing system consists of an in-line raw mill and 5-stage

preheater kiln system. Limestone (calcium carbonate) is the primary component. The kiln line

consists of an in-line raw mill, kiln, clinker cooler, baghouse, stack and associated duct work.

The clinker cool~r is used to cool the kiln product and exhaust from the clinker cooler is passed

through the clinker cooler baghouse then to the cooler exhaust stack. The exhaust from the kiln is

fed either through a baghouse to the main kiln stack or taken to heat the raw mill. The exhaust

from the mill is then passed through a baghouse to the main kiln stack.
4. TESTING METHODS

2

ACCI conducted testing following the United States Environmental Protection Agency (USEPA)

Title 40, Part 60, Appendix A, Testing Methods 1 through 5, and 23 at the kiln exhaust. Testing

was also conducted following 40 CFR part 63, subpart LLL and to comply with the requirements

of the Construction Permit, NSR Approval, and PSD Approval. All testing was done without

deviation from the referenced testing methods and procedures. The approved protocol and

relevant correspondence are contained in Appendix A.

4.1. Traverse Point Selection

USEPA Method 1 was utilized in the selection oftraverse points for the Main Cement Kiln, and

Clinker Cooler stacks. Twenty-four traverse points (twelve per diameter) were utilized to

establish gas flow rate for the Clinker Cooler exhaust stack, and twelve traverse points (six per

.diameter) were utilized on the Main Cement Kiln exhaust. Figure 1 presents an illustration of

the Main Cement Kiln Stack. Figure 2 presents an illustration ofthe Clinker Cooler Stack.

4.2. Gas Velocity

USEPA Method 2 was followed for the detennination of gas velocity and volumetric flow rate.

This procedure utilized S-type Pitot tube and inclined manometer to detennine stack-gas

velocity head. Gas temperature measurements were made using a Type K thermocouple and

.c:iigital pyrometer.

4.3. Stack Gas Molecula~ Weight

USEPA Method 3 was utilized for the detel'Dlipation ofstack-gas ~olecular weight. Fyrite gas

analyzers were used in the determination of the carbon dioxide (C02) and oxygen (02)

/0

concentrations. Three grab samples were analyzed for each test run. Nitrogen (N2) was {~

determined by the difference.

4.4. Stack Gas Moisture Content

USEPA Method 4 describes the procedure that was employed for the determination of the

moisture content of the stack gas. The gas moisture was detennined by quantitatively

\\SeIver1lOataIAPROJEC1U.ehigh CemenlIUnlOl1 Bridgo 02oOlSB\RllpClIfslMain Clinkor COoler\ropllft.d&f-partofll8ln.d.cooIlr.doc
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condensing stack gas in chilled impingers and a silica gel absorber. The amount of moisture

condensed was detennined by the volume of condensate collected and weight differential in the

silica gel. A calibmted dry gas meter was used to measure the volume of gas sampled. The

amount of water condensed and the volume of gas sampled were used to calculate the gas

moisture content. Moisture determination was performed concurrently with each test run to

allow determination of dry stack-gas molecular weight and to calculate the dry standard cubic

feet per minute (OSCFM) flow mte. Moisture sampling was conducted concurrently with the

Method 5/23 sampling.

4.5. Dioxin and Furan Determinations

USEPA Method 23, "Determination ofPolychlorinated Dibenzo-P-Dioxins and Polychlorinated

Dibenzofurans from Stationary Sources," was used to detennine the dioxin and furan (OIF)

emissions. Testing was conducted at two different opemting conditions, with the Raw Mill

opemting and Raw Mill not opemting. The traverse points selected in accordance with USEPA

Method 1 were isokinetically sampled for three, two hundred forty-minute test runs at each

opemting condition. This sample time resulted in an adequate sample volume for accurate mass

detenninations. DIF's are extmcted from the sample, separated by high resolution gas

chromatogmphy, and measured by high resolution mass spectrometry. DIF testing was

conducted on the Main Cement Kiln only. Tables 1 and 2 present the results ofthe DIF testing.

