05/i9/1998 15:54 2165268555 

21G52~ '15 ENUISAGE 

POST OFnCE BOX 152 

RICWtELD, OHIO 4-&286 

Tel: (.&40)-526-0990 

Fu: (.&40r526-&5!.$ 

Internet: bttp:/!www.enviJage-env.c:orn 

LmaiJ: envisage-env@eDvisage-env.cOID 

PAGE 01 

CQwfPLETE FACILITY EVALUATIONS 

-.--------------______ ~~~ __ • ~ __ --~y-~'~·-··._'~"'~) ... ~n-... c-.. '-... '-"~. __ .. ~"._' ... _ .. __ __ 

G STACK SAMPUNG 

G ENVIRONMENTAL AUOITS 

G NPOeS PERMITTING 

G SOURCE PERMITTING 

G ENVIRONMENTAL SITE ASSESSMENTS 

e;; TITL.2 V EMISSION STUOfES 

e; HAZARO COMMUNICAnON 

a; SARA TITlE IIf 

G INOUSTFUAL HYGIENE 

G INDOOR AIR MONITORING 

~b ____________________________ ~ •• ~ __________ ~~)_?tX~ •• W.=_=M'M~l'_=MrM.~'P~ .. __ ___ 

To: [ ___ r~=-----_'2~. ~~~d ________ --.J 

Fax #: ~I _:Z_I~~· -_ts:I..d~~8_-_<-I.....:..~~7~9~ ____ --, 

Date: tl.o-_~:.;-;.../9-y-!t~2:::....-______ ---' 

( 

Pages: I Including cover· ] 

Notes:j '--___ -------'] 

. . . 

Confld~h.lity Notice: This fllc5im.l. tntnsmissicn may eonl~in connC:entlal inronnatlon and is SQlely flgt the UN erCh. btMcNIl idtn!f'l~ as, :r~ 

reeiFient. I' you ~re net ::~I intCt'tded rllC;pient. you ~r. hear by notified trlat .ny dissemination. dl.tnb~l~n, UN or COPJ of ~ r.ce!miI. IS Slr:l;: I 

prohibited. Ir you receilfe thl$ :ran5mission in etrOt. pI.IM notify US imm~tely. or rerum the Innsm/So$iCl1 to US. the U.S. Mail. 
05/19/1998 15:54 2165268555 ENUISAGE PAGE 02 

MAY-l'9-'98 TUE 

AMERICAN ANALYTICAL LA SORA TORIES, IN r840 SOUTH MAIN STREET 

AKRON. OHIO 44311-1516 

(330) 535-1300 

FAX: (330) 536-7246 

TIlE©~DVE~ 

n IIAY 1 9 1998 

"SERVICE IS OUR SCIENCE" 

FAX TRANSMITTAL SHEET 

DATE: __ J_--,-I-,-r_~ ·"""",,2~e ____ _ 

nME; _. ___ 1--..0....,;,.,,;,;::;;:3.-5';......-_____ _ 

TO: 

COMPANY: 

A'TTN: l' .. * 

FAX NO: 

.' 

fRO,.,: 

NAME: 

MEMO:· 

This me$S8gl1 is intended for th. us. of tne individual or entity to which if ;s fldd"S$ed and may 

contain infomration that is ptfv,7eged. confidential attd .r8m~t from diselO$U", If the reeder of 

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the message to th. mtended ffJcipient, you al'8 hereby notified that any trl$$tmln.tlon, 

distribution, or copying of the communlcstion is strictly prohibited. If)'CIu h.". ~eivfld thi$ 

communication ;n error, pleeu notify us immediately by telephone end retum th. ori'iinel 

mflssege to us at the sOove .ddT'8ss via the Unlt~ St.tes Postal SefV;c.. Thank you. 

NOTE: Faxed analyUcal .... utts a" considered preliminary repcrts and .r. subjeet to 

change .fter rwview of .11 lnfonn8tion. 

Page 1 of 

1< B 
65/19/1998 15:54 21&5258555 ENUISAGE 

MAY-19-98 TLlE: 9 .: .. ~.~.~ ..... _., ____ ~ ...... _._. ••• •. 

., 

Initia' Volume 

Final Vol: 

z") . 

Matals Bla,,1< WOr1(sheeC • Water Matnx 

Fuma~M 

mL QC S .. tch: 

, 

--.,flJ ___ •mL PI"1IP 08tlt: 

d~~S-t) 

f.-~G21' 

e!ement I Meas. Cone. LL9IL I Anafysis Oat. -r Analyst 

Ag I I 

As ~~. (/ l/ .. ? 7-9c/' ~ 

Be 

Cd " (? st' s-- '{- PI' ~ 

Cr ,?$".() .s:. y .. p~ J 

Co 

Mo ~s-.tJ r-s .. f"P ~ 

Ni 

Pb ~~.t/ ~-.t? .. ?rI' ~ 

Sb 

Se I 

T1 

I I 

PAGE 63 

P.O= 
ENU I SAGE PAGE 84 

MAY-19-~e. TUE 9:~4 

A",e"ea" ~/'Ialyth:al Laboratories. Inc. 

Metals Chec:k Sc1"'~le Wol1<.sheet 

Fumac:e AA • Water Matmc 

Initial Volume ______ 6P ml. 

QC Satc:.": 

Final VOl: ___ 

S!;> ml. Prep Oatl!: t--< 7-lIl 

element I S~lkQ C.:Inc. J eriK conc.1 C:""IO Cone. J CHK I C;:~ I Oat., & InitIal. 

I!;lL "gil. ~qlL %~ 

Ag I J 

A$ .tt? Zl CJ7 2.<./p lIt? lit? f-c7~ 

Be 

Cd ,w /9. .. 9 1'1.¥ 9tf? 9p .s--y~ 

Cr ~ lj),<, tp.;:' . /f)/ IP~ i 

Cc 

Mo II? jC;., 9,~d" J()/ 99 s--.s-~ 

Ni 

Pb ~ 19 J? 1~9f/ 97 I 9J- f' .. ~ 9 ~ 

Sb 

Se I 

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I I I 

I I I I I I 

I I I I 

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P _ 03: 
II 

05/19/1998 15:54 2165268555 ENUISAGE PAGE OS 

MAY-19-98 TU~ 9:3~ 

..lmencat1 .l.naJYtlc::::ll Woor.1tcnes. Inc. 

MeQ&a M4IaTX SQlk. S~CI. 'Norxsnlte' 

.' .=:o.lrnac::! AA .. Water Matmc 

QC Saa:r. 4t' 5$0, 

Inr031 Valum. 5P tnt. ~ntG Oone; ~--? r -.9? 

;::O:"a, Vot: fl? ""1. S#"g'.IO: J 6~-t:>/ / 3.3/-01 .. &As: , 

e~enr I IntUaI C~ne. { Sfltk. C~"c:.1 M5 C:nc. } MSO Cln~ I MS J MSC I Oaw ~ 'nrUaiS 

1&411. JJQll. .:qL .u;lL. ~~ %~ 

Aq I I I I I 

As f?,7.t? I W ,2 /. 7j.:J ?/lr? r /1)7 /09' 4" ... ~? ~ 

Se } .. I 

Cd I 

Cr I z#_ Sf It? J1~ 3.6· .~ ItA/' ICD ~-t)y~ 

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Pb I I I 

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I I I f I ~ . 

I I I I I I I 

I I I J I r I 

t I I I I I 
AGENCY USE ONLY 

Date Received 

No, Assigned 

Premise No. 

A. Facility Information 

Namo Diamond Hard Chrome Inc. 

Contact Person Robert Tonkovich 

B. Testing Firm Information 

INTENT TO TEST NOTIFICATION 

(One source per sheet) Proposed Test Dato: 

I • " , ,,"v C'L:.e ;'.. Pre-test Meeting Desired? 

-r>;;s '/ ~ ; . . I. ,- ~,' :~·il(/. r.:/: /\':1, (f-); / • .1) IA"I:. ('/ 

h (-:// ,/. : I I. ~{ (,' J' ,;--~ . '/ /I / ,it /.~. ',r I. ....... ~ _ t~.·( L,., - I "-- t.... \. t. .. -.J " __ -L.,'.,,I I.' -.,-j 

/t i /, \,,-' I ,f 

Address 6110 Grand Avenue 

Cleveland, Ohio 44104 

T alaphone 216·391-3618 

Nome Envisage Environmental, Incorporated Address P.O. Box 152 

Richfield, Ohio 44286 

Contact Person Mr. Tyson Houchin Telephone 440-526·0990 

C. Test Plan and Emissions Unit Information Table: List the applicable information ullIJor Hitch respoctive column hltading. 

Emissions Unit II 

Chrome Plating Tanks II's 4,5 &6 

D. What is the rated capacity? 

Control 

Equipmenl 

Chrome Scrubber #2 

Monitoring 

Equipment 

Velocity Pressure 

Gauges 

PoUutantCs) 

To Be Tostad 

T otel Chrome 

Will Emissions Unit be operated at the maximum capacity givltn in its permit·to·install or permit·to-oparate? 

Specify how the operating rate will be determined during testing? C' See notes I, 2 and 3 on page 2,) 

EPA Tost 

MothodCs) 

1-4 

I " ) . "( . 

Yesl X 

Filtor Box 

Tamp 

Ambient 

Production records 

, \. . 

No. of 

Sempling 

Points 

25 

April 17. 1998 

No 

, Of 

eON~ 

Total No, of 

Time for Sampling 

T ast Run Runs 

120 3 

Wililhere be any modificelions to USEPA Reforonce Mothodlsl? Yesl=::=J Nol X Ilf yos, explain: __________________ _ 

Sampling LocationCs): Inlot:c=] Outlot:~ Simultanaous:c=JWiII cyclonic flow checkls) be conducted? Yel 

Fuel Semplino: Coal·Proxim'oto: c=] Ultimata: I=::=J Other (specify): ..;.m;.;.o::;/:.;;d;.:;s..;,c;.;.m.:-_______________________ _ 

EmiSSIon Roto to bo calculatod IIsi F·factor I=::=J Ultimate Cool Analysis LI __ ...1 Olher (specify): ..;m=u':.:d;:s..;,c;.;,m.:-__________ _ 

Arc "oncurrent Method 9 hlHdillUS to be perfurmed? Yec=J NOOLJ 

E. Sample Train Calibra1ion: EEl 3198 
I 

Intent To Test Notification 

General Notes on Chromium Sampling and Analysis 

The field emission sampling procedures used by Envisage Environmental, Incorporated, are presented in 

USEPA Reference Method 306, Determination of Chromium Emissions From Decorative and Hard Chromium 

Electroplating and Anodizing Operations. 

The chromium sampling train assembly may be found in the sampling train diagram. A brief description of its 

operation is presented below. 

Gas flow measurements will be conducted simultaneously with the chromium sampling so isokinetic rates can 

be maintained. The pitot system is zeroed and each leg is leak checked at greater than 3" H20 gage pressure 

for at least fifteen seconds. The average velocity pressure and temperature between the two runs will be used to 

calculate a chromium emission rate. The entire sampling train is vacuum leak checked from the nozzle opening 

at about (-)15" Hg gage pressure. The sample probe is positioned at the first sample point within the stack and 

sampling begins when the source reaches stability. 

Post-test run leak checks are performed as above with the sample train leak check conducted at the highest 

vacuum attained during the run and is held for one minute. 

Also incorporated into the field sampling and data analysis are those considerations and calculations contained 

in the following: 

1) Construction Details of Isokinetic Source Sampling Equipment, US EPA Doc. APTD - 0581, April 1971. 

2) Maintenance, Calibration, and Operations of Iso kinetic Source Sampling Equipment, US EPA Doc. 

APTD - 0576, March 1972. 

3) "A Method of Interpreting Stack Sampling Data," by W.S. Smith et ai, June 14 - 19,1970. 

Laboratory analyse,s-which are followed by Envisage Environmental are those procedures stated in USEPA 

Reference Methocf.30SA, Determination of Chromium Emissions From Decorative and Hard Chromium 

Electroplating and ,'Anodizing Operations, with associated calculations presented therein. Envisage 

Environmental Inc. ,illso uses the on-site sampling procedures and sample analysis quality control and quality 

assurance requirements as published in USEPA Document SOO/4-77/027b June 1987, Volume III. Part A and B: 

Quality Assura_nc~ Handbook for Pollution Measurement Systems: Volume III. Stationary Source Specific 

Meth~j1s; ~ - ~ 

\ .. 

Envisage 

Environmental 

Incorporated 

po. Box 152 Rlchflefd, OhiO 44286 

Phone (440) 526·0990 

----------------------------------------------------------------------------------
Intent To Test Notification 

Chromium 

F. Sampling Train Information 

Please refer to Sampling Train Diagram for schematic of proposed chromium sampling train. (Attachments No. 

1) 

Sampling for chromium emissions will be performed using the USEPA Method S sample train (excluding filter) 

in place of the Mason Jar method. The sampling train is assembled as follows: Method 5 probe and impingers. 

The four impingers contain in order - 100 ml. of 0.1 N NaOH, 100 ml. of 0.1 N NaOH, empty, and 200 g. of silica 

, gel. Glass probe liners will be used. The probe will be modified by installing a calibrated ''type K" thermocouple 

for probe exit temperature measurement. This modification will not alter the heater construction design as 

specified in APTD-OS81. 

The on-site sample recovery is carried out as follows: 

After the post test sample train leak checks have been performed, the probe assembly is disconnected from the 

sample train and rinsed and recovered with the absorbing solution. The probe is considered clean and may be 

reused for the next sampling run. 

After the leak check operations the impingers are removed from the sample train. wiped clean from sealing 

grease, and stored in their labeled and recorded sample case. 

Envisage 

Environmental I 

!~~X~5~~~h~=~~Q~oI286 I Phone 1~~OI 526'()990 

------
---l 

Intent To Test Notification 

Chromium 

i G. Laboratory Analysis 

The protocol used for the laboratory analysis of the collected samples is as presented in USEPA Reference 

Method 306. The impinger liquid catch is measured volumetrically. The liquid contents are combined. The 

I solutions are combined with the probe rinse and sent to an independent laboratory for analysis by Method 306. 

I 

i 

I 

I 

i 

l 

The silica gel is measured gravimetrically and its weight difference from its tare is determined and recorded as 

water vapor collected. The appropriate blanks from the test program are treated and recorded along with the 

above samples. 

----- .. _-----_._-- --- -

Envisage 

Environmental I, 

Incorporated 

PO Box 152 RIChllcld. 01\'0 44286 \ 

Phone (4401 526-0990 

--------------~ 
Intent To Test Notification 

H. Description of Operation 

, Three chrome tanks use chromic acid to provide a finished product with a smooth working surface. The 

emissions from this source go through a mist eliminator at the outlet of each tank and then go through a chrome 

scrubber before exiting into the atmosphere. 

I. Stack and Vent Diagram 

See Attachment #2 diagram. 

J. Safety 

I 

All standard safety procedures and precautions shall be followed. 

recommended: 

.K.. safety glasses with side shields 

.K.. chemical resistant goggles 

.K.. ear protection 

.K.. hard hat 

.K.. steel toed safety shoes 

..K.. long sleeved shirts 

flame retardant clothing 

respirator 

dusVparticle 

acid gas 

organic vapor 

SCBA 

The following personal protection is 

Envisage 

Environmental 

Incorporated 

PO Box 152 R,cl1held, OhIO 44266 \ 

Phone (4401 526·0990 J 
I 

Intent To Test Notification 

Attachment #1 

Chromium Sample Train 

Manometer 

I ______ ~--~-------------~-

ThanYlOmeters 

Dry Gas 

Meter 

Thermometer , 

".' :.: 

IlT1linger$ I nice Bath 

VaQlum Line 

-

Envisage 

Environmental 

Incorporated 

po. Box , 52 RlChllcld. OhiO 4428& 

Phone 14~01 576-0990 
~~-~----1 

Intent to Test Notification Attachment 2 I 

SAMPLE POINT LOCATIONS 

Facility: Diamond Hard Chrome Inc. 

Location: Chrome Scrubber #2 

Source No: 

inches 

2.1 1 [ o 

6.3 2 [ o 

10.5 3 [ 0 

14.7 4 [ 0 

5 [ 0 

18.9 

5 

o 

o 

0 

0 

0 

4 

Width 

o 

o 

0 

0 

0 

3 

Point # Distance In, From Inner Wall of Stack 

1 2.8 inches 

2 8.4 inches 

3 14.0 inches 

4 19.6 inches 

5 25.2 inches 

o 

o 

0 

0 

0 

2 

Stack Description = Rectangular 

Width 

Length 

1.9 

7.0 

4.08 

5 

2.0 

1.0 

3.5 

25 

o 

o 

0 

0 

0 

1 

] 

] 

28 inches 

21 inches 

o 

Point # 

-,-----

locahon 

1.9 

feet 

7.0 

feet 

Feet, Upstream Disturbance Distance 

Feet, Downstream Disturbance Distance 

Square Feet, Cross Section Area 

Number of Traverses 

Feet, Equivalent Diameter 

Equivalent Upstream Diameters 

Equivalent Downstream Diameters 

Total Number of Sampling Points 

Envisage .~ .----~--. Environmental 

~ 

, __ ,_. ____ ~'~_~ Incorporated 

~ P.O. Box 152 Richlleld. OhIO 44266 Phone (440) 526-0990 
Intent To Test Notification Attachment #3 

Tentative Equipment Specifications 

Control Unit (Meter Box) 

.1LEnvisage Environmental. Inc. 

_Andersen Samplers 

_Remanufactured RAe 

_DuPont Constant Flow Pumps 

Constant Monitoring Systems 

-X,. Thermo Environmental Chemiluminescence NO. NCh. NO. 

_Thermo Environmental CO. Model 48 

Sample Box 

-X,.EEI 

_Remanufactured RAC 

_EEl Special Design 

Impingers • per sample train (each set changed for each test run) 

.lLEEI 

-X,.EEI 

Sample Probe Liners 

Temperature 5ensors 

_Omega Engineering 

.lL Thermo Electric 

.lLFluke51 

_Fisher Scientific 

_Fisher Scientific 

Pressure Gauges 

.lLDwyer Incline Manometer 

_Dwyer Mallnhelic 

_Dwyer Magnhelic 

_CNlyer V Tube Manometer 

_CNlyer V Tube Manometer 

_CNlyer Microlector 

_Davis Electromanomeler 

Chemicals & Reagents 

.lLWater 

.lLAcelone 

.lLSilicaGel 

.lLVacuum Grease 

_Nitric Acid 

.lLSulfuric Acid 

.lLtsopropyl Alcohol 

.1LHydrogen Peroxide 

_Sodium Hydroxide 

length 

2 foot 

3 foot 

5 foot 

7 foot 

10 foot 

12 foot 

15 foot 

24 foot 

MB08·13 

MB lA, ZA, 01, 02 

MB 03·07 

SB 01,02, & 05·07 

SB03&04 

SB 08·11 

3 Modified Smith Greenburg 

1 Smith Greenburg 

Material 

SS, Pyrex, Quartz, Teflon 

SS, Pyrex, Quartz, Teflon 

55, Pyrex, Quartz, Teflon 

S5, Pyrex, Quartz, Teflon 

S5, Pyrex. Quartz, Teflon 

S5, Pyrex. Quartz. Teflon 

5S, Pyrex, Quartz, Teflon 

5S, Pyrex, Quartz, Tenon 

PYOI &02 

PY03·08 

PY09·14 

Mercury in Glass 

Bimetallic 

Type 

Oil, 0·10"HZ<> 

MagneliclMechanical 0 • 1 "HP 

MagneticlMechanical 0 • 10 "Hz<) 

Mercury 36" 

Waler 72" 

Waler 0 " 10 "H20 

Electric .001 •. 100 "H20 

Deionized & Distilled 

ACS Grade 

6. 16 Mesh 

Acetone Insoluble & Heat Resistant 

AC5Grade 

ACSGrade 

AC5Grade 

30% Solution 

Envisage 

Environmental 

Incorporated 

P.o. Box 152 n,chhcld. OhiO 44286 

Phone (4401 526·0990 

---------------------
.. 

Ohio. Envi rorlhen tal Protection Agency \ 

Agency 13 - Cleveland Division of Air Poll~tion Control 

, .' Stack Test Instrullent Monitoring Sheet 

:. Test date: i /c .. f Pr61.ise No. 13-18- Source Nos. 

iFacll1ty D' / ", Pacl lty '~1Ie:' i /;;';""'1.::,,~~d J-+~-.. :·tl Ct:,;-,:'):r~dress: oj.- ,~t' ,~; "L -...... r" . 

'. Sources (1.0.) anddJ _?<J/ (./11. 

, '~ol equip1ent: 7 S ~ .. [ ] batch 

-continuous 

Agency, 13 

, field llionitors ',.Jc; "{ ~ /; C t!T-/· J<je; ~{(- ~' . Testing- ,", -.-- -I- J\Testf~ . 

' •. fihh: ~ ;" v ,-(~ S '<.'. personnel: '-J '-1" -:;' ':'. 

''I'est· '. ,OAe j Ref':"er';":e':"n-c"'::e-~-/f-"':""-----------

'nethod (s): 3745-'. net.hod (s) 3 Co ~ 

Stack:[ J1.O •. [ ) brick, '[LY'E'RP [} round dia., ft. 2LW 

data: [ ] steel, £.:.r-rect. x L+W = ,Ports [ t"f"1\6ri zontal duct -d~i"a-':.~u·p~':"-';;";:"'''':''''----''d<'Ti'7:a-. --:d3':own=-_--;.....;..----

:at: r 1 vertical' stack ft. streanl ft. strewl 

i-lo. of points?r- Min:?;;;- Minutes 

traverses. .~ traverse J point;;,il per run ) :.l.)-

Gas net~r calib~, Probe length ":1 ft. I Cp = Nozz1~ dla. :31..2 ~-·in. 

factor Y = ), O/? Probe is [ ] glass, [ ] steel, { 1 All e 7- . (1.1 

No. of Sanples of (] coal, [ ] Process data 

samples [ ] sludge, [ ] sheets attached 

Date' Startlng Endlng Flilal Imtlal Net Final leak 

, nlo~ay-y'r tine tine .",.. volune volune volune check at 

( ] EST I ['1'"" DST ACF ACE' ACE' ? pressure 

Run 1 -

1J./').'/7S )<J II d )).. :j ~ 7J(;.'3:Z Y (. 0 (.1. <);Jfil Jf) 9· '";'/'1 I OJ{ ,\;. r;;; i ~ ~ 

Run 2 r..;!..:.,/fn J2~).f- '~~() ~/?', f"':.l I-' 7,(, _s5'-c' Je'1.·27'" r~J kf~ I L 

Run 3 

y: I /',.f

~"~ 

r;;;! 

I. ---:-2..;y.'J y:rs"'" Sf] y. '/.) .) "J.o-,) . \. 1J'I;3t CI(~S: 

Run 4 

'-

Total Range of Range of Range of Gas sanL- Saneling 

points stack 1\ P, /\ H, pIing & train , tested tertI[). I F in. w.g. in. w.g. analysis reCovery 

RUn 1 

'''). ~ i;~- 7 D ~l .• J/-- ~).Y: 1

f 0

." 

~f 

~ ... J'". 

(:-.,-r .- - Run 2 

'2 " ~ ~ '- ~ 9' c,1 ~~ ~ 9, .r~ .. - - "I. (' ~- C,3?c 

Rtln 3 

-')..) " - to s O.C7"~oU l j/ -):t-7 ---- . - --

Run 4· 

-- CQl(hents ~ 

---------------------------------------------------------------- 
SOURCE 

EVALUATION 

RESULTS 

PREPARED BY 

r· :. . - ~-...., 

, ~ , l. . J 

. ,.. :ii I J .-:; 

I.' ~~} ~ r .. ) 

Envisage 

Environmental 

Incorporated 

P.o. Box 152 Richfield, Ohio 44286 

Phone (216) 526-0990 
Envisage ':nvironmental Incorporated 

May 6,1998 

Mr. Robert Tankovich 

Diamond Hard Chrome 

6110GrandAve. 

Cleveland, Ohio 44 104 

Dear Mr. Tank.ovich : 

The following report is the result of the emission evaluation performed on April 21, 1998 al 

the Diamond Hard Chrome facility. Cleveland, Ohio. Testing was performed on the # 2 

Chrome Scrubber exhaust. The mass emissions of tolal chrome were determined on the 

oul let gas stream to determine compliance with the applicable permi! to operate and NSPS 

requirements. 

The results are true and accurate to the degree specified in the pertinent sections of the 

Code of Federal Regulations, in force at the time of testing. 

I look forward to answering any questions you may have and assisting you in the future. 

Respectfully submitted. 

ENVISAGE ~NVIR/M~ INC . 

e / . ) 

Tyson E. Houchin 

i' ~ 

Project Super/isor. Air Services 

P.O. Box 152 Rlchheld . OhiO 44286 Phone (440) 526·0990 Fax (d40) 526·8555 
· i --- ~~-- --------- -~---

TABLE OF CONTENTS 

INTRODUCTION 

DESCRIPTION OF PROGRAM 

TEST RESULTS SUMMARY 

TEST RESULTS DETAILED 

OPERATIONAL PARAMETERS 

SAMPLE POINT LOCATION DIAGRAM 

SAMPLING TRAIN DIAGRAM 

LABORATORY SECTION 

FI ELD DATA SHEETS 

CALIBRATION SECTION 

EMISSION SAMPLING NOMENCLATURE 

EMISSION SAMPLING CALCULATIONS 

.... _-_.- .. --. ------

PAGE NUMBER 

3 

5 - 6 

8 

10 

12 

14 

16 

18 - 21 

23 - 27 

29 - 31 

33 - 35 

37 - 39 

Envisage 

Environmental 

~ 

.. .. Incorporated 

po. Box '52 Rlcn!teld. OtllO ~·~2a6 W!l~_~ Phone (~.tOI526-0990 
INTRODUCTION 

. . 

2 

Envisage 

Environmental L~-,:,;:T;~Fil 

~ 

Incorporated 

~ P.O, Box 152 Richfield. Ohio 44286 Phorle (440) 526-0990 
INTRODUCTION 

Envisage Environmental Incorporated conducted emission sampling at the Diamond Hard Chrome facility. 

Cleveland, Ohio on April 21, 1998. The objective of the test program was to measure the mass emission rates of 

total chrome emitted into the atmosphere from the # 2 Chrome Scrubber exhaust. Emission sampling was 

conducted in triplicate with each of the test runs conducted over a one hundred and twenty-five (125) minute 

period. 

Mr. Robert Tankovich, Diamond Hard Chrome, coordinated the test program and operational procedures. The 

Envisage testing team consisted of Messrs. Tyson Houchin and Matthew Wahrer. 

The Cleveland Department of Air Pollution Control was represented by Mr. James Krause and Ms. Jane Bell. 

They were present throughout the testing period. 

'--------_._--.... ----_. -------_ .. _--------

Envisage 

Environmental 

Incorporated 

P.O. Box 152 R'CfltlCld. 011.0 -l-l28IJ 

Phooe 1~4')1 526·0930 
DESCRIPTION OF PROGRAM 

. 

. 

4 

Envisage 

: ..... ;:-.... ." .. _, Environmental 

\l_z:zt±t=1lncorporated 

-'"""" p.o. Box 152 R,chlu;tld. Ohio 44286 

Phono (440) 526-0990 
5 

SAMPLING AND ANALYTICAL PROCEDURES 

The sample collection and analysis techniques utilized for this test program were performed in accordance with 

the following USEPA Reference test methods: 

USEPA Method 1 

USEPA Method 2 

USEPA Method 3 

USEPA Method 4 

USEPA Method 306 

METHODS 1 

Sample and Velocity Traverses for Stationary Sources. 

Determination of Stack Gas Velocity and Volumetric Flow Rate. 

Gas Analysis for Carbon Dioxide, Oxygen, Excess Air, and Dry Molecular 

Weight. 

Determination of Moisture Content in Stack Gases. 

Determination of Chromium Emissions from Decorative and Hard 

Chromium Electroplating Operations and Anodizing Operations. 

The exhaust stack serving the #2 Chrome Scrubber is rectangular and had internal dimensions of 28 x 21 inches. 

The stack had an upstream distance of 48" (2.09 equivalent diameters) and a downstream distance of 23" (1.0 

equivalent diameter). Sampling was conducted through five (5) sample ports with a total of twenty-five sampling 

pOints used, five (5) sampling points per port. 

METHOD 2 

Three (3) foot ·S" type pitot tubes, and a Type K thermocouples were used for measuring the gas stream's 

velocity and temperature. The pressure drop, temperature and sample were taken and measured by traversing 

across the internal dimensions of the exhaust through the sample ports. 

METHOD 3 

Sampling for the determination of dry gas molecular weight was performed utilizing USEPA Method 3 procedures. 

Integrated samples were extracted from the stack during the sample runs. The sampling system con~isted of a 

stainless steel probe, followed by a Teflon sample line attached to a polyethylene squeeze pump. The squeeze 

pump was coupled with a leak free Tedlar bag. The concentration of oxygen and carbon dioxide in the sample 

was determined by using a Bacharach "Fyrite" Portable Gas Analyzer. Fyrite analysis provides for the selective 

absorption of oxygen in Burell Oxysorbent and carbon dioxide in potassium hydroxide solutions. The difference 

in gas volume before and after the absorption represents the amount of constituent gas in the Sample. Each 

sample was analyzed three (3) times, and the average of the readings for each run were used in calculating the 

emission rate. 

L_ Envisage 

Environmental 

Incorporated 

PO Box 152 RiChl:elcJ O!'.tO ·.·\26'j 

Phone (440, 526-0990 

------ -----~-- ----------_.----------
• -----~~-~ -~ --~ . -------, 

6 

METHOD 4 

The moisture content of the gas stream was determined by USEPA Method 4, impinger procedure. The impinger 

procedure consists of an integrated gas stream sample which is drawn through a series of chilled impingers and 

tarred dry silica gel, by means of calibrated dry gas meter. The net weight of liquid and liquid absorbed by the 

silica gel were recorded for the calculation of moisture content per sample volume. 

METHOD 306 

The chromium emissions exiting the exhaust stack were measured by following the procedures outlined in 

USEPA Method 306. The sampling train consisted of a glass nozzle connected to a heated Pyrex liner. The liner 

was connected to a series of impingers (Method 4) which contained; 100ml of sodium hydroxide in the first two, 

followed by an empty, and the final impinger containing the 200 grams of dry silica gel. 

Samples were taken from the gas stream isokinetically through the nozzle and sample train. Exit gas 

temperature of the impingers was maintained below 68°F. with an ice bath. At the conclusion of each test run the 

sample train was allowed to cool and a leak check of the train and pi tot tube was performed. After the leak check 

the probe and nozzle cleaning was performed in the field using a nylon bristled brush and a carrier liquid of 

sodium hydroxide. The field cleaning of the sampling probe and nozzle follows this procedure; At the conclusion 

of the test run the nozzle is removed, the inside surface is rinsed. brushed. and rinsed until visually clean of 

particulate matter. The rinse is collected in a glass sample bottle and capped with a teflon lined lid. The sample 

probe is rinsed into the same container by tilting the probe assembly and rotating so that the rinse liquid empties 

into the collection bottle. The nylon bristled brush is then introduced into the liner. By using a forward and 

rotating action the liner is brushed clean with copious amounts of sodium hydroxide. Visual inspection is then 

made and the process repeated until the rinse liquid is visually clean. A final rinse is then rotated down the 

inclined probe liner. The cleaning brushes are then rinsed and the sample bottle capped and secured in the 

appropriate test run container. 

The rinse samples including the impinger liquid are taken and analyzed in the laboratory. The impinger liquid is 

measured volumetrically and transferred to a storage bottle. The liquid is then transported to an independent 

laboratory for analysis of chromium. 

GENERAL 

All analytical procedures were performed in accordance with the methods speCified in the Code of Federal 

Regulations, Title 40, Part 60, Volume 43. 

Example calculations to determine the emission rates can be found in the example calculation section of this 

report. Envisage 

Environmental 

Incorporated 

p.o. Box 152 R,CI,licld. Oh,o 44286 

Phone (4401 526·0990 
i 

TEST RESULTS 

SUMMARY 

\ 
TEST RESULTS SUMMARY 

Diamond Hard Chrome 

Cleveland, Ohio 

#2 Chrome Plating Tank Scrubber Exhaust 

Chromium Emission Evaluation 

DATE: April 21, 1998 

PARAMETER 

Run 1 

Chromium Emissions 

Pounds/hour 2.32E-05 

Grains/dscf 4.32E-07 

mg/dscm 0.00099 

System Flow Rates 

Ft/Sec 25.86 

ACFM 6,336 

DSCFM 6,254 

Moisture Content 

Volume percent 1.25 

Sample Location Temperature 

Degrees Fahrenheit 69 

,--- '---- ------~--

8 

Run 2 Run 3 

2.17E-05 2.05E-05 

4.07E-07 3.60E-07 

0.00093 0.00082 

25.81 27.42 

6,322 6,717 

6,217 6,644 

1.83 1.28 

67 67 

Envisage 

Environmental 

~ 

._ Incorporated 

~ P.O. Box 152 Rlchfl~ld. OhiO ~.12Dr. Phono (4401 526·0990 

----- ----
TEST RESULTS 

. DETAILED 

. 

