*all results reported as moisture free

*all results pooled from all 7 samples

Average Low High Low High Low High

Metals (mg/kg)

0.36 0.17 0.59 0.6 n.d. 70 (2), (4) n.d. 26 (2)

23.17 1.95 65.70 61.4 n.d. 2200 (2), (4) n.d. 298 (2)

n.d. n.d. n.d. n.d. n.d. 206 (2) n.d. 32 (2), (3)

0.16 0.13 0.25 0.3 n.d. 160 (2) n.d. 17 (2)

27.40 3.01 73.20 70.2 n.d. 200 (2) n.d. 340 (2)

0.62 0.38 1.52 1.52*** n.d. 180 (2) n.d. 213 (2)

33.10 8.78 96.80 85.9** n.d. 1900 (2) n.d. 340 (2)

59.14 38.60 156.00 156*** n.d. 2500 (2) n.d. 15800 (2)

0.03 0.02 0.05 0.0 n.d. 63 (2) n.d. 1.1 (2)

2.11 1.06 5.05 4.27** n.d. 730 (2), (4) n.d. 540 (2)

0.28 0.27 0.31 0.31*** n.d. 150 (2) n.d. 66 (2), (3)

112.79 45.17 302.06 294.3 n.d. 6086 n.d. 17249

146.35 54.37 399.47 380.5 n.d. 8359 n.d. 17673.1

Halides

6.14 6.00 7.00 7*** 0.04 160 (4) ‐‐ ‐‐ ‐‐

102.14 90 130 125.6 n.d. 9080 (2) n.d. 5400 (2)

16.57 5 25 25*** n.d. 4900 (2), (4) n.d. 490 (2), (3)

Total Halides (mg/kg) 124.86 101.00 162.00 158 0.04 14140 0 5890

‐‐ ‐‐ ‐‐ ‐‐ n.d. 38000 (2) ‐‐ ‐‐ ‐‐

9.1 7.1 13.5 12.11** 700 5400 (2) ‐‐ ‐‐ ‐‐

31329 9300 110000 76060** ‐‐ ‐‐ ‐‐ 1600 27000 (2)

31.0 25.4 35.8 37.2* ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

24.7 18.6 41.7 41.7*** ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

13.0 10.0 26.0 26*** ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

‐‐ ‐‐ ‐‐ ‐‐ 4000 28000 (2) ‐‐ ‐‐ ‐‐

131.23 80.60 179.00 176.7* ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

36.9 21.7 49.4 53.06* 1000 26000 (2) ‐‐ ‐‐ ‐‐

193.71 144.00 221.00 237* 8600 56000 (2) ‐‐ ‐‐ ‐‐

Total Volatile Compounds (g/kg) 31768 9607 110566 76644 14300 153400 1600 27000

Minnesota C&D1

Cobalt  (HAP)

Chromium  (HAP)

Coal Wood/Biomass

Range 90% UPL

Results*

Range

Reference

Range

Bromine (mg/kg)

Lead  (HAP)

Manganese  (HAP)

Mercury  (HAP)

Nickel  (HAP)

Selenium  (HAP)

Total Low Volatile Metals (mg/kg)5

Total Metals (mg/kg)

Reference

Antimony  (HAP)

Arsenic  (HAP)

Beryllium  (HAP)

Cadmium  (HAP)

Ethyl benzene  (HAP)

Formaldehyde  (HAP)

Methylene chloride  (HAP/OH)

m,p‐Xylenes  (HAP)

o‐Xylenes  (HAP)

Total Xylenes

Naphthalene  (PAH)

Styrene  (HAP)

Toluene  (HAP)

Chlorine (mg/kg)

Fluorine (mg/kg)

Volatile Compounds (g/kg)

Benzene  (HAP)

Minnesota example comparison 1out of 275

Total Volatile Compounds (g/kg) 31768 9607 110566 76644 14300 153400 1600 27000

Semi‐Volatile Compounds (g/kg)

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

n.d. n.d. n.d. n.d. ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

8743 8240 8970 8970**** ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

9727 4450 15200 15200*** ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

Total Semi‐Volatile Compounds (g/kg) 18469 12690 24170 24170 ‐‐ ‐‐ ‐‐ ‐‐ ‐‐ ‐‐

NA NA NA NA 6000 253000 (2) ‐‐ ‐‐ ‐‐

NA NA NA NA 14000 2090000 (2) ‐‐ ‐‐ ‐‐

Total Polycyclic Aromatic Hydrocarbons (g/kg) ‐‐ ‐‐ ‐‐ ‐‐ 14000 2090000 ‐‐ ‐‐ ‐‐

Total Organic HAPs (mg/kg) 50 22 135 101 28 2243.4 1.6 27.0

* All 90% UPL Results reported as Normal              ** 90% UPL Result reported as Lognormal

*** 90% UPL Result Non‐Parametric       **** Maximum Value Used, Sample Size Too Small For Statistical Analysis

n.d. = Non‐Detect               '‐‐ = No Data

NA ‐ Not applicable; PAH's accounted for in testing of Volatile Compounds and Semi‐Volatile Compounds

Resources:

1: Sample Results from C&D Processing Facility in Minnesota. Facility is a member of CMRA.

2: EPA Letter "Contaminant Concentrations in Traditional Fuels: Tables for Comparison." November 29, 2011.

3: EPA Letter to Joseph Knapik‐ International Paper Products Corporation. October 5, 2011.

4: USGS Coal Database; http://energy.er.usgs.gov/coalqual.htm (all data based on coal from U.S.)

5: Low Volatile Metals as defined in 40 CFR 63.1219(e)(4)

Anthracene (PAH)

Acenaphthene (PAH)

Acenaphthylene (PAH)

Benzo(k)fluoranthene (PAH)

Chrysene (PAH)

Dibenz(a,h)anthracene (PAH)

Fluoranthene (PAH)

Benzo(a)anthracene (PAH)

Benzo(a)pyrene (PAH)

Benzo(b)fluoranthene (PAH)

Benzo(g,h,i)perylene (PAH)

Polycyclic Aromatic Hydrocarbons (g/kg)

16‐PAH

PAH (52 extractable ‐ includes previous 16)

Fluorene (PAH)

Indeno(1,2,3‐cd)pyrene (PAH)

Phenanthrene (PAH)

Pentachlorophenol6

Pyrene (PAH)

Phenol  (HAP)

Minnesota example comparison 1out of 275
*all results reported as moisture free

*all results pooled from all 7 samples

MDL Non‐Detect Average Standard Deviation Low High

Components as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free

‐‐ 0 13.80 1.09 12.05 15.2 15.47‐‐ 0.56 0.64 0.56 0.65 0.59 0.7 0.58 0.68 0.6 0.7 0.54 0.63 0.45 0.52 0 0.65 0.06 0.52 0.7 0.741‐‐ 71.45 81.24 70.08 80.57 68.59 80.89 69.24 81.37 69.96 81.44 69.98 81.24 70.31 81.24 0 81.14 0.31 80.57 81.44 81.61‐‐ 15.95 18.13 16.34 18.78 15.62 18.42 15.28 17.96 15.34 17.85 15.62 18.13 15.78 18.24 0 18.22 0.31 17.85 18.78 18.69‐‐ 0 6.00 0.05 5.95 6.12 6.12***‐‐ 0 50.51 0.16 50.20 50.72 50.75‐‐ 0 0.23 0.03 0.19 0.29 0.28‐‐ 0 42.60 0.23 42.36 43.08 43.08***‐‐ 0 0.02 0.00 0.01 0.021 0.022‐‐ 7602 8644 7179 8254 7142 8423 7338 8624 7408 8624 6919 8033 7620 8805 0 8487 267 8033 8805 8898

Metals (mg/kg)

0.08 0 0.36 0.15 0.17 0.59 0.58

0.12 0 23.17 24.87 1.95 65.7 61.44

0.008 0 0.008 0.000 0.008 0.008 n.d.0.007 0 0.16 0.04 0.13 0.25 0.3

0.02 0 27.40 27.83 3.01 73.2 70.240.04 0 0.62 0.41 0.38 1.52 1.52***0.13 0 33.10 30.47 8.8 96.8 85.9**

0.009 0 59.14 43.10 38.6 156 156***0.003 0 0.03 0.01 0.015 0.049 0.048

0.04 0 2.11 1.41 1.06 5.05 4.27**0.27 0 0.28 0.02 0.27 0.31 0.31***

Total Metals (mg/kg) ‐‐ ‐‐ 146.36 97.7 75.18 295.95 295.9***

Formaldehyde (g/kg)

420 0 31328.57 35510.88 9300 110000 76060**

Ions

6 0 6.14 0.38 6 7 7***

40 0 102.14 15.24 90 130 125.6

6 0 16.57 10.21 5 25 25***

Total Halogens (mg/kg) ‐‐ ‐‐ 124.86 24.07 101.00 161.00 161.9

Volatile Compounds (g/kg)

var 0 4.5 0.1 4.43 4.61 4.61***var 0 7.7 0.2 7.50 7.81 7.81***var 0 2.6 0.1 2.50 2.6 2.6***var 0 2.0 0.0 1.93 2 2***var 0 61.0 1.2 59.7 62 62***var 0 135.9 2.7 133 138 138***var 0 51.1 1.1 50.0 52.0 52***var 0 7.1 0.1 6.9 7.2 7.2***var 0 3.4 0.1 3.270 3.410 3.41***var 0 6.7 0.1 6.54 6.81 6.81***var 0 2.8 0.1 2.70 2.81 2.81***var 0 3.5 0.1 3.47 3.6 3.6***var 0 4.5 0.1 4.43 4.61 4.61***var 0 9.1 2.1 7.12 13.5 12.11**var 0 4.5 0.1 4.43 4.61 4.61***var 0 2.8 0.1 2.70 2.81 2.81***var 0 24.7 7.7 18.60 41.7 41.7***var 0 7.7 0.2 7.50 7.81 7.81***var 0 5.1 0.1 5.00 5.2 5.2***var 0 31.0 4.0 25.4 35.8 37.2var 0 131.2 29.5 80.60 179 176.7var 0 6.3 0.1 6.16 6.4 6.4***var 0 13.0 5.8 10.00 26 26***var 0 36.9 10.5 21.7 49.4 53.06var 0 4.9 0.1 4.8 5 5***var 0 193.7 28.1 144.0 221.0 237var 0 5.1 0.1 5.00 5.2 5.2***

Total Volatile Compounds (g/kg) ‐‐ ‐‐ 768.74 48.8 697.49 827.7 843.8

Semi‐Volatile Compounds (g/kg)

var 0 5681.4 83.0 5560 5730 5730***var 0 3698.6 53.7 3620 3730 3730***var 0 5958.6 87.8 5830 6010 6010***var 0 5144.3 78.1 5030 5190 5190***var 0 4512.9 63.4 4420 4550 4550***var 0 2080.0 34.2 2030 2100 2100***var 0 3698.6 53.7 3620 3730 3730***var 0 5324.3 78.1 5210 5370 5370***var 0 7667.1 107.3 7510 7730 7730***var 0 5057.1 73.2 4950 5100 5100***var 0 4780.0 68.3 4680 4820 4820***var 0 4257.1 48.6 4150 4280 4280***var 0 4152.9 63.4 4060 4190 4190***var 0 7217.1 107.3 7060 7280 7280***var 0 3878.6 53.7 3800 3910 3910***var 0 4242.9 63.4 4150 4280 4280***var 0 3341.4 48.8 3270 3370 3370***var 0 2350.0 34.2 2300 2370 2370***var 0 4690.0 68.3 4590 4730 4730***var 0 5324.3 78.1 5210 5370 5370***var 0 3698.6 53.7 3620 3730 3730***var 0 3975.7 58.6 3890 4010 4010***var 0 4022.9 157.7 3680 4100 4100***var 0 4152.9 63.4 4060 4190 4190***var 0 4152.9 63.4 4060 4190 4190***var 0 4780.0 68.3 4680 4820 4820***var 0 4332.9 63.4 4240 4370 4370***var 0 4242.9 63.4 4150 4280 4280***var 0 4332.9 63.4 4240 4370 4370***var 0 4960.0 68.3 4860 5000 5000***var 0 3071.4 48.8 3000 3100 3100***var 0 2797.1 39.0 2740 2820 2820***var 0 3698.6 53.7 3620 3730 3730***var 0 4422.9 63.4 4330 4460 4460***var 0 3521.4 48.8 3450 3550 3550***var 0 25050.0 48114.3 3190 134000 8970 var 0 3788.6 53.7 3710 3820 3820** *var 0 8935.7 5062.5 4190 15200 15200***var 0 4152.9 63.4 4060 4190 4190***

Total Semi‐Volatile Compounds (g/kg) ‐‐ ‐‐ 185767 45561 160490 288010 288010***

* All 90% UPL Results reported as Normal MRL = Method Reporting Limit

** 90% UPL Result reported as Lognormal MDL = Method Detection Limit = Nondetect; Reported as MDL

*** 90% UPL Result Non‐Parametric HAP = Hazardous Air Pollutant **** Outlier value of Pentachlorophenol not included. Outlier more than 392 times the standard deviation of remaining values.

‐‐ = Non‐Detect OH = Organic Halogen

n.d. = Only 1 Distinct Value, therefore no variance. N = Nitrogenated

170700

0.018

288010

827.7 760.7 780.2 697.5 788.5 813.7 712.9

3730 3730 3730

7730

160750 160490 175730 167440

4010

4190

8240

281.2

2100 20303730 36205190

20.6

3000

601039107730

6.16

5190

3730

7280 7280

90% UPLResults*

7.52.5

2

7.5

1.9359.7

50.56

0.25

42.41

4.61

13.5

Wednesday 8/15 (a) Wednesday 8/15 (b) Thursday 8/16

4.61

8.2

23.6

7.81 7.81

7.2

14.91 14.10.00950.7242.36

4.61

8.4

5.98

2.81

4.617.81

6.81

2.81

3.6

2.81

3.6

0.02150.5342.570.008

7.81

2.6

2

62

4.611.3186.1

3620

5

144

4.81

13.87

2100 2030

6.54

2.7

3.6

5.99 5.9587.3

0.014

50.20.23

42.6 43.08

295.9

4.43

133

6.934.433.47

13.45

2.7

41.74.43

26

21.7

5

3.270.27

6

25

130

110000

0.4350.4

156

177250

6010 58308940

5650

3820 37104370

15200

5190 5030

134000

4060

7730455037304190

4240

Friday 8/17

5026

6.16

4060

4010 38903550 3450

43303000

4460

468027404860

3730 3620500028204100 36804370 4240

468044205210751049503620

5370

4680

36204060

75105210

4820

36203270

4420

4250

3370 3270

2300

5370

21004010

201

5

12.05 13.03 15.2

6.12 6 5.99

50.57

0.2

50.5

4820

5100 5100 5100

18.67.81

4.81

2.8

22.1

7.5

4060 4190

6

0.22

3450

31005100

3910 39105370

39.2 48

166

5.2 5.2

5.2

31.6

6.4

10.6

7730

4.61

5

4.61

3620

37302820

4190

37304190 41904820 4820

3190 3190 8820 8970355031004190 4190

4460 4460

4370 4370

4190

4190

3550 3550

3730

4010419044604820

4100

3820 3820 3820

3550

3100 3100 3100

4100

4190

4370 4370

2820 2820

4010

4820 4820 4820

4100 41004370 4370 4370

5370

2370 2370 23705370 5370

4190

3730 37304450

4950

4280

13800 5360 13900

3820

3370 3370 3370

3710

4190

4280 4280 4280 42803910

4330

4190 4190 4190 41903370

4730

3730

5.2

33.2

4.61

2.81

6.4

10.2

221

5

2.81

5

34.6 30.2

5.2

140

49.4

5

10.441.7

6.4 6.16

11.8

125

25.428.2

5730 57304460

5 4.81

6010

5.2

215

2100

28203730

29.80

210072804730

12.30

5

207

2.81

21.7

7.5

5

24.67.81

5.2

2.7

35.8

1.9359.7

138 133 138

52

133

50

4.617.81

2.6

2

62

138

62

138

2.6

6.812.81

3.41 3.41

52 52

9.2 8.27

4.43

3.6

7.2

6.54

7.2

4.61

8.8

6.81

7.2

3.416.81

6.933.27 3.41

7.124.434.43

141.0 125.0

7.81

3.474.43

2.814.61 4.43

2.6

2

62

2.7

6.93

3.276.54

2.7

3.47

7.5 7.5

52 50

2.5 2.5

25

6 6

90

6

0.27 0.31

6

90

6

0.27 0.27

7

110

18000

95

5

106.3 92.5 75.2

0.3896.841.5

0.049

34.6

39.4 44.10.46

0.04 0.0320.4141.355.3

12.5

0.017

0.5965.7

0.008 0.008

0.3716.9

0.41

0.29

73.2

0.14

14

0.133.01

0.18

0.19

0.018 0.015

42.58

0.01

0.35

11.2 13.8

21.2

0.008

50.48

0.02

4.1

0.008161.0

0.008

0.14

0.008

0.1460.1

38.6

0.13

101.0

1.35 1.06 5.050.418.78

0.015 0.027

15.739.1

1.52

22

Manganese (HAP)

Chlorine (mg/kg)Fluorine (mg/kg)

Minnesota C&D SUMMARY

16.2

0.51 0.62

16000 17000

2.34

0.29 0.272.44

Monday 8/13 Wednesday Tuesday 8/14 8/15

0.182.21

42.57

0.23

0.25

Range

0.171.95

o‐Xylenes (HAP)Chloroform (HAP/OH)

9300

Bromine (mg/kg)1,1,2,2‐Tetrachloroethane (HAP/OH)

Mercury (HAP)Nickel (HAP)

Selenium (HAP)

142.0 102.0

1.9359.7

4.43

24

1.2

6

110

15000

25

6

90

4.61

34000

102.0

n‐Hexane (HAP)

1,2,4‐Trichlorobenzene (HAP/OH)

Styrene (HAP)

Tetrachloroethylene (HAP/OH)Toluene (HAP)

Chlorobenzene (HAP/OH)

Moisture (wt%)

Ash (wt%)Volatile Matter (wt%)

Fixed Carbon (wt%)

Heating Value (BTU/lb)

Antimony (HAP)Hydrogen (wt%)Carbon (wt%)

Nitrogen (wt%)Oxygen (wt%)Cadmium (HAP)

Chromium (HAP)

Cobalt (HAP)

Lead (HAP)Vinyl chlorideNaphthalene (HAP)

Methyl tert butyl ether (HAP)

Methylene chloride (HAP/OH)

2,4‐Dinitrotoluene (HAP/N)

2‐Methylnaphthalene

2,4,6‐Trichlorophenol (HAP/OH)2,4‐Dinitrophenol (HAP/N)

Sulfur (wt%)Nitrobenzene (HAP/N)

1,4‐Dichlorobenzene (HAP/OH)

Isopropylbenzene (HAP)

m,p‐Xylenes (HAP)

Methyl methacrylate (HAP)

HexachloroethaneFluoreneFluoranthene1‐Methylnaphthalene

2,4,5‐Trichlorophenol (HAP/OH)ChryseneDibenz(a,h)anthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneArsenic (HAP)Beryllium (HAP)Hexachlorobutadiene (HAP/OH)

Formaldehyde

4550

5560

6010

4550

50305830

3730 3730 3730

5730 5560

80.6 140 136 118

6.4

10

5.2

202

5730

PyrenePhenolPhenanthreneIndeno(1,2,3‐cd)pyrene

Naphthalene (HAP)

AcenaphtheneAcenaphthyleneAcetophenoneAnilinePentachlorophenol (HAP/OH)Biphenyl (HAP)

Bis(2‐ethylhexyl)phthalate (HAP)

Benzo(g,h,i)peryleneBenzo(k)fluorantheneDibenzofurans (D/F)

Dimethyl phthalate (HAP)

Hexachlorobenzene (HAP/OH)Hexachlorocyclopentadiene (HAP/OH)

Hexachlorobutadiene (HAP/OH)

4190

4150 42804680 4820

3730

4060

23704190

398040603890

41504060

4730

2370

5210

70604150 4280 4150

706038004590

3800

72803910

5210 5370

42804370 4240

4280

5370

23004150

Benzene (HAP)

Bromoform (HAP/OH)Acrolein (HAP)Acrylonitrile (HAP/N)Allyl chloride (HAP/OH)1,1,2‐Trichloroethane (HAP/OH)

4190

Acetonitrile (HAP/N)

4730

72804280 4280 4280

Anthracene

179

3,3‐Dichlorobenzidene (HAP/OH/N)4‐Nitrophenol (HAP/N)

5730

5370 5370

4550

5100

1,2,4‐Trichlorobenzene (HAP/OH)

1,4‐Dichlorobenzene(p) (HAP/OH)

3730 3620

5000 5000 5000 5000 4860

2740

Chloroprene (HAP/OH)Ethyl benzene (HAP)

48204280 4280 4280

4730 4590

42404060

7730

60104550

5190 51903730

Minnesota C&D Summary Table 2out of275
Minnesota C&D Summary Table 3out of275
Moisture (wt%) Ash (wt%) Volatile Matter (wt%) Fixed Carbon (wt%) Hydrogen (wt%) Carbon (wt%) Nitrogen (wt%) Oxygen (wt%) Sulfur (wt%) Heating Value (BTU/lb)

12.05 0.64 81.24 18.13 6.12 50.56 0.25 42.41 0.018 8644

13.03 0.65 80.57 18.78 6 50.57 0.2 42.58 0.01 8254

15.2 0.7 80.89 18.42 5.99 50.5 0.22 42.57 0.015 8423

14.91 0.68 81.37 17.96 6 50.72 0.23 42.36 0.009 8624

14.1 0.7 81.44 17.85 5.98 50.53 0.19 42.57 0.021 8624

13.87 0.63 81.24 18.13 5.99 50.48 0.29 42.6 0.014 8033

13.45 0.52 81.24 18.24 5.95 50.2 0.23 43.08 0.018 8805

Minnesota ProUCL Entry 4
Antimony  (HAP) Arsenic  (HAP) Beryllium  (HAP) Cadmium  (HAP) Chromium  (HAP) Cobalt  (HAP) Lead  (HAP) Manganese  (HAP) Mercury  (HAP) Nickel  (HAP)

0.59 65.7 0.008 0.25 73.2 0.38 96.8 41.5 0.049 2.44

0.18 2.21 0.008 0.18 4.1 0.41 41.3 55.3 0.04 2.34

0.37 16.9 0.008 0.14 21.2 0.46 12.5 39.4 0.017 1.2

0.17 1.95 0.008 0.13 3.01 0.51 34.6 44.1 0.032 1.31

0.41 11.2 0.008 0.14 14 0.41 8.78 38.6 0.015 1.35

0.35 13.8 0.008 0.13 16.2 0.62 15.7 39.1 0.02 1.06

0.43 50.4 0.008 0.14 60.1 1.52 22 156 0.027 5.05

Minnesota ProUCL Entry 5
Selenium  (HAP) Formaldehyde Bromine (mg/kg) Chlorine (mg/kg) Fluorine (mg/kg) 1,1,2,2‐Tetrachloroethane  (HAP/OH) 1,1,2‐Trichloroethane  (HAP/OH)

0.29 15000 6 110 25 4.61 7.81

0.27 34000 6 95 24 4.43 7.5

0.27 18000 6 90 5 4.43 7.5

0.27 16000 7 110 25 4.61 7.81

0.27 17000 6 90 6 4.61 7.81

0.31 9300 6 90 6 4.61 7.81

0.27 110000 6 130 25 4.43 7.5

Minnesota ProUCL Entry 6
1,2,4‐Trichlorobenzene  (HAP/OH) 1,4‐Dichlorobenzene(p)  (HAP/OH) Acetonitrile  (HAP/N) Acrolein  (HAP) Acrylonitrile  (HAP/N) Allyl chloride  (HAP/OH) Benzene  (HAP)

2.6 2 62 138 52 7.2 3.41

2.5 1.93 59.7 133 50 6.93 3.27

2.5 1.93 59.7 133 50 6.93 3.27

2.6 2 62 138 52 7.2 3.41

2.6 2 62 138 52 7.2 3.41

2.6 2 62 138 52 7.2 3.41

2.5 1.93 59.7 133 50 6.93 3.27

Minnesota ProUCL Entry 7
Bromoform  (HAP/OH) Chlorobenzene  (HAP/OH) Chloroform  (HAP/OH) Chloroprene  (HAP/OH) Ethyl benzene  (HAP) Hexachlorobutadiene  (HAP/OH)

6.81 2.81 3.6 4.61 9.2 4.61

6.54 2.7 3.47 4.43 7.12 4.43

6.54 2.7 3.47 4.43 8.27 4.43

6.81 2.81 3.6 4.61 8.2 4.61

6.81 2.81 3.6 4.61 8.4 4.61

6.81 2.81 3.6 4.61 8.8 4.61

6.54 2.7 3.47 4.43 13.5 4.43

Minnesota ProUCL Entry 8
Isopropylbenzene  (HAP) m,p‐Xylenes  (HAP) Methyl methacrylate  (HAP) Methyl tert butyl ether  (HAP) Methylene chloride  (HAP/OH) Naphthalene  (HAP)

2.81 24.6 7.81 5.2 25.4 179

2.7 21.7 7.5 5 35.8 125

2.8 22.1 7.5 5 34.6 140

2.81 18.6 7.81 5.2 30.2 80.6

2.81 20.6 7.81 5.2 33.2 140

2.81 23.6 7.81 5.2 31.6 136

2.7 41.7 7.5 5 26 118

Minnesota ProUCL Entry 9
n‐Hexane  (HAP) o‐Xylenes  (HAP) Styrene  (HAP) Tetrachloroethylene  (HAP/OH) Toluene  (HAP) Vinyl chloride 1,2,4‐Trichlorobenzene  (HAP/OH)

6.4 11.8 28.2 5 215 5.2 5730

6.16 12.3 29.8 4.81 207 5 5730

6.16 10.4 41.7 4.81 201 5 5730

6.4 10 49.4 5 166 5.2 5730

6.4 10.6 39.2 5 202 5.2 5560

6.4 10.2 48 5 221 5.2 5730

6.16 26 21.7 4.81 144 5 5560

Minnesota ProUCL Entry 10
1,4‐Dichlorobenzene  (HAP/OH) 1‐Methylnaphthalene 2,4,5‐Trichlorophenol  (HAP/OH) 2,4,6‐Trichlorophenol  (HAP/OH) 2,4‐Dinitrophenol  (HAP/N)

3730 6010 5190 4550 2100

3730 6010 5190 4550 2100

3730 6010 5190 4550 2100

3730 6010 5190 4550 2100

3620 5830 5030 4420 2030

3730 6010 5190 4550 2100

3620 5830 5030 4420 2030

Minnesota ProUCL Entry 11
2,4‐Dinitrotoluene  (HAP/N) 2‐Methylnaphthalene 3,3‐Dichlorobenzidene  (HAP/OH/N) 4‐Nitrophenol  (HAP/N) Acenaphthene Acenaphthylene Acetophenone Aniline

3730 5370 7730 5100 4820 4280 4190 7280

3730 5370 7730 5100 4820 4280 4190 7280

3730 5370 7730 5100 4820 4280 4190 7280

3730 5370 7730 5100 4820 4280 4190 7280

3620 5210 7510 4950 4680 4150 4060 7060

3730 5370 7730 5100 4820 4280 4190 7280

3620 5210 7510 4950 4680 4250 4060 7060

Minnesota ProUCL Entry 12
Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Biphenyl  (HAP) Bis(2‐ethylhexyl)phthalate  (HAP)

3910 4280 3370 2370 4730 5370 3730 4010

3910 4280 3370 2370 4730 5370 3730 4010

3910 4280 3370 2370 4730 5370 3730 4010

3910 4280 3370 2370 4730 5370 3730 4010

3800 4150 3270 2300 4590 5210 3620 3890

3910 4280 3370 2370 4730 5370 3730 4010

3800 4150 3270 2300 4590 5210 3620 3890

Minnesota ProUCL Entry 13
Chrysene Dibenz(a,h)anthracene Dibenzofurans  (D/F) Dimethyl phthalate  (HAP) Fluoranthene Fluorene Hexachlorobenzene  (HAP/OH) Hexachlorobutadiene  (HAP/OH)

4100 4190 4190 4820 4370 4280 4370 5000

4100 4190 4190 4820 4370 4280 4370 5000

4100 4190 4190 4820 4370 4280 4370 5000

4100 4190 4190 4820 4370 4280 4370 5000

3980 4060 4060 4680 4240 4150 4240 4860

4100 4190 4190 4820 4370 4280 4370 5000

3680 4060 4060 4680 4240 4150 4240 4860

Minnesota ProUCL Entry 14
Hexachlorocyclopentadiene  (HAP/OH) Hexachloroethane Indeno(1,2,3‐cd)pyrene Naphthalene  (HAP) Nitrobenzene  (HAP/N) Pentachlorophenol  (HAP/OH)

3100 2820 3730 4460 3550 3190

3100 2820 3730 4460 3550 3190

3100 2820 3730 4460 3550 8820

3100 2820 3730 4460 3550 8970

3000 2740 3620 4330 3450 8240

3100 2820 3730 4460 3550 8940

3000 2740 3620 4330 3450 134000

Minnesota ProUCL Entry 15
Phenanthrene Phenol Pyrene Total Metals Total Halogens Total VOC Total SVOC

3820 4450 4190 281.207 141 827.69 160750

3820 4190 4190 106.338 125 760.72 160490

3820 13800 4190 92.465 101 780.17 175730

3820 5360 4190 86.09 142 697.49 167440

3710 13900 4060 75.183 102 788.49 170700

3820 15200 4190 87.298 102 813.69 177250

3710 5650 4060 295.945 161 712.9 288010

Minnesota ProUCL Entry 16
Moisture

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 12.05 Minimum 2.489

Maximum 15.2 Maximum 2.721

Second Largest 14.91 Second Largest 2.702

First Quartile 13.24 First Quartile 2.583

Median 13.87 Median 2.63

Third Quartile 14.51 Third Quartile 2.674

Mean 13.8 Mean 2.622

SD 1.085 SD 0.0797

Coefficient of Variation 0.0786

Skewness ‐0.32

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.975 Shapiro Wilk Test Statistic 0.97

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 16.33   90% UTL with   90% Coverage 16.58

   90% UPL (t) 15.47   90% UPL (t) 15.56

90% Percentile (z) 15.19 90% Percentile (z) 15.24

95% Percentile (z) 15.59 95% Percentile (z) 15.69

99% Percentile (z) 16.33 99% Percentile (z) 16.57

Gamma Distribution Test Data Distribution Test

k star 106.1 Data appear Normal at 5% Significance Level

Theta Star 0.13

MLE of Mean 13.8

MLE of Standard Deviation 1.34

nu star 1486

A‐D Test Statistic 0.182 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 15.03

K‐S Test Statistic 0.148 95% Percentile 15.11

5% K‐S Critical Value 0.311 99% Percentile 15.18

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 15.2

Minnesota UPL Results 17
90% Percentile 15.54   90% Percentile Bootstrap UTL with   90% Coverage 15.2

95% Percentile 16.08   90% BCA Bootstrap UTL with   90% Coverage 15.2

99% Percentile 17.11   90% UPL 15.2

  90% Chebyshev UPL 17.28

   90% WH Approx. Gamma UPL 15.53 Upper Threshold Limit Based upon IQR 16.4

   90% HW Approx. Gamma UPL 15.54

   90% WH Approx. Gamma UTL with   90% Coverage 16.49

   90% HW Approx. Gamma UTL with   90% Coverage 16.51

Ash

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 0.52 Minimum ‐0.654

Maximum 0.7 Maximum ‐0.357

Second Largest 0.7 Second Largest ‐0.357

First Quartile 0.635 First Quartile ‐0.454

Median 0.65 Median ‐0.431

Third Quartile 0.69 Third Quartile ‐0.371

Mean 0.646 Mean ‐0.442

SD 0.0621 SD 0.103

Coefficient of Variation 0.0962

Skewness ‐1.585

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.834 Shapiro Wilk Test Statistic 0.806

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.791   90% UTL with   90% Coverage 0.817

   90% UPL (t) 0.741   90% UPL (t) 0.753

90% Percentile (z) 0.725 90% Percentile (z) 0.733

95% Percentile (z) 0.748 95% Percentile (z) 0.761

99% Percentile (z) 0.79 99% Percentile (z) 0.816

Gamma Distribution Test Data Distribution Test

k star 66.29 Data appear Normal at 5% Significance Level

Theta Star 0.00974

MLE of Mean 0.646

Minnesota UPL Results 18
MLE of Standard Deviation 0.0793

nu star 928.1

A‐D Test Statistic 0.598 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 0.7

K‐S Test Statistic 0.265 95% Percentile 0.7

5% K‐S Critical Value 0.311 99% Percentile 0.7

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.7

90% Percentile 0.749   90% Percentile Bootstrap UTL with   90% Coverage 0.7

95% Percentile 0.781   90% BCA Bootstrap UTL with   90% Coverage 0.7

99% Percentile 0.844   90% UPL 0.7

  90% Chebyshev UPL 0.845

   90% WH Approx. Gamma UPL 0.749 Upper Threshold Limit Based upon IQR 0.773

   90% HW Approx. Gamma UPL 0.75

   90% WH Approx. Gamma UTL with   90% Coverage 0.807

   90% HW Approx. Gamma UTL with   90% Coverage 0.809

Volatile Matter

General Statistics

Total Number of Observations 7 Number of Distinct Observations 5

Raw Statistics Log‐Transformed Statistics

Minimum 80.57 Minimum 4.389

Maximum 81.44 Maximum 4.4

Second Largest 81.37 Second Largest 4.399

First Quartile 81.07 First Quartile 4.395

Median 81.24 Median 4.397

Third Quartile 81.31 Third Quartile 4.398

Mean 81.14 Mean 4.396

SD 0.306 SD 0.00377

Coefficient of Variation 0.00377

Skewness ‐1.317

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.844 Shapiro Wilk Test Statistic 0.844

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

Minnesota UPL Results 19
   90% UTL with   90% Coverage 81.85   90% UTL with   90% Coverage 81.86

   90% UPL (t) 81.61   90% UPL (t) 81.61

90% Percentile (z) 81.53 90% Percentile (z) 81.53

95% Percentile (z) 81.64 95% Percentile (z) 81.65

99% Percentile (z) 81.85 99% Percentile (z) 81.86

Gamma Distribution Test Data Distribution Test

k star 46893 Data appear Normal at 5% Significance Level

Theta Star 0.00173

MLE of Mean 81.14

MLE of Standard Deviation 0.375

nu star 656499

A‐D Test Statistic 0.858 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 81.4

K‐S Test Statistic 0.351 95% Percentile 81.42

5% K‐S Critical Value 0.311 99% Percentile 81.44

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 81.44

90% Percentile 81.62   90% Percentile Bootstrap UTL with   90% Coverage 81.44

95% Percentile 81.76   90% BCA Bootstrap UTL with   90% Coverage 81.44

99% Percentile 82.02   90% UPL 81.44

  90% Chebyshev UPL 82.12

   90% WH Approx. Gamma UPL 81.61 Upper Threshold Limit Based upon IQR 81.67

   90% HW Approx. Gamma UPL 81.61

   90% WH Approx. Gamma UTL with   90% Coverage 81.86

   90% HW Approx. Gamma UTL with   90% Coverage 81.86

Fixed Carbon

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 17.85 Minimum 2.882

Maximum 18.78 Maximum 2.933

Second Largest 18.42 Second Largest 2.913

First Quartile 18.05 First Quartile 2.893

Median 18.13 Median 2.898

Third Quartile 18.33 Third Quartile 2.909

Mean 18.22 Mean 2.902

SD 0.309 SD 0.0169

Coefficient of Variation 0.017

Skewness 0.955

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

Minnesota UPL Results 20
The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.939 Shapiro Wilk Test Statistic 0.942

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 18.94   90% UTL with   90% Coverage 18.95

   90% UPL (t) 18.69   90% UPL (t) 18.69

90% Percentile (z) 18.61 90% Percentile (z) 18.61

95% Percentile (z) 18.72 95% Percentile (z) 18.73

99% Percentile (z) 18.94 99% Percentile (z) 18.94

Gamma Distribution Test Data Distribution Test

k star 2327 Data appear Normal at 5% Significance Level

Theta Star 0.00783

MLE of Mean 18.22

MLE of Standard Deviation 0.378

nu star 32584

A‐D Test Statistic 0.317 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 18.56

K‐S Test Statistic 0.218 95% Percentile 18.67

5% K‐S Critical Value 0.311 99% Percentile 18.76

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 18.78

90% Percentile 18.7   90% Percentile Bootstrap UTL with   90% Coverage 18.78

95% Percentile 18.84   90% BCA Bootstrap UTL with   90% Coverage 18.78

99% Percentile 19.11   90% UPL 18.78

  90% Chebyshev UPL 19.21

   90% WH Approx. Gamma UPL 18.69 Upper Threshold Limit Based upon IQR 18.76

   90% HW Approx. Gamma UPL 18.69

   90% WH Approx. Gamma UTL with   90% Coverage 18.94

   90% HW Approx. Gamma UTL with   90% Coverage 18.94

Hydrogen

General Statistics

Total Number of Observations 7 Number of Distinct Observations 5

Raw Statistics Log‐Transformed Statistics

Minimum 5.95 Minimum 1.783

Maximum 6.12 Maximum 1.812

Second Largest 6 Second Largest 1.792

First Quartile 5.985 First Quartile 1.789

Median 5.99 Median 1.79

Third Quartile 6 Third Quartile 1.792

Mean 6.004 Mean 1.792

SD 0.0538 SD 0.0089

Coefficient of Variation 0.00896

Skewness 2.051

Minnesota UPL Results 21
Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.741 Shapiro Wilk Test Statistic 0.743

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 6.13   90% UTL with   90% Coverage 6.13

   90% UPL (t) 6.087   90% UPL (t) 6.087

90% Percentile (z) 6.073 90% Percentile (z) 6.073

95% Percentile (z) 6.093 95% Percentile (z) 6.093

99% Percentile (z) 6.129 99% Percentile (z) 6.13

Gamma Distribution Test Data Distribution Test

k star 8374 Data do not follow a Discernable Distribution (0.05)

Theta Star 7.17E‐04

MLE of Mean 6.004

MLE of Standard Deviation 0.0656

nu star 117230

A‐D Test Statistic 2.209 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6.048

K‐S Test Statistic 0.57 95% Percentile 6.084

5% K‐S Critical Value 0.311 99% Percentile 6.113

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 6.12

90% Percentile 6.089   90% Percentile Bootstrap UTL with   90% Coverage 6.12

95% Percentile 6.113   90% BCA Bootstrap UTL with   90% Coverage 6.048

99% Percentile 6.158   90% UPL 6.12

  90% Chebyshev UPL 6.177

   90% WH Approx. Gamma UPL 6.087 Upper Threshold Limit Based upon IQR 6.023

   90% HW Approx. Gamma UPL 6.087

   90% WH Approx. Gamma UTL with   90% Coverage 6.13

   90% HW Approx. Gamma UTL with   90% Coverage 6.13

Carbon

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 50.2 Minimum 3.916

Minnesota UPL Results 22
Maximum 50.72 Maximum 3.926

Second Largest 50.57 Second Largest 3.923

First Quartile 50.49 First Quartile 3.922

Median 50.53 Median 3.923

Third Quartile 50.57 Third Quartile 3.923

Mean 50.51 Mean 3.922

SD 0.157 SD 0.00311

Coefficient of Variation 0.00311

Skewness ‐1.183

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.877 Shapiro Wilk Test Statistic 0.876

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 50.87   90% UTL with   90% Coverage 50.88

   90% UPL (t) 50.75   90% UPL (t) 50.75

90% Percentile (z) 50.71 90% Percentile (z) 50.71

95% Percentile (z) 50.77 95% Percentile (z) 50.77

99% Percentile (z) 50.87 99% Percentile (z) 50.88

Gamma Distribution Test Data Distribution Test

k star 68974 Data appear Normal at 5% Significance Level

Theta Star 7.32E‐04

MLE of Mean 50.51

MLE of Standard Deviation 0.192

nu star 965640

A‐D Test Statistic 0.862 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 50.63

K‐S Test Statistic 0.315 95% Percentile 50.68

5% K‐S Critical Value 0.311 99% Percentile 50.71

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 50.72

90% Percentile 50.76   90% Percentile Bootstrap UTL with   90% Coverage 50.72

95% Percentile 50.83   90% BCA Bootstrap UTL with   90% Coverage 50.72

99% Percentile 50.96   90% UPL 50.72

  90% Chebyshev UPL 51.01

   90% WH Approx. Gamma UPL 50.75 Upper Threshold Limit Based upon IQR 50.68

   90% HW Approx. Gamma UPL 50.75

   90% WH Approx. Gamma UTL with   90% Coverage 50.88

   90% HW Approx. Gamma UTL with   90% Coverage 50.88

Minnesota UPL Results 23
Nitrogen

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 0.19 Minimum ‐1.661

Maximum 0.29 Maximum ‐1.238

Second Largest 0.25 Second Largest ‐1.386

First Quartile 0.21 First Quartile ‐1.562

Median 0.23 Median ‐1.47

Third Quartile 0.24 Third Quartile ‐1.428

Mean 0.23 Mean ‐1.478

SD 0.0332 SD 0.14

Coefficient of Variation 0.144

Skewness 0.844

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.943 Shapiro Wilk Test Statistic 0.963

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.307   90% UTL with   90% Coverage 0.316

   90% UPL (t) 0.281   90% UPL (t) 0.283

90% Percentile (z) 0.273 90% Percentile (z) 0.273

95% Percentile (z) 0.285 95% Percentile (z) 0.287

99% Percentile (z) 0.307 99% Percentile (z) 0.316

Gamma Distribution Test Data Distribution Test

k star 33.48 Data appear Normal at 5% Significance Level

Theta Star 0.00687

MLE of Mean 0.23

MLE of Standard Deviation 0.0398

nu star 468.7

A‐D Test Statistic 0.242 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 0.266

K‐S Test Statistic 0.197 95% Percentile 0.278

5% K‐S Critical Value 0.311 99% Percentile 0.288

Data appear Gamma Distributed at 5% Significance Level

Minnesota UPL Results 24
Assuming Gamma Distribution   90% UTL with   90% Coverage 0.29

90% Percentile 0.282   90% Percentile Bootstrap UTL with   90% Coverage 0.29

95% Percentile 0.299   90% BCA Bootstrap UTL with   90% Coverage 0.29

99% Percentile 0.332   90% UPL 0.29

  90% Chebyshev UPL 0.336

   90% WH Approx. Gamma UPL 0.282 Upper Threshold Limit Based upon IQR 0.285

   90% HW Approx. Gamma UPL 0.282

   90% WH Approx. Gamma UTL with   90% Coverage 0.313

   90% HW Approx. Gamma UTL with   90% Coverage 0.314

Oxygen

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 42.36 Minimum 3.746

Maximum 43.08 Maximum 3.763

Second Largest 42.6 Second Largest 3.752

First Quartile 42.49 First Quartile 3.749

Median 42.57 Median 3.751

Third Quartile 42.59 Third Quartile 3.752

Mean 42.6 Mean 3.752

SD 0.233 SD 0.00546

Coefficient of Variation 0.00547

Skewness 1.731

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.79 Shapiro Wilk Test Statistic 0.792

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 43.14   90% UTL with   90% Coverage 43.14

   90% UPL (t) 42.95   90% UPL (t) 42.95

90% Percentile (z) 42.89 90% Percentile (z) 42.89

95% Percentile (z) 42.98 95% Percentile (z) 42.98

99% Percentile (z) 43.14 99% Percentile (z) 43.14

Gamma Distribution Test Data Distribution Test

k star 22351 Data do not follow a Discernable Distribution (0.05)

Minnesota UPL Results 25
Theta Star 0.00191

MLE of Mean 42.6

MLE of Standard Deviation 0.285

nu star 312910

A‐D Test Statistic 2.281 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 42.79

K‐S Test Statistic 0.523 95% Percentile 42.94

5% K‐S Critical Value 0.311 99% Percentile 43.05

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 43.08

90% Percentile 42.96   90% Percentile Bootstrap UTL with   90% Coverage 43.08

95% Percentile 43.07   90% BCA Bootstrap UTL with   90% Coverage 43.08

99% Percentile 43.26   90% UPL 43.08

  90% Chebyshev UPL 43.34

   90% WH Approx. Gamma UPL 42.95 Upper Threshold Limit Based upon IQR 42.74

   90% HW Approx. Gamma UPL 42.95

   90% WH Approx. Gamma UTL with   90% Coverage 43.14

   90% HW Approx. Gamma UTL with   90% Coverage 43.14

Sulfur

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 0.009 Minimum ‐4.711

Maximum 0.021 Maximum ‐3.863

Second Largest 0.018 Second Largest ‐4.017

First Quartile 0.012 First Quartile ‐4.437

Median 0.015 Median ‐4.2

Third Quartile 0.018 Third Quartile ‐4.017

Mean 0.015 Mean ‐4.24

SD 0.0044 SD 0.316

Coefficient of Variation 0.293

Skewness ‐0.198

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.944 Shapiro Wilk Test Statistic 0.919

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Minnesota UPL Results 26
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.0253   90% UTL with   90% Coverage 0.0301

   90% UPL (t) 0.0218   90% UPL (t) 0.0234

90% Percentile (z) 0.0206 90% Percentile (z) 0.0216

95% Percentile (z) 0.0222 95% Percentile (z) 0.0242

99% Percentile (z) 0.0252 99% Percentile (z) 0.03

Gamma Distribution Test Data Distribution Test

k star 7.227 Data appear Normal at 5% Significance Level

Theta Star 0.00208

MLE of Mean 0.015

MLE of Standard Deviation 0.00558

nu star 101.2

A‐D Test Statistic 0.331 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 0.0192

K‐S Test Statistic 0.204 95% Percentile 0.0201

5% K‐S Critical Value 0.312 99% Percentile 0.0208

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.021

90% Percentile 0.0224   90% Percentile Bootstrap UTL with   90% Coverage 0.021

95% Percentile 0.0252   90% BCA Bootstrap UTL with   90% Coverage 0.0192

99% Percentile 0.0309   90% UPL 0.021

  90% Chebyshev UPL 0.0291

   90% WH Approx. Gamma UPL 0.0227 Upper Threshold Limit Based upon IQR 0.027

   90% HW Approx. Gamma UPL 0.0229

   90% WH Approx. Gamma UTL with   90% Coverage 0.0279

   90% HW Approx. Gamma UTL with   90% Coverage 0.0283

Heating Value

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 8033 Minimum 8.991

Maximum 8805 Maximum 9.083

Second Largest 8644 Second Largest 9.065

First Quartile 8339 First Quartile 9.029

Median 8624 Median 9.062

Third Quartile 8634 Third Quartile 9.063

Mean 8487 Mean 9.046

SD 267 SD 0.0318

Coefficient of Variation 0.0315

Skewness ‐0.796

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Minnesota UPL Results 27
Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.921 Shapiro Wilk Test Statistic 0.916

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 9110   90% UTL with   90% Coverage 9136

   90% UPL (t) 8898   90% UPL (t) 8908

90% Percentile (z) 8829 90% Percentile (z) 8836

95% Percentile (z) 8926 95% Percentile (z) 8938

99% Percentile (z) 9108 99% Percentile (z) 9134

Gamma Distribution Test Data Distribution Test

k star 665.1 Data appear Normal at 5% Significance Level

Theta Star 12.76

MLE of Mean 8487

MLE of Standard Deviation 329.1

nu star 9311

A‐D Test Statistic 0.399 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 8708

K‐S Test Statistic 0.283 95% Percentile 8757

5% K‐S Critical Value 0.311 99% Percentile 8795

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 8805

90% Percentile 8911   90% Percentile Bootstrap UTL with   90% Coverage 8805

95% Percentile 9035   90% BCA Bootstrap UTL with   90% Coverage 8805

99% Percentile 9271   90% UPL 8805

  90% Chebyshev UPL 9343

   90% WH Approx. Gamma UPL 8905 Upper Threshold Limit Based upon IQR 9077

   90% HW Approx. Gamma UPL 8905

   90% WH Approx. Gamma UTL with   90% Coverage 9127

   90% HW Approx. Gamma UTL with   90% Coverage 9129

Antimony

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 0.17 Minimum ‐1.772

Maximum 0.59 Maximum ‐0.528

Second Largest 0.43 Second Largest ‐0.844

First Quartile 0.265 First Quartile ‐1.382

Median 0.37 Median ‐0.994

Third Quartile 0.42 Third Quartile ‐0.868

Mean 0.357 Mean ‐1.113

SD 0.147 SD 0.462

Coefficient of Variation 0.41

Minnesota UPL Results 28
Skewness 0.0777

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.928 Shapiro Wilk Test Statistic 0.882

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.699   90% UTL with   90% Coverage 0.964

   90% UPL (t) 0.583   90% UPL (t) 0.668

90% Percentile (z) 0.545 90% Percentile (z) 0.593

95% Percentile (z) 0.598 95% Percentile (z) 0.702

99% Percentile (z) 0.698 99% Percentile (z) 0.961

Gamma Distribution Test Data Distribution Test

k star 3.597 Data appear Normal at 5% Significance Level

Theta Star 0.0993

MLE of Mean 0.357

MLE of Standard Deviation 0.188

nu star 50.35

A‐D Test Statistic 0.447 Nonparametric Statistics

5% A‐D Critical Value 0.71 90% Percentile 0.494

K‐S Test Statistic 0.248 95% Percentile 0.542

5% K‐S Critical Value 0.313 99% Percentile 0.58

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.59

90% Percentile 0.61   90% Percentile Bootstrap UTL with   90% Coverage 0.59

95% Percentile 0.712   90% BCA Bootstrap UTL with   90% Coverage 0.59

99% Percentile 0.933   90% UPL 0.59

  90% Chebyshev UPL 0.827

   90% WH Approx. Gamma UPL 0.627 Upper Threshold Limit Based upon IQR 0.653

   90% HW Approx. Gamma UPL 0.635

   90% WH Approx. Gamma UTL with   90% Coverage 0.825

   90% HW Approx. Gamma UTL with   90% Coverage 0.852

Arsenic

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Minnesota UPL Results 29
Raw Statistics Log‐Transformed Statistics

Minimum 1.95 Minimum 0.668

Maximum 65.7 Maximum 4.185

Second Largest 50.4 Second Largest 3.92

First Quartile 6.705 First Quartile 1.604

Median 13.8 Median 2.625

Third Quartile 33.65 Third Quartile 3.374

Mean 23.17 Mean 2.491

SD 24.87 SD 1.37

Coefficient of Variation 1.073

Skewness 1.147

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.819 Shapiro Wilk Test Statistic 0.908

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 81.18   90% UTL with   90% Coverage 294.7

   90% UPL (t) 61.44   90% UPL (t) 99.35

90% Percentile (z) 55.03 90% Percentile (z) 69.81

95% Percentile (z) 64.07 95% Percentile (z) 114.8

99% Percentile (z) 81.02 99% Percentile (z) 292

Gamma Distribution Test Data Distribution Test

k star 0.608 Data appear Normal at 5% Significance Level

Theta Star 38.12

MLE of Mean 23.17

MLE of Standard Deviation 29.72

nu star 8.508

A‐D Test Statistic 0.336 Nonparametric Statistics

5% A‐D Critical Value 0.731 90% Percentile 56.52

K‐S Test Statistic 0.182 95% Percentile 61.11

5% K‐S Critical Value 0.321 99% Percentile 64.78

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 65.7

90% Percentile 60.08   90% Percentile Bootstrap UTL with   90% Coverage 65.7

95% Percentile 82.98   90% BCA Bootstrap UTL with   90% Coverage 65.7

99% Percentile 138.3   90% UPL 65.7

  90% Chebyshev UPL 102.9

   90% WH Approx. Gamma UPL 71.15 Upper Threshold Limit Based upon IQR 74.07

   90% HW Approx. Gamma UPL 74.94

Minnesota UPL Results 30
   90% WH Approx. Gamma UTL with   90% Coverage 124.5

   90% HW Approx. Gamma UTL with   90% Coverage 141.8

Beryllium

General Statistics

Total Number of Observations 7 Number of Distinct Observations 1

Warning: There is only one distinct observation value in this data set ‐ resulting in '0' variance!

ProUCL (or any other software) should not be used on such a data set!

The data set for variable Beryllium was not processed!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible, compute and collect Data Quality Objectives (DQOs) based sample size and analytical results.

The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV).

Cadmium

General Statistics

Total Number of Observations 7 Number of Distinct Observations 4

Raw Statistics Log‐Transformed Statistics

Minimum 0.13 Minimum ‐2.04

Maximum 0.25 Maximum ‐1.386

Second Largest 0.18 Second Largest ‐1.715

First Quartile 0.135 First Quartile ‐2.003

Median 0.14 Median ‐1.966

Third Quartile 0.16 Third Quartile ‐1.84

Mean 0.159 Mean ‐1.869

SD 0.0438 SD 0.239

Coefficient of Variation 0.276

Skewness 1.973

Warning:  There are only 4 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.704 Shapiro Wilk Test Statistic 0.746

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Minnesota UPL Results 31
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.261   90% UTL with   90% Coverage 0.27

   90% UPL (t) 0.226   90% UPL (t) 0.223

90% Percentile (z) 0.215 90% Percentile (z) 0.21

95% Percentile (z) 0.231 95% Percentile (z) 0.229

99% Percentile (z) 0.26 99% Percentile (z) 0.269

Gamma Distribution Test Data Distribution Test

k star 10.77 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0147

MLE of Mean 0.159

MLE of Standard Deviation 0.0483

nu star 150.8

A‐D Test Statistic 0.961 Nonparametric Statistics

5% A‐D Critical Value 0.707 90% Percentile 0.208

K‐S Test Statistic 0.388 95% Percentile 0.229

5% K‐S Critical Value 0.312 99% Percentile 0.246

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.25

90% Percentile 0.223   90% Percentile Bootstrap UTL with   90% Coverage 0.25

95% Percentile 0.245   90% BCA Bootstrap UTL with   90% Coverage 0.25

99% Percentile 0.292   90% UPL 0.25

  90% Chebyshev UPL 0.299

   90% WH Approx. Gamma UPL 0.224 Upper Threshold Limit Based upon IQR 0.198

   90% HW Approx. Gamma UPL 0.224

   90% WH Approx. Gamma UTL with   90% Coverage 0.266

   90% HW Approx. Gamma UTL with   90% Coverage 0.267

Chromium

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 3.01 Minimum 1.102

Maximum 73.2 Maximum 4.293

Second Largest 60.1 Second Largest 4.096

First Quartile 9.05 First Quartile 2.025

Median 16.2 Median 2.785

Third Quartile 40.65 Third Quartile 3.575

Mean 27.4 Mean 2.769

SD 27.83 SD 1.211

Coefficient of Variation 1.016

Skewness 1.08

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Minnesota UPL Results 32
Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.82 Shapiro Wilk Test Statistic 0.93

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 92.34   90% UTL with   90% Coverage 269.1

   90% UPL (t) 70.24   90% UPL (t) 102.8

90% Percentile (z) 63.07 90% Percentile (z) 75.27

95% Percentile (z) 73.18 95% Percentile (z) 116.9

99% Percentile (z) 92.15 99% Percentile (z) 266.9

Gamma Distribution Test Data Distribution Test

k star 0.7 Data appear Normal at 5% Significance Level

Theta Star 39.15

MLE of Mean 27.4

MLE of Standard Deviation 32.75

nu star 9.798

A‐D Test Statistic 0.329 Nonparametric Statistics

5% A‐D Critical Value 0.727 90% Percentile 65.34

K‐S Test Statistic 0.182 95% Percentile 69.27

5% K‐S Critical Value 0.319 99% Percentile 72.41

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 73.2

90% Percentile 68.79   90% Percentile Bootstrap UTL with   90% Coverage 73.2

95% Percentile 93.27   90% BCA Bootstrap UTL with   90% Coverage 73.2

99% Percentile 151.7   90% UPL 73.2

  90% Chebyshev UPL 116.7

   90% WH Approx. Gamma UPL 79.82 Upper Threshold Limit Based upon IQR 88.05

   90% HW Approx. Gamma UPL 83.19

   90% WH Approx. Gamma UTL with   90% Coverage 135.6

   90% HW Approx. Gamma UTL with   90% Coverage 151.2

Cobalt

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 0.38 Minimum ‐0.968

Maximum 1.52 Maximum 0.419

Second Largest 0.62 Second Largest ‐0.478

First Quartile 0.41 First Quartile ‐0.892

Median 0.46 Median ‐0.777

Third Quartile 0.565 Third Quartile ‐0.576

Mean 0.616 Mean ‐0.609

SD 0.407 SD 0.482

Coefficient of Variation 0.661

Minnesota UPL Results 33
Skewness 2.438

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.625 Shapiro Wilk Test Statistic 0.746

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.565   90% UTL with   90% Coverage 1.675

   90% UPL (t) 1.242   90% UPL (t) 1.143

90% Percentile (z) 1.137 90% Percentile (z) 1.009

95% Percentile (z) 1.285 95% Percentile (z) 1.202

99% Percentile (z) 1.562 99% Percentile (z) 1.67

Gamma Distribution Test Data Distribution Test

k star 2.498 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 0.246

MLE of Mean 0.616

MLE of Standard Deviation 0.39

nu star 34.97

A‐D Test Statistic 1.007 Nonparametric Statistics

5% A‐D Critical Value 0.71 90% Percentile 0.98

K‐S Test Statistic 0.297 95% Percentile 1.25

5% K‐S Critical Value 0.313 99% Percentile 1.466

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.52

90% Percentile 1.138   90% Percentile Bootstrap UTL with   90% Coverage 1.52

95% Percentile 1.364   90% BCA Bootstrap UTL with   90% Coverage 1.52

99% Percentile 1.858   90% UPL 1.52

  90% Chebyshev UPL 1.921

   90% WH Approx. Gamma UPL 1.176 Upper Threshold Limit Based upon IQR 0.798

   90% HW Approx. Gamma UPL 1.168

   90% WH Approx. Gamma UTL with   90% Coverage 1.618

   90% HW Approx. Gamma UTL with   90% Coverage 1.63

Lead

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Minnesota UPL Results 34
Raw Statistics Log‐Transformed Statistics

Minimum 8.78 Minimum 2.172

Maximum 96.8 Maximum 4.573

Second Largest 41.3 Second Largest 3.721

First Quartile 14.1 First Quartile 2.64

Median 22 Median 3.091

Third Quartile 37.95 Third Quartile 3.632

Mean 33.1 Mean 3.197

SD 30.47 SD 0.816

Coefficient of Variation 0.92

Skewness 1.892

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.788 Shapiro Wilk Test Statistic 0.97

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 104.2   90% UTL with   90% Coverage 164.2

   90% UPL (t) 79.99   90% UPL (t) 85.9

90% Percentile (z) 72.14 90% Percentile (z) 69.61

95% Percentile (z) 83.21 95% Percentile (z) 93.63

99% Percentile (z) 104 99% Percentile (z) 163.3

Gamma Distribution Test Data Distribution Test

k star 1.125 Data appear Gamma Distributed at 5% Significance Level

Theta Star 29.41

MLE of Mean 33.1

MLE of Standard Deviation 31.2

nu star 15.76

A‐D Test Statistic 0.303 Nonparametric Statistics

5% A‐D Critical Value 0.717 90% Percentile 63.5

K‐S Test Statistic 0.172 95% Percentile 80.15

5% K‐S Critical Value 0.316 99% Percentile 93.47

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 96.8

90% Percentile 74.02   90% Percentile Bootstrap UTL with   90% Coverage 96.8

95% Percentile 95.12   90% BCA Bootstrap UTL with   90% Coverage 96.8

99% Percentile 143.7   90% UPL 96.8

  90% Chebyshev UPL 130.8

   90% WH Approx. Gamma UPL 80.76 Upper Threshold Limit Based upon IQR 73.73

   90% HW Approx. Gamma UPL 81.55

Minnesota UPL Results 35
   90% WH Approx. Gamma UTL with   90% Coverage 125.4

   90% HW Approx. Gamma UTL with   90% Coverage 131.6

Manganese

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 38.6 Minimum 3.653

Maximum 156 Maximum 5.05

Second Largest 55.3 Second Largest 4.013

First Quartile 39.25 First Quartile 3.67

Median 41.5 Median 3.726

Third Quartile 49.7 Third Quartile 3.9

Mean 59.14 Mean 3.938

SD 43.1 SD 0.506

Coefficient of Variation 0.729

Skewness 2.55

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.556 Shapiro Wilk Test Statistic 0.64

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 159.7   90% UTL with   90% Coverage 167

   90% UPL (t) 125.5   90% UPL (t) 111.8

90% Percentile (z) 114.4 90% Percentile (z) 98.14

95% Percentile (z) 130 95% Percentile (z) 117.9

99% Percentile (z) 159.4 99% Percentile (z) 166.5

Gamma Distribution Test Data Distribution Test

k star 2.202 Data do not follow a Discernable Distribution (0.05)

Theta Star 26.85

MLE of Mean 59.14

MLE of Standard Deviation 39.85

nu star 30.83

A‐D Test Statistic 1.374 Nonparametric Statistics

5% A‐D Critical Value 0.71 90% Percentile 95.58

K‐S Test Statistic 0.354 95% Percentile 125.8

Minnesota UPL Results 36
5% K‐S Critical Value 0.313 99% Percentile 150

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 156

90% Percentile 112.5   90% Percentile Bootstrap UTL with   90% Coverage 156

95% Percentile 136.1   90% BCA Bootstrap UTL with   90% Coverage 156

99% Percentile 188.3   90% UPL 156

  90% Chebyshev UPL 197.4

   90% WH Approx. Gamma UPL 116.8 Upper Threshold Limit Based upon IQR 65.38

   90% HW Approx. Gamma UPL 115.5

   90% WH Approx. Gamma UTL with   90% Coverage 163.3

   90% HW Approx. Gamma UTL with   90% Coverage 164

Mercury

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 0.015 Minimum ‐4.2

Maximum 0.049 Maximum ‐3.016

Second Largest 0.04 Second Largest ‐3.219

First Quartile 0.0185 First Quartile ‐3.993

Median 0.027 Median ‐3.612

Third Quartile 0.036 Third Quartile ‐3.33

Mean 0.0286 Mean ‐3.639

SD 0.0126 SD 0.444

Coefficient of Variation 0.441

Skewness 0.626

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.934 Shapiro Wilk Test Statistic 0.955

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.058   90% UTL with   90% Coverage 0.074

   90% UPL (t) 0.048   90% UPL (t) 0.052

90% Percentile (z) 0.0447 90% Percentile (z) 0.0464

95% Percentile (z) 0.0493 95% Percentile (z) 0.0545

99% Percentile (z) 0.0579 99% Percentile (z) 0.0738

Minnesota UPL Results 37
Gamma Distribution Test Data Distribution Test

k star 3.591 Data appear Normal at 5% Significance Level

Theta Star 0.00796

MLE of Mean 0.0286

MLE of Standard Deviation 0.0151

nu star 50.28

A‐D Test Statistic 0.234 Nonparametric Statistics

5% A‐D Critical Value 0.71 90% Percentile 0.0436

K‐S Test Statistic 0.185 95% Percentile 0.0463

5% K‐S Critical Value 0.313 99% Percentile 0.0485

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.049

90% Percentile 0.0488   90% Percentile Bootstrap UTL with   90% Coverage 0.049

95% Percentile 0.057   90% BCA Bootstrap UTL with   90% Coverage 0.049

99% Percentile 0.0747   90% UPL 0.049

  90% Chebyshev UPL 0.069

   90% WH Approx. Gamma UPL 0.0501 Upper Threshold Limit Based upon IQR 0.0623

   90% HW Approx. Gamma UPL 0.0505

   90% WH Approx. Gamma UTL with   90% Coverage 0.066

   90% HW Approx. Gamma UTL with   90% Coverage 0.0676

Nickel

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 1.06 Minimum 0.0583

Maximum 5.05 Maximum 1.619

Second Largest 2.44 Second Largest 0.892

First Quartile 1.255 First Quartile 0.226

Median 1.35 Median 0.3

Third Quartile 2.39 Third Quartile 0.871

Mean 2.107 Mean 0.596

SD 1.411 SD 0.556

Coefficient of Variation 0.67

Skewness 1.884

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.756 Shapiro Wilk Test Statistic 0.869

Minnesota UPL Results 38
Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5.4   90% UTL with   90% Coverage 6.638

   90% UPL (t) 4.28   90% UPL (t) 4.27

90% Percentile (z) 3.916 90% Percentile (z) 3.7

95% Percentile (z) 4.429 95% Percentile (z) 4.528

99% Percentile (z) 5.391 99% Percentile (z) 6.613

Gamma Distribution Test Data Distribution Test

k star 2.099 Data appear Gamma Distributed at 5% Significance Level

Theta Star 1.004

MLE of Mean 2.107

MLE of Standard Deviation 1.454

nu star 29.39

A‐D Test Statistic 0.594 Nonparametric Statistics

5% A‐D Critical Value 0.711 90% Percentile 3.484

K‐S Test Statistic 0.294 95% Percentile 4.267

5% K‐S Critical Value 0.313 99% Percentile 4.893

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5.05

90% Percentile 4.052   90% Percentile Bootstrap UTL with   90% Coverage 5.05

95% Percentile 4.922   90% BCA Bootstrap UTL with   90% Coverage 5.05

99% Percentile 6.848   90% UPL 5.05

  90% Chebyshev UPL 6.634

   90% WH Approx. Gamma UPL 4.237 Upper Threshold Limit Based upon IQR 4.093

   90% HW Approx. Gamma UPL 4.241

   90% WH Approx. Gamma UTL with   90% Coverage 5.968

   90% HW Approx. Gamma UTL with   90% Coverage 6.097

Selenium

General Statistics

Total Number of Observations 7 Number of Distinct Observations 3

Raw Statistics Log‐Transformed Statistics

Minimum 0.27 Minimum ‐1.309

Maximum 0.31 Maximum ‐1.171

Second Largest 0.29 Second Largest ‐1.238

First Quartile 0.27 First Quartile ‐1.309

Median 0.27 Median ‐1.309

Third Quartile 0.28 Third Quartile ‐1.274

Mean 0.279 Mean ‐1.279

SD 0.0157 SD 0.0546

Coefficient of Variation 0.0565

Skewness 1.76

Warning:  There are only 3 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

Minnesota UPL Results 39
However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.647 Shapiro Wilk Test Statistic 0.648

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.315   90% UTL with   90% Coverage 0.316

   90% UPL (t) 0.303   90% UPL (t) 0.303

90% Percentile (z) 0.299 90% Percentile (z) 0.298

95% Percentile (z) 0.304 95% Percentile (z) 0.304

99% Percentile (z) 0.315 99% Percentile (z) 0.316

Gamma Distribution Test Data Distribution Test

k star 218.6 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00127

MLE of Mean 0.279

MLE of Standard Deviation 0.0188

nu star 3060

A‐D Test Statistic 1.329 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 0.298

K‐S Test Statistic 0.437 95% Percentile 0.304

5% K‐S Critical Value 0.311 99% Percentile 0.309

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.31

90% Percentile 0.303   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 0.31   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 0.324   90% UPL 0.31

  90% Chebyshev UPL 0.329

   90% WH Approx. Gamma UPL 0.303 Upper Threshold Limit Based upon IQR 0.295

   90% HW Approx. Gamma UPL 0.303

   90% WH Approx. Gamma UTL with   90% Coverage 0.316

   90% HW Approx. Gamma UTL with   90% Coverage 0.316

Formaldehyde

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 9300 Minimum 9.138

Maximum 110000 Maximum 11.61

Second Largest 34000 Second Largest 10.43

First Quartile 15500 First Quartile 9.648

Median 17000 Median 9.741

Minnesota UPL Results 40
Third Quartile 26000 Third Quartile 10.12

Mean 31329 Mean 10

SD 35511 SD 0.804

Coefficient of Variation 1.133

Skewness 2.412

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.626 Shapiro Wilk Test Statistic 0.84

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 114175   90% UTL with   90% Coverage 143962

   90% UPL (t) 85986   90% UPL (t) 76060

90% Percentile (z) 76838 90% Percentile (z) 61835

95% Percentile (z) 89739 95% Percentile (z) 82803

99% Percentile (z) 113939 99% Percentile (z) 143194

Gamma Distribution Test Data Distribution Test

k star 0.995 Data appear Lognormal at 5% Significance Level

Theta Star 31493

MLE of Mean 31329

MLE of Standard Deviation 31411

nu star 13.93

A‐D Test Statistic 0.879 Nonparametric Statistics

5% A‐D Critical Value 0.72 90% Percentile 64400

K‐S Test Statistic 0.354 95% Percentile 87200

5% K‐S Critical Value 0.317 99% Percentile 105440

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 110000

90% Percentile 72230   90% Percentile Bootstrap UTL with   90% Coverage 110000

95% Percentile 94026   90% BCA Bootstrap UTL with   90% Coverage 110000

99% Percentile 144655   90% UPL 110000

  90% Chebyshev UPL 145217

   90% WH Approx. Gamma UPL 78683 Upper Threshold Limit Based upon IQR 41750

   90% HW Approx. Gamma UPL 77881

   90% WH Approx. Gamma UTL with   90% Coverage 124893

   90% HW Approx. Gamma UTL with   90% Coverage 128051

Bromide

Minnesota UPL Results 41
General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 6 Minimum 1.792

Maximum 7 Maximum 1.946

Second Largest 6 Second Largest 1.792

First Quartile 6 First Quartile 1.792

Median 6 Median 1.792

Third Quartile 6 Third Quartile 1.792

Mean 6.143 Mean 1.814

SD 0.378 SD 0.0583

Coefficient of Variation 0.0615

Skewness 2.646

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.453 Shapiro Wilk Test Statistic 0.453

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7.025   90% UTL with   90% Coverage 7.027

   90% UPL (t) 6.725   90% UPL (t) 6.709

90% Percentile (z) 6.627 90% Percentile (z) 6.609

95% Percentile (z) 6.765 95% Percentile (z) 6.75

99% Percentile (z) 7.022 99% Percentile (z) 7.024

Gamma Distribution Test Data Distribution Test

k star 189.5 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0324

MLE of Mean 6.143

MLE of Standard Deviation 0.446

nu star 2653

A‐D Test Statistic 2.109 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6.4

K‐S Test Statistic 0.516 95% Percentile 6.7

5% K‐S Critical Value 0.311 99% Percentile 6.94

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7

Minnesota UPL Results 42
90% Percentile 6.721   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 6.895   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 7.228   90% UPL 7

  90% Chebyshev UPL 7.355

   90% WH Approx. Gamma UPL 6.714 Upper Threshold Limit Based upon IQR 6

   90% HW Approx. Gamma UPL 6.713

   90% WH Approx. Gamma UTL with   90% Coverage 7.026

   90% HW Approx. Gamma UTL with   90% Coverage 7.026

Chloride

General Statistics

Total Number of Observations 7 Number of Distinct Observations 4

Raw Statistics Log‐Transformed Statistics

Minimum 90 Minimum 4.5

Maximum 130 Maximum 4.868

Second Largest 110 Second Largest 4.7

First Quartile 90 First Quartile 4.5

Median 95 Median 4.554

Third Quartile 110 Third Quartile 4.7

Mean 102.1 Mean 4.617

SD 15.24 SD 0.143

Coefficient of Variation 0.149

Skewness 1.112

Warning:  There are only 4 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.82 Shapiro Wilk Test Statistic 0.83

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 137.7   90% UTL with   90% Coverage 141.2

   90% UPL (t) 125.6   90% UPL (t) 126.1

90% Percentile (z) 121.7 90% Percentile (z) 121.5

95% Percentile (z) 127.2 95% Percentile (z) 128

99% Percentile (z) 137.6 99% Percentile (z) 141

Gamma Distribution Test Data Distribution Test

k star 32.03 Data appear Normal at 5% Significance Level

Minnesota UPL Results 43
Theta Star 3.189

MLE of Mean 102.1

MLE of Standard Deviation 18.05

nu star 448.5

A‐D Test Statistic 0.629 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 118

K‐S Test Statistic 0.26 95% Percentile 124

5% K‐S Critical Value 0.311 99% Percentile 128.8

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 130

90% Percentile 125.8   90% Percentile Bootstrap UTL with   90% Coverage 130

95% Percentile 133.5   90% BCA Bootstrap UTL with   90% Coverage 118

99% Percentile 148.7   90% UPL 130

  90% Chebyshev UPL 151

   90% WH Approx. Gamma UPL 125.9 Upper Threshold Limit Based upon IQR 140

   90% HW Approx. Gamma UPL 125.9

   90% WH Approx. Gamma UTL with   90% Coverage 139.8

   90% HW Approx. Gamma UTL with   90% Coverage 140.1

Fluoride

General Statistics

Total Number of Observations 7 Number of Distinct Observations 4

Raw Statistics Log‐Transformed Statistics

Minimum 5 Minimum 1.609

Maximum 25 Maximum 3.219

Second Largest 25 Second Largest 3.219

First Quartile 6 First Quartile 1.792

Median 24 Median 3.178

Third Quartile 25 Third Quartile 3.219

Mean 16.57 Mean 2.575

SD 10.21 SD 0.792

Coefficient of Variation 0.616

Skewness ‐0.374

Warning:  There are only 4 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.697 Shapiro Wilk Test Statistic 0.71

Minnesota UPL Results 44
Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 40.4   90% UTL with   90% Coverage 83.42

   90% UPL (t) 32.29   90% UPL (t) 44.47

90% Percentile (z) 29.66 90% Percentile (z) 36.26

95% Percentile (z) 33.37 95% Percentile (z) 48.36

99% Percentile (z) 40.33 99% Percentile (z) 82.98

Gamma Distribution Test Data Distribution Test

k star 1.413 Data do not follow a Discernable Distribution (0.05)

Theta Star 11.73

MLE of Mean 16.57

MLE of Standard Deviation 13.94

nu star 19.78

A‐D Test Statistic 1.142 Nonparametric Statistics

5% A‐D Critical Value 0.714 90% Percentile 25

K‐S Test Statistic 0.364 95% Percentile 25

5% K‐S Critical Value 0.315 99% Percentile 25

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 25

90% Percentile 35.04   90% Percentile Bootstrap UTL with   90% Coverage 25

95% Percentile 44.05   90% BCA Bootstrap UTL with   90% Coverage 25

99% Percentile 64.46   90% UPL 25

  90% Chebyshev UPL 49.32

   90% WH Approx. Gamma UPL 38.02 Upper Threshold Limit Based upon IQR 53.5

   90% HW Approx. Gamma UPL 39.25

   90% WH Approx. Gamma UTL with   90% Coverage 56.8

   90% HW Approx. Gamma UTL with   90% Coverage 61.1

1,1,2,2‐Tetrachloroethane

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4.43 Minimum 1.488

Maximum 4.61 Maximum 1.528

Second Largest 4.61 Second Largest 1.528

First Quartile 4.43 First Quartile 1.488

Median 4.61 Median 1.528

Third Quartile 4.61 Third Quartile 1.528

Mean 4.533 Mean 1.511

SD 0.0962 SD 0.0213

Coefficient of Variation 0.0212

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

Minnesota UPL Results 45
However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4.757   90% UTL with   90% Coverage 4.763

   90% UPL (t) 4.681   90% UPL (t) 4.683

90% Percentile (z) 4.656 90% Percentile (z) 4.657

95% Percentile (z) 4.691 95% Percentile (z) 4.693

99% Percentile (z) 4.757 99% Percentile (z) 4.762

Gamma Distribution Test Data Distribution Test

k star 1474 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00308

MLE of Mean 4.533

MLE of Standard Deviation 0.118

nu star 20636

A‐D Test Statistic 1.296 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4.61

K‐S Test Statistic 0.378 95% Percentile 4.61

5% K‐S Critical Value 0.311 99% Percentile 4.61

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4.61

90% Percentile 4.685   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4.729   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4.812   90% UPL 4.61

  90% Chebyshev UPL 4.841

   90% WH Approx. Gamma UPL 4.682 Upper Threshold Limit Based upon IQR 4.88

   90% HW Approx. Gamma UPL 4.682

   90% WH Approx. Gamma UTL with   90% Coverage 4.761

   90% HW Approx. Gamma UTL with   90% Coverage 4.761

1,1,2‐Trichloroethane

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 7.5 Minimum 2.015

Maximum 7.81 Maximum 2.055

Second Largest 7.81 Second Largest 2.055

First Quartile 7.5 First Quartile 2.015

Median 7.81 Median 2.055

Minnesota UPL Results 46
Third Quartile 7.81 Third Quartile 2.055

Mean 7.677 Mean 2.038

SD 0.166 SD 0.0216

Coefficient of Variation 0.0216

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 8.064   90% UTL with   90% Coverage 8.073

   90% UPL (t) 7.932   90% UPL (t) 7.936

90% Percentile (z) 7.889 90% Percentile (z) 7.892

95% Percentile (z) 7.95 95% Percentile (z) 7.954

99% Percentile (z) 8.063 99% Percentile (z) 8.072

Gamma Distribution Test Data Distribution Test

k star 1425 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00539

MLE of Mean 7.677

MLE of Standard Deviation 0.203

nu star 19956

A‐D Test Statistic 1.296 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 7.81

K‐S Test Statistic 0.378 95% Percentile 7.81

5% K‐S Critical Value 0.311 99% Percentile 7.81

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7.81

90% Percentile 7.939   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 8.015   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 8.158   90% UPL 7.81

  90% Chebyshev UPL 8.209

   90% WH Approx. Gamma UPL 7.934 Upper Threshold Limit Based upon IQR 8.275

   90% HW Approx. Gamma UPL 7.935

   90% WH Approx. Gamma UTL with   90% Coverage 8.07

   90% HW Approx. Gamma UTL with   90% Coverage 8.071

Minnesota UPL Results 47
1,2,4‐Trichlorobenzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 2.5 Minimum 0.916

Maximum 2.6 Maximum 0.956

Second Largest 2.6 Second Largest 0.956

First Quartile 2.5 First Quartile 0.916

Median 2.6 Median 0.956

Third Quartile 2.6 Third Quartile 0.956

Mean 2.557 Mean 0.939

SD 0.0535 SD 0.021

Coefficient of Variation 0.0209

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2.682   90% UTL with   90% Coverage 2.685

   90% UPL (t) 2.639   90% UPL (t) 2.641

90% Percentile (z) 2.626 90% Percentile (z) 2.626

95% Percentile (z) 2.645 95% Percentile (z) 2.646

99% Percentile (z) 2.681 99% Percentile (z) 2.684

Gamma Distribution Test Data Distribution Test

k star 1520 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00168

MLE of Mean 2.557

MLE of Standard Deviation 0.0656

nu star 21280

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2.6

K‐S Test Statistic 0.378 95% Percentile 2.6

5% K‐S Critical Value 0.311 99% Percentile 2.6

Data not Gamma Distributed at 5% Significance Level

Minnesota UPL Results 48
Assuming Gamma Distribution   90% UTL with   90% Coverage 2.6

90% Percentile 2.642   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2.666   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2.712   90% UPL 2.6

  90% Chebyshev UPL 2.729

   90% WH Approx. Gamma UPL 2.64 Upper Threshold Limit Based upon IQR 2.75

   90% HW Approx. Gamma UPL 2.64

   90% WH Approx. Gamma UTL with   90% Coverage 2.684

   90% HW Approx. Gamma UTL with   90% Coverage 2.684

1,4‐Dichlorobenzene(p)

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 1.93 Minimum 0.658

Maximum 2 Maximum 0.693

Second Largest 2 Second Largest 0.693

First Quartile 1.93 First Quartile 0.658

Median 2 Median 0.693

Third Quartile 2 Third Quartile 0.693

Mean 1.97 Mean 0.678

SD 0.0374 SD 0.019

Coefficient of Variation 0.019

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2.057   90% UTL with   90% Coverage 2.059

   90% UPL (t) 2.028   90% UPL (t) 2.028

90% Percentile (z) 2.018 90% Percentile (z) 2.018

95% Percentile (z) 2.032 95% Percentile (z) 2.032

99% Percentile (z) 2.057 99% Percentile (z) 2.059

Minnesota UPL Results 49
Gamma Distribution Test Data Distribution Test

k star 1842 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00107

MLE of Mean 1.97

MLE of Standard Deviation 0.0459

nu star 25784

A‐D Test Statistic 1.3 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2

K‐S Test Statistic 0.378 95% Percentile 2

5% K‐S Critical Value 0.311 99% Percentile 2

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2

90% Percentile 2.029   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2.046   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2.078   90% UPL 2

  90% Chebyshev UPL 2.09

   90% WH Approx. Gamma UPL 2.028 Upper Threshold Limit Based upon IQR 2.105

   90% HW Approx. Gamma UPL 2.028

   90% WH Approx. Gamma UTL with   90% Coverage 2.059

   90% HW Approx. Gamma UTL with   90% Coverage 2.059

Acetonitrile

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 59.7 Minimum 4.089

Maximum 62 Maximum 4.127

Second Largest 62 Second Largest 4.127

First Quartile 59.7 First Quartile 4.089

Median 62 Median 4.127

Third Quartile 62 Third Quartile 4.127

Mean 61.01 Mean 4.111

SD 1.229 SD 0.0202

Coefficient of Variation 0.0201

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Minnesota UPL Results 50
Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 63.88   90% UTL with   90% Coverage 63.95

   90% UPL (t) 62.91   90% UPL (t) 62.93

90% Percentile (z) 62.59 90% Percentile (z) 62.6

95% Percentile (z) 63.04 95% Percentile (z) 63.07

99% Percentile (z) 63.87 99% Percentile (z) 63.94

Gamma Distribution Test Data Distribution Test

k star 1636 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0373

MLE of Mean 61.01

MLE of Standard Deviation 1.508

nu star 22905

A‐D Test Statistic 1.298 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 62

K‐S Test Statistic 0.378 95% Percentile 62

5% K‐S Critical Value 0.311 99% Percentile 62

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 62

90% Percentile 62.96   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 63.52   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 64.58   90% UPL 62

  90% Chebyshev UPL 64.96

   90% WH Approx. Gamma UPL 62.92 Upper Threshold Limit Based upon IQR 65.45

   90% HW Approx. Gamma UPL 62.92

   90% WH Approx. Gamma UTL with   90% Coverage 63.93

   90% HW Approx. Gamma UTL with   90% Coverage 63.93

Acrolein

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 133 Minimum 4.89

Maximum 138 Maximum 4.927

Second Largest 138 Second Largest 4.927

First Quartile 133 First Quartile 4.89

Median 138 Median 4.927

Third Quartile 138 Third Quartile 4.927

Mean 135.9 Mean 4.911

SD 2.673 SD 0.0197

Coefficient of Variation 0.0197

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

Minnesota UPL Results 51
It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 142.1   90% UTL with   90% Coverage 142.2

   90% UPL (t) 140   90% UPL (t) 140

90% Percentile (z) 139.3 90% Percentile (z) 139.3

95% Percentile (z) 140.3 95% Percentile (z) 140.3

99% Percentile (z) 142.1 99% Percentile (z) 142.2

Gamma Distribution Test Data Distribution Test

k star 1717 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0791

MLE of Mean 135.9

MLE of Standard Deviation 3.279

nu star 24031

A‐D Test Statistic 1.299 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 138

K‐S Test Statistic 0.378 95% Percentile 138

5% K‐S Critical Value 0.311 99% Percentile 138

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 138

90% Percentile 140.1   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 141.3   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 143.6   90% UPL 138

  90% Chebyshev UPL 144.4

   90% WH Approx. Gamma UPL 140 Upper Threshold Limit Based upon IQR 145.5

   90% HW Approx. Gamma UPL 140

   90% WH Approx. Gamma UTL with   90% Coverage 142.2

   90% HW Approx. Gamma UTL with   90% Coverage 142.2

Acrylonitrile

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 50 Minimum 3.912

Maximum 52 Maximum 3.951

Second Largest 52 Second Largest 3.951

Minnesota UPL Results 52
First Quartile 50 First Quartile 3.912

Median 52 Median 3.951

Third Quartile 52 Third Quartile 3.951

Mean 51.14 Mean 3.934

SD 1.069 SD 0.021

Coefficient of Variation 0.0209

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 53.64   90% UTL with   90% Coverage 53.7

   90% UPL (t) 52.79   90% UPL (t) 52.81

90% Percentile (z) 52.51 90% Percentile (z) 52.53

95% Percentile (z) 52.9 95% Percentile (z) 52.93

99% Percentile (z) 53.63 99% Percentile (z) 53.69

Gamma Distribution Test Data Distribution Test

k star 1520 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0336

MLE of Mean 51.14

MLE of Standard Deviation 1.312

nu star 21280

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 52

K‐S Test Statistic 0.378 95% Percentile 52

5% K‐S Critical Value 0.311 99% Percentile 52

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 52

90% Percentile 52.83   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 53.32   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 54.24   90% UPL 52

  90% Chebyshev UPL 54.57

   90% WH Approx. Gamma UPL 52.8 Upper Threshold Limit Based upon IQR 55

   90% HW Approx. Gamma UPL 52.8

   90% WH Approx. Gamma UTL with   90% Coverage 53.68

   90% HW Approx. Gamma UTL with   90% Coverage 53.68

Minnesota UPL Results 53
Allyl Chloride

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 6.93 Minimum 1.936

Maximum 7.2 Maximum 1.974

Second Largest 7.2 Second Largest 1.974

First Quartile 6.93 First Quartile 1.936

Median 7.2 Median 1.974

Third Quartile 7.2 Third Quartile 1.974

Mean 7.084 Mean 1.958

SD 0.144 SD 0.0204

Coefficient of Variation 0.0204

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7.421   90% UTL with   90% Coverage 7.429

   90% UPL (t) 7.306   90% UPL (t) 7.309

90% Percentile (z) 7.269 90% Percentile (z) 7.271

95% Percentile (z) 7.322 95% Percentile (z) 7.325

99% Percentile (z) 7.42 99% Percentile (z) 7.428

Gamma Distribution Test Data Distribution Test

k star 1600 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00443

MLE of Mean 7.084

MLE of Standard Deviation 0.177

nu star 22406

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 7.2

K‐S Test Statistic 0.378 95% Percentile 7.2

Minnesota UPL Results 54
5% K‐S Critical Value 0.311 99% Percentile 7.2

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7.2

90% Percentile 7.312   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 7.378   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 7.503   90% UPL 7.2

  90% Chebyshev UPL 7.547

   90% WH Approx. Gamma UPL 7.308 Upper Threshold Limit Based upon IQR 7.605

   90% HW Approx. Gamma UPL 7.309

   90% WH Approx. Gamma UTL with   90% Coverage 7.426

   90% HW Approx. Gamma UTL with   90% Coverage 7.427

Benzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3.27 Minimum 1.185

Maximum 3.41 Maximum 1.227

Second Largest 3.41 Second Largest 1.227

First Quartile 3.27 First Quartile 1.185

Median 3.41 Median 1.227

Third Quartile 3.41 Third Quartile 1.227

Mean 3.35 Mean 1.209

SD 0.0748 SD 0.0224

Coefficient of Variation 0.0223

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3.525   90% UTL with   90% Coverage 3.529

   90% UPL (t) 3.465   90% UPL (t) 3.467

90% Percentile (z) 3.446 90% Percentile (z) 3.447

95% Percentile (z) 3.473 95% Percentile (z) 3.475

Minnesota UPL Results 55
99% Percentile (z) 3.524 99% Percentile (z) 3.529

Gamma Distribution Test Data Distribution Test

k star 1331 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00252

MLE of Mean 3.35

MLE of Standard Deviation 0.0918

nu star 18628

A‐D Test Statistic 1.295 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3.41

K‐S Test Statistic 0.378 95% Percentile 3.41

5% K‐S Critical Value 0.311 99% Percentile 3.41

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3.41

90% Percentile 3.468   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3.502   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3.567   90% UPL 3.41

  90% Chebyshev UPL 3.59

   90% WH Approx. Gamma UPL 3.466 Upper Threshold Limit Based upon IQR 3.62

   90% HW Approx. Gamma UPL 3.466

   90% WH Approx. Gamma UTL with   90% Coverage 3.528

   90% HW Approx. Gamma UTL with   90% Coverage 3.528

Bromoform

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 6.54 Minimum 1.878

Maximum 6.81 Maximum 1.918

Second Largest 6.81 Second Largest 1.918

First Quartile 6.54 First Quartile 1.878

Median 6.81 Median 1.918

Third Quartile 6.81 Third Quartile 1.918

Mean 6.694 Mean 1.901

SD 0.144 SD 0.0216

Coefficient of Variation 0.0216

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Minnesota UPL Results 56
Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7.031   90% UTL with   90% Coverage 7.039

   90% UPL (t) 6.916   90% UPL (t) 6.919

90% Percentile (z) 6.879 90% Percentile (z) 6.881

95% Percentile (z) 6.932 95% Percentile (z) 6.935

99% Percentile (z) 7.03 99% Percentile (z) 7.038

Gamma Distribution Test Data Distribution Test

k star 1429 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00469

MLE of Mean 6.694

MLE of Standard Deviation 0.177

nu star 20003

A‐D Test Statistic 1.296 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6.81

K‐S Test Statistic 0.378 95% Percentile 6.81

5% K‐S Critical Value 0.311 99% Percentile 6.81

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 6.81

90% Percentile 6.922   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 6.988   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 7.113   90% UPL 6.81

  90% Chebyshev UPL 7.157

   90% WH Approx. Gamma UPL 6.918 Upper Threshold Limit Based upon IQR 7.215

   90% HW Approx. Gamma UPL 6.919

   90% WH Approx. Gamma UTL with   90% Coverage 7.036

   90% HW Approx. Gamma UTL with   90% Coverage 7.037

Chlorobenzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 2.7 Minimum 0.993

Maximum 2.81 Maximum 1.033

Second Largest 2.81 Second Largest 1.033

First Quartile 2.7 First Quartile 0.993

Median 2.81 Median 1.033

Third Quartile 2.81 Third Quartile 1.033

Mean 2.763 Mean 1.016

SD 0.0588 SD 0.0213

Coefficient of Variation 0.0213

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

Minnesota UPL Results 57
There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2.9   90% UTL with   90% Coverage 2.903

   90% UPL (t) 2.853   90% UPL (t) 2.855

90% Percentile (z) 2.838 90% Percentile (z) 2.839

95% Percentile (z) 2.86 95% Percentile (z) 2.861

99% Percentile (z) 2.9 99% Percentile (z) 2.903

Gamma Distribution Test Data Distribution Test

k star 1466 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00188

MLE of Mean 2.763

MLE of Standard Deviation 0.0722

nu star 20529

A‐D Test Statistic 1.296 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2.81

K‐S Test Statistic 0.378 95% Percentile 2.81

5% K‐S Critical Value 0.311 99% Percentile 2.81

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2.81

90% Percentile 2.856   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2.883   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2.933   90% UPL 2.81

  90% Chebyshev UPL 2.951

   90% WH Approx. Gamma UPL 2.854 Upper Threshold Limit Based upon IQR 2.975

   90% HW Approx. Gamma UPL 2.854

   90% WH Approx. Gamma UTL with   90% Coverage 2.902

   90% HW Approx. Gamma UTL with   90% Coverage 2.903

Chloroform

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3.47 Minimum 1.244

Minnesota UPL Results 58
Maximum 3.6 Maximum 1.281

Second Largest 3.6 Second Largest 1.281

First Quartile 3.47 First Quartile 1.244

Median 3.6 Median 1.281

Third Quartile 3.6 Third Quartile 1.281

Mean 3.544 Mean 1.265

SD 0.0695 SD 0.0197

Coefficient of Variation 0.0196

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3.706   90% UTL with   90% Coverage 3.71

   90% UPL (t) 3.651   90% UPL (t) 3.653

90% Percentile (z) 3.633 90% Percentile (z) 3.634

95% Percentile (z) 3.659 95% Percentile (z) 3.66

99% Percentile (z) 3.706 99% Percentile (z) 3.71

Gamma Distribution Test Data Distribution Test

k star 1728 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00205

MLE of Mean 3.544

MLE of Standard Deviation 0.0853

nu star 24195

A‐D Test Statistic 1.299 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3.6

K‐S Test Statistic 0.378 95% Percentile 3.6

5% K‐S Critical Value 0.311 99% Percentile 3.6

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3.6

90% Percentile 3.654   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3.686   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3.746   90% UPL 3.6

  90% Chebyshev UPL 3.767

   90% WH Approx. Gamma UPL 3.652 Upper Threshold Limit Based upon IQR 3.795

   90% HW Approx. Gamma UPL 3.652

Minnesota UPL Results 59
   90% WH Approx. Gamma UTL with   90% Coverage 3.709

   90% HW Approx. Gamma UTL with   90% Coverage 3.709

Chloroprene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4.43 Minimum 1.488

Maximum 4.61 Maximum 1.528

Second Largest 4.61 Second Largest 1.528

First Quartile 4.43 First Quartile 1.488

Median 4.61 Median 1.528

Third Quartile 4.61 Third Quartile 1.528

Mean 4.533 Mean 1.511

SD 0.0962 SD 0.0213

Coefficient of Variation 0.0212

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4.757   90% UTL with   90% Coverage 4.763

   90% UPL (t) 4.681   90% UPL (t) 4.683

90% Percentile (z) 4.656 90% Percentile (z) 4.657

95% Percentile (z) 4.691 95% Percentile (z) 4.693

99% Percentile (z) 4.757 99% Percentile (z) 4.762

Gamma Distribution Test Data Distribution Test

k star 1474 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00308

MLE of Mean 4.533

MLE of Standard Deviation 0.118

nu star 20636

A‐D Test Statistic 1.296 Nonparametric Statistics

Minnesota UPL Results 60
5% A‐D Critical Value 0.708 90% Percentile 4.61

K‐S Test Statistic 0.378 95% Percentile 4.61

5% K‐S Critical Value 0.311 99% Percentile 4.61

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4.61

90% Percentile 4.685   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4.729   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4.812   90% UPL 4.61

  90% Chebyshev UPL 4.841

   90% WH Approx. Gamma UPL 4.682 Upper Threshold Limit Based upon IQR 4.88

   90% HW Approx. Gamma UPL 4.682

   90% WH Approx. Gamma UTL with   90% Coverage 4.761

   90% HW Approx. Gamma UTL with   90% Coverage 4.761

Ethyl benzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 7.12 Minimum 1.963

