Dry Scrubber Blue Goose Combustion Data Septem ber 2011 Fyrite

Location : Dry

Scrubber Date 9/27/11 Time:

run O2 CO2

1 18 3 2 18 3 3 18 3
Avg 18 3

Molecular wt

1 29.2 2 29.2 3 29.2

AVG 29.2

diff 0

0 0

All diff must be less that 0.3
Analysts: O'Brien &Gere

Page 1Test ID: 9-27-11-POM-ABF Run #3 

### Value 0

0 0

250.00 110.00 0.0009 0.0000 0.0000 200.00 200.00 0.0009

240.00 140.00 0.0022 0.0022

970.00 1000.00 0.0001 0 0.00010



### Value 2.3000 0.9000 3.2000 Total mg of Particulate MCEM **Total mg of MCEM** 

# An **ode Bake Furnace Dry Scrubber Test #3** 

3W B W eight of MCEM From Blank (g) 3WNet of Extracted W ater Adjusted from Blank (g)

Total mg of Gaseous MCEM Volume of Deionized W ater Used 3W(ml) Volume of Deionized W ater Used in Blank (ml) 2M Net MCEM Adjusted from Blank (g)



# 9/27/2011

**MCEM Analysis Data** 1A Filter W eight (g)

3WW eight of Impinger W ater Plus Back Half Rinses Extracted (g). Volume of Acetone Used 3A (ml) Volume of MC Used 3M (ml) 3M W eight of MCEM From Back Glassware Rinses (g) 3M Net of MCEM Adjusted from Blanks (g)



### MCEM Analysis Calculations 1B QC Filter Blank (g) Net MCEM From Filter (g) Volume of Acetone Used 2A (ml) Volume of MC Used 2M (ml) 2M W eight of MCEM From Front Half Glassware Rinses (g) 4A W eight of Acetone Blank (g) 4M W eight of MC Blank (g) Volume of MC Used in Blank (ml) Volume of Acetone Used in Blank (ml)Test ID: 9-27-11-POM-ABF Run #3



### Value 0.5599 0.84 18 % O 2 in Anode Bake Furnace Gas Stream 3.0000 %CO 2 in Anode Bake Furnace Gas Stream 29.2 28.64223146 0.049800762 540.3 647.7 29 70 1.65 1.021 29 128 0.88 71.298 76.9 28.98 0.25 0.00034088462



### Value 69.1045094 35.51310 50.1 2.35821 26.8 1.26362 0.049801 0.059479 99.0692 Md = Stack gas dry molecular weight, (lb/lb-mole) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/27/2011**

**Method 5 Parameter**  p = Stack gas v elocity pressure (av g. sqrt  p - in. water) Cp = Pitot tube calibration coefficient

Total sampling time required for test (min) Ms = Stack gas (wet) molecular weight (lb/lb-mole) Bws = Stack gas moisture content

Vwc(std) Nozzle diameter (in) Area of Nozzle (ft^2)

Vm (std) = Volume of sample measured by DGM (dscf) Vs = Average stack gas v elocity Total impinger catch (ml) Tm = Absolute average dry gas meter temp (R). Ts = Stack gas absolute average temperature (R) Pm = Pressure at orifice meter (in. Hg) Ta = Sampling site ambient temperature, (°F)  H@ = Orifice meter calibration factor, (in. water) Y = Dry gas meter calibration factor Pbar = Barometric pressure, (in. Hg)

I = % Isokinetic variation



### Air Test Calculations  Hav g= average orifice meter differential Vm = Total sample volume from dry gas meter (dcf) Vlc Volume collected Ps = Absolute stack gas pressure (in Hg)

Vwc (std) = conv erted water v olume Total silica gel catch (ml) Vwsg (std) = conv erted silica gel water v olume Bws = fraction of gas that is moistureTest ID: 9-27-11-POM-ABF Run #3 LIMS ID#: 2011008911



### Value 2.3000 0.0023 0.9 0.0009 69.10450937

29 38.48 9.45 Green Carbon Baked tons/hr 0.049800762 61515.76211 3690945.7266 81992.64825 Acfm 64739.85631 Scfm 0.0007 Emission Rate of Total MCEM gr/dscf 0.27 6.49 0.1059 2.54 **0.38**

**0.029 Emission Rate of Gaseious MCEM lb/Ton of Green Carbon Baked**  **0.011 Emission Rate of Particulate MCEM lb/Ton of Green Carbon Baked**  **0.040 Emission Rate of Total MCEM lb/Ton of Green Carbon Baked** 

Start time: 9/27/2011 16:30:00 PM End time: 9/27/2011 18:444:00 PM

Qstd Flow of Anode Bake Furnace Emissions (dscf/hr)

Emission Rate of Gaseous MCEM lb/hr Emission Rate of Gaseous MCEM lb/d Emission Rate of Particulate MCEM lb/hr

**Emission Rate of Total MCEM lb/hr** Emission Rate of Particulate MCEM lb/d Pbar Barometric Pressure During Test (in Hg) Area of Anode Bake Furnace Stack (ft2)

Bws Moisture in Roof Emissions Qstd Flow of Anode Bake Furnace Emissions (dscf/min) Total mg of MCEM in Particulate Sample Total g of MCEM in Particulate Sample Total mg of MCEM in Gaseous Sample

Vm(std) Volume of Air Sampled by DGM (dscf) 

# An **ode Bake Furnace Dry Scrubber Test #3**  **9/27/2011**

**Combined Method 5 Parameter and Analytical**
Total g of MCEM in Gaseous Sample

## Value 3.2

0.0032 69.10450937

29 38.48 9.45 Green Carbon produced tons/hr 0.049800762 61558.2161 Qstd Flow of Anode Bake Furnace Emissions (dscf/min) 3693492.963 0.0007 Particulate gr/dscf **0.38 Particulate lb/hr** 

**0.040 Particulate Emissions from Anode Bake Furnace lb/Ton of Green Carbon Baked**  Qstd Flow of Anode Bake Furnace Emissions (dscf/hr) 

## Combined Method 5 Parameter and Analy **tical**

Vm(std) Volume of Air Sampled by DGM (dscf) Pbar Barometric Pressure During Test (in Hg) 

# An **ode Bake Furnace Emission Calculations Test #2 9/27/2011** 

Total mg of Particulate Total g of Particulate

Area of Anode Bake Furnace Stack (ft2 )

Bws Moisture in Anode Bake Furnace Emissions