. 

9 

Envisage 

,--.-.------- Environmental t_ ;~;(~;=~~~~~.~~o~42a6 
~ 

TEST RESULTS 

Diamond Hard Chrome 

#2 Chrome Plating Tank Scrubber Exhaust 

Chromium Emission Evaluation 

DATE: April 21, 1998 Symbol Units 

Time of Day 

Gas Volume-dry,std. Vmstd cu. ft. 

2 Condensate Vapor Vol. Vwstd cu. ft. 

3 Gas Stream Moisture Bws vol.dec 

4 Mol. Wt-flue gas (dry) Msd Ib/lb mo. 

5 Mol. Wt-flue gas (wet) Ms Ib/lb mo. 

6 Flue Gas Velocity Vs ft/sec 

7 Flue Gas Volume-Actual as ACFM 

8 Flue Gas Volume-Std. as (Std) DSCFM 

9 Concentrations Cs 

- Chromium gr/dscf 

10 Emission Rate E 

- Chromium Ib/hr 

11 Isokinetic Rate % 

l_~ _______________ ~ 

Run 1 

10:00 

12: 11 

103.56 

1.31 

0.0125 

28.84 

28.70 

25.86 

6,336 

6,254 

4.32E-07 

2.32E-OS 

101.6 

- ... -~-

10 

Run 2 Run 3 

12:25 14:49 

14:36 17:00 

102.24 107.10 

1.91 1.39 

0.0183 0.0128 

28.84 28.84 

28.64 28.70 

25.81 27.42 

6,322 6,717 

6,217 6,644 

4.07E-07 3.60E-07 

2.17E-OS 2.0SE-OS 

100.9 98.9 

Envisage 

Environmental 

, Incorporated .... ~.......",,;::,;,_ ~ 

~', PO So, 152 R,cnlleld or',o ,14286 

Phone 1440.526-0990 
OPERATIONAL 

PARAMETERS 

.... -...... -.--,-- .--- ~ . 1 

L_~~_~j 

. . 

11 

Envisage 

Environmental 

Incorporated 

p.o. Box 152 Richfield. OhiO 44286 

Phcne (440) 526·0990 
12 

Production Records (amps) 

for Test on 

April 21, 1998 

Run 1 

Tank 1 Tank 2 Tank 3 Total 

2547 3778 3259 9584 

2567 3780 3242 9589 

2554 3780 3215 9549 

2568 3760 3258 9586 

2572 3737 3270 9579 

2568 3728 3282 9578 

Average 9576.14 

Run 2 

Tank 1 Tank 2 Tank 3 Total 

2555 3714 3267 9536 

2556 3715 3255 9526 

2535 3700 3261 9496 

2542 3709 3268 9519 

2542 3710 3282 9534 

2545 3734 3290 9569 

2547 3736 3296 9579 

Average 9537 

Run 3 

Tank 1 Tank 2 Tank 3 Total 

2531 3760 3309 9600 

2527 3753 3315 9595 

2543 3741 3311 9595 

2536 3737 3335 9608 

2543 3729 3335 9607 

2525 3750 3320 9595 

Average 9600 
, 

,---..... -----_. - . 

SAMPLE POINT 

LOCATION DIAGRAM 

-_.----_ .... - --- .~--

13 

Envisage 

Environmental ,..;,;"",..~..;.,;;,.' 

~ 

Incorporated 

PO Box 152 RIchfIeld. OhJo 4·~2t16 1iI!iI~_m!l·ililllI Phone (4·101526·0990 
SAMPLE POINT LOCATIONS 

I 

I 

I 

Facility: 

Location: 

inches 

2.8 

8.4 

Diamond Hard Chrome 

#2 Chrome Scrubber Exhaust 

1 [ 0 0 

2 ( 0 0 

l_~ 

Width 

0 

0 

0 

0 

Stack Description = Rectangular 

Width 

Length 

0 

0 

21 inches 

28 inches 

0 

0 

- 4.0 

feet 

sam~le 

location 

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Environmental 

~ 

. _ _ Incorporated 

~ po, Box. 152 Rlcntleld. OI~IO "'.1286 Phone 1440i 526·09~O 
SAMPLING TRAIN 

DIAGRAM 

. . 

15 

Envisage :=:-;' 

~ 

.) ~.,"~~~:~:~~~al 

~ P.O.Bo.152 Rlchfleld.Oh,044266 Phone (440) 526·0990 
~ ----····~~~----~~----~--~~I i 

I I I I I 

I 

I

: 

" 

, 

T'Couple ~::::::== 

Pitot (';." ......... .. 

Nozzle c..).;;;,; nj 

"'-"'--., 

plus 

Pitot 

Manometer 

minus 

Heated Prob 

T'COUPle/ 

Orifice 

r

l

,11eter 

plus 

rc::::::====--l 

Thermometer 

Flexible Line 

/,/ 

I mpingers I nice Bath 

Thermometers 

PllrY"'In 

Vacuum Gage 

Main 

Valve 

Dry Gas Air-Tight ~(J)I ...... : 

tl,i,...t.-.r _____________ _ 

~-------
17 

LABORATORY SECTION 

Envisage 

[J25Yir:~~ ~nn:~~~~:~~~al ~I ~ p.o. Box 152 Richliere!. Ohio 44286 Phone (440) 526-0990 
-----_. 

LABORATORY SUMMARY SHEET 

Diamond Hard Chrome 

#2 Chrome Plating Tank Scrubber Exhaust 

Chromium Emission Evaluation 

DATE:Ap~21, 1998 Symbol Units Run 1 

Sampling Time t minutes 125.0 

2 Barometric Pressure Pb in. Hg 29.94 

3 StatiC Pressure Pg in. H2O 0.04 

Stack Pressure Ps in. Hg 29.94 

4 Gas Meter Volume Vm cu. ft. 109.34 

5 Stack Area A sQ. ft. 4.08 

6 Nozzle Diameter Dn dec. in. 0.31 

7 "Y" Factor 'h\QS-0 1.019 

8 Meter Temperature degrees F 112.2 

Tm degrees R 572.2 

9 Stack Temperature degrees F 68.6 

Ts degrees R 528.6 

10 Velocity Head (SORT) "P in. H2O 0.457 

11 Orifice Pressure "H in. H2O 2.69 

12 Carbon dioxide CO2 % 0.0 

13 Oxygen 02 % 20.9 

14 Carbon monoxide CO % 0.0 

15 Nitrogen N2 % 79.1 

16 Pitot Coefficient Cp 0.84 

17 Water Collected Vic ml 27.9 

18 Sample Weight: Mn 

- Chromium g 2.90E-06 

----------------- -------~ 

18 

Run 2 Run 3 

125.0 125.0 

29.94 29.94 

0.04 0.04 

29.94 29.94 

109.27 114.36 

4.08 4.08 

0.31 0.31 

1.019 1.019 

119.2 119.2 

579.2 579.2 

67.5 67.4 

527.5 527.4 

0.456 0.485 

2.69 3.03 

0.0 . 0.0 

20.9 20.9 

0.0 0.0 

79.1 79.1 

0.84 0.84 

40.6 29.5 

2.70E-06 2.50E-06 

Envisage 

Environmental 

Incorporated 

PO 80. 152 RICh"cld, OhiO .t4286 

Phono 144015260990 
Sample Date ~I L7..llq~ ~,~ 

Client Name I are Weights ""..,) 

Facility Name C ~ fIVr()..o ~ v}-\I\()·/Yl e Sample Turnaround y'l%J 

Location E"'J...b~ll ~I Final Weights V\..J 

USEPA R f e erence M et hod'-. '30," 

Run # -3 2- l Field Blanks 

Case # 3DI 30] 2-0 \ 4th case 

Moisture Collected 

Impinger #'s l-3 1-5 l-3 

Final vol "Lll) "2 !.-'f '2 IS""' 

• Initial vol ""2..0 tJ 2.0 C} "2.OD 

Net vol (C) 'UJ I) 

Silica Gel 

Impinger # q. Lt it 

Final wt '2.i.d.... C( "2..15"', b 1-14-/j' • Initial wt --:2- 0 CJ ,00 200\0 2sJry,o 

Net wt 11..\~ \ <J. b l4-.tf 

Particulate 

Probe Wash Beaker # # # # # 

volume, ml 

Final wt 

• Initial wt 

Net wt . 

Filter # # # # # 

Final wt 

• Initial wt 

Net wt 

Impingers Beaker # # # # # 

Final wt 

• Initial wt 

Net wt , ~ct • U414 r~\lTIg.;).1.» ~c~ 
AMERICAN - -ANALYTICAL -' -' LABORATORIES, - - -INC. 