Maximum 13.5 Maximum 2.603

Second Largest 9.2 Second Largest 2.219

First Quartile 8.235 First Quartile 2.108

Median 8.4 Median 2.128

Third Quartile 9 Third Quartile 2.197

Mean 9.07 Mean 2.186

SD 2.056 SD 0.2

Coefficient of Variation 0.227

Skewness 2.095

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.747 Shapiro Wilk Test Statistic 0.815

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 13.87   90% UTL with   90% Coverage 14.2

   90% UPL (t) 12.23   90% UPL (t) 12.11

90% Percentile (z) 11.7 90% Percentile (z) 11.5

95% Percentile (z) 12.45 95% Percentile (z) 12.37

Minnesota UPL Results 61
99% Percentile (z) 13.85 99% Percentile (z) 14.18

Gamma Distribution Test Data Distribution Test

k star 15.54 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 0.583

MLE of Mean 9.07

MLE of Standard Deviation 2.3

nu star 217.6

A‐D Test Statistic 0.773 Nonparametric Statistics

5% A‐D Critical Value 0.707 90% Percentile 10.92

K‐S Test Statistic 0.302 95% Percentile 12.21

5% K‐S Critical Value 0.311 99% Percentile 13.24

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 13.5

90% Percentile 12.11   90% Percentile Bootstrap UTL with   90% Coverage 13.5

95% Percentile 13.16   90% BCA Bootstrap UTL with   90% Coverage 13.5

99% Percentile 15.26   90% UPL 13.5

  90% Chebyshev UPL 15.66

   90% WH Approx. Gamma UPL 12.15 Upper Threshold Limit Based upon IQR 10.15

   90% HW Approx. Gamma UPL 12.14

   90% WH Approx. Gamma UTL with   90% Coverage 14.06

   90% HW Approx. Gamma UTL with   90% Coverage 14.09

Hexachlorobutadiene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4.43 Minimum 1.488

Maximum 4.61 Maximum 1.528

Second Largest 4.61 Second Largest 1.528

First Quartile 4.43 First Quartile 1.488

Median 4.61 Median 1.528

Third Quartile 4.61 Third Quartile 1.528

Mean 4.533 Mean 1.511

SD 0.0962 SD 0.0213

Coefficient of Variation 0.0212

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Minnesota UPL Results 62
Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4.757   90% UTL with   90% Coverage 4.763

   90% UPL (t) 4.681   90% UPL (t) 4.683

90% Percentile (z) 4.656 90% Percentile (z) 4.657

95% Percentile (z) 4.691 95% Percentile (z) 4.693

99% Percentile (z) 4.757 99% Percentile (z) 4.762

Gamma Distribution Test Data Distribution Test

k star 1474 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00308

MLE of Mean 4.533

MLE of Standard Deviation 0.118

nu star 20636

A‐D Test Statistic 1.296 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4.61

K‐S Test Statistic 0.378 95% Percentile 4.61

5% K‐S Critical Value 0.311 99% Percentile 4.61

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4.61

90% Percentile 4.685   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4.729   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4.812   90% UPL 4.61

  90% Chebyshev UPL 4.841

   90% WH Approx. Gamma UPL 4.682 Upper Threshold Limit Based upon IQR 4.88

   90% HW Approx. Gamma UPL 4.682

   90% WH Approx. Gamma UTL with   90% Coverage 4.761

   90% HW Approx. Gamma UTL with   90% Coverage 4.761

Isopropylbenzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 3

Raw Statistics Log‐Transformed Statistics

Minimum 2.7 Minimum 0.993

Maximum 2.81 Maximum 1.033

Second Largest 2.81 Second Largest 1.033

First Quartile 2.75 First Quartile 1.011

Median 2.81 Median 1.033

Third Quartile 2.81 Third Quartile 1.033

Mean 2.777 Mean 1.021

SD 0.0528 SD 0.0192

Coefficient of Variation 0.019

Skewness ‐1.21

Warning:  There are only 3 Distinct Values in this data

Minnesota UPL Results 63
There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.637 Shapiro Wilk Test Statistic 0.637

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2.9   90% UTL with   90% Coverage 2.904

   90% UPL (t) 2.858   90% UPL (t) 2.86

90% Percentile (z) 2.845 90% Percentile (z) 2.846

95% Percentile (z) 2.864 95% Percentile (z) 2.866

99% Percentile (z) 2.9 99% Percentile (z) 2.903

Gamma Distribution Test Data Distribution Test

k star 1822 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00152

MLE of Mean 2.777

MLE of Standard Deviation 0.0651

nu star 25512

A‐D Test Statistic 1.392 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2.81

K‐S Test Statistic 0.395 95% Percentile 2.81

5% K‐S Critical Value 0.311 99% Percentile 2.81

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2.81

90% Percentile 2.861   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2.885   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2.931   90% UPL 2.81

  90% Chebyshev UPL 2.947

   90% WH Approx. Gamma UPL 2.859 Upper Threshold Limit Based upon IQR 2.9

   90% HW Approx. Gamma UPL 2.86

   90% WH Approx. Gamma UTL with   90% Coverage 2.903

   90% HW Approx. Gamma UTL with   90% Coverage 2.903

m,p‐Xylenes

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 18.6 Minimum 2.923

Minnesota UPL Results 64
Maximum 41.7 Maximum 3.731

Second Largest 24.6 Second Largest 3.203

First Quartile 21.15 First Quartile 3.051

Median 22.1 Median 3.096

Third Quartile 24.1 Third Quartile 3.182

Mean 24.7 Mean 3.174

SD 7.746 SD 0.262

Coefficient of Variation 0.314

Skewness 2.295

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.7 Shapiro Wilk Test Statistic 0.787

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 42.77   90% UTL with   90% Coverage 44.01

   90% UPL (t) 36.62   90% UPL (t) 35.75

90% Percentile (z) 34.63 90% Percentile (z) 33.42

95% Percentile (z) 37.44 95% Percentile (z) 36.76

99% Percentile (z) 42.72 99% Percentile (z) 43.94

Gamma Distribution Test Data Distribution Test

k star 8.818 Data do not follow a Discernable Distribution (0.05)

Theta Star 2.801

MLE of Mean 24.7

MLE of Standard Deviation 8.318

nu star 123.5

A‐D Test Statistic 0.85 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 31.44

K‐S Test Statistic 0.329 95% Percentile 36.57

5% K‐S Critical Value 0.312 99% Percentile 40.67

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 41.7

90% Percentile 35.78   90% Percentile Bootstrap UTL with   90% Coverage 41.7

95% Percentile 39.78   90% BCA Bootstrap UTL with   90% Coverage 41.7

99% Percentile 48.04   90% UPL 41.7

  90% Chebyshev UPL 49.54

   90% WH Approx. Gamma UPL 36.03 Upper Threshold Limit Based upon IQR 28.53

   90% HW Approx. Gamma UPL 35.96

   90% WH Approx. Gamma UTL with   90% Coverage 43.46

   90% HW Approx. Gamma UTL with   90% Coverage 43.58

Minnesota UPL Results 65
Methyl methacrylate

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 7.5 Minimum 2.015

Maximum 7.81 Maximum 2.055

Second Largest 7.81 Second Largest 2.055

First Quartile 7.5 First Quartile 2.015

Median 7.81 Median 2.055

Third Quartile 7.81 Third Quartile 2.055

Mean 7.677 Mean 2.038

SD 0.166 SD 0.0216

Coefficient of Variation 0.0216

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 8.064   90% UTL with   90% Coverage 8.073

   90% UPL (t) 7.932   90% UPL (t) 7.936

90% Percentile (z) 7.889 90% Percentile (z) 7.892

95% Percentile (z) 7.95 95% Percentile (z) 7.954

99% Percentile (z) 8.063 99% Percentile (z) 8.072

Gamma Distribution Test Data Distribution Test

k star 1425 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00539

MLE of Mean 7.677

MLE of Standard Deviation 0.203

nu star 19956

A‐D Test Statistic 1.296 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 7.81

K‐S Test Statistic 0.378 95% Percentile 7.81

Minnesota UPL Results 66
5% K‐S Critical Value 0.311 99% Percentile 7.81

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7.81

90% Percentile 7.939   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 8.015   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 8.158   90% UPL 7.81

  90% Chebyshev UPL 8.209

   90% WH Approx. Gamma UPL 7.934 Upper Threshold Limit Based upon IQR 8.275

   90% HW Approx. Gamma UPL 7.935

   90% WH Approx. Gamma UTL with   90% Coverage 8.07

   90% HW Approx. Gamma UTL with   90% Coverage 8.071

Methyl tert butyl ether

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5 Minimum 1.609

Maximum 5.2 Maximum 1.649

Second Largest 5.2 Second Largest 1.649

First Quartile 5 First Quartile 1.609

Median 5.2 Median 1.649

Third Quartile 5.2 Third Quartile 1.649

Mean 5.114 Mean 1.632

SD 0.107 SD 0.021

Coefficient of Variation 0.0209

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5.364   90% UTL with   90% Coverage 5.37

   90% UPL (t) 5.279   90% UPL (t) 5.281

90% Percentile (z) 5.251 90% Percentile (z) 5.253

95% Percentile (z) 5.29 95% Percentile (z) 5.293

Minnesota UPL Results 67
99% Percentile (z) 5.363 99% Percentile (z) 5.369

Gamma Distribution Test Data Distribution Test

k star 1520 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00336

MLE of Mean 5.114

MLE of Standard Deviation 0.131

nu star 21280

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5.2

K‐S Test Statistic 0.378 95% Percentile 5.2

5% K‐S Critical Value 0.311 99% Percentile 5.2

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5.2

90% Percentile 5.283   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5.332   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5.424   90% UPL 5.2

  90% Chebyshev UPL 5.457

   90% WH Approx. Gamma UPL 5.28 Upper Threshold Limit Based upon IQR 5.5

   90% HW Approx. Gamma UPL 5.28

   90% WH Approx. Gamma UTL with   90% Coverage 5.368

   90% HW Approx. Gamma UTL with   90% Coverage 5.368

Methylene chloride

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 25.4 Minimum 3.235

Maximum 35.8 Maximum 3.578

Second Largest 34.6 Second Largest 3.544

First Quartile 28.1 First Quartile 3.333

Median 31.6 Median 3.453

Third Quartile 33.9 Third Quartile 3.523

Mean 30.97 Mean 3.425

SD 4.045 SD 0.135

Coefficient of Variation 0.131

Skewness ‐0.439

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Minnesota UPL Results 68
Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.921 Shapiro Wilk Test Statistic 0.906

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 40.41   90% UTL with   90% Coverage 42.07

   90% UPL (t) 37.2   90% UPL (t) 37.81

90% Percentile (z) 36.16 90% Percentile (z) 36.52

95% Percentile (z) 37.63 95% Percentile (z) 38.35

99% Percentile (z) 40.38 99% Percentile (z) 42.04

Gamma Distribution Test Data Distribution Test

k star 37.74 Data appear Normal at 5% Significance Level

Theta Star 0.821

MLE of Mean 30.97

MLE of Standard Deviation 5.041

nu star 528.4

A‐D Test Statistic 0.357 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 35.08

K‐S Test Statistic 0.195 95% Percentile 35.44

5% K‐S Critical Value 0.311 99% Percentile 35.73

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 35.8

90% Percentile 37.58   90% Percentile Bootstrap UTL with   90% Coverage 35.8

95% Percentile 39.7   90% BCA Bootstrap UTL with   90% Coverage 35.8

99% Percentile 43.89   90% UPL 35.8

  90% Chebyshev UPL 43.95

   90% WH Approx. Gamma UPL 37.58 Upper Threshold Limit Based upon IQR 42.6

   90% HW Approx. Gamma UPL 37.64

   90% WH Approx. Gamma UTL with   90% Coverage 41.43

   90% HW Approx. Gamma UTL with   90% Coverage 41.58

Naphthalene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 80.6 Minimum 4.389

Maximum 179 Maximum 5.187

Second Largest 140 Second Largest 4.942

First Quartile 121.5 First Quartile 4.799

Median 136 Median 4.913

Third Quartile 140 Third Quartile 4.942

Mean 131.2 Mean 4.853

SD 29.54 SD 0.243

Coefficient of Variation 0.225

Skewness ‐0.198

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

Minnesota UPL Results 69
If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.939 Shapiro Wilk Test Statistic 0.904

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 200.1   90% UTL with   90% Coverage 225.7

   90% UPL (t) 176.7   90% UPL (t) 186.2

90% Percentile (z) 169.1 90% Percentile (z) 174.9

95% Percentile (z) 179.8 95% Percentile (z) 191

99% Percentile (z) 199.9 99% Percentile (z) 225.3

Gamma Distribution Test Data Distribution Test

k star 12.18 Data appear Normal at 5% Significance Level

Theta Star 10.77

MLE of Mean 131.2

MLE of Standard Deviation 37.6

nu star 170.6

A‐D Test Statistic 0.409 Nonparametric Statistics

5% A‐D Critical Value 0.707 90% Percentile 155.6

K‐S Test Statistic 0.212 95% Percentile 167.3

5% K‐S Critical Value 0.311 99% Percentile 176.7

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 179

90% Percentile 181.1   90% Percentile Bootstrap UTL with   90% Coverage 179

95% Percentile 198.6   90% BCA Bootstrap UTL with   90% Coverage 155.6

99% Percentile 234.1   90% UPL 179

  90% Chebyshev UPL 226

   90% WH Approx. Gamma UPL 182 Upper Threshold Limit Based upon IQR 167.8

   90% HW Approx. Gamma UPL 183

   90% WH Approx. Gamma UTL with   90% Coverage 214.2

   90% HW Approx. Gamma UTL with   90% Coverage 216.7

n‐Hexane

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 6.16 Minimum 1.818

Maximum 6.4 Maximum 1.856

Second Largest 6.4 Second Largest 1.856

First Quartile 6.16 First Quartile 1.818

Median 6.4 Median 1.856

Minnesota UPL Results 70
Third Quartile 6.4 Third Quartile 1.856

Mean 6.297 Mean 1.84

SD 0.128 SD 0.0204

Coefficient of Variation 0.0204

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 6.596   90% UTL with   90% Coverage 6.603

   90% UPL (t) 6.495   90% UPL (t) 6.497

90% Percentile (z) 6.462 90% Percentile (z) 6.463

95% Percentile (z) 6.508 95% Percentile (z) 6.511

99% Percentile (z) 6.596 99% Percentile (z) 6.602

Gamma Distribution Test Data Distribution Test

k star 1600 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00393

MLE of Mean 6.297

MLE of Standard Deviation 0.157

nu star 22406

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6.4

K‐S Test Statistic 0.378 95% Percentile 6.4

5% K‐S Critical Value 0.311 99% Percentile 6.4

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 6.4

90% Percentile 6.5   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 6.558   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 6.669   90% UPL 6.4

  90% Chebyshev UPL 6.709

   90% WH Approx. Gamma UPL 6.496 Upper Threshold Limit Based upon IQR 6.76

   90% HW Approx. Gamma UPL 6.496

   90% WH Approx. Gamma UTL with   90% Coverage 6.601

   90% HW Approx. Gamma UTL with   90% Coverage 6.602

Minnesota UPL Results 71
o‐Xylenes

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 10 Minimum 2.303

Maximum 26 Maximum 3.258

Second Largest 12.3 Second Largest 2.51

First Quartile 10.3 First Quartile 2.332

Median 10.6 Median 2.361

Third Quartile 12.05 Third Quartile 2.489

Mean 13.04 Mean 2.509

SD 5.778 SD 0.339

Coefficient of Variation 0.443

Skewness 2.527

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.583 Shapiro Wilk Test Statistic 0.65

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 26.52   90% UTL with   90% Coverage 27.12

   90% UPL (t) 21.94   90% UPL (t) 20.72

90% Percentile (z) 20.45 90% Percentile (z) 18.99

95% Percentile (z) 22.55 95% Percentile (z) 21.48

99% Percentile (z) 26.48 99% Percentile (z) 27.06

Gamma Distribution Test Data Distribution Test

k star 5.016 Data do not follow a Discernable Distribution (0.05)

Theta Star 2.6

MLE of Mean 13.04

MLE of Standard Deviation 5.823

nu star 70.23

A‐D Test Statistic 1.293 Nonparametric Statistics

5% A‐D Critical Value 0.709 90% Percentile 17.78

K‐S Test Statistic 0.379 95% Percentile 21.89

5% K‐S Critical Value 0.312 99% Percentile 25.18

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 26

Minnesota UPL Results 72
90% Percentile 20.84   90% Percentile Bootstrap UTL with   90% Coverage 26

95% Percentile 23.86   90% BCA Bootstrap UTL with   90% Coverage 26

99% Percentile 30.24   90% UPL 26

  90% Chebyshev UPL 31.57

   90% WH Approx. Gamma UPL 21.15 Upper Threshold Limit Based upon IQR 14.68

   90% HW Approx. Gamma UPL 21.04

   90% WH Approx. Gamma UTL with   90% Coverage 26.85

   90% HW Approx. Gamma UTL with   90% Coverage 26.91

Styrene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 21.7 Minimum 3.077

Maximum 49.4 Maximum 3.9

Second Largest 48 Second Largest 3.871

First Quartile 29 First Quartile 3.367

Median 39.2 Median 3.669

Third Quartile 44.85 Third Quartile 3.801

Mean 36.86 Mean 3.569

SD 10.53 SD 0.306

Coefficient of Variation 0.286

Skewness ‐0.2

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.935 Shapiro Wilk Test Statistic 0.925

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 61.42   90% UTL with   90% Coverage 72.43

   90% UPL (t) 53.06   90% UPL (t) 56.81

90% Percentile (z) 50.35 90% Percentile (z) 52.51

95% Percentile (z) 54.17 95% Percentile (z) 58.68

99% Percentile (z) 61.35 99% Percentile (z) 72.29

Gamma Distribution Test Data Distribution Test

k star 7.655 Data appear Normal at 5% Significance Level

Theta Star 4.815

MLE of Mean 36.86

Minnesota UPL Results 73
MLE of Standard Deviation 13.32

nu star 107.2

A‐D Test Statistic 0.311 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 48.56

K‐S Test Statistic 0.196 95% Percentile 48.98

5% K‐S Critical Value 0.312 99% Percentile 49.32

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 49.4

90% Percentile 54.62   90% Percentile Bootstrap UTL with   90% Coverage 49.4

95% Percentile 61.15   90% BCA Bootstrap UTL with   90% Coverage 49.4

99% Percentile 74.68   90% UPL 49.4

  90% Chebyshev UPL 70.62

   90% WH Approx. Gamma UPL 55.2 Upper Threshold Limit Based upon IQR 68.63

   90% HW Approx. Gamma UPL 55.56

   90% WH Approx. Gamma UTL with   90% Coverage 67.38

   90% HW Approx. Gamma UTL with   90% Coverage 68.46

Tetrachloroethylene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4.81 Minimum 1.571

Maximum 5 Maximum 1.609

Second Largest 5 Second Largest 1.609

First Quartile 4.81 First Quartile 1.571

Median 5 Median 1.609

Third Quartile 5 Third Quartile 1.609

Mean 4.919 Mean 1.593

SD 0.102 SD 0.0207

Coefficient of Variation 0.0206

Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Minnesota UPL Results 74
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5.156   90% UTL with   90% Coverage 5.161

   90% UPL (t) 5.075   90% UPL (t) 5.077

90% Percentile (z) 5.049 90% Percentile (z) 5.05

95% Percentile (z) 5.086 95% Percentile (z) 5.088

99% Percentile (z) 5.155 99% Percentile (z) 5.16

Gamma Distribution Test Data Distribution Test

k star 1558 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00316

MLE of Mean 4.919

MLE of Standard Deviation 0.125

nu star 21810

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5

K‐S Test Statistic 0.378 95% Percentile 5

5% K‐S Critical Value 0.311 99% Percentile 5

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5

90% Percentile 5.079   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5.125   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5.213   90% UPL 5

  90% Chebyshev UPL 5.244

   90% WH Approx. Gamma UPL 5.076 Upper Threshold Limit Based upon IQR 5.285

   90% HW Approx. Gamma UPL 5.076

   90% WH Approx. Gamma UTL with   90% Coverage 5.159

   90% HW Approx. Gamma UTL with   90% Coverage 5.16

Toluene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 144 Minimum 4.97

Maximum 221 Maximum 5.398

Second Largest 215 Second Largest 5.371

First Quartile 183.5 First Quartile 5.208

Median 202 Median 5.308

Third Quartile 211 Third Quartile 5.352

Mean 193.7 Mean 5.256

SD 28.09 SD 0.156

Coefficient of Variation 0.145

Skewness ‐1.167

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Minnesota UPL Results 75
Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.857 Shapiro Wilk Test Statistic 0.832

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 259.3   90% UTL with   90% Coverage 276.3

   90% UPL (t) 237   90% UPL (t) 244

90% Percentile (z) 229.7 90% Percentile (z) 234.4

95% Percentile (z) 239.9 95% Percentile (z) 248.1

99% Percentile (z) 259.1 99% Percentile (z) 276

Gamma Distribution Test Data Distribution Test

k star 28.84 Data appear Normal at 5% Significance Level

Theta Star 6.716

MLE of Mean 193.7

MLE of Standard Deviation 36.07

nu star 403.8

A‐D Test Statistic 0.631 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 217.4

K‐S Test Statistic 0.336 95% Percentile 219.2

5% K‐S Critical Value 0.311 99% Percentile 220.6

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 221

90% Percentile 241.1   90% Percentile Bootstrap UTL with   90% Coverage 221

95% Percentile 256.6   90% BCA Bootstrap UTL with   90% Coverage 221

99% Percentile 287.3   90% UPL 221

  90% Chebyshev UPL 283.8

   90% WH Approx. Gamma UPL 241.3 Upper Threshold Limit Based upon IQR 252.3

   90% HW Approx. Gamma UPL 241.9

   90% WH Approx. Gamma UTL with   90% Coverage 269.4

   90% HW Approx. Gamma UTL with   90% Coverage 271

Vinyl Chloride

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5 Minimum 1.609

Maximum 5.2 Maximum 1.649

Second Largest 5.2 Second Largest 1.649

First Quartile 5 First Quartile 1.609

Median 5.2 Median 1.649

Third Quartile 5.2 Third Quartile 1.649

Mean 5.114 Mean 1.632

SD 0.107 SD 0.021

Coefficient of Variation 0.0209

Minnesota UPL Results 76
Skewness ‐0.374

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.663 Shapiro Wilk Test Statistic 0.663

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5.364   90% UTL with   90% Coverage 5.37

   90% UPL (t) 5.279   90% UPL (t) 5.281

90% Percentile (z) 5.251 90% Percentile (z) 5.253

95% Percentile (z) 5.29 95% Percentile (z) 5.293

99% Percentile (z) 5.363 99% Percentile (z) 5.369

Gamma Distribution Test Data Distribution Test

k star 1520 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00336

MLE of Mean 5.114

MLE of Standard Deviation 0.131

nu star 21280

A‐D Test Statistic 1.297 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5.2

K‐S Test Statistic 0.378 95% Percentile 5.2

5% K‐S Critical Value 0.311 99% Percentile 5.2

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5.2

90% Percentile 5.283   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5.332   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5.424   90% UPL 5.2

  90% Chebyshev UPL 5.457

   90% WH Approx. Gamma UPL 5.28 Upper Threshold Limit Based upon IQR 5.5

   90% HW Approx. Gamma UPL 5.28

   90% WH Approx. Gamma UTL with   90% Coverage 5.368

   90% HW Approx. Gamma UTL with   90% Coverage 5.368

1,2,3‐Trichlorobenzene

General Statistics

Minnesota UPL Results 77
Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5560 Minimum 8.623

Maximum 5730 Maximum 8.653

Second Largest 5730 Second Largest 8.653

First Quartile 5645 First Quartile 8.638

Median 5730 Median 8.653

Third Quartile 5730 Third Quartile 8.653

Mean 5681 Mean 8.645

SD 82.95 SD 0.0147

Coefficient of Variation 0.0146

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5875   90% UTL with   90% Coverage 5879

   90% UPL (t) 5809   90% UPL (t) 5811

90% Percentile (z) 5788 90% Percentile (z) 5789

95% Percentile (z) 5818 95% Percentile (z) 5820

99% Percentile (z) 5874 99% Percentile (z) 5878

Gamma Distribution Test Data Distribution Test

k star 3100 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.832

MLE of Mean 5681

MLE of Standard Deviation 102

nu star 43407

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5730

K‐S Test Statistic 0.451 95% Percentile 5730

5% K‐S Critical Value 0.311 99% Percentile 5730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5730

90% Percentile 5813   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5850   90% BCA Bootstrap UTL with   90% Coverage    N/A    

Minnesota UPL Results 78
99% Percentile 5921   90% UPL 5730

  90% Chebyshev UPL 5947

   90% WH Approx. Gamma UPL 5810 Upper Threshold Limit Based upon IQR 5858

   90% HW Approx. Gamma UPL 5810

   90% WH Approx. Gamma UTL with   90% Coverage 5878

   90% HW Approx. Gamma UTL with   90% Coverage 5878

1,4‐Dichlorobenzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3620 Minimum 8.194

Maximum 3730 Maximum 8.224

Second Largest 3730 Second Largest 8.224

First Quartile 3675 First Quartile 8.209

Median 3730 Median 8.224

Third Quartile 3730 Third Quartile 8.224

Mean 3699 Mean 8.216

SD 53.67 SD 0.0146

Coefficient of Variation 0.0145

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3824   90% UTL with   90% Coverage 3826

   90% UPL (t) 3781   90% UPL (t) 3782

90% Percentile (z) 3767 90% Percentile (z) 3768

95% Percentile (z) 3787 95% Percentile (z) 3788

99% Percentile (z) 3823 99% Percentile (z) 3826

Gamma Distribution Test Data Distribution Test

k star 3138 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.178

MLE of Mean 3699

Minnesota UPL Results 79
MLE of Standard Deviation 66.02

nu star 43939

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3730

K‐S Test Statistic 0.451 95% Percentile 3730

5% K‐S Critical Value 0.311 99% Percentile 3730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3730

90% Percentile 3783   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3808   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3854   90% UPL 3730

  90% Chebyshev UPL 3871

   90% WH Approx. Gamma UPL 3782 Upper Threshold Limit Based upon IQR 3813

   90% HW Approx. Gamma UPL 3782

   90% WH Approx. Gamma UTL with   90% Coverage 3826

   90% HW Approx. Gamma UTL with   90% Coverage 3826

1‐Methylnaphthalene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5830 Minimum 8.671

Maximum 6010 Maximum 8.701

Second Largest 6010 Second Largest 8.701

First Quartile 5920 First Quartile 8.686

Median 6010 Median 8.701

Third Quartile 6010 Third Quartile 8.701

Mean 5959 Mean 8.692

SD 87.83 SD 0.0148

Coefficient of Variation 0.0147

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Minnesota UPL Results 80
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 6163   90% UTL with   90% Coverage 6168

   90% UPL (t) 6094   90% UPL (t) 6096

90% Percentile (z) 6071 90% Percentile (z) 6072

95% Percentile (z) 6103 95% Percentile (z) 6105

99% Percentile (z) 6163 99% Percentile (z) 6167

Gamma Distribution Test Data Distribution Test

k star 3042 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.959

MLE of Mean 5959

MLE of Standard Deviation 108

nu star 42584

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6010

K‐S Test Statistic 0.451 95% Percentile 6010

5% K‐S Critical Value 0.311 99% Percentile 6010

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 6010

90% Percentile 6097   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 6137   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 6213   90% UPL 6010

  90% Chebyshev UPL 6240

   90% WH Approx. Gamma UPL 6095 Upper Threshold Limit Based upon IQR 6145

   90% HW Approx. Gamma UPL 6095

   90% WH Approx. Gamma UTL with   90% Coverage 6166

   90% HW Approx. Gamma UTL with   90% Coverage 6167

2,4,5‐Trichlorophenol

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5030 Minimum 8.523

Maximum 5190 Maximum 8.554

Second Largest 5190 Second Largest 8.554

First Quartile 5110 First Quartile 8.539

Median 5190 Median 8.554

Third Quartile 5190 Third Quartile 8.554

Mean 5144 Mean 8.546

SD 78.07 SD 0.0153

Coefficient of Variation 0.0152

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Minnesota UPL Results 81
Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5326   90% UTL with   90% Coverage 5330

   90% UPL (t) 5264   90% UPL (t) 5266

90% Percentile (z) 5244 90% Percentile (z) 5245

95% Percentile (z) 5273 95% Percentile (z) 5275

99% Percentile (z) 5326 99% Percentile (z) 5330

Gamma Distribution Test Data Distribution Test

k star 2869 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.793

MLE of Mean 5144

MLE of Standard Deviation 96.05

nu star 40161

A‐D Test Statistic 1.576 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5190

K‐S Test Statistic 0.451 95% Percentile 5190

5% K‐S Critical Value 0.311 99% Percentile 5190

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5190

90% Percentile 5268   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5303   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5370   90% UPL 5190

  90% Chebyshev UPL 5395

   90% WH Approx. Gamma UPL 5266 Upper Threshold Limit Based upon IQR 5310

   90% HW Approx. Gamma UPL 5266

   90% WH Approx. Gamma UTL with   90% Coverage 5329

   90% HW Approx. Gamma UTL with   90% Coverage 5329

2,4,6‐Trichlorophenol

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4420 Minimum 8.394

Maximum 4550 Maximum 8.423

Second Largest 4550 Second Largest 8.423

First Quartile 4485 First Quartile 8.408

Median 4550 Median 8.423

Third Quartile 4550 Third Quartile 8.423

Mean 4513 Mean 8.415

Minnesota UPL Results 82
SD 63.43 SD 0.0141

Coefficient of Variation 0.0141

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4661   90% UTL with   90% Coverage 4664

   90% UPL (t) 4610   90% UPL (t) 4612

90% Percentile (z) 4594 90% Percentile (z) 4595

95% Percentile (z) 4617 95% Percentile (z) 4619

99% Percentile (z) 4660 99% Percentile (z) 4663

Gamma Distribution Test Data Distribution Test

k star 3346 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.349

MLE of Mean 4513

MLE of Standard Deviation 78.01

nu star 46849

A‐D Test Statistic 1.58 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4550

K‐S Test Statistic 0.451 95% Percentile 4550

5% K‐S Critical Value 0.311 99% Percentile 4550

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4550

90% Percentile 4613   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4642   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4696   90% UPL 4550

  90% Chebyshev UPL 4716

   90% WH Approx. Gamma UPL 4611 Upper Threshold Limit Based upon IQR 4648

   90% HW Approx. Gamma UPL 4611

   90% WH Approx. Gamma UTL with   90% Coverage 4663

   90% HW Approx. Gamma UTL with   90% Coverage 4663

2,4‐Dinitrophenol

Minnesota UPL Results 83
General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 2030 Minimum 7.616

Maximum 2100 Maximum 7.65

Second Largest 2100 Second Largest 7.65

First Quartile 2065 First Quartile 7.633

Median 2100 Median 7.65

Third Quartile 2100 Third Quartile 7.65

Mean 2080 Mean 7.64

SD 34.16 SD 0.0165

Coefficient of Variation 0.0164

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2160   90% UTL with   90% Coverage 2162

   90% UPL (t) 2133   90% UPL (t) 2133

90% Percentile (z) 2124 90% Percentile (z) 2124

95% Percentile (z) 2136 95% Percentile (z) 2137

99% Percentile (z) 2159 99% Percentile (z) 2161

Gamma Distribution Test Data Distribution Test

k star 2448 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.85

MLE of Mean 2080

MLE of Standard Deviation 42.04

nu star 34277

A‐D Test Statistic 1.574 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2100

K‐S Test Statistic 0.451 95% Percentile 2100

5% K‐S Critical Value 0.311 99% Percentile 2100

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2100

Minnesota UPL Results 84
90% Percentile 2134   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2150   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2179   90% UPL 2100

  90% Chebyshev UPL 2190

   90% WH Approx. Gamma UPL 2133 Upper Threshold Limit Based upon IQR 2153

   90% HW Approx. Gamma UPL 2133

   90% WH Approx. Gamma UTL with   90% Coverage 2161

   90% HW Approx. Gamma UTL with   90% Coverage 2161

2,4‐Dinitrotoluene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3620 Minimum 8.194

Maximum 3730 Maximum 8.224

Second Largest 3730 Second Largest 8.224

First Quartile 3675 First Quartile 8.209

Median 3730 Median 8.224

Third Quartile 3730 Third Quartile 8.224

Mean 3699 Mean 8.216

SD 53.67 SD 0.0146

Coefficient of Variation 0.0145

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3824   90% UTL with   90% Coverage 3826

   90% UPL (t) 3781   90% UPL (t) 3782

90% Percentile (z) 3767 90% Percentile (z) 3768

95% Percentile (z) 3787 95% Percentile (z) 3788

99% Percentile (z) 3823 99% Percentile (z) 3826

Gamma Distribution Test Data Distribution Test

k star 3138 Data do not follow a Discernable Distribution (0.05)

Minnesota UPL Results 85
Theta Star 1.178

MLE of Mean 3699

MLE of Standard Deviation 66.02

nu star 43939

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3730

K‐S Test Statistic 0.451 95% Percentile 3730

5% K‐S Critical Value 0.311 99% Percentile 3730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3730

90% Percentile 3783   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3808   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3854   90% UPL 3730

  90% Chebyshev UPL 3871

   90% WH Approx. Gamma UPL 3782 Upper Threshold Limit Based upon IQR 3813

   90% HW Approx. Gamma UPL 3782

   90% WH Approx. Gamma UTL with   90% Coverage 3826

   90% HW Approx. Gamma UTL with   90% Coverage 3826

2‐Methylnaphthalene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5210 Minimum 8.558

Maximum 5370 Maximum 8.589

Second Largest 5370 Second Largest 8.589

First Quartile 5290 First Quartile 8.573

Median 5370 Median 8.589

Third Quartile 5370 Third Quartile 8.589

Mean 5324 Mean 8.58

SD 78.07 SD 0.0148

Coefficient of Variation 0.0147

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Minnesota UPL Results 86
Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5506   90% UTL with   90% Coverage 5510

   90% UPL (t) 5444   90% UPL (t) 5446

90% Percentile (z) 5424 90% Percentile (z) 5425

95% Percentile (z) 5453 95% Percentile (z) 5455

99% Percentile (z) 5506 99% Percentile (z) 5510

Gamma Distribution Test Data Distribution Test

k star 3074 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.732

MLE of Mean 5324

MLE of Standard Deviation 96.03

nu star 43033

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5370

K‐S Test Statistic 0.451 95% Percentile 5370

5% K‐S Critical Value 0.311 99% Percentile 5370

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5370

90% Percentile 5448   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5483   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5550   90% UPL 5370

  90% Chebyshev UPL 5575

   90% WH Approx. Gamma UPL 5446 Upper Threshold Limit Based upon IQR 5490

   90% HW Approx. Gamma UPL 5446

   90% WH Approx. Gamma UTL with   90% Coverage 5509

   90% HW Approx. Gamma UTL with   90% Coverage 5509

3,3‐Dichlorobenzidene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 7510 Minimum 8.924

Maximum 7730 Maximum 8.953

Second Largest 7730 Second Largest 8.953

First Quartile 7620 First Quartile 8.938

Median 7730 Median 8.953

Third Quartile 7730 Third Quartile 8.953

Mean 7667 Mean 8.945

SD 107.3 SD 0.0141

Coefficient of Variation 0.014

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

Minnesota UPL Results 87
However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7918   90% UTL with   90% Coverage 7923

   90% UPL (t) 7832   90% UPL (t) 7835

90% Percentile (z) 7805 90% Percentile (z) 7806

95% Percentile (z) 7844 95% Percentile (z) 7846

99% Percentile (z) 7917 99% Percentile (z) 7922

Gamma Distribution Test Data Distribution Test

k star 3373 Data do not follow a Discernable Distribution (0.05)

Theta Star 2.273

MLE of Mean 7667

MLE of Standard Deviation 132

nu star 47219

A‐D Test Statistic 1.58 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 7730

K‐S Test Statistic 0.451 95% Percentile 7730

5% K‐S Critical Value 0.311 99% Percentile 7730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7730

90% Percentile 7837   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 7886   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 7978   90% UPL 7730

  90% Chebyshev UPL 8011

   90% WH Approx. Gamma UPL 7834 Upper Threshold Limit Based upon IQR 7895

   90% HW Approx. Gamma UPL 7834

   90% WH Approx. Gamma UTL with   90% Coverage 7921

   90% HW Approx. Gamma UTL with   90% Coverage 7921

4‐Nitrophenol

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4950 Minimum 8.507

Maximum 5100 Maximum 8.537

Second Largest 5100 Second Largest 8.537

First Quartile 5025 First Quartile 8.522

Median 5100 Median 8.537

Minnesota UPL Results 88
Third Quartile 5100 Third Quartile 8.537

Mean 5057 Mean 8.528

SD 73.19 SD 0.0146

Coefficient of Variation 0.0145

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5228   90% UTL with   90% Coverage 5231

   90% UPL (t) 5170   90% UPL (t) 5171

90% Percentile (z) 5151 90% Percentile (z) 5152

95% Percentile (z) 5178 95% Percentile (z) 5179

99% Percentile (z) 5227 99% Percentile (z) 5231

Gamma Distribution Test Data Distribution Test

k star 3156 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.603

MLE of Mean 5057

MLE of Standard Deviation 90.03

nu star 44177

A‐D Test Statistic 1.579 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5100

K‐S Test Statistic 0.451 95% Percentile 5100

5% K‐S Critical Value 0.311 99% Percentile 5100

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5100

90% Percentile 5173   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5206   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5269   90% UPL 5100

  90% Chebyshev UPL 5292

   90% WH Approx. Gamma UPL 5171 Upper Threshold Limit Based upon IQR 5213

   90% HW Approx. Gamma UPL 5171

   90% WH Approx. Gamma UTL with   90% Coverage 5230

   90% HW Approx. Gamma UTL with   90% Coverage 5231

Minnesota UPL Results 89
Acenaphthene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4680 Minimum 8.451

Maximum 4820 Maximum 8.481

Second Largest 4820 Second Largest 8.481

First Quartile 4750 First Quartile 8.466

Median 4820 Median 8.481

Third Quartile 4820 Third Quartile 8.481

Mean 4780 Mean 8.472

SD 68.31 SD 0.0144

Coefficient of Variation 0.0143

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4939   90% UTL with   90% Coverage 4943

   90% UPL (t) 4885   90% UPL (t) 4887

90% Percentile (z) 4868 90% Percentile (z) 4868

95% Percentile (z) 4892 95% Percentile (z) 4894

99% Percentile (z) 4939 99% Percentile (z) 4942

Gamma Distribution Test Data Distribution Test

k star 3237 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.477

MLE of Mean 4780

MLE of Standard Deviation 84.02

nu star 45313

A‐D Test Statistic 1.579 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4820

K‐S Test Statistic 0.451 95% Percentile 4820

5% K‐S Critical Value 0.311 99% Percentile 4820

Data not Gamma Distributed at 5% Significance Level

Minnesota UPL Results 90
Assuming Gamma Distribution   90% UTL with   90% Coverage 4820

90% Percentile 4888   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4919   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4978   90% UPL 4820

  90% Chebyshev UPL 4999

   90% WH Approx. Gamma UPL 4886 Upper Threshold Limit Based upon IQR 4925

   90% HW Approx. Gamma UPL 4886

   90% WH Approx. Gamma UTL with   90% Coverage 4942

   90% HW Approx. Gamma UTL with   90% Coverage 4942

Acenaphthylene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 3

Raw Statistics Log‐Transformed Statistics

Minimum 4150 Minimum 8.331

Maximum 4280 Maximum 8.362

Second Largest 4280 Second Largest 8.362

First Quartile 4265 First Quartile 8.358

Median 4280 Median 8.362

Third Quartile 4280 Third Quartile 8.362

Mean 4257 Mean 8.356

SD 48.55 SD 0.0115

Coefficient of Variation 0.0114

Skewness ‐2.387

Warning:  There are only 3 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.574 Shapiro Wilk Test Statistic 0.573

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4370   90% UTL with   90% Coverage 4373

   90% UPL (t) 4332   90% UPL (t) 4333

90% Percentile (z) 4319 90% Percentile (z) 4320

95% Percentile (z) 4337 95% Percentile (z) 4338

99% Percentile (z) 4370 99% Percentile (z) 4373

Minnesota UPL Results 91
Gamma Distribution Test Data Distribution Test

k star 5059 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.841

MLE of Mean 4257

MLE of Standard Deviation 59.85

nu star 70827

A‐D Test Statistic 1.381 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4280

K‐S Test Statistic 0.408 95% Percentile 4280

5% K‐S Critical Value 0.311 99% Percentile 4280

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4280

90% Percentile 4334   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4356   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4398   90% UPL 4280

  90% Chebyshev UPL 4413

   90% WH Approx. Gamma UPL 4333 Upper Threshold Limit Based upon IQR 4303

   90% HW Approx. Gamma UPL 4333

   90% WH Approx. Gamma UTL with   90% Coverage 4372

   90% HW Approx. Gamma UTL with   90% Coverage 4372

Acetophenone

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4060 Minimum 8.309

Maximum 4190 Maximum 8.34

Second Largest 4190 Second Largest 8.34

First Quartile 4125 First Quartile 8.325

Median 4190 Median 8.34

Third Quartile 4190 Third Quartile 8.34

Mean 4153 Mean 8.331

SD 63.43 SD 0.0154

Coefficient of Variation 0.0153

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Minnesota UPL Results 92
Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4301   90% UTL with   90% Coverage 4304

   90% UPL (t) 4250   90% UPL (t) 4252

90% Percentile (z) 4234 90% Percentile (z) 4235

95% Percentile (z) 4257 95% Percentile (z) 4259

99% Percentile (z) 4300 99% Percentile (z) 4304

Gamma Distribution Test Data Distribution Test

k star 2832 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.467

MLE of Mean 4153

MLE of Standard Deviation 78.04

nu star 39644

A‐D Test Statistic 1.576 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4190

K‐S Test Statistic 0.451 95% Percentile 4190

5% K‐S Critical Value 0.311 99% Percentile 4190

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4190

90% Percentile 4253   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4282   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4337   90% UPL 4190

  90% Chebyshev UPL 4356

   90% WH Approx. Gamma UPL 4251 Upper Threshold Limit Based upon IQR 4288

   90% HW Approx. Gamma UPL 4252

   90% WH Approx. Gamma UTL with   90% Coverage 4303

   90% HW Approx. Gamma UTL with   90% Coverage 4303

Aniline

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 7060 Minimum 8.862

Maximum 7280 Maximum 8.893

Second Largest 7280 Second Largest 8.893

First Quartile 7170 First Quartile 8.878

Median 7280 Median 8.893

Third Quartile 7280 Third Quartile 8.893

Mean 7217 Mean 8.884

SD 107.3 SD 0.015

Coefficient of Variation 0.0149

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

Minnesota UPL Results 93
It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7468   90% UTL with   90% Coverage 7473

   90% UPL (t) 7382   90% UPL (t) 7385

90% Percentile (z) 7355 90% Percentile (z) 7356

95% Percentile (z) 7394 95% Percentile (z) 7396

99% Percentile (z) 7467 99% Percentile (z) 7472

Gamma Distribution Test Data Distribution Test

k star 2987 Data do not follow a Discernable Distribution (0.05)

Theta Star 2.416

MLE of Mean 7217

MLE of Standard Deviation 132.1

nu star 41817

A‐D Test Statistic 1.577 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 7280

K‐S Test Statistic 0.451 95% Percentile 7280

5% K‐S Critical Value 0.311 99% Percentile 7280

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7280

90% Percentile 7387   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 7436   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 7528   90% UPL 7280

  90% Chebyshev UPL 7561

   90% WH Approx. Gamma UPL 7384 Upper Threshold Limit Based upon IQR 7445

   90% HW Approx. Gamma UPL 7384

   90% WH Approx. Gamma UTL with   90% Coverage 7471

   90% HW Approx. Gamma UTL with   90% Coverage 7472

Anthracene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3800 Minimum 8.243

Maximum 3910 Maximum 8.271

Second Largest 3910 Second Largest 8.271

Minnesota UPL Results 94
First Quartile 3855 First Quartile 8.257

Median 3910 Median 8.271

Third Quartile 3910 Third Quartile 8.271

Mean 3879 Mean 8.263

SD 53.67 SD 0.0139

Coefficient of Variation 0.0138

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4004   90% UTL with   90% Coverage 4006

   90% UPL (t) 3961   90% UPL (t) 3962

90% Percentile (z) 3947 90% Percentile (z) 3948

95% Percentile (z) 3967 95% Percentile (z) 3968

99% Percentile (z) 4003 99% Percentile (z) 4006

Gamma Distribution Test Data Distribution Test

k star 3453 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.123

MLE of Mean 3879

MLE of Standard Deviation 66.01

nu star 48339

A‐D Test Statistic 1.581 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3910

K‐S Test Statistic 0.451 95% Percentile 3910

5% K‐S Critical Value 0.311 99% Percentile 3910

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3910

90% Percentile 3963   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3988   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4034   90% UPL 3910

  90% Chebyshev UPL 4051

   90% WH Approx. Gamma UPL 3962 Upper Threshold Limit Based upon IQR 3993

   90% HW Approx. Gamma UPL 3962

   90% WH Approx. Gamma UTL with   90% Coverage 4005

   90% HW Approx. Gamma UTL with   90% Coverage 4006

Minnesota UPL Results 95
Benzo(a)anthracene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4150 Minimum 8.331

Maximum 4280 Maximum 8.362

Second Largest 4280 Second Largest 8.362

First Quartile 4215 First Quartile 8.346

Median 4280 Median 8.362

Third Quartile 4280 Third Quartile 8.362

Mean 4243 Mean 8.353

SD 63.43 SD 0.0151

Coefficient of Variation 0.015

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4391   90% UTL with   90% Coverage 4394

   90% UPL (t) 4340   90% UPL (t) 4342

90% Percentile (z) 4324 90% Percentile (z) 4325

95% Percentile (z) 4347 95% Percentile (z) 4349

99% Percentile (z) 4390 99% Percentile (z) 4394

Gamma Distribution Test Data Distribution Test

k star 2956 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.435

MLE of Mean 4243

MLE of Standard Deviation 78.03

nu star 41388

A‐D Test Statistic 1.577 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4280

K‐S Test Statistic 0.451 95% Percentile 4280

Minnesota UPL Results 96
5% K‐S Critical Value 0.311 99% Percentile 4280

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4280

90% Percentile 4343   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4372   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4426   90% UPL 4280

  90% Chebyshev UPL 4446

   90% WH Approx. Gamma UPL 4341 Upper Threshold Limit Based upon IQR 4378

   90% HW Approx. Gamma UPL 4342

   90% WH Approx. Gamma UTL with   90% Coverage 4393

   90% HW Approx. Gamma UTL with   90% Coverage 4393

Benzo(a)pyrene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3270 Minimum 8.093

Maximum 3370 Maximum 8.123

Second Largest 3370 Second Largest 8.123

First Quartile 3320 First Quartile 8.108

Median 3370 Median 8.123

Third Quartile 3370 Third Quartile 8.123

Mean 3341 Mean 8.114

SD 48.8 SD 0.0147

Coefficient of Variation 0.0146

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3455   90% UTL with   90% Coverage 3458

   90% UPL (t) 3417   90% UPL (t) 3418

90% Percentile (z) 3404 90% Percentile (z) 3405

95% Percentile (z) 3422 95% Percentile (z) 3423

Minnesota UPL Results 97
99% Percentile (z) 3455 99% Percentile (z) 3457

Gamma Distribution Test Data Distribution Test

k star 3099 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.078

MLE of Mean 3341

MLE of Standard Deviation 60.02

nu star 43391

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3370

K‐S Test Statistic 0.451 95% Percentile 3370

5% K‐S Critical Value 0.311 99% Percentile 3370

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3370

90% Percentile 3419   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3441   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3483   90% UPL 3370

  90% Chebyshev UPL 3498

   90% WH Approx. Gamma UPL 3417 Upper Threshold Limit Based upon IQR 3445

   90% HW Approx. Gamma UPL 3417

   90% WH Approx. Gamma UTL with   90% Coverage 3457

   90% HW Approx. Gamma UTL with   90% Coverage 3457

Benzo(b)fluoranthene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 2300 Minimum 7.741

Maximum 2370 Maximum 7.771

Second Largest 2370 Second Largest 7.771

First Quartile 2335 First Quartile 7.756

Median 2370 Median 7.771

Third Quartile 2370 Third Quartile 7.771

Mean 2350 Mean 7.762

SD 34.16 SD 0.0146

Coefficient of Variation 0.0145

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Minnesota UPL Results 98
Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2430   90% UTL with   90% Coverage 2431

   90% UPL (t) 2403   90% UPL (t) 2403

90% Percentile (z) 2394 90% Percentile (z) 2394

95% Percentile (z) 2406 95% Percentile (z) 2407

99% Percentile (z) 2429 99% Percentile (z) 2431

Gamma Distribution Test Data Distribution Test

k star 3129 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.751

MLE of Mean 2350

MLE of Standard Deviation 42.01

nu star 43802

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2370

K‐S Test Statistic 0.451 95% Percentile 2370

5% K‐S Critical Value 0.311 99% Percentile 2370

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2370

90% Percentile 2404   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2420   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2449   90% UPL 2370

  90% Chebyshev UPL 2460

   90% WH Approx. Gamma UPL 2403 Upper Threshold Limit Based upon IQR 2423

   90% HW Approx. Gamma UPL 2403

   90% WH Approx. Gamma UTL with   90% Coverage 2431

   90% HW Approx. Gamma UTL with   90% Coverage 2431

Benzo(g,h,i)perylene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4590 Minimum 8.432

Maximum 4730 Maximum 8.462

Second Largest 4730 Second Largest 8.462

First Quartile 4660 First Quartile 8.447

Median 4730 Median 8.462

Third Quartile 4730 Third Quartile 8.462

Mean 4690 Mean 8.453

SD 68.31 SD 0.0147

Coefficient of Variation 0.0146

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

Minnesota UPL Results 99
There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4849   90% UTL with   90% Coverage 4853

   90% UPL (t) 4795   90% UPL (t) 4797

90% Percentile (z) 4778 90% Percentile (z) 4779

95% Percentile (z) 4802 95% Percentile (z) 4804

99% Percentile (z) 4849 99% Percentile (z) 4852

Gamma Distribution Test Data Distribution Test

k star 3115 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.505

MLE of Mean 4690

MLE of Standard Deviation 84.03

nu star 43615

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4730

K‐S Test Statistic 0.451 95% Percentile 4730

5% K‐S Critical Value 0.311 99% Percentile 4730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4730

90% Percentile 4798   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4829   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4888   90% UPL 4730

  90% Chebyshev UPL 4909

   90% WH Approx. Gamma UPL 4796 Upper Threshold Limit Based upon IQR 4835

   90% HW Approx. Gamma UPL 4796

   90% WH Approx. Gamma UTL with   90% Coverage 4852

   90% HW Approx. Gamma UTL with   90% Coverage 4852

Benzo(k)fluoranthene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 5210 Minimum 8.558

Minnesota UPL Results 100
Maximum 5370 Maximum 8.589

Second Largest 5370 Second Largest 8.589

First Quartile 5290 First Quartile 8.573

Median 5370 Median 8.589

Third Quartile 5370 Third Quartile 8.589

Mean 5324 Mean 8.58

SD 78.07 SD 0.0148

Coefficient of Variation 0.0147

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5506   90% UTL with   90% Coverage 5510

   90% UPL (t) 5444   90% UPL (t) 5446

90% Percentile (z) 5424 90% Percentile (z) 5425

95% Percentile (z) 5453 95% Percentile (z) 5455

99% Percentile (z) 5506 99% Percentile (z) 5510

Gamma Distribution Test Data Distribution Test

k star 3074 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.732

MLE of Mean 5324

MLE of Standard Deviation 96.03

nu star 43033

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5370

K‐S Test Statistic 0.451 95% Percentile 5370

5% K‐S Critical Value 0.311 99% Percentile 5370

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5370

90% Percentile 5448   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5483   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 5550   90% UPL 5370

  90% Chebyshev UPL 5575

   90% WH Approx. Gamma UPL 5446 Upper Threshold Limit Based upon IQR 5490

   90% HW Approx. Gamma UPL 5446

Minnesota UPL Results 101
   90% WH Approx. Gamma UTL with   90% Coverage 5509

   90% HW Approx. Gamma UTL with   90% Coverage 5509

Biphenyl

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3620 Minimum 8.194

Maximum 3730 Maximum 8.224

Second Largest 3730 Second Largest 8.224

First Quartile 3675 First Quartile 8.209

Median 3730 Median 8.224

Third Quartile 3730 Third Quartile 8.224

Mean 3699 Mean 8.216

SD 53.67 SD 0.0146

Coefficient of Variation 0.0145

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3824   90% UTL with   90% Coverage 3826

   90% UPL (t) 3781   90% UPL (t) 3782

90% Percentile (z) 3767 90% Percentile (z) 3768

95% Percentile (z) 3787 95% Percentile (z) 3788

99% Percentile (z) 3823 99% Percentile (z) 3826

Gamma Distribution Test Data Distribution Test

k star 3138 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.178

MLE of Mean 3699

MLE of Standard Deviation 66.02

nu star 43939

A‐D Test Statistic 1.578 Nonparametric Statistics

Minnesota UPL Results 102
5% A‐D Critical Value 0.708 90% Percentile 3730

K‐S Test Statistic 0.451 95% Percentile 3730

5% K‐S Critical Value 0.311 99% Percentile 3730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3730

90% Percentile 3783   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3808   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3854   90% UPL 3730

  90% Chebyshev UPL 3871

   90% WH Approx. Gamma UPL 3782 Upper Threshold Limit Based upon IQR 3813

   90% HW Approx. Gamma UPL 3782

   90% WH Approx. Gamma UTL with   90% Coverage 3826

   90% HW Approx. Gamma UTL with   90% Coverage 3826

Bis(2‐ethylhexyl)phthalate

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3890 Minimum 8.266

Maximum 4010 Maximum 8.297

Second Largest 4010 Second Largest 8.297

First Quartile 3950 First Quartile 8.281

Median 4010 Median 8.297

Third Quartile 4010 Third Quartile 8.297

Mean 3976 Mean 8.288

SD 58.55 SD 0.0148

Coefficient of Variation 0.0147

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4112   90% UTL with   90% Coverage 4115

   90% UPL (t) 4066   90% UPL (t) 4067

Minnesota UPL Results 103
90% Percentile (z) 4051 90% Percentile (z) 4052

95% Percentile (z) 4072 95% Percentile (z) 4073

99% Percentile (z) 4112 99% Percentile (z) 4115

Gamma Distribution Test Data Distribution Test

k star 3047 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.305

MLE of Mean 3976

MLE of Standard Deviation 72.03

nu star 42655

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4010

K‐S Test Statistic 0.451 95% Percentile 4010

5% K‐S Critical Value 0.311 99% Percentile 4010

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4010

90% Percentile 4068   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4095   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4145   90% UPL 4010

  90% Chebyshev UPL 4164

   90% WH Approx. Gamma UPL 4067 Upper Threshold Limit Based upon IQR 4100

   90% HW Approx. Gamma UPL 4067

   90% WH Approx. Gamma UTL with   90% Coverage 4114

   90% HW Approx. Gamma UTL with   90% Coverage 4114

Chrysene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 3

Raw Statistics Log‐Transformed Statistics

Minimum 3680 Minimum 8.211

Maximum 4100 Maximum 8.319

Second Largest 4100 Second Largest 8.319

First Quartile 4040 First Quartile 8.304

Median 4100 Median 8.319

Third Quartile 4100 Third Quartile 8.319

Mean 4023 Mean 8.299

SD 157.7 SD 0.0405

Coefficient of Variation 0.0392

Skewness ‐2.268

Warning:  There are only 3 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

Minnesota UPL Results 104
It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.596 Shapiro Wilk Test Statistic 0.592

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4391   90% UTL with   90% Coverage 4419

   90% UPL (t) 4266   90% UPL (t) 4279

90% Percentile (z) 4225 90% Percentile (z) 4234

95% Percentile (z) 4282 95% Percentile (z) 4297

99% Percentile (z) 4390 99% Percentile (z) 4417

Gamma Distribution Test Data Distribution Test

k star 415.4 Data do not follow a Discernable Distribution (0.05)

Theta Star 9.685

MLE of Mean 4023

MLE of Standard Deviation 197.4

nu star 5815

A‐D Test Statistic 1.462 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4100

K‐S Test Statistic 0.415 95% Percentile 4100

5% K‐S Critical Value 0.311 99% Percentile 4100

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4100

90% Percentile 4278   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4353   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4496   90% UPL 4100

  90% Chebyshev UPL 4528

   90% WH Approx. Gamma UPL 4274 Upper Threshold Limit Based upon IQR 4190

   90% HW Approx. Gamma UPL 4275

   90% WH Approx. Gamma UTL with   90% Coverage 4409

   90% HW Approx. Gamma UTL with   90% Coverage 4411

Dibenz(a,h)anthracene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4060 Minimum 8.309

Maximum 4190 Maximum 8.34

Second Largest 4190 Second Largest 8.34

First Quartile 4125 First Quartile 8.325

Median 4190 Median 8.34

Third Quartile 4190 Third Quartile 8.34

Mean 4153 Mean 8.331

SD 63.43 SD 0.0154

Coefficient of Variation 0.0153

Skewness ‐1.23

Minnesota UPL Results 105
Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4301   90% UTL with   90% Coverage 4304

   90% UPL (t) 4250   90% UPL (t) 4252

90% Percentile (z) 4234 90% Percentile (z) 4235

95% Percentile (z) 4257 95% Percentile (z) 4259

99% Percentile (z) 4300 99% Percentile (z) 4304

Gamma Distribution Test Data Distribution Test

k star 2832 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.467

MLE of Mean 4153

MLE of Standard Deviation 78.04

nu star 39644

A‐D Test Statistic 1.576 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4190

K‐S Test Statistic 0.451 95% Percentile 4190

5% K‐S Critical Value 0.311 99% Percentile 4190

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4190

90% Percentile 4253   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4282   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4337   90% UPL 4190

  90% Chebyshev UPL 4356

   90% WH Approx. Gamma UPL 4251 Upper Threshold Limit Based upon IQR 4288

   90% HW Approx. Gamma UPL 4252

   90% WH Approx. Gamma UTL with   90% Coverage 4303

   90% HW Approx. Gamma UTL with   90% Coverage 4303

Dibenzofurans

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Minnesota UPL Results 106
Raw Statistics Log‐Transformed Statistics

Minimum 4060 Minimum 8.309

Maximum 4190 Maximum 8.34

Second Largest 4190 Second Largest 8.34

First Quartile 4125 First Quartile 8.325

Median 4190 Median 8.34

Third Quartile 4190 Third Quartile 8.34

Mean 4153 Mean 8.331

SD 63.43 SD 0.0154

Coefficient of Variation 0.0153

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4301   90% UTL with   90% Coverage 4304

   90% UPL (t) 4250   90% UPL (t) 4252

90% Percentile (z) 4234 90% Percentile (z) 4235

95% Percentile (z) 4257 95% Percentile (z) 4259

99% Percentile (z) 4300 99% Percentile (z) 4304

Gamma Distribution Test Data Distribution Test

k star 2832 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.467

MLE of Mean 4153

MLE of Standard Deviation 78.04

nu star 39644

A‐D Test Statistic 1.576 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4190

K‐S Test Statistic 0.451 95% Percentile 4190

5% K‐S Critical Value 0.311 99% Percentile 4190

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4190

90% Percentile 4253   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4282   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4337   90% UPL 4190

  90% Chebyshev UPL 4356

Minnesota UPL Results 107
   90% WH Approx. Gamma UPL 4251 Upper Threshold Limit Based upon IQR 4288

   90% HW Approx. Gamma UPL 4252

   90% WH Approx. Gamma UTL with   90% Coverage 4303

   90% HW Approx. Gamma UTL with   90% Coverage 4303

Dimethyl phthalate

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4680 Minimum 8.451

Maximum 4820 Maximum 8.481

Second Largest 4820 Second Largest 8.481

First Quartile 4750 First Quartile 8.466

Median 4820 Median 8.481

Third Quartile 4820 Third Quartile 8.481

Mean 4780 Mean 8.472

SD 68.31 SD 0.0144

Coefficient of Variation 0.0143

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4939   90% UTL with   90% Coverage 4943

   90% UPL (t) 4885   90% UPL (t) 4887

90% Percentile (z) 4868 90% Percentile (z) 4868

95% Percentile (z) 4892 95% Percentile (z) 4894

99% Percentile (z) 4939 99% Percentile (z) 4942

Gamma Distribution Test Data Distribution Test

k star 3237 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.477

MLE of Mean 4780

MLE of Standard Deviation 84.02

nu star 45313

Minnesota UPL Results 108
A‐D Test Statistic 1.579 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4820

K‐S Test Statistic 0.451 95% Percentile 4820

5% K‐S Critical Value 0.311 99% Percentile 4820

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4820

90% Percentile 4888   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4919   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4978   90% UPL 4820

  90% Chebyshev UPL 4999

   90% WH Approx. Gamma UPL 4886 Upper Threshold Limit Based upon IQR 4925

   90% HW Approx. Gamma UPL 4886

   90% WH Approx. Gamma UTL with   90% Coverage 4942

   90% HW Approx. Gamma UTL with   90% Coverage 4942

Fluoranthene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4240 Minimum 8.352

Maximum 4370 Maximum 8.383

Second Largest 4370 Second Largest 8.383

First Quartile 4305 First Quartile 8.367

Median 4370 Median 8.383

Third Quartile 4370 Third Quartile 8.383

Mean 4333 Mean 8.374

SD 63.43 SD 0.0147

Coefficient of Variation 0.0146

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

Minnesota UPL Results 109
   90% UTL with   90% Coverage 4481   90% UTL with   90% Coverage 4484

   90% UPL (t) 4430   90% UPL (t) 4432

90% Percentile (z) 4414 90% Percentile (z) 4415

95% Percentile (z) 4437 95% Percentile (z) 4439

99% Percentile (z) 4480 99% Percentile (z) 4484

Gamma Distribution Test Data Distribution Test

k star 3084 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.405

MLE of Mean 4333

MLE of Standard Deviation 78.03

nu star 43171

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4370

K‐S Test Statistic 0.451 95% Percentile 4370

5% K‐S Critical Value 0.311 99% Percentile 4370

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4370

90% Percentile 4433   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4462   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4516   90% UPL 4370

  90% Chebyshev UPL 4536

   90% WH Approx. Gamma UPL 4431 Upper Threshold Limit Based upon IQR 4468

   90% HW Approx. Gamma UPL 4432

   90% WH Approx. Gamma UTL with   90% Coverage 4483

   90% HW Approx. Gamma UTL with   90% Coverage 4483

Fluorene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4150 Minimum 8.331

Maximum 4280 Maximum 8.362

Second Largest 4280 Second Largest 8.362

First Quartile 4215 First Quartile 8.346

Median 4280 Median 8.362

Third Quartile 4280 Third Quartile 8.362

Mean 4243 Mean 8.353

SD 63.43 SD 0.0151

Coefficient of Variation 0.015

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Minnesota UPL Results 110
Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4391   90% UTL with   90% Coverage 4394

