544 DK14140820472812633

DK141R

X X X X

X

X

Page 1 SANITIZED SUBMISSIONX



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Page 2 SANITIZED SUBMISSIONBruce Reinwald Owner Rhineland Specialties, Inc. 129 S Scoville Ave Oak Park IL 60302 reinwaldb@aol.com

Bruce Reinwald Owner Rhineland Specialties, Inc. 129 S Scoville Ave Oak Park IL 60302 reinwaldb@aol.com 708-445-0750



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X

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Page 3 SANITIZED SUBMISSION

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XXX 

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XXX


### X 384001 SOLVENT RED 252 CAS SAN.PDF XXX 

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See Attachment 025 (SOLVENT RED 252 STRUCTURES SAN.pdf)

SOLVENT RED 252 STRUCTURES SAN.pdf

Page 4 SANITIZED SUBMISSIONXXX

Coupling reaction

>95% 

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Page 5 SANITIZED SUBMISSIONPage 6 SANITIZED SUBMISSIONPage 7 SANITIZED SUBMISSIONSOLVENT RED 252

SOLVENT RED 252

Xanthylium, x-[2-(alcoxycarbonyl)phenyl]-bis(alkylamino)-dimethyl-, x'-[x''-[hydroxy-x'''-[[[[hydroxy-x''''-(phenyldiazenyl)-sulfo-2- naphthalenyl]amino]carbonyl]amino]sulfo-naphthalenyl]diazenyl]benzoate, sodium salt.

Page 8 SANITIZED SUBMISSIONXXX XXX 

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X Open, non-dispersive use. XXX X 100 15 0 100 0 0



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Page 9 SANITIZED SUBMISSIONPart I, Section C, 2.a. Additional Consumer Use Text

Category of Use XXX: Product is to be used in an ink paste (15% PMN Substance) in ball point pens.

Page 10 SANITIZED SUBMISSIONPage 11 SANITIZED SUBMISSIONPage 12 SANITIZED SUBMISSIONPage 13 SANITIZED SUBMISSIONPage 14 SANITIZED SUBMISSION0

Page 15 SANITIZED SUBMISSIONPage 16 SANITIZED SUBMISSIONThe PMN substance will be imported as an ingredient in the finished article.

No processing of the PMN substance will take place in the USA. The PMN subsatance will be discarded with paper as a component after use and in residual amounts from the original spent articles. Therefore, the amount of exposure and environmental release will be minimal.

Page 17 SANITIZED SUBMISSION001 Safety Data Sheet DOKU Brilliant Red 213-EU.pdf Worksheet: Physical State 6

002 BOILING POINT DETERMINATIONS Boiling Point Determination of F 213 Red_Short Report.pdf 10

003 FLAMMABILITY DETERMINATION Flammability Determination of F 213 Red.pdf Worksheet: Flammability 31

004 MELTING RANGE DETERMINATION Melting point_Melting range Determination of F 213 Red.pdf Worksheet: Other Property (Melting Range) 37

005 PARTITION COEFFICIENT DETERMINATION Partition Coefficient Determination of F 213 Red.pdf Worksheet: Octanol / water partition coefficient 47

006 RELATIVE DENSITY DETERMINATION Relative Density determination of F 213 Red.pdf Worksheet: Density 30

007 SELF IGNITION DETERMINATION Relative Self-Ignition Temperature Determination of F 29

008 WATER SOLUBILITY DETERMINATION Water Solubility Determination of F 213 Red.pdf Worksheet: Solubility In Water 39

009 28 DAY ORAL TOXICITY 28-Day Oral Toxicity Study with F 213 Red in the Rat.pdf 178

010 ACUTE DERMAL TOXICITY Acute Dermal Toxicity (Limit Test) with F 213 Red in the 54

011 ACUTE EYE IRRITATION Acute Eye Irritation Study with F 213 Red.pdf 52

012 ACUTE ORAL TOXICITY Acute Oral Toxicity (Acute Toxic 59
013 IN VITRO MAMMALIAN CELL GENE MUTATION In Vitro Mammalian Cell Gene Mutation Test_ Mouse 123

