DISCLAIMER STATEMENT 

This report has been reviewed by the U.S. Environmental 

Protection Agecny (EPA) and approved f or publication. Approval 

does not signify that the contents necessarily reflect the views and 

policies of EPA, nor does mention of trade names or commecial 

products constitute endorsement or recommendation for use. 

CONFIDENTIALITY STATEMENT 

Subsequent to the collection of data for this study, and the 

review of these data by each sanipled f acility, EPA solicited confidentiality statements from each plant regarding the data 

collected and plant identity. Although all facilities considered 

their data non-confidential, some plants requested that their 

identy be kept confidential. Therefore, to minimize the possibility of identifying these f acilities, all plants contained in 

this study are consistently referred to by an assisned code 

number that is considered confidential by EPA. 
qq6 > sa -303 

FATE OF PRIORITY TOXIC POLLUTANTS 

IN 

PUBLICLY OWNED TREATMENT WORKS 

FINAL REPORT 

VOLUME.I 

PREPARED FOR: 

EFFLUENT GUIDEI,INES DIVISION 

OFFICE OF WATER REGULATIONS AND STANDARDS I 

U.S. ENVIRONMENTAL PROTECTION AGENCY 

WASHINGTON, D.C. 20460 

PREPARED BY: 

BURNS AND ROE INDUSTRIAL SERVICES.CORPORATION 

PARAMUS, NEW JERSEY 07652 
PREFACE 

This document is being issued as the Final Report on a project 

initiated by the United States Environmental Protection Agency in 

1978 to study the occurrence and fate of the 129 priority toxic 

pollutants in 40 Publicly.Owned Treatment Works (POTW) and a 

supplemental study conducted at 10 addi.tional POTW. This report 

Consists of two volumes. Volume I contains the background and 

purpose of study, the POTW selection criteria, the samp].ing 

program details, the overall POTW data, evaluation of analytical 

results, and the preliminary conclusions of the study. Volume II 

contains the Daily Analytical Results which embody the basic data 

generated during the course of this study and which are the 

source for all other data compilations and analyses. 

ii 
TABLE OF CONTENTS 

SECTION PAGE 

I. SUMMARY, RESULTS AND CONCLUSIONS 1 

Summary 1, 

Results and Conclusions 1 

II. INTRODUCTION 3 ; 

Background 3 

Purpose 4 

III. POTW SELECTION AND DESCRIPTION 5 

Selection Criteria 5 

POTW Characteristics 7 

IV. DESCRIPTION OF FIELD SAMPLING PROGRAM 15 

Sampling Frequency 15 

Sampling Techniques 16 

Sample Points 17 

V. DATA ORGANIZATION AND INTERPRETATION 27 

Data Organization 27 

Laboratory Data Reporting Protocol 27 

Data Interpretation and Presentation 30 

Quality Assurance Program 31 

VI. EVALUATION AND DISCUSSION OF ANALYTICAL DATA 35 

Overview of Priority Pollutant Occurrence 35 

Summary of Influent Pollutant Concentrations 51 

Impact of Industrial Contribution on Influent .51 

Qual ity 

.Treatment or Removal-of Priority Pollutants in 56 

POTWs 

Reduction of Priority Pollutants by POTW 58 

Tr•eatment Processes 

POTW Priority , Pollutant Mass Balances 62 

Daily Variation of Influent - Pollutant Concen- 64 

trations 

Effect of Rainfall on Influent Concentrations 66 

Formation of Chlorinated Hydrocarbons 66 

Pollutants Detected in Sludges When Not 70 

Measured in the Influent 

Correlation of Influent and Effluent Concen- 70 

trations 

Discussion of 10-Plant Study Results 73 

iii 
TABLE OF CONTENTS (Continued) 

:.. 

PAGE. 

A-1 to A-52 

SECTION 

APPENDIX A Flow Diagrams - Plants 1 to 40 and 

51 to 60 - 

APPENDIX B Cumulative Distribution Curves of 

Effluent Coricentrations and Percent 

Removals for the.Twenty-four Most 

Frequently Found Priority Pollutants 

APPENDIX C Summary of Analytical Data - Plants 1 

to 40 and 51 to 60 

APPENDIX D Percent Occurrence of Pollutant 

Parameters - Plants 1 to 40 and 51 

to 60 

APPENDIX E Mass Balance in Pounds Per Day 

Plants 1 to 40 and 51 to 60 

B-1 to B-14 

C-1 to C-108 

D-1 to D-74 

E-1 to E-102 

iv 
LIST:OF:TAB.LES 

TABLE NO . TITLE PAGE 

1 POTW Characteristics 8 

2 Summary of Number of Samples Taken 18 

at Each Plant 

3 Occurrence of Priority Pollutants,in 36 

POTW Influents, POTWs.,1 to 40- 

4 Occurrence of Priority Pollutants in 39 

- POTW Effluents, POTWs ,1 to 40 

5 Occurrence of Priority Pollutants in 41 

POTW Raw Sludges, POTWs 1 to 40 

6 Occurrence of Priority Pollutants .in 45 

POTW Influents 

POTWs 51 to 60 

7 Occurrence of Priority Pollutants in 47 

POTW Effluents 

POTWs 51 to 60 

8 Occurrence of Priority Poll.utants in 49 

POTW Raw Sludges 

POTWs 51 to 60 

9 Summary of Selected Influent Pollutant 52 

Concentrations for POTWs 1`through 40 

10 Summary of Minimum Percent Removals 57 

Achieved by Secondary Treatment 

11 Median Removals of Selected Pollutants 61 

through POTW Treatment Processes 

12 Mass Balance Summary 63 

13 Daily Average Concentrations of Pol- 65 

lutants in POTW Influents 

14 Effect of Rainfall on Influent Total 67 

Metal Loading 

15 Effect of Rainfall on Influent Lead 68 

Loading 

16: Formation of Chlorinated Hydrocarbons 69 

During Chlorine Disinfection 

17 Occurrence of Priority Pollutants De- 71 

tected in Sludges When Not Detected 

in the Influents 

v 
LIST OF TABLES(Continued) 

TABLE NO . TITLE PAGE 

18 Correlation of Influent:and Effluent 72 

Concentration 

19 Comparison of Influent and Secondary 75 

Effluent Pollutant Masses -.POTW 51 

20 Comparison of Influent, Secondary Ef- 76 

fluent and Primary Industrial Effluent Pollutant Masses - POTW 52 

21 Comparison of Influent and Secondary 78 

Effluent Pollutant Masses - POTW 53 

22 Comparison of Influent, Secondary 80 

Effluent and Primary Industrial 

Effluent Pollutant Masses - POTW 54 

23 Comparison of Influent, Secondary Ef- 81 

fluent, Tertiary Effluent and Primary 

Industrial Effluent Pollutant Masses - 

POTW 55 , 

24 Comparison of Influent, Primary Efflu- 82 

ent and Tertiary Effluent Pollutant 

Masses - POTW 56 

25 Comparison of Influent, Secondary Ef- 84 

fluent and Primary Industrial Effluent 

Pollutant Masses - POTW 57 

26 Comparison of Influent and Secondary 85 

Effluent Masses - POTW 58 

27 Comparison of Influent and Secondary 86 

Effluent Pollutant Masses - POTW 59 

28 Comparison of Influent, Primary Efflu- 87 

ent, Secondary Effluent and Primary 

Industrial Effluent Pollutant Masses - 

POTW 60 

vi 
LIST OF FIGURES 

FI,GURE NO . TITLE PAGE 

1 Organization of the 50 POTW Compu- 28 

terized Data Base 

2 Correlation of Influent Tota1 Metals 53 

Concentration Versus Percent 

Industrial Flow 

3 Correlation of Influent Total.Vola- 54 

tiles Concentration Versus Percent 

Industrial Flow 

4 Correlation of Influent Tota1 Base 55 

Neutrals Concentration Versus Percent 

Industrial Flow 

5 Cumulative Distribution Curves, Total 59 

Metals and Total Volatiles Effluent 

Concentration and Percent Removal 

6 Cumulative Distribution Curves, Total 60 

Acids and Total Base Neutrals Effluent 

Concentration and Percent Removal 

vii 
ACKNOWLEDGEMENTS 

The EPA personnel contributing to this effort were: Project 

Officer, Robert M. Southworth, Effluent Guidelines Division; 

Program Manager, Thomas P. O'Farrell, Office of Water 

Regulations and Standards; and fo'rmer Project Officers, Arthur E. 

Shattuck, formerly of the Effluent Guidelines Division, and R. 

Dean Jarman, formerly of the Office of Research and Development, 

Center for Environmental Research Information. 

Additionally, the following EPA personnel are gratefully 

acknowledged for their valuable assistance and guidance: Jeffery 

D. Denit, Director, Effluent Guidelines Division; Harold B. 

Coughlin, Branch Chief, Effluent Guidelines Division; and 

John E. Riley, Former Branch Chief, Effluent Guidelines Division. 

Acknowledgement is also made to Burns and Roe Industrial Services 

Corporation, Paramus, New Jersey, the EPA contractor for the 

project. The following members of the technical staff made 

significant contributions to the overall project effort and execution of the sampling program: Arnold S. Vernick, Jameel Ahmad, 

Henry M. Celestino, Thomas Hayton, Gary C. Martin, James Millikin, 

and Mark V. Sadowski. Additionally, significant contributions 

were made by Howard D. Feiler and Paul J. Storch of JRB 

Associates, both former members of the Burns and Roe technical 

staff. .

The technical staff of E.C. Jordan Co. are also acknowledged for 

significant contributions in the preparation of the final report 

and for management and execution of the 10-POTW Supplemental 

Sampling Program. 
I . 

SUMMARY, RESULTS AND CONCLUSIONS 

SU MMARY 

In 1978, the United States Environmental Protection Agency (EPA) 

initiated a program to study the occurrence and fate of the 129 

priority pollutants in 40 Publicly Owned Treatment Works (POTWs). 

The first phase of this work was a two-plant pilot study designed 

to set operating parameters for the remainder of the 40 POTW 

study. In October 1979, EPA's Effluent Guidelines Division (EGD) 

published a report summarizing - the findings of the pilot study 

work, °Fate of Priority Pollutants in Publicly Owned Treatment 

Works-Pilot Study," EPA 440/1-79-300. Upon completion of ,half of 

the POTTnT project EGD published a report summarizing the findings 

for the first 20 POTWs, "Fate of Priority Pollutants in Publicly 

Owned Treatment Works-Interim Report," EPA 440/1-80-301. 

In this final report, data from all 40 POTWs plus 10 supplemental 

POTWs sampled under a parallel project are presented. At most of 

these plants, a minimum of 6 days of 24-hour sampling of 

influent, effluent and sludge streams was completed. Each sample 

was analyzed for conventional, selected non-conventional, and 

priority pollutants. 

Beyond presenting the occurrence and concentration of_priority 

pollutants in the 40 POTWs (and 10 supplemental POTWs) other specific phenomena and relationships are evaluated in this report. 

These items include: 

o Impact of industrial contribution on influent quality 

o Treatment or removal of priority pollutants in POTWs 

o Reduction of priority pollutants by individual POTW treatment 

processes 

o POTW priority pollutant mass balances 

o Daily variation of influent pollutant concentrations 

o Effect of rainf all on priority pollutant levels in POTW influents 

o Formation of chlorinated hydrocarbons through chlorine disinfection 

o Quantification of pollutants found in sludges but not detected 

in POTW influents 

o Correlation of influent and effluent priority pollutant levels. 

RESULTS AND CONCLUSIONS 

1. A total of 102 priority pollutants were detected, at least 

once, in POTW influents. 

2. In general, the higher the industri.alcontribution.to a POTW, 

the higher the concentration of priority pollutants in the 

POTW influents. 

s 
3. Based on the 40 POTW data base, 50 percent of secondary 

treatment plants achieved a minimum of 70 percent reduction 

of total priority pollutant metals, 82 percent reduction of 

total volatile priority pollutants, and 65 percent reduction 

of the total base neutral priority pollutants. 

4. Tertiary treatment processes reduced priority pollutants 

slightly better than secondary processes. Primary treatment 

was less effective than either secondary or tertiary processes. Activated sludge, trickling filter, rotating biological contactor and pure oxygen activated sludge processes 

were approximately equally effective in reducing priority 

pollutant concentrations. 

S. At plants where the metal priority pollutant mass balance was 

good, some organic priority pollutants in the influent were 

not always accounted for in the effluent or sludges. This 

indicates that, in general, a portion of the organic priority 

pollutants are biodegraded or, in the case of volatiles, 

stripped out of the wastewater. 

6. The mass loading of priority pollutants in POTW influents was 

higher on.weekdays than on weekends. This was true for the 

metals, volatiles and base neutral priority po - llutants. 

7. Heavy rainfall increased metallic priority pollutant mass 

loading at POTWs. 

8. Certain priority pollutant chlorinated hydrocarbons increased 

slightly in concentration during chlorine disinfection. 

9. Some pollutants not measured in POTW influents were regularly 

measured at high levels in the corresponding sludge streams. 

10.'For many conventional and priority pollutants, as influent 

concentrations increased effluent concentrations also 

increased. This implies that the removal rates for the 

priority pollutants are relatively constant and a fixed percentage of incremental loadings of these pollutants will be 

removed by secondary treatment. 
INTRODUCTION. 

BACKGROUND 

Pxiority,toxic pollutants enter navigable waters from a variety 

.of.point and-non-point sources. Prior to the initiation of this 

project, only scattered data existed on the impact, occurrence, 

and removal of toxic pollutants in Publicly Owned Treatment 

Works (POTW). Very little was known about the quantity of toxic 

.pollutants entering receiving streams from POTWs or the ability 

of POTWs to treat or remove toxic pollutants. 

In 1978, the United States Environmental Protection Agency. (EPA) 

initiated a project to systematically study the occurrence and 

fate of the 129 priority toxic pollutants in 40 POTWs. The scope 

of the overall project included an extensive sampling program for 

all priority pollutants and selected.conventional/non-conventional pollutants to be conducted at 40 geographically distributed POTWs representing'a variety of municipal treatment 

technologies, size ranges, and industrial flow contributions. 

The initial phase of the 40 POTW project was a two-plant pilot 

study designed to establish operating parameters for the full 

study. During this pilot study, logistical factors €or field 

sampling were tested to determine optimum sampling methodologies 

and an overall framework was established for studying the various 

aspects of POTW operations. The pilot study also served .to 

establish the analytical protocols and field and laboratory 

Quality Assurance/Quality Control (QA/QC) procedures that would 

be .used for the duration of the study and to determine the significance that industrial contribution should have on the POTW 

selection process. 

During the course of the 40 POTW study, EPA decided to increase 

the number of POTWs in the data base.to 50 by including.10.additional plants that were sampled under a separate program. Each 

of the latter 10 POTWs was characterized by one dominant industrial discharger that contributed all or most of the industrial 

flow. Sampling of these 10 POTWs mirrored the procedures, techniques, and sample points of the 40 POTW study. Moreover, the 

effluent from the dominant industry was also sampled'at 5 of 

these 10 plants as part of this supplamentary study. 

In October 1979, EPA's Effluent Guidelines Division published a 

report summarizing the findings of the pilot study: "Fate of 

Priority Pollutants in Publicly Owned Treatment Works -Pilot 

Study," (EPA-440/1-79-300). Subsequently, at the midpoint of the 

study when sampling at 20 of the 40 POTWs was completed, an 

interim report was published by EPA (October 1980) that presented 

3 
the data from the first 20 cities, including a number of preliminary conclusions regarding the occurrence•and fate of priority 

pollutants: "Fate of Priority Pollutants in Publicly Owned 

Treatment Works - Interim Report" (EPA-440/1-80-301). 

This document is the final project report and presents the findings of the full 40 POTW study and also includes the findings of 

the sampling program at the 10 additional POTWs. 

PURPOSE 

The basic objective of this study is to generate, compile, and 

report data on the occurrence and fate of the 129 priority toxic 

pollutants in 50 POTWs. Preliminary evaluations of the data are 

also conducted. This report presents, therefore, all of the 

collected data, results of the preliminary evaluations, and 

results of calculations to determine: 

1. The quantity of,priority pollutants in'the influent to 

the POTWs. 

2. The quantity of priority pollutants discharged from the 

POTWs. 

3. The quantity of pr•iority pollutants in the effluent from 

intermedi'ate process streams. 

4. The quantity of priority poll.utants in the POTW sludge 

streams. 

Information presented in this report can be useful to the scientific community and the engineering profession at large, the 

industrial community, governmental bodies including regulatory 

agencies at the Federal,'state, or local level, as well as the 

POTWs themselves. Depending on the intended use, the data base 

for'this study has the potential to yield further interpretations 

or conclusions beyond.those presented in this report. 

4 
III 

POTW SELECTION AND DESCRIPTION : 

SELECTION CRITERIA 

A major goal of this project was to.obtain priority toxic pollutant data from representative types of secondary:treatm.ent..:facilities that will exist after completion of EPA's Construction 

Grants Program. Primary factors considered in selecting the 

POTWs included: 

1. Treatment processes - 

2. POTW size 

3. Amount of indu- strial cont.r-ibution - 

4. Type of industrial contribution 

5. POTW operating efficiency 

6. Actual flow as a percent of design capacity 

7., Geographical distribution. 

The first 40 of the 50 POTWs included in this study are representative of the secondary treatment processes as reported in the 

1978 EPA Needs Survey. POTW selection incorporated a geographical and type of treatment mix that approximately profiled all 

POTWs over 5 MGD nationwide. Since activated sludge and 

trickling filter plants are the most prevalent, the 40 : POTWs are 

most heavily weighted with these types. The.40 POTWs included 26 

activated sludge plants, 7 trickling filter plants, 5 dual activated sludge and parallel trickling filter plants, one.aerated 

lagoon and one rotating biological contactor (RBC). The RBC 

plant was the only one of the 40 POTWs under 5 MGD, primarily 

because it was the most suitable RBC plant located with respectto all considered variables. POTWs from each EPA region are. 

included in the 40 POTWs. The number of plants in each regi,on is 

approximately proportional to the total number of POTWs over .5 . 

MGD in that region. The 40 POTWs were distributed geographically 

as follows: 

EPA Region No. of POTWs 

I 4 

II 3 

III 3 

IV 6 

V 9 

VI 3 

VII 3 

VIII 3 

IX 5 

X 1 

5 
POTWs from 25 different states were included among the 40 plants. 

Within the 40 POTWs, modifications of the activated sludge process such as contact stabilization, Kraus, and.pure oxygen are 

represented as well as some advanced waste treatment processes, 

notably tertiary mixed media filters and polishing ponds. 

Although according to the Needs Survey, most POTWs are in the 

smaller size range, plant selection favored plants over 5 MGD. 

This is primarily due to three reasons. First, although there 

are relatively fewer large POTWs, the large plants treat the bulk 

of the nation's wastewater. Second, EPA's General Pretreatment 

Regulations (40 CFR 423) primarily affect all POTWs larger than 

5 MGD. Third, for an intensive sampling program such as this, 

plants over 5 MGD also offer some logistical advantages. These 

plants are more likely to receive continuous flow over 24 hours, 

and often have more suitable sampling locations designed into the 

plant, as well as access to a greater number of sludge and 

sidestreams. POTWs of this size also tend to meter more of their 

plant flows and have better operational, laboratory and 

industrial flow records, which are necessary for subsequent analyses. Larger plants are more apt to have continuous staffing, 

which minimizes safety problems and provides some assurances 

against major plant equipment failures. 

Actual POTW flow as a percent of design capacity was also an 

important selection criterion. POTWs operating well below capacity do not give a fair representation of priority toxic pollutant treatment or removal. Although a few of the selected POTWs 

operated at a low percentage of their indicated design capacity, 

these plants generally had a significant percentage of the treatment processes off=line during the week of sampling. For 

example, at POTW 2, only half of the primary treatment capacity 

was in use when the plant was sampled. Likewise, at POTW 8, only 

seven of ten primary and five of nine secondary clarifiers were' 

in operation. At POTW 19, routinely, only 65 percent of the 

design capacity was on-line. 

With regard to industrial flow, POTWs ranging from close to zero 

to more than 50 percent industrial contribution are included. 

Similarly, industries in most of the 34 industrial categories 

currently under review by the Effluent Guidelines Division are 

covered by the study. Two of the early POTWs selected had virtually no industrial flow, and both had relatively low concentrations of priority toxic pollutants. Consequently, for the 

remainder of the 40 POTW study, EPA decided to select POTWs that 

had a mixture 'of industries, and generally 10 percent to 50 percent industrial flow. POTW sizes were also varied from 5 MGD to. 

200 MGD, (with the exception of the RBC plant), but no attempt 

was made to profile the national distribution for POTW flows or 

industrial flow percentages. 

Finally, although not all of the 40 plants always met the 30/30 

BOD/TSS secondary treatment requirements, POTWs were only 

.1 
selected if they 

required to meet 

of`the 40 plants 

requirement.) 

were operating at or near the efficiency 

secondary treatment regulations. (Twenty-seven 

had average effluent quality meeting.the 30/30 . 

In summary, the 40 POTWs were selected to present a variety of 

treatment plant operations, flows, and industrial contributions.- 

They were not meant to be a statistically valid`representation of' 

all POTWs in the country, but rather to provide some . inforination 

on the scope of priority toxic pollutant occurrence in municipal 

wastewater and on the fate of these pollutants;in secondary 

treatment facilities. „ 

The 10 supplemental POTWs were selected primarily to include a_ 

targeted industrial contributor, with secondary attention to all._ 

other selection criteria: A11 10 POTWs were located on the east. 

coast (EPA Regions II, III, IV and V) to minimize shipping and 

travel costs. One of the 40 POTWs (POTW 6) was resampled.as part 

of the 10 POTWs because it had a large plastics product manufacturer contributing to the influent and the first sampling episode 

indicated.exceptionally high volatile pollutant concentrations. 

The 10 supplemental POTWs ranged in size (average design flow) 

from 3 MGD to 42 MGD. Eight of these wer.e activated sludge 

plants (one followed by advanced treatment), one was a trickling 

filter plant and one was a lagoon system followed by land.application. 

POTW CHARACTERISTICS 

Flow diagrams for the 50 POTWs - are presented in Appendix A with 

pertinent notes-on any'plant irregularities that affected sampling. Table 1 presents information on the basic characteristics. 

of each POTW. Each of the 50 POTWs provided some form of secondary treatment, and nine plants further provided some advanced., 

wastewater treatment (AWT). Table 1 indicates the average design 

flow and the historical influent flow for t ~ e secondary treatment 

system at each plant. This table also indicates the type of 

sewerage system and percent industrial flow to the plant as estimated by plant personnel. The percent industrial flow is not 

always consistently defined by wastewater treatment plants'for. 

the following reasons: 

o Some plants had never surveyed their industries,.while other 

POTWs had knowledge only of major industries. These plants 

could only estimate industrial flows from histor'ical records 

or studies. 

o- Some POTWs included all commercial accounts in their 

-i.ndustrial flow definition, some plants included only 

selected commercial users and some did not include any. 

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12 
o Several POTWs had implemented pretreatment programs, which 

may have'affected the flows and organic loadings from their - 

industrial users. 

Following completion of the sampling phase of this study, EPA 

attempted to obtain a more`detailed estimate of industrial flow 

contributions by calling each POTW and requesting a list of all 

coritributing industries with their Standard Industrial Classification (SIC) codes. However, many of the same problems listed 

above were encountered. Consequently, Table 1 indicates the original POTW estimate of percent industrial flow, with the 

following exceptionsz 

o If the original estimate and the detailed survey were significantly different, the plant-was called to resolve the discrepancy. The more accurate number was then used. 

o At four POTWs (Nos. 2, 4, 5 and 9) where EPA had conducted 

separate in-depth , studi•es of the POTWs, the industrial flow 

percentages fxom these studies were used. ~ These, however, 

were all very close,to estimates provided by plant personnel. 

Table 1 also lists the types of industries that the POTWs indicated were significant contributors to their;system. 

~ 

13 

IV 

DESCRIPTION OF FIELD SAMPLING PROGRAM 

SAMPLING FREQUENCY 

A sampling period of six consecutive days, excluding Sundays, was 

selected for this study based on the findings of the two-plant 

pilot study as well as logistic factors. Consequently, for 35 of 

the 40 POTWs, six days of sampling were completed. At POTWs 3, 

8, and 35, only four days of sampling were accomplished. For 

POTW 3, the shorter sampling period was planned to permit analytical capacity for three 8-hour influent composite samples per 

day. At POTWs 8 and 35, POTW operational problems necessitated 

shortening the sampling programs. For the pilot program at 

POTWs 1 and 2, seven continuous days of sampling were conducted. 

Further, at POTW 1, an additional seven days of influent samples 

were collected. 

Generally, the 24 hour composite samples in this program were 

collected from 8 a.m. to 8 a.m., with grab samples for volatile 

organics (VOA), phenols, cyanide and oil and grease taken six 

times daily: at noon, 4:00 p.m., 8:00 p.m., midnight, 4:00 a.m. 

and 8:00 a.m. The six days of sampling normally excluded 

Sundays, from 8:00 a.m. Sunday to 8:00 a.m. Monday. 

At four plants in the 40-plant program, however, sampling was 

performed on a Sunday for a variety of reasons. At POTWs 1 

and 2, of course, seven consecutive days of sampling were performed. At POTW 9, sampling was started on Sunday to coordinate 

sampling periods with another EPA project occurring simultaneously in the same city. At POTW 27, sampling was initiated on 

a Sunday to complete the six day program before a holiday, which 

was judged no better for sampling than a Sunday. 

A six-day sampling period was also used for the additional 10 

POTWs included in this report. Those plants, designated POTWs 51 

through 60, were each sampled on a six consecutive day schedule. 

Sunday samples were collected at POTWs 51, 54, 56, and 58. 

The two POTWs in the pilot study (POTWs 1 and 2) were sampled for 

a longer period of time than those sampled afterward. This is 

because sampling at the pilot facilities was intended to determine the procedure best suited for obtaining the most representative samples from each treatment plant over the course of the 

entire 40-plant program. Thus, the sampling effort at the pilot 

plants focused on an appropriate sample frequency that represented the operation of the POTW, on which days yield the most 

representative samples, and on whether the final sampling plan 

could be limited to less than seven days, of sampling per week. 

15 

- ~: 

~ 
Investigation of the appropriate sampling points to be used in 

the remainder of the 40-plant program was another focus of the 

pilot study. Samples were taken at different intermediate points 

in the wastewater treatment processes to ascertain which sampling 

points would provide the best information on the fate of priority 

pollutants as they pass through the POTW. At POTW 1, influent, 

effluent, and sludge streams were sampled over 24 hours for seven 

consecutive days. Three, eight-hour composite samples of the 

influent and a second week of 24-hour influent samples were 

collected. At POTW 2, seven consecutive days of 24-hour sampling 

were completed. 

SAMPLING TECHNIQUES 

Generally, uniform sampling techniques were used at the first 40 

POTWs sampled in this study (POTWs 1-40). Sampling for the other 

10 plants (POTWs 51-60), although administered under a separate 

program, encompassed only minor variations in the techniques 

employed for the first 40 plants. The sampling techniques are 

described in detail in the Pilot Study report: "Fate of Priority 

Pollutants in Publicly Owned Treatment Works - Pilot Study" 

(EPA-440/1-79-300). 

To obtain the most representative.sample from each sample point, 

automatic samplers were used wherever possible to collect equalsized sample aliquots. Flow proportional samples were not 

collected during this study. Automatic sampling was only 

possible where flows were continuous and accessible to the 

sampling equipment. At the early plants, automatic sampler 

tubing was changed daily and sampler blanks were run before 

beginning each, day's new composite. Later in the program (after 

POTW 5), under a revised QA/QC program, this procedure was 

discontinued, with fresh Teflon tubina being used only when a 

sampler was set up at a new collection point. The automatic 

samplers were calibrated to pull sample aliquots of at least 100 

ml at time intervals not to exceed 30 minutes. Composites in the 

automatic samplers were collected in 2.5 or 5.0 gallon glass jars 

that were kept in an ice bath at 4 ° C for the entire 24-hour, . 

period of sampling. 

In cases where wastewater or sludge flows were intermittent or 

not pumpable, such as primary sludge, grab samples were 

collected. Grab samples were also taken where prescribed by 

EPA's sampling protocol. Grabs were collected at least six times 

a day and often more frequently. 

On occasion, as dictated by sample point configuration, samples 

were grabbed via an intermediate vessel. This method of sampling 

is a modification to the protocol for fractions such as oil and 

grease and volatile organics where the sample container is supposed to be filled directly from the wastewater stream. This 

modification was made at a few sample points for safety and prac16 
tical teasons since positioning of the sample container in most 

of these waste streams was either impossible or very dangerous, 

and the error introduced through use of an intermediate beaker 

was of lesser consequence. In all cases where an intermediate 

beaker was used, it was used exclusively at one point for the 

duration of sampling at the plant; it was repeatedly purged with 

fresh sample before each sample was collected. 

SAMPLE POINTS 

Sample points were selected so that the influent, effluent, and 

sludge priority toxic pollutant concentrations could be determined,-which, when combined with flow data, provided priority 

toxic pollutant mass balances through the POTWs. Other sample 

points were selected to best characterize wastewater and sludges 

at particular stages of treatment. At each plant, an effort was 

made to select sample points that allowed sample collection 

before contamination from other waste streams, recycle flows, or 

chemical additions. 

Table 2 lists all 'samples taken during the study (POTWs 1 to 40 

and 51 to 60). Additionally, the pl-ant flow diagrams in Appendix 

A provide the location of all sample points. In the following 

paragraphs, each sample point is briefly described and exceptions 

are noted. 

Tap Water 

Background samples of, the domestic water as supplied to the 

plants' service areas were taken at 28 of the 50 plants sampled 

during this study. Samples were taken at a frequently used sink 

within the plant premises. The tap water was allowed to run for 

a period of time prior to sample collection. At POTW 21, a 

manual composite of two points (off POTW premises) was taken to 

obtain a representative sample of the municipal supply during the 

sample ~ period. 

Influent (Total) 

Generally, total influent samples were collected prior to preaeration, grit removal, or recycle streams such as digester 

supernatant. To avoid potential automatic sampler tube fouling, 

influent samples were collected downstream of bar screens. When 

access to the influent was such tYiat representative samples could 

not be taken - via automatic sampling, grab composite aliquots were 

collected every two hours. When a total influent sample was not 

accessible, upstream samples of separate flows were taken and 

manually composited to create a total influent sample. 

17 
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20 
Influent (Other) 

At nine of the plants in this study, additional influent points 

were sampled. At POTW 14, an additional set of samples was taken 

at the City's second treatment plant (domestic sewage only). At 

POTW 15, an additional set of samples was taken of the industrial 

influent. POTW 16 had two treatment trains that were both 

sampled independently. POTW 30 had separate influent streams 

that did not combine until after primary treatment so separate 

influent samples were taken. At POTWs 52, 54, 55, 57, and 60, 

samples of the effluent from the plants major industrial 

discharger were also taken. The same criteria were used to 

choose the "Influent (Other)" points as were used to choose 

"Influent (Total)" points. 

Floatables 

At POTW 1, a complete set of samples of the skimmings from the 

primary clarifiers was taken. Manual composite samples were 

gathered by dipping into the floating layer at the location on 

the primary settling tanks where floatables are collected. 

Primary Effluent 

At 14 of the 50 POTWs, primary clarifier overflows, prior to 

secondary treatment, we"re sampled. In all instances, except 

POTW-39, automatic samplers were set.up in the channel between 

primary and secondary treatment. `The channels contained the 

well-mixed combined effluent flow from all primary tanks. At 

POTW 39, a portion of the primary effluent was discharged to 

infiltration/percolation (I/P) beds for limited periods each day. 

Grab samples of this influent to the I/P beds were taken. 

Secondary Effluent (Unchlorinated) 

At 21 of the 50 POTWs secondary effluent samples were collected 

prior to chlorine disinfection. This sample was collected either 

at the secondary clarifier overflow or in the channel leading to 

the chlorine contact chamber tank. In the majority of plants the 

next step in the treatment_ process was chlorine disinfection, but 

in some plants additional treatment prior to disinfection was 

practiced. At other plants, the unchlorinated effluent was the 

last accessible sampling point before final discharge. At 

POTW 15, the chlorination facilities were shut down in the middle 

of the sample wcek, resulting in 3 chlorinated and 3 unchlorinated samples. 

Secondary Effluent (Chlorinated) 

This sample point' represents the effluent from the chlorine contact chamber prior :to discharge to the receiving water. This 

type of sample was collected at 34 of the plants in this study. 

21 
Secondary Effluent (Other) 

At six of the 50 plants sampled in this study, more than one 

secondary effluent point was sampled (excluding pre-and postchlorination samples). At POTWs 10, 17, 27, and 37, both activated sludge and trickling filter effluents were sampled with the 

trickling filter effluent considered under this heading. The 

"Secondary Effluent (Other)" at POTW 19 was a dechlorinated 

effluent. POTW 39 had an infiltration/percolation (I/P) test 

facility that treated primary effluent. Effluent from these I/P 

beds was listed under this category. 

Tertiary Effluent (Unchlorinated) 

At POTWs 16 and 25, additional prechlorinated mixed media filter 

effluent samples were taken and analyzed for the organic priority 

toxic pollutants. 

Tertiary Effluent (Chlorinated) 

Four of the plants in this study which utilized mixed media 

filtration for tertiary treatment (POTWs 13, 21, 25, and 56) and 

three plants which utilized polishing ponds for tertiary treatment (POTWs 21, 22, and 23) were sampled after chlorine disinfection. 

Tertiary Effluent (Other) 

At POTW 16, mixed media filter effluent was combined with a portion of the trickling filter plant effluent and sampled after 

chlorination. One of the plants utilized a mixed media filter 

for tertiary treatment (POTW 38) but chlorinated the flow prior 

to the fi7,ter, and dechlorinated the effluent from the filter (12 

hours/day). The final effluent from this plant is listed under 

this heading. POTW 55 utilized spray irrigation as a tertiary 

treatment. The effluent from the irrigated fields (underdrains) 

was sampled at this facility. 

Gravity Thickener Overflow 

At POTWs 3, 29, 30, and 32, the overflow from the gravity thickners was recycled to the •head of the plant. Single grab samples 

were taken of this recycle stream at each plant. 

At POTW 59, the thickener overflow returns to the head of the 

primary tanks. A full set of 6 samples of this flow was taken at 

this plant. 

22 
Heat Treatment Decant 

At the two plants sampled that conditioned the sludge by heat 

treatment, ~ decant or supernatant samples from the heat treatment 

sludge decant (thickening) tanks were manually composited. At 

POTW 7, these samples were taken from a sample tap on the side of 

the decant tank (gravity flow), while at POTW 8 the decant 

samples were'.grabbed .from the sludge decant tank overflow weir. 

Vacuum Filter Filtrate 

Single grab samples of the filtrate from the vacuum filter at 

POTWs 1, 32, and 36 were obtained from the pressure line`s on the 

filters. A11 fractions were filled as one grab sample via an 

intermediate vessel. At POTW 26, manual composites were taken 

each day of the six day sampling period directly from the vacuum 

filter pumps. 

Digester Supernatant 

At POTWs 33, 34 and 36, the supernatant from the digesters was 

recycled to the head of the plant. Single grab samples were 

taken of this recycle stream at each plant. 

Other Intermediate Effluent 

At POTW 53, a complete set (6 days) of samples was taken of the 

effluent from the trickling filter prior to the polishing ponds. 

Other Recycle Line 

At two of the POTWs, unique recycle lines flowed back into the 

head :works of the plant. At POTW 26, an ash pit was decanted 

back to the headworks and at POTW 40, an aerobic digester supernatant flowed back into the influent wet well. Single grab 

samples were taken at each of these sample points. 

Other Source 

At POTW 26, a single grab sample was taken of the filter backwash 

that was recycled to the head of the.grit chambers. At POTW 30, 

two separate influent samples had to be taken to represent the 

total influent flow. One was considered °Influent (Other)," and 

the other was characterized as "Other Source." At POTW 40, the 

drying bed underflo,w was sampled as a single grab sample to 

characterize this additional recycle line. 

Primary Sludge (Raw) 

At each plant an attempt was made to sample the primary sludge as 

it was removed from the primary clarifiers, before any further 

treatment. Composite samples of the sludge were always collected 

23 
by grab sampling techniques for two reasons: sludge consistency 

and lack of continuous availability. The majority of the'se 

samples were taken from taps either on the sludge pumps themselves or on the lines conveying the sludge to storage or further 

treatment. Occasionally, the sludge point would be in a rising 

we11 controlled by telescoping valves. The consistency of this 

sample varied depending upon the means utilized by the respective 

plants for drawing the sludge from the primary tanks. Samples 

were taken so as to attempt to represent the average sludge consistency. This involved collecting sludge grabs spaced over the 

sampling day, or individual aliquots for each grab sample 

spanning definite pumping periods. Primary sludge samples were 

collected at 29 of the 50 plants. 

Primary Sludge (Digested) 

At POTW 10, raw primary sludge was pumped directly to digesters, 

with no accessible intermediate taps or valves for sampling. 

Consequently, six samples of the digested primary sludge were 

taken. This sample was collected from a pump tap as a manual 

grab composite. 

Primary Sludge (Thickened) 

At two of the POTWs (Nos. 3 and 18), the raw primary sludge was 

not accessible, necessitating collection of primary sludge after 

gravity thickening. Sampling procedures and techniques for this 

point were the same as the sampling procedures for the raw primary sludge. 

Primary Sludge (Other) 

POTtnT 30 had separate treatment trains through primary treatment 

which yielded two primary sludges. Both were raw pri.mary sludges 

with one listed as "raw" and the seqond one listed as "other." 

Waste Activated Sludge (Untreated) 

Waste activated slui3ge (WAS) sample points varied from plant to 

plant, depending on WAS stream accessibility. At some plants, 

WAS was accessible in rising wells prior to sludge conditioning. 

If the rising wells were sufficiently mixed, automatic samplers 

were used to gather WAS samples. At plants without rising wells, 

or when the well was not mixed, samples were taken from taps on 

the sludge pumps. Often, however, there were no accessible 

sampling points on the WAS line. In these cases, since WAS and 

return activated sludge are usually identical, samples were taken 

from the return sludge pumps or return sludge lines. The return 

sludge or waste activated sludge point was sampled at 27 of the 

50 plants. 

24 
Waste Activated Sludge-DAF Thickened 

At POTW 2, an additional sample of the waste activated sludge was 

taken after it had been conditioned in a dissolved air flotation 

(DAF) system. This was a,single grab sample. 

Secondary Sludge (Humus) 

These samples represent all the trickling filter (humus) sludges 

taken for this 50 POTW study. When the sludge consistency would 

allow, and if the sample point was accessible and well mixed, the 

samples were gathered via an automat'ic sampler. For all other 

cases, the samples were manually composited. 

Waste Activated Sludge (Other Thickened) 

At POTW 10, two manually collected composite samples were taken 

of the waste activated sludge after centrifugation. The samples 

were taken from a tap on the pump conveying the thickened sludge 

to the digesters. At POTW 50, the unthickened waste activated 

sludge was not accessible, so a complete set (6 days) of samples 

was taken of the gravity thickened waste activated sludge. 

Secondary Sludge (Other) 

At POTW 23, the secondary sludge was taken from the secondary . 

clarifiers after the aerated lagoons. At POTW 33, secondary 

sludge was taken from the secondary clarifiers after - the rotating 

biological contactors. 

Combined Sludge-Raw From Primary 

Fourteen of the 50 POTWs recycle their secondary sludge directly 

back into the primary clarifiers and have access to the sludge as 

it leaves the primary tanks. At these plants, a combined sludge 

sample was taken in the same manner descraibed for .primary sludge. 

These samples were composited directly f,rom.the primary tanks 

prior to any sludge conditioning. 

Combined Sludge-Secondary Thickened 

At POTWs 2 and 8, the secondary sludge a ~ ter DAF thickening was 

combined with unprocessed primary sludge for further processing. 

Samples of this combined sludge were take.n by grab sampling techniques. 

Nitrification Sludge 

Two of the plants followed their activatecl sludge process with 

nitrification processes (POTWs 20 and 25). At these plants, two 

grab samples of the waste nitrification sludge were taken. These 

samples were taken directly from the waste sludge as single grab 

samples. 

25 
Combined Sludge (Untreated) 

; 

,Y.. 

