**CBI? ICR_ID**  **Unit ID for One Distillation Colum** **n with Feed in the**  **Com posite Sam** **ple Unit IDs for Other** 

**Distillation Colum n(s)**  **with Feed in the Com** **posite Sam ple**  **Sam ple Date**  **Indicate if the sam** **ple was collected before**  **or after the desalter**  no AK5A0050 KUTP NA 5/1/2011 Not Applicable no AK5A0050 KUTP NA 6/1/2011 Not Applicable no AK5A0050 KUTP NA 7/1/2011 Not Applicable no AK5A0090 Crude1 Crude2, Crude3 6/27/2011 After no AK5A0090 Crude1 Crude2, Crude3 8/1/2011 After

no AK5A0090 Crude1 Crude2, Crude3 6/6/2011 After

no AL3C0030 110 6/8/2011 After no AL3C0030 210 5/11/2011 After no AL3C0030 210 5/11/2011 After no AL3C0030 110 7/6/2011 After no AL3C0030 210 5/11/2011 After no AL3C0030 110 5/11/2011 After no AL3D0010 Crude D8.1 7/26/2011 After no AL3D0010 Crude D8.1 6/28/2011 After no AL3D0010 Crude D8.1 5/25/2011 After no AL3D0020 Crude Unit 5/18/2011 Before no AL3D0020 Coker Unit 5/18/2011 After no AL3D0020 Crude Unit 7/26/2011 Before no AL3D0020 Coker Unit 6/27/2011 After no AL3D0020 Crude Unit 6/27/2011 Before no AL3D0020 Coker Unit 7/26/2011 After no AR3D0100 Crude Unit Not applicable 5/10/2011 Before no AR3D0100 Crude Unit Not applicable 7/18/2011 Before no AR3D0100 Crude Unit Not applicable 6/21/2011 Before

no AR3DO110 No. 4 CDU 6/10/2011 Purchased Condensate Before

no AR3DO110 No. 4 CDU 7/12/2011 Purchased Condensate Before

no AR3DO110 No. 4 CDU 5/3/2011 Purchased Condensate Before

no AR3DO110 No. 4 CDU 5/3/2011 Crude Before no AR3DO110 No. 4 CDU 7/12/2011 Crude Before no AR3DO110 No. 4 CDU 8/5/2011 Crude Before

no AR3DO110 No. 4 CDU 8/5/2011 Purchased Condensate Before

no AR3DO110 No. 4 CDU 6/10/2011 Crude Before no CA5A0120 11002 N/A 7/11/2011 Before no CA5A0120 11002 N/A 5/11/2011 Before no CA5A0120 11001 N/A 6/9/2011 Before no CA5A0120 11001 N/A 7/11/2011 Before no CA5A0120 11001 N/A 5/11/2011 Before no CA5A0120 11003 N/A 7/11/2011 Before no CA5A0120 11002 N/A 6/9/2011 Before no CA5A0120 11003 N/A 6/9/2011 Before no CA5A0120 11003 N/A 5/11/2011 Beforeno CA5A0190 U01-Crude 8/8/2011 Before

no CA5A0190 U01-Crude 7/7/2011 Before no CA5A0190 U01-Crude 8/8/2011 Before no CA5A0190 U01-Crude 7/7/2011 Before no CA5A0190 U01-Crude 8/8/2011 Before no CA5A0190 U01-Crude 7/7/2011 Before no CA5A0190 U01-Crude 6/6/2011 Before no CA5A0190 U01-Crude 6/6/2011 Before no CA5A0190 U01-Crude 6/6/2011 Before no CA5A0200 1103387-01 7/14/2011 Not Applicable no CA5A0200 1103788-01 8/8/2011 Not Applicable no CA5A0200 1102645-01 6/3/2011 Not Applicable no CA5A0210 Unit 399 6/15/2011 Before no CA5A0210 Unit 399 5/12/2011 Before no CA5A0210 Unit 399 7/15/2011 Before no CA5A0220 S-37-1 6/23/2011 Not Applicable no CA5A0220 S-37-1 7/26/2011 Not Applicable no CA5A0220 S-37-1 5/26/2011 Not Applicable

no CA5A0230(P1S1) Crude Unit No. 1 7/25/2011 Before

no CA5A0230(P1S2) Crude Unit No 2 5/23/2011 Before

no CA5A0230(P1S1) Crude Unit No. 1 5/23/2011 Before

no CA5A0230(P1S2) Crude Unit No 2 7/25/2011 Before

no CA5A0230(P1S1) Crude Unit No. 1 6/23/2011 Before

no CA5A0230(P1S2) Crude Unit No 2 6/23/2011 Before

no CA5A0310 Unit 10 Unit 11 6/15/2011 Before no CA5A0310 Unit 10 Unit 11 5/12/2011 Before no CA5A0310 Unit 10 Unit 11 7/15/2011 Before no CA5A0330 1-1 7/20/2011 Not Applicable no CA5A0330 1-1 6/20/2011 Not Applicable no CA5A0330 1-1 5/19/2011 Not Applicable no CO4A0340 #3Crude 7/27/2011 Before no CO4A0340 #3Crude 6/20/2011 Before no CO4A0340 #3Crude 5/17/2011 Before no CO4A0340 #1Crude (13) 7/28/2011 Before no CO4A0340 #1Crude (13) 6/21/2011 Before no CO4A0340 #1Crude (13) 5/19/2011 Before no CO4A0340 #2Crude (02) 7/27/2011 Before no CO4A0340 #2Crude (02) 6/20/2011 Before no CO4A0340 #2Crude (02) 5/17/2011 Before

no DE1A0360 21-CDU 7/22/2011 - 008-TF200 Before

no DE1A0360 21-CDU 7/22/2011 - 007-TF200 Before

no DE1A0360 21-CDU 7/22/2011 - 005-TF200 Before

no DE1A0360 21-CDU 6/17/2011 - 001-TF200 Before

no DE1A0360 21-CDU 6/17/2011 - 002-TF200 Beforeno DE1A0360 21-CDU 6/17/2011 - 005-TF200 Before

no DE1A0360 21-CDU 5/6/2011 - 012-TF274 Before

no DE1A0360 21-CDU 5/6/2011 - 009-TF400 Before

no IL2A0400 111 5/26/2011 Before no IL2A0400 111 4/26/2011 Before no IL2A0400 111 6/29/2011 Before no IL2A0410 1-D-1 N/A 4/27/2011 After no IL2A0410 1-D-1 N/A 7/13/2011 After no IL2A0410 1-D-1 N/A 6/17/2011 After no IL2A0420 01-Crude Unit 6/1/2011 After no IL2A0420 01-Crude Unit 4/25/2011 After no IL2A0420 01-Crude Unit 7/21/2011 Before no IN2A0440 11A Pipestill NA 6/30/2011 After no IN2A0440 11A Pipestill NA 4/28/2011 After no IN2A0440 11C Pipestill NA 5/31/2011 After no IN2A0440 11A Pipestill NA 5/31/2011 After no IN2A0440 11C Pipestill NA 4/28/2011 After no IN2A0440 11C Pipestill NA 6/30/2011 After no IN2A0440 12 Pipestill NA 5/31/2011 After no IN2A0440 12 Pipestill NA 6/30/2011 After no IN2A0440 12 Pipestill NA 4/28/2011 After no IN2A0450 Crude 6/29/2011 Before no IN2A0450 Crude 7/26/2011 Before

no IN2A0450 Crude 5/16/2011 Before

no KS2C0460 TK 80101 5/10/2011 Before no KS2C0460 TK 80101 5/10/2011 Before no KS2C0460 TK 80101 6/9/2011 Before no KS2C0460 TK 80101 7/10/2011 Before no KS2C0460 TK 80101 7/10/2011 Before no KS2C0460 TK 80101 5/10/2011 Before no KS2C0460 TK 80101 7/10/2011 Before no KS2C0470 FPU2 5/26/2011 After no KS2C0470 FPU2 4/20/2011 After no KS2C0470 FPU1 4/20/2011 After no KS2C0470 FPU2 7/7/2011 After no KS2C0470 FPU1 7/7/2011 After no KS2C0470 FPU1 5/26/2011 After no KS2C0480 3 7/1/2011 After no KS2C0480 3 5/25/2011 After no KS2C0480 3 8/2/2011 After no KY2A0490 1-041 5/20/2011 After no KY2A0490 2-023 6/20/2011 After no KY2A0490 1-041 4/20/2011 After no KY2A0490 2-023 5/20/2011 After no KY2A0490 1-041 6/20/2011 After no KY2A0490 2-023 4/20/2011 After

no LA3C0520 # 2 ACD Unit # 5 ACD Unit 6/2/2011 Before

no LA3C0520 # 2 ACD Unit # 5 ACD Unit 8/19/2011 Beforeno LA3C0520 # 2 ACD Unit # 5 ACD Unit 7/19/2011 Before

no LA3C0560 459 "CV-1" Not Applicable 4/28/2011 After

no LA3C0560 307 "C-Topper" Not Applicable 4/28/2011 After

no LA3C0560 301 "A-Topper" Not Applicable 5/25/2011 After

no LA3C0560 302 "B-Topper" Not Applicable 6/24/2011 After

no LA3C0560 307 "C-Topper" Not Applicable 5/25/2011 After

no LA3C0560 459 "CV-1" Not Applicable 5/13/20112 After

no LA3C0560 302 "B-Topper" Not Applicable 5/25/2011 After

no LA3C0560 307 "C-Topper" Not Applicable 6/24/2011 After

no LA3C0560 302 "B-Topper" Not Applicable 4/28/2011 After

no LA3C0560 459 "CV-1" Not Applicable 5/25/20112 After

no LA3C0560 301 "A-Topper" Not Applicable 4/28/2011 After

no LA3C0560 301 "A-Topper" Not Applicable 6/24/2011 After

no LA3C0590 PSLA9 N/A 5/5/2011 After no LA3C0590 PSLA10 N/A 5/5/2011 After no LA3C0590 PSLA7 N/A 6/9/2011 After no LA3C0590 PSLA7 N/A 5/5/2011 After no LA3C0590 PSLA10 N/A 6/9/2011 After no LA3C0590 PSLA9 N/A 7/6/2011 After no LA3C0590 PSLA10 N/A 7/6/2011 After no LA3C0590 PSLA8 N/A 5/5/2011 After no LA3C0590 PSLA7 N/A 7/6/2011 After no LA3C0590 PSLA8 N/A 7/6/2011 After no LA3C0590 PSLA8 N/A 6/9/2011 After no LA3C0590 PSLA9 N/A 6/9/2011 After no LA3C0600 NO 2 CRUDE 5/5/2011 After no LA3C0600 NO 2 CRUDE 7/5/2011 After no LA3C0600 NO 2 CRUDE 6/6/2011 After no LA3C0600 NO 1 CRUDE 6/6/2011 After no LA3C0600 NO 1 CRUDE 7/5/2011 After no LA3C0600 NO 1 CRUDE 5/5/2011 After no LA3C0610 U210 4/28/2011 After no LA3C0610 U210 7/13/2011 After no LA3C0610 U10 4/28/2011 After no LA3C0610 U210 5/31/2011 After no LA3C0610 U10 7/13/2011 After no LA3C0610 U10 5/31/2011 After no LA3C0620 VPS-2 N/A 5/23/2011 After no LA3C0620 VPS-1 N/A 5/23/2011 After no LA3C0620 VPS-1 N/A 6/28/2011 After no LA3C0620 VPS-1 N/A 8/1/2011 After no LA3C0620 VPS-2 N/A 8/1/2011 Afterno LA3C0620 VPS-2 N/A 6/28/2011 After

no LA3C0630 DISTILLING 6.23.11 After no LA3C0630 DISTILLING 7.20.11 After no LA3C0630 DISTILLING 5.17.11 After no LA3C0640 CR 6/17/2011 After no LA3C0640 CR 5/23/2011 After no LA3C0640 CR 7/15/2011 After no LA3C0670 CRUDE 4/28/2011 After no LA3C0670 CRUDE 6/30/2011 After no LA3C0670 CRUDE 5/24/2011 After

no LA3C0700 C1ATMOS 4/19/2011 Before

no LA3C0700 C1ATMOS 5/13/2011 Before

no LA3C0700 C1ATMOS 6/16/2011 Before

no LA3D0530 100 (Crude Unit) N/A 7/28/2011 Before no LA3D0530 100 (Crude Unit) N/A 6/23/2011 Before no LA3D0530 100 (Crude Unit) N/A 5/18/2011 Before no LA3D0540 Crude 1 N/A 7/6/2011 Before no LA3D0540 Crude 1 N/A 5/27/2011 Before no LA3D0540 Crude 1 N/A 4/25/2011 Before no LA3D0660 93 5/5/2011 Before no LA3D0660 93 6/29/2011 Before no LA3D0660 58 6/29/2011 Before no LA3D0660 93 7/31/2011 Before no LA3D0660 58 7/31/2011 Before no LA3D0660 58 5/5/2011 Before no MI2A0710 5 7/15/2011 After no MI2A0710 5 6/13/2011 After no MI2A0710 5 4/27/2011 After no MN2B0720 11-1 8/10/2011 After no MN2B0720 11-2 7/20/2011 After no MN2B0720 11-2 8/10/2011 After no MN2B0720 11-2 6/23/2011 After no MN2B0720 25 7/20/2011 After no MN2B0720 25 8/8/2011 After no MN2B0720 11-1 6/23/2011 After no MN2B0720 11-1 7/20/2011 After no MN2B0720 25 6/16/2011 After no MN2B0730 2 7/18/2011 After no MN2B0730 2 6/17/2011 After no MN2B0730 1 7/18/2011 After no MN2B0730 2 5/17/2011 After no MN2B0730 1 5/17/2011 After no MN2B0730 1 6/17/2011 After no MS3D0750 CDU N/A 7/5/2011 Not Applicable no MS3D0750 CDU N/A 6/11/2011 Not Applicable no MS3D0750 CDU N/A 7/5/2011 Not Applicable no MS3D0750 CDU N/A 5/10/2011 Not Applicable no MS3D0750 CDU N/A 6/12/2011 Not Applicable no MS3D0750 CDU N/A 5/10/2011 Not Applicable no MS3D0760 Crude Unit 7/28/2011 After no MS3D0760 Crude Unit 5/26/2011 After no MS3D0760 Crude Unit 6/29/2011 Afterno MT4A0770 #2 Crude Unit 4/21/2011 Before

no MT4A0770 #1 Crude Unit 4/21/2011 Before no MT4A0770 #2 Crude Unit 3/21/2011 Before no MT4A0770 #2 Crude Unit 5/24/2011 Before no MT4A0770 #1 Crude Unit 3/21/2011 Before no MT4A0770 #1 Crude Unit 5/24/2011 Before no MT4A0790 BIRF Crude 6/27/2011 Not Applicable no MT4A0790 BIRF Crude 6/27/2011 Not Applicable no MT4A0790 BIRF Crude 6/27/2011 Not Applicable no MT4A0790 BIRF Crude 4/27/2011 Not Applicable no MT4A0790 BIRF Crude 4/27/2011 Not Applicable no MT4A0790 BIRF Crude 4/27/2011 Not Applicable no MT4A0790 BIRF Crude 5/27/2011 Not Applicable no MT4A0790 BIRF Crude 5/27/2011 Not Applicable no MT4A0790 BIRF Crude 5/27/2011 Not Applicable no MT4A0800 1 5/20/2011 After no MT4A0800 1 4/20/2011 After no MT4A0800 1 6/21/2011 After no NJ1A0820 PT1-A 7/5/2011 Not Applicable no NJ1A0820 PT1-A 4/28/2011 Not Applicable no NJ1A0820 PT1-A 5/31/2011 Not Applicable no NJ1A0860 Crude Unit 7 atm 5/26/2011 After no NJ1A0860 Crude Unit 7 atm 4/28/2011 After no NJ1A0860 Crude Unit 6 atm 5/26/2011 After no NJ1A0860 Crude Unit 6 atm 6/29/2011 After no NJ1A0860 Crude Unit 7 atm 6/29/2011 After no NJ1A0860 Crude Unit 6 atm 4/28/2011 After no NM3E0880 CRUDE 8/3/2011 After no NM3E0880 CRUDE 7/7/2011 After no NM3E0880 CRUDE 5/11/2011 After no NM3E0890 002 N/A 06/07/2011 After no NM3E0890 002 N/A 07/07/2011 After no NM3E0890 002 N/A 06/07/2011 After no NM3E0890 002 N/A 08/03/2011 After no NM3E0890 002 N/A 08/03/2011 After no NM3E0890 002 N/A 07/07/2011 After no NM3E0891 082 N/A 08/04/2011 After no NM3E0891 082 N/A 08/04/2011 After no NM3E0891 082 N/A 06/08/2011 After no NM3E0891 082 N/A 06/08/2011 After no NM3E0891 082 N/A 07/06/2011 After no NM3E0891 082 N/A 07/06/2011 After no NV5A0810 Crude Unit 7/20/2011 Not Applicable no NV5A0810 Crude Unit 5/5/2011 Not Applicable no NV5A0810 Crude Unit 6/21/2011 Not Applicable no NV5A0810 Crude Unit 6/21/2011 Not Applicable no NV5A0810 Crude Unit 6/21/2011 Not Applicable no NV5A0810 Crude Unit 7/20/2011 Not Applicable no NV5A0810 Crude Unit 5/5/2011 Not Applicable no NV5A0810 Crude Unit 5/5/2011 Not Applicable no NV5A0810 Crude Unit 7/20/2011 Not Applicable no OH2A0910 Crude 2 NA 7/6/2011 Before no OH2A0910 Crude 1 NA 5/4/2011 Before no OH2A0910 Crude 1 NA 7/6/2011 Before no OH2A0910 Crude 1 NA 6/3/2011 Beforeno OH2A0910 Crude 2 NA 6/3/2011 Before

no OH2A0910 Crude 2 NA 5/4/2011 Before no OH2A0920 4-0 Crude 5/13/2011 After no OH2A0920 4-0 Crude 7/15/2011 After no OH2A0920 4-0 Crude 6/15/2011 After no OH2A0930 B004 None 6/17/2011 After no OH2A0930 B004 None 5/18/2011 After no OH2A0930 B004 None 7/18/2011 After no OH2A0940 P801-31 5/25/2011 After no OH2A0940 P801-31 4/27/2011 After no OH2A0940 P801-51 5/25/2011 After no OH2A0940 P801-51 4/27/2011 After no OH2A0940 P801-31 6/22/2011 After no OH2A0940 P801-51 6/22/2011 After no OK2C0960 #1 Crude 4/13/2011 Before no OK2C0960 #2 Crude 4/13/2011 Before no OK2C0960 #1 Crude 5/3/2011 Before no OK2C0960 #2 Crude 5/3/2011 Before no OK2C0960 #2 Crude 6/8/2011 Before no OK2C0960 #1 Crude 6/8/2011 Before no OK2C0970 CDU 6/1/2011 After no OK2C0970 CDU 6/28/2011 After no OK2C0970 CDU 7/26/2011 After no OK2C0980 CDU 6/28/2011 After no OK2C0980 CDU 7/26/2011 After no OK2C0980 CDU 6/1/2011 After no OK2C0990 100 5/2/2011 Before no OK2C0990 100 7/7/2011 Before no OK2C0990 100 6/7/2011 Before no PA1A1020 12-3 Crude Unit 15-1 Crude Unit 4/19/2011 Before no PA1A1020 12-3 Crude Unit 15-1 Crude Unit 6/28/2011 After no PA1A1020 12-3 Crude Unit 15-1 Crude Unit 5/26/2011 Before no PA1A1030 210A 210B 6/28/2011 After no PA1A1030 137 5/27/2011 After no PA1A1030 210A 210B 8/1/2011 After no PA1A1030 137 7/11/2011 After no PA1A1030 137 6/28/2011 After no PA1A1030 210A 210B 5/27/2011 After

no PA1B1010 Truck Unloading (PA Crude) 8/3/2011 Before

no PA1B1010 Railcar Unloading (Ohio Crude) 8/3/2011 Before

no PA1B1010Crude Unit Distillation Column (Mix) 8/1/2011 After

no PA1B1050 Crude Unit 7/7/2011 After no PA1B1050 Crude Unit 8/8/2011 After no PA1B1050 Crude Unit 6/7/2011 After no TN2A1060 01-WCU 04-ECU 6/13/2011 Before no TN2A1060 01-WCU 04-ECU 5/11/2011 Before no TN2A1060 01-WCU 04-ECU 7/13/2011 Before no TX3A1080 2 7/10/2011 After no TX3A1080 2 5/10/2011 After no TX3A1080 2 5/10/2011 After no TX3A1080 2 5/10/2011 Afterno TX3A1080 2 7/10/2011 After

no TX3A1080 2 7/10/2011 After no TX3A1080 2 6/10/2011 After no TX3A1080 2 6/10/2011 After no TX3A1080 2 6/10/2011 After

no TX3A1120 F-101 5/23/2011 After

no TX3A1120 C-1601 6/27/2011 After no TX3A1120 F-101 6/28/2011 After no TX3A1120 C-1601 8/2/2011 After

no TX3A1120 C-1601 5/19/2011 After

no TX3A1120 F-101 8/1/2011 After

no TX3A1190 (CRUDE 4) Atmospheric Crude Distillation NA 5/25/2011 After

no TX3A1190 (CRUDE 4) Atmospheric Crude Distillation NA 7/21/2011 After

no TX3A1190 (CRUDE 4) Atmospheric Crude Distillation NA 6/23/2011 After

no TX3A1290 Tk 200 7/14/2011 Before no TX3A1290 Tk 200 5/12/2011 Before no TX3A1290 Tk 338 Tk 339 5/12/2011 Before no TX3A1290 Tk 200 6/14/2011 Before

no TX3A1290 Tk 338 Tk 339 6/14/2011 Before

no TX3A1290 Tk 338 Tk 339 7/14/2011 Before

no TX3A1300 1 CRUDE N/A 6/2/2011 Before

no TX3A1300 2 CRUDE N/A 7/8/2011 Before

no TX3A1300 2 CRUDE N/A 6/2/2011 Before

no TX3A1300 1 CRUDE N/A 5/4/2011 Before

no TX3A1300 2 CRUDE N/A 5/4/2011 Beforeno TX3A1300 1 CRUDE N/A 7/8/2011 Before

no TX3B1110 PS3A NA 6/13/2011 Before no TX3B1110 PS3B NA 7/14/2011 Before no TX3B1110 PS3B NA 6/13/2011 Before no TX3B1110 PS3A NA 5/11/2011 Before no TX3B1110 PS3A NA 7/14/2011 Before no TX3B1110 PS3B NA 5/16/2011 Before no TX3B1130 10-U10 4/20/2011 Before no TX3B1130 10-U10 6/23/2011 Before no TX3B1130 10-U10 5/24/2011 Before no TX3B1150 CRUFU001 N/A 5/24/2011 After no TX3B1150 CRUFU001 N/A 6/24/2011 After no TX3B1150 CRUFU001 N/A 7/25/2011 After no TX3B1160 PS8 6/27/2011 Before no TX3B1160 PS3 7/1/2011 Before no TX3B1160 PS7N 5/27/2011 Before no TX3B1160 PS8 5/27/2011 Before no TX3B1160 PS3 6/1/2011 Before no TX3B1160 PS7S 6/27/2011 Before no TX3B1160 PS7N 6/27/2011 Before no TX3B1160 PS8 7/27/2011 Before no TX3B1160 PS7S 7/27/2011 Before no TX3B1160 PS7S 5/27/2011 Before no TX3B1160 PS7N 7/27/2011 Before no TX3B1160 PS3 8/1/2011 Before no TX3B1170 CUB -88 5/5/2011 Before no TX3B1170 CUA -88 5/5/2011 Before no TX3B1170 CUB -88 6/6/2011 Before no TX3B1170 CUA -88 6/6/2011 Before no TX3B1170 CUB -88 7/6/2011 Before no TX3B1170 CUA -88 7/6/2011 Before

no TX3B1180 42DS20 Desalter MID CRUDE 8/9/2011 After

no TX3B1180 40DH0 Desalter WEST CRUDE 8/9/2011 After

no TX3B1180 40DH0 Desalter WEST CRUDE 6/10/2011 After

no TX3B1180 40DH0 Desalter WEST CRUDE 7/13/2011 After

no TX3B1180 42DS20 Desalter MID CRUDE 7/13/2011 After

no TX3B1180 42DS20 Desalter MID CRUDE 6/10/2011 After

no TX3B1181 723A Desalter EAST CRUDE 8/9/2011 After

no TX3B1181 723A Desalter EAST CRUDE 7/13/2011 After

no TX3B1181 723A Desalter EAST CRUDE 6/10/2011 After

no TX3B1200 536-UNIT N/A 8/9/2011 After no TX3B1200 537-UNIT N/A 7/13/2011 Afterno TX3B1200 533-UNIT N/A 7/14/2011 After

no TX3B1200 533-UNIT N/A 5/17/2011 After

no TX3B1200 537-UNIT N/A 8/9/2011 After

no TX3B1200 536-UNIT N/A 6/10/2011 After

no TX3B1200 537-UNIT N/A 6/10/2011 After no TX3B1200 536-UNIT N/A 7/13/2011 After no TX3B1200 533-UNIT N/A 6/16/2011 After no TX3B1210 4 5 5/3/2011 After no TX3B1210 4 5 7/6/2011 After no TX3B1210 4 5 6/2/2011 After

no TX3B1220 Vacuum Pipe Stills 4 (VPS4) 5/16/2011 Before

no TX3B1220 Vacuum Pipe Stills 2 (VPS2) 5/16/2011 Before

no TX3B1220 Vacuum Pipe Stills 4 (VPS4) 6/13/2011 Before

no TX3B1220 Vacuum Pipe Stills 2 (VPS2) 6/13/2011 Before

no TX3B1220 Vacuum Pipe Stills 4 (VPS4) 7/11/2011 Before

no TX3B1220 Vacuum Pipe Stills 2 (VPS2) 7/11/2011 Before

no TX3B1250 AVU-146 AVU-147 7/11/2011 Before no TX3B1250 AVU-146 AVU-147 5/3/2011 Before no TX3B1250 AVU-146 AVU-147 6/6/2011 Before no TX3B1310 CRUDE 5/10/2011 Not Applicable no TX3B1310 CRUDE 7/8/2011 Not Applicable no TX3B1310 CRUDE 6/9/2011 Not Applicable

no TX3B1320 Distillation Feed -

Crude Desalter Effluent (Lab package# T81147) Not Applicable 7/12/2011 After

no TX3B1320 Distillation Feed -

Crude Desalter Effluent (Lab package# T78950) Not Applicable 6/17/2011 After

no TX3B1320 Distillation Feed -

Crude Desalter Effluent (Lab package# T76206) Not Applicable 5/16/2011 After

no TX3B1330 #1 & #2 Crude 6/15/2011 Before no TX3B1330 #3 Crude 6/15/2011 Before no TX3B1330 #3 Crude 8/2/2011 Before no TX3B1330 #1 & #2 Crude 7/20/2011 Before no TX3B1330 #3 Crude 5/11/2011 Before no TX3B1330 #1 & #2 Crude 5/11/2011 Before no UT4A1360 No.1 Crude Unit 7/21/2011 Not Applicable no UT4A1360 No.1 Crude Unit 4/18/2011 Not Applicableno UT4A1360 No.1 Crude Unit 5/11/2011 Not Applicable

no UT4A1370 Crude Unit 6/24/2011 Before no UT4A1370 Crude Unit 4/21/2011 Before no UT4A1370 Crude Unit 5/21/2011 Before no UT4A1380 7/6/2011 After no UT4A1380 8/5/2011 After no UT4A1380 6/6/2011 After no VI6A1530 CDU 5 7/11/2011 before no VI6A1530 CDU 5 5/11/2011 before no VI6A1530 CDU 5 6/14/2011 before no VI6A1530 CDU 6 6/14/2011 before no VI6A1530 CDU 6 7/11/2011 before no VI6A1530 CDU 6 5/11/2011 before

no WA5A140010-Crude (Atmospheric) NA 7/28/2011 After

no WA5A140010-Crude (Atmospheric) NA 6/30/2011 After

no WA5A140010-Crude (Atmospheric) NA 7/8/2011 After

no WA5A1410 VPS 7/13/2011 Before no WA5A1410 VPS 6/16/2011 Before no WA5A1410 VPS 5/11/2011 Before no WA5A1440 LCU 5/24/2011 After no WA5A1440 LCU 4/19/2011 After no WA5A1440 LCU 6/28/2011 After

no WI2B1460 P19 5/11/2011 After

no WI2B1460 P19 6/15/2011 After

no WI2B1460 P19 7/18/2011 After

no WV1B1450 CDU N/A 5/6/2011 After no WV1B1450 CDU N/A 7/11/2011 After no WV1B1450 CDU N/A 6/8/2011 After no WY4A1470 25 5/28/2011 Before no WY4A1470 25 7/1/2011 Before no WY4A1470 25 8/1/2011 Before no WY4A1480 Syncrude 6/28/2011 After no WY4A1480 North Dakota 88 6/28/2011 After no WY4A1480 Syncrude 5/27/2011 After no WY4A1480 North Dakota 88 5/27/2011 After no WY4A1480 Syncrude 4/28/2011 After no WY4A1480 North Dakota 88 4/28/2011 After no WY4A1490 Crude Unit None 7/7/2011 Not Applicable no WY4A1490 Crude Unit None 6/23/2011 Not Applicable no WY4A1490 Crude Unit None 5/25/2011 Not Applicable no WY4A1500 Crude Unit 6/7/2011 Not Applicable no WY4A1500 Crude Unit 6/7/2011 Not Applicable no WY4A1500 Crude Unit 8/2/2011 Not Applicable no WY4A1500 Crude Unit 5/12/2011 Not Applicableno WY4A1500 Crude Unit 5/12/2011 Not Applicable

no WY4A1510581 Crude Distillation 6/28/2011 Before no WY4A1510581 Crude Distillation 5/24/2011 Before no WY4A1510581 Crude Distillation 5/2/2011 Before no WY4A1510582 Crude Distillation 6/28/2011 Before no WY4A1510582 Crude Distillation 5/24/2011 Before no WY4A1510582 Crude Distillation 5/2/2011 Before no WY4A1510 1 NA 7/11/2011 Not Applicable no WY4A1510 1 NA 5/13/2011 Not Applicable no WY4A1510 1 NA 6/6/2011 Not Applicable

no WY4A1520 Crude Unit

(Prefract Tower Feed) N/A 7/20/2011 After

no WY4A1520 Crude Unit

(Prefract Tower Feed) N/A 6/17/2011 After

no WY4A1520 Crude Unit

(Prefract Tower Feed) N/A 5/23/2011 After**Higher Heating Value**

**(Btu/lb) Density** 

**(lb/ft 3** **) API** 

**Gravity Mercury,** 

**ppmw Chlorine,** 

**ppmw Sulfur,** 

**ppmw Antim** **ony,**

**ppmw** 18,787 56.88 23.70 < 0.040 < 396.0 15,300< 0.990 < 18,946 56.84 23.80 < 0.040 < 398.0 20,090< 0.980 < 18,833 56.81 23.90 < 0.040 < 395.0 154,000< 0.970 < 19,677 52.90 35.40 < 0.100 1.00 11,800< 1.00 < 20,045 49.30 47.70 < 0.100 1.00 10,200< 1.00 < 19,422 53.90 32.30 < 0.100 1.00 8,200< 1.00 < 16,000 50.29 44.10 < 0.012 < 17.00 1,200< 1.40 < 16,000 51.62 39.50 < 0.013 < 17.00 820.0< 1.10 < 19,000 52.29 37.40 < 0.015 < 16.00 1,300< 1.10 < 19,000 50.57 43.10 < 0.012 < 16.00 2,100< 1.10 < 20,000 52.30 37.30 < 0.015 < 16.00 2,500< 1.50 < 19,000 50.35 43.90 < 0.016 < 16.00 1,400< 1.50 < 19,000 49.80 45.80 < 0.013 26.00 4,000< 1.90 < 19,000 49.97 45.20 < 0.014 27.00 3,300< 1.50 < 19,000 49.52 46.80 < 0.014 23.00 1,900< 0.910 < 18,987 56.19 25.57 < 0.017 219.0 351.8< 0.990 < 18,215 60.14 15.22 < 0.015 137.0 496.5< 0.980 < 18,871 55.84 26.53 < 0.016 65.60 249.2< 0.960 < 18,413 59.09 17.85 < 0.016 1.60 346.1 1.60 < 18,673 56.03 26.00 < 0.017 0.61 310.4< 0.910 < 18,311 58.43 19.52 < 0.016 < 45.00 318.1< 0.870 < 19,400 56.80 < 0.008 < 4.00 5,630 0.427 19,200 57.00 23.70 < 0.008 50.70 5,710 0.142 19,100 56.94 24.00 < 57.00 9,790< < 16,400 43.97 69.40 < 0.005 < 1.00 <400.0 0.029 <

16,700 43.50 69.90 < 0.008 < 4.00 <1,000 0.184

17,500 43.80 61.10 < 0.002 < 4.00 1,480 0.146 < 19,100 56.20 34.30 < 0.002 142.0 16,000 0.176 < 19,200 53.40 32.20 < 0.008 < 4.00 19,300 0.274 19,200 53.90 32.80 0.004 57.20 16,140 0.148 < 18,900 47.20 54.10 0.005 < 4.00 <1,000 0.115 < 19,000 53.20 34.50 < 0.005 < 1.00 14,600 0.311 19,348 54.67 30.00 < 0.100 1.00 31,200< 1.00 < 18,754 54.39 30.90 < 0.100 1.00 27,000< 1.00 < 18,783 54.66 30.10 < 0.100 1.00 23,400< 1.00 < 19,700 54.62 30.20 < 0.100 1.00 13,800< 1.00 < 19,043 54.49 30.60 < 0.100 1.00 13,100< 1.00 < 19,670 54.17 31.50 < 0.100 1.00 11,400< 1.00 < 18,689 54.73 29.90 < 0.100 1.00 10,800< 1.00 < 19,541 54.02 32.00 < 0.100 1.00 9,400< 1.00 < 19,214 54.17 31.60 < 0.100 1.00 9,000< 1.00 <18,339 59.90 15.90 < 0.090 79.00 13,800< 25.0 <

15,658 59.90 16.10 < 0.083 67.00 14,000< 25.0 < 18,526 59.90 15.90 < 0.091 48.50 13,800< 24.0 < 15,592 59.90 16.10 < 0.092 66.50 14,000< 24.0 < 18,230 59.90 15.90 < 0.084 55.00 13,700< 23.0 < 15,277 59.90 16.10 < 0.090 70.50 13,000< 23.0 < 19,254 60.10 15.50 < 0.092 66.00 13,000< 23.0 < 20,435 60.10 15.50 < 0.097 68.50 13,000< 23.0 < 18,704 60.10 15.50 < 0.095 59.50 13,000< 22.0 < 25,893 61.44 12.20 < 449.0 58,000< < 17,661 60.98 13.30 < 231.0 55,000< < 19,212 60.68 13.50 < 340.0 51,000< < 17,757 58.71 18.90 < 72.00 33,000< < 18,211 58.59 19.20 < < 66.00 32,000< < 14,518 58.79 18.70 < 90.00 37,000< < 20,295 54.50 30.70 < < 27.0 4,900< < 18,251 54.40 30.90 < < 95.0 5,700< < 18,864 54.50 30.50 < 42.0 5,300< < 18,498 56.93 23.60 < 0.010 62.00 12,700< 0.100 18,499 56.97 23.50 < 0.010 68.00 16,600< 0.100 < 18,409 56.89 23.70 < 0.010 65.00 12,600< 0.100 < 17,711 57.37 22.40 < 0.010 130.0 12,500< 0.100 18,599 56.56 24.60 < 0.010 20.00 12,400< 0.100

< < < < < 16,200 56.42 25.00 < 54.50 15,000< < 18,424 56.93 23.60 < 80.50 11,000< < 15,263 57.04 23.30 < < 30.00 17,000< < 16,086 58.65 18.80 < 13.00 15,600< < 17,311 57.97 20.50 < 13.00 14,000< < 17,251 58.12 20.20 < 25.00 14,300< < 18,717 56.89 23.60 0.002 < 10.00 30,800< 1.00 < 18,689 56.76 24.00 0.005 10.90 27,200< 1.00 17,810 56.76 24.00 0.004 < 10.00 27,600< 1.00 19,235 52.19 37.60 0.004 11.90 2,770< 1.00 < 18,665 52.13 37.80 0.005 18.90 2,730< 1.00 < 19,054 52.13 37.80 0.005 22.60 2,670< 1.00 < 17,509 48.84 47.60 0.005 < 10.00 726.0< 1.00 < 19,411 48.90 47.40 0.006 < 10.00 970.0< 1.00 < 19,340 48.90 47.40 0.005 < 10.00 1,030< 1.00 < 19,046 56.00 26.20 < 0.100 118.0 10,512< 2.50 < 18,968 56.00 26.00 < 0.100 50.70 9,444< 2.50 < 18,755 56.60 24.40 < 0.100 120.4 8,283< 2.50 < 18,922 56.70 31.50 < 0.100 26.34 22,840< 2.50 < 18,994 53.80 32.50 < 0.100 60.33 20,993< 2.50 <18,888 54.10 24.20 < 0.100 45.95 9,925< 2.50 <

18,874 56.65 24.30 < 0.100 14.38 7,436< 1.25 < 18,944 53.44 33.50 < 0.100 62.28 24,158< 1.25 < 18,307 55.53 27.50 < 0.050 < 200.0 28,900< 0.500 < 16,840 55.46 27.70 < 0.050 < 200.0 28,500< 0.500 < 18,316 55.88 26.50 < 0.050 < 200.0 29,300< 0.500 < 18,800 56.39 25.00 0.006 420.0 17,000 0.300 < 17,500 57.18 23.00 0.006 < 250.0 21,000 0.230 < 18,600 57.50 22.00 0.010 < 350.0 16,000 0.240 19,090 52.88 35.40 0.003 7.50 7,410< 0.050 19,403 52.72 35.90 0.002 8.40 7,140< 0.050 < 18,990 52.85 35.50 0.002 96.90 6,840< 0.050 < 19,473 56.07 25.90 < 0.100 1.00 24,900< 1.00 < 19,298 55.72 26.90 < 0.100 1.00 22,700< 1.00 < 19,608 56.15 25.60 < 0.100 1.00 21,800< 1.00 < 19,596 55.45 27.60 < 0.100 1.00 21,600< 1.00 < 18,856 55.09 28.70 < 0.100 1.00 18,800< 1.00 < 19,750 53.36 33.80 < 0.100 1.00 17,300< 1.00 < 19,648 51.46 40.00 < 0.100 1.00 5,400< 1.00 < 19,829 51.41 40.10 < 0.100 1.00 4,200< 1.00 < 18,733 51.51 39.80 < 0.100 1.00 2,900< 1.00 < 18,662 53.43 33.06 < 0.002 2.70 3,402 0.009 18,799 53.00 34.40 0.003 2.00 2,437 0.003 18,908 52.88 34.77 < 0.002 3.10 2,753< 0.002 18,600 53.25 34.30 < < 12,000< < 18,800 53.22 34.40 < < 11,800< < 19,000 53.16 34.60 < < 10,700< < 19,000 53.03 35.00 < < 10,800< < 18,900 52.96 35.20 < < 11,100< < 18,700 53.28 34.20 < < 11,900< < 18,800 53.03 35.00 < < 10,900< < 19,131 55.11 28.65 < 98.20 21,610< < 19,190 55.73 26.87 < 171.0 <1,000< < 19,541 52.66 36.08 < 103.0 <1,000< < 19,164 55.68 27.02 < 225.0 19,530< < 19,603 52.14 34.57 < 149.0 5,050< < 19,683 52.60 36.29 < 74.10 4,420< < 19,054 54.48 30.50 < 37.00 16,350< < 18,952 55.10 28.80 < < 1.00 18,240< < 18,750 54.80 29.60 < 28.00 15,650< < 18,754 53.60 33.20 0.003 11.7 16,060< 0.050 < 19,234 53.18 34.50 0.004 4.80 7,250< 0.050 19,180 53.34 34.00 0.002 9.60 14,540< 0.050 < 19,250 52.67 36.10 0.007 8.00 5,960< 0.050 18,897 53.37 33.90 < 0.002 5.50 16,140< 0.050 < 19,433 53.31 34.10 0.002 8.60 8,050< 0.050 17,218 51.33 40.40 < 81.00 2,000< < 18,312 51.49 39.90 < 146.0 1,500< <18,166 50.07 40.90 < 562.0 1,300< <

17,189 57.23 22.70 < 476.0 19,200< < 17,552 55.75 27.00 < 510.0 13,700< < 17,850 53.38 33.80 < 80.70 10,700< < 17,347 54.38 30.80 < 161.0 12,600< < 17,319 54.25 31.20 < 108.0 7,410< < 15,511 57.75 21.40 < 98.40 11,000< < 17,130 54.69 29.90 < 94.50 8,900< < 17,731 54.44 30.70 < 194.0 13,100< < 16,858 55.47 27.60 < 434.0 11,300< < 17,535 58.00 20.70 < 74.90 20,800< < 19,314 50.89 41.90 < 577.0 6,920< < 17,934 50.82 42.30 < 321.0 2,000< < 17,969 53.80 32.60 < 0.100 78.40 5,900< 1.00 < 18,013 55.20 28.20 < 0.100 82.80 10,400< 1.00 < 17,313 56.20 25.50 < 0.100 135.0 19,300< 1.00 < 17,176 55.90 26.30 < 0.100 119.0 11,800< 1.00 < 16,886 55.50 27.50 < 0.100 159.0 16,500< 1.00 < 16,929 53.90 32.30 < 0.100 59.00 19,800< 1.00 < 16,649 56.20 25.60 < 0.100 62.80 29,000< 1.00 < 18,031 53.80 32.50 < 0.100 64.00 13,500< 1.00 < 16,660 56.10 25.80 < 0.100 66.00 36,600< 1.00 < 16,599 54.00 31.80 < 0.100 51.60 35,800< 1.00 < 17,052 53.90 32.20 < 0.100 133.0 28,300< 1.00 < 17,362 53.90 32.20 < 0.100 127.0 14,100< 1.00 < 16,680 59.40 17.10 < 0.100 174.0 19,200< 1.00 < 17,179 59.60 16.60 < 0.100 83.00 23,900< 1.00 < 15,863 58.00 20.60 < 0.100 71.40 25,900< 1.00 < 16,868 56.10 25.70 < 0.100 125.0 14,700< 1.00 < 17,123 54.60 30.20 < 0.100 79.80 19,800< 1.00 < 16,952 55.60 27.30 < 0.100 95.80 7,300< 1.00 < 19,015 54.40 30.70 < 0.002 11.60 19,950< 0.050 < 18,850 55.50 27.50 < 0.002 < 3.00 19,510< 0.050 < 19,034 54.10 31.70 < 0.002 19.80 16,770< 0.050 < 18,734 55.70 27.10 < 0.002 5.90 23,230< 0.050 < 18,869 54.70 30.00 < 0.002 7.70 20,670< 0.050 < 18,820 54.00 32.00 < 0.002 5.50 18,970< 0.050 < 18,961 54.86 29.29 < 0.016 1.30 22,630< 0.990 < 18,971 55.36 27.84 < 0.015 2.20 22,290< 0.980 < 18,945 54.66 29.87 < 0.016 < 30.00 25,280< 0.980 < 18,876 54.96 29.06 < 0.015 < 38.00 26,840< 0.920 < 18,870 54.60 30.13 < 0.016 < 38.00 26,180< 0.920 <18,837 54.67 29.84 < 0.015 < 36.00 26,070< 0.870 <

19,256 54.40 30.70 < 0.100 38.74 4,150< 2.50 < 19,312 53.70 32.90 < 0.100 19.90 3,795< 2.50 < 19,199 53.46 33.60 < 0.500 77.74 3,292< 1.25 < 18,914 53.79 32.60 < 0.100 5,071 9,983< 1.07 < 18,910 54.09 31.40 < 0.100 2,952 10,460< 1.06 < 19,090 54.09 31.60 < 0.100 2,401 9,182< 1.05 < 18,998 53.70 33.02 < 0.100 < 5.00 0.99 < 1.52 < 18,726 53.50 32.71 < 0.100 < 5.00 0.99 < 1.04 < 19,031 53.70 32.91 < 0.100 < 5.00 0.99 < 1.02 < 17,972 52.31 37.20 < 0.100 285.0 <1,000< 5.00 < 16,658 52.18 37.60 < 0.100 317.0 2,200< 2.00 < 18,253 52.86 35.50 < 0.100 123.0 3,300< 2.00 < 20,100 57.37 50.60 0.170 < 4.00 20.9 0.437 < 19,200 47.43 52.90 0.015 < 4.00 < 4.00 < 0.050 < 19,400 48.65 49.00 0.018 < 4.00 8.49 < 0.010 < 18,102 58.00 20.70 < 0.100 97.20 31.0 < 2.00 < 17,601 57.73 21.40 < 0.100 126.0 29.0 < 2.00 < 16,110 57.24 22.70 < 0.100 37.6 10.0 < 2.00 < 18,831 53.52 33.40 < 0.010 11.20 17,600< 0.100 < 18,211 52.07 38.00 < 0.005 9.00 8,540< 0.100 < 18,161 52.56 36.50 < 0.005 51.00 4,410< 0.100 18,680 51.12 41.10 < 0.005 3.10 3,740< 0.100 < 19,189 52.55 36.40 0.018 33.30 2,380< 0.100 < 19,124 50.80 42.20 < 0.010 37.10 3,870< 0.100 < 18,446 53.29 34.20 < 0.002 49.10 15,530< 0.050 < 18,510 53.58 33.30 < 0.002 5.60 16,230< 0.050 19,100 53.42 33.80 < 0.002 7.70 10,720< 0.050 < 19,620 52.34 37.20 < 0.100 1.00 27,800< 1.00 < 19,659 58.71 18.90 < 0.100 1.00 37,600< 1.00 < 19,551 50.79 42.40 < 0.100 1.00 37,100< 1.00 < 19,207 57.71 21.50 < 0.100 1.00 35,000< 1.00 < 19,865 58.16 20.30 < 0.100 1.00 34,600< 1.00 < 19,743 58.37 18.20 < 0.100 1.00 34,400< 1.00 < 19,335 57.88 21.10 < 0.100 1.00 33,400< 1.00 < 19,965 57.33 22.50 < 0.100 1.00 31,400< 1.00 < 19,236 55.99 26.20 < 0.100 1.00 30,200< 1.00 < 18,998 52.10 38.00 < 0.038 28.00 3,767< 0.992 < 19,469 56.30 25.50 < 0.040 50.00 2,666< 0.982 < 18,585 57.90 21.00 < 0.038 16.00 27,840< 0.978 < 18,677 57.10 22.90 < 0.040 58.00 21,860< 0.978 < 18,894 52.20 37.60 < 0.039 69.00 1,832< 0.977 < 18,939 51.50 39.90 < 0.039 < 1.00 17,400< 0.982 < 19,200 57.57 20.90 < 0.008 < 4.00 5,530< 0.050 < 19,300 56.51 < 0.005 < 40.00 4,430< 0.049 < 19,100 57.38 21.80 < 0.008 < 4.00 4,660 0.074 19,100 56.78 20.40 < 0.002 < 4.00 9,920 0.187 < 19,200 57.57 < 0.005 < 40.00 7,020< 0.049 < 19,300 57.28 22.10 < 0.002 < 4.00 5,880 0.193 < 18,463 58.78 18.71 < 0.017 82.50 394.2< 0.970 < 18,539 59.13 17.76 < 0.016 < 0.50 434.6< 0.940 < 18,459 59.35 17.20 < 0.016 170.0 418.8< 0.890 <18,597 57.10 23.00 < 0.038 35.00 20,690< <

18,758 56.60 24.10 < 0.039 16.00 24,660< < 18,613 57.20 22.70 < 0.039 < 1.00 28,000< < 18,607 57.10 23.00 < 0.040 34.00 24,660< < 18,645 56.90 23.80 < 0.039 < 1.00 26,700< < 23,280 56.60 24.50 < 0.039 25.00 23,280< < 18,231 56.10 25.90 < 1.00 < 200.0 30,200< 5.00 < 18,221 56.10 26.10 < 1.00 < 200.0 30,000< 5.00 < 18,094 56.10 25.90 < 1.00 < 200.0 29,300< 5.00 < 17,592 56.10 25.70 < 1.00 < 200.0 28,100< 5.00 < 17,701 56.10 25.90 < 1.00 < 200.0 28,000< 5.00 < 17,251 56.10 25.90 < 1.00 < 200.0 27,900< 5.00 < 18,470 56.20 25.70 < 1.00 < 200.0 26,000< 5.00 < 18,877 56.10 25.70 < 1.00 < 200.0 26,300< 5.00 < 19,111 56.20 25.70 < 1.00 < 200.0 25,800< 5.00 < 18,431 56.16 25.70 < < 26,400< < 17,749 56.10 26.00 < < 25,000< < 18,374 56.66 24.20 < < 28,600< < 19,200 56.19 25.70 < 0.032 < 49.00 <3,700< 2.10 < 20,100 56.52 24.80 < 0.033 < 43.00 <2,800< 2.10 < 18,100 56.56 24.70 < 0.033 57.00 <2,900< 1.90 < 18,751 54.20 31.20 < 0.100 260.0 24,638< 2.50 < 18,903 53.50 33.30 < 0.100 9.83 24,937< 2.50 < 18,901 54.90 29.10 < 0.100 78.20 17,984< 2.50 < 19,338 54.60 30.10 < 0.100 54.64 14,370< 2.50 < 18,940 54.00 31.90 < 0.100 54.64 24,362< 2.50 < 19,085 54.40 30.80 < 0.100 9.16 15,470< 1.25 < 19,339 50.48 43.40 0.040 25.0 925 0.997 19,683 50.74 42.50 0.039 47.0 1,030 0.966 19,618 50.54 43.20 0.039 < 1.00 1,452 0.963 19,039 53.55 33.29 < 0.040 116.0 15,520< 1.00 < 19,399 53.53 33.36 < 0.040 214.0 14,230< 1.00 < 19,353 53.55 33.30 < 0.040 92.60 15,460< 1.00 < 19,022 52.82 35.56 < 0.040 63.70 10,360< 1.00 < 18,973 52.83 35.55 < 0.020 74.70 10,530< 1.00 < 19,418 53.53 33.37 < 0.040 165.0 14,330< 1.00 < 19,011 53.14 34.56 < 0.020 94.30 12,490< 1.00 < 19,020 53.14 34.54 < 0.020 88.20 12,410< 1.00 < 19,525 52.74 35.83 < 0.040 129.0 10,210< 1.00 < 19,491 52.75 35.80 < 0.040 170.0 10,170< 1.00 < 19,470 52.63 36.18 < 0.040 212.0 9,520< 1.00 < 19,510 52.60 36.27 < 0.040 209.0 9,360< 1.00 < 19,219 7.51 25.60 < 0.040 < 500.0 6,500< 2.15 < 18,028 7.71 21.50 < 0.039 < 500.0 23,600< 2.08 < 18,501 7.66 22.50 < 0.040 < 500.0 20,100< 1.92 < 18,823 7.56 24.70 < 0.040 < 500.0 15,500< 1.88 < 18,990 7.49 26.10 < 0.040 < 500.0 5,100< 1.79 < 18,836 7.61 23.50 < 0.040 < 500.0 22,800< 1.78 < 18,802 7.52 25.40 0.052 < 500.0 5,900< 1.46 < 18,725 7.69 22.00 < 0.040 < 500.0 23,500< 1.35 < 18,705 7.54 25.00 < 0.040 < 500.0 20,300< 1.15 < 19,645 52.63 36.10 < 0.100 1.00 8,900< 1.00 < 18,957 55.83 26.60 < 0.100 1.00 29,300< 1.00 < 19,433 56.89 23.60 < 0.100 1.00 28,800< 1.00 < 19,608 56.15 25.60 < 0.100 1.00 21,800< 1.00 <18,245 51.85 38.70 < 0.100 1.00 21,200< 1.00 <

19,281 53.49 33.50 < 0.100 1.00 15,300< 1.00 < 19,185 53.30 34.20 0.006 11.40 14,700< 0.050 < 18,781 53.90 32.20 0.004 < 3.00 15,850< 0.050 < 19,108 51.70 39.30 0.005 4.90 4,540< 0.050 < 18,596 52.23 36.83 < 0.002 1.80 4,873< 0.002 18,884 51.78 38.28 0.003 3.10 5,650< 0.002 17,723 51.93 38.50 < 0.002< 1.00 5,012< 0.002 19,609 53.00 34.60 < 0.100 50.56 2,606< 1.25 < 19,527 53.00 35.10 < 0.100 71.24 2,985< 1.25 < 19,601 51.30 40.60 < 0.100 39.76 3,854< 1.25 < 19,477 51.50 40.00 < 0.100 128.3 4,770< 1.25 < 19,301 53.31 34.10 < 0.100 23.60 1,763< 1.25 < 19,198 51.15 41.10 < 0.100 16.42 3,673< 1.25 < 19,400 51.30 40.70 < 207.0 3,720< < 19,200 52.60 36.50 < 391.0 10,200< < 19,600 51.40 40.50 < 140.0 3,460< < 19,500 52.30 37.40 < 352.0 8,980< < 19,200 53.00 35.10 < 307.0 11,000< < 19,500 51.50 39.80 < 173.0 3,670< < 19,404 53.84 32.41 < 0.040 161.0 16,220< 1.00 < 19,685 51.60 39.51 < 0.020 161.0 4,080< 1.00 < 19,664 51.93 38.42 < 0.020 124.0 4,170< 1.00 < 19,820 52.42 36.86 < 0.020 599.0 4,030< 1.00 < 19,675 52.43 36.82 < 0.020 179.0 3,880< 1.00 < 19,765 52.46 36.72 < 0.040 148.0 3,670< 1.00 < 19,492 52.66 36.07 < 2.06 12,210< < 19,542 52.76 35.76 < 2.36 13,280< < 19,469 52.83 35.53 < 1.60 14,170< < 19,368 52.00 38.20 < 0.100 79.59 1,437< 2.50 < 19,360 52.80 35.00 < 0.100 40.97 1,189< 2.50 < 19,360 52.80 35.80 < 0.100 36.88 2,238< 2.50 < 19,357 53.00 35.20 < 0.100 69.12 1,430< 2.50 < 19,255 54.30 31.20 < 0.100 28.48 1,305< 2.50 < 19,316 53.20 34.60 < 0.100 37.94 1,800< 2.50 < 19,284 54.60 30.20 < 0.100 28.77 1,463< 2.50 < 19,285 55.30 28.20 < 0.100 24.73 1,984< 2.50 < 19,402 53.20 34.50 < 0.100 33.27 1,767< 2.50 < 19,318 66.67 1.00 < 0.020 182.0 720.0 3.80 18,998 66.67 1.00 < 0.020 1,171 410.0< 1.00

19,346 66.67 1.00 < 0.020 103.0 0.08 < 1.00 18,700 55.30 28.10 < 0.030 91.90 22,600< 1.00 < 1,870 55.60 27.40 < 0.040 55.50 21,900< 1.00 < 18,800 55.20 28.60 < 0.040 123.0 21,300< 1.00 < 19,047 52.21 37.51 < 138.0 3,590< < 19,419 50.62 42.83 < 235.0 3,410< < 19,701 52.14 37.74 < 164.0 3,760< < 18,936 53.40 34.00 0.005 < 10.00 1,500< 1.00 < 19,151 53.87 32.60 0.001 < 10.00 1,820< 1.00 < 18,893 53.91 32.50 0.001 < 10.00 1,820< 1.00 < 18,667 53.87 32.60 0.002 < 10.00 1,730< 1.00 <18,571 53.47 33.80 0.005 < 10.00 1,480< 1.00 <

18,788 53.57 33.50 0.003 < 10.00 1,480< 1.00 < 19,080 54.48 30.80 0.001 < 10.00 1,750< 1.00 < 19,170 54.07 32.00 0.002 < 10.00 1,680< 1.00 < 19,245 54.61 30.40 0.004 < 10.00 1,710< 1.00 < 19,328 52.30 37.10 < 0.038 48.00 8,000< 0.994 < 20,042 51.40 40.30 < 0.039 < 1.00 2,580< 0.991 < 18,398 52.20 37.80 < 0.039 48.00 6,390< 0.983 < 19,187 51.30 40.60 < 0.038 18.00 2,665< 0.971 < 19,504 51.20 40.70 < 0.038 < 1.00 3,700< 0.967 < 18,797 51.90 38.60 < 0.040 22.00 6,896< 0.959 < 19,300 51.29 40.55 < 0.005 31.80 5,550< 0.099 <

18,800 51.60 39.53 0.082 97.60 4,160 0.158 <

19,200 51.37 40.29 < 0.008 33.20 4,320< 0.049 < 19,277 57.50 21.78 < 230.0 2,690< < 19,300 57.44 21.96 < 196.0 2,940 0.266 < 19,733 51.41 39.92 < 285.0 4,810< < 19,085 57.46 21.92 < 136.0 2,940< < 19,648 52.23 37.48 < 87.60 5,200< < 19,697 52.32 37.22 < 196.0 5,250< <

19,865 50.52 42.59 < 314.0 2,220< <

19,693 51.02 41.10 < 163.0 2,500< <

19,359 50.92 41.39 < 269.0 2,720< <

19,969 49.98 44.19 < 168.0 960.0< <

19,732 50.74 41.92 < 215.0 4,180< <19,840 50.61 42.31 < 201.0 2,300< <

19,331 54.29 31.20 < 0.100 1.00 6,000< 1.00 < 19,374 55.80 26.80 < 0.100 1.00 30,200< 1.00 < 19,368 55.37 28.00 < 0.100 1.00 22,280< 1.00 < 19,460 53.52 33.60 < 0.100 1.00 7,800< 1.00 < 19,753 53.21 34.50 < 0.100 1.00 6,400< 1.00 < 19,444 54.69 30.00 < 0.100 1.00 2,800< 1.00 < 18,725 57.40 22.33 < 0.040 1.31 18,710< 10.0 < 18,768 57.60 21.97 < 0.020 1,170 22,830< 1.00 < 18,721 57.10 23.16 < < 21,110< < 24,574 53.38 34.00 0.100 0.25 0.26 2.50 20,095 51.75 35.50 0.100 0.25 0.26 25.0 22,329 52.57 33.10 0.100 0.25 0.29 20.0 18,888 54.20 31.50 < 0.037 21.00 15,940< 0.997 < 18,881 54.70 29.80 < 0.040 21.00 11,040< 0.989 < 18,694 58.00 20.70 < 0.040 30.00 28,820< 0.984 < 18,938 54.20 31.20 < 0.037 6.00 18,280< 0.984 < 18,609 54.60 30.00 < 0.037 15.00 20,230< 0.982 < 18,782 56.40 25.00 < 0.039 52.00 16,250< 0.982 < 18,533 57.70 21.50 < 0.039 212.0 34,630< 0.977 < 18,784 53.70 32.90 < 0.040 27.00 16,560< 0.977 < 18,772 55.90 26.40 < 0.039 38.00 17,250< 0.974 < 18,716 57.50 22.00 < 0.038 21.00 18,960< 0.969 < 18,473 57.60 21.70 < 0.039 19.00 33,720< 0.964 < 18,845 54.50 30.50 < 0.040 17.00 10,645< 0.962 < 18,382 54.87 29.63 < 0.100 18.70 22,700< 0.100 < 19,082 51.62 39.31 < 0.100 11.20 10,200< 0.100 < 18,199 54.70 30.12 < 0.020 17.90 19,300< 0.050 < 18,774 52.17 37.66 < 0.020 18.30 9,900< 0.050 < 17,982 55.14 28.82 < 0.002 13.50 18,680< 0.002 < 18,529 51.79 38.80 < 0.002 13.50 9,100< 0.002 < 20,076 52.33 37.20 < 0.100 1.00 1.03 < 1.00 < 19,950 53.47 33.80 < 0.100 1.00 1.38 < 1.00 < 19,411 54.27 31.40 < 0.100 1.00 1.32 < 1.00 < 19,825 53.84 32.70 < 0.100 1.00 1.08 < 1.00 < 19,898 53.20 34.60 < 0.100 1.00 0.92 < 1.00 < 19,609 52.90 35.50 < 0.100 1.00 0.83 < 1.00 < 20,096 50.58 42.40 < 0.100 1.00 0.15 < 1.00 < 19,900 51.12 40.80 < 0.100 1.00 0.19 < 1.00 < 19,106 50.88 41.50 < 0.100 1.00 0.24 < 1.00 < 18,386 59.09 17.80 < 0.100 76.12 24,767< 2.50 < 18,329 58.97 18.10 < 0.100 59.28 23,820< 2.50 <19,195 56.09 25.80 < 0.100 32.22 1,770< 2.50 <

19,095 56.00 26.00 < 0.100 91.70 1,790< 1.25 < 18,441 58.71 18.80 < 0.100 145.2 20,400< 1.25 <

18,405 58.99 18.00 < 0.100 156.2 24,100< 1.25 < 18,435 59.10 18.00 < 0.100 77.31 28,003< 1.25 < 18,566 59.20 17.70 < 0.100 46.28 25,582< 1.25 < 19,035 56.10 26.00 < 0.100 40.94 1,803< 1.25 < 19,602 50.89 42.00 0.014 8.60 1,570< 0.050 < 19,144 50.60 43.00 0.026 < 3.00 1,670< 0.050 < 19,358 50.80 42.30 0.019 6.40 1,540< 0.050 < 18,941 53.89 32.26 < 0.016 4.00 22,000< 1.00 < 19,355 53.51 33.43 < 0.016 2.90 20,450< 1.00 < 19,296 54.04 31.96 < 0.018 2.10 18,520< 0.990 < 19,428 53.36 33.88 < 0.017 1.70 22,270< 0.970 < 19,248 53.98 31.98 < 0.016 169.0 21,530< 0.950 < 19,449 53.07 34.78 < 0.016 784.0 17,880< 0.880 < 18,056 58.10 19.88 < 29.10 30,370 0.005 18,371 57.90 20.40 < 62.50 36,150< < 18,373 57.96 20.25 < 7.40 36,470< < 19,867 49.92 45.27 < 195.0 5,880< < 19,589 53.11 34.67 < 159.0 7,140< < 19,767 51.22 40.80 < 152.0 4,190< <

19,423 52.82 35.60 < 140.0 10,710< <

19,622 52.74 35.84 < 110.0 7,640< <

19,736 51.85 38.72 < 114.0 1,640< <

18,856 55.09 28.70 < 0.017 93.60 25,650< 0.960 < 18,572 58.03 20.57 < 0.017 103.0 26,460< 0.950 < 18,664 56.63 24.38 < 0.016 66.00 30,170< 0.930 < 19,241 54.52 30.35 < 0.016 136.0 21,950< 0.860 < 18,661 58.67 18.93 < 0.017 72.40 21,210< 0.620 < 18,890 55.28 28.14 < 0.015 47.80 17,500< 0.610 < 20,023 52.20 37.00 < 0.040 < 500.0 <500.0< 2.18 < 19,975 51.60 39.50 < 0.039 < 500.0 <500.0< 1.98 <19,967 50.70 42.10 < 0.039 < 500.0 <500.0< 1.74 <

19,615 51.30 40.50 < 293.0 442.0< < 19,714 51.80 39.00 < 82.00 450.0< < 19,704 51.80 38.90 < 89.00 475.0< < 19,788 50.78 42.28 0.020 2.67 3,650 1.00 20,086 50.39 43.63 0.020 2.85 3,090 1.00 19,176 50.44 43.47 0.040 1.10 2,590 1.00 18,570 56.82 23.90 < < 16,400< < 18,656 56.42 25.00 < < 15,200< < 18,600 56.53 24.70 < < 15,200< < 19,604 53.35 34.00 < < 1,400< < 19,664 52.81 35.70 < < 1,200< < 19,006 52.61 36.30 < < 1,600< < 19,994 55.02 29.00 < 0.100 1.00 11,900< 1.00 <

19,435 54.64 30.10 < 0.100 1.00 11,000< 1.00 < 19,627 54.39 30.90 < 0.100 1.00 9,600< 1.00 < 19,430 54.14 31.51 < 0.016 133.0 11,300< 0.950 < 19,374 54.32 30.95 < 0.017 100.0 11,650< 0.930 < 18,467 53.99 31.94 < 0.017 < 5.00 10,290< 0.600 < 19,000 54.53 30.50 < 0.016 190.0 8,900< 3.00 < 19,000 54.53 30.50 0.025 110.0 6,300< 2.80 < 19,000 54.53 30.50 < 0.016 < 30.00 8,800< 2.60 < 17,400 56.78 24.00 < 0.044 1,099 28,000< 0.990 <

17,700 57.15 23.00 < 0.039 < 350.0 14,000< 0.940 <

21,000 51.79 39.00 < 0.037 < 250.0 2,300< 0.940 < 19,705 50.70 42.60 < 0.100 69.90 689.0< 2.50 < 20,041 50.70 42.40 < 0.100 147.8 688.0< 2.50 < 19,672 50.60 42.80 < 0.100 45.69 650.0< 2.50 < 18,334 55.74 27.02 0.004 6.80 24,410 0.004 18,043 54.51 30.70 < 0.002< 1.00 23,320 0.003 18,450 54.91 29.50 0.003 < 1.00 21,390 0.004 18,688 53.16 34.50 < < 2,400< 18,466 50.92 41.90 < < 1,300< 18,341 53.83 32.60 < < 2,000< 18,396 50.89 42.20 < < 1,000< 18,737 53.58 33.30 < < 3,500< < 18,936 50.69 42.70 < < 1,200< < 19,334 51.80 38.80 < < 800.0< < 19,133 51.00 41.50 < < 700.0< < 18,379 51.40 40.40 < 13.00 600.0< < 20,090 46.55 57.90 < 0.040 < 500.0 <500.0< 2.35 < 20,004 47.10 55.70 < 0.040 < 500.0 1,500< 2.08 < 19,684 47.50 53.50 < 0.040 < 500.0 <500.0< 1.86 < 19,447 48.10 52.10 < 0.100 32.46 4,520< 1.25 <19,527 47.60 53.80 < 0.100 23.80 50.0 < 0.500 <

18,304 56.47 24.68 < 1.00 < 200.0 32,300< 5.00 < 18,346 56.62 24.34 < 1.00 < 200.0 28,300< 5.00 < 18,217 56.70 24.17 < 1.00 < 200.0 27,400< 5.00 < 18,195 51.54 39.81 < 1.00 < 200.0 2,400< 5.00 < 18,450 52.58 36.35 < 1.00 < 200.0 2,300< 5.00 < 18,708 51.39 40.22 < 1.00 < 200.0 1,800< 5.00 < 18,963 53.10 34.80 < 0.100 37.87 7,113< 2.50 < 19,090 52.96 35.20 < 0.100 138.5 6,840< 1.25 < 18,815 52.36 37.20 < 0.100 113.5 6,065< 1.25 < 19,241 51.48 40.00 < 0.100 33.43 1,805< 2.50 < 19,247 51.56 39.70 < 0.100 47.33 1,850< 1.25 < 19,476 51.42 40.20 < 0.100 71.91 1,764< 1.25 <**Arsenic,**

**ppmw Beryllium** **,**

**ppmw Cadm** **ium ,** 

**ppmw Chrom** **ium ,** 

**ppmw Cobalt,** 

**ppmw Lead,** 

**ppmw Manganese,** 

**ppmw Nickel,** 

**ppmw** 2.50< 0.990 < 0.990 < 4.00 <4.00 <0.990< 4.00 18.2 2.50< 0.980 < 0.980 < 3.90 < 3.90 <0.980< 3.90 19.6 2.40< 0.970 < 0.970 < 3.90 < 3.90 <0.970< 3.90 20.8 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.10< 0.290 < 0.360 < 0.720 <0.720<0.540< 0.720 < 2.90 0.840< 0.220 < 0.280 < 0.560 <0.560<0.420< 0.560 < 2.20 0.820< 0.220 < 0.270 < 0.540 <0.540 0.420< 0.540 < 2.20 0.810< 0.220 < 0.270 < 0.540 <0.540<0.400< 0.540 < 2.20 0.740< 0.290 < 0.370 < 0.740 <0.740<0.370< 0.740 < 2.90 0.740< 0.290 < 0.370 < 0.740 <0.740<0.370< 0.740 < 2.90 1.40< 0.380 < 0.480 < 0.960 <0.960<0.720< 0.960 < 3.80 1.10< 0.300 < 0.370 < 0.750 <0.750 1.00< 0.750 < 3.00 0.450< 0.180 < 0.230 < 0.450 <0.450 0.270< 0.450 < 1.80 0.990< 0.990 < 0.990 < 0.990 < 5.00 <0.990< 1.50 11.4 0.980< 0.490 < 0.490 < 0.980 <4.90 <0.980< 1.50 15.7 0.960< 0.480 < 0.480 < 0.960 <4.80 <0.960< 1.40 < 3.80 0.930< 0.460 < 0.460 < 0.930 <4.60 <0.930< 1.40 7.70 0.910< 0.460 < 0.460 < 0.910 <4.60 <0.910< 1.40 < 3.70 0.870< 0.430 < 0.430 < 0.870 <4.30 <0.870< 1.30 < 3.50 0.149< 0.050 < 0.050 0.451 0.357 0.160 0.356 3.02 0.105< 0.049 < 0.049 0.276 0.289 0.083 0.267 2.67 < < 0.302 0.327 0.060 0.174 2.93 0.100< 0.050 0.007 0.085 0.005 0.104 0.045 0.127

0.018< 0.050 < 0.050 0.050 <0.050 0.019 0.008 0.108

0.249< 0.050 < 0.050 0.204 <0.050 0.026 0.027 0.558 0.246< 0.050 0.006 0.377 0.160 0.141 0.150 6.53 0.085< 0.050 0.013 0.317 0.171 0.115 0.130 9.79 0.098< 0.050 < 0.050 0.328 0.206 0.129 0.086 10.7 0.097< 0.049 < 0.049 0.066 <0.049 0.052 0.011 0.104 0.044< 0.050 0.014 0.324 0.141 0.216 0.110 8.67 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.005.00< 5.00 < 2.50 < 2.50 <2.50 <5.00< 5.00 72.0

5.00< 5.00 < 2.50 < 2.50 <2.50 <5.00< 5.00 59.0 4.70< 4.70 < 2.40 < 2.40 <2.40 <4.70< 4.70 66.0 4.70< 4.70 < 2.40 < 2.40 <2.40 <4.70< 4.70 63.0 4.70< 4.70 < 2.30 < 2.30 <2.30 <4.70< 4.70 70.0 4.60< 4.60 < 2.30 < 2.30 <2.30 <4.60< 4.60 50.0 4.60< 4.60 < 2.30 < 2.30 <2.30 <4.60< 4.60 46.0 4.50< 4.50 < 2.30 < 2.30 <2.30 <4.50< 4.50 49.0 4.40< 4.40 < 2.20 < 2.20 <2.20 <4.40< 4.40 42.0 < < < < < < 87.0 < < < < < < 73.0 < < < < < < 46.0 < < < < < < 57.0 < < < < < < 57.0 < < < < < < 32.0 < < < < < < 30.0 < < < < < < 29.0 < < < < < < 25.0 0.200< 0.100 < 0.100 0.300 2.30 0.500 0.200 69.0 0.100< 0.100 < 0.100 < 0.100 0.600 0.700< 0.100 67.0 0.100< 0.100 < 0.100 0.300 2.10 0.600 0.400 58.0 0.200< 0.100 < 0.100 0.100 0.300 0.400< 0.100 58.0 0.034< 0.100 < 0.100 0.200 1.70 0.500< 0.100 45.0

< < < < < < <

< < < < < < 19.0 < < < < < < 17.0 < < < < < < 4.80 < < < 3.10 < 3.20 62.8 < < < 2.80 < 3.20 62.5 < < < 3.10 < < 61.4 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 17.5 1.21 < 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 16.9 1.39< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 16.7 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.37 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.37 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.27 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 0.602 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 0.570 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 3.91 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.80 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.44 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.36 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.321.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.58

0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 9.02 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 3.10 0.100< 0.200 < 0.200 < 0.500 <0.500<0.300< 0.500 14.1 0.100< 0.200 < 0.200 < 0.500 <0.500<0.300 5.86 <0.500 0.100< 0.200 < 0.200 < 0.500 <0.500<0.300< 0.500 <0.500 0.005< 0.0003 < 0.0004 0.140 0.064 0.040 0.110 17.0 0.005< 0.0003 0.010 0.059 0.054 0.010 0.160 11.0 0.240< 0.0003 < 0.0004 0.009 0.022 0.100 0.018 1.40 0.060< 0.050 < 0.050 < 0.050 0.090 0.060< 0.050 10.1 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 8.36 0.050< 0.050 < 0.050 < 0.050 0.060 0.090< 0.050 8.08 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 0.135< 0.002 < 0.002 0.076 0.014 0.164 0.162 1.45 0.050< 0.002 < 0.002 0.035 0.005 0.010 0.017 0.623 0.005< 0.002 < 0.002 0.008 <0.002<0.002 0.005 0.203

< < < < < < 10.2 < < < < < < 9.88 < < < < < < 8.96 < < < < < < 7.90 < < < < < < 5.04 < < < < < < < < < < < < < < < < < < < < 7.50 < < < < < < 5.72 < < < < < < 2.67 < < < < < < < < < < < < < < < < < < < < < < < < < < < 13.1 < < < < < < 25.0 < < < < < < 13.7 0.050< 0.050 < 0.050 < 0.050 <0.050 0.090< 0.050 11.0 0.210< 0.050 < 0.050 < 0.050 0.130 0.130< 0.050 8.62 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 7.88 0.120< 0.050 < 0.050 < 0.050 0.100 0.440< 0.050 5.44 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 5.66 0.130< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 5.60