014 IN VITRO MAMMALIAN CHROMOSOME ABERRATION IN VITRO MAMMALIAN CHROMOSOME ABERRATION 63

015 REPRODUCTION/DEVELOPMENTAL Reproduction_Developmental 273

016 REVERSE MUTATION ASSAY USING BACTERIA Reverse Mutation Assay using Bacteria (Salmonella 100

017 SKIN SENSITIZATION: LOCAL LYMPH NODE ASSAY Skin Sensitisation_Local Lymph Node Assay with F 213 Red.pdf 63

018 ACUTE TOXICITY TO ZEBRA FISH Acute Toxicity of F 213 Red to Zebrafish (Brachydanio rerio) in a 72

019 ACUTE TOXICITY TO DAPHNIA MAGNA Acute Toxicity of of F 213 Red to 81

020 GROWTH INHIBITION TEST ON ALGAE Growth Inhibition Test of F 213 Red on Algae 100

021 ACTIVATED SLUDGE RESPIRATION F 213 Red in an Activated 50 

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022 HYDDROLYSIS DETERMINATION AS FUNCTION OF pH Hydrolysis Determination of F 213 Red as a Function of pH 67

023 READY BIODEGRADABILITY Ready Biodegradability of F 213 Red in a Closed Bottle Test.pdf 63

024 SOLVENT RED 252 CAS SAN SOLVENT RED 252 CAS SAN.PDF Pt.I, Sec.B, 1c. 1

025 SOLVENT RED 252 STRUCTURE SAN SOLVENT RED 252 STRUCTURES SAN.pdf Pt.I, Sec.B, 1e. 1

Page 19 SANITIZED SUBMISSION001 

### X X Measured

006 

### X 1.357 Measured

008 

### X 0.00065 Measured 20



### X 005 Log Pow 2.94 Measured



### X 003 Did not ignite Measured



### X 004 224 deg.C Decomposition Measured Melting Range

Page 20 SANITIZED SUBMISSION

### ATTACHMENT HEADER SHEET

Attachment Number 001
Attachment Name Safety Data Sheet


### Associated PMN Section Number Worksheet: Physical State

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 002
Attachment Name BOILING POINT DETERMINATIONS


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 003
Attachment Name FLAMMABILITY DETERMINATION


### Associated PMN Section Number Worksheet: Flammability

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 004
Attachment Name MELTING RANGE DETERMINATION


### Associated PMN Section Number Worksheet: Other Property (Melting Range)

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 005
Attachment Name PARTITION COEFFICIENT DETERMINATION


### Associated PMN Section Number Worksheet: Octanol / water partition coefficient

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 006
Attachment Name RELATIVE DENSITY DETERMINATION


### Associated PMN Section Number

Worksheet: Density

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 007
Attachment Name SELF IGNITION DETERMINATION


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 008
Attachment Name WATER SOLUBILITY DETERMINATION


### Associated PMN Section Number Worksheet: Solubility In Water

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 009
Attachment Name 28 DAY ORAL TOXICITY


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 010
Attachment Name ACUTE DERMAL TOXICITY


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 011
Attachment Name ACUTE EYE IRRITATION


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 012
Attachment Name ACUTE ORAL TOXICITY


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 013
Attachment Name IN VITRO MAMMALIAN CELL GENE MUTATION


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 014
Attachment Name IN VITRO MAMMALIAN CHROMOSOME ABERRATION


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 015
Attachment Name REPRODUCTION/DEVELOPMENTAL TOXICITY SCREENING



### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 016
Attachment Name REVERSE MUTATION ASSAY USING BACTERIA


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 017
Attachment Name SKIN SENSITIZATION: LOCAL LYMPH NODE ASSAY


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 018
Attachment Name ACUTE TOXICITY TO ZEBRA FISH


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 019
Attachment Name ACUTE TOXICITY TO DAPHNIA MAGNA


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 020
Attachment Name GROWTH INHIBITION TEST ON ALGAE


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 021
Attachment Name ACTIVATED SLUDGE RESPIRATION INHIBITION TEST


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 022
Attachment Name HYDDROLYSIS DETERMINATION AS FUNCTION OF pH


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 023
Attachment Name READY BIODEGRADABILITY


### Associated PMN Section Number

N/A

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 024
Attachment Name SOLVENT RED 252 CAS SAN


### Associated PMN Section Number

Pt.I, Sec.B, 1c.

Does not contain CBI 

### Report Number DK14140820472812633

### ATTACHMENT HEADER SHEET

Attachment Number 025
Attachment Name SOLVENT RED 252 STRUCTURE SAN


### Associated PMN Section Number

Pt.I, Sec.B, 1e.

Does not contain CBI 

### Report Number DK14140820472812633