   90% UPL (t) 4340   90% UPL (t) 4342

90% Percentile (z) 4324 90% Percentile (z) 4325

95% Percentile (z) 4347 95% Percentile (z) 4349

99% Percentile (z) 4390 99% Percentile (z) 4394

Gamma Distribution Test Data Distribution Test

k star 2956 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.435

MLE of Mean 4243

MLE of Standard Deviation 78.03

nu star 41388

A‐D Test Statistic 1.577 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4280

K‐S Test Statistic 0.451 95% Percentile 4280

5% K‐S Critical Value 0.311 99% Percentile 4280

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4280

90% Percentile 4343   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4372   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4426   90% UPL 4280

  90% Chebyshev UPL 4446

   90% WH Approx. Gamma UPL 4341 Upper Threshold Limit Based upon IQR 4378

   90% HW Approx. Gamma UPL 4342

   90% WH Approx. Gamma UTL with   90% Coverage 4393

   90% HW Approx. Gamma UTL with   90% Coverage 4393

Hexachlorobenzene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4240 Minimum 8.352

Maximum 4370 Maximum 8.383

Second Largest 4370 Second Largest 8.383

First Quartile 4305 First Quartile 8.367

Median 4370 Median 8.383

Third Quartile 4370 Third Quartile 8.383

Mean 4333 Mean 8.374

SD 63.43 SD 0.0147

Coefficient of Variation 0.0146

Minnesota UPL Results 111
Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4481   90% UTL with   90% Coverage 4484

   90% UPL (t) 4430   90% UPL (t) 4432

90% Percentile (z) 4414 90% Percentile (z) 4415

95% Percentile (z) 4437 95% Percentile (z) 4439

99% Percentile (z) 4480 99% Percentile (z) 4484

Gamma Distribution Test Data Distribution Test

k star 3084 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.405

MLE of Mean 4333

MLE of Standard Deviation 78.03

nu star 43171

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4370

K‐S Test Statistic 0.451 95% Percentile 4370

5% K‐S Critical Value 0.311 99% Percentile 4370

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4370

90% Percentile 4433   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4462   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4516   90% UPL 4370

  90% Chebyshev UPL 4536

   90% WH Approx. Gamma UPL 4431 Upper Threshold Limit Based upon IQR 4468

   90% HW Approx. Gamma UPL 4432

   90% WH Approx. Gamma UTL with   90% Coverage 4483

   90% HW Approx. Gamma UTL with   90% Coverage 4483

Hexachlorobutadiene

General Statistics

Minnesota UPL Results 112
Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4860 Minimum 8.489

Maximum 5000 Maximum 8.517

Second Largest 5000 Second Largest 8.517

First Quartile 4930 First Quartile 8.503

Median 5000 Median 8.517

Third Quartile 5000 Third Quartile 8.517

Mean 4960 Mean 8.509

SD 68.31 SD 0.0139

Coefficient of Variation 0.0138

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 5119   90% UTL with   90% Coverage 5123

   90% UPL (t) 5065   90% UPL (t) 5067

90% Percentile (z) 5048 90% Percentile (z) 5048

95% Percentile (z) 5072 95% Percentile (z) 5074

99% Percentile (z) 5119 99% Percentile (z) 5122

Gamma Distribution Test Data Distribution Test

k star 3486 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.423

MLE of Mean 4960

MLE of Standard Deviation 84.01

nu star 48805

A‐D Test Statistic 1.581 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 5000

K‐S Test Statistic 0.451 95% Percentile 5000

5% K‐S Critical Value 0.311 99% Percentile 5000

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5000

90% Percentile 5068   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 5099   90% BCA Bootstrap UTL with   90% Coverage    N/A    

Minnesota UPL Results 113
99% Percentile 5158   90% UPL 5000

  90% Chebyshev UPL 5179

   90% WH Approx. Gamma UPL 5066 Upper Threshold Limit Based upon IQR 5105

   90% HW Approx. Gamma UPL 5066

   90% WH Approx. Gamma UTL with   90% Coverage 5121

   90% HW Approx. Gamma UTL with   90% Coverage 5122

Hexachlorocyclopentadiene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3000 Minimum 8.006

Maximum 3100 Maximum 8.039

Second Largest 3100 Second Largest 8.039

First Quartile 3050 First Quartile 8.023

Median 3100 Median 8.039

Third Quartile 3100 Third Quartile 8.039

Mean 3071 Mean 8.03

SD 48.8 SD 0.016

Coefficient of Variation 0.0159

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3185   90% UTL with   90% Coverage 3188

   90% UPL (t) 3147   90% UPL (t) 3148

90% Percentile (z) 3134 90% Percentile (z) 3135

95% Percentile (z) 3152 95% Percentile (z) 3153

99% Percentile (z) 3185 99% Percentile (z) 3188

Gamma Distribution Test Data Distribution Test

k star 2617 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.174

MLE of Mean 3071

Minnesota UPL Results 114
MLE of Standard Deviation 60.04

nu star 36634

A‐D Test Statistic 1.575 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3100

K‐S Test Statistic 0.451 95% Percentile 3100

5% K‐S Critical Value 0.311 99% Percentile 3100

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3100

90% Percentile 3149   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3171   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3213   90% UPL 3100

  90% Chebyshev UPL 3228

   90% WH Approx. Gamma UPL 3147 Upper Threshold Limit Based upon IQR 3175

   90% HW Approx. Gamma UPL 3147

   90% WH Approx. Gamma UTL with   90% Coverage 3187

   90% HW Approx. Gamma UTL with   90% Coverage 3187

Hexachloroethane

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 2740 Minimum 7.916

Maximum 2820 Maximum 7.944

Second Largest 2820 Second Largest 7.944

First Quartile 2780 First Quartile 7.93

Median 2820 Median 7.944

Third Quartile 2820 Third Quartile 7.944

Mean 2797 Mean 7.936

SD 39.04 SD 0.014

Coefficient of Variation 0.014

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Minnesota UPL Results 115
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2888   90% UTL with   90% Coverage 2890

   90% UPL (t) 2857   90% UPL (t) 2858

90% Percentile (z) 2847 90% Percentile (z) 2848

95% Percentile (z) 2861 95% Percentile (z) 2862

99% Percentile (z) 2888 99% Percentile (z) 2890

Gamma Distribution Test Data Distribution Test

k star 3395 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.824

MLE of Mean 2797

MLE of Standard Deviation 48.01

nu star 47529

A‐D Test Statistic 1.58 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 2820

K‐S Test Statistic 0.451 95% Percentile 2820

5% K‐S Critical Value 0.311 99% Percentile 2820

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2820

90% Percentile 2859   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 2877   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 2910   90% UPL 2820

  90% Chebyshev UPL 2922

   90% WH Approx. Gamma UPL 2858 Upper Threshold Limit Based upon IQR 2880

   90% HW Approx. Gamma UPL 2858

   90% WH Approx. Gamma UTL with   90% Coverage 2889

   90% HW Approx. Gamma UTL with   90% Coverage 2890

Indeno(1,2,3‐cd)pyrene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3620 Minimum 8.194

Maximum 3730 Maximum 8.224

Second Largest 3730 Second Largest 8.224

First Quartile 3675 First Quartile 8.209

Median 3730 Median 8.224

Third Quartile 3730 Third Quartile 8.224

Mean 3699 Mean 8.216

SD 53.67 SD 0.0146

Coefficient of Variation 0.0145

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Minnesota UPL Results 116
Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3824   90% UTL with   90% Coverage 3826

   90% UPL (t) 3781   90% UPL (t) 3782

90% Percentile (z) 3767 90% Percentile (z) 3768

95% Percentile (z) 3787 95% Percentile (z) 3788

99% Percentile (z) 3823 99% Percentile (z) 3826

Gamma Distribution Test Data Distribution Test

k star 3138 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.178

MLE of Mean 3699

MLE of Standard Deviation 66.02

nu star 43939

A‐D Test Statistic 1.578 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3730

K‐S Test Statistic 0.451 95% Percentile 3730

5% K‐S Critical Value 0.311 99% Percentile 3730

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3730

90% Percentile 3783   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3808   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3854   90% UPL 3730

  90% Chebyshev UPL 3871

   90% WH Approx. Gamma UPL 3782 Upper Threshold Limit Based upon IQR 3813

   90% HW Approx. Gamma UPL 3782

   90% WH Approx. Gamma UTL with   90% Coverage 3826

   90% HW Approx. Gamma UTL with   90% Coverage 3826

Naphthalene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4330 Minimum 8.373

Maximum 4460 Maximum 8.403

Second Largest 4460 Second Largest 8.403

First Quartile 4395 First Quartile 8.388

Median 4460 Median 8.403

Third Quartile 4460 Third Quartile 8.403

Mean 4423 Mean 8.394

Minnesota UPL Results 117
SD 63.43 SD 0.0144

Coefficient of Variation 0.0143

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4571   90% UTL with   90% Coverage 4574

   90% UPL (t) 4520   90% UPL (t) 4522

90% Percentile (z) 4504 90% Percentile (z) 4505

95% Percentile (z) 4527 95% Percentile (z) 4529

99% Percentile (z) 4570 99% Percentile (z) 4573

Gamma Distribution Test Data Distribution Test

k star 3214 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.376

MLE of Mean 4423

MLE of Standard Deviation 78.02

nu star 44991

A‐D Test Statistic 1.579 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4460

K‐S Test Statistic 0.451 95% Percentile 4460

5% K‐S Critical Value 0.311 99% Percentile 4460

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4460

90% Percentile 4523   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4552   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4606   90% UPL 4460

  90% Chebyshev UPL 4626

   90% WH Approx. Gamma UPL 4521 Upper Threshold Limit Based upon IQR 4558

   90% HW Approx. Gamma UPL 4521

   90% WH Approx. Gamma UTL with   90% Coverage 4573

   90% HW Approx. Gamma UTL with   90% Coverage 4573

Nitrobenzene

Minnesota UPL Results 118
General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3450 Minimum 8.146

Maximum 3550 Maximum 8.175

Second Largest 3550 Second Largest 8.175

First Quartile 3500 First Quartile 8.16

Median 3550 Median 8.175

Third Quartile 3550 Third Quartile 8.175

Mean 3521 Mean 8.167

SD 48.8 SD 0.0139

Coefficient of Variation 0.0139

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3635   90% UTL with   90% Coverage 3638

   90% UPL (t) 3597   90% UPL (t) 3598

90% Percentile (z) 3584 90% Percentile (z) 3585

95% Percentile (z) 3602 95% Percentile (z) 3603

99% Percentile (z) 3635 99% Percentile (z) 3637

Gamma Distribution Test Data Distribution Test

k star 3444 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.023

MLE of Mean 3521

MLE of Standard Deviation 60.01

nu star 48214

A‐D Test Statistic 1.581 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3550

K‐S Test Statistic 0.451 95% Percentile 3550

5% K‐S Critical Value 0.311 99% Percentile 3550

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3550

Minnesota UPL Results 119
90% Percentile 3599   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3621   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3663   90% UPL 3550

  90% Chebyshev UPL 3678

   90% WH Approx. Gamma UPL 3597 Upper Threshold Limit Based upon IQR 3625

   90% HW Approx. Gamma UPL 3597

   90% WH Approx. Gamma UTL with   90% Coverage 3637

   90% HW Approx. Gamma UTL with   90% Coverage 3637

Pentachlorophenol

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 3190 Minimum 8.068

Maximum 134000 Maximum 11.81

Second Largest 8970 Second Largest 9.102

First Quartile 5715 First Quartile 8.542

Median 8820 Median 9.085

Third Quartile 8955 Third Quartile 9.1

Mean 25050 Mean 9.178

SD 48114 SD 1.253

Coefficient of Variation 1.921

Skewness 2.629

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.501 Shapiro Wilk Test Statistic 0.748

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 137301   90% UTL with   90% Coverage 179905

   90% UPL (t) 99106   90% UPL (t) 66550

90% Percentile (z) 86711 90% Percentile (z) 48194

95% Percentile (z) 104191 95% Percentile (z) 75971

99% Percentile (z) 136981 99% Percentile (z) 178412

Gamma Distribution Test Data Distribution Test

k star 0.463 Data do not follow a Discernable Distribution (0.05)

Theta Star 54136

MLE of Mean 25050

Minnesota UPL Results 120
MLE of Standard Deviation 36825

nu star 6.478

A‐D Test Statistic 1.311 Nonparametric Statistics

5% A‐D Critical Value 0.743 90% Percentile 58982

K‐S Test Statistic 0.461 95% Percentile 96491

5% K‐S Critical Value 0.325 99% Percentile 126498

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 134000

90% Percentile 68847   90% Percentile Bootstrap UTL with   90% Coverage 134000

95% Percentile 98911   90% BCA Bootstrap UTL with   90% Coverage 134000

99% Percentile 173401   90% UPL 134000

  90% Chebyshev UPL 179359

   90% WH Approx. Gamma UPL 77797 Upper Threshold Limit Based upon IQR 13815

   90% HW Approx. Gamma UPL 74699

   90% WH Approx. Gamma UTL with   90% Coverage 146336

   90% HW Approx. Gamma UTL with   90% Coverage 150371

Phenanthrene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 3710 Minimum 8.219

Maximum 3820 Maximum 8.248

Second Largest 3820 Second Largest 8.248

First Quartile 3765 First Quartile 8.233

Median 3820 Median 8.248

Third Quartile 3820 Third Quartile 8.248

Mean 3789 Mean 8.24

SD 53.67 SD 0.0143

Coefficient of Variation 0.0142

Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Minnesota UPL Results 121
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 3914   90% UTL with   90% Coverage 3916

   90% UPL (t) 3871   90% UPL (t) 3872

90% Percentile (z) 3857 90% Percentile (z) 3858

95% Percentile (z) 3877 95% Percentile (z) 3878

99% Percentile (z) 3913 99% Percentile (z) 3916

Gamma Distribution Test Data Distribution Test

k star 3294 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.15

MLE of Mean 3789

MLE of Standard Deviation 66.01

nu star 46112

A‐D Test Statistic 1.58 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 3820

K‐S Test Statistic 0.451 95% Percentile 3820

5% K‐S Critical Value 0.311 99% Percentile 3820

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 3820

90% Percentile 3873   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 3898   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 3944   90% UPL 3820

  90% Chebyshev UPL 3961

   90% WH Approx. Gamma UPL 3872 Upper Threshold Limit Based upon IQR 3903

   90% HW Approx. Gamma UPL 3872

   90% WH Approx. Gamma UTL with   90% Coverage 3915

   90% HW Approx. Gamma UTL with   90% Coverage 3916

Phenol

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 4190 Minimum 8.34

Maximum 15200 Maximum 9.629

Second Largest 13900 Second Largest 9.54

First Quartile 4905 First Quartile 8.494

Median 5650 Median 8.639

Third Quartile 13850 Third Quartile 9.536

Mean 8936 Mean 8.953

SD 5062 SD 0.584

Coefficient of Variation 0.567

Skewness 0.369

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Minnesota UPL Results 122
Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.774 Shapiro Wilk Test Statistic 0.8

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 20746   90% UTL with   90% Coverage 30219

   90% UPL (t) 16728   90% UPL (t) 19001

90% Percentile (z) 15424 90% Percentile (z) 16345

95% Percentile (z) 17263 95% Percentile (z) 20212

99% Percentile (z) 20713 99% Percentile (z) 30102

Gamma Distribution Test Data Distribution Test

k star 2.154 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 4149

MLE of Mean 8936

MLE of Standard Deviation 6089

nu star 30.15

A‐D Test Statistic 0.812 Nonparametric Statistics

5% A‐D Critical Value 0.711 90% Percentile 14420

K‐S Test Statistic 0.306 95% Percentile 14810

5% K‐S Critical Value 0.313 99% Percentile 15122

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 15200

90% Percentile 17081   90% Percentile Bootstrap UTL with   90% Coverage 15200

95% Percentile 20709   90% BCA Bootstrap UTL with   90% Coverage 15200

99% Percentile 28720   90% UPL 15200

  90% Chebyshev UPL 25172

   90% WH Approx. Gamma UPL 17939 Upper Threshold Limit Based upon IQR 27268

   90% HW Approx. Gamma UPL 18164

   90% WH Approx. Gamma UTL with   90% Coverage 25190

   90% HW Approx. Gamma UTL with   90% Coverage 26147

Pyrene

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 4060 Minimum 8.309

Maximum 4190 Maximum 8.34

Second Largest 4190 Second Largest 8.34

First Quartile 4125 First Quartile 8.325

Median 4190 Median 8.34

Third Quartile 4190 Third Quartile 8.34

Mean 4153 Mean 8.331

SD 63.43 SD 0.0154

Coefficient of Variation 0.0153

Minnesota UPL Results 123
Skewness ‐1.23

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.601 Shapiro Wilk Test Statistic 0.601

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 4301   90% UTL with   90% Coverage 4304

   90% UPL (t) 4250   90% UPL (t) 4252

90% Percentile (z) 4234 90% Percentile (z) 4235

95% Percentile (z) 4257 95% Percentile (z) 4259

99% Percentile (z) 4300 99% Percentile (z) 4304

Gamma Distribution Test Data Distribution Test

k star 2832 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.467

MLE of Mean 4153

MLE of Standard Deviation 78.04

nu star 39644

A‐D Test Statistic 1.576 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 4190

K‐S Test Statistic 0.451 95% Percentile 4190

5% K‐S Critical Value 0.311 99% Percentile 4190

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 4190

90% Percentile 4253   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 4282   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 4337   90% UPL 4190

  90% Chebyshev UPL 4356

   90% WH Approx. Gamma UPL 4251 Upper Threshold Limit Based upon IQR 4288

   90% HW Approx. Gamma UPL 4252

   90% WH Approx. Gamma UTL with   90% Coverage 4303

   90% HW Approx. Gamma UTL with   90% Coverage 4303

Total Metals

General Statistics

Minnesota UPL Results 124
Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 75.18 Minimum 4.32

Maximum 295.9 Maximum 5.69

Second Largest 281.2 Second Largest 5.639

First Quartile 86.69 First Quartile 4.462

Median 92.47 Median 4.527

Third Quartile 193.8 Third Quartile 5.153

Mean 146.4 Mean 4.824

SD 97.68 SD 0.584

Coefficient of Variation 0.667

Skewness 1.2

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.695 Shapiro Wilk Test Statistic 0.753

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 374.3   90% UTL with   90% Coverage 485.6

   90% UPL (t) 296.7   90% UPL (t) 305.6

90% Percentile (z) 271.5 90% Percentile (z) 262.9

95% Percentile (z) 307 95% Percentile (z) 325

99% Percentile (z) 373.6 99% Percentile (z) 483.7

Gamma Distribution Test Data Distribution Test

k star 1.947 Data do not follow a Discernable Distribution (0.05)

Theta Star 75.18

MLE of Mean 146.4

MLE of Standard Deviation 104.9

nu star 27.26

A‐D Test Statistic 1.037 Nonparametric Statistics

5% A‐D Critical Value 0.712 90% Percentile 287.1

K‐S Test Statistic 0.353 95% Percentile 291.5

5% K‐S Critical Value 0.314 99% Percentile 295.1

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 295.9

90% Percentile 286.5   90% Percentile Bootstrap UTL with   90% Coverage 295.9

95% Percentile 350.1   90% BCA Bootstrap UTL with   90% Coverage 295.9

99% Percentile 491.6   90% UPL 295.9

  90% Chebyshev UPL 459.6

Minnesota UPL Results 125
   90% WH Approx. Gamma UPL 301.4 Upper Threshold Limit Based upon IQR 354.4

   90% HW Approx. Gamma UPL 302.2

   90% WH Approx. Gamma UTL with   90% Coverage 429.2

   90% HW Approx. Gamma UTL with   90% Coverage 440.4

Total Halogens

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 101 Minimum 4.615

Maximum 161 Maximum 5.081

Second Largest 142 Second Largest 4.956

First Quartile 102 First Quartile 4.625

Median 125 Median 4.828

Third Quartile 141.5 Third Quartile 4.952

Mean 124.9 Mean 4.811

SD 24.07 SD 0.192

Coefficient of Variation 0.193

Skewness 0.318

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.87 Shapiro Wilk Test Statistic 0.861

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 181   90% UTL with   90% Coverage 192.3

   90% UPL (t) 161.9   90% UPL (t) 165.1

90% Percentile (z) 155.7 90% Percentile (z) 157.2

95% Percentile (z) 164.4 95% Percentile (z) 168.5

99% Percentile (z) 180.8 99% Percentile (z) 192.1

Gamma Distribution Test Data Distribution Test

k star 18.24 Data appear Normal at 5% Significance Level

Theta Star 6.846

MLE of Mean 124.9

MLE of Standard Deviation 29.24

nu star 255.3

A‐D Test Statistic 0.535 Nonparametric Statistics

Minnesota UPL Results 126
5% A‐D Critical Value 0.707 90% Percentile 149.6

K‐S Test Statistic 0.28 95% Percentile 155.3

5% K‐S Critical Value 0.311 99% Percentile 159.9

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 161

90% Percentile 163.5   90% Percentile Bootstrap UTL with   90% Coverage 161

95% Percentile 176.5   90% BCA Bootstrap UTL with   90% Coverage 161

99% Percentile 202.7   90% UPL 161

  90% Chebyshev UPL 202

   90% WH Approx. Gamma UPL 163.9 Upper Threshold Limit Based upon IQR 200.8

   90% HW Approx. Gamma UPL 164.2

   90% WH Approx. Gamma UTL with   90% Coverage 187.7

   90% HW Approx. Gamma UTL with   90% Coverage 188.8

Total VOC

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 697.5 Minimum 6.547

Maximum 827.7 Maximum 6.719

Second Largest 813.7 Second Largest 6.702

First Quartile 736.8 First Quartile 6.602

Median 780.2 Median 6.66

Third Quartile 801.1 Third Quartile 6.686

Mean 768.7 Mean 6.643

SD 48.78 SD 0.0643

Coefficient of Variation 0.0635

Skewness ‐0.465

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.936 Shapiro Wilk Test Statistic 0.93

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 882.5   90% UTL with   90% Coverage 891.5

   90% UPL (t) 843.8   90% UPL (t) 847.2

90% Percentile (z) 831.2 90% Percentile (z) 833.3

95% Percentile (z) 849 95% Percentile (z) 853

Minnesota UPL Results 127
99% Percentile (z) 882.2 99% Percentile (z) 891.1

Gamma Distribution Test Data Distribution Test

k star 163 Data appear Normal at 5% Significance Level

Theta Star 4.717

MLE of Mean 768.7

MLE of Standard Deviation 60.22

nu star 2282

A‐D Test Statistic 0.306 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 819.3

K‐S Test Statistic 0.178 95% Percentile 823.5

5% K‐S Critical Value 0.311 99% Percentile 826.9

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 827.7

90% Percentile 846.8   90% Percentile Bootstrap UTL with   90% Coverage 827.7

95% Percentile 870.4   90% BCA Bootstrap UTL with   90% Coverage 827.7

99% Percentile 915.7   90% UPL 827.7

  90% Chebyshev UPL 925.2

   90% WH Approx. Gamma UPL 846 Upper Threshold Limit Based upon IQR 897.5

   90% HW Approx. Gamma UPL 846.3

   90% WH Approx. Gamma UTL with   90% Coverage 888.3

   90% HW Approx. Gamma UTL with   90% Coverage 889.1

Total SVOC

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 160490 Minimum 11.99

Maximum 288010 Maximum 12.57

Second Largest 177250 Second Largest 12.09

First Quartile 164095 First Quartile 12.01

Median 170700 Median 12.05

Third Quartile 176490 Third Quartile 12.08

Mean 185767 Mean 12.11

SD 45561 SD 0.206

Coefficient of Variation 0.245

Skewness 2.531

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Minnesota UPL Results 128
Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.589 Shapiro Wilk Test Statistic 0.63

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 292060   90% UTL with   90% Coverage 294382

   90% UPL (t) 255892   90% UPL (t) 249949

90% Percentile (z) 244155 90% Percentile (z) 237024

95% Percentile (z) 260708 95% Percentile (z) 255454

99% Percentile (z) 291757 99% Percentile (z) 293978

Gamma Distribution Test Data Distribution Test

k star 14.14 Data do not follow a Discernable Distribution (0.05)

Theta Star 13135

MLE of Mean 185767

MLE of Standard Deviation 49397

nu star 198

A‐D Test Statistic 1.339 Nonparametric Statistics

5% A‐D Critical Value 0.707 90% Percentile 221554

K‐S Test Statistic 0.422 95% Percentile 254782

5% K‐S Critical Value 0.311 99% Percentile 281364

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 288010

90% Percentile 251214   90% Percentile Bootstrap UTL with   90% Coverage 288010

95% Percentile 273774   90% BCA Bootstrap UTL with   90% Coverage 288010

99% Percentile 319530   90% UPL 288010

  90% Chebyshev UPL 331886

   90% WH Approx. Gamma UPL 252006 Upper Threshold Limit Based upon IQR 195083

   90% HW Approx. Gamma UPL 251498

   90% WH Approx. Gamma UTL with   90% Coverage 293436

   90% HW Approx. Gamma UTL with   90% Coverage 293654

Minnesota UPL Results 129
MDL

Components as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free

‐‐

‐‐

‐‐ 7600 7620 7310 7140

Metals (mg/kg)

0.08

0.12

0.008

0.007

0.02

0.04

0.13

0.009

0.003

0.04

0.27

Total Metals (mg/kg) ‐‐

Formaldehyde (g/kg)

420

Ions

40

6

Total Halogens (mg/kg) ‐‐

* All 90% UPL Results reported as Normal MRL = Method Reporting Limit

** 90% UPL Result reported as Lognormal MDL = Method Detection Limit = Nondetect; Reported as MDL

*** 90% UPL Result Non‐Parametric HAP = Hazardous Air Pollutant

‐‐ = Non‐Detect OH = Organic Halogen

n.d. = Only 1 Distinct Value, therefore no variance. N = Nitrogenated

Wash

1120.0 797.0 697.0 1340.0

Fluorine (mg/kg) ‐‐ ‐‐ 37

Selenium  (HAP) ‐‐ ‐‐ 0.6

Formaldehyde

Chlorine (mg/kg) 1120 797 660

‐‐

1340

49000 130000 46000 46000

10.6 5.5 12.2

‐‐

121.6 96.1 114.2 97.5

Nickel  (HAP) 2.65 1.26 2.93

Lead  (HAP) 26

2.16

Mercury  (HAP) 0.143 0.0188 0.0778 0.0284

Manganese  (HAP) 54.6 62.6 79.3 69.4

Cobalt  (HAP) 0.83 0.77 1.37 1.34

5.51

0.33

Chromium  (HAP) 12.3 10.2 10.8

Cadmium  (HAP) 0.26 0.27 0.31

Beryllium  (HAP) 0.03 0.03 0.17 0.08

4.2 2.9

Arsenic  (HAP) 8.2 6.8 8.9 3.6

Antimony  (HAP) 16.6 3.6

Sulfur (wt%) 0.455 0.516 0.608 0.625

0.76

Heating Value (BTU/lb)

Nitrogen (wt%) 0.77 1.26 0.7

21‐Mar 22‐Mar 23‐Mar 26‐Mar

Washington C&D Summary Table 130
Non‐

Detect Average

as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free as received Moist. Free

0 0.63

0 0.49

6820 7170 7920 6460 6770 7900 0 7271.00

0 4.47

0 10.42

0 0.088

0 0.31

0 16.27

0 1.16

0 10.60

0 74.66

0 0.06

0 3.47

7 0.60

‐‐ 121.68

0 61100.00

0 908.40

6 43.25

‐‐ 925.70

ington C&D SUMMARY

0.67

3.8

56.3

0.0367

1.29

‐‐

0.0632

4.18

516

47

35000

76.1

0.0733

2.74

‐‐

121.9

62000

0.63

7

90.5

0.61

7.4

34.3

1.58

13.2

127

0.27

0.136

42

1530 179 597

‐‐

2007.0 1530.0 179.0

29000

563.0 639.0 385.0

1960 385

44000

47 ‐‐ ‐‐

60000

105.0

‐‐

110000

210.5

11.6 7.8 8.3

0.6 0.6 ‐‐

167.7 106.1

0.0468 0.0614

12.2

0.051

78.3 65.5 63.1

2.78 2.49

7.2

2.4 1.8

6.86

0.6

6.3

1.63 1.18 1.45 0.78

0.26

46 14.4 15.1

0.51

0.07

13.2

0.11 0.04 0.13 0.05

14.3

0.34

11.6 5.1

0.32

3.5

26.2

0.17

0.33

1.7

0.18

0.486 0.394 0.731 0.355

28‐Mar 29‐Mar 30‐Mar 3‐Apr

0.55 0.39 0.42 0.55

27‐Mar 2‐Apr

Washington C&D Summary Table 131
*all results reported as moisture free

*all results pooled from all 7 samples

Standard

Deviation Low High

0.28 0.27 1.26 1.03

0.17 0.14 0.731 0.738

493.05 6820 7900 7986

4.64 0.60 16.6 11.28**

6.54 3.60 26.2 19.91

0.054 0.030 0.17 0.167

0.09 0.18 0.51 0.435

13.26 5.51 46 34.56**

0.37 0.67 1.63 1.69

6.20 3.8 26.0 20.05**

21.49 54.6 127 104.4**

0.03 0.019 0.143 0.110

3.18 1.26 12.2 6.971**

0.00 0.60 0.6 n.d.

39.3 76.11 210.52 178.7

32908.80 29000 130000 108359**

563.16 179 1960 1725.0

4.79 37 47 n.d.

565.32 179.00 2007 1746.0

Range 90% UPL

Results*

Washington C&D Summary Table 132
Nitrogen (wt%) Sulfur (wt%) Heating Value (BTU/lb) Antimony  (HAP)Arsenic  (HAP) Beryllium  (HAP) Cadmium  (HAPChromium  (HAP) Cobalt  (HAP)

0.77 0.455 7600 16.6 8.2 0.03 0.26 12.3 0.83

1.26 0.516 7620 3.6 6.8 0.03 0.27 10.2 0.77

0.7 0.608 7310 4.2 8.9 0.17 0.31 10.8 1.37

0.76 0.625 7140 2.9 3.6 0.08 0.33 5.51 1.34

0.55 0.486 6820 2.4 14.3 0.11 0.51 46 1.63

0.39 0.394 7170 1.8 11.6 0.04 0.34 14.4 1.18

0.27 0.136 7920 0.6 6.3 0.07 0.18 6.86 0.67

0.42 0.731 6460 3.5 26.2 0.17 0.33 34.3 1.58

0.63 0.61 6770 7.4 5.1 0.13 0.32 7.2 1.45

0.55 0.355 7900 1.7 13.2 0.05 0.26 15.1 0.78

Washington ProUCL Entry 133
Lead  (HAP) Manganese  (HAP) Mercury  (HAP) Nickel  (HAP) Selenium  (HAP)Formaldehyde Chlorine (mg/kg) Fluorine (mg/kg) Total Metals (Total Halogens (mg/kg)

26 54.6 0.143 2.65 49000 1120 121.613 1120

10.6 62.6 0.0188 1.26 130000 797 96.1488 797

5.5 79.3 0.0778 2.93 0.6 46000 660 37 114.1578 697

12.2 69.4 0.0284 2.16 46000 1340 97.5484 1340

11.6 78.3 0.051 12.2 0.6 29000 1960 47 167.701 2007

7.8 65.5 0.0468 2.78 0.6 60000 1530 106.0868 1530

3.8 56.3 0.0367 1.29 35000 179 76.1067 179

13.2 127 0.0632 4.18 44000 516 47 210.5232 563

7 90.5 0.0733 2.74 62000 597 42 121.9133 639

8.3 63.1 0.0614 2.49 110000 385 105.0414 385

Washington ProUCL Entry 134
Nitrogen

General Statistics

Total Number of Observations 10 Number of Distinct Observations 9

Raw Statistics Log‐Transformed Statistics

Minimum 0.27 Minimum ‐1.309

Maximum 1.26 Maximum 0.231

Second Largest 0.77 Second Largest ‐0.261

First Quartile 0.453 First Quartile ‐0.8

Median 0.59 Median ‐0.53

Third Quartile 0.745 Third Quartile ‐0.295

Mean 0.63 Mean ‐0.544

SD 0.275 SD 0.428

Coefficient of Variation 0.437

Skewness 1.228

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.909 Shapiro Wilk Test Statistic 0.978

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.199   90% UTL with   90% Coverage 1.406

   90% UPL (t) 1.029   90% UPL (t) 1.08

90% Percentile (z) 0.983 90% Percentile (z) 1.005

95% Percentile (z) 1.083 95% Percentile (z) 1.174

99% Percentile (z) 1.271 99% Percentile (z) 1.572

Gamma Distribution Test Data Distribution Test

k star 4.463 Data appear Normal at 5% Significance Level

Theta Star 0.141

MLE of Mean 0.63

MLE of Standard Deviation 0.298

nu star 89.26

A‐D Test Statistic 0.222 Nonparametric Statistics

5% A‐D Critical Value 0.728 90% Percentile 0.819

K‐S Test Statistic 0.157 95% Percentile 1.04

5% K‐S Critical Value 0.267 99% Percentile 1.216

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.26

90% Percentile 1.03   90% Percentile Bootstrap UTL with   90% Coverage 1.26

95% Percentile 1.187   90% BCA Bootstrap UTL with   90% Coverage 1.26

99% Percentile 1.521   90% UPL 1.211

  90% Chebyshev UPL 1.496

   90% WH Approx. Gamma UPL 1.049 Upper Threshold Limit Based upon IQR 1.184

   90% HW Approx. Gamma UPL 1.055

   90% WH Approx. Gamma UTL with   90% Coverage 1.296

   90% HW Approx. Gamma UTL with   90% Coverage 1.317

Sulfur

Washington UPL Results 135
General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 0.136 Minimum ‐1.995

Maximum 0.731 Maximum ‐0.313

Second Largest 0.625 Second Largest ‐0.47

First Quartile 0.409 First Quartile ‐0.895

Median 0.501 Median ‐0.692

Third Quartile 0.61 Third Quartile ‐0.495

Mean 0.492 Mean ‐0.791

SD 0.17 SD 0.478

Coefficient of Variation 0.345

Skewness ‐0.828

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.951 Shapiro Wilk Test Statistic 0.8

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.842   90% UTL with   90% Coverage 1.217

   90% UPL (t) 0.738   90% UPL (t) 0.907

90% Percentile (z) 0.709 90% Percentile (z) 0.837

95% Percentile (z) 0.771 95% Percentile (z) 0.995

99% Percentile (z) 0.886 99% Percentile (z) 1.379

Gamma Distribution Test Data Distribution Test

k star 4.516 Data appear Normal at 5% Significance Level

Theta Star 0.109

MLE of Mean 0.492

MLE of Standard Deviation 0.231

nu star 90.33

A‐D Test Statistic 0.567 Nonparametric Statistics

5% A‐D Critical Value 0.728 90% Percentile 0.636

K‐S Test Statistic 0.176 95% Percentile 0.683

5% K‐S Critical Value 0.267 99% Percentile 0.721

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.731

90% Percentile 0.801   90% Percentile Bootstrap UTL with   90% Coverage 0.731

95% Percentile 0.923   90% BCA Bootstrap UTL with   90% Coverage 0.731

99% Percentile 1.182   90% UPL 0.72

  90% Chebyshev UPL 1.026

   90% WH Approx. Gamma UPL 0.818 Upper Threshold Limit Based upon IQR 0.91

   90% HW Approx. Gamma UPL 0.835

   90% WH Approx. Gamma UTL with   90% Coverage 1.008

   90% HW Approx. Gamma UTL with   90% Coverage 1.046

Heating Value

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Washington UPL Results 136
Raw Statistics Log‐Transformed Statistics

Minimum 6460 Minimum 8.773

Maximum 7920 Maximum 8.977

Second Largest 7900 Second Largest 8.975

First Quartile 6900 First Quartile 8.839

Median 7240 Median 8.887

Third Quartile 7615 Third Quartile 8.938

Mean 7271 Mean 8.89

SD 493.1 SD 0.0683

Coefficient of Variation 0.0678

Skewness ‐0.178

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.952 Shapiro Wilk Test Statistic 0.95

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 8290   90% UTL with   90% Coverage 8356

   90% UPL (t) 7986   90% UPL (t) 8012

90% Percentile (z) 7903 90% Percentile (z) 7920

95% Percentile (z) 8082 95% Percentile (z) 8119

99% Percentile (z) 8418 99% Percentile (z) 8506

Gamma Distribution Test Data Distribution Test

k star 167.6 Data appear Normal at 5% Significance Level

Theta Star 43.39

MLE of Mean 7271

MLE of Standard Deviation 561.7

nu star 3352

A‐D Test Statistic 0.254 Nonparametric Statistics

5% A‐D Critical Value 0.724 90% Percentile 7902

K‐S Test Statistic 0.162 95% Percentile 7911

5% K‐S Critical Value 0.266 99% Percentile 7918

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7920

90% Percentile 7999   90% Percentile Bootstrap UTL with   90% Coverage 7920

95% Percentile 8219   90% BCA Bootstrap UTL with   90% Coverage 7920

99% Percentile 8641   90% UPL 7918

  90% Chebyshev UPL 8822

   90% WH Approx. Gamma UPL 8003 Upper Threshold Limit Based upon IQR 8688

   90% HW Approx. Gamma UPL 8005

   90% WH Approx. Gamma UTL with   90% Coverage 8332

   90% HW Approx. Gamma UTL with   90% Coverage 8338

Antimony

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 0.6 Minimum ‐0.511

Washington UPL Results 137
Maximum 16.6 Maximum 2.809

Second Largest 7.4 Second Largest 2.001

First Quartile 1.95 First Quartile 0.66

Median 3.2 Median 1.159

Third Quartile 4.05 Third Quartile 1.397

Mean 4.47 Mean 1.133

SD 4.643 SD 0.89

Coefficient of Variation 1.039

Skewness 2.355

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.711 Shapiro Wilk Test Statistic 0.969

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 14.06   90% UTL with   90% Coverage 19.51

   90% UPL (t) 11.2   90% UPL (t) 11.28

90% Percentile (z) 10.42 90% Percentile (z) 9.709

95% Percentile (z) 12.11 95% Percentile (z) 13.41

99% Percentile (z) 15.27 99% Percentile (z) 24.6

Gamma Distribution Test Data Distribution Test

k star 1.128 Data appear Gamma Distributed at 5% Significance Level

Theta Star 3.962

MLE of Mean 4.47

MLE of Standard Deviation 4.209

nu star 22.56

A‐D Test Statistic 0.427 Nonparametric Statistics

5% A‐D Critical Value 0.739 90% Percentile 8.32

K‐S Test Statistic 0.221 95% Percentile 12.46

5% K‐S Critical Value 0.271 99% Percentile 15.77

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 16.6

90% Percentile 9.991   90% Percentile Bootstrap UTL with   90% Coverage 16.6

95% Percentile 12.84   90% BCA Bootstrap UTL with   90% Coverage 16.6

99% Percentile 19.38   90% UPL 15.68

  90% Chebyshev UPL 19.08

   90% WH Approx. Gamma UPL 10.56 Upper Threshold Limit Based upon IQR 7.2

   90% HW Approx. Gamma UPL 10.62

   90% WH Approx. Gamma UTL with   90% Coverage 15.27

   90% HW Approx. Gamma UTL with   90% Coverage 15.85

Arsenic

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 3.6 Minimum 1.281

Maximum 26.2 Maximum 3.266

Second Largest 14.3 Second Largest 2.66

First Quartile 6.425 First Quartile 1.86

Washington UPL Results 138
Median 8.55 Median 2.145

Third Quartile 12.8 Third Quartile 2.548

Mean 10.42 Mean 2.192

SD 6.543 SD 0.572

Coefficient of Variation 0.628

Skewness 1.691

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.849 Shapiro Wilk Test Statistic 0.988

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 23.94   90% UTL with   90% Coverage 29.17

   90% UPL (t) 19.91   90% UPL (t) 20.51

90% Percentile (z) 18.81 90% Percentile (z) 18.62

95% Percentile (z) 21.18 95% Percentile (z) 22.92

99% Percentile (z) 25.64 99% Percentile (z) 33.85

Gamma Distribution Test Data Distribution Test

k star 2.476 Data appear Normal at 5% Significance Level

Theta Star 4.208

MLE of Mean 10.42

MLE of Standard Deviation 6.622

nu star 49.53

A‐D Test Statistic 0.223 Nonparametric Statistics

5% A‐D Critical Value 0.731 90% Percentile 15.49

K‐S Test Statistic 0.141 95% Percentile 20.85

5% K‐S Critical Value 0.268 99% Percentile 25.13

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 26.2

90% Percentile 19.29   90% Percentile Bootstrap UTL with   90% Coverage 26.2

95% Percentile 23.14   90% BCA Bootstrap UTL with   90% Coverage 26.2

99% Percentile 31.56   90% UPL 25.01

  90% Chebyshev UPL 31.01

   90% WH Approx. Gamma UPL 19.92 Upper Threshold Limit Based upon IQR 22.36

   90% HW Approx. Gamma UPL 20.01

   90% WH Approx. Gamma UTL with   90% Coverage 26.07

   90% HW Approx. Gamma UTL with   90% Coverage 26.63

Beryllium

General Statistics

Total Number of Observations 10 Number of Distinct Observations 8

Raw Statistics Log‐Transformed Statistics

Minimum 0.03 Minimum ‐3.507

Maximum 0.17 Maximum ‐1.772

Second Largest 0.17 Second Largest ‐1.772

First Quartile 0.0425 First Quartile ‐3.163

Median 0.075 Median ‐2.592

Third Quartile 0.125 Third Quartile ‐2.082

Mean 0.088 Mean ‐2.62

Washington UPL Results 139
SD 0.0543 SD 0.669

Coefficient of Variation 0.617

Skewness 0.542

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.886 Shapiro Wilk Test Statistic 0.916

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.2   90% UTL with   90% Coverage 0.29

   90% UPL (t) 0.167   90% UPL (t) 0.192

90% Percentile (z) 0.158 90% Percentile (z) 0.172

95% Percentile (z) 0.177 95% Percentile (z) 0.219

99% Percentile (z) 0.214 99% Percentile (z) 0.345

Gamma Distribution Test Data Distribution Test

k star 2.018 Data appear Normal at 5% Significance Level

Theta Star 0.0436

MLE of Mean 0.088

MLE of Standard Deviation 0.062

nu star 40.35

A‐D Test Statistic 0.342 Nonparametric Statistics

5% A‐D Critical Value 0.733 90% Percentile 0.17

K‐S Test Statistic 0.143 95% Percentile 0.17

5% K‐S Critical Value 0.269 99% Percentile 0.17

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.17

90% Percentile 0.171   90% Percentile Bootstrap UTL with   90% Coverage 0.17

95% Percentile 0.208   90% BCA Bootstrap UTL with   90% Coverage 0.17

99% Percentile 0.291   90% UPL 0.17

  90% Chebyshev UPL 0.259

   90% WH Approx. Gamma UPL 0.178 Upper Threshold Limit Based upon IQR 0.249

   90% HW Approx. Gamma UPL 0.181

   90% WH Approx. Gamma UTL with   90% Coverage 0.239

   90% HW Approx. Gamma UTL with   90% Coverage 0.248

Camium

General Statistics

Total Number of Observations 10 Number of Distinct Observations 8

Raw Statistics Log‐Transformed Statistics

Minimum 0.18 Minimum ‐1.715

Maximum 0.51 Maximum ‐0.673

Second Largest 0.34 Second Largest ‐1.079

First Quartile 0.263 First Quartile ‐1.338

Median 0.315 Median ‐1.155

Third Quartile 0.33 Third Quartile ‐1.109

Mean 0.311 Mean ‐1.2

SD 0.0852 SD 0.265

Coefficient of Variation 0.274

Washington UPL Results 140
Skewness 1.2

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.871 Shapiro Wilk Test Statistic 0.919

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.487   90% UTL with   90% Coverage 0.521

   90% UPL (t) 0.435   90% UPL (t) 0.443

90% Percentile (z) 0.42 90% Percentile (z) 0.423

95% Percentile (z) 0.451 95% Percentile (z) 0.466

99% Percentile (z) 0.509 99% Percentile (z) 0.558

Gamma Distribution Test Data Distribution Test

k star 11.16 Data appear Normal at 5% Significance Level

Theta Star 0.0279

MLE of Mean 0.311

MLE of Standard Deviation 0.0931

nu star 223.2

A‐D Test Statistic 0.509 Nonparametric Statistics

5% A‐D Critical Value 0.725 90% Percentile 0.357

K‐S Test Statistic 0.229 95% Percentile 0.434

5% K‐S Critical Value 0.266 99% Percentile 0.495

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.51

90% Percentile 0.435   90% Percentile Bootstrap UTL with   90% Coverage 0.51

95% Percentile 0.478   90% BCA Bootstrap UTL with   90% Coverage 0.51

99% Percentile 0.567   90% UPL 0.493

  90% Chebyshev UPL 0.579

   90% WH Approx. Gamma UPL 0.438 Upper Threshold Limit Based upon IQR 0.431

   90% HW Approx. Gamma UPL 0.439

   90% WH Approx. Gamma UTL with   90% Coverage 0.505

   90% HW Approx. Gamma UTL with   90% Coverage 0.508

Chromium

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 5.51 Minimum 1.707

Maximum 46 Maximum 3.829

Second Largest 34.3 Second Largest 3.535

First Quartile 7.95 First Quartile 2.061

Median 11.55 Median 2.445

Third Quartile 14.93 Third Quartile 2.703

Mean 16.27 Mean 2.556

SD 13.26 SD 0.68

Coefficient of Variation 0.815

Skewness 1.719

Washington UPL Results 141
Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.753 Shapiro Wilk Test Statistic 0.917

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 43.67   90% UTL with   90% Coverage 52.52

   90% UPL (t) 35.5   90% UPL (t) 34.56

90% Percentile (z) 33.26 90% Percentile (z) 30.81

95% Percentile (z) 38.08 95% Percentile (z) 39.44

99% Percentile (z) 47.12 99% Percentile (z) 62.69

Gamma Distribution Test Data Distribution Test

k star 1.677 Data appear Gamma Distributed at 5% Significance Level

Theta Star 9.699

MLE of Mean 16.27

MLE of Standard Deviation 12.56

nu star 33.55

A‐D Test Statistic 0.633 Nonparametric Statistics

5% A‐D Critical Value 0.735 90% Percentile 35.47

K‐S Test Statistic 0.256 95% Percentile 40.74

5% K‐S Critical Value 0.269 99% Percentile 44.95

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 46

90% Percentile 32.99   90% Percentile Bootstrap UTL with   90% Coverage 46

95% Percentile 40.84   90% BCA Bootstrap UTL with   90% Coverage 46

99% Percentile 58.42   90% UPL 44.83

  90% Chebyshev UPL 58

   90% WH Approx. Gamma UPL 34.42 Upper Threshold Limit Based upon IQR 25.39

   90% HW Approx. Gamma UPL 34.39

   90% WH Approx. Gamma UTL with   90% Coverage 47.2

   90% HW Approx. Gamma UTL with   90% Coverage 48.15

Cobalt

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 0.67 Minimum ‐0.4

Maximum 1.63 Maximum 0.489

Second Largest 1.58 Second Largest 0.457

First Quartile 0.793 First Quartile ‐0.233

Median 1.26 Median 0.229

Third Quartile 1.43 Third Quartile 0.357

Mean 1.16 Mean 0.0994

SD 0.366 SD 0.337

Coefficient of Variation 0.315

Skewness ‐0.143

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.887 Shapiro Wilk Test Statistic 0.873

Washington UPL Results 142
Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.916   90% UTL with   90% Coverage 2.218

   90% UPL (t) 1.69   90% UPL (t) 1.802

90% Percentile (z) 1.629 90% Percentile (z) 1.702

95% Percentile (z) 1.762 95% Percentile (z) 1.924

99% Percentile (z) 2.011 99% Percentile (z) 2.421

Gamma Distribution Test Data Distribution Test

k star 7.32 Data appear Normal at 5% Significance Level

Theta Star 0.158

MLE of Mean 1.16

MLE of Standard Deviation 0.429

nu star 146.4

A‐D Test Statistic 0.617 Nonparametric Statistics

5% A‐D Critical Value 0.725 90% Percentile 1.585

K‐S Test Statistic 0.22 95% Percentile 1.608

5% K‐S Critical Value 0.267 99% Percentile 1.626

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.63

90% Percentile 1.732   90% Percentile Bootstrap UTL with   90% Coverage 1.63

95% Percentile 1.943   90% BCA Bootstrap UTL with   90% Coverage 1.63

99% Percentile 2.382   90% UPL 1.625

  90% Chebyshev UPL 2.311

   90% WH Approx. Gamma UPL 1.754 Upper Threshold Limit Based upon IQR 2.386

   90% HW Approx. Gamma UPL 1.765

   90% WH Approx. Gamma UTL with   90% Coverage 2.081

   90% HW Approx. Gamma UTL with   90% Coverage 2.111

Lead

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 3.8 Minimum 1.335

Maximum 26 Maximum 3.258

Second Largest 13.2 Second Largest 2.58

First Quartile 7.2 First Quartile 1.973

Median 9.45 Median 2.239

Third Quartile 12.05 Third Quartile 2.489

Mean 10.6 Mean 2.231

SD 6.199 SD 0.529

Coefficient of Variation 0.585

Skewness 1.835

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.83 Shapiro Wilk Test Statistic 0.977

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Washington UPL Results 143
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 23.41   90% UTL with   90% Coverage 27.78

   90% UPL (t) 19.59   90% UPL (t) 20.05

90% Percentile (z) 18.54 90% Percentile (z) 18.34

95% Percentile (z) 20.8 95% Percentile (z) 22.23

99% Percentile (z) 25.02 99% Percentile (z) 31.88

Gamma Distribution Test Data Distribution Test

k star 2.868 Data appear Gamma Distributed at 5% Significance Level

Theta Star 3.695

MLE of Mean 10.6

MLE of Standard Deviation 6.259

nu star 57.37

A‐D Test Statistic 0.278 Nonparametric Statistics

5% A‐D Critical Value 0.729 90% Percentile 14.48

K‐S Test Statistic 0.168 95% Percentile 20.24

5% K‐S Critical Value 0.268 99% Percentile 24.85

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 26

90% Percentile 18.99   90% Percentile Bootstrap UTL with   90% Coverage 26

95% Percentile 22.53   90% BCA Bootstrap UTL with   90% Coverage 26

99% Percentile 30.24   90% UPL 24.72

  90% Chebyshev UPL 30.1

   90% WH Approx. Gamma UPL 19.52 Upper Threshold Limit Based upon IQR 19.33

   90% HW Approx. Gamma UPL 19.6

   90% WH Approx. Gamma UTL with   90% Coverage 25.14

   90% HW Approx. Gamma UTL with   90% Coverage 25.62

Manganese

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 54.6 Minimum 4

Maximum 127 Maximum 4.844

Second Largest 90.5 Second Largest 4.505

First Quartile 62.73 First Quartile 4.139

Median 67.45 Median 4.211

Third Quartile 79.05 Third Quartile 4.37

Mean 74.66 Mean 4.282

SD 21.49 SD 0.253

Coefficient of Variation 0.288

Skewness 1.806

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.821 Shapiro Wilk Test Statistic 0.902

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 119.1   90% UTL with   90% Coverage 122

   90% UPL (t) 105.8   90% UPL (t) 104.4

Washington UPL Results 144
90% Percentile (z) 102.2 90% Percentile (z) 100

95% Percentile (z) 110 95% Percentile (z) 109.7

99% Percentile (z) 124.6 99% Percentile (z) 130.3

Gamma Distribution Test Data Distribution Test

k star 11.4 Data appear Gamma Distributed at 5% Significance Level

Theta Star 6.548

MLE of Mean 74.66

MLE of Standard Deviation 22.11

nu star 228

A‐D Test Statistic 0.496 Nonparametric Statistics

5% A‐D Critical Value 0.725 90% Percentile 94.15

K‐S Test Statistic 0.182 95% Percentile 110.6

5% K‐S Critical Value 0.266 99% Percentile 123.7

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 127

90% Percentile 104   90% Percentile Bootstrap UTL with   90% Coverage 127

95% Percentile 114.4   90% BCA Bootstrap UTL with   90% Coverage 127

99% Percentile 135.5   90% UPL 123.4

  90% Chebyshev UPL 142.3

   90% WH Approx. Gamma UPL 104.8 Upper Threshold Limit Based upon IQR 103.5

   90% HW Approx. Gamma UPL 104.7

   90% WH Approx. Gamma UTL with   90% Coverage 120.6

   90% HW Approx. Gamma UTL with   90% Coverage 120.9

Mercury

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 0.0188 Minimum ‐3.974

Maximum 0.143 Maximum ‐1.945

Second Largest 0.0778 Second Largest ‐2.554

First Quartile 0.0392 First Quartile ‐3.244

Median 0.0562 Median ‐2.883

Third Quartile 0.0708 Third Quartile ‐2.65

Mean 0.06 Mean ‐2.954

SD 0.0348 SD 0.568

Coefficient of Variation 0.579

Skewness 1.523

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.878 Shapiro Wilk Test Statistic 0.982

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.132   90% UTL with   90% Coverage 0.169

   90% UPL (t) 0.11   90% UPL (t) 0.119

90% Percentile (z) 0.105 90% Percentile (z) 0.108

95% Percentile (z) 0.117 95% Percentile (z) 0.133

99% Percentile (z) 0.141 99% Percentile (z) 0.195

Washington UPL Results 145
Gamma Distribution Test Data Distribution Test

k star 2.653 Data appear Normal at 5% Significance Level

Theta Star 0.0226

MLE of Mean 0.06

MLE of Standard Deviation 0.0369

nu star 53.05

A‐D Test Statistic 0.199 Nonparametric Statistics

5% A‐D Critical Value 0.73 90% Percentile 0.0843

K‐S Test Statistic 0.145 95% Percentile 0.114

5% K‐S Critical Value 0.268 99% Percentile 0.137

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.143

90% Percentile 0.109   90% Percentile Bootstrap UTL with   90% Coverage 0.143

95% Percentile 0.131   90% BCA Bootstrap UTL with   90% Coverage 0.143

99% Percentile 0.177   90% UPL 0.136

  90% Chebyshev UPL 0.169

   90% WH Approx. Gamma UPL 0.113 Upper Threshold Limit Based upon IQR 0.118

   90% HW Approx. Gamma UPL 0.114

   90% WH Approx. Gamma UTL with   90% Coverage 0.147

   90% HW Approx. Gamma UTL with   90% Coverage 0.151

Nickel

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 1.26 Minimum 0.231

Maximum 12.2 Maximum 2.501

Second Largest 4.18 Second Largest 1.43

First Quartile 2.243 First Quartile 0.806

Median 2.695 Median 0.991

Third Quartile 2.893 Third Quartile 1.062

Mean 3.468 Mean 1.018

SD 3.18 SD 0.637

Coefficient of Variation 0.917

Skewness 2.767

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.607 Shapiro Wilk Test Statistic 0.858

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 10.04   90% UTL with   90% Coverage 10.32

   90% UPL (t) 8.08   90% UPL (t) 6.971

90% Percentile (z) 7.543 90% Percentile (z) 6.26

95% Percentile (z) 8.698 95% Percentile (z) 7.89

99% Percentile (z) 10.87 99% Percentile (z) 12.18

Gamma Distribution Test Data Distribution Test

k star 1.725 Data appear Lognormal at 5% Significance Level

Washington UPL Results 146
Theta Star 2.01

MLE of Mean 3.468

MLE of Standard Deviation 2.64

nu star 34.51

A‐D Test Statistic 0.959 Nonparametric Statistics

5% A‐D Critical Value 0.734 90% Percentile 4.982

K‐S Test Statistic 0.313 95% Percentile 8.591

5% K‐S Critical Value 0.269 99% Percentile 11.48

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 12.2

90% Percentile 6.986   90% Percentile Bootstrap UTL with   90% Coverage 12.2

95% Percentile 8.625   90% BCA Bootstrap UTL with   90% Coverage 12.2

99% Percentile 12.3   90% UPL 11.4

  90% Chebyshev UPL 13.47

   90% WH Approx. Gamma UPL 7.22 Upper Threshold Limit Based upon IQR 3.868

   90% HW Approx. Gamma UPL 7.14

   90% WH Approx. Gamma UTL with   90% Coverage 9.856

   90% HW Approx. Gamma UTL with   90% Coverage 9.911

Selenium

General Statistics

Total Number of Observations 3 Number of Distinct Observations 1

Number of Missing Values 3

Warning: This data set only has 3 observations!

Data set is too small to compute reliable and meaningful statistics and estimates!

The data set for variable Selenium was not processed!

It is suggested to collect at least 8 to 10 observations before using these statistical methods!

If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Formaldehyde

General Statistics

Total Number of Observations 10 Number of Distinct Observations 9

Raw Statistics Log‐Transformed Statistics

Minimum 29000 Minimum 10.28

Maximum 130000 Maximum 11.78

Second Largest 110000 Second Largest 11.61

First Quartile 44500 First Quartile 10.7

Median 47500 Median 10.77

Third Quartile 61500 Third Quartile 11.03

Mean 61100 Mean 10.91

SD 32909 SD 0.469

Coefficient of Variation 0.539

Skewness 1.479

Background Statistics

Washington UPL Results 147
Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.801 Shapiro Wilk Test Statistic 0.914

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 129090   90% UTL with   90% Coverage 144656

   90% UPL (t) 108835   90% UPL (t) 108359

90% Percentile (z) 103274 90% Percentile (z) 100096

95% Percentile (z) 115230 95% Percentile (z) 118708

99% Percentile (z) 137657 99% Percentile (z) 163461

Gamma Distribution Test Data Distribution Test

k star 3.421 Data appear Gamma Distributed at 5% Significance Level

Theta Star 17862

MLE of Mean 61100

MLE of Standard Deviation 33036

nu star 68.41

A‐D Test Statistic 0.627 Nonparametric Statistics

5% A‐D Critical Value 0.729 90% Percentile 112000

K‐S Test Statistic 0.227 95% Percentile 121000

5% K‐S Critical Value 0.268 99% Percentile 128200

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 130000

90% Percentile 105398   90% Percentile Bootstrap UTL with   90% Coverage 130000

95% Percentile 123566   90% BCA Bootstrap UTL with   90% Coverage 130000

99% Percentile 162678   90% UPL 128000

  90% Chebyshev UPL 164645

   90% WH Approx. Gamma UPL 107878 Upper Threshold Limit Based upon IQR 87000

   90% HW Approx. Gamma UPL 107912

   90% WH Approx. Gamma UTL with   90% Coverage 136568

   90% HW Approx. Gamma UTL with   90% Coverage 138180

Chloride

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 179 Minimum 5.187

Maximum 1960 Maximum 7.581

Second Largest 1530 Second Largest 7.333

First Quartile 536.3 First Quartile 6.283

Median 728.5 Median 6.587

Third Quartile 1285 Third Quartile 7.156

Mean 908.4 Mean 6.609

SD 563.2 SD 0.718

Coefficient of Variation 0.62

Skewness 0.664

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.948 Shapiro Wilk Test Statistic 0.966

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Washington UPL Results 148
Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2072   90% UTL with   90% Coverage 3267

   90% UPL (t) 1725   90% UPL (t) 2100

90% Percentile (z) 1630 90% Percentile (z) 1860

95% Percentile (z) 1835 95% Percentile (z) 2415

99% Percentile (z) 2219 99% Percentile (z) 3938

Gamma Distribution Test Data Distribution Test

k star 1.899 Data appear Normal at 5% Significance Level

Theta Star 478.3

MLE of Mean 908.4

MLE of Standard Deviation 659.2

nu star 37.98

A‐D Test Statistic 0.154 Nonparametric Statistics

5% A‐D Critical Value 0.733 90% Percentile 1573

K‐S Test Statistic 0.111 95% Percentile 1767

5% K‐S Critical Value 0.269 99% Percentile 1921

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1960

90% Percentile 1788   90% Percentile Bootstrap UTL with   90% Coverage 1960

95% Percentile 2190   90% BCA Bootstrap UTL with   90% Coverage 1960

99% Percentile 3085   90% UPL 1917

  90% Chebyshev UPL 2680

   90% WH Approx. Gamma UPL 1872 Upper Threshold Limit Based upon IQR 2408

   90% HW Approx. Gamma UPL 1912

   90% WH Approx. Gamma UTL with   90% Coverage 2525

   90% HW Approx. Gamma UTL with   90% Coverage 2648

Fluoride

General Statistics

Total Number of Observations 4 Number of Distinct Observations 3

Number of Missing Values 5

Warning: This data set only has 4 observations!

Data set is too small to compute reliable and meaningful statistics and estimates!

The data set for variable Fluoride was not processed!

It is suggested to collect at least 8 to 10 observations before using these statistical methods!

