Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. 

to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific 

This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were 

tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted 

yellow are required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fi

automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

D5865-04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If 

of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, ora

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results works

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a mi

3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you 

collected more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the uni

measure.
Information

nformation about chemical analyses of fuels 

, chlorine, fluorine, and metals, such as 

nd selenium. This spreadsheet is intended 

p to 4) fuel analyses at that specific boiler. 

esting for all 4 HAP surrogates were being 

Fields that are highlighted in 

down boxes, included. Gray fields are 

_Testing.xls).

ler on the Boiler Information worksheet.

fuel column of the Boiler Information 

 the Other Fuel Description column.

ethods worksheet. For example: "ASTM 

 Picklist worksheet (orange tab). If the units

le, please fill them in the blank, orange 

e in the Fuels Sample Results worksheet.

range highlighted cell).

 worksheet. You must provide a minimum of 

re not limited to that number if you have 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

628 Crystal River Unit 1 bituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

628 Crystal River Unit 1 As Received Higher Heating Value

628 Crystal River Unit 1 As Received % Moisture

628 Crystal River Unit 1 As Received % Ash

628 Crystal River Unit 1 As Received % Sulfur

628 Crystal River Unit 1 Dry basis Higher Heating Value

628 Crystal River Unit 1 Dry basis % Ash

628 Crystal River Unit 1 Dry basis % Sulfur

628 Crystal River Unit 1 Dry basis Antimony

628 Crystal River Unit 1 Dry basis Arsenic

628 Crystal River Unit 1 Dry basis Beryllium

628 Crystal River Unit 1 Dry basis Cadmium

628 Crystal River Unit 1 Dry basis Chlorine

628 Crystal River Unit 1 Dry basis Chromium

628 Crystal River Unit 1 Dry basis Cobalt

628 Crystal River Unit 1 Dry basis Fluorine

628 Crystal River Unit 1 Dry basis Lead

628 Crystal River Unit 1 Dry basis Manganese

628 Crystal River Unit 1 Dry basis Mercury

628 Crystal River Unit 1 Dry basis Nickel

628 Crystal River Unit 1 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5865

ASTM D3173

ASTM D3174

ASTM D4239

ASTM D5865

ASTM D3174

ASTM D4239

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D4208

ASTM D6357

ASTM D6357

ASTM D3761

ASTM D6357

ASTM D6357

ASTM D6722

ASTM D6357

ASTM D4606
EIA Facility Code Facility Name Boiler ID HAPs Test Group

628 Crystal River Unit 1 Mercury and non-mercury metalic HAPs

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

Run 1 3/23/2010 3/23/2010 12548.00 Btu/lb

Run 2 3/23/2010 3/23/2010 12333.00 Btu/lb

Run 3 3/24/2010 3/24/2010 12329.00 Btu/lb

 Fuel Testing Results


d non-mercury metalic HAPs

% Moisture

(as received)

% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

6.82 10.53 0.91 13466 Btu/lb 11.3

6.85 10.86 0.99 13240 Btu/lb 11.66

6.25 11.38 0.89 13151 Btu/lb 12.14


% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis) Arsenic Units

0.98 971 ppm 0.05 mg/g 0.96 mg/g 5.68 mg/g

1.06 1088 ppm 0.05 mg/g 1 mg/g 5.41 mg/g

0.95 810 ppm 0.05 mg/g 0.8 mg/g 5.08 mg/g


Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

2.53 mg/g 0.04 mg/g 17.94 mg/g 6.89 mg/g 17.2

2.59 mg/g 0.03 mg/g 18.5 mg/g 8.65 mg/g 17.7

2.25 mg/g 0.03 mg/g 19.24 mg/g 6.25 mg/g 17.29


Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

mg/g 14.23 mg/g 1.24 mg/g 104 ppm 7.78 mg/g

mg/g 14.58 mg/g 3.79 mg/g 112 ppm 7.86 mg/g

mg/g 24.52 mg/g 3.01 mg/g 134 ppm 7.72 mg/g


EIA Facility Code Facility Name Boiler ID HAPs Test Group

628 Crystal River Unit 1 Acid gas HAPs

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

Run 1 3/24/2010 3/24/2010 12263.00 Btu/lb

Run 2 3/25/2010 3/25/2010 12749.00 Btu/lb

Run 3 3/25/2010 3/25/2010 12666.00 Btu/lb

 Fuel Testing Results


% Moisture

(as received)

% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

6.18 11.9 0.9 13071 Btu/lb 12.68

5.56 9.54 0.82 13500 Btu/lb 10.1

5.36 9.89 0.83 13383 Btu/lb 10.45


% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis) Arsenic Units

0.96 987 ppm 0.05 mg/g 0.96 mg/g 6.75 mg/g

0.87 1704 ppm 0.04 mg/g 0.94 mg/g 3.68 mg/g

0.88 1872 ppm 0.03 mg/g 0.86 mg/g 3.3 mg/g


Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

2.1 mg/g 0.03 mg/g 22.38 mg/g 5.52 mg/g 16.79

2.7 mg/g 0.06 mg/g 15.87 mg/g 5.69 mg/g 15.04

2.38 mg/g 0.05 mg/g 14.16 mg/g 5.63 mg/g 13.92


Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

mg/g 14.36 mg/g 4.51 mg/g 104 ppm 7.54 mg/g

mg/g 12.76 mg/g 3.06 mg/g 69 ppm 6.76 mg/g

mg/g 10.51 mg/g 3.4 mg/g 50 ppm 6.21 mg/g


EIA Facility Code Facility Name Boiler ID HAPs Test Group

628 Crystal River Unit 1 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

Run 1 3/26/2010 3/26/2010 12255.00 Btu/lb

Run 2 3/26/2010 3/26/2010 12432.00 Btu/lb

Run 3 3/26/2010 3/26/2010 12494.00 Btu/lb

 Fuel Testing Results


/furan organic HAPs

% Moisture

(as received)

% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)

6.8 11.72 0.96 13149 Btu/lb 11.72

6.62 10.94 0.91 13313 Btu/lb 10.94

6.53 10.22 0.87 13367 Btu/lb 10.22


% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis) Arsenic Units

1.03 1890 ppm 0.06 mg/g 0.9 mg/g 4.9 mg/g

0.97 1505 ppm 0.05 mg/g 0.91 mg/g 5.22 mg/g

0.93 1330 ppm 0.04 mg/g 0.82 mg/g 4.51 mg/g


Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

2.46 mg/g 0.02 mg/g 17.54 mg/g 5.7 mg/g 12.47

2.51 mg/g 0.03 mg/g 18.37 mg/g 5.66 mg/g 15.24

2.42 mg/g 0.01 mg/g 17.36 mg/g 7.74 mg/g 15.13


Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

mg/g 14.62 mg/g 4.52 mg/g 69 ppm 10.15 mg/g

mg/g 14.91 mg/g 1.97 mg/g 77 ppm 9.24 mg/g

mg/g 13.2 mg/g 2.72 mg/g 69 ppm 7.86 mg/g


EIA Facility Code Facility Name Boiler ID HAPs Test Group

628 Crystal River Unit 1

Sample Number 

(minimum of 3 

composite samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating Value (HHV)

(as received) HHV Units

 Fuel Testing Results


% Moisture

(as received)

% Ash

(as received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Moisture

(Dry Basis)

% Ash

(Dry Basis)


% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis) Mercury Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis) Arsenic Units


Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)


Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the 

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μg/g

other mg/Kg

 unit of measure to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm