Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

-down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.EIA

Facility Code Facility Name Boiler ID Fuel Type 1

52007 Mecklenburg Power Station 1 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 52007 Mecklenburg Power Station 1 As Received Higher Heating Value 

### 52007 Mecklenburg Power Station 1 As Received % Moisture 

### 52007 Mecklenburg Power Station 1 As Received % Ash 

### 52007 Mecklenburg Power Station 1 As Received % Sulfur 

### 52007 Mecklenburg Power Station 1 Dry basis Higher Heating Value 

### 52007 Mecklenburg Power Station 1 Dry basis % Ash 

### 52007 Mecklenburg Power Station 1 Dry basis % Sulfur 

### 52007 Mecklenburg Power Station 1 Dry basis Antim ony 

### 52007 Mecklenburg Power Station 1 Dry basis Arsenic 

### 52007 Mecklenburg Power Station 1 Dry basis Beryllium 

### 52007 Mecklenburg Power Station 1 Dry basis Cadmium 

### 52007 Mecklenburg Power Station 1 Dry basis Chlorine 

### 52007 Mecklenburg Power Station 1 Dry basis Chromium 

### 52007 Mecklenburg Power Station 1 Dry basis Cobalt 

### 52007 Mecklenburg Power Station 1 Dry basis Fluorine 

### 52007 Mecklenburg Power Station 1 Dry basis Lead 

### 52007 Mecklenburg Power Station 1 Dry basis Manganese 

### 52007 Mecklenburg Power Station 1 Dry basis Mercury 

### 52007 Mecklenburg Power Station 1 Dry basis Nickel 

### 52007 Mecklenburg Power Station 1 Dry basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D3302 and ASTM D3173 ASTM D3174/D5142 ASTM D4239 Method B ASTM D5865 ASTM D3174/D5142 ASTM D4239 Method B ASTM D3683 ASTM D3683 ASTM D3683 ASTM D3683 ASTM D6721 ASTM D3683 ASTM D3683 ASTM D3761 ASTM D3683 ASTM D3683 ASTM D6722 ASTM D3683 ASTM D3683EIA Facility Code Facility Name Boiler ID 

### 52007 Mecklenburg Power Station 1

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) M26A/M30B/CEMS-RUN1 

### 3/30/2010 3/30/2010 12617.00 M26A/M30B/CEMS-RUN2 

### 3/31/2010 3/31/2010 13035.00 M26A/M30B/CEMS-RUN3 

### 4/1/2010 4/1/2010 13409.00 Fuel Testing ResultsHAPs Test Group



### Acid gas HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 8.25 7.78 1.14 13751 Btu/lb 4.85 8.66 1.18 13700 Btu/lb 4.76 8.89 1.04 14709HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### Btu/lb 8.48 1.24 2200 ppm 0.14 ppm Btu/lb 9.1 1.24 1900 ppm 0.14 ppm Btu/lb 9.33 1.09 2100 ppm 0.09 ppmAntimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 2 ppm 9 ppm 3 ppm < 2 ppm 19 < 2 ppm 9 ppm 3 ppm < 2 ppm 25 < 2 ppm 9 ppm 3 ppm < 2 ppm 18Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm 13 ppm 25 ppm 18 ppm < 2 ppm ppm 13 ppm 20 ppm 28 ppm < 2 ppm ppm 13 ppm 27 ppm 16 ppm < 2 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 191 ppm 11 ppm 84 ppm 11 ppm 64 ppm 11 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 

### 52007 Mecklenburg Power Station 1

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) OTM27/28-RUN1 

### 3/31/2010 3/31/2010 12772.00 OTM27/28-RUN2 

### 4/1/2010 4/1/2010 12547.00 OTM27/28-RUN3 

### 4/2/2010 4/2/2010 12906.00

M29-RUN1 

### 3/30/2010 3/30/2010 12809.00 M29-RUN2 

### 3/31/2010 3/31/2010 13128.00 M29-RUN3 

### 3/31/2010 3/31/2010 12926.00 Fuel Testing ResultsHAPs Test Group



### Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 5.96 9.25 1.06 13582 Btu/lb 6.7 9.02 1.02 13448 Btu/lb 5.36 8.96 1.08 13637

Btu/lb 5.19 9.85 0.98 13510 Btu/lb 5.08 7.81 0.98 13831 Btu/lb 5.8 8.43 1.17 13721HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### Btu/lb 9.84 1.13 1900 ppm 0.1 ppm Btu/lb 9.66 1.09 2000 ppm 0.11 ppm Btu/lb 9.47 1.14 1700 ppm 0.1 ppm

