prepared. The date on attached sheets needs to match the date noted below. 

General Reference 287.54 

Date Prepared/Revised 219/11 

c. 

County 

Indiana 

Color opaque white/orange Odor 

Number of Solid or Uquid Phases of Separation 

2 

10# 

Describe each phase 

- 1 -
c. 

d. 

a. 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

Facility Contact 

TIUe 

Phone 

Address Line 1 

Address Line 1 

Address City State ZIP 

Municipality 

c. Facility Contact 

Title 

Phone 

to processing or disposal facility In the 0 cuyd 0 gal 0 lb 

year. 0 lb 

-2-

0 ton 

Indiana 

(check one) 

{check one) 
D Fonn 26R 

0 Other {specify) 

Date Submitted: 

D I certify the Information required In Section B-2, Chemical Analysis was supplied to the Department for the year 

_and has not changed. 

Form Submitted: 0 Fonn 26R 

0 Other (specify) 

Date Submitted: 

D I certify the Information required In Section B-3, Process Description and Schematic, was supplied to the Department 

for the year_ and has not changed. 

Form Submitted: 0 Fonn 26R 

0 Other (specify) 

Date Submitted: 

-3-
Brine fluids are composited within the storage production tank or tank battery at each 

well site where gas production is occurring. Each automatic or manual ejection of 

formation fluids is deposited into the tank{s) and added to the previously ejected and 

stored quantity. Tanks are emptied into tank trucks for disposal at various PaDEP 

permitted waste disposal facilities on different schedules determined by individual well 

characteristics. Grab samples of the composited fluids were obtained at the 

represented well pads directly from the storage tank drain ports. All drain ports had 

small "built in" containment and storage "buckets" capable of retaining small amounts of 

lost fluids. 

Sa~ples were obtained with bottle sets prepared at the laboratory which contained 

appropriate preservatives, as necessary, depending on the specific test run requested. 

All chain of custody and handling/holding time requirements were met. In some cases, 

a larger sample was broken into appropriate sampling containers and smaller aliquot 

portions at the laboratory. 

Flowback samples were composited to the extent possible during the flowback process 

primarily during times where safety issues did not override sample collection 

requirements. 

Generally, a larger composite sample was broken into appropriate sampling containers 

and smaller aliquot portions at the laboratory or on the well location upon completion of 

the composite sampling process. Samples were distributed into bottle sets prepared at 

the laboratory which contained appropriate preservatives, as necessary, depending on 

the specific test run requested. All chain of custody and handling/holding time 

requirements were met. 

Drill cuttings were composite sampled during the drilling process at various times and 

combined into a composite sample for analyses at the laboratory. On several wells, 

cuttings from the vertical portion of the well bore were segregated from cuttings from 

the target Marcellus Formation and separate testing was completed on both sample 

composites. In some earlier cases during the utilization of open pits, composite 

samples were obtained from inactive drill pits. Safety concerns usually limited the 

randomness of the composite sample and composite grid sample positions were varied 

to the extent possible. 

Pit water {drill fluid) is currently discharged to closed containment and is re-conditioned 

and reused from well to well. 
Form 26R: Section 83a 

WASTE GENERATION PROCESS 

Pit Water "Drill Fluids" 

Remnant drill fluids are generated in the well bore during the penetration of the drill 

stem as it intercepts both ground water and formation fluids. These fluids are brought to 

the surface along with the drill ~ings, pieces of the intercepted rock strata, by the 

return flow system of the drilling process. 

Drill cuttings and drill fluids are isolated into separate waste streams. Cuttings are 

mixed with sawdust to absorb remnant fluid aod loaded out for disposal at a landfill. 

Fluids are currently stored in closed containers to be processed for reuse. 

Flowback: "Fracing Fluid" 

Flowback is produced from all fluids that flow back to surface during the "hydrofracing" 

process which occurs under pressure and results in the setting of a propant within the 

formation fractures. 

Production Fluid "Brine" 

During the production of natural gas, formation pressures bring remnant frac fluids, 

during the initial production phase, and formation fluids to the surface along with 

produced gas. 
Well I. D.# (various) Well I.D.#.(various) 

\\/ \\/ 

-a- -aCOUNTY A 

..... . ~....... __,.I' \ I 

\ / Well I. D.# (various) 

\ I -~/ \ I -0 \ /II' 

\ I / \ I // 

\ I / / 

. \ I / 

Well I.D.# (various) \ 1 // 

\\/ / \ I / 

-0- / " 

- COUNTYB 

cr ..... ~I ~o---- Fl.,..,L .. ..\<, :; ~ =ovo~ ~ Mobile Tank Truck 

~t"o~vc . .'tLot!\ Ocu 1t\~~~ l""\-..s :: ( 

J~ S brine (lYP.) 

Note: . Process producing waste: Gas well produced 

fluids (brines) are typically produced in 

conjuction wi.th natural gas. These fluids 

are brought to the surface utilizing either 

mechanical or physical lift procedures. 

_ s Road Transport 

----Landfill orTr~ +tv\ ~.,.J 'P \GV\ t 

() 

~ w 

:r: 

{.) 

C/) 

z 

0 

~ 

~ 0 

a.. 

(/) 

z 

~ 1-

1i11f 

~~~~ t 

.! ~ ~ 

i I ~ I ~ 

~~ ~ 

l

i - ~ ~ u -

~ g !~ 

~ I! Z N 

~ ~ l .. 

I 

~ a; 

; 

~ 

~ 
Report of Analysis 

Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

XTOEnergy 

395 Airport Road 

Indiana; PA 15701 

2fl612009 11:00 AM 

2!26fl009 12:43 PM 

3fl1fl009 

Bloom#8315 

Analyte 

Acidity to pH=8.3 

Alkalinity to pH=4.5 

Biological Oxygen Demand 05 

Chemical Oxygen Demand 

Ammonia as N I Distilled 

Chloride 

Kjeldahl Nitrogen as N 

pH(SM) 

Sulfate (ASTM) 

Total Nitrate+ Nitrite as N 

Aluminum - ICP 

Arsenic--ICP 

Barium -ICP 

Beryllium- ICP 

Boron 

Cadmium- ICP 

Calcium - ICP 

Chromium - ICP 

Cobalt-ICP 

Copper- ICP 

Hardness 

Analyst 

MS 

MS 

MAD 

AID 

AID 

MS 

AID 

MS 

KM 

JFW 

GJT 

GJT 

GJT 

GJT 

ES 

GJT 

GJT 

GJT 

GJT 

GJT 

DRM 

Comments; Radiologicals done by Benchmark Analytical 

~ DEP Certification fls 32-00382 

Analysis 

Date 

03/04/2009 

03/03fl009 

03/0212009 

03/02/2009 

03/0S/2009 

03/05fl009 

03/05/2009 

03/20!2009 

03/11/2009 

03/04!2009 

03/03/2009 

03/04/2009 

03/03/2009 

03/03/2009 

03/0312009 

03/03/2009 

03/0312009 

03/0312009 

03/0312009 

03/03fl009 

03/04/2009 

Sample ID#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Sample 

Result 

09 06141 

Waste Water 

Grab 

JW (Client) 

Bloom #8315 ~test 

Units Method 

189 mg/1 as CaC03 SM2310B 

147 mg/1 as CaC03 SM2320B 

148.1 mg/1 SM5210B 

2702.5 mgll SM5220D 

116.37 mgll )M4500NH3B & [ 

90602.0 mgll SM4500ClC 

127.7 mgll SM4500Norg-C,D 

5.55 su SM4500H-B 

ND mg/1 0516-02 

ND mg/1 SM4500N03E 

1.600 mgiJ 200.7/6010 

ND mg/1 200.7/6010 

4918.800 mg/1 200.7/6010 

ND mg/1 200.7/6010 

6.40 mg/1 SM4500B-B 

NO mg/1 200.716010 

10727.400 mg/1 200.7/6010 

ND mg/1 200.7/6010 

ND mg/1 200.7/6010 

ND mg/1 200.7/6010 

31695 mg/1 SM2340B 

MDL 

1 

20 

2.0 

500.0 

4.11 

1.0 

53.2 

0.01 

s 

0.05 

1.000 

1.000 

0.500 

0.500 

2.50 

0.500 

50.000 

0.500 

0.500 

0.500 

1 

jND=Not Detected 

Page 1 of3 
Report of Analysis 

Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

XTOEnergy 

395 Airport Road 

Indiana, PA 15701 

2!2612009 11:00 AM 

2126!2009 12:43 PM 

3(}.112009 

Bloom#8315 

Aoalyte 

Iron- ICP 

Iron,Dissolved-ICP 

Lead-ICP 

Lithium- ICP 

Magnesium-ICP 

Manganese - ICP 

Mercury 

Nickel- ICP 

Seleniwn-ICP 

Silver-ICP 

Sodium-ICP 

Strontium - ICP 

Zinc- ICP 

Osmotic Pressure 

Detergents, MBAS 

Ethylene Glycol 

Oil and Grease- HEM 

Phenolics, as Phenol 

Specific Conductance 

Total Dissolved Solids (TDS) 

Total Suspended Solids 

Analyst 

OJT 

GJT 

GJT 

GJT 

DRM 

GJT 

DMM 

GJT 

GJT 

GJT 

GJT 

DRM 

GJT 

AID 

JFW 

MetPeak 

CLM 

AID 

JH 

MAD 

MAD 

Comments: Radiologicals done by Benchmark Analytical 

Note: DEP Certification #Js 32-00382 

SampleiD#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Analysis Sample 

Date Result 

03/04fl009 112.900 

03104fl009 73.800 

03/03(}.009 ND 

03/03/2009 94.000 

03/04fl009 1192.000 

03/0312009 12.100 

03/06/2009 ND 

03/03/2009 ND 

03104fl009 ND 

03/03/2009 ND 

03/04/2009 35249.000 

03/04/2009 2845.000 

03/0412009 ND 

03/02(}.009 4050 

02127/2009 54.700 

03/0912009 93.904 

03/0412009 10.7 

03/06/2009 ND 

03/2312009 155133 

03/02fl009 179100 

03/02fl009 131 

09 06141 

WasteWater 

Grab 

1W (Client) 

Bloom #8315 Brine test 

Units Method 

mg/1 200.7/6010 

mg/l 200.7/6010 

mg/1 200.7/6010 

mgll 200.7/6010 

mgll 200.7/6010 

mg/1 200.7/6010 

mgll 245.1 

mgll 200.7/6010 

mg/1 200.7/6010 

mgll 200.7/6010 

mg/1 200.7/6010 

mgll 200.7/6010 

mg/1 200.7/6010 

mOslkg OSP 

mgll SM5540C 

mglkg 300.0M 

mg/l 1664A 

rngll 420.1 

uS/em SM2510B 

mg!l SM2540C 

mg/l SM2540D 

MDL 

1.000 

1.000 

0.500 

50.000 

500.000 

0.500 

0.0020 

0.500 

1.000 

0.500 

500.000 

10.000 

0.500 

1000 

10.000 

25.000 

5.0 

0.050 

I 

25 

5 

jND=Not Detected 

Page 2 of 3 
Report of Analysis 

Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

Radiologicals 

1) Benzene 

47) Toluene 

XTOEnergy 

395 Airport Road 

Indiana, PA 15701 

2126/2009 11:00 AM 

2126/2009 12:43 PM 

3121fl009 

Bloom ##8315 

Analyte Analyst 

enchma 

RO 

RO 

Comments; Radiologicals done by Benchmark Analytical 

Note: DEP Certification #s 32..()0382 

SampleiD#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Analysis Sample 

Date Result 

03/12/2009 • 

03/04/2009 ND 

03/0412009 ND 

09 06141 

Waste Water 

Grab 

IW (Client) 

Bloom #8315 Brine test 

Units Method 

nWl RAD-CTDHS 

ugiL 624/8260B 

ugiL 624/8260B 

MDL 

0.000 

20.00 

20.00 

FD=Not Detected 

Page 3 of3 
··, 

.. 

Name: Sample Start Date: Receipt Date: Report Date: Sample Site: I) Benzene 47) Toluene XTOEnergy 395 Airport Road Indiana, P A 1 5701 2/26/2009 2126/2009 1:47PM 3/S/2009 Bloom#8315 Analyte 

Note: DEP Certification #s 32-00382 

Report of Analysis 

Sample ID#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Analyst Analysis Sample 

Date Result 

RO 03/04n.009 ND 

RO 03/04n.009 ND 

09 06165 

Waste Water 

Trip Blank 

MH(Ciient) 

Trip Blank 

Units 

ug/L 

ug/L 

Method 

624/8260B 

624/8260B 

MDL 

1.00 

1.00 

Page 1 of 1 
COMPANY: Environmental Service Laboratories, Inc 

ADDRESS: 1803 Phlladafphia Strest 

PHONE: 

FAX: 

Indiana, PA 15701 

{124) 463-8378 

(724) 485-4209 

TEST REPORT 

0906069,06351,06841,06638,06637,06840,06141 

RECEIVED FOR LAB BY: DMB DATE: 03/08/2009 9:35 . 

PAGE: 1 of2 

POl: 

PWSIDi# 

Pqe 1 of2 

SAMPLE: qa 08141 

SAMPLED BY: DaYid A. Stilt 

Lab 10: O~B-007A 

S.mple Time 021281200911:00 

Gl'lb 

!!!l BuWI Y.!l5ald. Mea .u!!lll 

~ mi. &lallllll §Jars ~1111911 Et\11 aDIIltll..! 

Gloat Alpha 272.8 :t33U 1292 pOUL EPA900.0 ~88:30 D3/'1210t BPS.CV 

Grote Beta 637.4 :t 4&4.9 11512 pCUt. EPA900.0 03109109 8:30 0311':'08 BPS.CV 

-·--. -·· ·--·-·····--·-----·-·· . . ·····---··-·. ·----- -------.. -.-....... 

REMARKS: . 

The abcwe teat procedures meet all the requirements of NE:LAC and relate only to these samples . 

.. CV = Benchmark Analytlcs, Inc. Center Valley, PA; SA= Benchmark Analytios, loo. Sa~re, PA 

GER _. _/' .M ~ DATe: 3//612009 MANA - ------·-----~-" 'L!....~-·- -- --··--" ·----- --· ·----· 

7 
prepared. The date on attached sheets needs to match the .date noted below. 

General Reference 287.54 

Une 1 Company Mailing Address 2 

State Zip+4 Phone 

PA 15701 724-349-0600 

First Name Suffix 

Ben Mr. 

c. 

Number of Solid or Uquld Phases of Separation 

No 

Describe each phase of separation . .:..:.::~.=----------------; 

No 

- 1 -
~. d. 

a. 

c. 

b. 

Address Une 1 

Address Une 1 

Address City State ZIP 

Municipality 

rltle 

Phone 

Contact Name 

Volume of waste shipped to processing or D cu yd 181 gal D 1b 

steve@pabrine.com 

(check one) 

processing or being utilized. 

Facility Name 

Address Une 1 

Address Line 1 

Address City State ZIP 

Municipality 

Name 

Title 

Phone Email Address 

waste 

If "Yes", list the general pennit number or approval number. 

Volume of waste beneficially used in the previous year. D cuyd D gal D lb D ton 

- 2-

(check one) 
o

 Submltled: D Form 26R 

D Other (specify) 

Date Submltt8d: 

D I certify the Information required In Section B-2, Chemical Analysis was supplied to the Department for the year _and has not changed. 

Form Submitted: D Form26R 

D Other (specify) 

Date Submitted: 

0 I certify the Information required In Section B-3, Process Description and Schematic, was supplied to the Department for the year_ and has not changed. 

Form Submitted: 0 Form 26R 

Date Submitted: 

Name of Responsible Official 

Bernhardt Kissel 

Signature 

0 Other (specify) 

Shale 

Date 2-28-11 

-3-
Brine fluids are composited within the storage production tank or tank battery at each 

well site where gas production is occurring. Each automatic or manual ejection of 

formation fluids is deposited into the tank(s) and added to the previously ejected and 

stored quantity. Tanks are emptied into tank trucks for disposal at various PaDEP 

permitted waste disposal facilities on different schedules determined by individual well 

characteristics. Grab samples of the composited fluids were obtained at the 

represented well pads directly from the storage tank drain ports. All drain ports had 

small "built in" containment and storage "buckets" capable of retaining small amounts of 

lost fluids. 

Samples were obtained with bottle sets prepared at the laboratory which contained 

appropriate preservatives, as necessary, depending on the specific test run requested. 

All chain of custody and handling/holding time requirements were met. In some cases, 

a larger sample was broken into appropriate sampling containers and smaller aliquot 

portions at the laboratory. 

Flowback samples were composited to the extent possible during the flowback process 

primarily during times where safety issues did not override sample collection 

requirements. 

Generally, a larger composite sample was broken into appropriate sampling containers 

and smaller aliquot portions at the laboratory or on the well location upon completion of 

the composite sampling process. Samples were distributed into bottle sets prepared at the laboratory which contained appropriate preservatives, as necessary, depending on 

the specific test run requested. All chain of custody and handling/holding time 

requirements were met. 

Drill cuttings were composite sampled during the drilling process at various times and 

combined into a composite sample for analyses at the laboratory. On several wells, 

cuttings from the vertical portion of the well bore were segregated from cuttings from 

the target Marcellus Formation and separate testing was completed on both sample 

composites. In some earlier cases during the utilization of open pits, composite 

samples were obtained from inactive drill pits. Safety concerns usually limited the 

randomness of the composite sample and composite grid sample positions were varied 

to the extent possible. 

Pit water (drill fluid) is currently discharged to closed containment and is re-conditioned 

and reused from well to well. 
Form 26R: Section B3a 

WASTE GENERATION PROCESS 

Pit Water "Drill Fluids" 

Remnant drill fluids are generated in the well bore during the penetration of the drill 

stem as it intercepts both ground water and formation fluids. These fluids are brought to 

the surface along with the drill cuttings, pieces of the intercepted rock strata, by the 

return flow system of the drilling process. 

Drill and drill fluids are isolated into separate waste streams. Cuttings are 

mixed with sawdust to absorb remnant fluid and loaded out for disposal at a landfill. 

Fluids are currently stored in closed containers to be processed for reuse. 

Flowback: "Fracing Fluid" 

Flowback is produced from all fluids that flow back to surface during the "hydrofracing" 

process which occurs under pressure and results in the setting of a propant within the 

formation fractures. 

Production Fluid "Brine" 

During the production of natural gas, formation pressures bring remnant frac fluids, 

during the initial production phase, and formation fluids to the surface along with 

produced gas. 
Well I. D.# (various) Well r ... D.#.(various) 

-0 

'\/ -y-

~ /v, /1' 

I\ I 

\ / Well I. D.# (various) 

\ I ::::b/ 

\ I /II' 

\ I / 

\ I // 

\ I // 

. . \ I / 

Well I. D.# (various) \ 1 // 

'\/ / \ I ./ 

-0- / " ,-------. 

u~ '<'OF!"'"'~~; ~oVd~ Mobile Tank Truck 

~r--obl.vc..\1~.1\ Ocu'tt\~~~ 

- COUNTYB 

COUNTY A 

\MI<.S :: ( 

, J~ 5 brine (lYP.) 

Landfill Or' 

_ s Road Transport 

TrUA.+tv\(A+ 'Pl~t Note: . Process producing waste: Gas well produced 

fluids (brines) are typically produced in 

conjuction wi.th natural gas. These fluids 

are brought to the surface utilizing either 

mechanical or physical lift procedur_es. 

(.) 

w 

~ :r: 

~ 

z 

0 

~ 

~ 0 

0.. 

(/') 

~ 1-

,illf 

~~~I ii 

..! ~ ~ 

ill~~~~ 

~ ~ 

; ~ - le ~ Cl -

r !! ~ I! 

: ~ l~ 

II . 

~ 
Report of Analysis 

Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

XTOEnergy 

395 Airport Road 

Indiana, PA I 5701 

2/2612009 11:00 AM 

2/26/2009 12:43 PM 

31'21fl009 

Bloom#8315 

Analyte 

Acidity to pH=8.3 

Alkalinity to pH=4.5 

Biological Oxygen Demand 05 

Chemical Oxygen Demand 

Ammonia as N I Distilled 

Chloride 

Kjeldahl Nitrogen as N 

pH(SM) 

Sulfate (ASlM) 

Total Nitrate +Nitrite as N 

Aluminum - ICP 

Arsenic-ICP 

Barium-ICP 

Beryllium - ICP 

Boron 

Cadmium - ICP 

Calcium - ICP 

Chromium - ICP 

Cobalt-ICP 

Copper- ICP 

Hardness 

Analyst 

MS 

MS 

MAD 

AJD 

AID 

MS 

AID 

MS 

KM 

1FW 

GIT 

GJT 

GJT 

GIT 

ES 

GJT 

GJT 

GJT 

GIT 

GJT 

DRM 

Comments: Radiologicals done by Benchmark Analytical 

!ie!!!;. DEP Certification #Is 32..(){)3&2 

Analysis 

Date 

03104!2009 

03/03/2009 

03/0212009 

03/0212009 

03/05fl009 

03/05f2009 

03/05/2009 

03/2012009 

03/llf2009 

03/0412009 

03lo3/2009 

03/04fl009 

03/03/2009 

03/03/2009 

03/0312009 

03/03f2009 

03/0312009 

03/03f2009 

03/03/2009 

03/03/2009 

03/04/2009 

SampleiD#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Sample 

Result 

09 06141 

WasteWater 

Grab 

JW (Client) 

Bloom #8315 ~test 

Units Method 

189 mg/1 as CaC03 SM2310B 

I47 mg/1 as CaC03 SM2320B 

148.1 mgll SMS210B 

2702.5 mg/1 SM5220D 

116.37 mg/1 ~M4500NH3B & [ 

90602.0 mg/1 SM4500ClC 

127.7 mg/1 SM4500Norg-C,D 

5.55 su SM4500H-B 

ND mgll D516-02 

ND mg/1 SM4500N03E 

1.600 mg/1 200.7/6010 

ND mg/1 200.7/6010 

4918.800 mg/1 200.7/6010 

ND mg/1 200.7/6010 

6.40 mg/1 SM4500B-B 

ND mg/1 200.7/6010 

10727.400 mg/1 200.7/6010 

ND mg/1 200.7/6010 

ND mgll 200.7/6010 

ND mg/1 200.7/6010 

31695 mg/1 SM2340B 

MDL 

1 

20 

2.0 

500.0 

4.11 

1.0 

53.2 

0.01 

5 

0.05 

1.000 

1.000 

0.500 

0.500 

2.50 

0.500 

50.000 

0.500 

0.500 

0.500 

1 

jND=Not Detected 

Page 1 of3 
Report of Analysis 

Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

XTOEnergy 

395 Airport Road 

Indiana, PA 15701 

212612009 11:00 AM 

2126/2009 12:43 PM 

3/27/2009 

Bloom#831S 

Analyte 

Iron- ICP 

Iron,Dissolved-ICP 

Lead-ICP 

Lithimn- ICP 

Magnesium-ICP 

Manganese - ICP 

Mercury 

Nickel- ICP 

Selenium-ICP 

Silver-ICP 

Sodium-ICP 

Strontium - ICP 

Zinc- ICP 

Osmotic Pressure 

Detergents. MBAS 

Ethylene Glycol 

Oil and Grease- HEM 

Phenolics, as Phenol 

Specific Conductance 

Total Dissolved SoJids (TDS) 

Total Suspended Solids 

Analyst 

OJT 

GJT 

GIT 

GJT 

DRM 

GIT 

DMM 

orr 

GJT 

GJT 

OJT 

DRM 

GJT 

AID 

JFW 

IMetPeak 

CLM 

AID 

JH 

MAD 

MAD 

Comments: Radiologicals done by Benchmark Analytical 

Note; DEP Certification #s 32..00382 

SampleiD#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Analysis Sample 

Date Result 

03/04/2009 112.900 

03/0412009 73.800 

03/03/2009 ND 

03/03/2009 94.000 

03/04/2009 1192.000 

03/0312009 12.100 

03/06/2009 ND 

03/03/2009 ND 

03/0412009 ND 

03/03/2009 ND 

03/04/2009 35249.000 

03/04/2009 2845.000 

03/0412009 ND 

03/02/2009 4050 

02/27f1.009 54.700 

03/09/2009 93.904 

03/04f1.009 10.7 

03/06/2009 ND 

03/23/2009 155133 

03/02f1.009 179100 

03/02/2009 131 

09 06141 

WasteWater 

Grab 

1W (Client) 

Bloom #831 5 Brine test 

Units Method 

mg/1 200.7/6010 

mgll 200.7/6010 

mgll 200.7/6010 

mg.ll 200.7/6010 

mgll 200.7/6010 

mg.ll 200.7/6010 

mg.ll 245.1 

mg.ll 200.7/6010 

mgll 200.7/6010 

mgll 200.7/6010 

mg/1 200.7/6010 

mg/1 200.7/6010 

mg/1 200.7/6010 

mOslkg OSP 

mg/1 SMS540C 

mglkg 300.0M 

mg/1 1664A 

mgll 420.1 

uS/em SM2510B 

mgll SM2540C 

mgll SM2540D 

MDL 

1.000 

1.000 

0.500 

50.000 

500.000 

0.500 

0.0020 

0.500 

1.000 

0.500 

500.000 

10.000 

0.500 

1000 

10.000 

25.000 

5.0 

0.050 

1 

25 

5 

[NI>=Not Detected 

Page 2 of3 
Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

R.adiologicals 

1) Benzene 

47) Toluene 

XTOEnergy 

395 Airport Road 

Indiana, PA 15701 

212612009 11:00 AM 

212612009 12:43 PM 

3121fl009 

Bloom ##8315 

Analyte 

Report of Analysis 

SampleiD#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Analyst Analysis Sample 

Date Result 

enchmw 03/1212009 "' 

RO 03/04/2009 ND 

RO 03/04/2009 ND 

Comments: Radiologicals done by Benchmark Analytical 

Note: DBP Certification #s 32..00382 

09 06141 

Waste Water 

Grab 

JW (Client) 

Bloom #831 5 Brine test 

Units Method 

mg/1 RAD-CIDHS 

ug/L 624/8260B 

ug/L 624/8260B 

MDL 

0.000 

20.00 

20.00 

fD=Not Detected 

Page 3 of3 
Name: 

Sample Start Date: 

Receipt Date: 

Report Date: 

Sample Site: 

1) Benzene 

47) Toluene 

XTOEnergy 

395 Airport Road 

Indiana, PA 15701 

2/26/2009 

2/26/2009 1:47PM 

3/S/2009 

Bloom#8315 

Analyte 

Nota: DEP Certification #s 32-00382 

Report of Analysis 

SampleiD#: 

Sample Type: 

Sample Source: 

Sampler: 

Client Sample ID: 

Analyst Analysis Sample 

Date Result 

RO 03/04/2009 ND 

RO 03/04/2009 ND 

09 06165 

Waste Water 

Trip Blank 

MH (Client) 

Trip Blank 

Units 

ug/L 

ug/L 

Method MDL 

624/82608 1.00 

624/82608 1.00 

IND=Not Detected 

Page 1 of 1 
COMPANY: Environmental Service Laboratories, Inc 

ADDRESS: 1803 PhUadafphia Street 

Indiana, PA 15701 

PHONE: {124) 463-8378 TEST REPORT 

FAX: (724) 455-4209 

0906069,06351,06841,06638,06637,08840.06141 

RECEIVED FOR LAB BY: DMB DATE: 03/08/2009 9:35 . 

PAGE: 1 or2 

PO#: 

PWSIO# 

PIIJO 1 of2 

SAMPLE: C!8 08141 

SAMPLED BY: David A. Stilt 

Lab 10: 08030&4G-007A 

S.mple Time 02/281200911:00 

Grab 

!!It 8uWl Y!af!. .MDa .u.!!IJl .Malhml M.ttL Mlll!lll b!S A!lab!:lllliiKI &l!ll!ll! 

Gloat Alpha 272.9 :t 338.4 12512 pOUt. EPA900.0 03IOQic)t 8:30 c311me BPS.CV 

GroleBeta 837.4 :t 4M.9 11112 pCUL EPA&OO.O 03109109 8:30 

0311~ BPS.CV 

-·--. -·· ·-··----·---·--- --·--· 0 

-

····---····-. 0 

·----- ---------

.. 

-

.... ·-· 

REMARKS: . 

The above test prooedures meet all the requirements of NeLAC and relate only to these samples . 

.. CV = Benchmark Analytlca, Inc. Center Valley, PA; SA = Benchmark Analytios, lno. Sayre, PA 

"' ./- I'M ~ DATe: 3/1612009 

MANAGER _ -----------~--.l.!.....~-.. ··--· --··--- .---- ---· ·-----

7