At POTW 1 1 a manual' W flow"composite sample"

, of

~ both primary and 

waste activated sludges was taken and analyzed as a combined 

sample of the total sludge. At POTW 7, the separate sludge from 

the primary settling tanks was not accessible, so a sample of' theP y slud e ~ was taken after it was combin., 

, . -. . 

ith;the waste 

activated slud e spri.o.r to: heat treatment. 

 ~. 

rimar 

_ gg eW 

• ' 

. .. . 

g

:o th~

,,. 

AritOchamber

the

reventin c tsamt,l din s~of the ri

is re turned t e aerated • 

g p g p g p mary sludge alone. 

Spince yhe slud e'is'nPt acce ~

hsebcomWhen 9 ' it is g rem~oved ° from the 

rl.mar tanks, a sam le oft binea` slud e' `rior to heat 

: treatment was taken. ' , . - . - .. , , , • ~~ ,:; ~ , , 

~. ' y, , , 

, :, ,.., 

, 

. 

Combined Sludge (y Both" Tliickened')" 

Att the four POTWs wh:ere sludge,from the secondary clarifiers was 

not immediately :;ac 'cessible, - (Nos. 3, 17; 59, ` and' 60 ), samples were 

taken after the - ' sludge- ' had;; been gravitym thicken`ed `and combined 

with the thickened, prima'ry . sludge, ` 

Combined Sludge, (Dige'sted ) 

At POTWs 4, 5, 6, and 57, the combined sludge sample was taken° 

after anaerobic digestion. 

Combined.Sludge (Heat Treated) 

In 

on 

 an , effort' to - ekploare' ,th'e. eff

sams

les • fhe' he p 

pziori.ty pollutan:ts, sludge p, rom th

t;treatment' rocessrt 

e heat treatment 

systems at POTWs `7,,8, 30_, and 60 were taken.'" 

: _ . 

Combined Sludge. (Oth°er) ° " 

At POTW:16, which has two parallel treatment trains, two separate 

primary clarifier sludge's we're, sampled.; At ,this particular 

plant, the pr`imary tank sludges: included the waste secondary 

sludges because these.sludges,were recycl'ed to the head of the 

primary systems. ' One trickling filter'combined sludge was categorized under this heading, whereas, the combined sludge from the 

parall,el plant was categorized as, "Combined Sludge - Raw from 

Primary .

17 

. . .... . .:> • . . .. . . .,.. - . . 

Combination of Sources 

At POTW 10, two manual coinposite samples of the aerobic digester 

feed were taken. The sample was a -combinat,ion of the thickened 

waste activated-sludge and` the floatables`. Manual samples were 

taken at this point from a tap on the sludge feed pump. 

4. 
v 

DATA ORGANIZATION AND INTERPRETATION 

DATA ORGANIZATION 

All analytical data developed during the 50 POTW study were 

stored on computer using the RAMIS II (Rapid Access Nianagement 

Information System, Release 2.1.0) Data Base Management System 

(DBMS). A description of the data elements computerized and 

their approximate organization is presented in Figure 1. The use 

of a DBMS provided, , significant cost savings.in data storage and 

retrieval and increased flexibility in programming all output 

tables and files. Where statistical evaluations were required 

for data analyses, the'Oniversity of California, Los Angeles BMDP 

Biomedical Computer Programs (P-Series, 1979) were utilized. 

The overall data base genera~ed during the course of this study 

is derived from a total of 1532 individual water, wastewater, 

sludge and tap water samples that were collected at the 50 POTWs 

and analyzed for conventional, non-conventional and the 129 

priority toxic pollutants. A significant number of blank 

samples, duplicate samples and spiked samples were also analyzed 

for QA/QC purposes. 

LABORATORY DATA REPORTING PROTOCOL 

The 50 POTW sampling program spanned approximately 2-1/2 years 

and analyses were conducted by several different laboratories. 

Consequently, to assure maximum consistency, most of the•laboratories calibrated their equipment against a standard "cocktail" 

of known priority pollutant concentrations which were prepared by 

EPA. However, there were some minor variations in reporting formats used by the various laboratories. Most notably: 

1.` The EPA Region 7 laboratory reported each pollutant in each 

wastewater sample as its measured concentration, as less than 

a specific reported detection limit (LT value), or as below 

the detection limit with a trace (unquantified) amount 

detected. 

2. Several EPA contract laboratories reported each pollutant in. 

each sample as either a measured concentration, or as 

"Not-Detected." 

3. Several EPA contract laboratories reported each pollutant in 

each sample as either a measured concentration or as less 

than an average detection limit for that pollutant. Commonly 

reported detection limits for organic priority pollutants 

were 5 ug/1 and 10 ug/1. 

27 
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4. Two EPA contract laboratories that performed sludge analyses 

reported each pollutant for each sample as present at a 

measured concentration, as "Not-Detected," or as not run 

because of analytical interferences. 

5. One EPA contract laboratory, which analyzed the pilot study 

samples, reported each pollutant for each sample as a 

measured concentration, as "Not=Detected" or as detected, but 

less than a reported detection limit (LT value). This last 

condition was not:usable by .the computer programs for the 

subsequent data`base analyses, since it was indistinguishable 

from the reporting format from Region17, where the "LT value" 

had a different meaning. Consequently, the "LT values" for 

this laboratory'were: made consistent with the Region 7 definition•by;assuming,a concentration of half the detection 

lim:it. For exampie,:a 'reported analysis`of "Detected at iess 

than 10 ug/1" was entered on the data base as 5 ug/1. The 

original values have also been maintained on the computer. 

In order to 'convenientl,y handle- all `of the reportirig formats on 

the computerized data; base,,every.analytical result was entered 

with a"key" code, used ih conjunction with the data value. The 

codes"and combinations used and their.meanings,are<as follows:: 

CODE .. , DATA VALUE _ MEANING 

0 any Detected,'at the concentration listed 

1 any Less than the concentration listed 

2 any Detected at greater than the concentration listed 

3 any Detected, but_ not quantified at lower 

than the concentration listed 

4 0 An analytical interference prevented the 

-. determination of the pres.ence or quanification of the pollutant t

4 > 0 Ananalytical interference was present, -

bu

.

t the concentration is estimated as 

reported 

5 any An analytical interference was present, 

but the pollutant was not detected above 

the concentration listed 

6 0 No analysis was run or reported 

7 0 Reported as "Not-Detected" 

at 
CODE DATA VALUE MEANING _ 

8 0 The compound was detected, but,.could not 

be- quantified 

8 > 0 A pesticide - was detected by"GC-EC at.the 

concentration listed,`but.:GC-MS did not, 

confirm the presence of this pollutant. 

DATA INTERPRETATION AND PRESENTATION 

In presenting the overall POTW data, four different formats are 

utilized in this report; namely, the Daily Tables, the Summary of 

Analytical Data Tables, the Mass Balance Tables and the Summary 

of Percent Occurrence Tables. A brief discussion of each of 

these formats follows. 

Daily Tables 

A Daily Table was selected as the basic format to report the analytical results corresponding to each day of sampling at a POTW. 

The Daily Tables were compiled by assembling the analytical.data 

on the pollutant parameters reported by the various laboratories 

for each day of sampling for all sample points at each of the 50 

POTWs. Accordingly, the Daily Tables embody the basic data on 

the conventional, non-conventional and priority pollutants in the 

wastewaters and the sludge streams of the POTWs.- Due to the 

extensive amount of data obtained,"the Daily Tables for each of 

the 50 POTWs are presented in Volume II , of"this report.` 

Summary of Analytical Data Tables 

These tables present the averages of each po-llutant parameter 

found at each sample point of a POTW over the duration of its 

sample period. These tables are derived from the Daily Tables by 

averagi.ngover the total number of days in the sampling period 

for a particular plant. The Summary of Analytical Data Tables 

for each of the 50 POTWs are presented in Appendix C of this 

Volume. 

Percent Occurrence Tables 

These tables present the percent of times each pollutant was 

found at each sampling point at each plant. In all cases where 

pollutant concentrations were reported by the laboratories in 

terms of "not detected" (ND) or °less than the detection limit" 

(L), i.t was assumed in the calculation of occurrence percentage 

that the pollutant did not occur in the analyzed sample. Percent 

Occurrence Tables for each of the 50 POTWs are presented in 

Appendix D of this Volume, and are summarized for the 40 and 10 

POTW data bases in Section VI. 

30 
Mass Balance Tables 

The Mass Balance Table for a POTW shows the average pounds per 

day of each pollutant entering the POTW,-as well as the daily 

pounds of that pollutant exiting the POTW. Mass Balance Tables 

are derived from the Summary of Analytical Data Tables and the 

appropriate flow quantities for the wastewater_ and sludge 

streams. In some cases samples could not be obtained from all 

recycle lines that would be necessary to obtain an exact mass 

balance. Mass Balance Tables based on the major wastewater and 

sludge streams for all 50 POTWs are presented in Appendix E of 

this Volume. 

QUALITY ASSURANCE PROGRAM 

As part of an agreement among the Office of Water Regulations and 

Standards, Effluent Guidelines Division, EPA's Region VII 

Laboratory and other contract laboratories, a Quality Assurance 

Program was designed and executed to provide estimates of data 

quality for priority toxic pollutant analyses performed:by the 

various laboratories. An interim and final report have each beenprepared. For the sludge and water samples, QA/QC results are - 

summarized in the following paragraphs. However, analytical 

results reported by the laboratories and utilized in this study 

have not been adjusted for any QA/QC findings. 

QA/QC activities in the £ield consisted primarily of colledting 

duplicate and blank samples. In general, during each sampling 

episode the.field crew collected the following QA/QC samples: 

o One duplicate sample at each sample point; 

• One sampler blank for all wastewater sample points at each' 

POTW; 

• One sampler (or fiel'd) blank for each sludge sampling point;' 

o Trip (or VOA) blanks.for one wastewater sample point, filled 

in the field; and 

o Trip (or VOA) blanks for each sludge sampling point, filled 

in the field. 

A sampler blank consists of ultrapure deionized water pumped - 

through autoinatic samplers and associated tubing and analyzed forpriority toxic pollutant acid, base/neutral and pesticide parameters. Where an automatic sampler was not used, this blank (often 

called a field blank) consists of filling a sample container with 

ultrapure water at the field site and analyzing for the same 

parameters. VOA (or trip) blanks consist of filling VOA vials 

with the ultrapure water, exposing them to the environment at the - 

treatment plant and sealing them air tight with no entrapped air. 

31 
These samples were analyzed for the volatile priority pollutant 

fraction. 

The purpose of the blanks was to identify field and analytical 

contamination such as methylene chloride (a solvent used extensively both during bottle preparation and laboratory analysis) or 

phthalate ethers (which may be associated with the sample 

tubing). The analysis of blanks is critical, especially when the 

purge-trap technique (which is susceptible to contamination by 

residues from concentrated samples or vapors in the laboratory) 

is employed. Sporadic occurrences of inethylene chloride were 

identified in several of the VOA blank samples. Thus in 

reviewing the methylene chloride results, it sho.uld be kept in 

mind that methylene chloride results which deviate significantly 

from the mean may in fact be the result of field and/or laboratory contamination.' No other pollutants were identified * 

repeatedly or in high concentration in the blank water samples. 

The precision of the analytical results can be expressed by the 

standard deviation of the results of multiple duplicate or spike 

analyses for a selected pollutant. The precision of the analytical results refers to the ability to reproduce the same results, 

regardless of whether the results are true values or the results 

of systematic analytical errors. In summary, the lower the standard deviation the higher the analytical precision. 

Accuracy, on the other hand, is a measure of the correctness of 

the analytical results in comparison to the actual amount of the 

analyte present. Known quantities of priority pollutants and/or 

surrogate spikes (compounds with identical chemical structures as 

that of a given pollutant except that the surrogate has a unique 

aspect which is more readily identifiable) were added to both 

wastewater samples and blank samples. Wastewater spike data 

constitute matrix spike results; blank spike results are referred 

to as method spike results. The percent recovery is a measure of 

the analytical accuracy for the respective parameters. As previously indicated, the standard deviation of the percent recovery 

is a measure of the parameter analytical precision. The discussion below presents an analysis of the QA/QC data for the 

wastewater and sludge samples. 

Regarding the wastewater samples, the results of the QA/QC 

program indicated some variation between the various laboratories 

used. For the acid fractions, the mean recovery rates at the 

different laboratories ranged from 63 percent to 100 percent, and 

for base-neutrals the range was from 48 percent to 74 percent. 

For the volatile organic fraction, the mean recoveries ranged 

from 57 percent to 100 percent. The EPA Region VII laboratory, 

which handled the majority of wastewater samples for this study, 

had mean recoveries of 71 percent for acids with a standard 

deviation of 28 percent, 73 percent for base neutrals (38 percent 

standard deviation), 81 percent for pesticides (36 percent stan-- 

32 
dard deviation) and 100 percent for volatiles (17 percent standard deviation). 

Metal priority pollutants had the most consistent recovery rates, 

especially at concentrations above 25 ug/1. For the priority 

pollutant metals (excluding asbestos and cyanide), recoveries 

ranged between 83.9 percent (arsenic) to 99.9 (mercury) and 

averaged 90 percent for the group. Standard deviations ranged 

from 6.1 percent (beryllium) to 36.8 percent (thallium). 

The sludge samples showed significantly higher variations in 

recovery rates and larger standard deviations than the wastewater 

samples. For the individual,organic priority pollutants, recoverie.s ranged from 0 percent to over 100 percent, with the same 

range for the standard deviations. As an example, the recoveries 

and standard deviations for the two most frequently occuring 

organic priority pollutants in sludges are indicated below: 

Toluene 

Mean 

Recovery Standard 

(percent) Deviation 

Bis-2-ethylhexyl 

phthalate 

Mean 

Recovery Standard' 

(percent) Deviation 

Primary sludges 148 175 65 34 

Secondary sludges 146 237 75 28 

Combined sludges 106 93 64 44 

Percent recoveries for metals were more consistent, with the 

individual recoveries in primary, secondary and combined sludges 

ranging from 61 percent (for cadmium) with a 53 percent standard 

deviation to 136 percent (for lead) with a 131 percent standard 

deviation. 

33 

vi 

EVALUATION AND DISCUSSION OF ANALYTICAL DATA 

OVERVIEW OF PRIORITY POLLUTANT OCCURRENCE 

Tables 3, 4, and 5 present occurrence data and concentration 

ranges for influent, secondary effluent and raw sludge samples 

for POTWs 1 through 40. The same data for the 10 supplemental 

POTWs are presented in Tables &, 7, and 8. For each of the 129 

priority pollutants these tables indicate the total number of 

samples analyzed, the number and percentage of times each pollutant was detected and the minimum and maximum concentrations of 

the detected pollutants. 

Tables 3 through 8 present a broad-based overview of priority 

pollutant occurrence, and all appropriate samples collected 

during this study are included. Consequently, the 40 and 10 

POTWs are not weighted equally, but according to the number of 

influent, effluent or sludge samples collected at the various 

plants. For example, this number ranges from a 1ow of 4 influent 

samples collected at POTWs 8 and 35 to 28 influent samples 

collected at POTW 1. Additionally, at POTWs where prechlorinated 

and chlorinated secondary etfluent samples were collected, both 

were included in the effluent occurrence t,ables. For these 

reasons, it is not meaningful to present "average" values for 

each,pollutant. 

For the purposes of interpreting the analytical data, the following assumptions were made in developing Tables,3 through 8: 

o A11 pollutants reported as '°Not-Detected" or "Less Than 

Detection Limit" were assumed not detected. 

o Unconfirmed pesti.cides were assumed not detected. 

o Samples where interferences prevented any analysis of that 

sample were not counted as data points. Where the laboratory reported an interference but quantified the result, a 

valid sample value was assumed. 

o Values reported as below the detection limit but present in 

trace quantities were assumed detected. 

The number of samples from each plant corresponds to the number 

of samples reported in Table 2. 

For Tables 3, 4 and 5, the following samples were considered in 

the definition of influent, effluent or raw sludge. 

Influent: All samples labeled Influent (Total), Influent 

t er and Other Source (at POTW 30 only). A total of 288 

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42 
influent samples were collected for the 40 POTWs. For some 

parameters, a lower number of samples are reported because 

of either interferences in the analysis or bottles broken or 

lost in transit or at the laboratories. 

Second aryEffluent: A11 samples labeled Secondary Effluent 

TURTo—rinated), Secondary Effluent (Other) and Secondary Effluent (Unchlorinated) were included. At dual plants where 

parallel unit processes were sampled, both effluents are 

included. A total of 303 samples were collected for the 40 

POTWs, although for many parameters a lower number of analyses were reported for the reasons outlined above. At plants 

where the secondary effluent was sampled both before and 

after the chlorination step, metals were generally sampled 

only at the final effluent, which explains the lower number 

of reported metals analyses. 

Raw Slud es: All unthickened or thickened primary, seconary, or combined sludge samples were included in this 

table, while digested and heat treated sludges were 

excluded. The sample points listed in Table 2 that are 

included are: 

o Combined Sludge (Both Thickened) 

o (Other) 

o Combined Sludge (Untreated) 

o Combined Sludge (Raw From Primary) 

o Combined Sludge (Secondary Thickened) 

o Primary Sludge (Other) 

o Primary Sludge (Untreated) 

o Primary Sludge (Thickened) 

o Secondary Sludge (Humus) 

o Secondary Sludge (Other) 

o Waste Activated Sludge (Untreated) 

o Waste Activated Sludge (Thickened) 

o Waste Activated Sludge (Other Thickened) 

A total of 443 sludge samples were collected, although a lower 

number is usually reported because of the rnany analytical 

interferences. 

The occurrence data in Table 3 show that in influent samples from 

the 40 POTW data-base, a total of 102 priority pollutants were 

measured at least once above their detection limits. However, 

only 40 pollutants were detected in 10 percent or more of these 

samples, and 24 pollutants were measured in approximately 50 percent or more of the samples. The majority of the data evaluations in this section focus on these 24 pollutants. 

Table 4 indicates that 90 priority pollutants were detected in 

any secondary effluent, although only 12 were detected in more 

than 50 percent of the samples, and 30 were detected in 10 per- 

, 43 
cent or more of the samples. In both the influent and effluent 

samples, copper, cyanide, and zinc were the most commonly 

measured pollutants. 

Priority pollutant occurrence in raw sludge samples is presented 

in Table 5. A total of 78 pollutants were detected at least 

once, and 22 pollutants were detected in more than half the 

samples, while 43 pollutants were detected in more than 10 percent of the samples. Twelve of the 16 most commonly occurring 

pollutants were metals. ' 

Tables 6, 7 and 8 show the occurrence,of priority pollutants in 

the 10 supplemental POTWs influent, effluent and sludge samples, 

respectively. These tables are based on the same sample locations for the 40 POTWs with the following exceptions.,: 

Influent : A11 influent samples are Influent (Total): 

Effluent: All effluent samples are Secondary Effluent 

Chlorinated) except Plant 55 where samples were unchlorinated and Plant 56 where only Tertiary Chlorinated Effluent 

was sampled. 

Raw Sludge: All raw 

~ocations: 

o Primary*Sludge 

o Combined Sludge 

o , Combined Sludge 

o Waste Activated 

o Waste Activated 

sludge samples are from the_following 

(Raw) 

(Untreated) 

(Both Thickened) 

Sludge (Untreated) and 

Sludge (Other Thickened) 

In total, 60 influent samples, 60 effluent samples and 81 sludge 

samples were taken. Similar to the reasons"stated abovet the 

number of samples analyzed may be less than these values. In 

addition, analytical capacity was not available to perform organics analyses on approximately 50 percent of the sludge samples 

in the supplemental study. Therefore, where some metals have° , 

reported v.alues for all 81 samples, the organic fractions have a 

maximum of 42 reported values. 

The most frequently found pollutants in the 10 supplemental 

plants are nearly i.dentical to those found in the 40 plant study. 

A further discussion of the 10 plant data is presented later in 

this section. 

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50 
SUMMARY OF INFLUENT POLLUTANT CONCENTRATIONS 

Table 9 presents the average and median influent concentrations 

for the priority pollutants detected in more than 50 percent,of 

all influent samples. Several different definitions of "average" 

were utilized, since each may be more meaningful for specific 

applications. The first column'is the average of the average 

value from each of the 40 POTWs. This method assigns an equal 

weight to each POTW. For several parameters, such as methylene 

chloride and 1,1,1-trichloroethane, very high values from a few 

POTWs have significant impact on the overall average. The second 

column indicates the median value from the same data base of the 

40 POTW plant average. The few plants with very high concentrations for a pollutant do not have major significance in the 

median computation. The third method presents the flow.weighted 

average concentrations, based on the same 40'POTW indiviclual 

plant average concentrations and that plant's reported flow 

during the sampling period. For most parameters the flow 

weighted average is close to the average of the .40 ,POTW . individual averages. 

For the calculations used in developing Table 9, all influentvalues reported below the detection limit, or "Not-Detected" were 

averaged as zero. Also, unconfirmed pesticides were averaged as 

zero since they have previously been assumed to"be not detected. 

Table 9 is most meaningful when utilized in conjunction with 

Table 3, which indicates the percentage occurrence for each 

priority pollutant in POTW influents. 

IMPACT OF INDUSTRIAL CONTRIBUTION ON INFLUENT QUALITY 

The amount of industrial wastewater discharged to the 40 POTWs 

ranged from 2 percent to a maximum of 65 percent of their aver-age 

flow (see Table 1). Review of the influent priority pollutant 

data reveals that, in general, the higher the industrial contri= 

bution, the greater the concentration. This trend is exhibited 

for all of the major priority pollutant fractions. Figures 2, 3 

and 4 present plots of the percent industrial contributions versus the sum of influent priority pollutant concentrations'for the 

metals, volatiles, and base neutrals, respectively. A11 three 

plots indicate a fair amount of data point scatter, but all three 

have least square fits with a positive slope. This indicates a 

tendency for the total priority toxic pollutant concentrations to 

increase when percent industrial flow increases. There are a 

number of other factors that might be expected to influence 

priority toxic pollutant concentrations. Among the major ones 

are: 

o The inconsistencies between POTWs in the definition of 

industrial flow (this was discussed in Section II). 

o Differences between plants in their collection systeins and 

the'nature of the non-industrial "background" contribution. 

51 
~O N ~ 

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.0 \O+ 

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J.~ 

af JpJ EO ro iJ iJ 

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52 
FIGURE 2 

CORRELATION OF PERCENT INDUSTRIAL FLOW 

TO INFLUENT TOTAL METALS CONCENTRATION 

10500 

9750 

~ 

~ 

~ 8250 

a 

~ 

c 

~ 6750 

ro N 

-p 

c 

a~ 

U 

o 5250 

U 

m 

r-i 

~ 

~ 

U 

~ 

• 

Number of POTW's at 

Coincident Plotting aositions 

41 = 1 ` =2 ® =3 

Regression Line 

• 

I'MC (ug%1) = 49.2 PIF (%) + 296.8 

Correlation Coe£ficient (R) 

0.366 

Number of POTW's Included 

40 

rt 3750 (d 

-p 

0 

H 

2250 

° 750 

10 20 30 40 50 60 70 

Percent Industrial Flow - PIF 

-53 
24500 

21000 

~ 

\ 

~ 

~ 

v 17500 

~ 

~ 

~ 

0 

'+~ , 14000 

~ 

u 

~ 

~ 

a~ 

U 

~ 

0 

V 10500 

m " 

a~ 

~ 

~ 

~ 

~ 

~ 7000 

~ 

~t 

4J 

0 

H 

3500 

FIGURE 3 

CORRELATION OF PERCENT INDUSTRIAL FLOW 

TO INFLUENT TOTAL VOLATILES CONCENTRATION 

m 

• 

Number of POTW's at 

Coincident Plotting Positions 

• = 1 ,0, = 2 ■ =3 

Regression Line 

• • 

TVC(ug/1) = 83.2 PIF(%) + 36.2 

Correlation Coefficient (R) 

0.266 

Number of POTW's Included 

• • 

40 

• 

• • 

~ '~o•• •_ ~ • ~ • A • 

~ -~ -- 

10 20 30 40. 50 

Percent Industrial Flow - PIF 

60 

54 
FIGURE 4 

CORRELATION OF PERCENT INDUSTRIAL FLOW 

TO INFLUENT TOTAL BASE-NEUTRALS CONCENTRATION 

1050 

~ 

~ 

~ 900 

v 

U 

z 

H 

c 750 0 ., j 

-p ~ 

~ 

+~ ~ 

~l 

~ 600 

0 

U 

Ul 

r-1 

~ 

H 

~ 450 

~ 

z 

a~ 

~ 

~d 

~ 

~ 300 

rt 

~ 

0 

H 

150 

• 

Number of POTW's at 

Coincident Plotting Positions 

• = 1 ♦ = 2 i = 3 

Regression Line 

TBNC (ug/1) = 1. 0 PIF (%) + 96 

Correlation Coefficient (R) 

0.09"1 

Number of POTW's Included 

37 

• 

• 

• • 

• ® 

•• •• • ~ 

~ •• • .• •• • •"j ~ • ~ • 

0 

10 20 30 40 50 GJ 

Percent Industrial Flow - PIF 

55 
This has the greatest influence at POTWs with low influent 

priority pollutant concentrations. 

.o Different levels of pretreatment program development and 

enforcement between the different cities. 

Additionally, the contribution of priority toxic pollutants is 

associated largely with specific industrial categories. The preceding analysis only dealt with the total reported industrial 

flow, and not with only those industries that are expected to 

contribute priority pollutants. However, during the time frame 

of the 40 POTW sampling program, only about 25 percent of the 

plants had completed their Industrial Waste Survey associated 

with their pretreatment program. Consequently, most plants did 

not have a complete and thorough list of all of their contributing industries. 

To determine whether the correlation could be strengthened by the 

screening of certain data subject to the above interferences, two 

additional analyses were attempted. The first was to examine the 

correlation for only POTWs that had higher influent concentrations of priority pollutants than the average of the 40 

POTWs averages. This minimized the interferences from the plants 

where the detection limits or nature of non-industrial sewage had 

the most significant effects on the reported concentrations. 

This analysis resulted in a much improved correlation coefficient 

for total metals (R increased from 0.366 to 0.677.) _However, the 

correlation coefficients for total volatiles and total base 

neutrals both decreased slightly (from R= 0.266 to 0.141 and 

R= 0.091 to 0.083, respectively.) 

The second analysis consisted of screening those POTWs (nine) 

that had initiated their pretreatment programs. It was hypothesized that these nine cities would have significantly lower 

influent priority pollutant concentrations than cities with similar industrial contributors that had not yet developed or 

enforced any pretreatment regulations. This screening resulted 

in a more uniform data base of 31 POTWs with a large variety of 

industrial flow. For these 31 POTWs, the correlation coefficients for the total metals, total volatiles and total base 

neutrals all increased slightly; from 0.366 to 0.418, from 0.266 

to 0.342,`and from 0.091 to 0.130, respectively. 

TREATMENT OR'REMOVAL OF PRIORITY POLLUTANTS IN POTWS 

Appendix B presents cumulative distributions of the percent 

removals and effluent concentrations for the 24 priority pollutants 

detected 50 percent or more of the time in POTW influents. Table 

10 summarizes the data presented in Appendix B. In Table 10, 

percent removals are presented for two subgroups of analytical 

data: removals where the priority pollutant ,average influent 

concentration was greater than zero, and removals when the plant 

56 
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57 
average influent concentration.was signific.antly above the 

pollutant's de.tection limit: °For -tYie ~ purposes of Table 10, 

"significantly above the detection limit" was defined as four 

times the most frequent, detect.ion_; 11mit., :This minimi.zes theeffect of the detection limit`. on, calculating percent removals. 

The number of data points for each subgroup is indicated by N. 

Minimum percent removals and effluent levels can be read directly 

from Appendix B for any desired percent of POTWS in the data 

base. 

Table 10 shows that 50 percent of the POTWs sampled achieved 

minimum priority - pollutant metal removals ranging from 35 percent 

to 97 percent. For the selected organic priority pollutants 50 

percent of the POTWs achieve minimum removals of.51 percent to 

over 99 percent. Many of the organic removal rates that are 

close to 100 percent occur primarily because the average pollutant concentration in the influent was sli.ghtly above that 

pollutant's detection limit and the pollutant was not detected in 

the e£fluent sample. This is illustrated in Table 10 by comparing the number of sample points between the two different 

subgroups. For many of the organic pollutants, there were an 

insufficient number of ineaningful data sets to draw accurate 

conclusions about pollutant removal rates. 

Figures 5 and 6 present cumulative distributions for the four 

major priority pollutant fractions. These curves summarize the 

data presented in Appendix B and Table 10. In Figures 5 and 6 

and Table 10, all values reported as "not detected" or assumed to 

be "not detected" were averaged as 0 in both influent and 

effluent samples. .This procedure will slightly overstate removal 

of pollutants near their detection lirnit in the influent, but 

these cases have minimum impact on the median removals and percentile removals presented. 

It is important to note that the data in the above analyses only 

indicate the reduction of a pollutant from the influent to the 

secondary eff luent at POTWs . They do not ind icate that the 

pollutant has been treated by the POTW, but ha.s only been removed 

by one of the many removal mechanisms possible (biodegredation, 

adsoprtion, clarification, air stripping, etc.). Estimates of 

the ultimate fate of these,pollutants are best obtained from the 

mass balance tables preserit`ed in a subsequent section. 

REDUCTION OF PRIORITY - POLLUTANTS BY POTW TREATMENT PROCESSES 

Table 11 summarizes the median removals for selected. conventional 

and priority toxic pollutants by the various types of treatment 

plants sampled in the 40 POTW study. The types of treatment 

plants are activated sludge plants, trickling filter plants, 

pure oxygen activated sludge plants, an RBC plant, an aerated 

lagoon and four treatment plants that have both activated sludge 

processes and trickling filters in parallel modes. POTW 8, which 

: 
FIGURE 5 

CUMULATIVE'DISTRIBUTION CURVES 

TOTAL METALS AND TOTAL VOLATILES EFFLUENT CONCENTRATION 

AND PERCENT REMOVAL 

Metals Volatiles 

100 

~) 80 

~ 

> 60 

0 

a 

4J 40 

0 

v 

U 

}~ 

po, 20 

0 

100 

80 

60 

40 

20 

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has an activated sludge process that treats 96 percent of 

influent flow and trickling filters that treat 4 percent of 

in£luent flow was included with the activated sludge plants. At 

plants where primary or tertiary effluent was sampled, removals 

by those treatment processes are also indicated. Several plants 

were excluded from this data base because they consisted of a 

combi.nation of fixed and suspended growth biological treatment in 

series . 

Table 11 shows that among the treatment plants examined, 

trickling filters, activated sludge, the RBC, and the pure oxygen 

systems achieved good removals of conventional pollutants and 

most of the measurable priority pollutants. At those plants that 

h3d activated sludge and parallel trickling filtration plants, 

the activated sludge plant appeared to remove slightly more 

priority pollutant metals and organics than the trickling filter 

plants. However, for some parameters the trickling filter plants 

achiAved higher removal rates. 

Primary treatment was less effective than any secondary treatment 

for conventional and priority pollutant removal. It sho.uld be 

noted that the primary effluent samples from this study may not 

be representative of primary treatment plants. The major reason 

iS that secondary treatment plants generate a much greater volume 

of sludge than primary treatment plants, and many of the sludge 

processing side streams are returned to the primary tanks. This 

often causes the influent to the primary tanks to be much higher 

in organic loading than the influent to a typical pri:mary treatment plant. Nevertheless, primary treatment removed from 10 percent to'57 percent of priority pollutant metals and from 0 percent to 56 percent of the priority pollutant organics, based on 

the plant influent and the primary effluent. Tertiary treatment 

was slightly more effective than average secondary treatment for 

removing conventional and priority pollutants based on eight 

plants that had either.mixed media filtration or polishing ponds. 

POTW PRIORITY POLLUTANT MASS BALANCES 

As indicated in Section V, mass balances for conventional, 

selected non-conventional and priority pollutants are included in 

Appendix E. These mass balance tables should, in theory, show 

the same pounds entering the plant as leaving it for conservative 

pollutants such as metals which cannot be degraded but settle out 

in sludges or remain in the water stream. On the other hand, 

pollutants which are degraded, stripped into the atmosphere or 

otherwise removed from the'water and sludge streams should show a 

lower mass exiting the plant than entering in the influent. Due 

to possible inaccuracies in the sludge flow informati.on obtained 

from the plants and/or analytical inaccuracies in the sludge analyses, good mass balances for the conservative pollutants could 

not be developed for several of the POTWs. However, Table 12 

summar`izes`the mass balances for 6 POTWs where the percent dif62 
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ference between the pounds of total metals in the incoming and 

outgoing streams were reasonably close. For these six plants, it 

is assumed that the balances for all other pollutants should be 

equally accurate. 

Table 12 shows that deviation from total prinrity pollutant metal 

mass balances range between a gain of 11 percent and a loss of 12 

percent. Volatile pollutants were always lost and ranged from 13 

percent lost to 96 percent lost. It should be noted that the 

smallest loss, at POTW 32, was abnormally influenced by methlyene 

chloride values which accounted for over 95 percent of both the 

incoming and outgoing balance. By looking at the daily data 

tables for POTW 32, it appears that some laboratory or other contamination was experienced. The mass balance for base neutral 

pollutants ranged from a 10 percent gain to an 88 percent loss. 

The acid extractables were found too infrequently and at such low 

levels that meaningful conclusions were difficult to draw. 

The results•discussed above support the concept that metals are 

conservative in a treatment process while organics are either 

biodegraded or otherwise lost. The greater loss of volatile 

priority toxic pollutants compared to the base neutrals or total 

organic priority pollutants, also supports the idea that volatiles may be stripped out of the wastewater during aeration in 

addition to being biodegraded. 

DAILY VARIATION OF INFLUENT POLLUTANT CONCENTRATIONS 

Table 13 presents the daily average concentration of selected 

conventional, non-conventional and priority pollutants as well as 

the total priority pollutant fractions in POTW influent samples. 

With the exception of Sundays, at least one 24-hour composite 

influent sample was taken for each day of the week at 38 of the 

40 POTWs. Sunday samples were only taken at four of the 40 POTWs 

(see Section IV). 

Table 13 does not reveal any particular concentration trend among 

the five working days. None of these five days of the week 

showed a consistently high or lower concentration of the priority 

pollutant fractions of most individual pollutants. However, for 

every toxic pollutant fraction, as well as all priority pollutants metals and the conventional parameters indicated, the 

t4onday through Friday average concentration was always higher 

than the Saturday or Sunday average. The Sunday data should be 

viewed cautiously because of the abbreviated data base it represents. One discrepancy in Table 13 is that the volatile pollutant concentration on Saturday is much higher than the sum of the 

individual volatile pollutants listed for Saturday. This was 

caused primarily by a pollutant (1,2-dichloroethane) not listed 

i.n Table 13, but which accounted for an average concentration of 

over 800 ug/1 over the 40 plant data even though =it was infrequently detected. 

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65 
EFFECT OF RAINFALL ON INFLUENT CONCENTRATIONS 

During the week of sampling at 14 of the 40 POTWs, at least one 

day of heavy rainfall occurred. Table 14 presents the influent 

total priority pollutant metals loadings at these plants before 

and after the rainfall day and the average of all other days' 

loadings. The type of sewer system in each of these plants is 

also presented. Although there are many factors than can affect 

these data (weather prior to the sampling episode, infiltr.at'ion/ 

inflow problems, whether rainfall occurred on weekdays or 

weekends, etc.), there is a clear tendency shown for metals 

loadings to be highest on the days of and following rainfall than 

compared to the other periods. The peak flow occurred either 

during the day of rainfall or on the day after. Peak flow may 

occur on the day following rainfall because of either the detention time in the sewer system, which was not documented, or the 

rai.nfall may have occurred near the end of the sampling period. 

At several of the plants in Table 14, it was raining on the first 

day of sampling so no preceding dry weather periods could be 

included in the averages of other days. 

Table 15 presents a similar analysis for lead only. It was anticipated that lead would show this same tendency because of its 

widespread use in gasoline and the deposition of lead particles 

on pavement. As can be seen from Table 15, the same trends were 

indicated for lead as were indicated for the total metal pollutants. 

It should be noted that the data on Tables 14 and 15 are only an 

indication of the effects of rainfall. There were many interfering factors with this analysis, such as light rainfall during 

sampling periods which was unrecorded at thc treatment plant, or 

multi.ple days of rainfall during the six day sampling period. In 

these latter cases, only the first heavy rainfall was used and 

subsequent days were averaged as other days. In all cases for 

the rainfall analysis, pollutants measured below their detection 

limit in the influent were averaged as 0. 

FORMATION OF CHLORINATED HYDROCARBONS 

Table 16 presents a summary of occurrences where the secondary or 

tertiary chlorinated effluent had a higher concentration of a 

chlorinated hydrocarbon than the corresponding pre-chlorinated 

secondary effluent. Inconsequential data points were excluded 

from consideration by requiring that the post-chlorinated sample 

have a larger measured concentration than the pre-chlorinated 

sample's. Furthermore, some control tests run on some frequently 

occurring non-chlorinated compounds indicated that random 

variation would account for a pollutant being higher in the 

effluent than in the influent in approximately 25 percent of the 

cases where it was detected. Consequently, Table 16 only presents pollutants which exceeded the number of occurrences that 

might have been predicted by random variation. 

.. 
TABLE 14 

EFFECT OF RAINFALL 

ON INFLIIENT TOTAL NETALS LOADING 

(Pounds per Day) 

FIRST DAY OF 

gE(~7ER HEAVY RAINFALL DAY AFTER AVERAGE OF ALL 

PLANT NO. TYPE DORING SAMPLING PERIOD HEAVY RAINFALL OTHER DAYS 

4' 

50$ 

dorobined ~ 1286 (1) 392 396 (3) 

61 Separate 708 (1) 335 547 

9 Combined 197 102 204 

85$ 

94 (2) 66 

52 (g) 

13 Combined 

14 Combined 167 174 138 (3) 

18 Combined 824 250 268 

22 Separate 300 (1) 315 252 (3) 

75 (1) 162 103 (3) 23 Separate 

26 

67$ 

Combined 1346, (1) 994 993 (3) 

27 Separate 1305 (1) 2001 1263 (3) 

32 Separate 82 58 40 

34 Separate 193 (2) 1104 85 

35 

25$ 

Combined 107 163 88 

36 

10$ 

Combined 605 498 329 

(1) Rainfall occurred during first day of sampling 

(2) Heavy rains preceded the sampling episode 

(3) Additional rainfall occurred after first day of heavy rain 

67 
TABLE 15 

EFFECT OF RAINFALL 

ON INFLUENT LEAD LOADING 

(Pounds per Day) ° 

FIRST DAY OF 

SEWER EMVY RAINFALL DAY AFTER AVERAGE OF ALL PLANT NO. T7CPE DtJRING SAMPLING PERIOD HEAVY RAINFALL OTEER DAYS 

5 014 

4 Combined , 216(1) 54 63(3 ) 

6 Separate 18( 1 ) 5 12 

9 Combined 48 30 39 

858 

13 Combined 14(2) 8.0 6.0 (3) 

14 Combined 4 0 0 (3) 

18 Ccmbined 234 68 43 

22 Separatd 27(1) 40 32(3) 

23 Separate 0(1) 0 3 (3) 

67% 

26 Combined 247(1) 141 0(3 ) 

27 Separate 0( 1 ) 0 0(3) 

32 Separate 10 6.0 3 

34 Separate 22(2) 18 16 

25$ 

35 Combined 0 38 0 

10% 

36 Combined 57 66 42( 3 ) 

(1) Rainfall occurred during first day of sampling 

(2) Heavy rains preceded the sampling episode 

(3)Additional rainfall occurred after first day of heavy rainfall 

68 
TABLE 16 

FORMATION OF CHLORINATED HYDROCARBONS 

DURING CHLORINE DISINFECTION 

,Number of Average Concentration 

Parameter Occurrences. Pre-Chlorinated Post-Chlorinated 

Chloroform 39 2 ug/1 10 ug/1 

Dichlorobromomethane 27 - 1,ug/1 7 ug/1 

Chlorodibromomethane 13 1 ug/1 8 ug/1 

Gamma-BHC 25 62 ng/1 147 ng/1 

Note: Only instances where post-chlorinated sample had larger measured 

value than pre-chlorinated sample are included. 

.• 
Chloroform increased in concentration through the chlorination 

process in 39 instances. The average pre-chlorinated concentration was 2 ug/1 for these occurrences, and the average 

chlorinated effluent was 10 ug/1. For dichlorodibromomethane, 

there were 27 instances where it increased (from 1 ug/1 to 

7 ug/1, average). Chlorodibromomethane and gamma-BHC also 

increased significantly more often than can be explained by random variation. 

POLLUTANTS DETECTED IN SLUDGES WHEN NOT MEASURED IN THE INFLUENT 

Table 17 presents a summary of the priority pollutants that were 

detected in one or more sludge streams but were not detected in 

the corresponding influent sample. In many cases this occurs 

because the influent concentrations were too low to be measured, 

but the pollutant may have concentrated sufficiently in the 

sludge stream to be quantified. For example, arsenic and antimony were both detected in less than 15 percent of all POTW 

influent samples. However, both were detected consistently in 

sludge streams. Arsenic was detected 110 times in a primary 

sludge at an average concentration,of 186 ug/1 when it was not 

detected in the influent. It was also detected 84 times in combined sludges (384 ug/1 average) and 99 times in secondary 

sludges (77 ug/1) when not detected in the influent. 

The significance of Table 17 is that several pollutants only 

infrequently measured in POTW influents may, in fact; be frequently present in the influent at levels below their detection 

limit. 

CORRELATION OF INFLUENT AND EFFLUENT CONCENTRATIONS 

For all of the priority pollutants that occurred in over 50 percent of the influent samples, the correlation between plant 

average influent concentration and effluent concentration was 

tested. Table 18 presents the results for these pollutants as 

we11 as for BOD and TSS. For all of the metals on Table 18, the 

slope of the line computed by the least squares fit was between 

0.02 and 0.325 indicating that the majority of an incremental 

increase in influent concentration is removed by the POTW and 

cloes not pass through to the effluent. Interestingly, the 

highest slope was obtained for nickel, which also had the lowest 

median removal of the heavy metals (see Table 10). 

The organic priority pollutants exhibited the same trend as the 

metals. The correlation coefficients ranged between 0.059 and 

0.977. The slopes of the best fit line ranged between 0.003 and 

0.860. These slopes also indicate that the majority of most 

organic priority pollutants are removed by the secondary treatment process at the.40 POTWs. 

Based on the data in Table 18 it is reasonable to conclude that 

for many priority pollutants an increase in the influent con70 
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71 
TABLE 18 

CORRELATION OF INFLUENT AND EFFLUENT CONCENTRATION 

Correlation Slope of 

Parameter Coefficient Best Fit Line( 1 ) Intercept 

BOD .374 .069 10.4 

TSS .182 .024 17.7 

Cadmium .966 .060 1.2 

Chromium .402 .059 25.3 

Copper .536 .072 24.7 

Cyanide .102 .020 152.6 

Learl .354 .050 10.8 

Mercury 329 .130 71.4 

Nickel .795 .325 26.1 

Silver .523 .150 -0.1 

zinc .855 .256 -15.8 

Benzene .082 .004 1.0 

Bis(2-ethylhexyl) Phthalate .669 .347 7.1 

Butyl Benzyl Phthalate .207 .011 0.6 

Chloroform .837 .392 0.9 

Di-N-Butyl Phthalate .243 .081 2.8 

Diethyl Phthalate .476 .075 0.1 

Ethylbenzene .558 .037 0.4 

Methylene Chloride .977 .860 -73.5 

Naphthalene .589 :059 -0.1 

Phenol .287 .009 1.2 

Tetrachloroethylene .966 .151 2.0 

Toluene .059 .003 11.3 

Trichloroethylene .899 .110 -1.1 

1,1,1-Trichloroethylene .996 .130 0.2 

1,2-Trans-Dichloroethylene .444 .091 0.2 

(1) Least-Squares Regression (Effluent Concentration is the Dependent 

Variable). 

72 
centration will result in an increase in the effluent concentration. In many cases, the effluent increase is close to 

1-removal rate for that pollutant. Using zinc as an example, the 

data on Table 18 indicate that the effluent zinc concentration 

can be predicted by: 

Ceffluent = (0.256) Cinfluent - 15.8 (in ug/1) 

For an influent concentration of 723 ug/1 (the average of the 40 

POTW averages) an effluent of 169 ug/1 is predicted. 

Alternately, using the median removal for zinc of 77 percent from 

Table 10, an effluent of 166 ug/1 (723 x(1-.77)) is predicted 

for the sarne influent concentration. 

For several pollutants on Table 18, the high correlation coefficients also imply that the influent concentration is the single 

most important predictor of the effluent concentration. The 

importance of this relationship is that the percentage removal of 

pollutants at POTWs is not significantly dependent upon the 

influent concentration, but is relatively constant over the range 

of concentrations experienced in this study. 

DISCUSSION OF 10-PLANT STUDY RESULTS 

The initial 40 POTWs included in this study were specifically 

selected to obtain a cross-section of secondary treatment processes reflected in the 1978 EPA Needs Survey. These POTWs'vary 

in treatment capacity, influent characteristics, and industrial 

flows. POTWs 51 to 60 were selected as examples of POTWs that 

serve one primary industry or industrial category. The prominent 

industries that discharge to these 10 POTWs distinguishes this 

group of treatment plants from those represented in the 40 POTW 

survey. For this reason, the results from the 10 POTWs are not 

included in any of the summary evaluations. Instead, the 10 POTW 

data base is reviewed separately from the 40 POTW study. 

Table 1 presents a summary of the biological treatment processes, 

design flows, actual flows (the average six day flow volumes 

observed during the respective sample episodes), estimated percent industrial flow and a listing of the major industrial categories for the 10 POTWs. Percent industrial flows varied from 

less than one percent at POTW 52 to greater than 60 percent at 

POTW 55. At five of the POTWs included in the 10 POTW data base 

(POTWs 52, 54, 55, 57, and 60), samples were also collected at 

the dominant contributing industry auring two of the six sampling 

episodes. Selected pollutant mass contributions from the 

industrial dischargers can thus be compared with the pollutant 

mass of the influent, secondary effluent, and sludge streams 

sampled. Tables 19 through 28 present the average influent mass, 

secondary effluent mass (or tertiary effluent mass if 

applicable), appropriate percent removals, dominant industrial 

discharger mass (if sampled), and percentage of mass attributable 

73 
to the dominant industrial discharger for each of the 10 POTWs. 

Data results presented in these tables are for selected conventional and nonconventional pollutants as well as priori,ty pollutants detected in the influent waste stream greater than 50 

percent of the time. 

The dominant industry that discharges to POTW 51 is the gum and 

wood chemical industry. Benzene, toluene, ethylbenzepe, phenol, 

copper, chromium, nickel and zinc are the priority pollutants.. 

most often detected in the wastewaters discharged by the gum and ' 

wood chemicals industry. Toluene is the primary solvent used 

throughout the industry while benzene and ethylbenzene may be 

present as a result of contaminating toluene and xylene, respectively. A number of the metals are used as catalyst in various 

processes. 

A total of 29 priority pollutants were detected at least once 

during the six-day sampling effort in the influent waste stream 

compared to 17 priority pollutants detected in the secondary 

effluent waste stream. Bis(2-ethylhexyl)-phthalate, 

chloroethane, and toluene were the organic priority pollutant 

parameters detected at the highest concentration-in the influent; 

zinc, copper, lead, chromium, nickel, mercury, and arsenic were 

the priority pollutant metals detected 100 percent of the time in 

not only the influent, but also in the secondary effluent, primary sludge, secondary sludge and heat treatment supernatant 

recycle line. 

Treatmeftt efficiencies were good overall, with the exception of 

chloroethane. The chloroethane concentrations at the chlorinated 

secondary effluent location were greater than the influent concentration during five of the six sampling periods; average concentrations also indicated an increase in the chloroethane 

eoncentration after treatment. In contrast, toluene (another 

volatile organic priority pollutant) was not detectecl in the 

secondary waste stream. The mass balance table for POTW 51 in 

Appendix E shows that the seven metals listed above tend to concentrate in the primary sludge. 

POTW 52 had the lowest average flow (1.1 MGD) of the 50 POTWs 

sampled. The effluent waste stream from a wood preserving plant 

that discharges to POTW 52 was also sampled during this sampling 

effort. The effluent waste stream from the wood preserving plant 

was a low volume (5,000 gpd) waste stream but contained the 

following priority toxic pollutants at the listed concentrations: 

benzene 185 ug/1 

toluene 230 ug/1 

2,4,6-trichlorophenol 250 ug/1 

2,4-dimethylphenol 3,950 ug/1 

2-nitrophenol 215 ug/1 

pentachlorophenol 2,350 ug/1 

74 
Influent Secondary Effluent 

Parameter lbs/day lbs/day $ Removal 

BOD 98,309 1,199 99 

TSS°' 167,213 2,998 98 

COD 285,491 20,061 93 

Oil & Grease 12,947 2,671 79 

Benzene 2.2 ND 100 

Chloroethane 137 207 NR 

Chloroform 6.0 3.5 42 

Ethylbenzene 8.4 1.0 88 

Methylene Chloride 12.2 4.8 61 

Tolueneg 93.3 ND 100 

1,1,1-Trichloroethane 1.9 ND 100 

Tetrachloroethylene 7.3 ND 100 

Trichloroethylene 3.6 ND 100 

1,2-Trans-Dichloroethylene 1.7 ND 100 

Bis(2-Ethylhexyl)Phthalate 143 63.1 56 

Di-N-Octyl Phthalate 7.8 2.0 74 

Diethyl Phthalate 3.1 0.6 81 

Chromium 52.4 5.1 90 

Copper 109 6.3 94 

Lead 64 4.5 93 

Mercury 0.5 ND 100 

Nickel 15.1 2.0 87 

Silver 14.6 0.5 97 

Zinc 265 43.4 84 

Arsenic 0.4 0.2 50 

Fraction 

Conventional/ 

Nonconventinal 

*Volatiles 

*Base-Neutrals 

*Metals 

TABLE 19 

COMPARISON OF INFLUENT AND SECONDARY EFFLUENT POLLUTANT MASSES 

POTW 51 

ND = Not Detected 

NR = No Removal 

* 3 Pollutants detected in influent greater than 50 percent of time. 

75 
TABLE 20 

COMPARISON OF INFLUENT, SECONDARY EFFLUENT 

AND PRIMARY INDUSTRIAL EFFLUENT POLLUTANT MASSES 

POTW 52 

Influent Secondary Effluent Primary Industrial Contributorl 

Fraction Parameter lba/day lbs/day % Removal 1bs/day % of Influent Mass 

Canventional/ 

Nonconventional BOD 1,624 479 71 57 4 

TSS 951 257 73 15 2 

COD 2,200 888 60 415 19 

Oil & Grease 295 231 22 '` 0.8 <1 

•Volatiles Toluene 0.1 <0:1 NA <0.1 NA 

Chlorobenzene <0.1 <0.1 NA <0.1 NA 

Tetrachloroethylene <0.1 ND 100 <0.1 NA 

Trich loroethylene 0.1 <0.1 NA ®.1 NA 

*8aee Neutrals Acenaphthene 0.4 0.1 75 0.9 100 

Fluroanthene 0.3 0.2 33 0.64 100. 

Di-N-8uty1 Phthalate 0.4 0.2 50 <0.1 NA 

Anthracene 2.5 <0.1 >96 1.42, 57; 

Fluorene 0.4 <0.1 >75 <0.1 <25. 

Phenanthrene 2.2 <0.1 >95 0.16 7 

Pyrene 0.1 <0.1 NA <0.1 NA 

Bis(2-Ethylhexyl)Phthalate 0.1 0.1 NR m.1 NA . 

Diethyl Phthalate <0.1 <0.1 NA <0.1 NA 

Bis(2-Chloroethoxy)Methane 0.1 ND 100 <0.1 NA 

Chrysene <0.1 ND 100 0.27 NA 

1,2-Benzanthracene <0.1 ND 100 <0.1 NA 

+Acid Extr®ct Phenol 2.9 <0.1` ° >97 0.227 8 

2,4-0imethylphenol 0.2 <0.1 >50 0:165 82 

2,4,6-Trichlorophenol <0.1 ND,• 100 ® .1 NA 

•Metals Copper 0.3 0.1 67 <0.1 <33 

Silver <0.1 <0.1 NA <0.1 NA 

Zinc 1.0 0.6 40 m.1 <10 

Mercury <0.1 ND 100 <0.1 NA 

Nickel <0.1 0.1 NR <0.1 NA 

NA a Not apparent due to the low observed concentrations 

ND a Not detected 

NR = oVo removal 

< : Less than 

> a Greater than 

*= Pollutants detected in influent greater then 50 percent of time. 

i/Wood Preserving Plant 

76 & 
phenol 5,450 ug/1 

acenaphthene 22,250 ug/1 

fluoranthene 15 , 3,50 li g/1 

naphthalene 26,850 ug/1 

1,2-benzanthracene 1,050 ug/1 

3-4-benzofluoranthene 4,405 ug/1 

11,12-benzofluoranthene_ ;..'._;. 4,405 ug/1 

6,500 ug/1 

anthracene 34,050 ug/1 

1,12-benzoperylene 684 ug/1 

fluorene 1,500 ug/1 

phenanthrene 32,000 ug/1 

1,2:5,6-dibenzanthracene 1,160 ug/1 

indeno (1,2,3-C,D) pyrene 3,100 ug/1 

Diluti.on of the wood preserving wastewater with domestic sewage 

significantly reduced the coricentration of the priority pollutants. Pentachlorphenol, a process chemical used at the wood 

preserving plant, was surprisingly not detected in the influent 

waste stream at the POTW on four of six occasions. The mass 

balance table in Appendix E and the results presented in Table 20 

summarize the treatment efficiency for the tri"ckling filter 

treatment system. Conventional pollutant removals were low; 

priority pollutant removals were slightly better. In several 

cases, the actual pollutant removal could not be interpreted due 

to the low mass observed. Zinc, lead, copper, and several base/ 

neutral parameters exhibited a definite affinity to concentrate 

in.the primary sludge. 

Over 47 percent of the influent wastewater flow to POTW 53 is 

attributable to the combined waste stream from seven textile 

mills. Toxic'pollutants that may be expected to be present in 

the wastewater emanating from textile mills include 17 organic 

priority pollutants [acrylonitrile, benzene, 1,2,4-trichlorobenzene, 2,4,6-trichlorophenol, parachlorometacresol, chloroform, 

1,2-dichlorobenzene, ethylbenzene, trichlorofluoromethane, 

naphthalene, N-nitrosodi-n-propylamine, pentachlorophenol, phenol, bis(2-ethylhexyl)phthalate, tetrachloroethylene, toluene, 

and trichloroethylene], 9 metals (cadmium, chromium, copper, 

lead, mercury, nickel, selenium, silver and zinc) and cyanide. 

These pollutants are predominately associated with the.fibers, 

pigments, dyes,•fiber preservatives, coating formulations, 

dyestuffs or, cleaning solvents used throughout the industry. 

Tetrachloroethylene and trichlorethylene`were the volatile organic parameters in the influent detected at the highest average 

concentrations; acenaphthene and 1,2,4-trichlorobenzene were the 

prevalent base/neutral compounds; and zinc, copper, and nickel 

had the highest average priority pollutant metal concentrations. 

With the _exception of chloroform, which showed a net increase as 

a result of activated sludge - chlorination treatment, organic 

priority pollutant treatment was high. The•four dominant organic 

77 
TABLE 21 

COMPARISON OF INFLIIENT AND•SECONDARY EFFLUENT POLLIJTANT MASSES 

POTW 53 

Fraction Parameter 

Conventional/ 

Nonconventional BOD 

TSS 

COD 

Oil & Grease 

*Volatiles Methylene Chloride 

1,1,1-Trichloroethane 

Chloroform 

1,2-Trans-Dichloroethylene 

Tetrachloroethylene 

Toluene 

Ethylbenzene 

Trichloroethylene 

*Base-Neutrals Acenaphthene 

Naphthalene 

1,2,4-Trichlorobenzene 

Bis(2-Ethy1hexy1)Phtha1ate 

Di-N-Butyl Phthalate 

Diethyl Phthalate 

1,2-Dichlorobenzene 

*Acid Extract Phenol 

*Metals Antimony 

Arsenic 

Chromium 

Copper 

Nickel 

Silver 

zinc 

Lead 

Mercury 

Influent Secondary Effluent 

lbs/day lbs/day $ Removal 

7,859 89.2 99 

6,244 384 94 

20,203 5,169 74 

868 398 54 

1.1 0.3 73 

2.3 <0.1 >96 

0.5 1.8 NR 

0.8 ND 100 

20.8 ND 100 

0.3 <0.1 >67 

0.8 ND 100 

4.0 ND 100 

26.7 <0.1 >99 

2.5 ND 100 

42.0 0.2 100 

1.4 0.4 71 

0.3 0.1 67 

0.3 0.4 NR 

0.1 ND 100 

2.3 <0.1 >96 

0.7 0.6 14 

0.2 0.1 50 

0.6 0.2 67 

5.4 1.2 78 

5.3 4.6 13 

0.2 <0.1 >50 

13.4 6.5 51 

1.3 ND 100 

<0.1 <0.1 NA 

NA = Not apparent due to the low observed concentrations 

ND = Nat detected 

NR = Na removal 

< = Less thari 

> - Greater than 

*= Pollutants detected in influent'greater than 50 percent of time. 

W] 
compounds listed above were each reduced by over 99 percent. 

Primary treatment followed by roughing filters accounted for 65 

percent of the volatile organic removal and 84 percent of the 

base/neutral reduction. The remaining reduction was a result of 

the activated sludge process. Metals removal was not as good as 

organic removals, especially the reductions resulting from the 

primary clarifiers and roughing filters. 

POTW 54 is an activated sludge treatment system that receives 

approximately one percent of its influent flow from a herbicide 

manufacturer. The herbicide waste is pretreated (toluene extraction, dilution tank, resin absorption basins, and a lime basin 

with a carbon dioxide stripping column) prior to being discharged 

to the POTW. Residual pesticides from clean-up operations as 

well as toluene from'the manufacturing processes were anticipated 

to be present in the waste stream. The toluene loading from the 

industrial source represents 81 percent of the influent load to 

the POTW while pesticides were not detected in the influent 

stream. Removals at the POTW vary as shown in Table 22. Low 

removals were observed for chloroform, methylene chloride 

bis(2-ethylhexyl)-phthalate, lead, and selenium.. 

A pulp and paper mill that discharges to POTW 55 accounts for 56 

percent of the average influent flow to the POTW. Becausa of the 

extensive detention period through the treatment process of POTW 

55, the percent pollutant removals should be viewed cautiously. 

The time period between the influent and secondary effluentsamples may be several months due to the storage lagoon detention 

period. The time of travel through the soil in the spray irrigation fields extends the time period even further for the influent 

and tertiary effluent samples. Furthermore, flow rates may not 

coincide due to precipitation, evaporation, evapotranspiration, 

and percolation influences. 

Based on data from the six-day sampling period, the treatment 

facility appears to be well acclimated to effectively treat the 

influent wastewater. Though the influent volatile organic 

loadings were extremely high, the volatile organic priority 

pollutant removals were excellent (only the 28 percent for 

chloroethane was lower than the average 77 percent volatile 

removals). Priority pollutant removals were good overall with 

the exception of bis(2-ethylhexyl)-phthalate which showed no 

reduction. 

POTW 56 serves several industries including a steel mill, several 

electroplating operations, metal fabricators and electrical product manufacturing processes. The industrial flow is over 25 percent of the total plant influent. As might be expected from the 

contributing industrial mix, significant quantities of inetals and 

cyanides were detected in the influent waste stream. Primary 

treatment metal removals were fair (Table 24). Secondary treatment followed by filtration further reduced the metal loading to 

79 
TABLE 22 

COMPARISON OF INFLUENT, SECONDARY EFFLUENT 

AND PRIMARY INDUSTRIAL EFFLUENT POLLUTANT MASSES 

POTW 54 

Influent Secondary inf.luent .Primary Industrial Contributor l 

Fraction Parameter Ibs/day Ibs/da Removal. Ibs/da x of Influent Mass 

Conventional/ 

Nonoonventional 800- 

TSS 

COD 

011 3 Grease 

el/olati les 1,1,1 Trich loroethene 

Chloroform 

Methylene Chlorlde 

Tetrachioroethylene 

Toluene 

"Base Neutrals Bis(2-Ethylhexyl)Phthalate 

D1-N-Butyi Phthalate 

Diethyl Phthalate 

*Acfd Ex1'ract 2,4-Dichlorophenol 

*Ketais Chromlum 

Copper 

Lead 

Silver 

Z1nc 

14ercury 

Selenium 

1,741 737 96 76 0.5 

31,008 6,138 80 3,973 13 

39,614 2,824 93 2,463 6 

4,231 737 83 0.9 <i 

1.7 0.4 79 ND 0 

0.8 0.6 17 <0.1 <13 

0.4 0.4 NR <0.1 <25 

0.6 0.1 80 40.1 <16 

0.7 <0.1 100 0.6 81 

10.9 9.8 10 0.14 1 

1.3 0.4 70 <0.1 . <8 

0.2 ND . 100 . <0.1 <50 

51.2 23.4 54 <0.1 0 

1.8 0.5 73 0.09 5 

2.6 0.2 90 <0.1 <4 

1511 11.3 25 0.7 5 

1.0 <0.1 >90 <0.1 <10 

14.0 2.0 86 <0.1 <1 

0.1 ND 100 <0.1 <10 

0.2 0.8 NR y <0.1 <50 

NA = Not apparent due to the lar observed concentrations 

ND = Not detected 

NR n No removal 

< = Less than 

> = Greater than 

* s Pollutants detected in influent greater than 50 percent of time. 

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TABLE 24 

COMPARISON OF INFLUENT, PRIMARY EFFLUENT AND 

TERTIARY EFFLUENT POLLUTANT MASSES 

Fractlon Parameter 

Conventionai/ 

Nonconventional BOD 

TSS 

COD 

Oil 3 Grease 

*Volattles Benzene 

1,2 Trans-D(chloroethylene 

Ethyibenzene 

Toluene 

Trichloroethylene 

1,1,1 Trlchioroethane 

Tetrachloroethylene 

Methylene Chloride 

*Base-Neutrals Bts(2-ethylhexyi)phthalate 

D1-N-Butyl Phthalate 

Diethyi Phthalate 

Naphthalene 

Butyl Benzyi Phthalate 

*Acld Extract Phenoi 

4 Pesttcldes Gamma-BFIC 

*Metals Arsenic 

Chromium 

Copper 

Nicicel 

Zinc 

Sllver 

Lead 

Mercury 

Selenium 

*Other Cyanide 

POTW 56 

Influent Primary Effluent Tertlary Effiuent 

Ibs/day Ibs/da ¢ Removal Ibs/day K Removal 

11,329 3,165 72 - - 

59,097 22,981 61 568 99 

54,029 31,375 42 - - 

5,614 2,339 59 1,263 76 

0.2 0.1 50 0.1 50 

0.6 0.8 NR <0.1 >83 

0.1 0.1 NR <0.1 NR 

0.5 0.4 20 <0.1 >80 

8.0 7.6 5 3.6 52 

0.4 2.6 NR 0.6 NR 

1.8 1.1 38 0.3 83 

0.3 0.7 NR 0.3 NR 

1.1 3.2 NR 0.1 88 

0.3 0.1 50 <0.1 >67 

0.5 0.3 33 <0.1 •>80 

0.5 4.4 - ND 100 

0.2 <1.4 - <0.1 >50 

0.7 0.1 80 ND 100 

<0.1 0.1 NR <0.1 17 

4.4 0.6 88 0.3 91 

78.7 19.0 76 4.8 93 

36.7 14.0 62 1.5 96 

26.0 16.5 37 12.3 48 

924 440 52 179 81 

0.4 0.3 33 ND 100 

80.3 29.9 63 14.7 80 

<0.1 <0.1 75 ND 100 

0.4 0.1 67 1.3 NR 

8.4 2.9 66 4.5 43 

NO = Not detected 

NR = No removal 

< - Less than 

> a Greater than 

*= Poliutants detected In influent greater than 50 percent of time. 

: 
the receiving streams Nickel, as has been the case at other 

POTWs, had poor primary and secondary/tertiary treatment 'removals. Eight volatile priority pollutant compounds and five base/ 

neutral compounds were detected more than 50 percent of the time 

in the influent waste stream. Except for trichloroethylene and 

tetrachloroethylene, all organic priority pollutant influent 

average concentrations were below 10 ug/1. Primary treatment 

afforded little, if any, organic priority pollutant removal; 

secondary/tertiary treatment provided fair removals. 

POTW 57 was previously sampled during the 40 POTW survey (iden° 

tified as POTW 6). This treatment facility serves several 

industries including chemical/plastics manufacturing, electroplating, and the food processing industries. Industrial -flow 

amounts to about 15 percent of the POTW influent. The most 

significant industry (polyvinyl chloride manufacturing operation) 

was simultaneously sampled for a 48-hour period as part of the 

program. Extremely high vinyl chloride in the influent waste 

stream to the POTW during the first six-day sampling episode 

warranted verification sampling at the PVC plant. 

Grab samples or VOAs were randomly taken twice per day at the PVC 

plant while VOA grab samples at the POTW influent were taken six 

times per day, once every four hours. This variation in the 

sampling methodologies accounts for the difference in vinyl 

chloride mass loading between the POTW influent and the industry 

sample location. Vinyl chloride removals as a result of combined 

primary and secondary treatment averaged 93 percent. - Other - volatile organic priority pollutants present at average concentrations greater than 50 ug/1 were trichloroethylene and methyl 

chloride. Percent removals were 44 and 98 percent, respectively. 

Influent metal concentrations were high in comparison to the 

other 48 POTWs-sampled. Removals were good; ni.ckel was poorest 

at 45 percent removal. Pollutants in base/neutral, acid extractable, and pesticide fractions were not significantly 'present 

during the study. 

POTW 58 serves several industries, predominantly the pulp and 

paper industry and a steel mill. Industrial flow averages 30 to 

40 percent of the POTW influent. Phenol was the prevalent 

priority pollutant.present in the influent waste stream 

(795 ug/1). Phenol mass removal through the POTW averaged 99 

percent. Phenol showed no tendency to concentrate in either of 

the sludge waste streams, indicating that biodegradation may be 

the primary removal mechanism for phenol. Chloroethane and 

bis(2-ethylhexyl)phthalate showed no reduction while methylene 

chloride and nickel yielded only 14 percent and 16 percent reductions after secondary treatment. 

Several industrial operations contribute approximately 17 percent 

of the influent flow to POTW 59, with.pharmaceutical products 

manufacturing and metal plating operations comprising the most 

M. 
TABLE 25 

COMPARISON OF INFLUENT, SECONDARY EFFLUENT AND 

PRIMARY INDUSTRIAL EFFLUENT POLLUTANT MASSES 

POTW 57 

Primary 

Infiuent Secondary Effluent Industrial Contr:Ibutort 

Fractlon Parameter Ibs/day Ibs/day Removal Ibs/day x of influent Mass 

Conventionai/ 

Nonconv®nttonal 80D 11,785 539 95 1,622 14 

TSS 26,716 2,232 92 662 2 

COD 52,347 4,578 91 2,951 -6. 

011 S Grease 9,427 1,260 86 161 2 

*Volattles Chloroform 0.3 0.3 NR '. N5 NS 

1,2 Trans-0i ch loroethy`l ene 1.5 0.1 91 : NS NS 

Ethylbenzene 0.3 1.0 NR NS NS 

Methylene Chlortde 0.9 1.1 NR NS NS 

Toluene• 2.0 40.1 >98 NS NS 

Trichtoroethylene 12.5 7.0 44 NS NS 

Yinyl Chloride 2,527 178 93 362 14 

1,1,1 Trlchloroethane 1.3 ND 100 NS NS 

Methyf Chloride 11.4 0.2 98 'NS NS 

Tetrachloroethylene 1.4 ND 100 NS NS 

Benz®ne 0.2 ND 100 NS NS 

*Base Neutrals Bis(2-ethylhexyl)phthatate 1.6 1.2 26 : NS NS 

Netals Antimony 0.2 <011 60 <0.1 <50 

Arsenic 0.2 0.1 50 <0.1 <50 

Cadmium 44.2 4.4 90 <0.1 <1 

Chromtum 65.1 6.6 90 0.35 <1 

Copper 3C.8 3.7 90 0.17. <i 

Lead 7.5 ND >51 0.14 2 

Mercury 0.2 <0.1 90 <0.1 <50 

Nidcel 20.2 11.1 45 = 0.87 4 

Silver 0.7 0.1 81 <0.1 <14 

Zinc 178 29.2 84 2.64 1 

*Other Cyanide 5.6 ND >92 <0.1 Q 

NO - Not detected 

NR = No removal 

NS ■ Not sampled 

< x Less than 

> s Gr®ater than 

*= Pollutants detected in influent greater than 50 percent of ttme. 

1 /Palyvinyl Chiorlde Manufacturer 

o 
*Volatiles 

*Base-Neutrals 

*Acid Fxtract 

*Metals 

Benzene 18.6 

Toluene 0.9 

Chloroethane 29.2 

Methylene-Chlorid,e 1.4 

.Tetrachloroethyle.ne 1.6 

'Bis(2-ethylhexyl)phthalate 12.2 

Di-N-But,yl Phthalate 1.6 

Fluoranthene 0.8 

Di-N-Octyl Phthalate 1.1 

Diethyl Phthalate 1.0 

Pyrene 0.6 

.1,2-Diphenylhydrazine 0.6 

2,4-Dimethyl Phenol 0.5 

Phenol 147 

Cadmium 1.5 

Chromium 17.7 

Copper 46.5 

Lead 36.9 

Nickel 48..9 

Silver 2•0 

zinc 33.4 

Antimony; 6.1 

1.7 

ND 

38.6 

1.2 

ND 

20.8 

0.6 

ND 

<0.1 

<0.1 

ND 

<0.1 

ND 

1.1 

0.6 

6.6 

7.3 

15.9 

41.0 

2.3 

11.7 

1.4 

91 

100 

NR 

14 

100 

NR 

63 

100 

>91 

>90 

100 

>83 

100 

99 

60 

63 

84 

57 

16 

NR 

65 

77 

TABLE 26 

COMPARISON OF INFLUENT AND SECONDARY EFFLUENT POLLUTANT MASSES 

POTW 58 

Irifluent Secondary Effluent 

Fraction Parameter lbs/day lbs/day $ Removal 

Conventional/ 

Nonconventional BOD _. 17,069 2,882 83 

TSS 21,406 2,023 91 

COD 60,773 15,299 75 

Oil & Grease 3,691 3,691 20 

*Other Cyanide 30.3 12.0 60 

ND = Not detected 

NR = No removal 

< = Less than 

> 3 Greater than 

*= Pollutants detected in•influent greater than 50 percent of time. 

~'V 
TABLE 27 

COMPARISON OF INFLUENT AND SECONDARY EFFLUENT POLLUTANT MASSES 

POTW 59 

Influent Secondary Effluent 

Fraction Parameter lbs/day lbs/day $ Removal 

Conventional/ 

Nonconventional BOD 39,198 1,630 96 

TSS 123,825 3,627 97 

COD 97,953 43,278 56 

Oil & Grease 18,402 2,038 89 

*Volatiles Benzene 1.6 ND 120 

1,1,1-Trichloroethane 6.0 1.1 79 

Chloroform 2.0 1.6 13 

Ethylbenzene 12.3 <0.1 100 

Methylene Chloride 15.9 11.4 28 

Tetrachloroethylene 57.4 11.6 79 

Toluene 77.5 0.9 99 

Trichloroethylene 17.0 2.6 84 

1,2-Trans-Dichloroethylene 0.8 ND 100 

*Base-Neutrals Bis(2-Ethylhexyl)Phthalate 72.5 9.8 86 

Naphthalene 6.7 ND 100 

Di-N-Butyl Phthalate 15.1 1.1 92 

Di-N-Octyl Phthalate 2.5 1.2 50 

1,2-Dichlorobenzene 0.6 <0.1 100 

*Acid Extract Phenol 17.2 0.7 96 

*Metals Chromium 113 59.1 47 

Copper 41.8 4.5 89 

Mercury <0.1 <0.1 83 

Nickel 41.8 24.0 42 

Silver 2.4 0.4 80 

Zinc 195 50.0 74 

*Other Cyanide 9.3 3.4 63 

ND = Not detected 

< = Less than 

*= Pollutants detected in influent greater than 50 percent of time. 

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i 
significant sources of this flow. Toluene, tetrachloroethylene, 

and bis(2-ethylhexyl)phthalate were the organic priority pollutants detected at the highest influent concentrations. Percent 

removals for these pollutants were 99, 79, and 86 percent, 

respectively. The two volatile compounds were not concentrated 

in the sludge stream which indicates that air-stripping and/or 

biodegradation are the treatment reduction process. Bis(2-ethylhexyl)phthalate was detected at significant levels in the sludge 

streams indicating bioflocculation may be the significant treatment process for this compound. Of the priority pollutant metals 

detected more than 50 percent of the time, chromium and nickel 

showed the lowest removal rates at 47 and 42 percent, respectively. Other than nickel and chromium, copper was the metal 

with the highest influent concentration; copper removal was 89 

percent through secondary treatment. 

Approximately 13 percent of the influent flow to POTW 60 is from 

a leather tanning and finishing plant. Table 28 compares the 

pollutant mass for the industry source with the POTW influent, 

primary eff luent, and secondary effluent streams. Chromium, a 

process chemical used in the tanning process, was the priority 

pollutant detected at the highest influent concentration to the 

POTW. Ferric chloride was added to the tannery waste stream to 

aid sedimentation of-chromium. Eighty percent of the chromium 

load was found to settle out as a result of primary sedimentation. The activated sludge process further removed chromium 

for a net removal of 98' percent. Thirty-two other priority 

pollutants were detected in the influent waste stream over 50 

percent of the time. Overall removals for those pollutants were 

excellent., except for nickel (19 percent removal) and cyanide (no 

removal). 

.. 
" APPENDIX A 

FLOW DIAGRAMS 

PLANTS 1 to 40 AND 51 to 60 

~ 

A-1 
Af y • qy . ,~ ef'i,~~..i'f1~Y ~~ E , ~ ,~J~.e~$ 

. 

FLOW DIAGRAM PLANT NO. 1 

120 MGD (design) 

, ; ,~t ~,,~ • 

_ `. - K . f, .:~ "" a: ,. r ,r • ~ 

... ...... 

. . . . 

. , 

c. , ® Sample Points ~ Screening 

1. Influent 

2. Prechlorinated Effluent 

~ 3. Final Effluent 

4. Primary Sludge 

5.Flotables 

Grit 6. Waste Activated Sludge 

Removal 7. Filtrate 

8. Combined from Point's 4 and 6. 

1 

P reaeratio n 

O 

r.. 

~ tC 

p ~, s 

4 ~ 

.. cc 

. •>Primary Gravity. ,. . iZ 

Clarification ; 

- 

` Thickening 

.. _ 

; ~ 

., • 

5 

7 

Diffused v 

: 

° ° J °~ 

Vacuum 

° Filtration ~ , 

f 

. 

Incineration 

Aeration r°' .. 

c 

~ .. . 

cts 

c 

~ 

~ 

6 ' 

cn Landfill° 

Secondary DAF 

Clarification Thickening 

2 

Chlorination 

3 

—Some ash .is recycled to the secondary clarifiers. 

Discharge 

A-2 
FLOW DIAGRAM PLANT NO: 2 15 MGD (design) 

Screening ® Sample Points 

1. Influent 

~ 2. Prechtorinated Effluent 

3. Final Effluent 

4, Primary Sludge 

_ 5. Waste Activated Sludge 

Grit Removal 6. Thickened Waste Activated Sludge 

7. Combined Sludge 

Comminution 

Preaeration Land 

Application 

4&7 

Primary Sludge" 'Heat 

Clarification Storage Treatment 

Diffused ° _ 

Decant 

Decanting Aeration 

6. 

Secondary 5 DAF Filtrate Vacuum, Clarification Thickening Filtration . " 

2 

, . _ 

Chlorination Incineration 

Lagoon 

Discharge 

— Heat treatment and incineration not in operation during + sampling 

— During sampiing, plant operating with only half of its prfmary cfarifiers and aeration tanks. 

— Activated sludge was wasted for five of seven days during the satiipling program. 

A- 3 
FLOW DIAGRAM PLANT NO. 3 

14 MGD (design) 

. .. ' .'.4i. .,... 

~ Sample Points 

1. I nfl uent 

2. Prechlorinated Effluent 

3. Final Effluent 

4. Thickener Overflow 

5. Thickened Primary Sludge 

Screening 

6. Combined Sludge 

~ 

1 

0 

~ 

Grit , 

L 

Removal O 

4 

Primary Gravity u~ 

Clarification Thickening 

ca 

~ 

— 

~ 

5 ~ .Q 

- 

~ 

cn 

Diffused 6 Vacuum 

Aeration m° • Filtration r 

Secondary 

Clarification 

db 2 

DAF 

Thickening 

Landfill 

Chlorination 

3 

Discharge 

— Prechlorination utilized only when necessary. 

A-4 
FLOW DIAGRAM . PLANT NO. 4 

120 MGD (design) 

1 

® Sample Points 

1. Influent 

2. Final Effluent 

3. Combined Sludge 

Screening 

4. Digested Siudge 

- 

, . Y 

c 

c~ 

Y 

Grit c ~ 

Removal ~/~ a 

VJ Y 

c 

~ 

U 

3. 4 

Primary Anaerobic ; Centrifugation Clarification Digestion 

~ 

c 

Diffused c° co 

Aeration c 

a~ o. 

~ U) 

Secondary DAF Incineration Clarification W A S Thickening 

Chlorination Landfill 

2 

Discharge 

— AII plant recycle lines are returned to the influent Iine, which accounts for only 6% of the 

plant flow. This influent was not sampled. 

— Prechlorination utilized for odor control. 

— DAF Thickened Sludge is pumped directly to centrifuges, if necessary. 

A-5 
FLOW DIAGRAM PLANT NO. 5 

25 MGD (design) 

® Sample Points 

Screening 1. Influent 

2. Final Effluent 

3. Combined Sludge 

y 4. Digested Sludge 

Grit 

Removal 

Supernatant 

Comminution 

Overflow 

Primary 3 Gravity Anaerobic 

Clarification Thickening Digestion 

m 

-rn a _- 

~ 

~ c 

Diffused ~ ~ 

Aeration > ~ p 4 

Q 

U . 

+. 

N 

ct7 

~ 

Secondary Lagoon 

Clarification Disposal 

Chlorination 

I 

t

2 

Discharge 

— During wet conditions, the plant routinely treats an additional 50 MGD through the primary 

system and a separate chlorination facility. 

A-6 
FLOW DIAGRAM ;..PLANT° ~lO. 6 

7.4 MGD (design) 

. ~{~:a;•< . ~ 

screening 

Grit 

Removal 

Chlorination 

~ 2 

Discharge A-7 
Primary Sludge 

Clarification Storage 

a~ 

a~ 

~ 

:3 

m 

Diffused 

a 

°' Decant 

~ 

Aeration ~ U 

Q 

~ 

~ 

Heat 

Treatment 

El 

Decanting 

(5~ 5 

FLOW DIAGRAM PLANT NO. 7 

66 MGD (design) 

® Sample Points 

1. Influent 

2. Prechlorinated Effluent 

Screening 3. Combined Sludge 

4. Heat Treatment Decant 

1 5. Heat Treated Sludge 

Grit 

Removal 

Overflow 

3 

Secondary Filtrate 

Clarification 

2 

Vacuum 

Filtration 

Chlorination Landfill 

Incineration 

Discharge 

Landfill 

, ; 
FLOW DIAGRAM PLANT NO. 8 

1 50 MGD (design) ~ ? 

Screening Screening 

® Sample Points 

1. I nfluent 

2. influent 

3. Final Effluent 

4. Primary Sludge 

Aerated 5. Combined Sludge 

Grit Removal 6. Heat Treated Sludge 

7. Heat Treatment Decant 

Primary 

Clarification 

4 

Subnatant DAF 

Thickening 

Diffused Sludge Trickling 

Aeration Storage Filtration 

il 5 

Secondary Heat Treatment Secondary 

Clarification Clarification 

7Decant 

Microscreening Decanting Chlorination 

6 

Vacuum Filtrate Discharge 

Reaeration Filtration 

Chlorination 

3 — During sampling, plant flow was less than half of design capacity. 

— Influent sample was flow composited from Points 1 and 2. 

Oischarge 

A-9 
FLOW DIAGRAM PLANT NO. 9 

60 MGD (desigri) 

® Sample Points 

1. Influent 

Screening 2. Final Effluent 

_ 3. Primary Sludge 

4. Waste Activated Sludge 

Grit 

Removal 

Subnatant 

3 

Primary Sludge DAF. 

H 

<.>. 

Clarification 

.,. . , 

Holding 

. 

Thickening 

x. 

Diffused" co 

6 

Belt Filter Vacuum 

Aeration _ ._. Dewatering Filtration 

,. u_ 

Secondary 4 ru.. . 

Incineration Clarification 

• , 

, 

. 

_ .. .. ; 

Chlorination 

 •~ .. ~ • 

Ash Lagoon 

~ 

2 

Landfil0 

Discharge 

— Chlorinated effluent sampled immediately after chlorine injection. 

A-10 
FLOW DIAGRAM PLANT NO: 10 

42 MGD (design) 

(2) Sampie Points 

•1: Influent 

Screening 2. Final Effluent (AS) 

3. Thickened Waste Activated Sludge 

4. Digested Studge (Aerobic) 

5. Combined Sludge 

6. Digested Sludge (Anaerobic) 

Comminution 7. Secondary Sludge (Humus) 

8. Prechlorinated Effluent 

9. Final Effluent (TF) 

Occasional Backwash 

Splitter Box From Tertiary Treatment 

1 

Grit Removal _. . _ -- _ -,- 3 _. . Grit Removal 

0 

w 

~ > 

.. @ O 

-. ., 

~j , uPrimary Primary Sludge Degritting Primary 

Clarification Clarification 

a~ 

rn v 

Aeration ~ Gravity Trickling 

(Diffused & y Centrifugation" Thickening ~ Filtration 

Mechanical). E 

~ 

¢ 3 

a~ ~ 

~ ~ 

Secondary , ~ ~ 7 

Classification Aerobic Vacuum o Secondary 

& Digestion Filtration V Clarification 

Chlorination 

Thickened 5 8 2 4 W.A.S. 

Offsite Anaerobic Chlorination 

Discharge Disposal Digestion 

6 9 

Offsite Disposal Discharge 

— This plant also utilizes a 9 MGD tertiary treatment process. The effluent from this process 

is used for irrigation. Filter backwash is returned to the head of the trickling filter system. 

— Thickened waste activated sludge is blended with the vacuum filtered primary sludge resulting 

in a sludge concentration of approximately 5 to 6% solids before anaerobic digestion. 

A-11 
FLOW DIAGFiAM PLANT NO. 11 

45 MGD (design) 

A1 

Screening 

Grit 

Removal 

Screening 

® Sample Points 

1. Influent 

2. Prechlorinated Efffuent 

3. Final Effluent 

4. Combined Sludge 

5: Secondary Sludge (Humus) 

~ 

c 

c~ 

~ 

ca 

c 

~ 

a~ 

a 3 

m 

Primary 4 

Anaerobic Drying` ; 

Clarification Digestion Beds 

Trickling 

Filtration 

Secondary 5 

Clarification 

2 

Chlorination 

3 

Discharge 

A-12 

Land 

Application 
_ 2. Primary Effluent 

3. Final Ef.f,luent 

4. Primary Sludge ° 

40 MGD (design) 5. Waste Activated Slud je f Fi ltrate : 

Screening 

1 

Primary 

Clarification 

2 

a 

Mechanical 

Aeration 

Secondary 

Clarification 

Chlorination 

1 

~ 

Degritting.., ~ 3 ------~--- 

0 

_... . ~ 

O

°. , 

Gravity 

Thickening, , 

5 Vacuum ` 

Filtration 

Landfill 

3 ,..... 

Discharge _ 

— Waste Activated Sludge sample taken from Return Activated Sludge line. 

A-13 - 
FLOW DIAGRAM PLANT NO. 13 

24 MGD (design) 

~ Supernatant 

Screening 

(?Q 1 

® Sarnpie Points 

1. Influent 

2. Secondary Effluent 

3. Final Effluent 

4. Primary Sludge 

5. Waste Activated Sludge 

G rit 

Removal 

Primary 

Clarification 

Diffused 

Aeration 

Secondary 

Clarification 

r 

y 

(4 

~ 

Y 

U 

l4 m 

4 Anaerobic 

Digestion 

m 

rn 

~ 

~ 

~ 

~ 

a~ 

,., 

cII 

> 

U 

Q 

... N 

fA 

5 ~ 

Land 

Application 

00 2 

Sand 

Filtration 

Chlorination 

3 

Discharge 

— Influent was sampied from one of two parallel wastewater streams not containing 

supernatant or backwash. 

A-14 
w DtAGRAMi ; PLANT NO. 14 

20.6 MGD (design) 

(2) Sampk~ ,Poiliits 

1.'Influ6nt' 

screenirid 2.Final Effl,qqnt 

3.Co rnbined Sludge 

4.Waste Activated Sludge 

_,§.,,jjjfjqeptjp, Qther Plant 

Comminution 

co 

-C0 

CL 

Ght 

Romoval 

Primary 3 Anaerobic Off-Site Disposal Clarification Digestioh 

Diffused ca 

Aeration 

co 

4 

Secondary 

Clarification 

I nf i uent to another, plant. , 

within same city Was also sampled 

(Domestic Flow). , 

5 

Chiorination 

2 

Discharge 

A- 1.5 
FLOW DIAGRAM PLANT NO. 15 

75 MGD (design) 

Industrial Domestic 

k1 i 

v ® Sample Points 

Comminution 1. Influent (Industrial) 

2. Influent (Combined) 

3. Final Effluent 

4. Primary Sludge 

5. Combined Sludge 

Screening 

Grit 

Removal 

Preaeration 

4~4 

Supernatant 

4 

Primary Anaerobic Sand 

Clarification ,~, ~ Digestion Drying Beds 

Trickling N O 

Filtration E Disposal 

~ 

_ 

Secondary 

Clarification 

Polishing 

(l.agoon) & 

Chlorination 

3 

— Sample points 4 and 5 consisted of primary and combined sludges. One pump was utilized 

to pump sludge from each set of clarifiers. Humus was returned to one set of clarifiers 

resulting in a combined sludge. 

— The final effluent was not chlorinated throughout the sampling week. 

A-16 
Primary 4 

Clarification 

a~ 

~ 

~ 

~ 

~ 

Z 

Trickling co 

Filtration c 

(Roughing) 0 

v 

~ 

N Y 

~ 

~ 

I 

Secondary 

Clarification 

110 MGD (design) 

Screening 

1 

Aerated 

G rit 

Removal 

Mechanical 

Aeration 

FLOW DIAGRAM PLANT NO. 16 30 MGD (design) 

,. 

~ 

® Sample Points Screening 

1. Influent 

2. Prechlorinated Effluent 

3. Finai Effluent 6 

4. Combined Sludge 

5. Combined Sludge (Other) 

6. Influent (Other) Grit 

Removal 

~ 

5 

Primary 

Clarification 

a~ 

~ 

~ 

~ 

~ 

a 

C: Trickling 

o Filtration 

U 

(D 

U) 

~ 

Y 

~ 

~ 

~ 

Anaerobic Secondary 

Digestion Clarification 

Tertiary Aerobic 

Clarification Digestion 

Mixed 

Media 

Filtration 

2 

Chlorination 

3 

Discharqe Deep Well Injection 

A-17 
FLOW DIAGRAM PLANT NO. 17 

38 MGD (design) (2)Sample Points 

1. Influent 

1 2. Final Effluent (Activated Sludge) 

3. Primary Sludge 

4. Waste Activated Sludge 

5. Combined Sludge 

6. Final Effluent (Trickling Filter) 

Grit Removal Grit Removal 

Primary 

Clarification 

3 

~

Primary 

Clarification 

Diffused 

Aeration 

Secondary 

Clarification 

4 

3 0 

~ 

a~ > 

O 

Overflow 

Decant 

Decant 

Aerobic 

Digestion 

Gravity 

Thickening 

b0 5 

Anaerobic 

Digestion 

~ 

Trickling 

Filtration 

Secondary 

Clarification 

I 

Chlorination Lagoon Chlor'ination 

k2 6 

Discharge 

Discharge 

A-18 
100 MGD (design) 

I 

Screening 

FLOW DIAGRAM PLANT NO. 18 

® Sample Points 

1. Influent 

2. Prechlorinated Effluent 

3. Waste Activated Sludge 

4. Primary Sludge 

Grit Removal 

1 

Sludge from 

Other Plant 

I -~ 

Primary 

Clarification 

Overflow 

Degritting 

Supernatant 

Centrate 

Centrifugation - 

~ 

c 

~ 

W 

c 

L 

~ 

Q. 

c~n Aerobic 

Digestion 

Diffused 

Aeration 

T - 

3 

Secondary 

Clarification 

2 

[—Chlorination 

Gravity 

Thickening 

4 

Anaerobic 

Digestion 

v Lagoon 

Discharge and 

Land Application 

—Sludge from two other POTWs accounts for approximately 10% of tfie total sludge. 

A-19 
FLOW DIAGRAM PLANT NO. 19 

120 MGD (design) Cooling Water 

from Oxygen Plant 

1 ® Sample Points 

Filtrate 1. Influent I 

2. Primary Effluent 

Supernatant 3. Secondary Effluent 

4. Final Effluent ,. 

Centrate 5. Primary Sludge 

6. Waste Activated Sludge 

Screening °- 

Filtrate 

Grit Removal 

Primary 5 Anaerobic Vacuum 

Clarification Digestion Filtration 

0 2 Centrate 

Pure Oxygen 

Aeration 

Landfill 

6 Centrifugation Secondary 

Ciarification 

3 

FChlorination 

Dechlorination 

4 — Influent was composited from two points prior 

to any recycieiines and prechiorination. 

Discharge 

A-20 
F.LOW ,DIAGRAM pLANT N0. 20. ' 

143 MGD (design) 

® Sample Points 

i.,lntluent 

Screen(ng 2. - Secondary Effluent 

3. Final Effluent 

" 4. Primary Sludge 

~ 5. Waste Activated.Sludge 

6. Nitrification Sludge 

Comminution 

Decant (Turned off during Sampling) 

Grit 

Removal 

4 Sludge Primary Anaerobic Drying Clarification Digestion Beds 

Subnatant 

Aeration Disposal (Diffused) 

~ 

ca 

Secondary •c , DAF 

U 

o 

Clarification 

00 2 

L 

3 Nitrification 

~ (Kraus) 

m 

d 

~ 

Final 

Clarification 

Thickening 

6 

I Mixed I I{ Media 

Filtration 

— An undocumented amount of primary effluent 

is passed directly to the nitrification unit. 

3 

Chlorination Dechlorination 

77~— 

Discharge 

A-21 
FLOW DIAGRAM PLANT NO. 21 

55 MGD (design) 

I _ 

Screening 

OCl l 

Grit 

Removal 

® Sample Points 

1. Influent 

2. Secondary Effluent 

3. Final Effluent 

4. Primary Sludge 

5. Waste Activated Sludge 

Filtrate 

Anaerobic 

Digestion 

Sludge 

Settling 

(Lagoon) 

Gravity ~ 

T. hickening 

4 

Primary 

Clarification 

~ 

c 

c~ 

co 

c 

~ 

m 

a 

Trickling 

~ CD 

Filtration 

5 

Secondary 

Clarification 

2 

Oxidation 

Pond 

Vacuum 

Filtration 3 

0 

~ 

a~ 

~ 

c 

Sludge ~ 

Drying Beds 

3 

0 

~ 

a~ 

p Disposal 

Seasonal Flow to Tertiary Treatment 

(Not in operation during sampling) 

Chlorination 

Dechlorination 

(Pond) 

t 3 

—(Recycles were stopped during sampling period) 

A-22 
FLOW DIAGRAM

r. 

 PLANT NO. 22 

.. 

15 MGD (design) ® Sample Points 

1: Infiuent 

2. Secondary Effluent 

3. Finai Effluen# _ 

Screenin g 4. Combined Sludge 

Grit 

Screening Removal 

Comminution 

,. 

.__ 

. 

' 

... . .>~ F., • _ ; ,.. ,_." _ _ ., ., . ...., _- = 

1• 

Grit 

Removal 

Supernatant 

4• 

Primary Anaerobic; Sludge 

Clarificatio.n Digestion ', Storage '. 

_c.. 

~ 

co 

d - 

_:. : •. :: 

Trickting 

., . ..: Drying 

Filtration 3 Beds 

(Roughing) cn 

. IJnderfl6ni .` 

a~ 

Diffused co ~ 

Aeration 

~ ~ Disposal 

N (o ' 

~ 

Secondary 

Clarification 

2 _ 

Post 

Aeration 

(Lagoon) 

Chlorination 

3 

Discharge 

A-23 
FLOW DIAGRAM PLANT NO. 23 

27 MGD 

(design) ® Sample Points 

1. Influent (Combined) 

2. Secondary Effluent 

3. Final Effluent 

Screening Screening 4. Primary Sludge 

5. Secondary Sludge 

1 1 

Grit 

Grit Removal Removal 

Primary 

4 -- 

~ 

Clarification cc ~ o 

7 ~ a) 0 

FAnaerobic 

C 

D 

Drying Trickling 

Filtration 

(Roughing) gestion Bed 

Mechanical 

Aeration 

(Lagoon) 

2 .- 

c 

c~ 

in 

c 

~ 

a> 

Chlorination a :3 

rn 

5 

Secondary Aerobic 

Clarificatjon ' Digestion 

Post 

Aeration 

(Lagoon) 

3 

Discharge 

— Inf9uent samples were flow proportioned. 

A-24 

Disposal 
FLOW DIAGRAM PLANT NO. 24 

64 MGD (design) 

661 

Screening 

Grit 

Removal 

® Sample Points 

1. Influent 

2. Final Effluent 

3. Combined Sludge 

4. Secondary Sludge (Humus) 

Primary 3 Sludge 

Clarificatio 1 Storage 

Trickling Filtrate Vacuum 

Filtration Filtration 

~ 

E 

~ 

_ 

4 

Secondary 

Clarification Landfill 

Post 

Aeration 

(Lagoon) 

Chlorination 

2 

Discharge 

A-25 
FLOW DIAGRAM PLANT NO. 25 

60 MGD (design) 

® Sample Points 

1. Influent 

2. Secondary Effluent 

Preaeration 3. Prechlorinated Tertiary Effiuent: 

4. Final Effluent 

5. Primary Sludge p 

6. Waste Activated`Sludge= 

7. Tertiacy Siudge 

Screening'' Undertiow' 

Grit Removal 

Primary 5 Anaerobic Drying 

Ciarification Digestion Beds 

Pure Oxygen - 

Aeration Landfiil 

6 

.. 

~ 

. 

Secondary E

co 

Clarification CD a 

~ 

2 

CD 

3 

Pure Oxygen 0 . 

Aeration ~ 

O _ .... 

Tertiary 7 Aerobic 

Clarification Digestion 

Denitrification Gravity 

Filtration Thickening 3 . . ... 

0 

~ m v 

Post 

c 

= Sand 

Aeration Drying Beds 

3 

Chlorination Landfiil 

4 — An undocumented amount of primary effluent is passed directly 

to the nitrification unit. 

Discharge A- 2"6 
FLOW DIAGRAM PLANT NO. 26 

200 MGD (design) 

® Sampie Points 

1. Influent 

2. Final Effluent - 

3. Combined Sludge 

4. Waste Activated Sludge 

Screening 5. Filtrate 

6. Vacuum Filter Backwash 

7. Ash Pit Decant 

1 

Grit Removal 

7 ®ecant A 

6 5 

Primary 3 Vacuum incineration 

Clarification Filtration 

Diffused Ash Pit 

Aeration 

4 Landfill 

Secondary 

Clarification 

Chlorination 

2 

Discharge 

A-27 
FLOW DIAGRAM PLANT NO. 27 

200 MGD (design) 

1, 

Occasional ® Sampie Points 

Industrial 1. Infiuent._ 

Sludge 2. Prechlorinated Effluent (TF) 

Screbning 3. Secondary Sludge,.(Humus) 

4. Combined Sludge 

5. Waste Activated Sludge 

6. Prechlorinated Effluent -< 

(Activated Sludge) 

= 3 

0 

~ d Grit Removal 

~ 

O 

Primary 

Clarification 

4 Waste Activated Sludge 

Trickling Gravity Deg riffing Diffused 

Filtration Thickening Aeration 

Decant 

5 

Secondary 3 Anaerobic Siudge Sludge Sludge Secondary - 

Ctarification Digestion Storage Clarification 

Humus 

2 Sludge - 

6 

Elutriate 

Mixing 

Elutriation o 

L 

'u:. 

Chiorination Vacuum 

Filtration 

Dried for 

Public Use 

Discharge industrial Landfili 

Reuse 

— A portion of the unchlorinated secondary effluent was used for production water at a local 

lndustry. 

— No supernatant is withdrawn from anaerobic digester. 

A-28 
Chlorination 

3 

Discharge 

A-29 
Primary 

Clarification 

2 

~ 

Trickling 

Filter 

(High Rate) 

~ 

~ 

E 

~ 

_ 

4 

FLOW DIAGRAM PLANT NO. 29 

8.5 MGD (design) Sample Points 

1. Influent 

2. Primary Effluent 

1 3. Final Effluent 

4. Secondary Sludge (Humus) 

S. Combined Sludge 

Screening 

Supernatant 

Grit Removal 

Secondary 

Clarification 

Chlorination 

3 

Discharge 

5 Vacuum Sludge 

Filtration Storage 

'Filtrate= - 

Scrubber Washwater 

Incineration 

Landfill 

A- 30 
FLOW DIAGRAM PLANT IVO. 30 

24 MGD (design) 

Domestic lndustrial 

Screenin;g Screening 

1 5 

Comminution Comminution 

(g Sampte Points 

1. Influent (Domestic) 

2. Primary Sludge (Domestic) 

3. Primary Effluent (Combined) 

4. Final Effluent 

5. Influent (industrial) 

6. Primary Sludge (Industrial) 

7. Waste ActivatedtSludge 

8. Thickener Overflow 

9. Heat Treatment Sludge 

Primary Primary 

Clarification Clarification 

2 3 6 Overflow 

Mechanical E

egritting 

Aeration 

-- 

Centrate 

7 

Secondary Centrifugation Clarification 

.8 

Gravity 

Thickening 

Heat 

Treatment 

Chlorination 

4 

Discharge 

Decant 

Filtrate 

Decanting 

9 

Vacuum 

Filtration 

Landfill 

A-31 
53 MGD (design) 

FLOW DIAGRAM PLANT NO. 31 

~ Sampie Points 

1. Influent 

2. Prechlorinated Effluent 

3. Final Effiuent 

4. Combined Sludge 

5. Waste Activated Sludge 

Screening 

1 Overflow 

Primary 

Clarification 

4 

Degritting Gravity 

" Thickening 

Mechanical Filtrate Vacuum 

Aeration Filtration 

Subnatant 

Secondary 

Clarification 

E 

DAF Thickening ~_~ I Incineration 

Scrubber Washwater 

Chlorination Off-site 

Disposal 

3 

— If the waste activated sludge is not returned to the primary clarification unit, both sludges are 

treated separately and combined in the vacuum filtration unit prior to incineration. 

A- 32 
160 MGD (design) 

Screening 

t1S1 1 

FLOW DIIAGRAM PLANT NO. 32 

® Sample Points 

1. Influent 

2. Primary Effluent 

3. Final Effluent 

4. Primary Sludge 

5. Waste Activated Sludge 

6. Thickener Overflow 

7. Filtrate 

Comminution 

Grit 

Removal 

Primary 

Clarification 

4 2 

Diffused & 

Mechanical 

Aeration 

4 

3 0 

zE 

a~ 

p 6 

Gravity 

Thickening 

a~ 

co L 

~ 7 

Vacuum 

Filtration 

Landfill 

5 

Secondary 

Clarification 

Chlorination 

9 

Discharge 

A-33 
FLOW DIAGRAM PLANT NO. 33 

5 MGD (design) i& Sample Points 

7. Influent 

1 . . 2. Primary Effluent. 

3. Final Effluent 

4. Primary Sludge 

S. Waste Activated Sludge 

6. Digester Supernatant 

Comminution 

w 

c 

~ 

Grit 

Removal ? e c 

; 6 . 

. 4 _. 

Primary Anaerobic Centrifugation Clarification Digestio'n _ 

2 

Rotati ng 

Biological 

Contactors Land 

Application 

5 ... 

Secondary 

Ciarification 

Chlorination 

3 

Discharge 

A- 34` 
FLOW DIAGRAM PLANT NO. 34 .` 

30 MGD (design) Sample Points 

1., Influent 

2. Primary Effluent 

3. Final Effluent 

4. Primary Sludge 

Screening 5. Waste Activated Sludge 

6. Digester Supernatant 

1 

Grit 

Removal 

Supernatant g 

4 

Primary Anaerobic 

Clarification Digestion ' 

2 Centrate . 

Diffused 

Aeration 

5 

Secondary Centrifugation Clarification 

Chlorination 

3 

Discharge 

,r 

c 

c~ 

U 

a~ 

0 

Lagoon 

A-35 
26 MGD (design) 

60 1 

Screening 

Comminution 

Grit 

Removal 

FLOW DIAGRAM PLANT NO. 35 

~ Sample Points 

1. Influent 

2. Prechlorinated Effluent 

3. Primary Sludge 

4. Waste Activated Sludge 

Overflow 

3 

Primary 

Clarification 

Diffused 

Aeration 

Gravity 

Thickening 

Heat 

Treatment 

Decant 

Decanting 

Filtrate 

Secondary 

Clarification 

2 

Chlorination 

4 Vacuum 

Fiftration 

Landfitl 

Discharge 

A- 36 
FLOW DIAGRAM PLANT N0..36 

45MGD (design) 

f~ 1 

® Sample Points 

Screening 1. Influent 

2. Final Effluent 

3. Primary Sludge 

4. Waste Activated Sludge 

5. Digester Supernatant 

6. Fittrate 

Grit 

Removal 

Overflow 

Comminution 

Supernatant 

5 

Primary 3 Anaerobic - Gravity , 

Clarification Digestion Thickening 

; 

4 

Diffused Filtrate 6 Vacuum 

Aeration Filtration 

4 

~ 

a Secondary 

Clarification 

a, LandfiN 

w . 

.,. 

Chlorination U ' 

Q 

(D ~.. 

2 

y 

~ 

~ —Discharging of waste activated sludge is a temporary function. 

Discharge 

— Gravity thickener is utiliied only during the. winter. 

A-37 - 
FLOW DIAGRAM PLANT NO. 37 

66 (VIGD (design) 

Screening 

1 

Grit 

Removal 

Humus 

To Other Plant 

® Sample Points 

1. Influent 

2. Primary Effluent 

3. Finat Effluent (Activated Slu 

4. Waste Activated Sludge 

5. Primary Sludge 

6. Secondary Sludge (Humus) 

7. Final Effluent (Trickling FiltE 

To Other Plant ~ 

Primary 

Clarification 

b~ 2 5 

Anaerobic 

Digestion 

Diffused 

Aeration 

Secondary 4 

Clarification 

3 

.r 

c 

c~ 

~ 

c 

.n 

~ 

~ 

~ 

c 

co 

DAF m 

Thickening ~ 

a 

~ 

~ 

Trickling 

Filtration 

6 Secondary 

Sludge Clarification 

7 

Anaerobic 

Digestion 

~rCe ~ ntrate 

Centrifugation 

~ 

Discharge A-38 

Composting 
PLOW DIAGRAM PLANT NO:'38 

37.5. MGD (design) 

(3 Sampie Points 

1: Influent 

2. Primary Effluent 

3. Secondary Effluenf 

Screening 4. Final Effluent 

- 5. Primary Sludge 

6. Waste Activated Sludge 

1 

5 

Prima.ry 

Clarification 

2 

Diffused 

Aeration 

Secondary 6 

Clarification 

3 

Chiorination s 

CIS ;Sfudge Returned to 

Y U Trunklirte for . 

co Processing by Downstream 

00 Treatment Plant 

Multi-Media 

Filtration 

Dechiorination 

4 

' . . . . 

Reuse or 

, - . . . , - . . .. . . , . . . .. . . . .r a - •w::, 

- 

Discharge 

A- 39 
FLOW DIAGRAM PLANT NO. 39 

15.5 MGD (design) 

a1 

Screening 

® Sample Points 

1. Influent 

2. Final Effluent 

3. Secondary Sludge (Humus) 

4. Combined Sludge 

5. Influent Infiltration Percolation 

6. Effluent Infiltration Percolation 

Grit 

Removal 

Overflow 

4 

Primary 

~ Clarification 

~ 

E 5 ~ 

_ 

Trickling 

Filtration 

~ 

Secondary 

Clarification 

Gravity 

Thickening 

Supernatant 

Infiltration Anaerobic 

Percolation Digestion 

6 

Filtrate 

Vacuum 

Filtration 

Discharge 

Chlorination 

~ 

Landfill 

Discharge 

A-40 
FLOW DIAGRAM PLANT NO. 40 

8 MGD (design) 

Screening 

tXl 1 

Grit 

Removal 

Underflow 

® Sampie Points 

1. Influent 

2. Final Effluent 

3. Secondary Sludge (Humus) 

4. Combined Sludge 

5. Digester Subnatant 

6. Underflow (Drying Beds) 

~ 

(n I 

E 

~ 

_ 

3 

Primary 4 Anaerobic Drying 

Clarification Digestion , Beds 

... c 

m ~ Trickling ~ c v, 

Filtration ~ 8 ~ N Landill 

~ ~ 

Secondary Aerobic 

Clarification Digestion 

(Alternate 

Humus) 

Chlorination 

; 

2 Y 

~ 

Discharge ~ 

d 

A-41 
FLOW DIAGRAM PLANT NO. 51 

40 MGD design) 

Screening 

~ Sample Points 

1. Influent 

1 2. Final Effluent 

3. Primary Sludge 

4. Waste Activated Sludge 

Aerated 5. Heat Treatment Decant 

Grit 

Removal 

4 Centrate 

Preaeration 

Supernatant 

Prima ry 3 Anaerobic Centrifuge 

Clarification Digestion 

~ 

a~ 

. 

Diffused 

co 

Heat 

Aeration a n Treatment 

a~ ? Zi 

co 

~ 

~ 

~ ., 4 

Decant 5 

Secondary Decanting 

Clarification 

Filtrate Vacuum 

Chlorination Filtration 

2 

- i 

Scrubber Washwater 

Incineration 

Discharge 

Off-site 

A-42 Disposal 
FLOW DIAGRAM PLANT NO. 52 

3 MGD (design) 

1 [~ Sample Points 

influent 

2. Final Effluent 

Screening 

3. Combined Sludge 

Grit 

Removal 

Primary 3 Anaerobic 

' Clarification Digestion 

Supernatant 

E— 

Trickling 

Filtration 

Secondary 

Clarification 

Chlorination 

2 

Discharge 

Subnatant Drying 

Beds 

Land 

Application 

A-43 
FLOW DIAGRAM PLANT NO. 53 

6.0 MGD (design) 

Screening 

1 

Grit 

Removal 

® Sample Points 

1. Influent 

2. Intermediate Effluent 

3. Final Effluent 

4. Secondary Sludge 

S. Combined Sludge 

Primary 

Clarification 

Supernatant 

5TI Anaerobic 

Digestion Beds I + 

m 

o~ 

a 

~ 

C/3 

v 

a~ 

cc > 

~ 

0 

Q 

m 

~ 

co 

Trickling 

Filtration' 

,(Roughing) 

2 

Diffused 

Aeration 

Subnatant 

r 

Disposai 

~ 

4 

Secondary 

Clarification 

Chlorination 

3 

Discharge 

A-'44 
FLOW DIAGRAM ' PLANT NO. 54 

15.5 MGD (design) 

1 ~ 

~ Sampie Points 

1. Influent (industrial) 

Fomminution 2. Influent (total) 

3. Finai Effluent 

Supernatant 4. Waste Activated Sludge 

5. Combined Sludge 

Grit ' 

Removal 

~ • v 

~ . 

. 

~ 

~ Preaeration 

"a c

> 

~ 

~ 

4 

ID 

~ 

co 

~ 5 

Sludge Primary Anaerobic Storage Clarification Digestion Porrd., 

Diffused 

4 Aeration 

Secondary 

Clarification 

Chlorination 

3 

Discharge 

A-45 
FLOW DIAGRAM PLANT NO. 55 

42 MGD (design 

~ Sample Points 

1 1. Influent (industrial) 

2. Influent (total) , 

3: Intermediate Effluent 

2 4. Final Effluent 

Aeration 

(Lagoons) 

Secondary 

Clarification 

(Lagoons) 

Storage 

(Lagoons) 

3 

Infiltration 

Percolation 

4 

Discharge 

A-46 
4 

FLOW DIAGRAM PLANT NO. 56 

30 MGD (design) 

(h~ 1 

Screening 

® Sample Points 

1. Influent 

2. Primary Effluent 

3. Final Effluent 

4. Combined Sludge 

5. Waste Activated Sludge 

► 

_ 

Grit ` 

Removal 

a~ 

rn. 

~ 

~ 

~ 

~ 

~ 

co 

> 

~ 

U 

¢ 

a~ ~ 

~ 

~ co 

co 

3 

~ U 

m 

L 5 

a~ ~ 

i7L 

Primary 

Clarification 

+

6'~) 2 

Diffused 

Aeration 

Secondary 

Clarification 

Chlorination 

Filtration 

3 

Discharge 

A-47 ~ 
FLOW DIAGRAMIVO PLANT NO. 57 

7.4 MGD (design) 

1 6?j 1 

® Sample Points 

Screening 1. Influent (industrial) 

2. dinfiuent (total) 

3. Final Efftuent 

2 4. Primary Sludge 

S. Digested Sludge 

Grit 

Removal 

Filtrate 

Preaeration 

Supernatant 

Primary. 

4 Anaerobic 5 

Clarification Digestion 

Mechanical Supernatant Belt 

Aeration Filtration 

Secondary 

Clarification 

Waste 

Activated 

Sludge Dissolved 

Ai r 

Flotation 

Drying 

Beds 

Chlorination Landfill 

3 

Discharge 

A-48 
FLOW DIAGRAM PLANT NO. 58 

23 MGD (design) 

Screening 

& i' 

® Sample Points 

1. Influent 

2. Final Effluent 

3. Primary Sludge 

4. Waste Activated Sludge (thickened) 

Grit 

Removal 

Preaeration 

Supernatant 

Primary 

3 Anaerobic 

Clarification Digestion 

Diffused Filtrate Vacuum 

Aeration Filtration 

OverFlow 

Secondary W.A.S. Gravity 

4 

Clarification Thickening 

Land 

Application 

Chlorination 

b0 2 

Discharge 

A-49 
FLOW DIAGRAM PLANT NO. 59 

35 MGD (desigri) 

® Sample Points 

1. Influent 

Screening 2. Final Effluent 

3. .Gravity Thickener Overflow 

4. Combined Sludge (thickened) 

1 

Grit 

Removal 

Overflow 3 

4 

Primary Gravity Anaerobic 

Clarification Thickening Digestion 

Supernatant 

Diffused 

~ 

°? Sludge 

Aeration > ~ Storage 

U .0 

Q ~ 

a: co 

~ 

~ 

~ 

Secondary 

Clarification 

Ocean 

Disposal 

Chlorination 

2 

Discharge 

A-50 
FLOW DIAGRAM PLANT NO. 60 

5.0 MGD (design) 

Screening 

Comminution 

W 1A 

Industrial 

Wastes 

Rt 2 

l& Sample Points 

1. Influent (total) 

2. Influent (industrial) 

3. Primary Effluent 

4. Final Effluent 

5. Combined Sludge (thickened) 

6. Heat Treated Sludge 

Grit 

Removal 

Chemical 

Addition & 

Mixing 

Primary 

Clarification 

(Y 3 

Diffused ~ 

Aeration Fn 

~ 

a 

`a 

~ } 

c 

a 

Secondary 

Clarification 

Primary 5 

Sludge Gravity '001-wi Thickening 

Overflow 

a~ 

Decant 

Fi Itrate 

1B 

Heat 

Treatment 

Decanting 

6 

Vacuum 

Filtration 

Chlorination Incineration 

,~ 4 

— Influent (total) sampie is a flow-proportioned 

composite of locations 1 A and 1 B. 

Discharge — Incineration was not in use. Landfill 

A-51 
A-52 ' 
APPENDIX B 

CUMULATIVE DISTRIBUTION CURVES 

OF 

EFFLUENT CONCENTRATIONS AND PERCENT REMOVALS 

FOR THE` 

TWENTY-FOUR MOST FREQUENTLY FOUND POLLUTANTS 

Cr 
n=40 

0 20 40 60 80 

100 

A 

... 

80 

~ 

~ 60 

~ a 

,1 40 

~ 

a~ 

~ 

a 20 

0 

0 20 40 60 . 80 100 

100 

80 

60 

40 

20 

0 

CUMULATIVE DISTRIBUTION CURVES 

Copper Chromium 

~ nl 

~ 

` 

~ 

~ 

~ 

0 

IV cd 

~ 

~ 

c 

~ 

0 

U 

~ 

~ 

m 

~ 

~ W 

w 

W 

200 

160 

120 

80 

40 

— 

0 20 40 60 80 100 0 20 4u bu rsu luu 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentra•tion greater than zero 

B-2 
CUMULATIVE DISTRIBUTION CURVES 

Nickel Cadmium 

n=36 

A 

LE 

100 

80 

60 

40 

20 

0 

0 20 40 60 80 100 0 20 40 60- 80 100 

AI 400 

... 

100 

.. 

~ 

~ 

:3 . 320 ~ 

n= 36 

80 

~ 

0 

~ 240 60 

~ 

~ 

c.) 160 40 

~ 

-o 

U 

41 80 20 

~ 

~ 

w 

. w 0 4° 

0 20 40 60 80 100 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-3 
100 

~ 80 

,.. 

~ 

y 60 

~ 

4J 40 

c~ 

c~ 

a 20 

0 ~ 

u 

s 

n=34 

100 

80 

60 

40 

20 

0 

n=35 

.. 

0 20 40 60 80 100 0 20 40 60 80 100 

~ 

1.0 

0.8 

0.6 

0.4 

0.2 

0 

.-. 

Al 200 

~ 

~ 

~ 160 

0 

O 

~ 120 

~ 

+~ 

~ 80 

~ 

a v 

~ 40 

a~ 

~ 

~ 

44 

`N w 0 

CUMULATIVE DISTRIBUTION CURVES 

Lead Mercury 

0 20 40 60 80 100 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

,B-4 
n=40 

0 20 40 60 80 100 

100 

r. 

n~ 80 

~ 

> 60 

0. 

a~ a 

41 40 

~ 

a~ 

U 

}~ 

w 20 

1 0 

0 20 40 60 80 100 

100 

80 

60 

40 

20 

0. 

CUMULATIVE DISTRIBUTION CURVES 

Silver Z inc 

Al 15 

~ 

~ 

~ 

~ 12 

... 

c 

0 

~ 9 

~ 

~4 

43 

~ 

oci 6 

c 

0 

U 

4J 

c 3 

a~ 

~ 

~ 

w 

". W 0 

500 

400 

300 

200 

100 

0 

n=40 

0 20 40 60 80 100 0 20 40 60 80 100 

I Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-5 
100 

Al 80 

... 

~ 60 

~ 

a 

c~ 40 

~ a

U 

$4 

w 20 

~ 

~ 

n=40 100 

80 

60 

40 

20 

0 

n=40 

0 20 40 60 80 100 0 20 40 60 80 100 

CUMULATIVE DISTRIBUTION CURVES 

Cyanide Toluene 

.,. 

340 

n=40 

240 

180 

120 

60 

0 

0 20 40 60 80 100 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= num,ber of plants with average influent concentration greater than zero 

~ 

~ 

~ 

... 

~ 

0 

~ 

~ 

~ 

U 

~ 

O 

t~ 

4J 

c 

a~ 

~ 

~ 

w 

w 

W 

B-6 
CUMULATIVE DISTRIBUTION CURVES 

Benzene 1,1,1 Trichloroethane 

100 100 

n=38 1 

80 80 

60 60 

40 40 

~ 20 20 

0 I 

0 20 40 60 80 100 0 20 40 60 80 100 

n=32 

1000 

800 

600 

400 

200 

n=38 1 

0 20 40 60 80 100 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-7 
100 

80 

60 

40 

20 

0 

.. 

~ 

60 

100 

C80 

ra 

41 40 

9 

u H 

~ 20 

~ 

CUMULATIVE DISTRIBUTION CURVES ` 

Ethylbenzene Chloroform 

0 20 40 60 80 100 0 20 40 60 80 100 

.~. 

A( 75 

10 

~ n=39 

~ 

~ 8 60 ~ 

V 

M 

~ 6 45 

(d 

44 

~ 4 30 

c 

0 

~ 

41 2 15 

m 

~ f 

w 0 t I I 0 

0 20 40 60 80 ,00 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater thaiL zero 

B-8 
00 

~ 

80 

M40 

0 

0 20 40 60 80 100 

100 

80 

60 

40 

20 

0 

CUMULATIVE DISTRIBUZ'ION CURVES ^ 

Tetrachloroethylene Trichloroethylene 

0 20 40 60 80 100 

100 

80 

60 

40 

20 

0 

0 20 40 60 80 100 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-9 
CUMULATIVE DISTRIBUTION CURVES 

1,2 Trans Dichloroethylene Methylene Chloride 

100 

~ 

Al 80 

~ 

> 60 

~ a 

41 40 

a~ 

U $fi 

a, 20 

n--32 1 

100 

80 

60 

40 

20 

0 

n=40 

y 

0 20 40 60 80 100 0 20 40 60 80 10 

.-. 

Al 10 1000 

i n=32 n=40 

~ 8 800 

~ 

0 6 600 

~ 

a~ 4 400 

U 

O 

U 

~ 2 200 

~ 

a~ 

~ 

~ 

w 0 0 

W 

0 20 40 60 80 100 0' 20 40 60 80 1 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-10 
Bis(2-Ethylhexl) Phthalate 

100 

n=40 

80 

60 

40 

20 

0 

to r 

Phenol 

n=38 

t 

n0 

I 

CUMULATIVE DISTRIBUTION CURVES 

0 20 40 60 80 100 0 20 40 60 80 100 

5 100 

n=38 n=40 

0 80 

60 

0 40 

5 " 20 

U Gu 4U l'w ov 1vv 

Percent of Plants Percent of Plants 

. n= number of plants with average influent concentration greater than zero 

8.-11 
CUMULATIVE DISTRIBUTION CURVES 

Butyl Benzyl Pnthalate Naphthalene 

100 

nl 80 

~ 

~ 

~ 60 

~ 

a 

4J 40 

c~ 

U 

$4 

p, 20 

0 

n=35 

1 

IN 

) 20 40 60 80 100 

100 

80 

60 

40 

20 

0 

0 20 40 

t 

60 80 

~ 

Al 10 

~ 

~ 

tr' 8 ~ 

~ 

~ 

0 

~ 6 

a 

~ 

~ 4 

~ 0 

U 

4J 2 

m 

~ • 

~ 

W 0 

10 

8 

6 

4 

2 

0 

0 20 40 60 80 100 0 20 40 60 80 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-12 
CT3MULATIVE DISTRIBUTION CURVES 

100 Di-N-Butyl Phthalate 1( Diethyl Phthalate 

80 

~] 

40 

20 

0' 

n=31 1 

0 20 40 60 80 100 0 20 40 60 80 100 

2.5 

2.0 

1.5 

1.0 

.5 

0 

0 20 40 60 80 100 0 20 40 60 80 100 

Percent of Plants Percent of Plants 

NOTE: n= number of plants with average influent concentration greater than zero 

B-13 
B-14 
APPENDIX C 

SUMMARY OF ANALYTICAL DATA 

PLANTS 1 to 40 AND 51 to 60 

C-i 
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APPENDIX E 

MASS BALANCE IN POUNDS PER DAY 

PLANTS 1 to 40 AND 51 to 60 

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