Btu/lb 10.39 1.04 2100 ppm 0.08 ppm Btu/lb 8.23 1.03 2000 ppm 0.08 ppm Btu/lb 8.95 1.24 770 ppm 0.12 ppmAntimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 2 ppm 6 ppm 4 ppm < 2 ppm 25 < 2 ppm 7 ppm 4 ppm < 2 ppm 20 < 2 ppm 8 ppm 3 ppm < 2 ppm 20

< 2 ppm 6 ppm 4 ppm < 2 ppm 26 < 2 ppm 5 ppm 3 ppm < 2 ppm 22 < 2 ppm 10 ppm 3 ppm < 2 ppm 23Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm 14 ppm 20 ppm 25 ppm < 2 ppm ppm 14 ppm 29 ppm 18 ppm < 2 ppm ppm 13 ppm 23 ppm 16 ppm < 2 ppm

ppm 14 ppm 24 ppm 20 ppm < 2 ppm ppm 12 ppm 20 ppm 23 ppm < 2 ppm ppm 16 ppm 22 ppm 22 ppm < 2 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 140 ppm 12 ppm 73 ppm 12 ppm 66 ppm 11 ppm

85 ppm 13 ppm 69 ppm 11 ppm 70 ppm 12 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 

### 52007 Mecklenburg Power Station 1

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) M30B-RUN2 

### 3/31/2010 3/31/2010 12660.00 M26A/M30B/CEMS-RUN3 

### 4/1/2010 4/1/2010 13409.00 M30B-RUN4 

### 4/1/2010 4/1/2010 12922.00 Fuel Testing ResultsHAPs Test Group



### Mercury and non-mercury metalic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 6.19 9.67 1.18 13495 Btu/lb 4.76 8.89 1.04 14079 Btu/lb 4.93 9.46 0.95 13592HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### Btu/lb 10.3 1.26 970 ppm 0.11 ppm Btu/lb 9.33 1.09 2100 ppm 0.09 ppm Btu/lb 9.95 1 1800 ppm 0.09 ppmAntimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 2 ppm 13 ppm 4 ppm < 2 ppm 24 < 2 ppm 9 ppm 3 ppm < 2 ppm 18 < 2 ppm 6 ppm 4 ppm < 2 ppm 20Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm 17 ppm 16 ppm 17 ppm < 2 ppm ppm 13 ppm 27 ppm 16 ppm < 2 ppm ppm 12 ppm 30 ppm 16 ppm < 2 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon Carbon 

### 64 ppm 13 ppm 64 ppm 11 ppm 65 ppm 11 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wtEIA Facility Code Facility Name Boiler ID 

### 52007 Mecklenburg Power Station 1

Sample Number (minimum of 3 composite samples) Test Start Date (MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) M26A/M30B/CEMS-RUN1 

### 3/30/2010 3/30/2010 12617.00 M26A/M30B/CEMS-RUN2 

### 3/31/2010 3/31/2010 13035.00 M26A/M30B/CEMS-RUN3 

### 4/1/2010 4/1/2010 13409.00 Fuel Testing ResultsHAPs Test Group



### Non-dioxin/furan organic HAPs

HHV Units % Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) 

### Btu/lb 8.25 7.78 1.14 13751 Btu/lb 4.85 8.66 1.18 13700 Btu/lb 4.76 8.89 1.04 14709HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units 

### Btu/lb 8.48 1.24 2200 ppm 0.14 ppm Btu/lb 9.1 1.24 1900 ppm 0.14 ppm Btu/lb 9.33 1.09 2100 ppm 0.09 ppmAntimony

(Dry Basis) Antimony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) 

### < 2 ppm 9 ppm 3 ppm < 2 ppm 19 < 2 ppm 9 ppm 3 ppm < 2 ppm 25 < 2 ppm 9 ppm 3 ppm < 2 ppm 18Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units 

### ppm 13 ppm 25 ppm 18 ppm < 2 ppm ppm 13 ppm 20 ppm 28 ppm < 2 ppm ppm 13 ppm 27 ppm 16 ppm < 2 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Fluorine (Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles As h Fixed Carbon 

### 191 ppm 11 ppm 84 ppm 11 ppm 64 ppm 11 ppm Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Carbon Hydrogen Nitrogen Total Sulfur Oxygen

Ultimate Analy

ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/Kg ppmUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm