Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

-down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

-down boxes to fill in the units of

measure.Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1 3179 Hatfields Ferry Power Station 1 bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis Analyte

3179 Hatfields Ferry Power Station 1 As Received Higher Heating Value 3179 Hatfields Ferry Power Station 1 As Received % Moisture 3179 Hatfields Ferry Power Station 1 As Received % Ash 3179 Hatfields Ferry Power Station 1 As Received % Sulfur 3179 Hatfields Ferry Power Station 1 Dry basis Higher Heating Value 3179 Hatfields Ferry Power Station 1 Dry basis % Ash 3179 Hatfields Ferry Power Station 1 Dry basis % Sulfur 3179 Hatfields Ferry Power Station 1 Dry basis Antim ony 3179 Hatfields Ferry Power Station 1 Dry basis Arsenic 3179 Hatfields Ferry Power Station 1 Dry basis Beryllium 3179 Hatfields Ferry Power Station 1 Dry basis Cadmium 3179 Hatfields Ferry Power Station 1 Dry basis Chlorine 3179 Hatfields Ferry Power Station 1 Dry basis Chromium 3179 Hatfields Ferry Power Station 1 Dry basis Cobalt 3179 Hatfields Ferry Power Station 1 Dry basis Fluorine 3179 Hatfields Ferry Power Station 1 Dry basis Lead 3179 Hatfields Ferry Power Station 1 Dry basis Manganese 3179 Hatfields Ferry Power Station 1 Dry basis Mercury 3179 Hatfields Ferry Power Station 1 Dry basis Nickel 3179 Hatfields Ferry Power Station 1 Dry basis SeleniumAnalysis M ethod for each Analyte

(example: ASTM D5865-04) ASTM D5865 ASTM D3172 ASTM D3172 ASTM D3172 ASTM D5865 ASTM D3172 ASTM D3172 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D6357 ASTM D4208-02 ASTM D6357 ASTM D6357 ASTM D3761-02 ASTM D6357 ASTM D6357 ASTM D6722-01 ASTM D6357 ASTM D4606/D6357EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 3179 Hatfields Ferry Power Station 1 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units M5/28, M29 1 5/10/2010 5/10/2010 12618.00 Btu/lb M5/28, M29 2 5/11/2010 5/11/2010 12821.00 Btu/lb M5/28, M29 3 5/11/2010 5/11/2010 12694.00 Btu/lb M30 B1 5/11/2010 5/11/2010 12808.00 Btu/lb M30 R2 5/11/2010 5/11/2010 12844.00 Btu/lb M30 R3 5/11/2010 5/11/2010 12657.00 Btu/lb Fuel Testing ResultsMercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 2.33 11.88 1.90 12919.00 Btu/lb 12.16 1.95 2.08 11.47 2.09 13094.00 Btu/lb 11.71 2.13 2.25 11.74 2.16 12986.00 Btu/lb 12.01 2.21 1.91 11.47 2.12 13057.00 Btu/lb 11.69 1.48 1.94 11.35 2.11 13098.00 Btu/lb 11.57 2.15 2.33 11.78 2.12 12959.00 Btu/lb 12.06 2.17Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 370.00 mg/Kg 0.064 mg/Kg 0.20 mg/Kg 4.23 mg/Kg 0.774 408.00 mg/Kg 0.059 mg/Kg 0.16 mg/Kg 3.22 mg/Kg 0.743 400.00 mg/Kg 0.057 mg/Kg 0.17 mg/Kg 3.68 mg/Kg 0.775 423.00 mg/Kg 0.057 mg/Kg 0.14 mg/Kg 3.05 mg/Kg 0.749 416.00 mg/Kg 0.057 mg/Kg 0.16 mg/Kg 3.33 mg/Kg 0.745 413.00 mg/Kg 0.057 mg/Kg 0.18 mg/Kg 3.42 mg/Kg 0.783Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg 0.09 mg/Kg 14.90 mg/Kg 3.84 mg/Kg 24.70 mg/Kg mg/Kg 0.06 mg/Kg 13.70 mg/Kg 3.07 mg/Kg 24.50 mg/Kg mg/Kg 0.07 mg/Kg 14.40 mg/Kg 3.48 mg/Kg 26.30 mg/Kg mg/Kg 0.04 mg/Kg 13.90 mg/Kg 2.81 mg/Kg 23.80 mg/Kg mg/Kg 0.06 mg/Kg 13.70 mg/Kg 4.11 mg/Kg 24.50 mg/Kg mg/Kg 0.05 mg/Kg 14.60 mg/Kg 3.43 mg/Kg 27.00 mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 7.40 mg/Kg 0.81 mg/Kg 4.43 mg/Kg 6.86 mg/Kg 0.72 mg/Kg 4.07 mg/Kg 7.37 mg/Kg 0.74 mg/Kg 4.32 mg/Kg 7.07 mg/Kg 0.46 mg/Kg 56.00 mg/Kg 4.14 mg/Kg 6.89 mg/Kg 0.63 mg/Kg 64.00 mg/Kg 4.11 mg/Kg 7.45 mg/Kg 0.62 mg/Kg 61.00 mg/Kg 4.37 mg/Kg Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 36.97 12.16 50.87 72.53 4.81 1.41 1.95 37.76 11.71 50.53 73.14 4.81 1.43 2.13 37.69 12.01 50.30 72.51 4.89 1.42 2.21 37.90 11.69 50.41 73.07 4.88 1.48 2.16 38.41 11.57 50.02 73.52 4.91 1.45 2.15 38.04 12.06 49.90 72.44 4.86 1.38 2.17 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen

7.14 6.78 6.96 6.72 6.40 7.09EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 3179 Hatfields Ferry Power Station 1 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units M6C,M0011, M25A R1 5/12/2010 5/12/2010 12730.00 Btu/lb M6C, M0011, M25A R2

5/12/2010 5/12/2010 12634.00 Btu/lb M6C, M0011, M25A R3

5/12/2010 5/12/2010 12475.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 2.06 12.29 1.70 12997.00 Btu/lb 12.55 1.74 1.94 12.84 1.70 12884.00 Btu/lb 13.09 1.73 2.09 13.57 1.76 12742.00 Btu/lb 13.86 1.80Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 367.00 mg/Kg mg/Kg mg/Kg mg/Kg 344.00 mg/Kg mg/Kg mg/Kg mg/Kg 327.00 mg/Kg mg/Kg mg/Kg mg/KgBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units mg/Kg mg/Kg 58.00 mg/Kg mg/Kg mg/Kg mg/Kg 65.00 mg/Kg mg/Kg mg/Kg mg/Kg 72.00 mg/Kg mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

36.34 12.55 51.11 72.94 4.81 1.47 1.74 36.59 13.09 50.32 72.60 4.77 1.52 1.73 37.01 13.86 49.13 71.09 4.70 1.48 1.80 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 6.49 6.29 7.07EIA

Facility Code Facility

Name Boiler ID HAPs Test Group 3179 Hatfields Ferry Power Station 1 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units M26A R1 5/12/2010 5/12/2010 12696.00 Btu/lb M26A R2 5/12/2010 5/12/2010 12622.00 Btu/lb M26A R3 5/12/2010 5/12/2010 12663.00 Btu/lb U1 CTM 033 1 5/13/2010 5/13/2010 12594.00 Btu/lb U1 CTM 033 2 5/13/2010 5/13/2010 12649.00 Btu/lb U1 CTM 033 3 5/13/2010 5/13/2010 12673.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 2.01 12.30 1.67 12957.00 Btu/lb 12.55 1.70 2.48 11.64 2.06 12943.00 Btu/lb 11.94 2.11 2.60 11.19 1.96 13001.00 Btu/lb 11.49 2.01 2.59 11.88 2.07 12929.00 Btu/lb 12.20 2.13 2.54 11.36 2.00 12978.00 Btu/lb 11.66 2.05 2.52 11.37 2.06 13001.00 Btu/lb 11.66 2.11Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 358.00 mg/Kg mg/Kg mg/Kg mg/Kg 447.00 mg/Kg mg/Kg mg/Kg mg/Kg 433.00 mg/Kg mg/Kg mg/Kg mg/Kg 464.00 mg/Kg mg/Kg mg/Kg mg/Kg 439.00 mg/Kg mg/Kg mg/Kg mg/Kg 445.00 mg/Kg mg/Kg mg/Kg mg/KgBeryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/KgNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units mg/Kg mg/Kg 65.00 mg/Kg mg/Kg mg/Kg mg/Kg 62.00 mg/Kg mg/Kg mg/Kg mg/Kg 61.00 mg/Kg mg/Kg mg/Kg mg/Kg 67.00 mg/Kg mg/Kg mg/Kg mg/Kg 57.00 mg/Kg mg/Kg mg/Kg mg/Kg 62.00 mg/Kg mg/KgNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles Ash Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur

37.20 12.55 50.25 72.87 4.79 1.51 1.70 37.67 11.94 50.39 72.43 4.89 1.44 2.11 38.02 11.49 50.49 72.42 4.81 1.42 2.01 37.72 12.20 50.08 72.22 4.84 1.46 2.13 38.34 11.66 50.00 72.95 4.86 1.43 2.05 38.34 11.66 50.00 72.83 4.83 1.45 2.11 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 6.58 7.19 7.85 7.15 7.05 7.12Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm mg/Kg