INDUSTRIAL HYGIENE AND ENVIRONMENTAL SCIENCES 

840 S. MAIN STREET 

AKRON, OHIO 44311-1516 

(330) 535-1300 

email: AAL@imperium.net 

WUII!; JI) 

SAH!'U::S COl.l.EC'I'ED 1J't ~I,I/TII 

SAMPLB ANALYSIS REPORT 

RKl'ORT IIISUKD 'fO, 

'l'yson lIouchi" 

£nvlllil9" t;IIVilUIIIlI"lIl .. 1 

P,O,Box 152 

Kichfldd. ohiu ~Hd .. 

WOkK ORUEk II ; "II 04')JI 

~ROJECr SAMPL£S KECt;IVt;u ; u4/2~/~d 

SAKi'LB 

DATE 

O~/21/\1ij 

0~/21hll 

(14/21/~tI 

o~/:!II'ja 

FIBLD HUHBER 

LAB HUHBER 

Run 1 

!iH041H 'OIA 

Run :.it 

!lIIO~nl O~A 

Run 1 

9110-l111,OlA 

eLK 

91104331 . U4A 

SAMPLB 

DESCRIPTI01' 

U, IN 11 .. 011 

0, III 11 .. 011 

:.I 2 !>III I 

0, 1Il NaOIl 

215ml 

SAMPLB 

VOLUHB 

219 ML 

223 Ml. 

:.lIS Ml. 

20U ML 

Rc:vlew.:d By, 

ANALYTB(S) 

Chl'o,nluRl 

ChL'oullum 

Chromium 

ChL'omium 

, Patrick Dunn 

ANALYSIS REI'OK'I't:U; o,,>/u'.>/'i1J 

SAMPLE TYI'!:: 

DK'rKC1'10N 

RESULT(S) U1UTS LIMIT MElKOD 

0.001!! ... J/B ....... ).., U.00U55 MULh .. d )00 

o.oon '''';J/S''llIjllu u.OUUSG Mutholl }U6 

0, 0015 ".J/~""'I' \u 0, UOU54 M"li.ud l06 

< 0.00050 ""J/S,""pi" 0 OUII<,O ~I"rhod )06 

... ACCREDITED OV TI H:: I\MEI1ICAN IN!)I JSTHII\L IIYGIENE ASSOCIA TION • 
• ---lean ,. --·· .... ieall ·'--,tori("- ' .. -. . abc y ~--------------------------------------~>s~----------~· 

04U ;:,. Main ;:,t. lei (33uJ :1.50-130(1 - JV\LNo.: Iff 0/ -)) / Akron. OH 44311-1516 Fax (330) 535-7246 Analysis 

email: AAL@lmperium.net Authorization I 

Company Namo: Phono ~1\d-S'2.{,-OqI\O -... ,~O 

o f! 00 

E: "f'f, <; pq c; ~ (\hf, (\{) N (n ft\·n:n ... FAX K/ .!! (VJ 

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ProJecl Namlllocallon AAl QuoleNa <Q. L4 c 

L l\A<) 1\'1 j; Sc..(l.1I 00' t"1- =¢2 ~ ~ ;:t' 

Repon To: Cltenl PrOject No Ij 

-ri50N \40\.l("~\~ C\fb-/l £\\ 

I I Samplod By CloentP 0 No. 

ISignalure) fY\ \til\. ,'\t I! 

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Oalo Sampled TImaSamplod Samplo ... Sample OoacJlptlon o! I 

~ I! • c MaIJl. ., ~~ : 

- I 

~ -21"~q, lo:oo A- .1" ~C).Ot\ ~ R.VtJ \ 4 30b C.H~r'l1s- I x.. 

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RelinquIshed By Oalo Tuna Roce:od.,V ;' 

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/// " Fa:" Results? __ (lux ,harges apply) 

L~~/lI~ Turn-Around 

K~ 9-,...-tJ,)" .\ (t .... """ lll,. J/t:tX\ J;2. :st;r" -t- Project Type: NI'DES __ UST VAP IL,~'!./(/Z , Normal -- -- CHAIN (') , 

/9':I(} 0 (, )/; 'LJ,1>{7 Rush Days 

OF Spaciallnslluct.ons 

CUSTODY / I J . _bI '.....-- Rush work n:lluires prior 

approval of lab om tory. - [/ I . , /' ~ /' Surcharges apply to all rush rY )~- ,-t:tfo/ "y. //!l,m· 

~ work. Surcharge rate depends 

Rec:olVQcl ot lab by. - ~f..- . \... / - "£-L- Oato I on type of work perfonned. I'(;) 

~UodbY' f,p II P ..... 

0010 _! -r 17'" 

(Cb.lr;r'stgnalutU M".I Ac<;"'"l".ny Roquoolj 03132 Ohio EPA Cenilied I AUlA Accredited Visit our web site at hup:/Iwww.aalinc.wm 

"n,-,.-.g ,'UnahJl~ hor.~o cu)lulHe' 1tUl-rwwh.-dg~~ Ihe, ""'''00 nlQiJ .I~ .... 'u .. • 10 UUI l.eflll'io lito • .., «NlIU_.$ unlh" Ic,,~n·c III u." '<)1111 
t" 

-; -

FIELD DATA SHEETS 

22 

Envisage 

Environmental L22DIT:::-:l Incorporated ~_ ~ P.o. Bolt 152 Richfield. Ohio 44286 Phonll(44D) 526·099D 
Facility 

Date 

Source Name 

Sampling Location 

Operator -n:}. 

Ambient Temperature 

Barometric Pressure ,2"Lq~ . 

Static Pressure 

Heater Box Setting 

Probe Setting 

Rheostat Setting YI , J ... 

Traverse Point Locations 

1. ~.? 7. 

2. j.y 8. 

3. 1'10 9. 

4. IC/.u 10. 

5. "2.J':2 11. 

6. 12. 

Sampling Location Diagram 

f/,.fY) St' "I 0.1.; ~ 1-,;, Sr .. i,L. I'· ~ C V!Jf.J"r 

. ;--:: 

, ·l)'ci:-:lj 'l..i,~ '--~ ; ~ / , • 'b "-1 : I, 

l I I ....-... I . 

Notes: 

c~ I z. 

£i-~ .It{ 

1<." 12.33 

Field Data Cover Sheet 

I 

Probe Length 3 

Probe ID# 

do"L. Pitot Correction Factor .~( 

Nozzle Diameter , ~1"1...\"" 

Assumed Moisture ..:tit 

Meter Box ID # 111/3 /0 

Meter "H 2. 0 3 

Meter Yc Factor /tJlf 

Sample Train ID# 3l7.) 

Thermocouple ID# /, Z, 3' 

Cvclonic Flow Check / 

Upstream Distance ~!' " 

Downstream Distance " Z.!! ., c, 

Stack Dimensions ~)' 21 

Nozzle Calibration Diameter 1 . ~{Z.5 

Diameter 2 , ~~<"' 

Diameter 3 . 3/;:.( 

Test Team Members 

EEl Team Leader 

Facility Contact 

EPA Representative -:r~ &~ f I 

() '3t' J" /1 J . /~ .... 

a~~~ /' <)/~fI9P -

23 
Facl~ty 

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Point 

tlurrbe. 

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~ 

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3 

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5 

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1 

7. 

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5' I 0 I UDe lea lonecos 

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P,OS5UfO 

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10 

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21 

"1..'5 

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17 

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111-

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Pob ... T~ne Velocity Head Slack Stack 

Nurrbe. otOay P,eSSUte Tolll'. DIY TelTp, Wol 

sqrt "P 'f "f 

QYII~Il;(' / "P '11,0 aq~"P 'F 'F 

10 t; ..5 a.~ 

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~ l'o.I·TeSI" o H20 ;;.:.2 ___ C=--_--!.H2=O 
Fac lIy 0 .. , P. 2-= 0 I 

Point Sample Time Gas Meier Velocity I-Iead Orillce Slack Gas Malor Pump Filler Holder 

Temp 

(o)F 

Probe 

Temp 

("IF 

Number Volume Pressure Pressure Temp, Temp Vacuum 

(minutes) (cubic It) "P ("HzO) sqrt "P I"HzO) (OF) Inlel (")F Oudet rH9) 

I .5b LC./~."s1. .'2.\ r~"<1 L'S-(', It'i 1It.l log 2·0 'V/~ 71{5 

'Z 5~ td'i.(H.I. to .'itl1- -1,·1{1 (,1 1~1- /0'1' 'Z.o '1-~ 'Vll{ 

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8D {,t}-1. 01.- ,1.l' ,5:>Q 359. 118' it"! Ito 'l,.,a '2~q '2.44 

Implngor 

Temp 

(OF) 

u-' 

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Point Sample Time Gas MeIer Vtllocity Ilead Orifice Stack Gas Meter Pump Filler Holder Probe Impinger 

Number Volume Pressure Pressure Temp. Temp Vacuum Tamp Temp Temp 

(minutes) (cubic It) "P ("H2O) sqrt "P ('HaC) (OF) Inlet (O)F Oullet rUg) (O)F (O)F (OF) 

I '/ \'J.~t4 '1ltJ ,S') 7,t/ , Jj10 J..?u 1/1 /1'/ /11 ~.6 ")..tJ-) "L'~? c...'S 

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<- -.......... .. I'J - ,-, .; I " .' ( 

): I /1. ) , ( . "; ) l 1... l I .,..0 ..., ~~ 

.4)L //110 
FliC II)' O~t 

Slack Gas Malar Pump Fllle, Holda, P,obe 

Temp. Temp Vacuum Temp Temp 

Poinl Sample Time Gas Mela, Velocity Head Orillce 

Numbe, Volume Pressu,e Pressure 

(minutes) (cubic II) "P ("HlO) sqrt"P ("H20) (Of) Inlel (O)F Oullet ("Hg) (0}F (·)F 

'1.. 

3 

I 

I /t7v ct l S-d /..t e (t-,.. & J7Lt- \ ,72. 67J 1'27 lIlt- 2.0 '2Lt L 2..3"2.. 

IIII---=Z-t---!-/~()('":.-.--t---"ct~l C{..::...:t:...-J\~~.c:t~~{_(---IIft~3ob~+-.u..\\!..l..\ fi ~ i "2.b \llt- • ':1..0 ~ '?" 7J 7 

Impinge, 

Temp 

(OF) 

~t -

,. 
r-------------------~----------------------,----------------------~ 28 

CALIBRATION SECTION 

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Phone (440) 526·0990 
~ 

PITOT TUBE CALIBRATION 

Pitot Tube 10 36 

Date March 6. 1998 

Technician Kinat 

• Pstd 

A 0.82 

B 0.82 

A 0.44 

B 0.44 

A 0.26 

B 0.26 

Average Cp for A 

Average Cp for B 

Average Deviation A 

Average Deviation B 

Average 

Pi tot Tube 10 36 1/8 nozzle 

Date March 6, 1998 

Technician Kinat 

'Pstd 

A 0.82 

B 0.82 

A 0.44 

B 0.44 

A 0.26 

B 0.26 

Average Cp for A 

Average Cp for B 

Average Deviation A 

Average Deviation B 

Average 

Pi tot Tube 10 36 1/2 nozzle 

Date March 6, 1998 

Technician Kinat 

• Pstd 

A 0.82 

B 0.82 

A 0.44 

B 0.44 

A 0.26 

B 0.26 

Average Cp for A 

Average Cp for B 

Average Deviation A 

Average Deviation B 

Average 

'Pp 

1.15 

1.15 

0.6 

0.6 

0.35 

0.36 

0.846 

0.842 

0.001 

0.004 

0.844 

'Pp 

1.15 

1.15 

0.6 

0.6 

0.35 

0.35 

0.846 

0.846 

0.001 

0.001 

0.846 

'Pp 

1.15 

1.15 

0.6 

0.6 

0.35 

0.35 

0.S46 

0.S46 

0.001 

0.001 

0.846 

29 

Cp Dev from Av 

0.836 0.010 

0.836 0.006 

0.848 0.002 

0.848 0.C06 

0.853 0.008 

0.841 0.000 

Cp Dev from Av 

0.836 0.010 

0.836 0.010 

0.848 0.002 

0.848 0.002 

0.853 0.008 

0.853 0.008 

Cp Dev from Av 

0.836 0.010 

0.836 0.010 

0.848 0.002 

0.848 0.002 

0.S53 O.OOS 

0.853 0.008 

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-------------------------_.----------
DRY GAS METER CALmRATION 

Using Wet Test Meter 

30 

Meter Box Number 

Calibration Date 

MB10 

02/24/98 

67 

28.49 

deg F, Ambient Temp. 

"Hg, Baro. Press. 

Technician 

Dry Gas Meter 

Orifice Differential 

Meter Temperature 

Volume 

Vacuum 

Wet Test Meter 

Time of Test 

Totals 

Orifice Differential 

Volume 

Temperature 

Delta H@ 

Y Factor 

CALCULATIONS 

GM Dye 

"H20 

deg F 

cu ft 

"Hg 

"H2O 

cu ft 

degF 

minutes 

.75 cfm 

1.0 

75.0 

4.945 

0.0 

-1.0 

5.024 

62.8 

9.28 

1.91 

1.037 

Dry Gas Meter MB 10 

Average Delta H@ 

Average Y Factor 

Y = Vw • Pbar .. (Tm) 

NOMENCLATURE 

Orifice Differential 

Temperature 

Volume 

Time of Test 

Vm * [ Pbar + (-H /13.6) ) .. (Tw) 

-H@ = .0317 ""H .. Tmo" min 

Pbar • (Tm)" Vw 

= "H 

=T 

= cu ft 

= min 

Dry Gas Meter 

Wet Test Meter 

Barometric Pressure 

2.0 

76.0 

5.080 

0.0 

-2.0 

5.028 

62.6 

6.73 

2.05 

1.010 

3.0 

78.3 

5.050 

0.0 

-3.0 

5.029 

62.6 

5.52 

2.06 

1.018 

2.03 

1.019 

= sub m 

= sub w 

= Pbar 

4.0 

80.8 

5.095 

0.0 

-4.0 

5.028 

62.6 

4.85 

2.12 

1.011 

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EMTIC GUIDELINE DOCUMENT GD-026 

Alternative Method 5 Post Test Calibration 

Company: 

Test Date: 

Meterbox 10: 

Time of Test 

Volume of Meter 

Temperature of Meter 

Barometric Pressure 

Delta H 

Delta H@ 

% Oxygen 

% Carbon Dioxide 

% Carbon Monoxide 

% Nitrogen 

Diamond Hard Chrome 

4/21/98 

min 

dscf 

Deg F 

Deg R 

in. Hg 

H20 

H20 

10 

Dry Molecular Weight of St Md 

Dry Gas Meter Calib. Check Value Yqa 

Y Factor 

Difference 

Average Difference 

Run 1 

125.00 

109.34 

68.60 

528.60 

29.94 

2.69 

2.03 

0.00 

20.90 

0.00 

81.00 

28.84 

0.987 

1.019 

0.97 

0.97 

Run 2 

125.00 

109.27 

67.48 

527.48 

29.94 

2.69 

2.03 

0.00 

20.90 

0.00 

81.00 

28.84 

0.987 

1.019 

0.97 

31 

Run 3 

125.00 

114.36 

67.40 

527.40 

29.94 

3.03 

2.03 

0.00 

20.90 

0.00 

81.00 

28.84 

1.000 

1.019 

0.98 

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~ p.o. Box 152 Richfield. 01110 44285 Phone 1440) 526-09S0 
EMISSION SAMPLING 

NOMENCLATURE 

32 

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L ,."~:- .. " -_. Incorporated 

__ 

""" ________________ ~_"_""l P.O" Box 152 Rlchheld.Ohlo4J286 I __ ._ ._ ~ Phone (440)526-0990 

p. = 

P sid = 

PPM = 

Pw = 

"P avg = 

a = 

Qsld = 

R = 

t = 

Tm = 

Ts = 

T$ld = 

Vt,c = 

vac = 

Vm = 

V m(std)= 

= 

I 

SAMPLING NOMENCLATURE - continued 

Absolute gas stream pressure, (Pbar + P /13.6) in. of Hg• 

Absolute pressure at standard conditions, 29.92 in. of Hg• 

Parts per million 

Density of water, 0.0022 Ib./ml. 

Average of the square roots of the velocity head readings, in. of H20. 

Volumetric flow rate at gas stream conditions, A.C.F.M. 

Dry volumetric gas flow rate corrected to standard conditions. D.S.C.F.M. 

Ideal gas constant. 21.85 in. of Hg-fe/ oR-lb.-mole. 

Total sampling time, minutes. 

Average dry gas meter temperature, oR. 

Average absolute gas stream temperature, oR. 

Standard absolute temperature. 528° rankine. 

" 

Volume of water collected in impingers and silica gel, ml. 

Volatile organic compounds 

Volume of gas sample measured at meter box (meter conditions), ft.3. 

Volume of gas sample measured at meter box (corrected to standard 

conditions), ft.3, 

Average gas stream velocity, fUsee. 

34 

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c- __ . _______ • __ . ___ . __ _ ____________ ~_~~ _ ... __ . ____ ~ Phone (440)526·0990 J 
v.N($I.c!} = 

13.6 = 

%C02 = 

%02 = 

%CO = 

%N2 = 

35 

SAMPLING NOMENCLA TUAE • continued 

Volume of water vapor in gas sample (standard conditions), ft. 3. 

Specific gravity of mercury (H~. 

Percent by volume of CO2 in gas stream (dry basis). 

Percent by volume of O2 in gas stream (dry basis). 

Percent by volume of CO in gas stream (dry basis). 

Percent by volume of N2 in gas stream (dry basis). 

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Phone (4010) 526·0990 
i 

I i _____________ _ 

EMISSION SAMPLING 

CALCULATIONS 

~~~~.-. ----- - -- ~~~-

36 

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~ 

_ .. Incorporated 

p.o. Bo~ 152 RI.:tlf'el{l, or..:) <:':~8ij ~_""""""",~, Pnore 1440) 526·09,0 
EXAMPLE CALCULATIONS 

Diamond Hard Chrome 

#2 Chrome Plating Tank Scrubber Exhaust 

Run # 1 

Start Time 10:00 

Finish Time 12: 11 

Sample Time (t) 125.00 

Barometric Pressure (Pb) = 29.94 

Stack Pressure IPs) 29.94 

Stack Area (As) 4.08 

Stack Temp. ITs) 68.60 

Nozzle Diameter (Dnl = 0.31 

Velocity Head (A PI = 0.46 

Orifice Pressure (A H) = 2.69 

Meter Y Factor IYI 1.019 

Volume of H20 Collected (Vic = 27.90 

minutes 

in. Hg 

in. Hg 

sq. ft. 

Degrees F. 

dec. in. 

in. H2O 

in. H2O 

ml 

Pitot Factor (Cp) 

Gas Analysis 

Sample Weights IMn) 

Chromium 

Vm std. = Vm x [Tstd/(Tm + 460)J x [Pb + CH 113.61 I Pstd»J x Y 

Vwlstd} = 0.04707 x Vic 

Bws = Vw(std) I [Vm(stdl + Vw(std)J 

Md = (.44 x %C02) + (.32 x %02) + (.28 x (%N2 + %CO) 

Ms = (Md x (1 - Bws}J + (18.0 x Bws) 

Vs = 85.49 x Cp x SORT(dPJ) x (SORT{(Ts + 460) I (Ms x Ps}J 

Os = Vs x As x 60 

Os(std) = Os x 11 - Bws) x [Tstd I (Ts + 460)] x (Pb + Ps/13.6) / 29.92 

Cs = 15.43 x IMn 1 Vm {stdll 

E = Qstd x Cs x (1 Ib I 7000 grains) x (60 minutes / 1 hour) 

37 

= 0.00 

0.84 %J 

20.90 % 02 

0.00 % CO 

79.10 % N2 

0.000003 grams 

103.56 

= 1.31 

0.0125 

28.84 

28.70 

25.86 

6,336 

. 

= 6,254 

= 4.32E-07 

= 0.00002 

I = {[100 x Ts x ((K3 x Vic) + IVm 1 Tm» x (Pbar + (-H 1 13.6»J / 60 x An x Vs x Ps x t = 101.55 

- --~----'-'---

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__ P.O. Box 152 RCht'e:d Cn,oJ·'2i''', PhorJe (':40/ 526~09:}:) 
I 

,. 

EXAMPLE CALCULATIONS 

Diamond Hard Chrome 

#2 Chrome Plating Tank Scrubber Exhaust 

Run # 2 

Start Time 12:25 

Finish Time 14:36 

Sample Time (t) 125.00 

Barometric Pressure IPb) 29.94 

Stack Pressure IPs) = 29.94 

Stack Area (As) = 4.08 

Stack Temp. (Ts) = 67.48 

Nozzle Diameter (On) 0.31 

Velocity Head (A P) = 0.46 

Orifice Pressure (A H) 2.69 

Meter Y Factor (Y) 1.019 

Volume of H20 Collected (Vic = 40.60 

minutes 

in. Hg 

in. Hg 

sq.ft. 

Degrees F. 

dec. in. 

in. H2O 

in. H2O 

ml 

Pitot Factor (Cp) 

Gas Analysis 

Sample Weights IMn) 

Chromium 

Vm std. = Vm x (TstdllTm + 460)1 x (Pb + ("H 113.6)1 Pstd))1 x Y 

Vwlstd) = 0.04707 x Vic 

Bws = Vw(std) I (Vm(std) + Vw(std)l 

Md = 1.44 x %C02) + (.32 x %02) + 1.28 x I%N2 - %CO) 

Ms = (Md x (1 " Bws)1 + (18.0 x Bws) 

Vs = 85.49 x Cp x SQRT(dP)) x (SQRT{(Ts + 460) I (Ms x Ps}1 

Os = Vs x As x 60 

Oslstd) = Qs x (1 " Bws) x (Tstd I ITs + 460)1 x IPb + Ps/13.6) 1 29.92 

Cs = 15.43 x IMn I Vm (std)) 

E = Qstd x Cs x (lib I 7000 grains) x (60 minutes 1 1 hour) 

I = {(100 x Ts x IIK3 x Vic) + (Vm ITm)) x (Pbar + ("H 113.6))1/60 x An x Vs x Ps x t 

38 

0.84 

0.00 % CO 

20.90 % 02 

0.00 % CO 

79.10 % N2 

= 0.000003 grams 

102.24 

1.91 

0.0183 

= 28.84 

= 28.64 

25.81 

= 9,322 

6,217 

4.07E·07 

= 0.00002 

100.86 

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~ po_ So. 152 Rjc-'~~jC".:l O'lIU ·:·:2d·-Phong i~~OJ 526-09)0 

------------------ ---------
EXAMPLE CALCULATIONS 

Diamond Hard Chrome 

#2 Chrome Plating Tank Scrubber Exhaust 

Run # 

Start Time 

Finish Time 

Sample Time (tl 

Barometric Pressure IPb) 

Stack Pressure (Ps) 

Stack Area (As) 

Stack Temp. (Ts) 

Nozzle Diameter IOn) 

Velocity Head (A PI 

Orifice Pressure {A HI 

= 

= 

= 

Meter Y Factor (V) = 

Volume of H20 Collected IVlc = 

3 

14:49 

17:00 

125.00 

29.94 

29.94 

4.08 

67.40 

0.31 

0.49 

3.03 

1.019 

29.50 

minutes 

in. Hg 

in. Hg 

sq. ft. 

Degrees F. 

dec. in. 

in. H2O 

in. H2O 

ml 

Pitot Factor (Cp) 

Gas Analysis 

Sample Weights (Mn) 

Chromium 

Vm std. = Vm x [Tstd/lTm + 46011 x (Pb + I A H / 13.6) / Pstdll] x Y 

Vw(stdl = 0.04707 x Vic 

Bws = Vw{stdl / [Vmlstdl + Vw(stdl) 

Md = (.44 x %C021 + (.32 x %021 + [.28 x I%N2 + %CO) 

Ms = [Md x (1 - Bws)) + (18.0 x Bws) 

Vs = 85.49 x Cp x SQRT[dPll x [SORT{(Ts + 4601 IIMs x Ps}) 

Os = Vs x As x 60 

Oslstd) = Os x (1 - Bws) x [Tstd / ITs + 460)) x (Pb + Ps/13.6) /29.92 

Cs = 15.43 x IMn / Vm (std)) 

E = Ostd x Cs x (1 Ib / 7000 grains) x (60 minutes / 1 hour) 

39 

0.84 

0.00 % CO 

20.90 % 02 

0.00 % CO 

79.10 % N2 

= 0.000003 grams 

107.10 

1.39 

= 0.0128 

28.84 

= 28.70 

27.42 

6,717 

= 6,644 

= 3.60E-07 

= 0.00002 

I = {[100 x Ts x ((K3 x Vic) + (Vm I Tml) x (Pbar + (AH /13.6))) /60 x An x Vs x Ps x t 98.87 

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