**FORM A -1** 

**COMPA NY INFORMA**  **TION**

**I. Parent Company / Legal Corporate Owner Information**

1. Legal Parent Company / Legal Corporate Name Example Resins 2. Mailing Address 123 Example Resins Rd 3. City Any town 4. State North Carolina 5. Zip Code 28590 6. County Any County

501-750 7. Size of Com pany

(approximate number of employees including all subsidiaries, branches, and related establishments owned):



### Page 1 of 1 **DRA FT** PVC Section 114 Survey Part 1 06/23/2009**FORM P**

**PROCESS VENT EMISSIONS TESTING DA TA** 

**Instructions**
1. Copy this worksheet as necessary for pollutants/compounds sampled on different dates. 2. For multiple control devices, users may copy this worksheet within this workbook.

**Control Equipment ID:** Indicate whether the inlet to the control device is from the PVC process only ("dedicated") or from the PVC process and another process unit (non-PVC) ("combined"):

**Parameter**

Test Date (mm/dd/y

y) **Required Operating Parameters During Test** Total Heat Input (MMBtu/hr) Fuel 1 Feed Rate HHV Fuel 2 Feed Rate HHV Fuel 3 Feed Rate HHV Flow Rate Temperature Moisture O2 CO2 Number of PVC resin grades being produced during sampling Number of PVC resin grades being produced (as percentage of all resin grades produced by facility) **Testing Data** Compound Benzene Chloroethane Chloroform Chloroprene 1,1-Dichloroethane 1,2-Dichloroethane n-Hexane Methylene chloride Toluene 1,1,1-Trichloroethane 1,1,2-TrichloroethaneVinylidene chloride

Acetophenone Bis(2-ethylhexyl) phthalate (DEHP) 1,4-Dichlorobenzene 2,4-Dinitrophenol Hexachlorobutadiene Hydroquinone Naphthalene Phenol 1,2,4-Trichlorobenzene Acetaldehyde 1,3-Butadiene Chlorobenzene Chloromethane Cumene Ethylbenzene Ethylene glycol Formaldehyde Methanol 1,1,2,2-Tetrachloroethane 2,2,4-Trimethylpentane Vinyl acetate Vinyl bromide Xylenes (isomers and mixtures) Vinyl chloride Methane (CH4)C-2

Combined

**CA S Number**  **Run #1 Run #2**  **Run #3 Units** 
Enter the CAS number for each pollutant/compound. Do not include dashes. Select appropriate unit from list.

4/1/2014 4/1/2014 4/1/2014

19.6 17.1 15.9 MMBTU/hr Natural Gas Natural Gas Natural Gas

19.6 17.1 15.9 MMBTU/hr 337 337 337 BTU/scf

MMBTU/hr BTU/scf

MMBTU/hr BTU/scf 8790.1 8867.3 8930.8 dscfm 451 447 457 deg F 15.1 14.9 14.5 % 6.7 5.9 7.05 % 8.7 8.9 8.7 % 1 1 1 20 20 20 %

CAS Number 71432 0.02 0.02 0.02 ppm vd @ 3% O2 75003 0.005 0.005 0.005 ppm vd @ 3% O2 67663 0.05502 0.00429 0.55921 ppm vd @ 3% O2 126998 0.47091 0.84152 0.48407 ppm vd @ 3% O2 75343 0.34632 0.22430 0.63035 ppm vd @ 3% O2 107062 0.23618 0.10824 0.31487 ppm vd @ 3% O2 110543 0.61394 0.00318 0.04897 ppm vd @ 3% O2 75092 0.28723 0.77804 0.74157 ppm vd @ 3% O2 108883 0.08046 0.05573 0.30012 ppm vd @ 3% O2 71556 0.16892 0.95882 0.95167 ppm vd @ 3% O2 79005 0.32749 0.35141 0.42412 ppm vd @ 3% O2 Enter numerical value only.

Enter numerical value only

.75354 0.31693 0.34155 0.02419 ppm vd @ 3% O2

98862 0.46181 0.89753 0.21937 ppm vd @ 3% O2 117817 0.73100 0.84955 0.84679 ppm vd @ 3% O2 106467 0.76541 0.38040 0.60674 ppm vd @ 3% O2 51285 0.02045 0.12233 0.15984 ppm vd @ 3% O2 87683 0.44470 0.85413 0.92067 ppm vd @ 3% O2 123319 0.03777 0.56408 0.40106 ppm vd @ 3% O2 91203 0.78022 0.00196 0.80266 ppm vd @ 3% O2 108952 0.26708 0.18864 0.19807 ppm vd @ 3% O2 120821 0.40474 0.39410 0.81911 ppm vd @ 3% O2 75070 0.95814 0.35858 0.46405 ppm vd @ 3% O2 106990 0.09809 0.74534 0.87695 ppm vd @ 3% O2 108907 0.09093 0.29692 0.92321 ppm vd @ 3% O2 74873 0.56775 0.35855 0.13606 ppm vd @ 3% O2 98828 0.67384 0.28638 0.23619 ppm vd @ 3% O2 100414 0.23047 0.93697 0.09574 ppm vd @ 3% O2 107211 0.65432 0.42177 0.24037 ppm vd @ 3% O2 50000 0.89907 0.94252 0.35415 ppm vd @ 3% O2 67561 0.16015 0.99542 0.78944 ppm vd @ 3% O2 79345 0.18766 0.64299 0.27044 ppm vd @ 3% O2 540841 0.94718 0.64250 0.78853 ppm vd @ 3% O2 108054 0.59784 0.89953 0.09221 ppm vd @ 3% O2 593602 0.36167 0.72758 0.28526 ppm vd @ 3% O2 1330207 0.98577 0.41794 0.58376 ppm vd @ 3% O2 75014 0.03283 0.84356 0.75999 ppbvd @ 3% O2 74828 1.22400 0.99840 1.11340 ppm vd @ 3% O2**Run # 1 Detection Run # 2 Detection**  **Run # 3 Detection**

Identify the status of measured values relative to the detection

levels Identify the status of measured

values relative to the detection

levels Identify the status of measured

values relative to the detection

levels

BDL BDL DLL BDL BDL BDL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADLADL ADL ADL

ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL ADL**An alysis M**  **ethod Used Note(s)** 

Wh ere applicable, select the analysis method

used. For all pollutants/compounds, provide any other information supporting information you think is necessary about this test report.

SW-846 Method 8260B Reporting average concentration; runs #1 and #2 are BDL. SW-846 Method 8260B All 3 runs are BDL. SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260B SW-846 Method 8260BSW-846 Method 8260B

SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D SW-846 Method 8270D US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18 US EPA Method 18**FORM Q**

**TOTA L HYDROCA** **RBON 30-DA Y MONITORING** 

**Instructions**
1. For multiple control devices, users may copy this worksheet within this workbook. 2. Add additional rows as necessary to provide 30 days of monitoring data.

**Control Equipment ID:**

**Date and Time THC Reading**  **CH4 Reading O2 level in exhaust gas** 

MM/DD/YYYY HH:MM (ppmvd as propane @ 3% O2) (ppmvd @ 3% O2) (% by volume, dry)

04/01/2014 15:00 27.4 1.56 8 04/01/2014 15:15 30.2 1.24 10 04/01/2014 15:30 40.5 1.33 5 04/01/2014 15:45 20.6 1.78 6 04/01/2014 16:00 20.3 1.15 8 04/01/2014 16:15 28.9 1.14 9 04/01/2014 16:30 35.1 1.67 10 04/01/2014 16:45 30.2 1.63 8 04/01/2014 17:00 32.7 1.64 6 04/01/2014 17:15 25.4 1.27 5 04/01/2014 17:30 29.4 1.23 10 Indicate whether the inlet to the control device is from the PVC process only ("dedicated") or from the PVC process and another process unit (non-PVC) ("combined"):C-2

Combined

**Moisture in exhaust gas**  **PVC Type PVC Grade**  **Control Device Temperature** 

(% by volume) (e.g., suspension, dispersion/emulsion, bulk, etc.) (e.g., GP, HMW , LMW , etc.) (degF)

17 Suspension HMW 469 18 Suspension HMW 473 12 Suspension HMW 461 16 Suspension HMW 494 13 Suspension HMW 455 10 Suspension HMW 480 11 Suspension HMW 452 13 Suspension HMW 450 20 Suspension HMW 459 13 Suspension HMW 470 17 Suspension HMW 488**Control Device**

**Operations Indicator THC Monitoring**  **Operations Indicator** (note periods of start-up, Shutdown, malfunctions, or normal operation) (note periods of abnormal operations)
Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal Normal