4.6. Particulate Matter Determinations

USEPA Method 5 "Determination ofParticulate Emissionsfrom Stationary Sources, " was used

to determine the particulate emissions. The USEPA Method 5 sampling tmin was combined

with the USEPA Method 23 sampling !min resulting in three, two hundred forty-minute test runs

on the Main Cement Kiln at each of the two opemting conditions. Three 60-minute sampling

runs were conducted on the Clinker Cooler exhaust stack. Tables 3, 4, and 5 present the results

ofthe particulate matter (PM) testing.

4.7. Opacity Determinations

Opacity data was obtained from certified continuous opacity monitors located on the Main Kiln

exhaust, and the Clinker Cooler exhaust in approved locations. Three 60-minute data segments
4

were obtained in blocks of 6-minute averages. Tables 7 and 8 present the results ofthe opacity

monitoring on the Main Kiln exha~ and Clinker Cooler exhaust, respectively.

4.8. Carbon Monoxide and Total Hydrocarbon Determinations

Carbon monoxide (CO) and total hydrocarbon (THC) emissions data were obtained from

certified analyzers located on the Main Kiln exhaust stack in an approved location. Three 60-

minute data points were obtained and are reported in terms of pounds per hour (lblhr), in one

hour averages. Table 6 present the results ofthe CO and THC emissions.

5. TESTING LOCATION

Particulate and DIF sampling was perfonned at the outlet ofthe Main Cement Kiln exhaust, after

all control equipment. A diagram showing testing locations, stack dimensions, and distances to

the nearest upstream. and downstream flow disturbances is included as Figure 1. The traverse

and sampling locations on the exhaust stack are installed on the 13.71 foot diameter circular

duct. The four sampling ports installed are approximately 295.28 feet downstream (21.5 duct

diameters) and 69.55 feet (5.1 duct diameters) upstream. ofthe nearest flow disturbance.

Particulate sampling, and opacity monitoring were also perfonned on the Clinker Cooler exhaust.

Figure 2 is a diagram showing testing locations, stack dimensions, and distances to the nearest

upstream and downstream flow disturbances. The traverse and sampling locations on exhaust

stack are installed on the 11.33 foot diameter circular duct. The four sampling ports installed are

approximately 57.4 feet downstream (5.1 duct diameters) and 33.96 feet (3.0 duct diameters)

upstream ofthe nearest flow disturbance.

6. TESTING SUMMARY

DIF tests results for the kilns are presented in Tables 1 and 2 for Raw Mill On and Raw Mill Off

conditions, respectively. Particulate test results are presented in Tables 3, 4, and 5 for the Kiln

Raw Mill On, Kiln Raw Mill Off, and the Clinker Cooler, respectively. Appendix B contains the

C computerized data sheets and the field data sheets. The test results indicated compliance with the
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Construction Permit and Subpart LLL emission limits. Appendix C contains Lehigh recorded

process parameters. These parameters include the kiln operation log, laboratory control sheets,

pre-ESP inlet temperature readings, calculations for raw material input, and associate clinker

production and documents for data verification. Appendix D contains laboratory analytical data.

Appendices E and F contain equipment calibrations, certification data and sample calculations,

respectively.

7. CONCLUSION

ACCI conducted a compliance testing program on August 20, and September 10 through 13,

2002 for DIF, opacity and PM on the Main Cement Kiln exhaust, and PM and opacity on the

Clinker Cooler exhaust at the Lehigh facility located in Union Bridge, Maryland. Main Kiln

tests were conducted with the raw mill on and off. All tests were conducted in strict accordance

with the applicable USEPA methodologies. Emission rates were shown to be in compliance with

the applicable permit limits.
Table 3. Particulate Matter Test Resulls, Main Kiln Stack, Raw Mill On. SeplembeT II and 12, 2002

( Lehigh Cement Company. Union Bridge, Maryland

Test IhLll Run I R~2 R~J A\'erage

Dale Seplemba' II, 2002 September II, 2002 Septembcf 12, 2002

SwtTime 8:02AM 8:46PM 12:S3 PM

End Time 8:21 PM 12:51 AM 4:58 PM

Flow Rate (ACFM) 335,320 322,231 352,457 336,669

Flow Roue (SCFM) 256,863 251,794 264,550 257,735

Flow Rale (DSCFM) 220,557 220,838 233,167 225,054

Sample Volume (DSCF) 177.79 172.l8 181.36 177.11

Sample Volume (DSCM) 5.03 4.88 5.14 5.02

Carbon Dioxide (dry volume 'Yo) 25.00 25.00 26.00 25.33

Oxygen (dry volume %) 4.00 4.00 3.00 3.67

Waler Vapor (volume %) 14.13 12.29 11.64 12.69

Stick Temperature (oF) 217.9 205.8 230.6 21S.1

Percent ofIsokinetic Sampling (%) 98.4 95.2 94.7 96.1

Particulale wlo AB Correction (mg) 6.150 6.550 1.750 4.811

AB Correction (mg) 1.659 1.619 20>4 1.777

Particulate with AB Correction (mg) 4.491 4.931 0.350 3.257

I>y F«d (IOnsIhour) 393.6 393.6 426.1 404.4

I>yF«d (meuie IOnsIbour)111 357.1 357.1 386.5 366.9

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Results

Parliculale Results

Emis.sion Concentration (gr2insJDSCF) 0.00039 0.00044 0.ססOO3 0.00029

Emission Limit (grainslDSCF) 0.01510

Emission Rale (lbIhr) 0.74 0.84 0.06 O.H

Emission Rate (lbJlon Dry Feed) 0.0019 0.0021 0.0001 0.0014

Emission Rale (kp) 0.33 0.38 om 0.25

Emission Rate (kgfMg Dry Feed) (II 0.00094 0.00106 0,ססOO7 0.00069

Emission Limit (kgfMg Dry Feed) (I) 0.l5

AB

ACFM

OSCF

DSCFM

DSCM

SCFM

wI.

'(I) 1 metric Ion "1000 kg'" t Mg.

Acetone Blank.

Aet\l31 cubic feet per minute

Dry Standard cubie feet

Dry standard cubic feel per minute

Dry standard cubic meIer

Standard cubic feet pttminute

Wilh (lUI

OF

kg

'''''''

Ibho.

Mg

m,

dryvolwne %

Degrees Fahrenheit

Kilogram

Pounds per hour

Pounds per ton

Mega.gram

Milligram

Pe=t b)' Volume, dry ba.sis

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AS

ACFM

DSCF

DSCFM

DSCM

sen1

wlo

'(I) 1 rnftrlc: tOD -1000 kg - J Mg.

Acetone 8111lk

Actual cubic (eel per minute

Dry SWM!.ud cubic feet

Dry standard cubic feet per minute

Dry standard cubic meter

Standard cubic feet per minute

With oul

OF

kg

Ibilu

lblton

Mg

mg

dry volume %

Degrc-es Fahrenheit

Kilogram

Pound! pel hour

Pounds per Ion

Megagram

Milligram

Percent by Volume:, dry basis

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Table 5. Particulate Maller Test Results, Clinker Cooler. August 20, 2002

Lehigh Cemenl Comp3ny, Union Bridge, Maryland

Test Dati R=1 Run 2 Run 3 A\-enge

"", Augu~1 20, 2002 "u&\lS1 20, 2002 Au&USI 20, 2002

SwtTime 10:20 AM 11:56AM 1:25 PM

End Time 11:30 AM I:~PM 2:)) PM

flo.... Rate (ACFM) 195,150 192,IS9 19.1,2&8 193.866

Flow Rate (SCFM) 1S7,7!9 155,173 156,601 156,491

Flow Rate (DSCFM) 154,624 151,862 1S1,827 l52,TIl

Samp1l: Volume (OSCF) 43.53 44.95 45.53 44.67

Sample Volume (DSCM) 1.23 1.27 1.29 1.27

Carbon Dioxide (dry volumc ~.) 0.00 0.00 0.00 0.00

O"ygen (dry volume ~.) 21.00 21.00 21.00 21.00

WataVapor (,'olume: %) 1.96 2.13 ].05 2.38

Suck Tempcature (oF) 189.4 190.0 191.2 190~

Percent of lsokinclic Sampling (-4) 93.4 98.2 99.' 97.0

Paniculatc wlo AD COlTeclion (mg) 9.450 7.150 7.800 8.133

AD Correction (lOg) 0.106 0.127 0.099 0.111

Particulate \l.ith AD CoJTe'Clion (mg) 9.344 7.023 7.701 8.0n

"'" F=I (IOnsIbow) 402.3 402.3 ..,J ..2.3

"'" F=I (mroic IOnsIOOur)lll 365.0 365.0 365.0 365.0

( Rcsults

PaniClilatc Rcsults

ErrUsion Concmtr.ltion (gninsIDSCF) 0.00331 0.(X)241 0.00261 0.0027&

Emission Limit (gn;insIDSCF) 0.01290

Emission Rate (lhIhr) 'J' 3.14 3.40 3.64

Emission Rate (Ibllon Dry Feed) 0.0109 0.0078 O.OO~ 0.0091

Emis.sion Ratc (kglht) 1.99 1.42 U4 1.65

Emission R<J.te (kglMg Dry Feed) ill 0.00546 0.00390 0.00422 o.oom

Emis.sion Limit (kg/M8 Dry Feed) tl) 0.15

AB

ACFM

DSCF

DSCFM

DSCM

SCfl,i

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(1'1 metric too - 1000 kg -I Mg.

Acetone Blank

Actual cubic fcct per minute

Dry standard cubic feet

Dry s\:ll1dard cubic feci pet minute

Dry sWlCbtd cubic mctn

SUndant cubic feet per minule

Without

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kg

Iblton

'''''"

Mg

mg

dry \"Olwnc ./.

Degrecs Fahrenheit

Kilognm

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Potmd5 per ton

Megagram

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UNION BRIOGE PlANT

.1-G:5 FEED '. i.co CLINKER ~/lO ('O.l.( 11"'Q:l.lt...O- 1e/14\')

SUBJECT: KILN ~ODLJcr/OI'J r:::c..TA DuRING ~uRCE TEST"lNGr

DATE: 10/\"'4/02

9/10 - \"3/02-

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DATE: 10/\4/02.

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7S [)oJ 1),140 GA90 1.1 21" 7' Do3 0.240 0.00 JJ 214 7$ A_[)oJ 0.140 0.490 I.J ZI4 7S 0.)" Q.6OJ 1.01 2m~ n.6

~- 41-'0.33' ICI' ....... 0.000 lilen

-- ~.IM n) -- 0.000 1itcn T__

J1U9li lebef h.... 0.000 Iclryamdliten

lqIiszer fial_ IIlilill_ anmGam lim! mJ lnltillml 1IlI0ain

I 0.0 6SU 100.0 "',0 % 0.0 uo.o 1llQ.0 30.0

1 0.0 0.0 0.0 0.0

4 297.1 l60A )6.1 0.0 , 0.0 0.0

6 0.0 0.0 ., 0.0 0.0

• 0.0 0.0 , 0.0 0.0

10 0.0 0.0

Total 291.1 250.4 36,7 llS.0 zoo.o 'UO w, WI (W,-W. V, VI (V.-VI,

Client: lAllil!l f.-DIsc: Scp!emba' It 2002 ProjecIHo: 0200468 Tall.ocaIiolI: EshwdSIKli:

PlMll: UlIlan 8ridat, MI> TalRcm: Runl UIlI: Main Kiln TaiSlIlCTcme: 8:02AM UlIilOpeftlioa: RawMUlOn TCIlFiNall'l'lmt: 11:21 PM

Bllll ildltliftpIll. Red II aC1Ib11tiolL Pialt is a ftl_loaall en"-slim. GlftD kam_loacdl Olllllil~

Rm..1alIIil CO+N1 71.00 %oIy CaalnIIBa: APBX'" w_CaIla:tE4(V,. V.) SlS.O mI Mcla D"-(O,U aeOn) 1.741 III. Up W_VapotCancIalseoI(V"C(&IoI)} 21.$16 ", Mc!crCali1lmioo F.!Of(YlS) 1.0110 WIlUCaIJmat(W,· WJ 31S.7 I TatTime (1lleta) Z40 IIlilIIIlCI WIllr Vapar illSiliuGel (V""$lol)) 1.730 "f EIanlaxlrie Prasutt (PIrat) 2US Ill. HI Va.L WIlUVapor illGoSlIDCl(Vw(Ild)) 29.166 ICf Slid SIIlicPraaw'e (Pa) -tJJO bLHP Vt!lllneDryaaM~(Vm) 179.296 dKr SlIICk DiunclzJ(0.) 164.5 indlcs Va.L IlryGuMclcftd SlaIIcL(V~$loI) '77.791 dsd NcIzdc DiImcla(DlI) 0.304 iDcllcs V"DrJrOuM~(Vm(lll)1 S.o17 dacm COl V.OO %cltf Vctl DrJrOu MtlmI:I Sl:IIId.(Vm(IId)lll') 5.034 cbcm

