# a.

**~---** 

# -D[)_,-8

# C· ll-1-002 

# RECEIVED 'l 

### JUL 3 

## D ·i REGION 7 .

### j TfXAS AIRCONTROLBOARD___

# n Exhaust Emission Sampling Acme Brick Company **J~/** 

### Sealy, TX 

# (27_.. (t7 

### June 18, 1991 Armstrong **Environm~ntal,** 

### Inc. Project W-1059-91 Report Prepared For: Mr. Dick Ethier Acme Brick Company P.O. Box 397 Sealy, TX 77474 Report Prepared June 21, 1991 By: Armstrong Environmental, Inc.

4747 Irving Blvd. Suite 204 Dallas, Texas 75356 (214) 631-0021 AP-42 Section Reference Report Sect. Reference



# II ' I ; 

## ACME' BRICK d'mt II.PI 

### July 1, 1991 

# RECEIVED JUL 3· J991 REGION 7 TEXASAIR 

### CONTROlBOARD <; 

### Randy Hami1 ton Texas Air Control Board Permits Division .· **..._~~** 

### 6330 Hwy 290 E Austin, Tx. 78723 Dear Mr. Hamilton: This is the test that was done by Armstrong Environmental, Inc. in regard to our permit R-9540. If you have any questions, please call. Sincerely, 

# ;!~~ R. Ethier Regional Engineer cc: Jodena Henneke Region 7 INc. !I'i
**C~ry**5/-.., (

**?'""~ ;VIc..ot..._~,** 

ACMEBRICKCOMPANY ADMslond Justinlndustl1e8, Inc. D n AtW"C/7_ SEALY.TEXAS77474 - TEL:4091885-4124 I fCONTACT REPORT--MRI Project No. 4602-01 From: Date of Contact: Contacted by: Company/Agency: Telephone Number: Brian Shrager, Environmental Engineering Department April 19, 1995 Telephone Acme Brick Company (817) 382-3573 Person(s) Contacted/Title(s) Mike Vickers CONTACT SUMMARY: Mr. Vickers was contacted to obtain production rates for the 6/18/91 emission test conducted at Acme Brick in Sealy, Texas. The report stated that 16 cars per day were being produced, but did not include the number of bricks per car or the weight of a fired brick. Mr. Vickers stated that the fired bricks weighed 4 pounds each, and that each kiln car carried 14,400 bricks. These data will be used to determine the tons per hour of fired brick produced during the test. In addition, Mr. Vickers stated that the kiln scrubber is a packed bed tower that uses 1/8" to 3/8" limestone as the scrubbing media.

## I. TABLE OF CONTENTS I. INTRODUCTION II. SUMMARY III. PROCEDURES IV. APPENDICES A - CALCULATION SUMMARIES B - ANALYTICAL SUMMARIES C - FIELD DATA SHEETS D - OPACITY SHEETS E - PRODUCTION DATA F - EQUIPMENT CALIBRATIONS G - RESUMES Page 1 2-19

20 21-29 30-49 50-59 60-65 66-68 69-94 95-99

## 1.· I. INTRODUCTION A series of tests were performed on the Kiln exhaust stack and the Dryer Room exhaust stack at the Acme Brick facility in Sealy, TX on June 18, 1991. The purpose of this test series was to determine compliance with the Special Provisions of Permit R-9540. Testing was conducted following procedures detailed in Title 40: Code of Federal Regulations (40:CFR). Sampling was performed by Richard Taylor, Jerry Salinas, Larry Whicher, Tom Armstrong and Matt Taylor of Armstrong Environmental, Inc. using four NAPP Model 31 sampling trains. Sampling was performed over a seven hour period. Submitted by: Armstrong Environmental, Inc.



# ~~ Richard Taylor Project Manager RT/os 

## @

1

# a. II. SUMMARY A series of tests were performed on the Kiln exhaust and the Dryer Room exhaust at the Acme Brick facility in Sealy, TX on June 18, 1991. Sampling was performed following procedures detailed in Title 40: Code of Federal Regulations. Results of this test series are summarized in Tables 1 and 2. Witnessing the test series was Mike Vance of the Texas Air Control Board. The emission rates for Sulfur Dioxide, Hydrogen Fluoride, and Particulate Matter in lbs/hr. are as follows: 2 3 Average

RUN 

### t 1 2 3 Average KILN EXHAUST STACK POLLUTANT EMISSIONS,lb/hr ALLOWABLE Particulate 4.107 7.3 HF 0.0675 0.6 S02 12.14 28.4 Particulate 4.241 7.3 HF 0.0762 0.6 S02 12.56 28.4 Particulate 4.903 7.3 HF 0.0846 0.6 S02 12.47 28.4 Particulate 4.417 7.3 HF v--0.0761 0.6 S02 v12.37 28.4 DRYER ROOM EXHAUST STACK POLLUTANT EMISSIONS,lbs/hr ALLOWABLE S02 0.4261 0.6 HF <0.0107 0.3 S02 0.4445 0.6 HF <0.0113 0.3 S02 0.5140 0.6 HF <0.0134 0.3 S02 0.4615 0.6 HF <0.0118 0.3 2

## II.. Opacity readings were taken for three hours on the Kiln exhaust during the test repetitions. No visible emissions were detected. Test results indicate that these two sources are in compliance according to the Special Provisions of Permit number R-9540.

3 

# 7

## I. SUMMARY OF EMISSIONS TEST DATA TABLE: 1 PLANT: Acme Brick LOCATION: Kiln Exhaust OPERATOR: R. Taylor, J. Salinas TEST DATE: June 18, 1991 REPETITION: 1 STACK GAS Temperature, F Velocity, fps Volume Flow, acfm Moisture, % C02, % 02, % SAMPLE scfm scfh Start Time, hrs:min Finish Time, hrs:min Volume, scf Isokinetic Ratio % SULFUR DIOXIDE Sample Weight, mg Concentration, ppm Emissions, lb/hr HYDROGEN FLUORIDE Sample Weight, mg Concentration, ppm Emissions, lbs/hr Particulate Sample Weight, mg Concentration, gr/scf Emissions, lbs/hr OPACITY Highest 6 min. Ave. 281.2 66.41 48005 31391 1883483 8.142 3.0 18.0 9:55am 9:59am 29.367 97.33 86.24 38.94 12.14 0.2472 0.6934 0.0675 29.04 0.0153 4.107 0

4 2 282.5 65.86 47607 31225 1873479 7.705 4.0 18.0 11:42am 12:45pm 29.319 97.68 89.53 40.49 12.56 0.2775 0.7869 0.0762 30.10 0.0158 4.241 0 3 281.3 66.43 48024 31527 1891614 7.770 3.0 18.5 1:08pm 2:10pm 29.614 97.72 88.98 39.81 12.47 0.2956 0.8650 0.0846 34.81 0.0181 4.903 0

## I. SUMMARY OF EMISSIONS TEST DATA TABLE: 2 PLANT: Acme Brick LOCATION: Dryer Stack OPERATOR: L. Whicher, T. Armstrong TEST DATE: June 18, 1991 REPETITION: 1 STACK GAS Temperature, F Velocity, fps Volume Flow, acfm Moisture, % C02, % 02, % SAMPLE scfm scfh Start Time, hrs:min Finish Time, hrs:min Volume, scf SULFUR DIOXIDE Sample Weight, mg Concentration, ppm Emissions, lb/hr HYDROGEN FLUORIDE Sample Weight, mg Concentration, ppm Emissions, lbs/hr 105.8 57.71 67975 59860 3591585 5.292 0 21 8:50am 9:20am 15.450 0.824 0.7167 0.4261 <0.0212 <0.0579 <0.0107

5 2 108.5 56.39 66414 58696 3521744 4.544 0 21 9:53am !0:23am 14.522 0.824 0.7625 0.4445 <0.0213 <0.0622 <0.0113 3 108.5 56.95 67078 57914 3474850 6.748 0 21 !0:55am !1:25am 12.389 0.824 0.8938 0.5140 <0.0216 <0.0744 <0.0134

# a.

**l'=l'l~,..** 

# --·:.i 1· :; , ..

**~** ; ':- 

### ··a· 

### r.• .;, .'. •! ":_-) , I '--' L'

**-..a~ ~**  **~** 

### GENERAL PROVISIONS R-9540 MA39 5/90 

### 1. Equivalency of Methods - It shall be the responsibility of the holder of this permit to demonstrate or otherwise justify the equivalency of emission control methods, sam- pling or other emission testing methods and monitoring methods proposed as alternatives to methods indicated in the provisions of this permit. Alternative methods shall be applied for in writing and shall be reviewed and approved by the Executive Director prior to their use in fulfilling any requirements of this permit. 2. Sampling Requirements - If sampling of stacks or process vents is required, the holder of this permit must contact the Quality Assurance Division of the Texas Air Control Board (TACB) prior to sampling to obtain the proper data forms and procedures. The holder of this permit is also responsible for providing sampling facilities and con- ducting the sampling operations at his own expense. 3• Appeal - This ·permit may be appealed pUrsuant to Rule 103.81 of the Procedural Rules of the TACB and Section 382.032 of the Texas Clean Air Act. Failure to take such appeal constitutes acceptance by the applicant of all terms of the permit. 4• Construction Progress - Start of construction, construction interruptions exceeding 45 

### days and completion of construc- tion shall be reported to the appropriate regional office of the TACB not later than 10 working days after occurrence of the event. This provision shall not apply to operating permits. 5. Recordkeepinq - Information and data concerningproduction, operating hours, sampling and monitoring data, if appli- cable, fuel type and fuel sulfur content, 

### if applicable, shall be maintained in a file at the plant site and made available at the request of personnel from the TACB or any local air pollution control program having jurisdiction. The file shall be retained for at least two years following the date that the information or data is obtained. 6. Maintenance of Emission control - The facilities covered by this permit shall not be operated unless all air pollu- tion emission capture equipment and abatement equipment are maintained in good working order and operating properly during normal facility operations. 6

### 1 ..



# I SPECIAL PROVISIONS R-9540 

### 1. This permit covers only those sources of emissions listed in the attached table entitled 11

### Emission Sources - MaximUlll Allowable Emission Rates, 11 

### and those sources are limited to the emission limits and other conditions specified in that attached table. 2. Fuel fired in the brick manufacturing facility 

### is limited to pipeline quality natural gas. Use of any other fuel will require a modirication to this permit. 3. Emission from the kiln stack shall not exceed 5 percent opacity as determined by EPA Reference Method 9. The occurrence of visible emissions so determined shall also be considered a violation of the hourly particulate matter (PM) mass emission limit of Special Provision No. 1. 

### 4. The holder of this permit shall perform stack sampling and other testing as required to establish the actual pattern and quantities of air contaminants being emitted into the atmosphere from the kiln and dryer stacks. Sampling shall be conducted in accordance with appropriate procedures of the TACB Sampling Procedures Manual and EPA Reference Method 9 for opacity. The holder of this permit is responsible for providing sampling and testing facilities and conducting the sampling and testing operation at his expense. A. The TACB Regional Office 

### in Houston shall be contacted as soon as testing is scheduled but not less than 45 days prior·to sampling to schedule a pretest meeting. The notice shall include: 1. Date for pretest meeting. 2. Date sampling will occur. 3. Name of firm conducting sampling. 4. Type of sampling equipment to be used. 

## s. Method or procedure to be used in sampling. The purpose of the pretest meeting is to review the necessary sampling and testing procedures, to provide the proper data forms for recording pertinent data and to review the format procedures for submitting the test reports. A written proposed description of any deviation from sampling procedures specified in permit 7 

# -------- 

# --- ---- 

# ---- 

# /I

## I. 

# ( / I / I

( 

# DRAFT provision or TACB or EPA sampling procedures shall be made available to the TACB at or prior to the pretest meeting. The Regional Director or the Director of the Quality Assurance Division may approve or disapprove of any deviation from specified sampling procedures•. Requests to waive testing for any pollutant specified in B or 

## c of this provision shall be submitted to the TACB Permits Program. B. 

### Air contaminants to be tested for from the kiln exhaust stack include (but are not limited to) HF, 

## so2 

### and PM. 

## c. Air contaminants to be tested for from the dryer room exhaust include (but are not limited to) HF 

### and 

## so2• 

### D. Sampling shall occur within 60 

### days after achieving the new maximum production rate of 16 

### cars/day, but no later than 180 

### days after initial startup of the kiln following the completion of construction on the plant expansion. If 

### the normal production rate exceeds by more than 10 

### percent the rate maintained during sampling, the company must notify the 

### Regional Director in Houston and the 

### TACB may require additional sampling to demonstrate continued compliance with the emission limits of this permit. E. Two copies of the sampling report shall be forwarded to the TACB within 30 

### days after sampling is completed. Sampling reports shall follow the format requirements of Chapter 14 

### of the TACB Sampling Procedures Manual. The reports shall be distributed as follows: One copy to the TACB Regional Office in Houston. one copy to the Permits Program, TACB Austin Office. 5. Hydrogen fluoride shall be sampled at the exit of the dry scrubber. The use of stain tube indicators or a portable analyzer specifically designed for measuring HF concentration in ppmv is acceptable for this evaluation. Any other method approved by the Regional Director or the Quality Assurance Division is also acceptable. A hot air probe or equivalent should be used with stain tubes to prevent introduction of error in results becuase of high stack temperatures. With stain tubes, three readings should be averaged to obtain one result. commencing upon initial startup of the dry scrubber, sampling shall be conducted on a weekly basis and shall 8 

## ----· ·---------- 

# /}

# a. .·. / /' BY:TACB 9-20-90 ;11:56AM 03.... 713 346 1159;# 5 

# D·RAFT continue at this frequency for the first month of operation. Then, if these results consistently indicate scrubber outlet HF concentrations less than 7 ppmv (4 ppmv at maximum kiln air flow), the sampling shall be performed at least monthly. These measurements will be used as an indicator of compliance. If the measured concentration is above 7 ppm HF, the TACB shall be notified as soon as practical and additional testing may be required. 6. Kiln exhaust shall be routed through the scrubber during all periods of kiln operation. Any bypassing of the scrubber or scrubber malfunction that may cause excessive emissions shall be reported to the Houston Regional Office as soon as practical, but not later than one week after such occurrence. Each report shall include a discussion of the conditions that necessitated the bypassing or caused the malfunction. If a full bed of limestone is not maintained, HF emission sampling shall be conducted daily during the period until the supply is r.eplenished. 1. 

### The following information shall be made and maintained by the source for a period of two years on a rolling retention basis and shall be made available on request to representatives of the TACB or EPA or any local air pollution control program having jurisdiction: A. The results of all HF emission indication tests of the scrubber exhaust. B. Any period of kiln operation during which the scrubber is bypassed. 

## c. Limestone consumption of the dry scrubber.

9

## 13. 'fl,j,j40 ll:l::t;+;o EMISSION SOURCES - MAXIMUM ALLOWABLE EMISSION RATES R-9540 

### his table lists the maximum allowable emission rates and all sources of air contaminants on the-applicant's property covered by this permit. The emis- sion rates shown are those derived from information submitted as part of the application for permit and are the maximum rates allowed for these facil- ities. Any proposed increase in emission rates may require an application

or a modification of the facilities covered by this permit.
(1) (2) (3) (4) 

### Kiln Exhaust Stack W/ Dry Scrubber Dryer Room Exhaust AIR CONTAMINANTS 

### DATA Air Contaminant Na 3 S02 (4) HF (4) 

### PM 

## co voc NOx -S02 HF 28.4 0.6 7.3 

### 1.2 0.2 3.5 0.6 0.3 68.9 2.5 32.0

5.2 

### o.s 15.5



### 2.7 1.4 Emission point identification - either specific equipment designation or emission point number from plot plan. Specific point source name. VOC - volatile organic compounds as defined in General Rule 101.1 NOx - total oxides of nitrogen S02 - 

### sulfur dioxide

PM - particulate matter as defined in General Rule 101.1 

## co - carbon monoxide Hourly rates derive from highest one-hour emission rate measured; annual rates derive from average of three one-hour emission rate measurements. Emission rates are based on and the facilities are limited by the following maximum operating schedule:

**Hrsjday~2~4** 

### ______Daysjweek._.7 ______ weeksfyear __

**s~2--** 

## __or Hrs/year ____ **~s~7~6~o**

### __ __ 

# IJ:BAFT 10



# \~

## I. Company Name.__ ..;;.;A;.;;.cme.;;;;.;;......;B;;;.;r;..;i;..;c;...k;.._ ________ TACB Account No._________ _ City __ Se_a_l 4 Y

__________ county Austin TACB Region ___ ? ____ _ Testing required by:___ **T_~_CB** __________________________ __ TACB Pennit No. R 9540 PSD Pennit No ·------...:NSPS SUbpart ______ _ (INCLUDE A COPY OF PERMIT SPECIAL PROVISIONS) Source Tested Kiln Exhaust Stack TACB E. I. Point No. 1 

# ------- Stack Height ____ **~7~2....;f~t~·;..._**__________ ___:Stack Diameter ____ **,_·_~4..;;.;7...:i=n=ch==e=s**___ ___ SAMPLING PORTS LOCATION: Downstream Distance to Obstruct:i.on:--_....;1;...9_f_t_._ Upstream Distance to Obstruction 22.5 ft. Checked for cyclonic flow?_x_Yes __ No Cyclonic flow present? __ Yes...x__No (INCLUDE A DRAWING OF 5rACK SHOW!ro SAMPLING PORTS & MEASURn1ENTS) Design Operating Rate:---------------...:Maximum Operating Rate 16 cars/day Normal Operating Rate Operating Schedule 8760 hrs/day TACB Test Observer ___ **~Mi='=ke~V~an==ce~-------------**

11

# I. Company Name. _ ___;;A:.;..cm_e_B_r_ic_k __________ TACB Account No.__________ _ City Sealy County ___ **A.;..u_s~t~i~n** 