< < < < < < <

< < < < < < << < < < < < <

< < < < < < 17.2

< < < < < < 9.89

< < < < < < 4.50

< < < < < < 3.28

< < < < < < 3.06

< < < < < < 2.93

< < < < < < 2.22

< < < < < < 2.11

< < < < < < 1.09

< < < < < < <

< < < < < < <

< < < < < < < 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 6.16 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 2.67 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 2.00 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 1.78 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 1.63 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 1.48 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 1.45 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 1.03 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 <0.500 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 <0.500 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 <0.500 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 <0.500 1.00< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 9.68 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 6.28 1.00< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 4.64 1.00< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 2.28 1.00< 0.500 < 0.500 < 0.500 <0.500<1.00< 0.500 <0.500 1.00< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500 0.050< 0.050 < 0.050 < 0.050 0.200<0.050< 0.050 15.7 0.050< 0.050 < 0.050 0.070 0.230<0.050 1.06 20.4 0.050< 0.050 < 0.050 < 0.050 0.180<0.050< 0.050 11.7 0.050< 0.050 < 0.050 0.060 0.220<0.050 0.160 22.9 0.050< 0.050 < 0.050 < 0.050 0.190<0.050< 0.050 16.4 0.050< 0.050 < 0.050 < 0.050 0.120<0.050< 0.050 14.2 0.990< 0.500 < 0.500 < 0.990 < 5.00 <0.990< 1.50 < 4.00 0.980< 0.490 < 0.490 < 0.980 <4.90 <0.980< 1.50 8.10 0.910< 0.450 < 0.450 < 0.930 <4.50 <0.930< 1.40 < 3.70 0.920< 0.460 < 0.460 < 0.920 <4.60 <0.920< 1.40 < 3.70 0.920< 0.460 < 0.460 < 0.920 <4.60 <0.920< 1.40 < 3.700.910< 0.460 < 0.460 < 0.870 <4.60 <0.870< 1.40 < 3.50

1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.65 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.26 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 3.07 0.540< 0.050 < 0.270 < 0.540 <0.540<0.540< 0.540 6.40 0.530< 0.050 < 0.270 < 0.530 <0.530<0.530< 0.530 5.54 0.530< 0.050 < 0.260 < 0.530 <0.530<0.530< 0.530 3.73 0.760< 0.080 < 0.380 < 0.760 <0.760<0.760< 0.760 4.75 0.520< 0.050 < 0.260 < 0.520 <0.520<0.520< 0.520 3.59 0.510< 0.050 < 0.250 < 0.510 <0.510<0.510< 0.510 3.67 5.00< 2.50 < 2.50 < 2.50 <2.50 <2.50< 2.50 < 2.50 2.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.11 2.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.49 0.050< 0.050 < 0.050 0.203 <0.050 0.326 0.288 0.658 0.050< 0.050 < 0.050 0.157 <0.050 0.199< 0.050 0.587 0.010< 0.010 0.027 0.090 <0.010 0.870 0.191 0.136 2.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 2.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 2.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 0.100< 0.100 < 0.100 0.100 0.100 0.200 0.100 7.70 0.100< 0.100 < 0.100 < 0.100 <0.100<0.100 0.100 2.80 0.200< 0.100 < 0.100 0.200 <0.100 0.800 0.500 2.20 0.100< 0.100 < 0.100 0.100 <0.100 0.400 0.200 1.40 0.100< 0.100 < 0.100 0.200 0.100 0.300 0.200 1.40 0.100< 0.100 < 0.100 0.100 <0.100 0.700 0.100 1.00 0.050< 0.050 < 0.050 0.080 0.090<0.050< 0.050 20.2 0.060< 0.050 < 0.050 0.130 0.060 0.050< 0.050 25.6 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 15.8 1.00< 1.00 < 1.00 < 1.00 < 1.00 6.94< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 2.48 < 0.992 < 0.992 < 3.97 < 3.97 <0.992< 3.97 1.58 2.45 < 0.982 < 0.982 < 3.93 < 3.93 <0.982< 3.93 1.43 2.45 < 0.978 < 0.978 < 3.91 < 3.91 <0.978< 3.91 47.0 2.44< 0.978 < 0.978 < 3.91 < 3.91 <0.978< 3.91 2.95 2.44< 0.977 < 0.977 < 3.91 < 3.91 <0.977< 3.91 35.9 2.46< 0.982 < 0.982 2.03 < 3.93 <0.982< 3.93 <0.982 0.099< 0.050 < 0.050 0.168 0.135<0.050 0.307 3.37 0.099< 0.049 < 0.049 0.231 0.152<0.049 0.147 5.36 0.117< 0.049 < 0.049 0.248 0.172<0.049 0.414 4.14 0.246< 0.049 < 0.049 0.326 0.141 0.144 0.278 3.38 0.098< 0.049 < 0.049 0.196 0.133 0.108 0.239 3.32 0.246< 0.049 < 0.049 0.333 0.143<0.049 0.102 5.23 0.970< 0.490 < 0.490 < 0.970 <4.90 <0.970< 1.50 < 3.90 0.940< 0.470 < 0.470 1.20 <4.70 <0.940< 1.40 10.4 0.890< 0.440 < 0.440 < 0.890 <4.40 <0.890< 1.30 < 3.50< < 2.26 < < < 33.9 < < < < < < 21.8 < < < < < < 36.2 < < < < < < 27.4 < < < < < < 27.2 < < < < < < 18.0 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 10.0 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 9.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 8.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 8.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 8.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 8.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 8.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 7.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 7.00 < < < < < < 8.00 < < < < < < 8.00 < < < < < < 7.00 2.10< 0.210 < 0.520 < 1.00 < 5.20 <2.10< 1.50 < 4.10 2.10< 0.210 < 0.520 < 1.00 < 5.20 <2.10< 1.50 < 4.10 1.90< 0.190 < 0.490 < 0.970 <4.90 <1.90< 1.50 < 3.90 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 5.07 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 10.7 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 5.42 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 3.26 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 3.06 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 5.62 2.490 0.997 0.997 3.99 3.99 0.997 3.99 1.00 2.410 0.966 0.966 3.86 3.86 0.966 3.86 0.966 2.410 0.963 0.963 3.85 3.85 0.963 3.85 1.00 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 7.35 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 4.91 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 4.89 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 3.60 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 3.53 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 3.43 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 2.84 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 2.77 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.71 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.49 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.43 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.32 1.34< 1.07 < 0.456 < 5.36 <0.724<3.49 < 2.15 14.8 1.30< 1.04 < 0.442 < 5.20 <0.702<26.0< 2.08 14.8 1.20< 0.958 < 0.407 < 4.79 <0.647<23.9 < 1.92 11.4 1.18 < 0.941 < 0.400 < 4.70 <0.635<23.5 < 1.88 11.2 1.12< 0.894 < 0.380 < 4.47 <0.603<22.3 < 1.79 16.5 1.11 < 0.890 < 0.378 < 4.45 <0.601<2.89 < 1.78 10.8 0.914< 0.731 < 0.311 < 3.65 <0.493<18.3 < 1.46 11.2 0.842< 0.674 < 0.286 < 3.37 <0.455<16.8 < 1.35 12.9 0.718< 0.574 < 0.244 < 2.87 <0.388<1.87 < 1.15 16.1 1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 1.26 1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.001.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00

1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00 0.050< 0.050 < 0.050 < 0.050 0.080 0.290< 0.050 17.5 0.050< 0.050 < 0.050 0.070 0.140<0.050< 0.050 19.4 0.050< 0.050 < 0.050 < 0.050 <0.050 0.230 0.050 5.32 0.006< 0.002 < 0.002 0.044 0.035 0.004 0.008 1.36 0.012< 0.002 0.004 0.121 0.046 0.015 0.012 1.85 0.003< 0.002 < 0.002 0.007 0.016 0.007 0.005 0.958 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 0.900 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 0.880 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 0.630 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 0.402 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 0.728 < < < < < < 3.10 < < < < < < 5.30 < < < < < < 3.80 < < < < < < 1.60 < < < < < < 6.40 < < < < < < 2.90 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00 0.826 7.85 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.76 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.66 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 3.63 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 2.23 1.00< 0.200 < 0.200 < 0.500 < 1.00 <1.00< 0.500 1.99 < < < < < < 4.47 < < < < < < 3.24 < < < < < < 1.95 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 3.79 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.25 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.88 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 3.52 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.47 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.46 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.27 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.52 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.36 2.65 < 0.500 < 0.500 4.41 <2.00 <2.00< 2.00 7.27 2.91 < 0.500 < 0.500 4.33 <2.00 <2.00 2.23 < 2.00

2.53 < 0.500 < 0.500 3.52 <2.00 <2.00< 2.00 < 2.00 5.00< 5.00 < 1.00 < 1.00 < 5.00 <1.00< 1.00 32.0 5.00< 5.00 < 1.00 < 1.00 < 5.00 <1.00< 1.00 32.0 5.00< 5.00 < 1.00 < 1.00 < 5.00 <1.00< 1.00 32.0 < < < < < < 1.39 < < 0.268 < < < 1.26 < < < < < < 1.04 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 5.80 0.500< 1.00 < 0.500 < 0.500 < 1.00 <0.500< 0.500 5.44 0.500< 1.00 < 0.500 < 0.500 < 1.00 <0.500< 0.500 5.35 0.500< 1.00 < 0.500 < 0.500 < 1.00 <0.500< 0.500 5.121.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 5.11

1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 5.06 1.00< 1.00 < 1.00 < 1.00 < 1.00 1.94< 1.00 4.55 1.00< 1.00 < 1.00 < 1.00 < 1.00 1.15 < 1.00 4.43 1.00< 1.00 < 1.00 < 1.00 < 1.00 2.39 < 1.00 4.33 2.48 < 0.994 < 0.994 < 3.97 < 3.97 <0.994< 3.97 3.00 2.48 < 0.991 < 0.991 < 3.97 < 3.97 <0.991< 3.97 1.43 2.46< 0.983 < 0.983 < 3.93 < 3.93 <0.983< 3.93 2.43 2.43 < 0.971 < 0.971 < 3.88 < 3.88 <0.971< 3.88 1.23 2.42< 0.967 < 0.967 < 3.87 < 3.87 <0.967< 3.87 1.58 2.40< 0.959 < 0.959 < 3.83 < 3.83 <0.959< 3.83 3.44 0.198< 0.099 0.223 0.320 0.449 3.12 1.42 2.61

0.099< 0.050 < 0.050 0.234 <0.050 0.051 0.081 1.88

0.098< 0.049 < 0.049 0.275 <0.049 0.095 0.062 1.93

< < < < < < 2.04 < 0.013 0.160 0.112< 0.290 2.46 < < < < < 0.068 3.09 < < < < < < 1.88

< < < < < < 1.51

< < < < < < 1.01

< < < < < < 1.51

< < < < < < 1.09

< < < < < < 1.06

< 0.174 < < < < 0.907

< < < < 0.228< 0.334< < < < < < <

1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 1.05 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 10.0< 2.00 < 2.00 < 5.00 < 10.0 <10.0< 5.00 35.0 1.00< 0.200 < 0.200 < 0.500 < 1.00 18.2< 0.500 9.46 < < < < < < 40.2 2.50 2.50 2.50 2.50 2.50 2.50 2.50 7.59 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.50 2.49< 0.997 < 0.997 < 3.99 < 3.99 <0.997< 3.99 10.6 2.47 < 0.989 < 0.989 < 3.95 < 3.95 <0.989< 3.95 11.7 2.46< 0.984 < 0.984 < 3.94 < 3.94 <0.984< 3.94 51.6 2.46< 0.984 < 0.984 < 3.94 < 3.94 <0.984< 3.94 12.0 2.45 < 0.982 < 0.982 < 3.93 < 3.93 <0.982< 3.93 15.1 2.45 < 0.982 < 0.982 < 3.93 < 3.93 <0.982< 3.93 12.7 2.44< 0.977 < 0.977 < 3.91 < 3.91 <0.977< 3.91 54.2 2.44< 0.977 < 0.977 < 3.91 < 3.91 <0.977< 3.91 9.97 2.43 < 0.974 < 0.974 < 3.89 < 3.89 <0.974< 3.89 15.0 2.42< 0.969 < 0.969 < 3.88 < 3.88 <0.969< 3.88 36.8 2.41 < 0.964 < 0.964 < 3.86 < 3.86 <0.964< 3.86 54.7 2.41 < 0.962 < 0.962 < 3.85 < 3.85 <0.962< 3.85 10.7 0.100< 0.100 < 0.100 < 0.100 <0.020<0.100< 0.100 3.02 0.100< 0.100 < 0.100 < 0.100 <0.100<0.100< 0.100 1.07 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 4.18 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 1.06 0.002< 0.002 < 0.003 < 0.004 <0.002<0.003< 0.002 0.203 0.002< 0.002 < 0.002 < 0.006 <0.002<0.003< 0.002 0.039 1.00< 1.00 < 1.00 1.28 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 1.12 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 1.02 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 2.00< 1.00 < 1.00 < 2.00 < 1.00 <1.00< 2.00 1.77 2.00< 1.00 < 1.00 < 2.00 < 1.00 <1.00< 2.00 1.652.00< 1.00 < 1.00 < 2.00 < 1.00 <1.00< 2.00 1.61

0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 1.61 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 17.3

0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 8.72 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500 0.730 2.72 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500 0.050< 0.050 < 0.050 < 0.050 <0.050<0.050< 0.050 1.76 0.050< 0.050 < 0.050 < 0.050 0.070 0.090 0.060 2.34 0.050< 0.050 < 0.050 < 0.050 0.070<0.050< 0.050 2.25 1.00< 0.500 < 0.500 < 1.00 < 5.00 <1.00< 1.50 5.30 1.00< 0.510 < 0.510 < 1.00 < 5.10 <1.00< 1.50 < 4.00 0.990< 0.500 < 0.500 < 0.990 < 5.00 <0.990< 1.50 < 4.00 0.970< 0.480 < 0.480 < 0.970 <4.80 <0.970< 1.50 < 3.90 0.950< 0.480 < 0.480 < 0.950 <4.80 <0.950< 1.40 < 3.80 0.880< 0.440 < 0.440 < 0.880 <4.40 <0.880< 1.30 < 3.50 0.007< < 0.023 0.007< 0.006 1.19

0.052 < < < < < 1.94 < < < < < < 1.06 < < < < < 0.114 1.65 < < < < < < 1.60 < < < < < < <

< < < < < < <

< < < < < < <

< < < < < < <

0.960< 0.480 < 0.480 < 0.960 <4.80 <0.960< 1.40 < 3.80 0.950< 0.480 < 0.480 < 0.950 <4.80 <0.950< 1.40 < 3.80 0.930< 0.460 < 0.460 < 0.930 <4.60 <0.930< 1.40 < 3.60 0.860< 0.430 < 0.430 < 0.860 <4.30 <0.860< 1.30 < 3.40 0.620< 0.310 < 0.310 < 0.620 < 3.10 <0.620< 0.940 3.90 0.610< 0.300 < 0.300 < 0.610 < 3.00 <0.610< 0.910 7.70 1.36< 1.09 < 0.464 < 5.46 <0.737<3.55 < 2.18 < 10.9 1.24< 0.990 < 0.421 < 4.95 <0.668<24.8 < 1.98 < 9.901.09< 0.870 < 0.370 < 4.68 <0.587<23.4< 1.74 < 8.70 < < < < < < 4.32 < < < < < < 2.97 < < < < < < 2.91 1.00 0.200 0.200 0.500 1.00 1.00 0.500 2.05 1.00 0.200 0.200 0.500 1.00 1.00 0.500 2.03 1.00 0.200 0.200 0.500 1.00 1.00 0.500 1.27 < < < < < < 40.5 < < < < < < 31.3 < < < < < < 14.8 < < < < < < 14.6 < < < < < < 13.9 < < < < < < 12.8

1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00

1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 < 1.00< 1.00 < 1.00 0.950< 0.480 < 0.480 < 0.950 <4.80 <0.950< 1.40 < 3.80 0.930< 0.470 < 0.470 < 0.930 <4.70 <0.930< 1.40 < 3.70 0.600< 0.300 < 0.300 < 0.600 < 3.00 <0.600< 0.900 2.50 3.00< 0.250 < 0.490 < 1.30 <0.490<1.50< 0.980 4.40 2.80< 0.240 < 0.470 < 1.20 <0.470<1.40< 0.940 9.40 2.60< 0.220 < 0.430 < 1.10 <0.430<1.30< 0.860 5.10 0.500< 0.050 < 0.099 < 0.150 <0.150 0.730 0.110 9.10

0.470< 0.047 < 0.094 0.140 <0.140<0.350< 0.094 8.00

0.470< 0.047 < 0.190 0.370 <0.190<0.350< 0.180 0.740 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 0.013< 0.002 0.002 0.048 0.016 0.005 0.019 3.01 0.008< 0.002 < 0.002 0.008 0.012 0.073 0.003 2.33 0.005< 0.002 < 0.002 0.028 0.011 0.077 0.034 1.80 0.600< < < < < < < 0.600< < < < < < < 0.050< < < < < < < 0.050< < < < < < < < < < < < < < < < < < < < < < < 0.600 < < < 2.00 < < 3.30 < < < 0.600 < < < < < < 0.700 1.47 < 1.18 < 0.499 < 5.88 <0.793<29.4< 2.35 < 11.8 1.30< 1.04 < 0.441 < 5.19 <0.701<26.0< 2.08 < 10.4 1.16< 0.931 < 0.396 < 4.66 <0.628<23.3 < 1.86 < 9.31 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.5000.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500

5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 14.0 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 13.0 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 12.0 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 < 5.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 < 5.00 5.00< 5.00 < 1.00 < 5.00 < 5.00 <5.00< 5.00 < 5.00 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 2.45 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 5.47 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 1.99 1.00< 1.00 < 1.00 < 1.00 < 1.00 <1.00< 1.00 < 1.00 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500 0.500< 0.500 < 0.500 < 0.500 <0.500<0.500< 0.500 <0.500**Selenium ,** 

**ppmw If the crude oil or interm** **ediate slate being fed to the distillation colum n during the tim** **e of this**

**sam ple is significantly different than the crude oil or interm** **ediate slate used during 2010, briefly explain**  < 0.990 < 0.980 < 0.970 < 1.00 < 1.00

< 1.00 Crude 3 has not operated in 2011. However, the Crude 1, Crude 2, and Crude 3 units all process crude oil from the same source. < 1.10 < 0.840 < 0.820 < 0.810 < 0.740 < 0.740 < 1.40 < 1.10 < 0.450 < 0.990 Ty pical feed < 0.980 Ty pical feed < 0.960 Ty pical feed < 0.930 Ty pical feed < 0.910 Ty pical feed < 0.870 Ty pical feed < 0.248 < 0.247 <

< 0.250

< 0.250

< 0.249

< 0.246 0.204 < 0.098

< 0.097 0.072 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 Method 200.8 was used for analyzing metals for all samples. < 1.00 < 1.00 < 1.00 < 1.00< 10.0

< 9.90 < 9.40 < 9.40 < 9.30 < 9.30 < 9.20 < 9.10 < 8.80 < < < < < < < < <

< 0.100

< 0.100

< 0.100

< 0.100

< 0.100

< Crude Unit No. 2 was during the month of June

< < < < < < < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00

< 1.00 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.

< 1.00 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.

< 1.00 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.

< 1.00 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.

< 1.00 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.< 1.00 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.

< 0.500 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column.

< 0.500 The Delaware City Refinery was idled for all of the year 2010. No crude was fed to the distillation column. < 0.500 < 0.500 < 0.500 0.570 N / A 0.360 N / A 0.210 N / A 0.130 0.120 0.110 < 1.00 < 1.00 Method 200.8 was used for analyzing metals for all samples. < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 0.063 0.037 0.004 This sample was taken during refining of approximately 60% Illinois Basin crude and 40% Marcellus

crude, by volume. The crude oil refined during 2010 was 98.64 % Illinois Basin crude and 1.36 % Marcellus crude, by volume. < < < < < < < < < < < < < 0.692 < < 0.140 0.080 0.080 na 0.080 0.060 < 0.050

< While Calcasieu Refining Company runs a variety of crudes, in general the crude slate at the time of these tests was not significatly different from 2010.

< While Calcasieu Refining Company runs a variety of crudes, in general the crude slate at the time of these tests was not significatly different from 2010.< While Calcasieu Refining Company runs a variety of crudes, in general the crude slate at the time of these tests was not significatly different from 2010.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 21.8 aBDL 1.7 respectively for CV-1 Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 28.5 aBDL 1.5 respectively for C-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 39.9 aBDL 0.2 respectively for A-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 28.2 aBDL 1.5 respectively for B-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 28.5 aBDL 1.5 respectively for C-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 21.8 aBDL 1.7 respectively for CV-1 Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 28.2 aBDL 1.5 respectively for B-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 28.5 aBDL 1.5 respectively for C-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 28.2 aBDL 1.5 respectively for B-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 21.8 aBDL 1.7 respectively for CV-1 Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 39.9 aBDL 0.2 respectively for A-Topper.

< CITGO LCMC ran 43 different crudes in 2010. The 2010 average API gravity aBDL Sulfur wt % was 39.9 aBDL 0.2 respectively for A-Topper. < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 0.140 0.130 0.130 0.100 0.090 0.080 < 0.990 Normal base crude slate < 0.980 Normal base crude slate < 0.930 Normal base crude slate < 0.920 Normal base crude slate < 0.920 Normal base crude slate< 0.870 Normal base crude slate

< 1.00 < 1.00 < 0.500 < 1.07 < 1.06 < 1.05 < 1.52 < 1.04 < 1.02

< 5.00 Our refinery processes crude oil from multiple suppliers, and is constantly altering the composition of unit feed.

< 1.00 Our refinery processes crude oil from multiple suppliers, and is constantly altering the composition of unit feed.

< 1.00 Our refinery processes crude oil from multiple suppliers, and is constantly altering the composition of unit feed. < 0.250 Ty pical crude slate < 0.250 Ty pical crude slate < 0.050 Ty pical crude slate < 2.00 Ty pical crude slate < 2.00 Ty pical crude slate < 2.00 Ty pical crude slate < 0.100 N/A < 0.100 N/A < 0.100 N/A < 0.100 N/A < 0.100 N/A < 0.100 N/A 0.150 0.140 0.140 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 0.992 < 0.982 < 0.978 < 0.978 < 0.977 0.577 < 0.249 Not processed in 2010 < 0.247 Not processed in 2010 < 0.246 N/A < 0.246 N/A < 0.244 N/A < 0.025 Not processed in 2010 < 0.970 Ty pical feed < 0.940 Ty pical feed < 0.890 Ty pical feed0.647

0.584 < < < < < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < < < < 2.10 < 2.10 < 1.90 1.17 < 1.00 < 1.00 < 1.00 < 1.00 < 0.500 0.997 0.966 0.963 < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 1.00 N/A < 4.56 < 4.42 < 4.07 < 4.00 < 3.80 < 3.78 < 3.11 < 2.86 < 2.44 < 1.00 Method 200.8 was used for analyzing metals for all samples. < 1.00 Method 200.8 was used for analyzing metals for all samples. < 1.00 Method 200.8 was used for analyzing metals for all samples. < 1.00 Method 200.8 was used for analyzing metals for all samples.< 1.00 Method 200.8 was used for analyzing metals for all samples.

< 1.00 Method 200.8 was used for analyzing metals for all samples. 0.160 0.140 0.080 0.029 0.029 0.014 < 0.500 < 0.500 < 0.500 < 0.500 0.405 0.367 0.800 0.600 0.500 0.500 < < < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < < < < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00 < 1.00

< 1.00

< 1.00

< 1.00

< 1.00 < 1.00 < 1.00 < < < < 1.00 < 1.00 < 1.00 < 1.00< 1.00

< 1.00 < 1.00 < 1.00 < 1.00

< 0.994 A blending test was being run resulting in a higher percentage of sour crude in the feed. Samples from June and August are more representative of 2010 crude slate. < 0.991 < 0.983 < 0.971

< 0.967 A blending test was being run resulting in a higher percentage of sour crude in the feed. Samples from June and August are more representative of 2010 crude slate. < 0.959

< 0.496 NA - Data for Sulfur content and API Gravity during recent sampling is very similar to data for 2010

< 0.248 NA - Data for Sulfur content and API Gravity during recent sampling is very similar to data for 2010

< 0.245 NA - Data for Sulfur content and API Gravity during recent sampling is very similar to data for 2010 1.31 0.800 0.441 05/12/11 sample is Tk 338 only <

< 06/14/2011 sample is a composite of Tk 338 and Tk339 that was put into service following the first round of sampling

< 07/14/2011 sample is a composite of Tk 338 and Tk339 that was put into service following the first round of sampling

< J=the raw calculated analyte conc in the sample (uncorrected for background levels/blanks and other potential sources of sampling and analytical contamination), though less than the reported quantitation limit is greater than the detection limit. Because the reported result is below the quantitation limit for this project/sample (or test procedure), GC/MS organics results may or MAY NOT have been verified as to the presence and relatvie ration or target ions.

< J=the raw calculated analyte conc in the sample (uncorrected for background levels/blanks and other potential sources of sampling and analytical contamination), though less than the reported quantitation limit is greater than the detection limit. Because the reported result is below the quantitation limit for this project/sample (or test procedure), GC/MS organics results may or MAY NOT have been verified as to the presence and relatvie ration or target ions.

< J=the raw calculated analyte conc in the sample (uncorrected for background levels/blanks and other potential sources of sampling and analytical contamination), though less than the reported quantitation limit is greater than the detection limit. Because the reported result is below the quantitation limit for this project/sample (or test procedure), GC/MS organics results may or MAY NOT have been verified as to the presence and relatvie ration or target ions.

< J=the raw calculated analyte conc in the sample (uncorrected for background levels/blanks and other potential sources of sampling and analytical contamination), though less than the reported quantitation limit is greater than the detection limit. Because the reported result is below the quantitation limit for this project/sample (or test procedure), GC/MS organics results may or MAY NOT have been verified as to the presence and relatvie ration or target ions.

< J=the raw calculated analyte conc in the sample (uncorrected for background levels/blanks and other potential sources of sampling and analytical contamination), though less than the reported quantitation limit is greater than the detection limit. Because the reported result is below the quantitation limit for this project/sample (or test procedure), GC/MS organics results may or MAY NOT have been verified as to the presence and relatvie ration or target ions.< J=the raw calculated analyte conc in the sample (uncorrected for background levels/blanks and other potential sources of sampling and analytical contamination), though less than the reported quantitation limit is greater than the detection limit. Because the reported result is below the quantitation limit for this project/sample (or test procedure), GC/MS organics results may or MAY NOT have been verified as to the presence and relatvie ration or target ions. < 1.00 < 1.00 < 1.00 < 1.00 Method 200.8 was used for analyzing metals for all samples. < 1.00 < 1.00 < 10.0 < 1.00 < 2.50 No different from the 2010 feed 2.50 No different from the 2010 feed 2.50 No different from the 2010 feed < 0.997 < 0.989 < 0.984 < 0.984 < 0.982 < 0.982 < 0.977 < 0.977 < 0.974 < 0.969 < 0.964 < 0.962 < 0.100 N/A < 0.100 N/A < 0.050 N/A < 0.050 N/A < 0.002 N/A < 0.002 N/A

< 1.00

< 1.00

< 1.00

< 1.00

< 1.00

< 1.00

< 1.00

< 1.00

< 1.00

< 2.00 < 2.00< 2.00 Not significantly different

0.700 Not significantly different 0.560 Crude slate is variable based on spot purchases of various crudes, availability, and refining margins. The

mix of crudes run during the sampling was significantly different than the average slate run in 2010.

< 0.500 Crude slate is variable based on spot purchases of various crudes, availability, and refining margins. The

mix of crudes run during the sampling was significantly different than the average slate run in 2010.

< 0.500 < 0.500 < 0.500 Not significantly different 0.080 0.050 < 0.050

< 1.00

< 1.00

< 0.990

< 0.970

< 0.950

< 0.880 0.011 no signifigant difference < no signifigant difference < no signifigant difference 0.447 No difference < No difference < No difference

< Not Applicable

< Not Applicable

< Not Applicable

< 0.960 < 0.950 < 0.930 < 0.860 < 0.620 < 0.610 < 4.64 < 4.21< 3.70

< LOQ = Limit of Quantitation (i.e. reporting or practical quantitation limit) < LOQ = Limit of Quantitation (i.e. reporting or practical quantitation limit) < LOQ = Limit of Quantitation (i.e. reporting or practical quantitation limit) 1.00 1.00 1.00 < N/A < N/A < N/A < N/A < N/A < N/A

< 1.00 Cherry Point’s first Component 3 crude oil sample was delayed until June 2 due to a crude distillation

process turnaround in May 2011 w hich compressed the sampling schedule for the second and third crude samples. The third sample was inside the 30-day sampling period in order to obtain the analytical results in time to report the results by August 31, 2011.

< 1.00 Method 200.8 was used for analyzing metals for all samples.

< 1.00

< 0.950 not significantly different < 0.930 not significantly different < 0.600 not significantly different < 4.90 < 4.70 < 4.30

< 1.50 The variability in the data across the three samples is largely due to the diverse crude slate run at the

Suerpior, Wisconsin refinery. However, that diverse crude slate is representative of the slate run throughout 2010 and prior years.

< 1.40 The variability in the data across the three samples is largely due to the diverse crude slate run at the

Suerpior, Wisconsin refinery. However, that diverse crude slate is representative of the slate run throughout 2010 and prior years.

< 1.40 The variability in the data across the three samples is largely due to the diverse crude slate run at the

Suerpior, Wisconsin refinery. However, that diverse crude slate is representative of the slate run throughout 2010 and prior years. < 1.00 N/A < 1.00 N/A < 1.00 N/A 0.024 0.011 0.011 < < < < < < 0.700 0.600 0.500 < 4.99 U-Crude < 4.41 Condensate < 3.96 U-Crude 0.650 Condensate< 0.500 U-Crude

< 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 5.00 < 1.00 0.670 < 0.500

< 1.00

< 0.500

< 0.500**ICR_ID Indicate if the sam** **ple was collected before or**  **after the desalter Avg** 

**Higher Heating**  **Value (Btu/lb)** **Avg**

**Density (lb/ft** **3 )** **Avg API**

**Gravity Total** 

**Entries Count**  **Count for**

**Mercury Detection Lim** **it Determ** **ination DL for** 

**Mercury Avg** 

**Mercury, ppmw**  AK5A0050 N/A 18,855 56.84 23.80 3 3 BDL 0.020 AK5A0090 After 19,715 52.03 38.47 3 3 BDL 0.050 AL3C0030 After 18,167 51.24 40.88 6 6 BDL 0.007 AL3D0010 After 19,00049.76 45.93 3 3 BDL 0.007 AL3D0020 After 18,578 57.62 21.78 6 6 BDL 0.008 AR3D0100 Before 19,233 56.91 23.85 3 3 BDL 0.004 AR3DO110 Before 18,25049.40 48.54 8 6 DLL 0.005 CA5A0120 Before 19,194 54.44 30.76 9 9 BDL 0.050 CA5A0190 Before 17,779 59.97 15.83 9 9 BDL 0.045 CA5A0200 N/A 20,922 61.03 13.00 3 3 BDL #DIV/0! CA5A0210 Before 16,829 58.69 18.93 3 3 BDL #DIV/0! CA5A0220 N/A 19,137 54.47 30.70 3 3 BDL #DIV/0! CA5A0230 Before 18,343 56.94 23.56 6 6 BDL 0.005 CA5A0310 Before 16,629 56.80 23.97 3 3 BDL #DIV/0! CA5A0330 N/A 16,883 58.25 19.83 3 3 BDL #DIV/0! CO4A0340 Before 18,714 52.61 36.36 9 0 ADL 0.005 DE1A0360 Before 18,924 55.41 27.83 8 8 BDL 0.050 IL2A0400 Before 17,821 55.62 27.23 3 3 BDL 0.025 IL2A0410 After 18,300 57.02 23.33 3 0 ADL 0.007 IL2A0420 After 19,161 52.82 35.60 3 0 ADL 0.002 IN2A0440 After 19,421 54.03 32.04 9 9 BDL 0.050 IN2A0450 Before 18,790 53.10 34.08 3 2 DLL 0.002 KS2C0460 Before 18,829 53.13 34.67 7 7 BDL #DIV/0! KS2C0470 After 19,385 53.99 31.58 6 6 BDL #DIV/0! KS2C0480 After 18,919 54.79 29.63 3 3 BDL #DIV/0! KY2A0490 After 19,125 53.25 34.30 6 1 DLL 0.003 LA3C0520 Before 17,899 50.96 40.40 3 3 BDL #DIV/0! LA3C0560 After 17,439 54.75 30.00 12 12 BDL #DIV/0! LA3C0590 After 17,220 54.87 29.38 12 12 BDL 0.050 LA3C0600 After 16,778 57.22 22.92 6 6 BDL 0.050 LA3C0610 After 18,887 54.73 29.83 6 6 BDL 0.001 LA3C0620 After 18,910 54.85 29.34 6 6 BDL 0.008 LA3C0630 After 19,256 53.85 32.40 3 3 BDL 0.117 LA3C0640 After 18,971 53.99 31.87 3 3 BDL 0.050 LA3C0670 After 18,918 53.63 32.88 3 3 BDL 0.050 LA3C0700 Before 17,628 52.45 36.77 3 3 BDL 0.050 LA3D0530 Before 19,567 51.15 50.83 3 0 ADL 0.068 LA3D0540 Before 17,271 57.66 21.60 3 3 BDL 0.050 LA3D0660 Before 18,699 52.10 37.93 6 5 DLL 0.009 MI2A0710 After 18,685 53.43 33.77 3 3 BDL 0.001 MN2B0720 After 19,576 56.36 25.37 9 9 BDL 0.050 MN2B0730 After 18,927 54.52 30.82 6 6 BDL 0.019 MS3D0750 N/A 19,200 57.18 21.30 6 6 BDL 0.003 MS3D0760 After 18,487 59.08 17.89 3 3 BDL 0.008 MT4A0770 Before 19,417 56.92 23.52 6 6 BDL 0.020 MT4A0790 N/A 18,172 56.12 25.83 9 9 BDL 0.500 MT4A0800 After 18,185 56.31 25.30 3 3 BDL #DIV/0! NJ1A0820 N/A 19,133 56.42 25.07 3 3 BDL 0.016NJ1A0860 After 18,986 54.27 31.07 6 6 BDL 0.050

NM3E0880 After 19,547 50.59 43.03 3 0 ADL 0.039 NM3E0890 After 19,201 53.30 34.07 6 6 BDL 0.018 NM3E0891 After 19,338 52.83 35.53 6 6 BDL 0.017 NV5A0810 N/A 18,737 7.59 24.03 9 8 DLL 0.041 OH2A0910 Before 19,195 54.47 30.68 6 6 BDL 0.050 OH2A0920 After 19,025 52.97 35.23 3 0 ADL 0.005 OH2A0930 After 18,401 51.98 37.87 3 2 DLL 0.002 OH2A0940 After 19,452 52.21 37.58 6 6 BDL 0.050 OK2C0960 Before 19,400 52.02 38.33 6 6 BDL #DIV/0! OK2C0970 After 19,584 52.46 36.78 3 3 BDL 0.013 OK2C0980 After 19,753 52.43 36.80 3 3 BDL 0.013 OK2C0990 Before 19,501 52.75 35.79 3 3 BDL #DIV/0! PA1A1020 Before 19,363 52.53 36.33 3 3 BDL 0.050 PA1A1030 After 19,317 53.93 32.32 6 6 BDL 0.050 PA1B1010 Before 19,221 66.67 1.00 3 3 BDL 0.010 PA1B1050 After 13,123 55.37 28.03 3 3 BDL 0.018 TN2A1060 Before 19,389 51.66 39.36 3 3 BDL #DIV/0! TX3A1080 After 18,945 53.92 32.47 9 0 ADL 0.003 TX3A1120 After 19,209 51.72 39.18 6 6 BDL 0.019 TX3A1190 After 19,100 51.42 40.12 3 2 DLL 0.032 TX3A1290 Before 19,457 54.73 30.05 6 6 BDL #DIV/0! TX3A1300 Before 19,743 50.63 42.25 6 6 BDL #DIV/0! TX3B1110 Before 19,455 54.48 30.68 6 6 BDL 0.050 TX3B1130 Before 18,738 57.37 22.49 3 3 BDL 0.015 TX3B1150 After 22,333 52.57 34.20 3 0 ADL 0.100 TX3B1160 Before 18,743 55.75 26.93 12 12 BDL 0.019 TX3B1170 Before 18,491 53.38 34.06 6 6 BDL 0.020 TX3B1180 After 19,795 53.34 34.20 6 6 BDL 0.050 TX3B1181 After 19,701 50.86 41.57 3 3 BDL 0.050 TX3B1200 After 18,654 58.03 20.69 9 9 BDL 0.050 TX3B1210 After 19,368 50.76 42.43 3 0 ADL 0.020 TX3B1220 Before 19,286 53.64 33.05 6 6 BDL 0.008 TX3B1250 Before 18,267 57.99 20.18 3 3 BDL #DIV/0! TX3B1310 N/A 19,741 51.42 40.25 3 3 BDL #DIV/0! TX3B1320 After 19,594 52.47 36.72 3 3 BDL #DIV/0! TX3B1330 Before 18,814 56.37 25.18 6 6 BDL 0.008 UT4A1360 N/A 19,988 51.50 39.53 3 3 BDL 0.020 UT4A1370 Before 19,678 51.63 39.47 3 3 BDL #DIV/0! UT4A1380 After 19,683 50.54 43.13 3 0 ADL 0.027 VI6A1530 Before 19,017 54.76 29.93 6 6 BDL #DIV/0! WA5A1400 After 19,685 54.69 30.00 3 3 BDL 0.050 WA5A1410 Before 19,090 54.15 31.47 3 3 BDL 0.008 WA5A1440 After 19,000 54.53 30.50 3 2 DLL 0.019 WI2B1460 After 18,700 55.24 28.67 3 3 BDL 0.020 WV1B1450 After 19,806 50.67 42.60 3 3 BDL 0.050 WY4A1470 Before 18,276 55.06 29.07 3 1 DLL 0.003 WY4A1480 After 18,594 52.18 37.87 6 6 BDL #DIV/0! WY4A1490 N/A 18,949 51.40 40.23 3 3 BDL #DIV/0! WY4A1500 N/A 19,75047.37 54.60 5 5 BDL 0.032 WY4A1510 Before 18,565 53.75 32.97 9 9 BDL 0.350 WY4A1520 After 19,321 51.49 39.97 3 3 BDL 0.050**Count for**

**Chlorine Detection Lim** **it Determ** **ination DL for** 

**Chlorine Avg** 

**Chlorine, ppmw**  **Count for**

**Sulfur Detection**  **Limit Determ** **ination DL for** 

**Sulfur Avg** 

**Sulfur, ppmw**  **Count for**

**Antim ony**  **Detection Limit**  **Determ ina**  **tion DL for**  **Antim ony**  **Avg**

**Antim ony,**  **ppmw** 3 BDL 198.2 0 ADL 63,130.0 3 BDL 0.490 0 ADL 1.0 0 ADL 10,066.7 3 BDL 0.500 6 BDL 8.2 0 ADL 1,553.3 6 BDL 0.642 0 ADL 25.3 0 ADL 3,066.7 3 BDL 0.718 1 DLL 78.1 0 ADL 345.4 5 DLL 1.052 1 DLL 37.2 0 ADL 7,043.3 1 DLL 0.285 6 DLL 27.2 3 DLL 8,740.0 0 ADL 0.173 0 ADL 1.0 0 ADL 16,566.7 9 BDL 0.500 0 ADL 64.5 0 ADL 13,477.8 9 BDL 11.778 0 ADL 340.0 0 ADL 54,666.7 3 BDL #DIV/0! 1 DLL 76.0 0 ADL 34,000.0 3 BDL #DIV/0! 2 DLL 54.7 0 ADL 5,300.0 3 BDL #DIV/0! 1 DLL 69.0 1 DLL 13,360.0 6 BDL 0.050 1 DLL 55.0 0 ADL 14,333.3 3 BDL #DIV/0! 0 ADL 17.0 0 ADL 14,633.3 3 BDL #DIV/0! 5 DLL 12.7 0 ADL 10,721.8 9 BDL 0.500 0 ADL 62.3 0 ADL 14,198.9 8 BDL 1.094 3 BDL 100.0 0 ADL 28,900.0 3 BDL 0.250 2 DLL 340.0 0 ADL 18,000.0 0 ADL 0.257 0 ADL 37.6 0 ADL 7,130.0 3 BDL 0.025 0 ADL 1.0 0 ADL 15,511.1 9 BDL 0.500 0 ADL 2.6 0 ADL 2,864.0 1 DLL 0.005 7 BDL #DIV/0! 0 ADL 11,314.3 7 BDL #DIV/0! 0 ADL 136.7 2 DLL 8,768.3 6 BDL #DIV/0! 1 DLL 22.0 0 ADL 16,746.7 3 BDL #DIV/0! 0 ADL 8.0 0 ADL 11,333.3 6 BDL 0.025 0 ADL 263.0 0 ADL 1,600.0 3 BDL #DIV/0! 0 ADL 260.8 0 ADL 11,469.2 12 BDL #DIV/0! 0 ADL 94.8 0 ADL 20,083.3 12 BDL 0.500 0 ADL 104.8 0 ADL 18,466.7 6 BDL 0.500 1 DLL 8.9 0 ADL 19,850.0 6 BDL 0.025 4 DLL 24.3 0 ADL 24,881.7 6 BDL 0.472 0 ADL 45.5 0 ADL 3,745.7 3 BDL 1.042 0 ADL 3,474.7 0 ADL 9,875.0 3 BDL 0.530 3 BDL 2.5 0 ADL 1.0 3 BDL 0.597 0 ADL 241.7 1 DLL 2,166.7 3 BDL 1.500 3 BDL 2.0 1 DLL 11.1 2 DLL 0.166 0 ADL 86.9 0 ADL 23.3 3 BDL 1.000 0 ADL 24.1 0 ADL 6,756.7 6 BDL 0.050 0 ADL 20.8 0 ADL 14,160.0 3 BDL 0.025 0 ADL 1.0 0 ADL 33,500.0 9 BDL 0.500 1 DLL 37.0 0 ADL 12,560.8 6 BDL 0.491 6 BDL 8.0 0 ADL 6,240.0 3 DLL 0.100 1 DLL 84.3 0 ADL 415.9 3 BDL 0.467 2 DLL 18.7 0 ADL 24,665.0 6 BDL #DIV/0! 9 BDL 100.0 0 ADL 27,955.6 9 BDL 2.500 3 BDL #DIV/0! 0 ADL 26,666.7 3 BDL #DIV/0! 2 DLL 49.7 3 BDL 1,566.7 3 BDL 1.0170 ADL 77.7 0 ADL 20,293.5 6 BDL 1.146

1 DLL 24.3 0 ADL 1,135.7 0 ADL 0.975 0 ADL 121.0 0 ADL 13,405.0 6 BDL 0.500 0 ADL 150.4 0 ADL 10,693.3 6 BDL 0.500 9 BDL 250.0 0 ADL 15,922.2 9 BDL 0.864 0 ADL 1.0 0 ADL 20,883.3 6 BDL 0.500 1 DLL 6.4 0 ADL 11,696.7 3 BDL 0.025 1 DLL 2.0 0 ADL 5,178.3 3 BDL 0.001 0 ADL 55.0 0 ADL 3,275.2 6 BDL 0.625 0 ADL 261.7 0 ADL 6,838.3 6 BDL #DIV/0! 0 ADL 148.7 0 ADL 8,156.7 3 BDL 0.500 0 ADL 308.7 0 ADL 3,860.0 3 BDL 0.500 0 ADL 2.0 0 ADL 13,220.0 3 BDL #DIV/0! 0 ADL 52.5 0 ADL 1,621.3 3 BDL 1.250 0 ADL 37.1 0 ADL 1,624.8 6 BDL 1.250 0 ADL 485.3 0 ADL 376.7 2 DLL 1.933 0 ADL 90.1 0 ADL 21,933.3 3 BDL 0.500 0 ADL 179.0 0 ADL 3,586.7 3 BDL #DIV/0! 9 BDL 5.0 0 ADL 1,663.3 9 BDL 0.500 2 DLL 23.0 0 ADL 5,038.5 6 BDL 0.489 0 ADL 54.2 0 ADL 4,676.7 2 DLL 0.102 0 ADL 188.4 0 ADL 3,971.7 5 DLL 0.266 0 ADL 221.7 0 ADL 2,480.0 6 BDL #DIV/0! 0 ADL 1.0 0 ADL 12,580.0 6 BDL 0.500 1 DLL 585.7 0 ADL 20,883.3 3 BDL 2.750 0 ADL 0.3 0 ADL 0.3 0 ADL 15.833 0 ADL 39.9 0 ADL 20,193.8 12 BDL 0.489 0 ADL 15.5 0 ADL 14,980.0 6 BDL 0.025 0 ADL 1.0 0 ADL 1.1 6 BDL 0.500 0 ADL 1.0 0 ADL 0.2 3 BDL 0.500 0 ADL 80.6 0 ADL 16,892.8 9 BDL 0.833 1 DLL 6.0 0 ADL 1,593.3 3 BDL 0.025 0 ADL 160.6 0 ADL 20,441.7 6 BDL 0.483 0 ADL 33.0 0 ADL 34,330.0 2 DLL 0.005 0 ADL 168.7 0 ADL 5,736.7 3 BDL #DIV/0! 0 ADL 121.3 0 ADL 6,663.3 3 BDL #DIV/0! 0 ADL 86.5 0 ADL 23,823.3 6 BDL 0.411 3 BDL 250.0 3 BDL 250.0 3 BDL 0.983 0 ADL 154.7 0 ADL 455.7 3 BDL #DIV/0! 0 ADL 2.2 0 ADL 3,110.0 0 ADL 1.000 6 BDL #DIV/0! 0 ADL 8,500.0 6 BDL #DIV/0! 0 ADL 1.0 0 ADL 10,833.3 3 BDL 0.500 1 DLL 79.3 0 ADL 11,080.0 3 BDL 0.413 1 DLL 110.0 0 ADL 8,000.0 3 BDL 1.400 2 DLL 566.3 0 ADL 14,766.7 3 BDL 0.478 0 ADL 87.8 0 ADL 675.7 3 BDL 1.250 2 DLL 2.9 0 ADL 23,040.0 0 ADL 0.004 6 BDL #DIV/0! 0 ADL 1,900.0 6 BDL #DIV/0! 2 DLL 13.0 0 ADL 700.0 3 BDL #DIV/0! 3 DLL 311.3 2 DLL 1,414.0 5 BDL 0.804 6 DLL 165.5 0 ADL 12,724.2 9 BDL 1.944 0 ADL 50.9 0 ADL 1,806.3 3 BDL 0.833**Count for**

**Arsenic Detection**  **Limit Determ** **ina tion**  **DL for**

**Arsenic Avg** 

**Arsenic, ppmw**  **Count for**

**Beryllium Detection**  **Limit Determ** **ina tion**  **DL for Beryllium**  **Avg**

**Beryllium ,**  **ppmw Count for** 

**Cadm ium**  **Detection Limit**  **Determ ina**  **tion DL for**  **Cadm ium**  **Avg**

**Cadm ium** **, ppmw**  3 BDL 1.233 3 BDL 0.490 3 BDL 0.490 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 6 BDL 0.421 6 BDL 0.128 6 BDL 0.160 3 BDL 0.492 3 BDL 0.143 3 BDL 0.180 6 BDL 0.470 6 BDL 0.276 6 BDL 0.276 1 DLL 0.127 3 BDL 0.025 3 BDL 0.025 5 DLL 0.117 8 BDL 0.025 4 DLL 0.030 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 9 BDL 2.344 9 BDL 2.344 9 BDL 1.178 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 DLL 0.127 6 BDL 0.050 6 BDL 0.050 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 7 DLL 1.067 9 BDL 0.500 9 BDL 0.500 8 BDL 0.438 8 BDL 0.438 8 BDL 0.438 3 BDL 0.050 3 BDL 0.100 3 BDL 0.100 2 DLL 0.083 3 BDL 0.000 2 DLL 0.004 2 DLL 0.053 3 BDL 0.025 3 BDL 0.025 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 0 ADL 0.064 3 BDL 0.001 3 BDL 0.001 7 BDL #DIV/0! 7 BDL #DIV/0! 7 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 DLL 0.102 6 BDL 0.025 6 BDL 0.025 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 12 BDL #DIV/0! 12 BDL #DIV/0! 12 BDL #DIV/0! 12 BDL 0.500 12 BDL 0.250 12 BDL 0.250 6 BDL 0.500 6 BDL 0.250 6 BDL 0.250 6 BDL 0.025 6 BDL 0.025 6 BDL 0.025 6 BDL 0.469 6 BDL 0.235 6 BDL 0.235 3 BDL 0.417 3 BDL 0.417 3 BDL 0.417 3 BDL 0.267 3 BDL 0.025 3 BDL 0.133 3 BDL 0.298 3 BDL 0.030 3 BDL 0.148 3 BDL 1.500 3 BDL 0.750 3 BDL 0.750 3 BDL 0.018 3 BDL 0.018 2 DLL 0.042 3 BDL 1.000 3 BDL 0.500 3 BDL 0.500 5 DLL 0.117 6 BDL 0.050 6 BDL 0.050 2 DLL 0.053 3 BDL 0.025 3 BDL 0.025 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 6 BDL 1.227 6 BDL 0.491 6 BDL 0.491 5 DLL 0.151 6 BDL 0.025 6 BDL 0.025 3 BDL 0.467 3 BDL 0.233 3 BDL 0.233 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 9 BDL 2.500 9 BDL 2.500 9 BDL 0.500 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL 1.017 3 BDL 0.102 3 BDL 0.2556 BDL 0.458 6 BDL 0.458 6 BDL 0.458

0 ADL 2.437 0 ADL 0.975 0 ADL 0.975 6 BDL 0.500 6 BDL 0.100 6 BDL 0.100 6 BDL 0.500 6 BDL 0.100 6 BDL 0.100 9 BDL 0.540 9 BDL 0.432 9 BDL 0.184 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 3 BDL 0.025 3 BDL 0.025 3 BDL 0.025 0 ADL 0.007 3 BDL 0.001 2 DLL 0.003 6 BDL 0.250 6 BDL 0.250 6 BDL 0.250 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL 0.500 3 BDL 0.100 3 BDL 0.100 3 BDL 0.500 3 BDL 0.100 3 BDL 0.100 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 0 ADL 2.697 3 BDL 0.250 3 BDL 0.250 3 BDL 2.500 3 BDL 2.500 3 BDL 0.500 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 9 BDL 0.417 9 BDL 0.500 9 BDL 0.417 6 BDL 1.223 6 BDL 0.489 6 BDL 0.489 3 BDL 0.066 3 BDL 0.033 2 DLL 0.107 6 BDL #DIV/0! 6 BDL #DIV/0! 5 DLL 0.013 6 BDL #DIV/0! 6 BDL #DIV/0! 5 DLL 0.174 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 3 BDL 2.750 3 BDL 0.550 3 BDL 0.550 0 ADL 2.500 0 ADL 2.500 0 ADL 2.500 12 BDL 1.222 12 BDL 0.489 12 BDL 0.489 6 BDL 0.025 6 BDL 0.025 6 BDL 0.025 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 9 BDL 0.500 9 BDL 0.333 9 BDL 0.333 3 BDL 0.025 3 BDL 0.025 3 BDL 0.025 6 BDL 0.483 6 BDL 0.243 6 BDL 0.243 2 DLL 0.007 2 DLL 0.052 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 6 BDL 0.411 6 BDL 0.205 6 BDL 0.205 3 BDL 0.615 3 BDL 0.492 3 BDL 0.209 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 1.000 0 ADL 0.200 0 ADL 0.200 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 3 BDL 0.413 3 BDL 0.208 3 BDL 0.208 3 BDL 1.400 3 BDL 0.118 3 BDL 0.232 3 BDL 0.240 3 BDL 0.024 3 BDL 0.064 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 0 ADL 0.009 3 BDL 0.001 2 DLL 0.002 2 DLL 0.325 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 5 BDL 0.493 5 BDL 0.415 5 BDL 0.234 9 BDL 1.778 9 BDL 1.778 9 BDL 0.444 3 BDL 0.333 3 BDL 0.333 3 BDL 0.333**Count for**

**Chrom ium**  **Detection Limit**  **Determ ina**  **tion DL for**  **Chrom ium**  **Avg**

**Chrom ium** **, ppmw**  **Count for**

**Cobalt Detection**  **Limit Determ** **inati on**  **DL for**

**Cobalt Avg** 

**Cobalt, ppmw**  **Count for**

**Lead Detection**  **Limit Determ** **ina tion**  **DL for**

**Lead Avg Lead,** 

**ppmw** 3 BDL 1.967 3 BDL 1.967 3 BDL 0.490 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 6 BDL 0.320 6 BDL 0.320 5 DLL 0.420 3 BDL 0.360 3 BDL 0.360 1 DLL 0.663 6 BDL 0.470 6 BDL 2.350 6 BDL 0.470 0 ADL 0.343 0 ADL 0.324 0 ADL 0.101 0 ADL 0.219 3 DLL 0.104 0 ADL 0.100 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 9 BDL 1.178 9 BDL 1.178 9 BDL 2.344 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 2 DLL 0.200 1 DLL 1.400 1 DLL 0.540 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 3.000 3 BDL #DIV/0! 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 8 BDL 0.438 8 BDL 0.438 8 BDL 0.438 3 BDL 0.250 3 BDL 0.250 3 BDL 0.150 0 ADL 0.069 0 ADL 0.047 0 ADL 0.050 3 BDL 0.025 1 DLL 0.067 1 DLL 0.067 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 0 ADL 0.040 1 DLL 0.007 1 DLL 0.059 7 BDL #DIV/0! 7 BDL #DIV/0! 7 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 6 BDL 0.025 4 DLL 0.072 3 DLL 0.135 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 12 BDL #DIV/0! 12 BDL #DIV/0! 12 BDL #DIV/0! 12 BDL 0.250 12 BDL 0.250 12 BDL 0.500 6 BDL 0.250 6 BDL 0.250 6 BDL 0.333 4 DLL 0.055 0 ADL 0.190 6 BDL 0.025 6 BDL 0.468 6 BDL 2.350 6 BDL 0.468 3 BDL 0.417 3 BDL 0.417 3 BDL 0.417 3 BDL 0.267 3 BDL 0.267 3 BDL 0.267 3 BDL 0.298 3 BDL 0.298 3 BDL 0.298 3 BDL 0.750 3 BDL 0.750 3 BDL 0.750 0 ADL 0.150 3 BDL 0.018 0 ADL 0.465 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 1 DLL 0.133 4 DLL 0.100 1 DLL 0.417 1 DLL 0.087 1 DLL 0.067 2 DLL 0.050 9 BDL 0.500 9 BDL 0.500 8 DLL 1.660 5 DLL 3.610 6 BDL 1.963 6 BDL 0.491 0 ADL 0.250 0 ADL 0.146 4 DLL 0.075 2 DLL 1.020 3 BDL 2.333 3 BDL 0.467 5 DLL 2.260 6 BDL #DIV/0! 6 BDL #DIV/0! 9 BDL 2.500 9 BDL 2.500 9 BDL 2.500 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL 0.495 3 BDL 2.550 3 BDL 1.0176 BDL 0.458 6 BDL 0.458 6 BDL 0.458

0 ADL 3.900 0 ADL 3.900 0 ADL 0.975 6 BDL 0.250 6 BDL 0.500 6 BDL 0.500 6 BDL 0.250 6 BDL 0.500 6 BDL 0.500 9 BDL 2.159 9 BDL 0.292 9 BDL 7.725 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 2 DLL 0.057 1 DLL 0.090 1 DLL 0.190 0 ADL 0.057 0 ADL 0.032 0 ADL 0.009 6 BDL 0.250 6 BDL 0.250 6 BDL 0.250 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL 0.250 3 BDL 0.500 3 BDL 0.500 3 BDL 0.250 3 BDL 0.500 3 BDL 0.500 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 0 ADL 4.087 3 BDL 1.000 3 BDL 1.000 3 BDL 0.500 3 BDL 2.500 3 BDL 0.500 2 DLL 0.268 3 BDL #DIV/0! 3 BDL #DIV/0! 9 BDL 0.417 9 BDL 0.500 6 DLL 1.109 6 BDL 1.954 6 BDL 1.954 6 BDL 0.489 0 ADL 0.276 2 DLL 0.182 0 ADL 1.089 5 DLL 0.160 5 DLL 0.112 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 5 DLL 0.228 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 3 BDL 1.375 3 BDL 2.750 2 DLL 14.100 0 ADL 2.500 0 ADL 2.500 0 ADL 2.500 12 BDL 1.958 12 BDL 1.958 12 BDL 0.489 6 BDL 0.026 6 BDL 0.019 6 BDL 0.026 5 DLL 1.047 6 BDL 0.500 6 BDL 0.500 1 DLL 1.047 3 BDL 0.500 3 BDL 0.500 9 BDL 0.500 9 BDL 0.333 9 BDL 0.333 3 BDL 0.025 1 DLL 0.063 2 DLL 0.063 6 BDL 0.483 6 BDL 2.425 6 BDL 0.483 2 DLL 0.023 2 DLL 0.007 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 6 BDL 0.411 6 BDL 2.050 6 BDL 0.411 3 BDL 2.515 3 BDL 0.332 3 BDL 8.625 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 0.500 0 ADL 1.000 0 ADL 1.000 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 3 BDL 0.413 3 BDL 2.083 3 BDL 0.413 3 BDL 0.600 3 BDL 0.232 3 BDL 0.700 1 DLL 0.220 3 BDL 0.080 2 DLL 0.477 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 0 ADL 0.028 0 ADL 0.013 0 ADL 0.051 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 1 DLL 1.950 3 BDL #DIV/0! 3 BDL #DIV/0! 5 BDL 1.673 5 BDL 0.312 5 BDL 7.970 9 BDL 1.778 9 BDL 1.778 9 BDL 1.778 3 BDL 0.333 3 BDL 0.333 3 BDL 0.333**Count for**

**Manganes e Detection**  **Limit Determ** **ina tion**  **DL for Manganese**  **Avg**

**Manganese, ppmw**  **Count for**

**Nickel Detection**  **Limit Determ** **inatio n**  **DL for Nickel Avg**  **Nickel, ppmw**  **Count for**

**Selenium Detection**  **Limit Determ** **ina tion**  **DL for**

**Selenium Avg** 

**Selenium ,**  **ppmw** 3 BDL 1.967 0 ADL 19.533 3 BDL 0.490 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 6 BDL 0.320 6 BDL 1.275 6 BDL 0.421 3 BDL 0.360 3 BDL 1.433 3 BDL 0.492 6 BDL 0.708 3 DLL 7.633 6 BDL 0.470 0 ADL 0.266 0 ADL 2.873 3 BDL 0.124 0 ADL 0.071 0 ADL 4.573 6 DLL 0.183 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 9 BDL 2.344 0 ADL 57.444 9 BDL 4.689 3 BDL #DIV/0! 0 ADL 68.667 3 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 48.667 3 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 28.000 3 BDL #DIV/0! 4 DLL 0.180 1 DLL 59.400 6 BDL 0.050 3 BDL #DIV/0! 0 ADL 13.600 3 BDL #DIV/0! 1 DLL 3.200 0 ADL 62.233 3 BDL #DIV/0! 9 BDL 0.500 1 DLL 6.365 9 BDL 0.500 8 BDL 0.438 0 ADL 3.441 8 BDL 0.438 2 DLL 2.287 2 DLL 5.033 3 BDL 0.250 0 ADL 0.096 0 ADL 9.800 0 ADL 0.380 3 BDL 0.025 0 ADL 8.847 0 ADL 0.120 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 0 ADL 0.061 0 ADL 0.757 0 ADL 0.035 7 BDL #DIV/0! 2 DLL 8.396 7 BDL #DIV/0! 6 BDL #DIV/0! 3 DLL 5.297 6 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 17.267 2 DLL 0.692 6 BDL 0.025 0 ADL 7.367 1 DLL 0.082 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 12 BDL #DIV/0! 3 DLL 5.142 12 BDL #DIV/0! 12 BDL 0.250 4 DLL 1.683 12 BDL 0.500 6 BDL 0.250 2 DLL 3.980 6 BDL 0.500 4 DLL 0.237 0 ADL 16.883 0 ADL 0.112 6 BDL 0.717 5 DLL 4.450 6 BDL 0.468 3 BDL 0.417 0 ADL 1.993 3 BDL 0.417 3 BDL 0.267 0 ADL 5.223 3 BDL 0.530 3 BDL 0.298 0 ADL 4.003 3 BDL 0.597 3 BDL 0.750 1 DLL 2.033 3 BDL 1.167 1 DLL 0.176 0 ADL 0.460 3 BDL 0.092 3 BDL 0.500 3 BDL 0.500 3 BDL 1.000 0 ADL 0.200 0 ADL 2.750 6 BDL 0.050 3 BDL 0.025 0 ADL 20.533 0 ADL 0.143 9 BDL 0.500 9 BDL 0.500 9 BDL 0.500 6 BDL 1.963 1 DLL 14.974 5 DLL 0.914 0 ADL 0.248 0 ADL 4.133 6 BDL 0.105 3 BDL 0.700 2 DLL 5.933 3 BDL 0.467 6 BDL #DIV/0! 0 ADL 27.417 4 DLL 0.616 9 BDL 2.500 0 ADL 8.111 9 BDL 2.500 3 BDL #DIV/0! 0 ADL 7.667 3 BDL #DIV/0! 3 BDL 0.750 3 BDL 2.017 3 BDL 1.0176 BDL 0.458 0 ADL 5.522 5 DLL 0.945

0 ADL 3.900 0 ADL 0.986 0 ADL 0.975 6 BDL 0.250 0 ADL 4.618 6 BDL 0.500 6 BDL 0.250 0 ADL 1.927 6 BDL 0.500 9 BDL 0.864 0 ADL 13.300 9 BDL 1.836 6 BDL 0.500 5 DLL 1.043 6 BDL 0.500 2 DLL 0.050 0 ADL 14.073 0 ADL 0.127 0 ADL 0.008 0 ADL 1.388 0 ADL 0.024 6 BDL 0.250 1 DLL 0.673 4 DLL 0.462 6 BDL #DIV/0! 0 ADL 3.850 2 DLL 0.600 2 DLL 0.609 0 ADL 3.757 3 BDL 0.500 3 BDL 0.250 0 ADL 2.617 3 BDL 0.500 3 BDL #DIV/0! 0 ADL 3.220 3 BDL #DIV/0! 3 BDL 0.500 0 ADL 2.640 3 BDL 0.500 6 BDL 0.500 0 ADL 2.267 6 BDL 0.500 2 DLL 2.077 2 DLL 3.757 3 BDL 0.500 3 BDL 0.500 0 ADL 32.000 3 BDL 0.500 3 BDL #DIV/0! 0 ADL 1.230 3 BDL #DIV/0! 9 BDL 0.417 0 ADL 5.021 9 BDL 0.500 6 BDL 1.954 0 ADL 2.185 6 BDL 0.489 0 ADL 0.521 0 ADL 2.140 3 BDL 0.165 4 DLL 0.179 0 ADL 1.998 3 DLL 0.850 6 BDL #DIV/0! 1 DLL 0.980 6 BDL #DIV/0! 6 BDL 0.500 5 DLL 1.008 6 BDL 0.500 3 BDL 1.375 0 ADL 28.220 3 BDL 2.750 0 ADL 2.500 0 ADL 4.197 0 ADL 2.500 12 BDL 1.958 0 ADL 24.589 12 BDL 0.489 6 BDL 0.025 0 ADL 1.596 6 BDL 0.025 6 BDL 0.500 6 BDL 0.500 6 BDL 0.500 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 8 DLL 1.026 2 DLL 4.042 7 DLL 1.029 2 DLL 0.053 0 ADL 2.117 1 DLL 0.060 6 BDL 0.725 5 DLL 4.083 6 BDL 0.483 2 DLL 0.006 0 ADL 1.399 2 DLL 0.011 2 DLL 0.114 1 DLL 1.625 2 DLL 0.447 3 BDL #DIV/0! 3 BDL #DIV/0! 3 BDL #DIV/0! 6 BDL 0.613 4 DLL 4.367 6 BDL 0.411 3 BDL 0.983 3 BDL 4.917 3 BDL 2.092 3 BDL #DIV/0! 0 ADL 3.400 3 BDL #DIV/0! 0 ADL 0.500 0 ADL 1.783 0 ADL 1.000 6 BDL #DIV/0! 0 ADL 21.317 6 BDL #DIV/0! 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 3 BDL 0.617 2 DLL 3.333 3 BDL 0.413 3 BDL 0.463 0 ADL 6.300 3 BDL 2.317 2 DLL 0.128 0 ADL 5.947 3 BDL 0.717 3 BDL 0.500 3 BDL 0.500 3 BDL 0.500 0 ADL 0.019 0 ADL 2.377 0 ADL 0.016 6 BDL #DIV/0! 6 BDL #DIV/0! 6 BDL #DIV/0! 3 BDL #DIV/0! 0 ADL 1.100 0 ADL 0.600 5 BDL 0.729 5 BDL 3.251 4 DLL 2.902 9 BDL 1.778 3 DLL 7.101 8 DLL 3.574 3 BDL 0.333 3 BDL 0.333 3 BDL 0.333**Count for**

**Before Desalter** **Count For**

**After Desalter**  0 0 0 3 0 6 0 3 3 3 3 0 8 0 9 0 9 0 0 0 3 0 0 0 6 0 3 0 0 0 9 0 8 0 3 0 0 3 1 2 0 9 3 0 7 0 0 6 0 3 0 6 3 0 0 12 0 12 0 6 0 6 0 6 0 3 0 3 0 3 3 0 3 0 3 0 6 0 0 3 0 9 0 6 0 0 0 3 6 0 0 0 0 3 0 00 6

0 3 0 6 0 6 0 0 6 0 0 3 0 3 0 6 6 0 0 3 0 3 3 0 2 1 0 6 2 1 0 3 3 0 0 9 0 6 0 3 6 0 6 0 6 0 3 0 0 3 12 0 6 0 0 6 0 3 0 9 0 3 6 0 3 0 0 0 0 3 6 0 0 0 3 0 0 3 6 0 0 3 3 0 0 3 0 3 0 3 3 0 0 6 0 0 0 0 6 0 0 3

### ICR_ID plant_name

AK5A0040Crude Oil Topping Plant AK5A0050Kuparuk Plant AK5A0060Petro Star North Pole Refinery AK5A0070Petro Star Valdez Refinery AK5A0080Tesoro Alaska Company, Kenai Refinery AK5A0090Flint Hills Resources Alaska LLC AL3C0030Mobile Site AL3D0010Goodway Refining, LLC AL3D0020Hunt Refining Company AR3D0100Martin Operating Partnership,LP AR3D0110Lion Oil Company CA5A0120BP West Coast Products LLC, Refinery CA5A0130El Segundo Refinery CA5A0140Chevron Products Co, Richmond Refinery CA5A0150Alon Bakersfield Refining CA5A0160Shell Oil Products US CA5A0170Wilmington-LA Refinery CA5A0180Edgington Oil Company CA5A0190Torrance Refinery CA5A0200Santa Maria Refining Company CA5A0210Valero Wilmington Asphalt Plant CA5A0220Kern Oil & Refining Company CA5A0230Paramount Petroleum Corporation CA5A0240San Joaquin Refining Company, Inc. CA5A0260ConocoPhillips Los Angeles Refinery Carson CA5A0270ConocoPhillips Los Angeles Refinery Wilmington CA5A0280ConocoPhillips San Francisco Refinery at Rodeo CA5A0290SANTA MARIA FACILITY CA5A0300Golden Eagle Refinery CA5A0310Valero Wilmington Refinery CA5A0320Benicia Refinery CA5A0330Lunday-Thagard Company CO4A0340Commerce City Refinery DE1A0360Delaware City Refinery GA1A0370NuStar Savannah Asphalt Refinery, LLC HI5A0380Hawaii Refinery HI5A0390Kapolei Refinery IL2A0400 CITGO Lemont Refinery IL2A0410 Joliet Refinery IL2A0420 Marathon Petroleum Company LP, Illinois Refining Division IL2A0430 Wood River Refinery IN2A0440BP Whiting Refinery IN2A0450CountryMark Cooperative LLP KS2C0460Coffeyville Refinery KS2C0470National Cooperative Refinery Association KS2C0480Frontier El Dorado Refining Co.

### KY2A0490Marathon Petroleum Company - Catlettsburg Refinery

KY2A0500Somerset Energy Refining LLC LA3C0510PELICAN REFINING CO LLC LA3C0520Calcasieu Refining Company LA3C0560CITGO Petroleum Lake Charles Manufacturing Complex LA3C0570ConocoPhillips LA3C0590ExxonMobil Refining & Supply Baton Rouge Refinery LA3C0600Chalmette Refining, L. L. C. LA3C0610Marathon Petroleum Company LP LA3C0620Motiva Enterprises Convent Refinery LA3C0630Norco Refinery LA3C0640Meraux Refinery LA3C0650Saint Charles Refinery LA3C0670Placid Refining Company LLC LA3C0690Alliance Refinery LA3C0700Alon Refining Krotz Springs, Inc. LA3D0530Calumet Lubricants Company Cotton Valley Refinery LA3D0540Calumet Lubricants Company Princeton Refinery LA3D0660Calumet Lubricants, LP MI2A0710Michigan Refining Division MN2B0720Flint Hills Resources Pine Bend LLC Pine Bend Refinery MN2B0730St. Paul Park Refining Co. LLC MS3C0740Pascagoula Refinery MS3D0750Ergon Refining, Inc. MS3D0760Rogerslacey Refinery MT4A0770CHS Inc. MT4A0780ConocoPhillips-Billings MT4A0790ExxonMobil Billings Refinery MT4A0800Montana Refining Company, Inc. ND2B0900Mandan Refinery NJ1A0820Port Reading Refinery NJ1A0830Perth Amboy Asphalt Refinery NJ1A0840NuStar Asphalt Refining, LLC NJ1A0850Bayway Refinery NJ1A0860Paulsboro Refining Company LLC NM3E0880Western Refining Southwest, Inc. - Gallup NM3E0890Artesia Refinery NM3E0891Lovington Refinery NV5A0810Foreland-Eagle Springs Refinery OH2A0910BP Toledo Refinery OH2A0920Marathon Petroleum Company LP - Ohio Refining Division OH2A0930Lima Refining Company OH2A0940Toledo Refining Company LLC OK2C0950ConocoPhillips Ponca City Refinery OK2C0960Wynnewood Refining Company OK2C0970Holly Tulsa East Refinery OK2C0980Holly Tulsa West Refinery

### OK2C0990Valero Ardmore Refinery

OK2C1000Ventura Refinery PA1A1020Sunoco Inc., Marcus Hook Refinery PA1A1030Sunoco, Inc. (R&M) - Philadelphia Refinery PA1A1040ConocoPhillips Trainer Refinery PA1B1010American Refining Group, Inc. PA1B1050United Refining Company TN2A1060Memphis Refinery - CBI TX3A1070AGE Refining, Inc. TX3A1080Big Spring Refinery TX3A1120El Paso Refinery TX3A1190Delek Refinery TX3A1230Borger, Refinery TX3A1290Three Rivers Refinery TX3A1300Diamond Shamrock Refining Company, L.P. TX3B1090TOTAL Port Arthur Refinery TX3B1110BP Texas City Refinery TX3B1130CITGO Refining & Chemicals L.P. (CITGO East Plant Refinery) TX3B1131CITGO Refining & Chemicals L.P. (CITGO West Plant Refinery) TX3B11400352004101 TX3B1150Pasadena Refining System Inc. TX3B1160Baytown Refinery TX3B1170Beaumont Refinery TX3B1180Flint Hills Resources, LLC Corpus Christi West Refinery TX3B1181Flint Hills Resources, LLC Corpus Christi East Refinery TX3B1200Houston Refining LP TX3B1210Texas Refining Division TX3B1220Motiva Enterprises LLC Port Arthur Refinery TX3B1240ConocoPhillips, Sweeny Refinery TX3B1250035200l104 TX3B1260Deer Park Refining Limited Partnership (EIA ID# 1339570101) TX3B1270BTB Refining, LLC TX3B1310352004101 TX3B1320Houston Refinery TX3B1330Valero Texas City Plant UT4A1340Tesoro Refining and Marketing Company UT4A1350Salt Lake Refinery UT4A1360Silver Eagle Refining-Woods Cross UT4A1370Big West Oil, LLC UT4A1380Woods Cross Refinery VA1A1390Western Refining Yorktown, Inc. VI6A1530 Hovensa L.L.C. WA5A1400BP Cherry Point Refinery WA5A1410Shell Oil Products US- Puget Sound Refinery WA5A1420Anacortes Refinery WA5A1430Ferndale Refinery WA5A1440U.S. Oil & Refining Co.

### WI2B1460Murphy Oil USA, Inc. Superior Refinery

WV1B1450Ergon-West Virginia WY4A1470Cheyenne Refinery WY4A1480Sinclair Casper Refining Company WY4A1490Douglas Refinery -WY4A1490 WY4A1500Silver Eagle Refining-Evanston WY4A1510Sinclair Refinery WY4A1520Newcastle Refinery

### FACILITY_NAME

BP Exploration (Alaska) Inc. ConocoPhillips Kuparuk Plant Petro Star Inc. - North Pole PETRO STAR VALDEZ REFY Tesoro Alaska Petroleum Company Kenai Refinery FLINT HILLS RESOURCES ALASKA LLC. Shell Chemical Company Goodway Refining LLC HUNT REFINING CO A CORPORATION Cross Oil Refining & Marketing, Inc. LION OIL COMPANY BP CARSON REFINERY CHEVRON USA PRODUCTS CO. CHEVRON PRODUCTS CO. RICHMOND REFINERY Big West Oil LLC (prev. Shell Oil Products US) SHELL OIL PRODUCTS US - MARTINEZ REFINERY Shell Oil Products US - Wilmington EDGINGTON OIL COMPANY MOBIL OIL CORP Greka Energy VALERO WILMINGTON ASPHALT PLANT KERN OIL & REFINING COMPANY PARAMOUNT PETROLEUM CORP SAN JOAQUIN REFINING COMPANY INCORPORATED CONOCOPHILLIPS CARSON PLANT UNION OIL CO LOS ANG REFINERY CONOCOPHILLIPS SAN FRANCISCO AREA REFINERY AT RODEO CONOCOPHILLIPS SANTA MARIA FACILITY- REFINERY TESORO REFINING AND MARKETING Valero Refining Co. - Wilmington (prev. Ultramar Inc.) VALERO REFINING CO CALIFORNIA BENICIA REFINERY LUNDAY-THAGARD OIL CO SUNCOR DENVER REFINERY Valero Refining Co. (prev. Motiva Enterprises LLC) CITGO Asphalt Refining Company CHEVRON PRODUCTS CO - HAWAII REFINERY TESORO HAWAII CORPORATION REFINERY-KAPOLEI CITGO Petroleum Corp EXXONMOBIL-JOLIET REFINERY MARATHON PETROLEUM CO LLC CONOCOPHILLIPS CO WOOD RIVER REFINERY BP PRODUCTS NORTH AMERICA INC, WHITING REFINERY COUNTRYMARK COOPERATIVE, INC COFFEYVILLE RESOURCES REFINING & MARKETING NATIONAL COOPERATIVE REFINERY FRONTIER EL DORADO REFINING COMPANY

### MARATHON ASHLAND PETROLEUM/CATLETTSBURG

SOMERSET REFINERY PELICAN REFINING COMPANY CALCASIEU REFINING CO CITGO PETROLEUM CORPORATION CONOCOPHILLIPS CO - LAKE CHARLES REFINERY TETRA PROCESS SERVICES LC EXXON REF LACATION BATON ROUGE EXXONMOBIL REFINERY COMPLEX MARATHON ASHLAND PETROLEUM LLC MOTIVA ENTERPRISES LLC/CONVENT REFINERY MOTIVA ENTERPRISES LLC - NORCO REFINERY MURPHY OIL USA INC MERAUX TERMINAL VALERO SAINT CHARLES REFINERY PLACID REFINING CO LLC/PORT ALLEN REFINERY BP OIL COMPANY ALLIANCE REFINERY VALERO REFINING CO/KROTZ SPRINGS REFINERY CALUMET LUBRICANTS CO - COTTON VALLEY REFI Calumet Lubricants Co. LP - Princeton CALUMET SHREVEPORT LUBRICANTS AND WAXES LLC/SHREVEPORT REFINERY MARATHON ASHLAND PETROLEUM FLINT HILLS RESOURCES LP MARATHON PETROLEUM CO LLC SAINT PAUL PARK REFINER CHEVRON TEXACO PRODUCTS COMPANY, PASCAGO ERGON REFINING INC HUNT SOUTHLAND REFINING COMPANY CENEX INC LAUREL REFINERY CONOCO INCORPORATED REFINERY EXXON BILLINGS REFINERY MONTANA REFINING COMPANY Tesoro - Mandan AMERADA HESS CORP PACKAGING CHEVRON PRODUCTS COMPANY CITGO ASPHALT REFINING COMPANY BAYWAY CHEMICAL PLANT OF INFINEUM USA VALERO REFINING CO Giant Refining Co. - Ciniza Refinery Navajo Refining Co. - Artesia Navajo Refining Co. - Lovington EAGLE SPRINGS REFINERY BP OIL COMPANY TOLEDO REFINNERY MARATHON PETROLEUM COMPANY LLC, CANTON REFINERY Valero Refining Co. (prev. Premcor Refining Group) SUNOCO INC. TOLEDO REFINERY CONOCOPHILLIPS CO PONCA CITY REFI NERY WYNNEWOOD REFINING CO SINCLAIR OIL TULSA REFINING TULSA TRUCKING SUNOCO PIPELINE LP - SUNOCO BALLINGER - COLEMAN COUNTY TX

### VALERO RFNRY CO/ARDMORE RFNRY

Ventura Refining & Transmission, LLC SUNOCO MARCUS HOOK REF SUNOCO GIRARD POINT REFINERY CONOCOPHILLIPS CO. TRAINER REFINERY AMERICAN REFINING GROUP INC UNITED REFINING CO/WARREN PLT Valero Refining Co. (prev. Premcor Refining, prev. Williams Refining LLC) AGE Refining & Manufacturing FINA OIL & CHEMICAL EL PASO REFINERY DELEK TYLER REFINERY ConocoPhillips Co. - Borger (prev. Phillips 66 Co.) VALERO THREE RIVERS REFINERY Valero Energy Corp. - McKee (prev. Diamond Shamrock Refining) TOTAL PETROCHEMICALS USA INC. - PORT ARTHUR REFINERY BP TEXAS CITY REFINERY CITGO EAST PLANT REFINERY CITGO REFINING & CHEMICALS CO LP VALERO REFINING TEXAS LP CORPUS CHRISTI EAST PLANT PASADENA REFINING SYSTEM PRSI WEST DEMOLITION PROJECT EXXONMOBIL REF & SUPPLY EXXONMOBIL OIL BEAUMONT REFINERY FLINT HILLS RESOURCES LP - WEST PLANT KOCH REFINING COMPANY CHANNEL ENERGY ENERGY MARATHON ASHLAND PETROLEUM CO LLC PORT ARTHUR REFINERY PHILLIPS 66 COMPANY SWEENY COMPLEX Valero Refining Co. - Port Arthur (prev. Premcor Refining Group Inc.) SHELL OIL DEER PARK TRIGEANT LTD VALERO REFINING - TEXAS L.P. VALERO REFINING HOUSTON REFINERY Valero Refining Co. Texas Tesoro - Salt Lake City CHEVRON USA PRODUCTS COMPANY Silver Eagle Refining Big West Oil Co. (Flying J) HOLLY REFINING & MARKETING, FKA PHILLIPS 66 COMPANY GIANT YORKTOWN REFINERY HOVENSA LLC BP West Coast Products - Cherry Point SHELL OIL ANACORTES REFINERY ANACORTES REFINERY TESORO NORTHWEST COMPANY CONOCOPHILLIPS CO FERNDALE REFINERY U.S. OIL & REFINING CO.

### MURPHY OIL USA, INC., SUPERIOR REFINERY

ERGON - WEST VIRGINIA, INC. FRONTIER REFINING INC. Little America Refining Co. (Sinclair) Garco Energy Douglas Refinery SILVER EAGLE REFINING-EVANSTON SINCLAIR OIL CORPORATION WYOMING REFINING COMPANY

### LOCATION_ADDRESS CITY STATE

Prudhoe Bay Oilfield Prudhoe Bay AK Kuparuk Oilfield North Slope Borough AK 1200 H & H LN. NORTH POLE AK 2.5 MILE DAYVILLE RD. VALDEZ AK 54741 TESORO ROAD KENAI AK 1100 H&H LANE NORTH POLE AK 400 INDUSTRIAL PKWY SARALAND AL 4745 Ross Road Atmore AL 1855 FAIRLAWN RD TUSCALOOSA AL 484 East 6th Street Smackover AR 1000 MCHENRY DRIVE EL DORADO AR 1801 E SEPULVEDA BLVD CARSON CA 324 W EL SEGUNDO BLVD EL SEGUNDO CA 841 CHEVRON WAY RICHMOND CA 6451 ROSEDALE HWY (AREA 1 & 2) BAKERSFIELD CA 3485 PACHECO BLVD MARTINEZ CA 2101 E PACIFIC COAST HWY WILMINGTON CA 2400 E ARTESIA BLVD LONG BEACH CA 3700 WEST 190TH ST TORRANCE CA 1660 SINTON ROAD SANTA MARIA CA 1651 ALAMEDA ST WILMINGTON CA 7724 EAST PANAMA LANE BAKERSFIELD CA 14700 DOWNEY AVE PARAMOUNT CA 3542 SHELL ST BAKERSFIELD CA 1520 E SEPULVEDA BLVD CARSON CA 1660 W ANAHEIM ST WILMINGTON CA 1380 SAN PABLO AVE RODEO CA 2555 WILLOW ROAD ARROYO GRANDE CA Avon Refinery MARTINEZ CA 2402 E. ANAHEIM ST. WILMINGTON CA 3400 EAST 2ND BENICIA CA 9301 GARFIELD AVENUE SOUTH GATE CA 5801 BRIGHTON BLVD COMMERCE CITY CO 2000 WRANGLE HILL RD DELAWARE CITY DE 7 FOUNDATION DRIVE SAVANNAH GA 91-480 MALAKOLE ST. KAPOLEI HI 91-325 KOMOHANA ST KAPOLEI HI 135TH ST & NEW AVE LEMONT IL 25915 SE FRONTAGE ROAD CHANNAHON IL 100 MARATHON AVENUE ROBINSON IL 900 S CENTRAL AVE ROXANA IL 2815 INDIANAPOLIS BOULEVARD WHITING IN 1200 REFINERY RD MOUNT VERNON IN 400 NORTH LINDEN COFFEYVILLE KS 1391 IRON HORSE ROAD MC PHERSON KS 1401 S. DOUGLAS ROAD EL DORADO KS

### 11631 US ROUTE 23 CATLETTSBURG KY

600 MONTICELLO RD SOMERSET KY 4646 LA HWY 3059 LAKE CHARLES LA 4359 W TANK FARM RD LAKE CHARLES LA 4401 HIGHWAY 108 LAKE CHARLES LA 2200 OLD SPANISH TRAIL WESTLAKE LA 4045 SCENIC HWY BATON ROUGE LA 500 W. ST. BERNARD HWY CHALMETTE LA HWY. 61 & MARATHON AVE. GARYVILLE LA HWY 70 & HWY 44 CONVENT LA 15536 RIVER RD NORCO LA 2500 EAST SAINT BERNARD HIGHWAY MERAUX LA 14902 RIVER RD. NORCO LA 1940 LA HWY 1, NORTH PORT ALLEN LA 15551 HIGHWAY 23 SOUTH BELLE CHASSE LA HIGHWAY 105 SOUTH KROTZ SPRINGS LA 1756 OLD HWY 7 COTTON VALLEY LA 10234 HWY 157 PRINCETON LA 3333 MIDWAY SHREVEPORT LA 1300 S FORT ST DETROIT MI 12555 CLARK ROAD ROSEMOUNT MN 300 3RD STREET ST. PAUL PARK MN 250 INDUSTRIAL ROAD PASCAGOULA MS 2611 HAINING RD VICKSBURG MS HIGHWAY 11 NORTH SANDERSVILLE MS 803 HWY 212 S LAUREL MT 401 S 23RD ST BILLINGS MT 700 EXXON MOBILE RD BILLINGS MT 1900 10TH ST NE GREAT FALLS MT 900 OLD RED TRAIL NE MANDAN ND 750 CLIFF ROAD PORT READING NJ 1200 STATE ST PERTH AMBOY NJ 4 PARADISE RD PAULSBORO NJ 1400 PARK AVE LINDEN NJ 800 BILLINGSPORT RD PAULSBORO NJ 17 MILES E OF GALLUP ON I-40, EXIT 39 JAMESTOWN NM 501 E MAIN ST ARTESIA NM 5 MILES S. OF LOVINGTON ON HWY. 18 LOVINGTON NM HC 34, BOX 34830 ELY NV 4001 CEDAR POINT ROAD OREGON OH 2408 GAMBRINUS AVENUE SW CANTON OH 1150 SOUTH METCALF STREET LIMA OH 1819 WOODVILLE ROAD OREGON OH 1000 S PINE ST PONCA CITY OK 906 S POWELL WYNNEWOOD OK 902 W 25TH ST TULSA OK 1700 S UNION AVE TULSA OK

### HWY. 142 & E. CAMERON RD. ARDMORE OK

24322 East 910 Road Thomas OK 100 GREEN ST MARCUS HOOK PA 3144 PASSYUNK AVE PHILADELPHIA PA 4101 POST RD TRAINER PA 77 N KENDALL AVE BRADFORD PA 15 BRADLEY ST WARREN PA 543 West Mallory Avenue Memphis TN 7811 S. PRESA ST. SAN ANTONIO TX I. 20 AT REFINERY ROAD BIG SPRING TX 6501 TROWBRIDGE EL PASO TX 1702 E COMMERCE ST TYLER TX SPUR 119 NORTH BORGER TX 301 LEROY STREET THREE RIVERS TX 6701 FM 119 SUNRAY TX HIGHWAY 366 AND 32ND STREET PORT ARTHUR TX 2401 5TH AVE S TEXAS CITY TX 1801 NUECES BAY BLVD CORPUS CHRISTI TX 7350 INTERSTATE HWY. 37 CORPUS CHRISTI TX 1300 CANTWELL LN CORPUS CHRISTI TX 111 RED BLUFF ROAD PASADENA TX 2800 DECKER DR BAYTOWN TX 1795 BURT STREET BEAUMONT TX 2825 SUNTIDE ROAD CORPUS CHRISTI TX 1700 NUECES BAY BOULEVARD CORPUS CHRISTI TX 12000 LAWNDALE ST HOUSTON TX 1320 LOOP 197 S. TEXAS CITY TX 2100 HOUSTON AVE PORT ARTHUR TX 2611 COUNTY ROAD 314 BRAZORIA TX 1801 S. GULFWAY DRIVE PORT ARTHUR TX 5900 HIGHWAY 225 DEER PARK TX 6600 UP RIVER ROAD CORPUS CHRISTI TX 5900 UP RIVER ROAD CORPUS CHRISTI TX 9701 MANCHESTER HOUSTON TX LOOP 197 SOUTH AND 14TH ST TEXAS CITY TX 474 West 900 North SALT LAKE CITY UT 2351 N 1100 W SALT LAKE CITY UT 2355 South 1100 West WOODS CROSS UT 333 W CENTER ST NORTH SALT LAKE UT 393 South 800 West Woods Cross UT 2201 GOODWIN NECK RD GRAFTON VA 1 ESTATE HOPE CHRISTIANSTED VI 4519 GRANDVIEW RD BLAINE WA 8505 SOUTH TEXAS ROAD ANACORTES WA 10200 W MARCH POINT RD ANACORTES WA 3901 UNICK RD FERNDALE WA 3001 MARSHALL AVE TACOMA WA

### 2407 STINSON AVE SUPERIOR WI

ROUTE 2 SOUTH NEWELL WV 2700 EAST 5TH STREET CHEYENNE WY 5700 E. HWY. 20/26 CASPER WY 2070 Hwy 59 Douglas WY 2990 COUNTY RD. 180 EVANSTON WY 100 E LINCOLN AVE SINCLAIR WY 740 W MAIN STREET NEWCASTLE WY

### COUNTY_NAME ZIPCODE

North Slope Borough 99734 North Slope Borough 99734 Fairbanks North Star Borough 997051239 Valdez-Cordova Census Area 996863389 Kenai Peninsula Borough 99611 Fairbanks North Star Borough 99705 Mobile County 36571 Escambia County 36502 Tuscaloosa County 35401 Union County 71762 Union County 71730 Los Angeles County 90745 Los Angeles County 90245 Contra Costa County 94801 Kern County 93308 Contra Costa County 94553-0000 Los Angeles County 90744 Los Angeles County 90805 Los Angeles County 905092929 Santa Barbara County 93454 Los Angeles County 90744 Kern County 93307 Los Angeles County 90723 Kern County 93308 Los Angeles County 90745 Los Angeles County 90744 Contra Costa County 94572 San Luis Obispo County 93420 Contra Costa County 94553 Los Angeles County 90744 Solano County 94510 Los Angeles County 90280 Adams County 80022 New Castle County 19706 Chatham County 31408 Honolulu County 96707 Honolulu County 96707 Will County 60439 Will County 60410 Crawford County 62454 Madison County 62084 Lake County 46394 Posey County 47620 Montgomery County 67337 McPherson County 67460 Butler County 67042

### Boyd County 41129

Pulaski County 42501 Calcasieu Parish 70616 Calcasieu Parish 70605 Calcasieu Parish 70601 Calcasieu Parish 70669 East Baton Rouge Parish 70805 St. Bernard Parish 70043 St. John the Baptist Parish 70051 St. James Parish 70723 St. Charles Parish 70079 St. Bernard Parish 70075 St. Charles Parish 70079 West Baton Rouge Parish 70767 Plaquemines Parish 70037 St. Landry Parish 70750 Webster Parish 71018 Bossier Parish 71067 Caddo Parish 71133-3099 Wayne County 482171294 Dakota County 55068 Washington County 55071 Jackson County 395813201 Warren County 39183 Jones County 39477 Yellowstone County 59044 Yellowstone County 59101 Yellowstone County 59101 Cascade County 59404 Morton County 58554 Middlesex County 07064 Middlesex County 08861 Gloucester County 08066 Union County 07036 Gloucester County 08066 McKinley County 87347 Eddy County 88210 Lea County 88260 Nye County 89301 Lucas County 43616 Stark County 44706 Allen County 45804 Lucas County 43616 Kay County 74601-7501 Garvin County 73098 Tulsa County 74107 Tulsa County 74107

### Carter County 73401

Custer County 73669 Delaware County 19061 Philadelphia County 19145 Delaware County 19061 McKean County 16701 Warren County 16365-3224 Shelby County 38109 Bexar County 78223 Howard County 79721 El Paso County 79905 Smith County 75702 Hutchinson County 79007 Live Oak County 78071 Moore County 79086 Jefferson County 77640 Galveston County 77590 Nueces County 78407 Nueces County 78409 Nueces County 78407 Harris County 77501 Harris County 77520 Jefferson County 77701 Nueces County 78409 Nueces County 78408 Harris County 77017 Galveston County 77590 Jefferson County 77640 Brazoria County 77422 Jefferson County 77640 Harris County 77536 Nueces County 78409 Nueces County 78412 Harris County 77012 Galveston County 77590 Salt Lake County 841031494 Salt Lake County 84116 Davis County 84087 Davis County 84054 Davis County 84087 York County 23692 St. Croix 00820 Whatcom County 98230 Skagit County 98221 Skagit County 98221 Whatcom County 98248 Pierce County 98421

### Douglas County 54880

Hancock County 26050 Laramie County 82007 Natrona County 82609 Converse County Uinta County 82930 Carbon County 82334 Weston County 82701

### ICR_ID Indicate if the sample was collected before or after the desalter Avg Higher Heating Value (Btu/lb) Avg Density (lb/ft3) Avg API Gravity AK5A0050 N/A 18,855 56.84 23.80 AK5A0090 After 19,715 52.03 38.47 AL3C0030 After 18,167 51.24 40.88 AL3D0010 After 19,000 49.76 45.93 AL3D0020 After 18,578 57.62 21.78 AR3D0100 Before 19,233 56.91 23.85 AR3DO110 Before 18,250 49.40 48.54 CA5A0120 Before 19,194 54.44 30.76 CA5A0190 Before 17,779 59.97 15.83 CA5A0200 N/A 20,922 61.03 13.00 CA5A0210 Before 16,829 58.69 18.93 CA5A0220 N/A 19,137 54.47 30.70 CA5A0230 Before 18,343 56.94 23.56 CA5A0310 Before 16,629 56.80 23.97 CA5A0330 N/A 16,883 58.25 19.83 CO4A0340 Before 18,714 52.61 36.36 DE1A0360 Before 18,924 55.41 27.83 IL2A0400 Before 17,821 55.62 27.23 IL2A0410 After 18,300 57.02 23.33 IL2A0420 After 19,161 52.82 35.60 IN2A0440 After 19,421 54.03 32.04 IN2A0450 Before 18,790 53.10 34.08 KS2C0460 Before 18,829 53.13 34.67 KS2C0470 After 19,385 53.99 31.58 KS2C0480 After 18,919 54.79 29.63 KY2A0490 After 19,125 53.25 34.30 LA3C0520 Before 17,899 50.96 40.40 LA3C0560 After 17,439 54.75 30.00 LA3C0590 After 17,220 54.87 29.38 LA3C0600 After 16,778 57.22 22.92 LA3C0610 After 18,887 54.73 29.83 LA3C0620 After 18,910 54.85 29.34 LA3C0630 After 19,256 53.85 32.40 LA3C0640 After 18,971 53.99 31.87 LA3C0670 After 18,918 53.63 32.88 LA3C0700 Before 17,628 52.45 36.77 LA3D0530 Before 19,567 51.15 50.83 LA3D0540 Before 17,271 57.66 21.60 LA3D0660 Before 18,699 52.10 37.93 MI2A0710 After 18,685 53.43 33.77 MN2B0720 After 19,576 56.36 25.37 MN2B0730 After 18,927 54.52 30.82 MS3D0750 N/A 19,200 57.18 21.30 MS3D0760 After 18,487 59.08 17.89

### MT4A0770 Before 19,417 56.92 23.52

MT4A0790 N/A 18,172 56.12 25.83 MT4A0800 After 18,185 56.31 25.30 NJ1A0820 N/A 19,133 56.42 25.07 NJ1A0860 After 18,986 54.27 31.07 NM3E0880 After 19,547 50.59 43.03 NM3E0890 After 19,201 53.30 34.07 NM3E0891 After 19,338 52.83 35.53 NV5A0810 N/A 18,737 7.59 24.03 OH2A0910 Before 19,195 54.47 30.68 OH2A0920 After 19,025 52.97 35.23 OH2A0930 After 18,401 51.98 37.87 OH2A0940 After 19,452 52.21 37.58 OK2C0960 Before 19,400 52.02 38.33 OK2C0970 After 19,584 52.46 36.78 OK2C0980 After 19,753 52.43 36.80 OK2C0990 Before 19,501 52.75 35.79 PA1A1020 Before 19,363 52.53 36.33 PA1A1030 After 19,317 53.93 32.32 PA1B1010 Before 19,221 66.67 1.00 PA1B1050 After 13,123 55.37 28.03 TN2A1060 Before 19,389 51.66 39.36 TX3A1080 After 18,945 53.92 32.47 TX3A1120 After 19,209 51.72 39.18 TX3A1190 After 19,100 51.42 40.12 TX3A1290 Before 19,457 54.73 30.05 TX3A1300 Before 19,743 50.63 42.25 TX3B1110 Before 19,455 54.48 30.68 TX3B1130 Before 18,738 57.37 22.49 TX3B1150 After 22,333 52.57 34.20 TX3B1160 Before 18,743 55.75 26.93 TX3B1170 Before 18,491 53.38 34.06 TX3B1180 After 19,795 53.34 34.20 TX3B1181 After 19,701 50.86 41.57 TX3B1200 After 18,654 58.03 20.69 TX3B1210 After 19,368 50.76 42.43 TX3B1220 Before 19,286 53.64 33.05 TX3B1250 Before 18,267 57.99 20.18 TX3B1310 N/A 19,741 51.42 40.25 TX3B1320 After 19,594 52.47 36.72 TX3B1330 Before 18,814 56.37 25.18 UT4A1360 N/A 19,988 51.50 39.53 UT4A1370 Before 19,678 51.63 39.47 UT4A1380 After 19,683 50.54 43.13 VI6A1530 Before 19,017 54.76 29.93 WA5A1400 After 19,685 54.69 30.00 WA5A1410 Before 19,090 54.15 31.47

### WA5A1440 After 19,000 54.53 30.50

WI2B1460 After 18,700 55.24 28.67 WV1B1450 After 19,806 50.67 42.60 WY4A1470 Before 18,276 55.06 29.07 WY4A1480 After 18,594 52.18 37.87 WY4A1490 N/A 18,949 51.40 40.23 WY4A1500 N/A 19,750 47.37 54.60 WY4A1510 Before 18,565 53.75 32.97 WY4A1520 After 19,321 51.49 39.97

### DL for

Mercury Avg Mercury,

ppmw DL for ChlorineAvg Chlorine, ppmw DL for SulfurAvg Sulfur, ppmw BDL 0.020 BDL 198 ADL 63,130 BDL 0.050 ADL 1.00 ADL 10,067 BDL 0.007 BDL 8.17 ADL 1,553 BDL 0.007 ADL 25.3 ADL 3,067 BDL 0.008 DLL 78.1 ADL 345 BDL 0.004 DLL 37.2 ADL 7,043 DLL 0.005 DLL 27.2 DLL 8,740 BDL 0.050 ADL 1.00 ADL 16,567 BDL 0.045 ADL 64.5 ADL 13,478 BDL #DIV/0! ADL 340 ADL 54,667 BDL #DIV/0! DLL 76.0 ADL 34,000 BDL #DIV/0! DLL 54.7 ADL 5,300 BDL 0.005 DLL 69.0 DLL 13,360 BDL #DIV/0! DLL 55.0 ADL 14,333 BDL #DIV/0! ADL 17.0 ADL 14,633 ADL 0.00 DLL 12.7 ADL 10,722 BDL 0.050 ADL 62.3 ADL 14,199 BDL 0.025 BDL 100 ADL 28,900 ADL 0.007 DLL 340 ADL 18,000 ADL 0.002 ADL 37.6 ADL 7,130 BDL 0.050 ADL 1.00 ADL 15,511 DLL 0.002 ADL 2.60 ADL 2,864 BDL #DIV/0! BDL #DIV/0! ADL 11,314 BDL #DIV/0! ADL 137 DLL 8,768 BDL #DIV/0! DLL 22.0 ADL 16,747 DLL 0.003 ADL 8.03 ADL 11,333 BDL #DIV/0! ADL 263 ADL 1,600 BDL #DIV/0! ADL 261 ADL 11,469 BDL 0.050 ADL 94.8 ADL 20,083 BDL 0.050 ADL 105 ADL 18,467 BDL 0.001 DLL 8.92 ADL 19,850 BDL 0.008 DLL 24.3 ADL 24,882 BDL 0.117 ADL 45.5 ADL 3,746 BDL 0.050 ADL 3,475 ADL 9,875 BDL 0.050 BDL 2.50 ADL 0.986 BDL 0.050 ADL 242 DLL 2,167 ADL 0.068 BDL 2.00 DLL 11.1 BDL 0.050 ADL 86.9 ADL 23.3 DLL 0.009 ADL 24.1 ADL 6,757 BDL 0.001 ADL 20.8 ADL 14,160 BDL 0.050 ADL 1.00 ADL 33,500 BDL 0.019 DLL 37.0 ADL 12,561 BDL 0.003 BDL 8.00 ADL 6,240 BDL 0.008 DLL 84.3 ADL 416

### BDL 0.020 DLL 18.7 ADL 24,665

BDL 0.500 BDL 100 ADL 27,956 BDL #DIV/0! BDL #DIV/0! ADL 26,667 BDL 0.016 DLL 49.7 BDL 1,567 BDL 0.050 ADL 77.7 ADL 20,294 ADL 0.039 DLL 24.3 ADL 1,136 BDL 0.018 ADL 121 ADL 13,405 BDL 0.017 ADL 150 ADL 10,693 DLL 0.041 BDL 250 ADL 15,922 BDL 0.050 ADL 1.00 ADL 20,883 ADL 0.005 DLL 6.43 ADL 11,697 DLL 0.002 DLL 1.97 ADL 5,178 BDL 0.050 ADL 55.0 ADL 3,275 BDL #DIV/0! ADL 262 ADL 6,838 BDL 0.013 ADL 149 ADL 8,157 BDL 0.013 ADL 309 ADL 3,860 BDL #DIV/0! ADL 2.01 ADL 13,220 BDL 0.050 ADL 52.5 ADL 1,621 BDL 0.050 ADL 37.1 ADL 1,625 BDL 0.010 ADL 485 ADL 377 BDL 0.018 ADL 90.1 ADL 21,933 BDL #DIV/0! ADL 179 ADL 3,587 ADL 0.003 BDL 5.00 ADL 1,663 BDL 0.019 DLL 23.0 ADL 5,039 DLL 0.032 ADL 54.2 ADL 4,677 BDL #DIV/0! ADL 188 ADL 3,972 BDL #DIV/0! ADL 222 ADL 2,480 BDL 0.050 ADL 1.00 ADL 12,580 BDL 0.015 DLL 586 ADL 20,883 ADL 0.100 ADL 0.250 ADL 0.273 BDL 0.019 ADL 39.9 ADL 20,194 BDL 0.020 ADL 15.5 ADL 14,980 BDL 0.050 ADL 1.00 ADL 1.09 BDL 0.050 ADL 1.00 ADL 0.193 BDL 0.050 ADL 80.6 ADL 16,893 ADL 0.020 DLL 6.00 ADL 1,593 BDL 0.008 ADL 161 ADL 20,442 BDL #DIV/0! ADL 33.0 ADL 34,330 BDL #DIV/0! ADL 169 ADL 5,737 BDL #DIV/0! ADL 121 ADL 6,663 BDL 0.008 ADL 86.5 ADL 23,823 BDL 0.020 BDL 250 BDL 250 BDL #DIV/0! ADL 155 ADL 456 ADL 0.027 ADL 2.21 ADL 3,110 BDL #DIV/0! BDL #DIV/0! ADL 8,500 BDL 0.050 ADL 1.00 ADL 10,833 BDL 0.008 DLL 79.3 ADL 11,080

### DLL 0.019 DLL 110 ADL 8,000

BDL 0.020 DLL 566 ADL 14,767 BDL 0.050 ADL 87.8 ADL 676 DLL 0.003 DLL 2.93 ADL 23,040 BDL #DIV/0! BDL #DIV/0! ADL 1,900 BDL #DIV/0! DLL 13.0 ADL 700 BDL 0.032 DLL 311 DLL 1,414 BDL 0.350 DLL 166 ADL 12,724 BDL 0.050 ADL 50.9 ADL 1,806

### DL for AntimonyAvg Antimony, ppmw DL for ArsenicAvg Arsenic, ppmw DL for BerylliumAvg Beryllium, ppmw BDL 0.490 BDL 1.23 BDL 0.490 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.642 BDL 0.421 BDL 0.128 BDL 0.718 BDL 0.492 BDL 0.143 DLL 1.05 BDL 0.470 BDL 0.276 DLL 0.285 DLL 0.127 BDL 0.025 ADL 0.173 DLL 0.117 BDL 0.025 BDL 0.500 BDL 0.500 BDL 0.500 BDL 11.8 BDL 2.34 BDL 2.34 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.050 DLL 0.127 BDL 0.050 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.500 DLL 1.07 BDL 0.500 BDL 1.09 BDL 0.438 BDL 0.438 BDL 0.250 BDL 0.050 BDL 0.100 ADL 0.257 DLL 0.083 BDL 0.0001 BDL 0.025 DLL 0.053 BDL 0.025 BDL 0.500 BDL 0.500 BDL 0.500 DLL 0.005 ADL 0.064 BDL 0.001 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.025 DLL 0.102 BDL 0.025 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.500 BDL 0.500 BDL 0.250 BDL 0.500 BDL 0.500 BDL 0.250 BDL 0.025 BDL 0.025 BDL 0.025 BDL 0.472 BDL 0.469 BDL 0.235 BDL 1.04 BDL 0.417 BDL 0.417 BDL 0.530 BDL 0.267 BDL 0.025 BDL 0.597 BDL 0.298 BDL 0.030 BDL 1.50 BDL 1.50 BDL 0.750 DLL 0.166 BDL 0.018 BDL 0.018 BDL 1.00 BDL 1.00 BDL 0.500 BDL 0.050 DLL 0.117 BDL 0.050 BDL 0.025 DLL 0.053 BDL 0.025 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.491 BDL 1.23 BDL 0.491 DLL 0.100 DLL 0.151 BDL 0.025 BDL 0.467 BDL 0.467 BDL 0.233

### BDL #DIV/0! BDL #DIV/0! BDL #DIV/0!

BDL 2.50 BDL 2.50 BDL 2.50 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 1.02 BDL 1.02 BDL 0.102 BDL 1.15 BDL 0.458 BDL 0.458 ADL 0.975 ADL 2.44 ADL 0.975 BDL 0.500 BDL 0.500 BDL 0.100 BDL 0.500 BDL 0.500 BDL 0.100 BDL 0.864 BDL 0.540 BDL 0.432 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.025 BDL 0.025 BDL 0.025 BDL 0.001 ADL 0.007 BDL 0.001 BDL 0.625 BDL 0.250 BDL 0.250 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.500 BDL 0.500 BDL 0.100 BDL 0.500 BDL 0.500 BDL 0.100 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 1.25 BDL 0.500 BDL 0.500 BDL 1.25 BDL 0.500 BDL 0.500 DLL 1.93 ADL 2.70 BDL 0.250 BDL 0.500 BDL 2.50 BDL 2.50 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.500 BDL 0.417 BDL 0.500 BDL 0.489 BDL 1.22 BDL 0.489 DLL 0.102 BDL 0.066 BDL 0.033 DLL 0.266 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.500 BDL 0.500 BDL 0.500 BDL 2.75 BDL 2.75 BDL 0.55 ADL 15.8 ADL 2.50 ADL 2.50 BDL 0.489 BDL 1.22 BDL 0.489 BDL 0.025 BDL 0.025 BDL 0.025 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.833 BDL 0.500 BDL 0.333 BDL 0.025 BDL 0.025 BDL 0.025 BDL 0.483 BDL 0.483 BDL 0.243 DLL 0.005 DLL 0.007 DLL 0.052 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.411 BDL 0.411 BDL 0.205 BDL 0.983 BDL 0.615 BDL 0.492 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! ADL 1.00 ADL 1.00 ADL 0.200 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.413 BDL 0.413 BDL 0.208

### BDL 1.40 BDL 1.40 BDL 0.118

BDL 0.478 BDL 0.240 BDL 0.024 BDL 1.25 BDL 0.500 BDL 0.500 ADL 0.004 ADL 0.009 BDL 0.001 BDL #DIV/0! DLL 0.325 BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.804 BDL 0.493 BDL 0.415 BDL 1.94 BDL 1.78 BDL 1.78 BDL 0.833 BDL 0.333 BDL 0.333

### DL for CadmiumAvg Cadmium, ppmw DL for

ChromiumAvg Chromium,

ppmw DL for CobaltAvg Cobalt, ppmw DL for Lead BDL 0.490 BDL 1.97 BDL 1.97 BDL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.160 BDL 0.320 BDL 0.320 DLL BDL 0.180 BDL 0.360 BDL 0.360 DLL BDL 0.276 BDL 0.470 BDL 2.35 BDL BDL 0.025 ADL 0.343 ADL 0.324 ADL DLL 0.030 ADL 0.219 DLL 0.104 ADL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 1.18 BDL 1.18 BDL 1.18 BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.050 DLL 0.200 DLL 1.40 DLL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! ADL 3.00 BDL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.438 BDL 0.438 BDL 0.438 BDL BDL 0.100 BDL 0.250 BDL 0.250 BDL DLL 0.004 ADL 0.069 ADL 0.047 ADL BDL 0.025 BDL 0.025 DLL 0.067 DLL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.001 ADL 0.040 DLL 0.007 DLL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.025 BDL 0.025 DLL 0.072 DLL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.250 BDL 0.250 BDL 0.250 BDL BDL 0.250 BDL 0.250 BDL 0.250 BDL BDL 0.025 DLL 0.055 ADL 0.190 BDL BDL 0.235 BDL 0.468 BDL 2.35 BDL BDL 0.417 BDL 0.417 BDL 0.417 BDL BDL 0.133 BDL 0.267 BDL 0.267 BDL BDL 0.148 BDL 0.298 BDL 0.298 BDL BDL 0.750 BDL 0.750 BDL 0.750 BDL DLL 0.042 ADL 0.150 BDL 0.018 ADL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.050 DLL 0.133 DLL 0.100 DLL BDL 0.025 DLL 0.087 DLL 0.067 DLL BDL 0.500 BDL 0.500 BDL 0.500 DLL BDL 0.491 DLL 3.61 BDL 1.96 BDL BDL 0.025 ADL 0.250 ADL 0.146 DLL BDL 0.233 DLL 1.02 BDL 2.33 BDL

### BDL #DIV/0! DLL 2.26 BDL #DIV/0! BDL

BDL 0.500 BDL 2.50 BDL 2.50 BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.255 BDL 0.495 BDL 2.55 BDL BDL 0.458 BDL 0.458 BDL 0.458 BDL ADL 0.975 ADL 3.90 ADL 3.90 ADL BDL 0.100 BDL 0.250 BDL 0.500 BDL BDL 0.100 BDL 0.250 BDL 0.500 BDL BDL 0.184 BDL 2.16 BDL 0.292 BDL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.025 DLL 0.057 DLL 0.090 DLL DLL 0.003 ADL 0.057 ADL 0.032 ADL BDL 0.250 BDL 0.250 BDL 0.250 BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.100 BDL 0.250 BDL 0.500 BDL BDL 0.100 BDL 0.250 BDL 0.500 BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.250 ADL 4.09 BDL 1.00 BDL BDL 0.500 BDL 0.500 BDL 2.50 BDL BDL #DIV/0! DLL 0.268 BDL #DIV/0! BDL BDL 0.417 BDL 0.417 BDL 0.500 DLL BDL 0.489 BDL 1.95 BDL 1.95 BDL DLL 0.107 ADL 0.276 DLL 0.182 ADL DLL 0.013 DLL 0.160 DLL 0.112 BDL DLL 0.174 BDL #DIV/0! BDL #DIV/0! DLL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.550 BDL 1.38 BDL 2.75 DLL ADL 2.50 ADL 2.50 ADL 2.50 ADL BDL 0.489 BDL 1.96 BDL 1.96 BDL BDL 0.025 BDL 0.026 BDL 0.019 BDL BDL 0.500 DLL 1.05 BDL 0.500 BDL BDL 0.500 DLL 1.05 BDL 0.500 BDL BDL 0.333 BDL 0.500 BDL 0.333 BDL BDL 0.025 BDL 0.025 DLL 0.063 DLL BDL 0.243 BDL 0.483 BDL 2.43 BDL BDL #DIV/0! DLL 0.023 DLL 0.007 BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.205 BDL 0.411 BDL 2.05 BDL BDL 0.209 BDL 2.52 BDL 0.332 BDL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL ADL 0.200 ADL 0.500 ADL 1.00 ADL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL 0.500 BDL 0.500 BDL 0.500 BDL BDL 0.208 BDL 0.413 BDL 2.08 BDL

### BDL 0.232 BDL 0.600 BDL 0.232 BDL

BDL 0.064 DLL 0.220 BDL 0.080 DLL BDL 0.500 BDL 0.500 BDL 0.500 BDL DLL 0.002 ADL 0.028 ADL 0.013 ADL BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL BDL #DIV/0! DLL 1.95 BDL #DIV/0! BDL BDL 0.234 BDL 1.67 BDL 0.312 BDL BDL 0.444 BDL 1.78 BDL 1.78 BDL BDL 0.333 BDL 0.333 BDL 0.333 BDL

### Avg Lead,

ppmw DL for ManganeseAvg Manganese, ppmw DL for NickelAvg Nickel, ppmw DL for Selenium 0.490 BDL 1.97 ADL 19.5 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.420 BDL 0.320 BDL 1.28 BDL 0.663 BDL 0.360 BDL 1.43 BDL 0.470 BDL 0.708 DLL 7.63 BDL 0.101 ADL 0.266 ADL 2.87 BDL 0.100 ADL 0.071 ADL 4.57 DLL 0.500 BDL 0.500 BDL 0.500 BDL 2.34 BDL 2.34 ADL 57.4 BDL #DIV/0! BDL #DIV/0! ADL 68.7 BDL #DIV/0! BDL #DIV/0! ADL 48.7 BDL #DIV/0! BDL #DIV/0! ADL 28.0 BDL 0.540 DLL 0.180 DLL 59.4 BDL #DIV/0! BDL #DIV/0! ADL 13.6 BDL #DIV/0! DLL 3.20 ADL 62.2 BDL 0.500 BDL 0.500 DLL 6.36 BDL 0.438 BDL 0.438 ADL 3.44 BDL 0.150 DLL 2.29 DLL 5.03 BDL 0.050 ADL 0.096 ADL 9.80 ADL 0.067 BDL 0.025 ADL 8.85 ADL 0.500 BDL 0.500 BDL 0.500 BDL 0.059 ADL 0.061 ADL 0.757 ADL #DIV/0! BDL #DIV/0! DLL 8.40 BDL #DIV/0! BDL #DIV/0! DLL 5.30 BDL #DIV/0! BDL #DIV/0! ADL 17.3 DLL 0.135 BDL 0.025 ADL 7.37 DLL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! DLL 5.14 BDL 0.500 BDL 0.250 DLL 1.68 BDL 0.333 BDL 0.250 DLL 3.98 BDL 0.025 DLL 0.237 ADL 16.9 ADL 0.468 BDL 0.717 DLL 4.45 BDL 0.417 BDL 0.417 ADL 1.99 BDL 0.267 BDL 0.267 ADL 5.22 BDL 0.298 BDL 0.298 ADL 4.00 BDL 0.750 BDL 0.750 DLL 2.03 BDL 0.465 DLL 0.176 ADL 0.460 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.417 ADL 0.200 ADL 2.75 BDL 0.050 BDL 0.025 ADL 20.5 ADL 1.66 BDL 0.500 BDL 0.500 BDL 0.491 BDL 1.96 DLL 15.0 DLL 0.075 ADL 0.248 ADL 4.13 BDL 0.467 BDL 0.700 DLL 5.93 BDL

### #DIV/0! BDL #DIV/0! ADL 27.4 DLL

2.50 BDL 2.50 ADL 8.11 BDL #DIV/0! BDL #DIV/0! ADL 7.67 BDL 1.02 BDL 0.750 BDL 2.02 BDL 0.458 BDL 0.458 ADL 5.52 DLL 0.975 ADL 3.90 ADL 0.986 ADL 0.500 BDL 0.250 ADL 4.62 BDL 0.500 BDL 0.250 ADL 1.93 BDL 7.73 BDL 0.864 ADL 13.3 BDL 0.500 BDL 0.500 DLL 1.04 BDL 0.190 DLL 0.050 ADL 14.1 ADL 0.009 ADL 0.008 ADL 1.39 ADL 0.250 BDL 0.250 DLL 0.673 DLL #DIV/0! BDL #DIV/0! ADL 3.85 DLL 0.500 DLL 0.609 ADL 3.76 BDL 0.500 BDL 0.250 ADL 2.62 BDL #DIV/0! BDL #DIV/0! ADL 3.22 BDL 0.500 BDL 0.500 ADL 2.64 BDL 0.500 BDL 0.500 ADL 2.27 BDL 1.00 DLL 2.08 DLL 3.76 BDL 0.500 BDL 0.500 ADL 32.0 BDL #DIV/0! BDL #DIV/0! ADL 1.23 BDL 1.11 BDL 0.417 ADL 5.02 BDL 0.489 BDL 1.95 ADL 2.19 BDL 1.09 ADL 0.521 ADL 2.14 BDL #DIV/0! DLL 0.179 ADL 2.00 DLL 0.228 BDL #DIV/0! DLL 0.980 BDL 0.500 BDL 0.500 DLL 1.01 BDL 14.1 BDL 1.38 ADL 28.2 BDL 2.50 ADL 2.50 ADL 4.20 ADL 0.489 BDL 1.96 ADL 24.6 BDL 0.026 BDL 0.025 ADL 1.60 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.333 DLL 1.03 DLL 4.04 DLL 0.063 DLL 0.053 ADL 2.12 DLL 0.483 BDL 0.725 DLL 4.08 BDL #DIV/0! DLL 0.006 ADL 1.40 DLL #DIV/0! DLL 0.114 DLL 1.63 DLL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL 0.411 BDL 0.613 DLL 4.37 BDL 8.63 BDL 0.983 BDL 4.92 BDL #DIV/0! BDL #DIV/0! ADL 3.40 BDL 1.00 ADL 0.500 ADL 1.78 ADL #DIV/0! BDL #DIV/0! ADL 21.3 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.413 BDL 0.617 DLL 3.33 BDL

### 0.700 BDL 0.463 ADL 6.30 BDL

0.477 DLL 0.128 ADL 5.95 BDL 0.500 BDL 0.500 BDL 0.500 BDL 0.051 ADL 0.019 ADL 2.38 ADL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! BDL #DIV/0! ADL 1.10 ADL 7.97 BDL 0.729 BDL 3.25 DLL 1.78 BDL 1.78 DLL 7.10 DLL 0.333 BDL 0.333 BDL 0.333 BDL

### Avg Selenium,

ppmw 0.490 0.500 0.421 0.492 0.470 0.124 0.183 0.500 4.69 #DIV/0! #DIV/0! #DIV/0! 0.050 #DIV/0! #DIV/0! 0.500 0.438 0.250 0.380 0.120 0.500 0.035 #DIV/0! #DIV/0! 0.692 0.082 #DIV/0! #DIV/0! 0.500 0.500 0.112 0.468 0.417 0.530 0.597 1.17 0.092 1.00 0.050 0.143 0.500 0.914 0.105 0.467

### 0.616

2.50 #DIV/0! 1.02 0.945 0.975 0.500 0.500 1.84 0.500 0.127 0.024 0.462 0.600 0.500 0.500 #DIV/0! 0.500 0.500 0.500 0.500 #DIV/0! 0.500 0.489 0.165 0.850 #DIV/0! 0.500 2.75 2.50 0.489 0.025 0.500 0.500 1.03 0.060 0.483 0.011 0.447 #DIV/0! 0.411 2.09 #DIV/0! 1.00 #DIV/0! 0.500 0.413

### 2.32

0.717 0.500 0.016 #DIV/0! 0.600 2.90 3.57 0.333

### Distillation Feed Component **Avg Value Median Value**  **Low High** 

Higher Heating Value (Btu/lb) 18,887 18,991 13,123 22,333 Density (lb/ft3

### ) 53.96 53.99 7.59 66.7 API Gravity 31.23 31.52 1.00 54.6 Avg Mercury, ppmw 0.035 0.018 0.001 0.50 Avg Sulfur, ppmw 10,390 7,825 0.193 63,130 Avg Chlorine, ppmw 107.1 38.8 0.25 3,475 Avg Antimony, ppmw 0.758 0.489 0.0005 15.8 Avg Arsenic, ppmw 0.535 0.417 0.001 2.80 Avg Beryllium, ppmw 0.323 0.135 0.0001 2.50 Avg Cadmium, ppmw 0.257 0.170 0.001 2.50 Avg Chromium, ppmw 0.596 0.309 0.007 4.09 Avg Cobalt, ppmw 0.675 0.417 0.001 3.90 Avg Lead, ppmw 0.774 0.420 0.003 14.1 Avg Manganese, ppmw 0.554 0.327 0.005 3.90 Avg Nickel, ppmw 10.7 4.20 0.123 98.6 Avg Selenium, ppmw 0.618 0.489 0.003 4.69

**Distillation Feed Component** **Avg Value, *ppmw****Avg Value, *mg/bbl** **Sectorwide Throughput 1** 

### (Mg/yr) Avg Mercury* 0.029 4.08 21.8 Avg Sulfur* 11,873 1,649,869 8,798,841 Avg Chlorine*2 

### 97.9 13,604 72,553 Avg Antimony* 0.591 82.3 439 Avg Arsenic* 0.429 59.8 319 Avg Beryllium* 0.269 37.5 200 Avg Cadmium* 0.241 33.4 178 Avg Chromium* 0.428 59.6 318 Avg Cobalt* 0.612 85.3 455 Avg Lead* 0.517 71.8 383 Avg Manganese* 0.468 65.1 347 Avg Nickel* 10.9 1,515 8,078 

### Sectorwide Aggregates **Table V-1: Facility-by-Facility Sector Avgs**

**Table V-2: Weighted Actual Barrel Throughput Sector Avgs**

### Avg Selenium* 0.489 68.0 363

Higher Heating Value (Btu/lb) 18,861 18,861

- Density (lb/ft3

### ) 54.56 54.56

- API Gravity 30.54 30.54

-

Range 0-25 25-30 30-40 >40 Total Count of Facilities 29 24 60 17 130

Range 0-1,000 1,000-7,000 7,000-20,000 >20,000Total Count of Facilities 29 33 46 22 130

Range 0-2.0 2.0-30.0 30.0-100 >100 Total Count of Facilities 15 38 43 30 126

Range 0-0.010 0.010-0.030 0.030-0.050 >0.050 Total Count of Facilities 45 23 30 8 106

Range 0-0.020 0.020-0.100 0.100-1.00 >1.00 Total Count of Facilities 12 23 59 13 107 **Lead (ppmw) Specific Ranges Mercury (ppmw) Specific Ranges**  **Sulfur (ppmw) Specific Ranges API Gravity Specific Ranges**  

## Table V-3: Select Feed Component Ranges and Facility Counts

**Chlorine (ppmw) Specific Ranges** 1: Assumes an annual operating capacity of 16,911,000 bbl/cd at 86.4 % utilization rate (source: EIA, 2010 Operating Year). 2: Error in chlorine content may have been introduced due to samples taken both before and after the desalter. *: All Distillation Feed Component values with this value are in the respective units of the column unless otherwise noted (i.e. Higher Heating Value, Density, and API Gravity).

### Range 0-1.00 1.00-5.00 5.00-20.0 >20.0 Total

Count of Facilities 21 50 34 22 127 **Nickel (ppmw) Specific Ranges**