OZ 4.00 %rt.. SQd:Ablllzle~(h} ZU3 III.H. Pilot Tube Coeltkitm (Cp) 0.84 StIdI AlMluleT~ (Tu-a> 6n.6 R F.@6IFud760_na 0 dlc;111U"UlII H2O VIplt Plasm:@I\OI SIIICkTcqL 3US bLHI

SlmlladT~ 61 F H20 &:r lhc;as d utIlDIi<m (Bwa) 1.00ll0 YOll'iarlim

SlIIId&nIPreaure 760 -Ila H2O illlhe PIIfllllItea oIala (8",,) 0.1413 YrI1. fnclioa

H2O In lhc PI I1SCIll (Iowa of1lle ZB",,) 0.1413 YrI1. fnelioll

lbc Ou $lIamSa!lnted Willi ta01 NO PiIoI T_c.zat(Kp) 85.49 DI)a.. Mo~WeiF* (Mil) 32.16 lhIllNaole McltrT~(Tm) 77.6 F Wd au Ma!ecuIarWeidtJ(Pols) 30.16 lM!HaIllc

SlICkT~(T..YJ) 217.9 F OuVcloclly (VI) 37.86 IlII

0ri!Qrm- Drop (dllaYIl 2.010 ia.HP Ana suet(AI) 147.627 fal

f,iasVcIoctlJ ".(<11").'&\11 0.6lU2 III.Hp'11Z AcluaIGu~ JJSJ20 KIm F. @ ~CoaoIilloat 0 clrel1lU"11ll1 SIzzdudG.FIawmc 2SliMJ "1m F. @SUa. Omcl. " Aclaal OZ 0 dlc:111U"U~ DI7 SlIIIotud AU Fkrwntc no.m cbc!aI KI1llIIlllocI4 0.04101 ACIIII:I1ha FIowA!a 9,495 IClD'llll5 K2JnetbD44 0.0471' aetll SIllld:udG.. 1,,214 ICID'INa KIIIldlIooIS

~,

11.64 Rlia.H; DI)' Stmda!d Gu flowruc 6,246 cIsccMfliII 0.09U Ana Nozzhr CAD) O.OOO~ t/ SlIllQnI ~Ic \'Oluaz llS.J n)JIlHnoIe r-orzookim:lic Saqlqf1l 9UJ %