### _____ TACB
**Region.-~7~------** 

### Testing required by:___ T_A:_CB _________________________ __ TACB Permit No. R 9540 PSD Permit No._______ ..,:NSPS Subpart ______ _ (INCLUDE A COPY OF PERMIT SPECIAL PROVISIONS) Source Tested. __ **....;;D;.;;ry~er.;;.....;R;;.;.oo;...;;.;;m__;;Exha;;...__us_t** 

### _________ TACB E. I. Point No._2 _____ _ Stack

**Height~**

### ____ 65_f_t_. ________ **~Stack** 

### Diameter ___ 6_0_in_c_h_e_s ____ _ SAMPLING PORTS 

### LOCATION: Downstream Distance to Obstruction 23 ft. Upstream Distance to Obstruction 40 

### ft• Checked 

### for cyclonic

**flow?~Yes** 

### __ No Cyclonic flow present? __ Yes_x_No (INCLUDE A DRAWING 

### OF STACK SHOWIN; SAMPLING PORTS & MEASUREMENTS) 

### Design Operating **Rate~---------~Maximum** 

### Operating Rate 16 cars/day Normal Operating Rate Operating Schedule 8760 hrs/year TACB Test **Observer_~Mi-·~k~e_V.;..an~ce~----------**



### 12

# a. FIGURE I

.C7" 

### 0

13 22.5'

1!r 

### ACME BRICK KILN EXHAUST



# 17

## I. FIGURE II 

## AQ.AE BRICK DRYER STACK 6011 

## 0 23'

14

# a. ' ) 1 ·j ., 

### Pollutant Sampled: .PM· KILN 

### Exhaust **--------~~~~~-------------------------** 

### Run No. Run No. · Run No. Run No. 

## ,. Results Date Sampled 6/18/91 6/18/91 . 6/18/91 

# ><

**~~** 

# ~

# ~**~** 

# ~ Time - 0:59an: 5p lQpm 

### No. of Points Sampled 

### I 

## I

**~** 24 24 I 24 I 

# _,.,- --.......... • I 

### Operating/Feed Rate 16 

### cars/day 16 

### cars/day 16 

### cars/day! 16 

### cars/day !

**~** 

### Operating Rate (Maximum) 100 100 100 

## i 100 

### Stack Temperature 281.2 282.5 281.3 281.7 

### Stack Flow Rate (DSCFM) 31391 31225 31527 31381 

### Percent Moisture 8.142 7.705 7.770 7.872 

### Percent Oxygen 18 18 18.5 

# ' 18.17 

### Percent Carbon Dioxide 

# I 3 4 3 3.333 

### Percent Isokinetic 97.33 97.68 97.72 

# I 97.577 

### Excess Air 630.3 694.4 831.3 718.8 

### Pollutant Concentration9f'cf I 0.0153 0.0158 . 0.0181 

### i 0.0164 I 

# ' I 

### Mass Emission Rate, ·Lbs/hr 4.107 4.241 t 

# , 4.417 

### 14.903 I i 

### Emissions (NSPS Units) 

# -- 

# ----- 

# ------1 - I

. I 

# ------ TACB Permit Allowable Rate 7.3 

### lbs/hr g.3 

### lbs/hr 7.3 

### lbs/hr' 

# I 7.3 

### lbs/hr 

## -· 

# ----1 NSPS Allowable Emissions 

## - 

# ---- 

# ------ Regulation Allowable Rate 

# ---- 

# ------ ------- ------ TACB Regulation No. 

# ------ ------- -------- ------- Pre 

### Date Post
. Dry Gas Meter Calibrated 6/11/91 6/19/91 

### Pitot Tube Calibrated 6/19/91 

### Nozzle Calibrated 6/18/91 ' 15 

# ;qI ., ., I ·, 

### Pollutant Sampled: . HF KILN EXHAUST 

### Run No. Run No. · Run No. Date Sampled 6/18/91 6/18/91 6/18/91 

### Time


## 9.~ _ 0:25am


# ~ m

# ~ 3_E!1 

### No. of Points Sampled 1 1 

### I 1 I I • I 

### Operating/Feed Rate 16 cars/day 16 cars/day 16 cars/day

### f

**~** 

### Operating Rate (Maximum} 100 100 

### Stack Temperature 281.2 282.5 

### Stack Flow Rate (DSCFM) 31291 31225 

### Percent Moisture 8.142 7.705 

### Percent Oxygen 18 18 

### Percent Carbon Dioxide 

# I3 4 

### Percent Isokinetic 

# ---- 

# --- Excess Air 630.3 694.4 

### Pollutant Concentration,

**p~** 0.6934 0.7869 

### Mass Emission Rate,-Lbs/hr 0.0675 0.0762 

### Emissions (NSPS Units) 

# ----- -----. TACB Permit Allowable Rate 0.6 0.6 

## -· NSPS Allowable Emissions 

# -- 

# ------ Regulation Allowable Rate 

# ---- ------ TACB Regulation No. 

# ----- ------- Pre 

### Date
. Dry Gas Meter Calibrated 6/13/91 

### Pitot Tube Calibrated 6/19/91 

### Nozzle Calibrated 6/18/91 16 ! 100 

# 1 281.3 31527 7.770 18.5 

# ' 3 

## I 

# ----- 831.8 I ,0.8650 

### j I l I 

## f f0.0846



# ·---~ 0.6 

# , ----1
----- ------ Post 6/19/91 

### Run No. ,. Results



### ~ 

# _,_.,- --...........



# ~

# >< 

# >< 16 cars/day 100 281.7 31381 7.872 18.17 3.333 

# ------ 718.8 0.7816 I 

### 1o.o761 

# '------- I 

# Io.6



# ------ 

# -------- -------

## £!. I

**-~** 

### Pollutant Sampled: .S02· 

# ------------------------------------------- KILN EXHAUST 

### Run No. Run No. · Run No. Run No. ,. Results Date Sampled



# ~ 6/18/91 6/18/91 6/18/91



# ~~ 11:4?::>m ___.



# ~ 

# ">< Time


### ~45PJ _ 0:59am



# ~- **Op~** No. of Points Sampled 

### I 

## t **~** 24 24 24 I 

# _...,..,- -............. • I 

### Operating/Feed Rate 16 cars/day 16 cars/day 16 cars/day! 16 cars/day !

**~** 

### Operating Rate (Maximum) 100 100 100 

## i 100 

### Stack Temperature 281.2 282.5 281.3 281.7 

### Stack Flow Rate (DSCFM) 31391 31225 31527 31381 

### Percent Moisture 8!h42·:-
**7:.76s~= 1~~Tf6C**  1:.81ii·-· 

### Percent Oxygen 18 18 18.5 18.17 

### Percent Carbon Dioxide 

# I 3 4 3 3.333 

### Percent Isokinetic 97.33 97.68 97.72 

## I 97.577 

### Excess Air 630.3 694.4 831.8 718.8 

## ' Pollutant Concentration, PPM 38.94 10.49 39.81 i 39.75 ! I 

# ' I 

### Mass Emission Rate,·Lbs/hr 12.14 12.56 

# i 12.47 

# ; I 12.37 i 

### Emissions (NSPS Units) 

# I 

# ' -- 

# ----- 

# ---- ------ TACB Permit Allowable Rate 28.4 28.4 28.4 

# ' I 28.4 

# -- NSPS Allowable Emissions 

# ---- ----- ---- 

# I ------ Regulation Allowable Rate 

# ------ 

# ---- -------- ------- TACB Regulation No. 

# ------ 

# ------ ------- ------- Pre 

### Date Post · Dry 

### Gas Meter Calibrated 6/11/91 

# -------------------- 6/19/91 

### Pitot Tube Calibrated 6/19/91 

### Nozzle Calibrated 6/18/91 17 

# cJ-1**Pollut~nt** 

### Sampled: DRYER STACK

**so~** 

### Run No. Run No. Run No. . 

### Run No. 

### .. Date Sampled 6/18/91 6/18/91 6/18/91 . 

### Time



# ~ ..,.. 9:20am



# ~ am 

# ~~ 1:25am ! I 

### No. of Points Sampled 16 16 

### 1 16 1 I 

### Operating/Feed Rate 16 cars/da} 16 cars/day 

### i 16 cars/dayj

**~** 

### Operating Rate (Maximum) 100 100 

### Stack Temperature 105.8 108.5 

### Stack Flow Rate (DSCFM) 59860 58696 

### Percent Moisture 5.292 4.544 

### Percent Oxygen 

# I 21 21 

### Percent Carbon Dioxide 

# I 0 0 

### Percent Isokinetic 

# ---- - -- Excess Air 

# ---- ------- Pollutant Concentration,PPM 0.7167 0.7625 

### Mass Emission Rate, ·Lb6/hr 0.4261 0.4445 

### Emissions (NSPS Units) 

# --- ------- TACB Permit Allowable Rate 0.6 0.6 

# ·- NSPS Allowable Emissions 

# --- 

# I----- Regulation Allowable Rate 

# ---- ----- TACB Regulation No. 

# ----- ------- Pre 

### Date

- Dry Gas Meter Calibrated 6/11/91 

### Pitot Tube Calibrated 6/19/91 

### Nozzle Calibrated 6/18/91 18 ! 100 

## i 108.5 57914 

# ' 6.748 

### I 21 

# I 0 

## .I 

# ------ ------- .o. 8938 

# ! I I 

# i0.5140 I ! i



# --------~

0.6


# ----- 

# I I 

# ------- 

# ---------- Post 6/19.91 I i I 

# 1 

# l Results



# ~ 

# >< 

# ><

16 cars/day 100 107.6 58823 5.528 21 0


# ----- -------- {) 7Ql 0.4615


# ---------- 0.6 

# I

---------- 

# --------- ----------

## I. Run No. Run No. Run No. . 

### Run No. " 

### Results Date Sampled 6/18/91 6/18/91 

# :::><: nme



# ~~ -

**~q~?n~m** 

# ~ **·?":l~m** 

## ~· 1



## ~ ;::.m 

# >-<:::::: ! 

### i No. of Points Sampled 16 16 i 16 I 

# . I 

## i Operating/Feed Rate 16 cars/da' 16 cars/day 16 cars/davi !

**~** 

### Operating Rate (Maximum) 100 100 100 

# ; Stack Temperature 105.8 108.5 108.5 

### Stack Flow Rate (OSCFM) 59860 58696 57914 f 

### Percent Moisture 5.292 4.544 6.748 

### I Percent Oxygen 21 21 21 J 

### Percent Carbon Dioxide 

### f 0 0 0 

### Percent Isokinetic 

## .I 

## - 

# --- 

# - - --- t Excess Air 

# ----- -------- 

# ------1 Pollutant Concentration,PPM <.0.0579

**~0.0622** 

### Mass Emission Rate, LbS/hr <0.0107

**~.0113** 

### . Emissions (NSPS Units) 

# ---- -----

TACB Permit Allowable Rate 0.3 0.3 

### -· NSPS Allowable Emissions 

## - 

# -- Regulation Allowable Rate 

# ------ TACB Regulation No. 

# ----- ----- Pre


### . Dry Gas Meter Calibrated 6/10/91 

### Pitot Tube Calibrated Nozzle Calibrated 19 

### Date 6/19/91 6/18/91 l ·ko.o744 

## !

i i I j(0.0134 ! I 

## (



# ------- 0.3


# ----- 

# I : ------
----- Post 6/19/91 

# >< 1 F.

**,-.::~rc:::** /t'!=!v 100 107.6 58823 5.528 

# I 21

0



## ------


# -------- (0.065 I i<0.0118 

## I 

# ------- 

# I 0.3 

# I

------
--------


# ---------

## I. III. PROCEDURES The procedure for emissions sampling followed USEPA test methods as detailed in Title 40: Code of Federal Regulations. The following methods were used: Method 1 2 3 4 

### 5 Title Sample and Velocity Traverses from Stationary Sources Determination of Stack Gas Velocity and Volumetric Flow {Type S Pitot) Gas Analysis for C02, 02, Excess Air and Dry Molecular Weight Determination of Moisture Content in Stack Gas Determination of Particulate Emissions from Stationary Sources 6 Determination of Sulfur Dioxide Emissions from Stationary Sources 9 Visual Determination of the Opacity of Emissions from Stationary Sources C02 and 02 were determined using a Fyrite analyzer Hydrogen Fluoride was determined following Method 13 ; Flouride in Stack Gases in the Texas Air Control Board's Laboratory Methods Manual. S02 and particulate testing was conducted on the Kiln exhaust stack for 2.5 minutes at each of 24 points, 12 points per traverse using a 60 inch glass lined sampling probe with a 0.1883 inch ID stainless steel nozzle and a NaPP Model 31 Method 5 sampling train. Hydrogen Fluoride was conducted on the Kiln exhaust using a seperate sampling train with a 36 inch stainless steel probe with a 0.5 inch stainless steel nozzle positioned in the middle of the stack pulling at a constant rate for 30 minutes. Hydrogen flouride and S02 sampling was conducted on the Dryer Room exhaust stack using two seperate sampling trains pulling at a constant rate for 30 minutes. A five foot stainless steel sampling probe with a 0.4375 inch ID nozzle was used for HF sampling and a five foot glass lined probe with a 0.5 inch ID sampling nozzle was used for S02 sampling. A 16 point velocity traverse was taken prior to each test run. 20

## I.

APPENDIX A

## fJ. ACME BRICK KILN EX. 6118191 Repetition # 1 SAMPLE VOLUME, STANDARD CUBIC FEET (((HI13.6) I TM) * Y * VM * 17.64 

### = 29.36731 VOLUME OF WATER VAPOR, STANDARD CUBIC FEET VLC * 0.04707 

### = 2.602971 FRACTIONAL MOISTURE CONTENT VWSTD I {VMSTD + VWSTD) 

### = 8.141846E-02 PARTICULATE CONCENTRATION, GRISCF DB {MNIVMSTD) * 0.01543 = 1.525803E-02 PARTICULATE CONCENTRATION, LBSISCF DB (MNIVMSTD) *

**2.205~-06** 

### = 2.180425E-06 MOLECULAR WEIGHT OF STACK GAS, DRY BASIS (C02 * .44) + ( 02 

## * .32} + ( ( N2 + CO} * .28} 

## = 29.2 MOLECULAR WEIGHT OF STACK GAS, WET BASIS (MD * (1- BWS}} + (18 * BWS} 

## = 28.28811 STACK PRESSURE, INCHES OF MERCURY (SP I 13.6} + PBAR 

### = 29.8603 STACK GAS VELOCITY, FPS (SQR(((TS + 460} I MS} IPS}) * CP * DP * 85.49 

### = 66.4077 STACK GAS VOLUME, ACFM V * AS * 60 

### = 48004.8 STACK GAS VOLUME, SCFH (((528*PBAR}I(TS+460}129.92)) *AS*V*(1-BWS) * 3600 = 1883483 PARTICULATE EMISSIONS, LBSIHR CS * QS = 4.106793 ISOKINETIC RATIO, % ((VMSTDI17.64}+(.002669*VLC)}IANIVIPSIT*(TS+460)*1.667 

## = 97.32756 EXCESS AIR 

## = 630.2523 21

## I. ACME BRICK KILN EX. 6/18/91 Repetition # 

### 1 PRESSURE DROP ACROSS ORIFICE, H 

### = .8745 METER CO-EFFICIENT, Y = 

### .968129 METER TEMPERATURE, TM 

### = 100.77 BAROMETRIC PRESSURE, PBAR 

### = 29.9 GAS METER VOLUME, VM 

### = 32.182 LIQUID COLLECTED, VLC 

### = 55.3 PARTICULATE SAMPLE WEIGHT, MN = 

### 29.04 STATIC PRESSURE, SP 

### = -.54 STACK TEMPERATURE, TS 

### = 281.2 PITOT CO-EFFICIENT, CP 

## = .84 SQUARE ROOT OF DELTA P; DP 

### = .9872 AREA OF STACK, AS 

## = 12.048 TEST DURATION, T 

### = 60 AREA OF NOZZLE, AN 

### = 1.933872E-04 C02 % = 3 02 % = 

### 18 

### co % 

## = 0

22 

# ;)7

## C.

,. ACME BRICK KILN EX. 6118191 Repetition # 2 SAMPLE VOLUME, STANDARD CUBIC FEET (((HI13.6) I TM) * Y * VM * 17.64 

### = 29.31967 VOLUME OF WATER VAPOR, STANDARD CUBIC FEET VLC * 0.04707 

### = 2.44764 FRACTIONAL MOISTURE CONTENT VWSTD I (VMSTD + VWSTD} 

### = 7.704903E-02 PARTICULATE CONCENTRATION, GRISCF DB (MNIVMSTD} * 0.01543 =· 1.584067E-02 PARTICULATE CONCENTRATION, LBSISCF DB (MNIVMSTD} * 2.205A-06 

## = 2.263686E-06 MOLECULAR WEIGHT OF STACK GAS, DRY BASIS {C02 * .44} + { 02 * .32) + { { N2 + CO} * .28} 

## = 29.36 MOLECULAR WEIGHT OF STACK GAS, WET BASIS {MD* {1- BWS}) + {18 * BWS) 

## = 28.48473 STACK PRESSURE, INCHES OF MERCURY {SP I 13.6} + PBAR 

### = 29.86287 STACK GAS VELOCITY, FPS {SQR{ ( {TS + 460} I MS} I PS}) * CP * DP * 85.49 = 65.85755 STACK GAS VOLUME, ACFM V * AS * 60 = 47607.11 STACK GAS VOLUME, SCFH {({528*PBAR)I(TS+460)129.92)} *AS*V*{l-BWS) * 3600 

## = 1873479 PARTICULATE EMISSIONS, LBSIHR CS * QS 

### = 4.240967 ISOKINETIC RATIO, % {(VMSTDI17.64}+{.002669*VLC))IANIVIPSIT*(TS+460}*1.667 = 97.68002 EXCESS AIR = 694.4447 23

## I. ACME BRICK KILN EX. 6/18/91 Repetition # 2 PRESSURE DROP ACROSS ORIFICE, H 

### = .8829 METER CO-EFFICIENT, 

### Y 

### = .968129 METER TEMPERATURE, TM 

## = 104.66 BAROMETRIC PRESSURE, PBAR 

### = 29.9 GAS METER VOLUME, VM 

### = 32.352 LIQUID COLLECTED, VLC 

### = 52 PARTICULATE SAMPLE WEIGHT, MN 

## = 30.1 STATIC PRESSURE, SP = -.505 STACK TEMPERATURE, TS 

### = 282.5 PITOT CO-EFFICIENT, CP 

### = .84 SQUARE ROOT OF DELTA P, DP 

## = .9816 AREA OF STACK, AS = 12.048 TEST DURATION, T 

### = 60 AREA OF NOZZLE, AN 

## = 1.933872E-04 C02 % = 4 02 % 

### = 18 

### co % 

### = 0

24

## I. ACME BRICK KILN EX. 6118191 Repetition # 3 SAMPLE VOLUME, STANDARD CUBIC FEET (((HI13.6) I TM) * Y * VM * 17.64 

### = 29.61394 VOLUME OF WATER VAPOR, STANDARD· CUBIC FEET VLC * 0.04707 

### = 2.49471 FRACTIONAL MOISTURE CONTENT VWSTD 

### I (VMSTD + VWSTD) = 7.769588E-02 PARTICULATE CONCENTRATION, GRISCF DB (MNIVMSTD) * 0.01543 

### = 1.813735E-02 PARTICULATE CONCENTRATION, LBSISCF DB (MNIVMSTD) * 2.205A-06 

## = 2.591889E-06 MOLECULAR WEIGHT OF STACK GAS, DRY BASIS (C02 * .44) + ( 02 * .32) + ( ( N2 + CO) * .28) = 29.22 MOLECULAR WEIGHT OF STACK GAS, WET BASIS (MD* (1- BWS)) + (18 

## * BWS) 

### = 28.34825 STACK PRESSURE, INCHES OF MERCURY (SP 

### I 13.6) + PBAR = 29.86176 STACK GAS VELOCITY, FPS (SQR(((TS + 460) 

### I MS) IPS)) * CP * DP * 85.49 

## = 66.43415 STACK GAS VOLUME, ACFM V * AS * 60 

## = 48023.92 STACK GAS VOLUME, SCFH (((528*PBAR)I(TS+460)129.92)) *AS*V*(1-BWS) * 3600 

## = 1891614 PARTICULATE EMISSIONS, LBSIHR CS 

### * QS 

### = 4.902853 ISOKINETIC RATIO, % ((VMSTDI17.64)+(.002669*VLC))IANIVIPSIT*(TS+460)*1.667 

## = 97.7182 EXCESS AIR = 831.8349 25

## D. ACME BRICK KILN EX. 6/18/91 Repetition # 

### 3 PRESSURE DROP ACROSS ORIFICE, H 

### = .9071 METER CO-EFFICIENT, Y 

### = .968129 METER TEMPERATURE, TM = 

### 102.4 BAROMETRIC PRESSURE, PBAR = 

### 29.9 GAS METER VOLUME, VM = 

### 32.544 LIQUID COLLECTED, VLC 

### = 53 PARTICULATE SAMPLE WEIGHT, MN 

## = 34.81 STATIC PRESSURE, SP = 

### -.52 STACK TEMPERATURE, TS 

### = 281.3 PITOT CO-EFFICIENT, CP = 

### .84 SQUARE ROOT OF DELTA P, DP = 

### .9886 AREA OF STACK, AS 

## = 12.048 TEST DURATION, T 

### = 60 AREA OF NOZZLE, AN 

### = 1.933872E-04 C02 % = 

### 3 02 % = 

### 18.5 

### co % = 0

26 

# 3/

## I. ACME BRICK DRYER STACK REPETION # 1 6/18/91 MOLECULAR WEIGHT OF STACK GAS, DRY BASIS, MD (.44 

### * %C02) + (.32 *% 02) + (.28 * (N2 +CO))= 28.84 MOLECULAR WEIGHT OF STACK GAS, WET BASIS, MS MD 

## * (1 - BWS) + (18 

## * BWS) = 28.2664 STACK GAS PRESSURE, IN HG, PS PBAR + (STATIC/13.6) = 29.81177 STACK GAS VELOCITY, FPS 85.49 

## * CP 

## * (SQR P(TS 

### I (PS 

## * MS))) = 57.7135 VOLUME FLOW RATE, ACFM 60 

## * AS 

## * VS = 67974.95 VOLUME FLOW RATE, SCFH 3600 

## * (1- BWS) * VS *AS* ((528 * PBAR) I (TS 

## * 29.92)) 

### = 3591585 %C02 = 0 %02 = 21 %CO 

### = 0 %N2 

## = 79 STACK TEMPERATURE, F 

### = 105.8 SQUARE ROOT OF DELTA P 

## = .9808 STATIC PRESSURE, IN H20 = -1.2 BAROMETRIC PRESSURE, IN HG = 29.9 PERCENT WATER VAPOR (BWS 

## * 100) = 5.2915 AREA OF STACK, SQUARE FT. = 19.63 PITOT CO-EFFICIENT, CP = .84

27

## £!. ACME BRICK DRYER STACK REPETION # 2 6118191 MOLECULAR WEIGHT OF STACK GAS, DRY BASIS, MD (.44 * %C02) + (.32 *% 02) + (.28 * (N2 +CO)) 

### = 28.84 MOLECULAR WEIGHT OF STACK GAS, WET BASIS, MS MD 

### * (1 - BWS) + (18 * BWS) 

## = 28.34748 STACK GAS PRESSURE, IN HG, PS PBAR + (STATICI13.6) = 29.82647 STACK GAS VELOCITY, FPS 85.49 * CP * (SQR P(TS I (PS * MS))) 

## = 56.38788 VOLUME FLOW RATE, ACFM 60 * AS * VS 

## = 66413.65 VOLUME FLOW RATE, SCFH 3600 * (1- BWS) * VS *AS * ((528 * PBAR) 

### I (TS 

## * 29.92)) 

### = 3521744 %C02 = 0 .%02 

## = 21

%CO 

## = 0 %N2 

## = 79 STACK TEMPERATURE, F 

## = 108.5 SQUARE ROOT OF DELTA P 

## = .9576 STATIC PRESSURE, IN H20 

## = -1 BAROMETRIC PRESSURE, IN HG 

### = 29.9 PERCENT WATER VAPOR (BWS 

## * 100) 

### = 4.5435 AREA OF STACK, SQUARE FT. 

### = 19.63 PITOT CO-EFFICIENT, CP 

## = .84

28

# a. ACME BRICK DRYER STACK REPETION # 3 6/18/91 MOLECULAR WEIGHT OF STACK GAS, DRY BASIS, MD (.44 * %C02) + (.32 * % 02) + (.28 * (N2 + CO)) 

## = 28.84 MOLECULAR WEIGHT OF STACK GAS, WET BASIS, MS MD * (1 - BWS) + (18 * BWS) 

## = 28.10852 STACK GAS PRESSURE, IN HG, PS PBAR + (STATIC/13.6) = 29.82647 STACK GAS VELOCITY, FPS 85.49 * CP * (SQR P(TS I CPS* MS))) = 56.95231 VOLUME FLOW RATE, ACFM 60 * AS * VS 

### = 67078.43 VOLUME FLOW RATE, SCFH 3600 * (1- BWS) * VS *AS 

## * ((528 

## * PBAR) 

### I (TS 

## * 29.92)) = 3474850 %C02 = 0 %02 

## = 21 . %CO 

## = 0

%N2 

## = 79 STACK TEMPERATURE, F = 108.5 SQUARE ROOT OF DELTA P 

## = .9631 STATIC PRESSURE, IN H20 

## = -1 BAROMETRIC PRESSURE, IN HG 

## = 29.9 PERCENT WATER VAPOR (BWS * 100) 

## = 6.748 AREA OF STACK, SQUARE FT. 

## = 19.63 PITOT CO-EFFICIENT, CP 

## = .84

29

## I.

APPENDIX B

## C.
S02 Data Reduction ACME BRICK KILN EX. 6118191 Repetition 1 Volume of sample, VM STD (((HI 13.6) + .PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

### = 29.36731 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

## = 2.602971 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 8.141846 % S02 concentration, lbslscf (MN I VMSTD) 

## * 2.205

**~** 10-6 = 6.475201E-06 LBSISCF S02 Concentration, ppm (385.2 I MW) 

## * LBSISCF 

## = 38.93611 PPM Delta H, H 

## = .8745 Inches H20 Meter Temperature 

### = 100.77 F Barometric Pressure, PBAR 

### = 29.9 inches HG Meter Volume, VM 

## = 32.182 CU. FT. Meter Co-efficient, 

### Y 

### = .968129 Liquid collected, VLC 

## = 55.3 MLS Sample weight, MN 

## = 86.24 MG S02 Molecular Weight = 64.06

30

## C. HF Data Reduction ACME BRICK KILN EX. 6118191 Repetition 1 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 = 15.13946 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

### = .9978841 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 6.183695 % HF concentration, lbslscf (MN 

### I VMSTD} 

## * 2.205 A 10-6 

## = 3.600366E-08 LBSISCF HF Concentration, ppm (385.2 I MW) 

## * LBSISCF 

## = .6934305 PPM Delta H, H = 1 Inches H20 Meter Temperature = 95.67 F Barometric Pressure, PBAR 

## = 29.9 inches HG Meter Volume, VM 

### = 16.409 CU. FT. Meter Co-efficient, Y 

## = .969636 Liquid collected, VLC 

### = 21.2 MLS Sample weight, MN 

## = .2472 MG HF Molecular Weight 

### = 20**~1** 

# 37

# a. S02 Data Reduction ACME BRICK KILN EX. 6118191 Repetition 2 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

## = 29.31967 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

### = 2.44764 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 7.704903 % S02 concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 

## = 6.733149E-06 LBSISCF S02 Concentration, ppm (385.2 I MW) 

## * LBSISCF 

### = 40.48718 PPM Delta H, H 

### = .8829 Inches H20 Meter Temperature = 104.66 F Barometric Pressure, PBAR = 29.9 inches HG Meter Volume, VM = 32.352 CU. FT. Meter Co-efficient, 

### Y 

### = .968129 Liquid collected, VLC = 52 MLS Sample weight, MN 

### = 89.53 MG S02 Molecular Weight 

### = 64.06

32

## 1.. HF Data Reduction ACME BRICK KILN EX. 6118191 Repetition 2 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

## = 14.97613 DSCF Volume of water vapor, VWSTD VLC 

### * 0.04707 

### = 1.275597 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) = 7.848991 % HF concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 = 4.085751E-08 LBSISCF HF Concentration, ppm (385.2 I MW) 

## * LBSISCF 

## = .7869156 PPM Delta H, H = 1 Inches H20 Meter Temperature 

## = 108.2 F Barometric Pressure, PBAR = 29.9 inches HG Meter Volume, VM = 16.598 CU. FT. Meter Co-efficient, 

### Y 

## = .969636 Liquid collected, VLC = 27.1 MLS Sample weight, MN 

## = .2775 MG HF Molecular Weight = 20

33 

# 39

## I. S02 Data Reduction ACME BRICK KILN EX. 6118191 Repetition 3 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

### = 29.63291 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 = 2.49471 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 7.765 % S02 concentration, lbslscf (MN 

### I VMSTD) 

## * 2.205 A 10-6 = 6.621047E-06 LBSISCF S02 Concentration, ppm (385.2 

### I MW) 

## * LBSISCF = 39.8131 PPM Delta H, H 

## = .9071 Inches H20 Meter Temperature = 102.04 F Barometric Pressure, PBAR 

### = 29.9 inches HG Meter Volume, VM 

## = 32.544 CU. FT. Meter Co-efficient, Y 

## = .968129 Liquid collected, VLC 

## = 53 MLS Sample weight, MN 

## = 88.98001 MG S02 Molecular Weight 

## = 64.06

34HF Data Reduction ACME BRICK KILN EX. 6118191 Repetition 3 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

## = 14.5132 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

### = 1.073196 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 6.885466 % HF concentration, lbslscf (MN I VMSTD) 

## * 2.205

**~** 10-6 

### = 4.491071E-08 LBSISCF HF Concentration, ppm (385.2 

### I MW) 

## * LBSISCF 

### = .8649802 PPM Delta H, H 

### = 1 Inches H20 Meter Temperature 

### = 112.83 F Barometric Pressure, PBAR 

## = 29.9 inches HG Meter Volume, VM 

## = 16.216 

## cu. FT. Meter Co-efficient, 

### Y = .969636 Liquid collected, VLC 

### = 22.8 MLS Sample weight, MN 

## = .2956 MG HF Molecular Weight = 20

35

# a. S02 Data Reduction ACME BRICK DRYER STACK 6118191 Repetition 2 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

### = 14.32813 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

### = .513063 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

### = 3.45702 % S02 concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 

## = 1.268079E-07 LBSISCF S02 Concentration, ppm (385.2 I MW) 

## * LBSISCF 

### = .7625103 PPM Delta H, H 

### = .8333 Inches H20 Meter Temperature 

## = 113.2 F Barometric Pressure, PBAR = 29.5 inches HG Meter Volume, VM 

### = 15.6 

## cu. FT. Meter Co-efficient, Y = 1.0096 Liquid collected, VLC 

### = 10.9 MLS Sample weight, MN = .824 MG S02 Molecular Weight 

## = 64.06

# a. HF Data Reduction ACME BRICK DRYER STACK 6118191 Repetition 1 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 = 15.54716 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

### = .795483 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) = 4.867531 % HF concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 = 3.006724E-09 LBSISCF HF.Concentration, ppm (385.2 I MW) 

## * LBSISCF = (5.790949E-02 PPM Delta H, H = 1 Inches H20 Meter Temperature = 112.8 F Barometric Pressure, PBAR 

## = 29.5 inches HG Meter Volume, VM 

### = 16.885 CU. FT. Meter Co-efficient, Y = 1.011 Liquid collected, VLC 

### = 16.9 MLS Sample weight, MN = (.0212 MG HF Molecular Weight 

## = 20 

# (.o!G1

# !~hv

37

### ~. S02 Data Reduction ACME BRICK DRYER STACK 6118191 Repetition 1 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

### = 15.24389 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

### = .9366929 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 5.788995 % S02 concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 

## = 1.191901E-07 LBSISCF S02 Concentration, ppm (385.2 I MW) 

## * LBSISCF 

### = .7167033 PPM Delta H, H 

### = .85 Inches H20 Meter Temperature = 105.9 F . Barometric Pressure, PBAR 

### = 29.5 inches HG

Meter Volume, VM = 16.385 CU. FT. Meter Co-efficient, 

### Y 

## = 1.0096 Liquid collected, VLC 

### = 19.9 MLS Sample weight, MN 

### = .824 MG S02 Molecular Weight 

## = 64.06

38

# C .. HF Data Reduction ACME BRICK DRYER STACK 6118191 Repetition 2 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

### = 14.54473 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 

## = .875502 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) = 5.677621 % HF concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 

### = 3.229109E-09 LBSISCF HF Concentration, ppm (385.2 

### I MW) 

## * LBSISCF 

### = 6.219264E-02 PPM Delta H, H 

## = .95 Inches H20 Meter Temperature = 118.7 F Barometric Pressure, PBAR = 29.5 inches HG Meter Volume, VM = 15.961 CU. FT. Meter Co-efficient, Y 

## = 1.011 Liquid collected, VLC 

## = 18.6 MLS Sample weight, MN 

# = .0213 MG HF Molecular Weight 

### = 20

39

## C. S02 Data Reduction ACME BRICK DRYER STACK 6118191 Repetition 3 Volume of sample, VM STD (((HI 13.6) + PBAR) I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

## = 12.22401 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 = .866088 SCFH Fractional moisture content, % VWSTD I (VMSTD .+ VWSTD) = 6.616358 % S02 concentration, lbslscf (MN I VMSTD) 

## * 2.205

**~** 10-6 

### = 1.486353E-07 LBSISCF S02 Concentration, ppm (385.2 I MW) 

## * LBSISCF 

## = .8937609 PPM Delta H, H 

### = .8667 Inches H20 Meter Temperature 

## = 124.7 F Barometric Pressure, PBAR 

### = 29.5 inches HG Meter Volume, VM 

### = 13.575 CU. FT. Meter Co-efficient, Y = 1.0096 Liquid collected, VLC 

### = 18.4 MLS Sample weight, MN = .824 MG S02 Molecular Weight 

## = 64.06

40

## l HF Data Reduction ACME BRICK DRYER STACK 6118191 Repetition 3 Volume of sample, VM STD (((HI 13.6) + PBAR) 

### I (TM + 460) 

## * Y 

## * VM 

## * 17.64 

### = 12.32624 DSCF Volume of water vapor, VWSTD VLC 

## * 0.04707 = .922572 SCFH Fractional moisture content, % VWSTD I (VMSTD + VWSTD) 

## = 6.963431 % HF concentration, lbslscf (MN I VMSTD) 

## * 2.205 A 10-6 

## = 3.863951E-08 LBSISCF HF Concentration, ppm (385.2 

### I MW) 

## * LBSISCF 

## = .744197 PPM Delta H, H = .9667 Inches H20 Meter Temperature = 128.8 F Barometric Pressure, PBAR = 29.5 inches HG Meter Volume, VM 

## = 13.762 CU. FT. Meter Co-efficient, Y = 1.011 Liquid collected, VLC 

## = 19.6 MLS Sample weight, MN 

### = .216 MG HF Molecular Weight 

## = 20

41 

# 47

## I. PARTICULATE company

# ,/fw. &cf' ANALYTICAL OATA

**FOR~** 

### Location: 

# 1(/t,/11 

# CX Date: 

# 6"

# /j'g/. <=t/ I 

### Run Number:_ ___;· 

# ~-----&.~_tJ 

# __ _ Densi t

### y (?

### a ) :

### --:'-.;.1.-.¥_{_)_a-. __ Liquid Level Mprked7_-=V";..._ __ Blank Concentration(Ca).

**~** 

### Rinse Volume(Vaw)



## ~~ **~** Residue 

### in Rinse (Wa) 

# =Ca·Vaw.Pa ----- Date of Weighing 

# b/1{/'11 Date of Weighing.

# 6/2o/'1f

. Average Grass W t



## ._CJ~9_7.;....:· **/L~..J;;;..; 2** ·;_(_.__ _ 

### Gross W t


## ._1.:....4...:.......;.9~/t~~~~....~.l

# __ _ Gross W t.


## _9...:.....;..\j....:.Cf...:.FJ-_~~*..:....}---- Less Blank Residue (Wa) 

### c:) 

# ------------ Tare wt. 

# '14'}

# 0 f 

# ,.s-

**~**

# . Weight of Particulate in Acetone Rinse



### 0(1,~ 

## . Date of 

# Weighing~///;·,/ ·oate of Weighing

**~-:2,0-9/** 

### Gross Filter Weight

# #-ZJ,. 02. Gross F'ilter Weight:l

## /;&.I0 Average Gross W t. __ 

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## £i.

APPENDIX E

\

## rJ.

,. WesternAtlas International A Lmon!Ora!aer Company L A B0 RA T 0 R Y T E S T S JOB NUMBER: 911502 CLIENT I.D•••••••••: DATE SAMPLED•••••••: 02/25/91 TIME SAMPLED•••••••: 00:00 CUSTOMER: Acme Brick UORK DESCRIPTION•••: LPG 1-25-91 thru 2-25·91 TEST DESCRIPTION FINAL RESULT Analysis of Natural Gas Carbon Dioxide 1.94 Nitrogen 0.56 Methane 92.52 Ethane 3.67 Propane 0.74 lsobutane 0.13 N-Butane 0.13 Isopentane 0.07 N-Pentane 0.05 Hexanes Plus 0.18 Total 100.00 Ethane Plus 1.386 Propane Plus 0.409 Butane plus 0.207 Specific Gravity 0.6110 Gross Heating Value, Dry 1040 Gross Heating Value, Wet 1022 Pressure Base 14.65

APPROVED BY: 03/25/91 LIMITS/*DILUTION *1 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.01 0.001 0.0()1 0.001 0 0 0 0

PAGE: 1 

### CORE LABORATORIES R E S UL T S ATTN: Ken Thompson LABORATORY J.D•••: 911502-0001 DATE RECEIVED••••: 03/21/91 TIME RECEIVED••••: 13:24 REMARKS••••••••••: UNITS OF MEASURE TEST METHOD Mol % Mol % Mol % Mol % Mol % Mol % Mol % Mol % Mol % Mol % Mol % GPM GP:4 GPM (Air = 1.000) BTU BTU psia GC ASTM D-1945 ASTM D-1945 ASTM 0·1945 ASTM D-1945 ASTM D-1945 ASTM D-1945 ASTM D-1945 ASTM D-1945 ASTM D-1945 ASTM D-1945 ASTM D-3588 ASTM D-3588 ASTM D-3588

P. 0. Box 34282 Houston, TX 77234-4282 (713) 943-9776 DATE 11/13/90 TECHN

Tr,e ana•yses. op•n•ons or •nterpretat•ons conta•neo ,, !n•s report are baseel upon ooservat•OJlS,jlnC -a:'.:'··a· s...pc11e0 by the client tor wnose e:r.::

**~~** .e ana confrdent•at use tt'HS reporr has been

**~aoe** The tnterpretar•ons or op•n•ons exoressea rec•esent !l"le oesr JUdgement ol Core Lat:Ct)or es :are ·_at)oratorres assumes no respons•O·

**~.** 3ra makes nowarranty or representations expressor •rnphea. as ro the oroouctlv•ty. proper operar•ons. or prolllacteness nowever of any 011 gas :ca• or c!r-er m1nera1. property. well or sa,.,c .. ::mnecuonw•th wn•ctl such report**·~ed.r-­** re1•eC o.;pon tor any reason wnatsoever / 

### Jp

""-;. ,. J ": **~** •• .... . ' :-· .. ( ) I " I ,_C''\ ;/ 8C_IVJE ·aR I CK CDMPA.t::!.Y.. SEALY, TEXAS

f **~** ....... **~** r.:,; T I ME : 12 I 50 I 54 IJATE1 &/18/91

KET KEP UCP GO 61 62 63 64 GS 66 67 68 RC RCB ECP HAS MUB !:>ETPOINTa 170 (I" .1799 1730 1825 1920 197(1 2(1(1(1 20(15 2013 2013 1920 1460 146(1 .3(1" 99 85
ACTUAL a 158 83" .1756 1723 1826 1919 1970 2001 2005 2010 2009 1921 1498 1496 3(1" 36 10'3
DAMPER POSITIONSa KED DCD CAB HAS ECD MUB

83" 70" 20" 99" 30" (I"

)

PUSH SCHEDULEa 301 0 FLASHa OFF FLASH NUMBERa 0 AUTO UPDATEa OFF CONTROL MODEl KED• AUTO KEDF• MAN. ECDa MAN. MUS• AUTO COMMENTS I ••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••••

. . "' ............................................................................................................................... .

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--=:> **~**0'1 co **~ ~**  **~** RECORDER • 2 READINGS *******************************************************************************************************************************•

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NO. 1 154 CHANNt:L NO. 4 211 CHANNEL NO. 7 72 CHANNEL NO. 10 102 CHANNEL NO. 13 530 CHANNEL NO. 16 1987 CHANNEL NO. 19 2018 CHANNEL NO. 22 **~009** CHANNEL NO. 25 2035 CHANNEL NO. 28 2008 13a11a01DISTURBANCE MAKE-UP BURNER PILOT LIGHT OUT PREHEAT

FLAI'IE OUT 13a11a55DISTURBANCE MAKE-UP BURNER PILOT LIGHT OUT MAKE-UP

BURNER OVER-TEMP. CHANNEL NO. 2 191 CHANNEL NO. 5 240 CHANNEL NO. 8 24 CHANNEL NO. 11 1601 CHANNEL NO. 14 798 CHANNEL NO. 17 2008 CHANNEL NO. 20 1992 CHANNEL NO. 23

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## ti

APPENDIX F

### ,. **~ETER** 

### BOX CALIBRATION SUMMARY METER BOX # 

### 6 6-11-91 BAROMETRIC PRESSURE = 29.7 DELTA H = .5 VW = 5 TW =

**80.~** 

### VD = 5.215 TD = 82.5 TIME = 11.083 TEST METER Y = .998 METER BOX Y = .9592084 METER BOX H = 1.412014 DELTA H = 

### 1 VW = 5 TW = 80.75 VD = 

### 5.262 TD = 87.25 TIME= 8.616999 TEST METER Y = 1.003 METER BOX Y = 

### .9621338 METER BOX H = 

### 1.693878 DELTA H = 1.5 VW = 10 TW = 

### 81 VD = 10.648 TD = 92.5 TIME = 

### 14.25 TEST METER Y = 1.003 METER BOX Y = 

### .958425 METER BOX H = 

### 1.72221 DELTA H 

## = 2 

## vw = 10 TW 

## = 81.5 VD 

## = 10.475 TD = 

### 97.25 TIME 

## = METER BOX Y = 

### .9795356 METER BOX H = 

### 1.736327 DELTA H 

## = 3 

## vw = 

### 10 TW 

## = 82.25 VD 

## = 10.484 TD 

## = 99.25 TIME 

## = METER BOX Y 

## = .9735558 METER BOX H 

## = 1.757373 DELTA H 

## = 4 

## vw 

## = 10 TW 

## = 82.5 VD 

## = 10.441 TD 

## = 100.5 TIME 

## = METER BOX Y 

## = .9759184 METER BOX H 

## = 1.782478 AVERAGE Y = 

### .9681294 AVERAGE H = 

### 1.684047 12.433 TEST METER Y = 

### 1.002 10.217 TEST METER Y 

## = .997 8.917 TEST METER Y 

## = .996

69

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### 1 6/10/91 

### BAROMETRIC PRESSURE 

### = 29.7 

### DELTA H 

### = .5 

### VW 

## = 5 

### VD = 4.995 

### TD 

### = 87.3 

### METER BOXY= 1.00474 

### METER BOX H 

### = 1.606965 

### TW 

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### DELTA H 

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## = 5 

### VD = 5.052 

### TD = 93.8 

### METER BOX Y = 1.008063 

### METER BOX H 

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### = 11.81 

### TW = 84 

### TIME 

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### DELTA H 

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### VW 

## = 10 

### TW 

## = 84.5 2 

### TEST METER Y 

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### TEST METER Y = 1.003 

### VD = 10.196 

### TD 

## = 100.8 

### TIME = 14.55 

### TEST METER Y = 1.003 

### METER BOXY = 1.009419 

### METER BOX H 

### = 1.791876 

### TW = 84.8 

### DELTA VD = 

### METER METER H 

## = 2 10.28 

### BOX Y = BOX H 

### = 

## vw 

## = 10 

### TD 

## = 106.8 1.009072 1.769043 

### TIME = 12.58 

### DELTA H = 3 

### VD 

### = 10.241 

### METER BOX Y 

### = METER BOX H 

### = VW 

## = 10 TW 

## = 85 

### TD = 110 

### TIME 

## =

1.010689 10.36 

### DELTA H 

### = 4 

### VD 

### = 10.2 

### TD METER BOX Y 

### = METER BOX H = 1.79086 

## vw 

## = 10



## = 113.3 1.015612 1.784978 

### · AVERAGE Y = 1.009599



### AVERAGE H 

### = 1.743768 TW 

## = TIME 85.8 

## = 8.97

72 

### TEST METER Y 

## = 1.002 

### TEST METER Y 

### = .997 

### TEST METER Y 

### = .996

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### BAROMETRIC PRESSURE = 29.7 

### DELTA H = .5 VD = 5.44 

### TD METER BOX Y 

### = METER BOX H 

### = 

## vw = 5 

### = 98.5 .9349788 1.596815 

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## = 87.25 

### TIME = 11.811 

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### VW = 5 

### TW = 87.25 

### TEST METER Y 

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### VD = 5.375 

### TD = 103.5 

### TIME= 8.791001 

### TEST METER Y 

### = 1.003 

### METER BOX Y 

### = .9583557 

### METER BOX H 

### = 1.753546 

### DELTA H 

### = 1.5 

### VW = 10 

### TW = 87.75 

### VD = 10.65 

### TD = 107.75 

### TIME = 14.455 

### TEST METER Y 

### = 1.003 

### METER BOX Y 

### = .9725598 

### METER BOX H 

### = 1.767819 

### DELTA H 

### = 2 

### VW = 10 

### TW = 88.5 

### VD = 10.57 

### TD = 113.5 

### TIME = 12.18 

### TEST METER Y 

### = 1.002 

### METER BOX Y 

### = .9862896 

### METER BOX H 

### = 1.661297 

### VW = 10 

### TW = 89.25 

### DELTA H 

### = 3 

### VD = 10.501 

### METER BOX Y = METER BOX H 

### = TD = 113.5 

### TIME = 10.01 .9840431 

### DELTA H 

### = 4 

### VD = 10.445 

### METER BOX Y = METER BOX H = 1.687715 

### VW 

## = 10 

### TW 

## = 89.5 

### TD = 111.25 

### TIME = .9815892 1.695547 

### AVERAGE Y = .969636 

### AVERAGE H = 1.69379 8.668

75 

### TEST METER Y 

### = .997 

### TEST METER Y = .996

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## I. METER BOX CALIBRATION SUMMARY METER BOX # 

### 4 6-11-91 

### BAROMETRIC PRESSURE= 29.7 

### DELTA H 

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### TO 

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### TEST METER Y 

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### METER BOXY 

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### VW 

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### TW 

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### VD 

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### TD 

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### TIME 

## = 13.881 

### TEST METER Y 

## = 1.003 

### METER BOX Y = 1.014194 

### METER BOX H 

### = 1.625862 

### DELTA H 

## = 2 

## vw 

## = 10 

### TW 

## = 84 

### VD 

## = 10.234 

### TD 

## = 105.75 

### TIME 

## = 12.165 

### . TEST METER Y 

## = 1.002 

### METER BOX Y 

## = 1.013218 

### METER BOX H 

### = 1.652457 

### DELTA H 

### = 3 

## vw 

## = 10 

### TW 

## = 84 

### VD 

### = 10.186 

### TD 

## = 107.75 

### TIME 

### = 10.065 

### TEST METER Y 

### = .997 

### METER BOX Y 

### = 1.013996 

### METER BOX H 

## = 1.6908 

### DELTA H 

### = 4 

## vw 

## = 10 

### TW 

## = 84.25 

### VD 

### = 10.134 

### TD 

## = 109.75 

### TIME 

## = 8.383001 

### TEST METER Y 

### = .996 

### .METER BOX Y 

### = 1.01879 

### METER BOX H 

## = 1.559819 

### AVERAGE y 

## = 1.011212 

### AVERAGE H 

## = 1.624737

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## vw VD 

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## vw VD 

## = 10.315 

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1.004624 1.68899 

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1.007317 1.624187 

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## = 1.65151 90 

### TIME 90 

### TIME 

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### TIME =

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### TEST METER Y = 1.003 17.03 

### TEST METER Y 

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### TEST METER Y 

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TIME = 16.96 TEST METER Y = 1.003 17.06 TEST METER Y = 1.003

86

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94

### APPENDIX G

## El. 

# fArmstrong

**~** 

# Environmental, Inc. 47471rving Boulevard, *204 

# .. Dallas,Texas 75247 

### • (214) 631·0021 

### • FAX (214)905..Q634



### RESUME OF Richard Taylor EDUCATION Southwest Texas State University B.S. Environmental Studies San Marcos, Texas PROFESSIONAL EXPERIENCE : February, 1991 - Present April, 1988 - February, 1991 January, 1988 - April, 1988 September, 1987 - January, 1988

95 

### Project Manag.er Armstrong Environmental, Inc. Dallas, Texas Project Manager Turner Engineering, Inc. Dallas, Texas Assistant Manager Better Buys Sport Shoes Weatherford, Texas Substitute Teacher Cedar Hill I.S.D. Cedar Hill, Texas

# a. 

# if Armstrong

**~** 

# Environmental, Inc. 47471rving Boulevard, #204 

### • Dallas, Texas 75247 

### • (214) 631-0021 

### • FAX (214) 905-0634 RESUME OF: Larry Whicher EDUCATION: B.S. Geology Western New Mexico University, Silver City, NM PROFESSIONAL EXPERIENCE: January, 1991 - Present April, 1988 - January, 1991 February, 1987 - April 1988 Project Manager Armstrong Environmental, Inc. Dallas, Texas Project Manager Turner Engineering, Inc. Da1las, Texas Electronic Distribution Lex Electronics Dallas, Texas February 1986 - November 1986 Office Manager Amerex Rent-A-Car Dallas, Texas

96

# fArmstrong

**~** 

# Environmental, Inc. 47471rving Boulevard, #204 

### • Dallas, Texas 75247 

### • (214) 631-0021 

### • FAX {214) 905-0634



### RESUME OF Jerry Salinas EDUCATION Sunset High School, June 1988 PROFESSIONAL EXPERIENCE : February, 1991 - Present August, 1988 - February, 1991 March, 1984 - August, 1988

97 

### Technician Armstrong Environmental, Inc. Dallas, Texas Technician Turner Engineering, Inc. Dallas, Texas Service Assistant Stevens Park Golf Course Dallas, Texas

## 1: 

# if Armstrong

**~** 

# Environmental, Inc. 47471rving Boulevard, #204 

### • Dallas, Texas 75247 

### • (214) 631·0021 

### • RESUME OF: Matthew A. Taylor EDUCATION: Cedar Hill High School 

### PROFFESSIONAL EXPRIENCE: February, 1991 - Present August, 1990 - February, 1991 November, 1988 - 

### July, 1990 Technician Armstrong Environmental, Inc. Dallas, Texas Technician Turner Engineering, Inc. Dallas, Texas Lab Technician 

### Dixico, Inc. Dallas, Texas

98 FAX (214) 905.0634[' 

# f=Arms.trong

**~** 

# Envtronmental, Inc. • 47471rving Boulevard, 1204 Dallas. Texas 75247 

### • (214) 631-0021 

### • FAX (214) 905-0634 RESUME OF: Thomas Armstrong EDUCATION: College of Dupage, Glen Ellyn, Illinois PROFESSIONAL EXPERIENCE: February, 1991 - Present April, 1984 - February, 1991 1976 - 1984 1975 - 1976 President Armstrong Environmental, Inc. Dallas, Texas Vice-President Turner Engineering, Inc. Dallas, TX Project Manager The Almega Corporation Bensenville, Illinois Environmental Specialist Particle Data Labs, Ltd. Elmhurst, Illinois Mr. Armstrong has 15 years experience in performing field and laboratory analysis of air pollutants. 

### Mr. Armstrong has tested for air pollutants in a variety of industries, including chemical, steel food, power generation, pharmaceutical, ceramics, petrochemical, and cement. Mr. Armstrong has performed ambient and stack tests for particulate, SOx, NOx, hydrocarbons, TRS and others using virtually all current test methods and procedures. 99 

# ;(D