bl!lmIIll hrdml'" Asrhmt"'nk

DIy Fad Rala II> "7.01 mctI'k !OllIIIr Ac>ceoIle lIl'Uh-ma No. 16-f DlyFcalRm )95.60 tooIIIr ACItone dmsi1)' [pJ 0.7199 pi WN!) CoftIaioer No. 164 Acttoae!dzzlk YO!wm (Va) 100.0 ml FIVllllblffilla No. OOJ Filial(lalaI) wti&fd i afttt CYqIGIUiaa m,s94,60 rna Am- Wa&/) Voh=c (Vaw) 210 ml FiIIaI(_I)-;1!d2aRcl'~ 112,.594.60 me ~WuhFillal(lOIIl)Wti;llll 114,28104 ma FilIaZ(lGW)wda!dllllr_Clttlohlle ~) 0.00 rrIJ A_WubFi!lal(lOIIl)Wtfalll2 1I4,U1A ma Awnl" II:laI (1aQ1) -;&!n .fta CYIpOAlioft 112.594.60 rrIJ ~WubT...Wcll!d i 114,211.l1 ma Tlftwe!aM 1 IIU9J.6O ma AccNM WubTare Wci&llt 2 "',271.8 .... Tlnwclaht2 112,$9UO ma "-Wa&/) WclFi Olin :1..60110 JIll T... _~4IifT_(tbsoIIIecvaNe) 0.00 rna RcUchlo ia Acetol:re Wub (Wa) ""18 JIll A-etIln:'ftIaltI 11U9UO ma AmuncWubPIl1lculalc 0.9412 !Ill AftIIC fbW CtollJ)wciPllIlimD .-....., wei&IU 1.00 DlJ F......WFJ1IcrFiaaJ(lolII)Wcil!d i 404.4 ,.,. ~ofmiolac of-.-.en....,...a!klIl(mJ 1.00 rna FI'OIIt IlIIfFIlw FIa&l (tolIJ) Wci&!lt 2 -co..... ms "-blulk__~(Ca)C1I!azllled 0.0121 mwa F_lUJIfileaTmWciPlI .coo... JIll ArtfoM blaall camctlcDa. 01_.... 0.0013 % F_IbIIFilea1i#WcijftlZ .coo... ma "-1I11ft1l rtSiolac CCllICalbtIcm (Ca)=d 0.0100 mr/& FlllIIt KIlfFillaP'utlculalll U300 ma Tocal Patio;aJIIe Mal(mJ 4.4912 JIll Dte"wrppn,

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A·I 0,42 0.641 U 211 14

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A·2 0,27 0.601 2.0 211 74

A·2 o.J7 0.601 2.0 211 74

A·2 0,27 0._ 2.0 210 14

A·2 0,2S 0,592 U 210 74

A·l 0.23 0.43ll I.J 20B 74

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A.J 0.24 0.490 U 107 74

- A·l 0.24 0.490 1.2 206 7l

B.t' 0.43 0.656 2.4 204 7l

B·I 0.40 0.632 2.2 204 7l

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B-1 0.40 0.6)2 2.2 204 72

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0-2 0.40 0.632 2.2 201 7)

B-2 0.40 0.632 2.2 201 73

B·l 0.24 o.c9O 1.2 201 72

B·l 0.24 o.c9O 1.2 201 73

B·l 0.24 0,490 1.2 201 72

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Crl 0.4) 0.656 2,4 2" 72

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Co2 0.31 0.616 2.1 207 72

Co2 0.31 0.616 2.1 207 n Co2 0.31 0.616 2.1 m n Co2 0.27 0.601 2.0 m 12

C·2 o.z7 0.520 1.4 20J n Co2 o.z9 0.539 1.5 202 n Co2 0.29 0.529 I.J 202 12

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1),2 0.31 0.616 2,1 202 12

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I 0.0 sso.O 100.0 450.0

2 0.0 130.0 100.0 Jo.O

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4 29ll.9 251.2 l2.7 0.0 , 0.0 0.0

6 0.0 0.0

7 0.0 0.0

1 0.0 0.0

9 0.0 0.0

10 0.0 0.0

T..01 290.9 258,2 22.7 630.0 _0 41lO.0

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Dian: Ldlfllh TeuDate: Scp!_11,2002

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Meta C&1illn.ionF_(Yd) 1.0:110 W_CcIl<cl<d (W,. WO! 32.7 , TOIlr.... (ThctI) 240 ...- W_V_ill SlIico Od(V"'£{Sld) 1.542 ..r _P.......(",.,) 29.50 ... H. VoL W_V_ In O. SUad.(VWlSldI) 24.135 ..r S1XI<_ "'-"" (PIl -0.27 iII.H,O VoIwne Dty 0.M_(Villi 171.156 elKr

S1XI< __DiImclc«Dt) (Da) 164,5 iacllcs VoL Dtyo.MdendSlalId.(Vm(Sld)) 172.113 doer

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SltckT_(lUvai 205.1 F (]aVdodIy (Val lUI lVo

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A·2 0.41 0.648 2..2 no 75

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B-J 0.34 0.513 1.1 D2 T7

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0.3 o.JO 0.541 1.6 m 14

1).3 0.)0 0.541 1.6 m .. A_p OAO 0.02 2.12 230.6 11.2

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F, @SllD:llntCGllditiael 0 dKOlll'"lfll1 SlI2IIImIau n.- 264-''lI scfm

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