If possible, compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Total Metals

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 76.11 Minimum 4.332

Maximum 210.5 Maximum 5.35

Washington UPL Results 149
Second Largest 167.7 Second Largest 5.122

First Quartile 99.42 First Quartile 4.599

Median 110.1 Median 4.701

Third Quartile 121.8 Third Quartile 4.803

Mean 121.7 Mean 4.761

SD 39.3 SD 0.29

Coefficient of Variation 0.323

Skewness 1.52

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.843 Shapiro Wilk Test Statistic 0.923

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 202.9   90% UTL with   90% Coverage 212.7

   90% UPL (t) 178.7   90% UPL (t) 178

90% Percentile (z) 172 90% Percentile (z) 169.4

95% Percentile (z) 186.3 95% Percentile (z) 188.3

99% Percentile (z) 213.1 99% Percentile (z) 229.4

Gamma Distribution Test Data Distribution Test

k star 8.85 Data appear Normal at 5% Significance Level

Theta Star 13.75

MLE of Mean 121.7

MLE of Standard Deviation 40.9

nu star 177

A‐D Test Statistic 0.547 Nonparametric Statistics

5% A‐D Critical Value 0.725 90% Percentile 172

K‐S Test Statistic 0.26 95% Percentile 191.3

5% K‐S Critical Value 0.267 99% Percentile 206.7

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 210.5

90% Percentile 176.2   90% Percentile Bootstrap UTL with   90% Coverage 210.5

95% Percentile 195.8   90% BCA Bootstrap UTL with   90% Coverage 210.5

99% Percentile 236.4   90% UPL 206.2

  90% Chebyshev UPL 245.3

   90% WH Approx. Gamma UPL 177.8 Upper Threshold Limit Based upon IQR 155.5

   90% HW Approx. Gamma UPL 177.8

   90% WH Approx. Gamma UTL with   90% Coverage 208.1

   90% HW Approx. Gamma UTL with   90% Coverage 209.1

Total Halogens

General Statistics

Total Number of Observations 10 Number of Distinct Observations 10

Raw Statistics Log‐Transformed Statistics

Minimum 179 Minimum 5.187

Maximum 2007 Maximum 7.604

Second Largest 1530 Second Largest 7.333

First Quartile 582 First Quartile 6.365

Median 747 Median 6.614

Washington UPL Results 150
Third Quartile 1285 Third Quartile 7.156

Mean 925.7 Mean 6.632

SD 565.3 SD 0.714

Coefficient of Variation 0.611

Skewness 0.695

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.952 Shapiro Wilk Test Statistic 0.962

Shapiro Wilk Critical Value 0.842 Shapiro Wilk Critical Value 0.842

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2094   90% UTL with   90% Coverage 3318

   90% UPL (t) 1746   90% UPL (t) 2138

90% Percentile (z) 1650 90% Percentile (z) 1895

95% Percentile (z) 1856 95% Percentile (z) 2456

99% Percentile (z) 2241 99% Percentile (z) 3996

Gamma Distribution Test Data Distribution Test

k star 1.938 Data appear Normal at 5% Significance Level

Theta Star 477.6

MLE of Mean 925.7

MLE of Standard Deviation 664.9

nu star 38.76

A‐D Test Statistic 0.15 Nonparametric Statistics

5% A‐D Critical Value 0.733 90% Percentile 1578

K‐S Test Statistic 0.112 95% Percentile 1792

5% K‐S Critical Value 0.269 99% Percentile 1964

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 2007

90% Percentile 1814   90% Percentile Bootstrap UTL with   90% Coverage 2007

95% Percentile 2218   90% BCA Bootstrap UTL with   90% Coverage 2007

99% Percentile 3115   90% UPL 1959

  90% Chebyshev UPL 2704

   90% WH Approx. Gamma UPL 1897 Upper Threshold Limit Based upon IQR 2340

   90% HW Approx. Gamma UPL 1939

   90% WH Approx. Gamma UTL with   90% Coverage 2552

   90% HW Approx. Gamma UTL with   90% Coverage 2678

Washington UPL Results 151
Components

Metals (mg/kg)

Total Metals (mg/kg)

Ions

Total Halogens (mg/kg)

* All 90% UPL Results reported as Normal MRL = Method Reporting Limit

** 90% UPL Result reported as Lognormal MDL = Method Detection Limit

*** 90% UPL Result Non‐Parametric HAP = Hazardous Air Pollutant

‐‐ = Non‐Detect OH = Organic Halogen

n.d. = Only 1 Distinct Value, therefore no variance. N = Nitrogenated

7157 6702 6900 7172 5587 6617

0.09 0.11

0.99

0.55 0.57 1.5 0.58

18.47

0.53 0.74

11.9 13.5 10.3 23.1 19.5

15.87 19.63 14.88 30.34

62

73

17 61

0.8

0.4

2

0.4 0.4

0.08

80.4

18.4

143.5

Fluorine (mg/kg)

110.9 143.5 175.3 102.6

Chlorine (mg/kg) 99 130 165 79.5 124

137.5 260.5 370.5 143.5 33.0 85.5

Nickel  (HAP)

Selenium  (HAP) 0.8

Manganese  (HAP)

Mercury  (HAP) 0.08 0.08 0.08

Lead  (HAP) 20 60 210 18

0.3 0.08

Cobalt  (HAP)

Chromium  (HAP) 60 100 80 26

6.3

0.39

Beryllium  (HAP)

22 11

Heating Value (BTU/lb)

Antimony  (HAP)

Cadmium  (HAP)

8.2

0.2

13

0.4 0.4

Arsenic  (HAP) 57 100 80

0.18 0.15

Nitrogen (wt%) 0.09 0.14 0.09 0.16

23

Sulfur (wt%) 0.18 0.17 0.17 0.16

Moisture (wt%)

Ash (wt%)

4/18 Comp. 4/19 Comp. 4/30 Comp. 5/1 Comp. 5/2 Comp. 5/3 Comp.

Mass. C&D Summary Table 152
7059 7243 7022 6872 6251

0.08 0.09 0.12

0.76

55.5

72.3

0.67 0.96

22.7 14.5 13.94 28.3 20.82

0.89 1.06 0.67 0.52 0.71

53.7 60.6 104.1

0.68

466.4

26 21

0.98

0.99

135.9 83.9

31.8 11.2

72.73

0.4 0.39

16 180

13 180

0.2

2

6035 6763

0.15 0.17

0.08

0.39 0.39

32

89.4 150

12.1 17.7 13.9

0.78

8.5 8.9

84.4 107.1 163.9

0.4

43 50 220

140.7 106.4 462.5

0.78

0.18

2

6444 6568

0.16 0.18

37 47

184.6 105.6

15

15.1 15.75 19.6

0.6

349.5

4 180

154 155 86.9

20.3 29.6 18.7

0.98

71

31

388.2

0.08 0.08

29.3 12.5

83.0 73.1

2

5/16 Comp. 5/17 Comp.

130

0.18

80

174.3

174.5 460.0 23.5

0.79

0.98

0.08 0.1 0.08 0.07 0.07

47

0.08

9.5 19

240

0.08 0.08

0.79 0.78

0.39 0.39

44

0.2

0.4 0.4 0.4

210

0.2

92

59 130

7434

210 4 150

0.18 0.18 0.18

0.09 0.09 0.09 0.15

0.17

13.3 16.6

5/15 Comp.

0.16 0.11

5/4 Comp. 5/7 Comp. 5/8 Comp. 5/9 Comp. 5/10 Comp. 5/11 Comp. 5/14 Comp.

Mass. C&D Summary Table 153
0.17

6481 6947

21.4 22 16.86

1.22 0.99 0.87 0.65

20.3

46.6

2

0.08 0.08 0.08

104.1 109.1

27 42 7.5

30 48 8.5

0.08 0.08 0.08

37 56 33

100

186.1 188.1 228.1

83 68

0.99

58

0.08

327.5 159.5 423.5

194.6

19.4 37.7

86.5

0.08 0.08

1

178.4 136

16.2

173.7

0.2

0.39 0.39 0.4

68

0.15 0.08 0.09

140 21 52

0.16 0.17

6676

17

6608

460.5

170 28

67.1

230

58.0

11.37

0.39

120

110

0.17

5/21 Comp. 5/22 Comp.

0.08

4/18 Re Comp. 4/19 Re Comp. 4/30 Re Comp. 5/1 Re Comp.

39.1

110 240 47 19 23

0.08

0.8

66 64 95

5/18 Comp. 5/23 Comp. 5/2 Re Comp. 5/3 Re Comp.

Mass. C&D Summary Table 154
50 86 32 100

5/11 Re Comp. 5/14 Re Comp. 5/15 Re Comp.

0.08 0.08

103.7

12

0.08 0.08

201.1

89

159.9 81.1

20

47

6.6 8.8

103.1 111.1

16 17

114.1 87.1 266.1 86.1

0.08 0.08 0.08 0.08

16 52

0.08 0.08

13 5

45 15 120 32 40 50

53 20 130 37 50 56

65 29

5/4 Re Comp. 5/7 Re Comp. 5/8 Re Comp. 5/9 Re Comp. 5/10 Re Comp. 5/16 Re Comp. 5/17 Re Comp.

Mass. C&D Summary Table 155
16 14

0.39

0.35 0.08 0.08

0.76 0.9 1.09

9.12 31.9 18.87

0.66

7655 5468 6427 7713

26

6541 6935

0.07

18 56 2.2

82 52

46

0.07

0.39

34 54

37 62

0.08

33.9 13.3 28.9 14.9

23.2 14.1 33.9 13.3 28.9 14.9

240.5 49.5

23.2 14.1

372.7 52.1 303.7 308.5

0.4

18 10 19

200 9.6

0.4 0.4

99 150 120 16

54 140 110

0.19 0.14 0.17 0.19

150

0.39

0.2 0.08 0.21 0.09 0.09 0.09

170

18.6

0.18 0.17

11.4

5/10 Grab

15.7

5/8 Grab

0.56 0.6

4/30 Grab 5/2 Grab 5/4 Grab

0.08 0.08

89.1 172.1

20 9.7

178.1 107.8

0.08 0.08

76

5/18 Re Comp. 5/22 5/21 Re Comp. Re Comp. 5/23 Re Comp. 4/18 Grab

Mass. C&D Summary Table 156
18

0.08 0.08 0.08

6.1

0.94

0.18

0.76 0.49

7159 7435 6875

0.17

0.55 0.82

6918

0.08

280 2 5.4

22

21

48.5

33.8 31.8

33.8 31.8

150

314.5 8.0 322.1

19 0.49 170

0.08 0.08

0.09 0.09

0.4

15

0.4

16.6 17.2

16.6 17.2

142.5 125.2

0.41 0.4

34

90 120

2

2.7

0.18 0.18

0.09 0.14

14 12.78

5/14 Grab 5/16 Grab 4/30 Re Grab

12.7 17.5

5/18 Grab 5/22 Grab 4/18 Re Grab

31.5

12

9.7

9.7

0.08

35 2.5 2

0.58

242.6 97.6 442.1

30 52 220

0.08 0.08

177 43 220

5/2 Re Grab 5/4 Re Grab 5/8 Re Grab 5/10 Re Grab

Mass. C&D Summary Table 157
*all results reported as moisture free

*all results pooled from all 7 samples

Non‐

Detect Average

Standard

Deviation Low High

31 18.20 5.34 9.12 31.9 25.31

31 0.76 0.23 0.49 1.5 1.062**

31 0.11 0.04 0.08 0.21 0.16***

31 0.17 0.01 0.14 0.19 0.18***

31 6788.80 520.79 5468.00 7713 7483

56 2.00 0.00 2.00 2 n.d.

1 63.72 59.28 0.94 220 187.8**

56 0.200 0.000 0.200 0.2 n.d.

31 0.40 0.01 0.39 0.41 0.4***

1 69.38 63.04 0.49 240 179***

56 0.79 0.01 0.78 0.8 0.8

1 43.75 62.33 2.0 280.0 129***

56 57.80 19.74 31.0 80 91.0

1 0.10 0.08 0.070 0.580 0.080

56 0.98 0.01 0.98 0.99 0.99

56 0.87 0.11 0.78 1 1.0

‐‐ 182.37 136.1 8.01 466 460.3**

41 104.32 41.37 47 178 160.6

31 20.21 8.12 10 38 31.48**

‐‐ 89.75 59.62 13.30 194.6 175.2***

56.1 9.1

0.08

20 6.9

18 0.9

18 1.2

0.08

18.9 13.9

6.5 2.4

5.3

0.12 0.08

6.1

6.4

5.9

5/14 Re Grab 5/18 5/16 Re Grab Re Grab 5/22 Re Grab

Range 90% UPL

Results*

Mass. C&D Summary Table 158
Moisture (wAsh (wt%) Nitrogen (wSulfur (wt%Heating Va Antimony   Arsenic  (HABeryllium  (Cadmium  (

30 30 30 30 30 5 60 5 30

15.87 0.55 0.09 0.18 7157 57 0.4

19.63 0.57 0.14 0.17 6702 100 0.4

18.47 1.5 0.09 0.17 6900 80 0.4

14.88 0.58 0.09 0.18 7172 2 22 0.2 0.4

30.34 0.53 0.11 0.15 5587 11 0.4

23 0.74 0.16 0.16 6617 6.3 0.39

13.3 0.67 0.09 0.18 7434 44 0.39

16.6 0.76 0.09 0.18 7059 2 92 0.2 0.39

15.1 0.6 0.16 0.18 7243 210 0.4

15.75 0.89 0.09 0.18 7022 4 0.4

19.6 1.06 0.15 0.17 6872 150 0.4

22.7 0.67 0.08 0.16 6251 2 37 0.2 0.39

14.5 0.52 0.09 0.18 6444 47 0.39

13.94 0.71 0.12 0.18 6568 210 0.4

28.3 0.96 0.11 0.15 6035 13 0.4

20.82 0.68 0.08 0.17 6763 2 180 0.2 0.39

21.4 1.22 0.08 0.17 6608 110 0.39

20.3 0.99 0.15 0.17 6676 140 0.39

22 0.87 0.08 0.16 6481 21 0.39

16.86 0.65 0.09 0.17 6947 2 52 0.2 0.4

66

64

95

27

42

7.5

45

15

120

32

40

50

47

65

29

89

76

46

34

54

9.12 0.76 0.2 0.19 7655 170 0.4

31.9 0.9 0.08 0.14 5468 16 0.4

18.87 1.09 0.21 0.17 6427 54 0.39

11.4 0.56 0.09 0.19 7713 140 0.4

15.7 0.6 0.09 0.18 6541 110 0.39

Mass. ProUCL Entry 159
18.6 0.66 0.09 0.17 6935 14 0.39

14 0.55 0.09 0.18 7159 18 0.41

12.78 0.82 0.14 0.18 7435 2.7 0.4

12.7 0.76 0.09 0.18 6918 15 0.4

17.5 0.49 0.09 0.17 6875 0.94 0.4

150

22

177

43

220

9.7

18

1.2

5.9

6.1

Mass. ProUCL Entry 160
Chromium Cobalt  (HALead  (HAP)ManganeseMercury  (HNickel  (HA Selenium  ( Total Meta Chlorine (m

60 5 60 5 60 5 5 60 20

60 20 0.08 137.48 99

100 60 0.08 260.48 130

80 210 0.08 370.48 165

26 0.8 17 73 0.3 0.99 0.8 143.49 79.5

13 61 0.08 85.48 124

8.2 18 0.08 32.97 62

59 71 0.08 174.47 53.7

130 0.79 130 31 0.08 0.98 0.79 388.23 60.6

240 9.5 0.08 459.98 154

4 15 0.1 23.5 155

180 19 0.08 349.48 86.9

43 0.78 8.5 47 0.07 0.98 0.78 140.7 72.3

50 8.9 0.07 106.36 89.4

220 32 0.08 462.48 150

16 26 0.08 55.48 104.1

180 0.78 21 80 0.08 0.98 0.99 466.42 72.73

120 230 0.08 460.47 46.6

170 17 0.08 327.47 178.4

28 110 0.08 159.47 67.1

68 0.8 240 58 0.08 0.99 1 423.47 136

83 37 0.08 186.08

68 56 0.08 188.08

100 33 0.08 228.08

30 47 0.08 104.08

48 19 0.08 109.08

8.5 23 0.08 39.08

53 16 0.08 114.08

20 52 0.08 87.08

130 16 0.08 266.08

37 17 0.08 86.08

50 13 0.08 103.08

56 5 0.08 111.08

50 6.6 0.08 103.68

86 8.8 0.08 159.88

32 20 0.08 81.08

100 12 0.08 201.08

82 20 0.08 178.08

52 9.7 0.08 107.78

37 18 0.08 89.08

62 56 0.08 172.08

200 2.2 0.08 372.68

9.6 26 0.07 52.07

99 150 0.35 303.74

150 18 0.08 308.48

120 10 0.08 240.47

Mass. ProUCL Entry 161
16 19 0.07 49.46

34 90 0.08 142.49

2 120 0.08 125.18

19 280 0.08 314.48

0.49 6.1 0.08 8.01

170 2 0.08 322.08

21 5.4 0.08 48.48

30 35 0.58 242.58

52 2.5 0.08 97.58

220 2 0.08 442.08

9.7 12 0.08 31.48

18 20 0.08 56.08

0.9 6.9 0.08 9.08

6.4 6.5 0.12 18.92

5.3 2.4 0.08 13.88

Mass. ProUCL Entry 162
Fluorine (mTotal Halogens (mg/kg)

30 30

11.9 110.9

13.5 143.5

10.3 175.3

23.1 102.6

19.5 143.5

18.4 80.4

29.3 83

12.5 73.1

20.3 174.3

29.6 184.6

18.7 105.6

12.1 84.4

17.7 107.1

13.9 163.9

31.8 135.9

11.2 83.93

11.37 57.97

16.2 194.6

19.4 86.5

37.7 173.7

23.2 23.2

14.1 14.1

33.9 33.9

13.3 13.3

28.9 28.9

Mass. ProUCL Entry 163
14.9 14.9

16.6 16.6

17.2 17.2

33.8 33.8

31.8 31.8

Mass. ProUCL Entry 164
Moisture

General Statistics

Total Number of Observations 30 Number of Distinct Observations 30

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 9.12 Minimum 2.21

Maximum 31.9 Maximum 3.463

Second Largest 30.34 Second Largest 3.412

First Quartile 14.6 First Quartile 2.681

Median 17.18 Median 2.844

Third Quartile 20.69 Third Quartile 3.03

Mean 18.2 Mean 2.862

SD 5.337 SD 0.283

Coefficient of Variation 0.293

Skewness 0.947

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.934 Shapiro Wilk Test Statistic 0.984

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 27.04   90% UTL with   90% Coverage 27.98

   90% UPL (t) 25.31   90% UPL (t) 25.53

90% Percentile (z) 25.04 90% Percentile (z) 25.16

95% Percentile (z) 26.98 95% Percentile (z) 27.88

99% Percentile (z) 30.61 99% Percentile (z) 33.82

Gamma Distribution Test Data Distribution Test

k star 11.64 Data appear Normal at 5% Significance Level

Theta Star 1.563

MLE of Mean 18.2

MLE of Standard Deviation 5.334

nu star 698.4

A‐D Test Statistic 0.273 Nonparametric Statistics

5% A‐D Critical Value 0.745 90% Percentile 23.53

K‐S Test Statistic 0.0839 95% Percentile 29.42

5% K‐S Critical Value 0.16 99% Percentile 31.45

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 30.34

90% Percentile 25.28   90% Percentile Bootstrap UTL with   90% Coverage 30.34

95% Percentile 27.77   90% BCA Bootstrap UTL with   90% Coverage 30.34

99% Percentile 32.84   90% UPL 27.77

  90% Chebyshev UPL 34.47

   90% WH Approx. Gamma UPL 25.37 Upper Threshold Limit Based upon IQR 29.83

   90% HW Approx. Gamma UPL 25.4

   90% WH Approx. Gamma UTL with   90% Coverage 27.51

   90% HW Approx. Gamma UTL with   90% Coverage 27.61

Ash

Mass. UPL Results 165
General Statistics

Total Number of Observations 30 Number of Distinct Observations 25

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.49 Minimum ‐0.713

Maximum 1.5 Maximum 0.405

Second Largest 1.22 Second Largest 0.199

First Quartile 0.585 First Quartile ‐0.536

Median 0.695 Median ‐0.364

Third Quartile 0.885 Third Quartile ‐0.122

Mean 0.764 Mean ‐0.309

SD 0.234 SD 0.277

Coefficient of Variation 0.306

Skewness 1.384

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.883 Shapiro Wilk Test Statistic 0.95

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.151   90% UTL with   90% Coverage 1.162

   90% UPL (t) 1.075   90% UPL (t) 1.062

90% Percentile (z) 1.063 90% Percentile (z) 1.047

95% Percentile (z) 1.148 95% Percentile (z) 1.158

99% Percentile (z) 1.307 99% Percentile (z) 1.398

Gamma Distribution Test Data Distribution Test

k star 11.62 Data appear Gamma Distributed at 5% Significance Level

Theta Star 0.0657

MLE of Mean 0.764

MLE of Standard Deviation 0.224

nu star 697.3

A‐D Test Statistic 0.603 Nonparametric Statistics

5% A‐D Critical Value 0.745 90% Percentile 1.063

K‐S Test Statistic 0.136 95% Percentile 1.162

5% K‐S Critical Value 0.16 99% Percentile 1.419

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.22

90% Percentile 1.061   90% Percentile Bootstrap UTL with   90% Coverage 1.22

95% Percentile 1.166   90% BCA Bootstrap UTL with   90% Coverage 1.22

99% Percentile 1.379   90% UPL 1.087

  90% Chebyshev UPL 1.476

   90% WH Approx. Gamma UPL 1.064 Upper Threshold Limit Based upon IQR 1.335

   90% HW Approx. Gamma UPL 1.064

   90% WH Approx. Gamma UTL with   90% Coverage 1.154

   90% HW Approx. Gamma UTL with   90% Coverage 1.156

Nitrogen

General Statistics

Mass. UPL Results 166
Total Number of Observations 30 Number of Distinct Observations 9

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.08 Minimum ‐2.526

Maximum 0.21 Maximum ‐1.561

Second Largest 0.2 Second Largest ‐1.609

First Quartile 0.09 First Quartile ‐2.408

Median 0.09 Median ‐2.408

Third Quartile 0.135 Third Quartile ‐2.005

Mean 0.11 Mean ‐2.248

SD 0.0363 SD 0.287

Coefficient of Variation 0.329

Skewness 1.445

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.754 Shapiro Wilk Test Statistic 0.795

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.171   90% UTL with   90% Coverage 0.17

   90% UPL (t) 0.159   90% UPL (t) 0.155

90% Percentile (z) 0.157 90% Percentile (z) 0.153

95% Percentile (z) 0.17 95% Percentile (z) 0.169

99% Percentile (z) 0.195 99% Percentile (z) 0.206

Gamma Distribution Test Data Distribution Test

k star 10.48 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0105

MLE of Mean 0.11

MLE of Standard Deviation 0.0341

nu star 629

A‐D Test Statistic 2.879 Nonparametric Statistics

5% A‐D Critical Value 0.745 90% Percentile 0.16

K‐S Test Statistic 0.35 95% Percentile 0.182

5% K‐S Critical Value 0.16 99% Percentile 0.207

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.2

90% Percentile 0.156   90% Percentile Bootstrap UTL with   90% Coverage 0.2

95% Percentile 0.172   90% BCA Bootstrap UTL with   90% Coverage 0.164

99% Percentile 0.205   90% UPL 0.16

  90% Chebyshev UPL 0.221

   90% WH Approx. Gamma UPL 0.156 Upper Threshold Limit Based upon IQR 0.203

   90% HW Approx. Gamma UPL 0.156

   90% WH Approx. Gamma UTL with   90% Coverage 0.17

   90% HW Approx. Gamma UTL with   90% Coverage 0.17

Sulfur

General Statistics

Total Number of Observations 30 Number of Distinct Observations 6

Mass. UPL Results 167
Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.14 Minimum ‐1.966

Maximum 0.19 Maximum ‐1.661

Second Largest 0.19 Second Largest ‐1.661

First Quartile 0.17 First Quartile ‐1.772

Median 0.17 Median ‐1.772

Third Quartile 0.18 Third Quartile ‐1.715

Mean 0.172 Mean ‐1.763

SD 0.0116 SD 0.0698

Coefficient of Variation 0.0672

Skewness ‐0.991

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.872 Shapiro Wilk Test Statistic 0.856

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.191   90% UTL with   90% Coverage 0.193

   90% UPL (t) 0.187   90% UPL (t) 0.188

90% Percentile (z) 0.187 90% Percentile (z) 0.188

95% Percentile (z) 0.191 95% Percentile (z) 0.192

99% Percentile (z) 0.199 99% Percentile (z) 0.202

Gamma Distribution Test Data Distribution Test

k star 196.2 Data do not follow a Discernable Distribution (0.05)

Theta Star 8.77E‐04

MLE of Mean 0.172

MLE of Standard Deviation 0.0123

nu star 11769

A‐D Test Statistic 1.773 Nonparametric Statistics

5% A‐D Critical Value 0.745 90% Percentile 0.18

K‐S Test Statistic 0.24 95% Percentile 0.186

5% K‐S Critical Value 0.16 99% Percentile 0.19

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.19

90% Percentile 0.188   90% Percentile Bootstrap UTL with   90% Coverage 0.19

95% Percentile 0.193   90% BCA Bootstrap UTL with   90% Coverage 0.18

99% Percentile 0.202   90% UPL 0.18

  90% Chebyshev UPL 0.207

   90% WH Approx. Gamma UPL 0.188 Upper Threshold Limit Based upon IQR 0.195

   90% HW Approx. Gamma UPL 0.188

   90% WH Approx. Gamma UTL with   90% Coverage 0.192

   90% HW Approx. Gamma UTL with   90% Coverage 0.192

Heating Value

General Statistics

Total Number of Observations 30 Number of Distinct Observations 30

Number of Missing Values 20

Mass. UPL Results 168
Raw Statistics Log‐Transformed Statistics

Minimum 5468 Minimum 8.607

Maximum 7713 Maximum 8.951

Second Largest 7655 Second Largest 8.943

First Quartile 6548 First Quartile 8.787

Median 6874 Median 8.835

Third Quartile 7133 Third Quartile 8.872

Mean 6789 Mean 8.82

SD 520.8 SD 0.0792

Coefficient of Variation 0.0767

Skewness ‐0.656

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.957 Shapiro Wilk Test Statistic 0.936

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7652   90% UTL with   90% Coverage 7718

   90% UPL (t) 7483   90% UPL (t) 7523

90% Percentile (z) 7456 90% Percentile (z) 7492

95% Percentile (z) 7645 95% Percentile (z) 7711

99% Percentile (z) 8000 99% Percentile (z) 8138

Gamma Distribution Test Data Distribution Test

k star 151.9 Data appear Normal at 5% Significance Level

Theta Star 44.68

MLE of Mean 6789

MLE of Standard Deviation 550.8

nu star 9116

A‐D Test Statistic 0.481 Nonparametric Statistics

5% A‐D Critical Value 0.745 90% Percentile 7434

K‐S Test Statistic 0.115 95% Percentile 7556

5% K‐S Critical Value 0.16 99% Percentile 7696

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7655

90% Percentile 7504   90% Percentile Bootstrap UTL with   90% Coverage 7655

95% Percentile 7719   90% BCA Bootstrap UTL with   90% Coverage 7655

99% Percentile 8135   90% UPL 7435

  90% Chebyshev UPL 8377

   90% WH Approx. Gamma UPL 7508 Upper Threshold Limit Based upon IQR 8010

   90% HW Approx. Gamma UPL 7511

   90% WH Approx. Gamma UTL with   90% Coverage 7694

   90% HW Approx. Gamma UTL with   90% Coverage 7699

Antimony

General Statistics

Total Number of Observations 5 Number of Distinct Observations 1

Number of Missing Values 15

Mass. UPL Results 169
Warning: There is only one distinct observation value in this data set ‐ resulting in '0' variance!

ProUCL (or any other software) should not be used on such a data set!

The data set for variable Antimony was not processed!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible, compute and collect Data Quality Objectives (DQOs) based sample size and analytical results.

The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV).

Arsenic

General Statistics

Total Number of Observations 60 Number of Distinct Observations 51

Raw Statistics Log‐Transformed Statistics

Minimum 0.94 Minimum ‐0.0619

Maximum 220 Maximum 5.394

Second Largest 210 Second Largest 5.347

First Quartile 17.5 First Quartile 2.861

Median 45.5 Median 3.818

Third Quartile 92.75 Third Quartile 4.53

Mean 63.72 Mean 3.593

SD 59.28 SD 1.257

Coefficient of Variation 0.93

Skewness 1.157

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.182 Lilliefors Test Statistic 0.114

Lilliefors Critical Value 0.114 Lilliefors Critical Value 0.114

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 154.2   90% UTL with   90% Coverage 247.4

   90% UPL (t) 141.2   90% UPL (t) 187.8

90% Percentile (z) 139.7 90% Percentile (z) 182

95% Percentile (z) 161.2 95% Percentile (z) 287.3

99% Percentile (z) 201.6 99% Percentile (z) 676.7

Gamma Distribution Test Data Distribution Test

k star 0.984 Data appear Gamma Distributed at 5% Significance Level

Theta Star 64.74

MLE of Mean 63.72

MLE of Standard Deviation 64.23

nu star 118.1

A‐D Test Statistic 0.211 Nonparametric Statistics

5% A‐D Critical Value 0.779 90% Percentile 152

K‐S Test Statistic 0.0569 95% Percentile 181.5

5% K‐S Critical Value 0.118 99% Percentile 214.1

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 177

90% Percentile 147.3   90% Percentile Bootstrap UTL with   90% Coverage 180

95% Percentile 192   90% BCA Bootstrap UTL with   90% Coverage 177.3

99% Percentile 295.8   90% UPL 168

  90% Chebyshev UPL 243

Mass. UPL Results 170
   90% WH Approx. Gamma UPL 146.9 Upper Threshold Limit Based upon IQR 205.6

   90% HW Approx. Gamma UPL 151.6

   90% WH Approx. Gamma UTL with   90% Coverage 172

   90% HW Approx. Gamma UTL with   90% Coverage 180.8

Beryllium

General Statistics

Total Number of Observations 5 Number of Distinct Observations 1

Number of Missing Values 15

Warning: There is only one distinct observation value in this data set ‐ resulting in '0' variance!

ProUCL (or any other software) should not be used on such a data set!

The data set for variable Beryllium was not processed!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible, compute and collect Data Quality Objectives (DQOs) based sample size and analytical results.

The Project Team may decide to use alternative site specific values to estimate environmental parameters (e.g., EPC, BTV).

Cadmium

General Statistics

Total Number of Observations 30 Number of Distinct Observations 3

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.39 Minimum ‐0.942

Maximum 0.41 Maximum ‐0.892

Second Largest 0.4 Second Largest ‐0.916

First Quartile 0.39 First Quartile ‐0.942

Median 0.4 Median ‐0.916

Third Quartile 0.4 Third Quartile ‐0.916

Mean 0.396 Mean ‐0.926

SD 0.00556 SD 0.014

Coefficient of Variation 0.014

Skewness 0.0735

Warning:  There are only 3 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.717 Shapiro Wilk Test Statistic 0.716

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

Mass. UPL Results 171
   90% UTL with   90% Coverage 0.406   90% UTL with   90% Coverage 0.406

   90% UPL (t) 0.404   90% UPL (t) 0.404

90% Percentile (z) 0.403 90% Percentile (z) 0.403

95% Percentile (z) 0.405 95% Percentile (z) 0.406

99% Percentile (z) 0.409 99% Percentile (z) 0.409

Gamma Distribution Test Data Distribution Test

k star 4732 Data do not follow a Discernable Distribution (0.05)

Theta Star 8.38E‐05

MLE of Mean 0.396

MLE of Standard Deviation 0.00576

nu star 283931

A‐D Test Statistic 4.462 Nonparametric Statistics

5% A‐D Critical Value 0.745 90% Percentile 0.4

K‐S Test Statistic 0.35 95% Percentile 0.4

5% K‐S Critical Value 0.16 99% Percentile 0.407

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.4

90% Percentile 0.404   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 0.406   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 0.41   90% UPL 0.4

  90% Chebyshev UPL 0.413

   90% WH Approx. Gamma UPL 0.404 Upper Threshold Limit Based upon IQR 0.415

   90% HW Approx. Gamma UPL 0.404

   90% WH Approx. Gamma UTL with   90% Coverage 0.406

   90% HW Approx. Gamma UTL with   90% Coverage 0.406

Chromium

General Statistics

Total Number of Observations 60 Number of Distinct Observations 46

Raw Statistics Log‐Transformed Statistics

Minimum 0.49 Minimum ‐0.713

Maximum 240 Maximum 5.481

Second Largest 220 Second Largest 5.394

First Quartile 19.75 First Quartile 2.983

Median 51 Median 3.932

Third Quartile 100 Third Quartile 4.605

Mean 69.38 Mean 3.663

SD 63.04 SD 1.33

Coefficient of Variation 0.908

Skewness 1.12

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.163 Lilliefors Test Statistic 0.129

Lilliefors Critical Value 0.114 Lilliefors Critical Value 0.114

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 165.6   90% UTL with   90% Coverage 296.5

   90% UPL (t) 151.8   90% UPL (t) 221.5

90% Percentile (z) 150.2 90% Percentile (z) 214.2

Mass. UPL Results 172
95% Percentile (z) 173.1 95% Percentile (z) 347.3

99% Percentile (z) 216 99% Percentile (z) 859.4

Gamma Distribution Test Data Distribution Test

k star 0.962 Data appear Gamma Distributed at 5% Significance Level

Theta Star 72.14

MLE of Mean 69.38

MLE of Standard Deviation 70.75

nu star 115.4

A‐D Test Statistic 0.192 Nonparametric Statistics

5% A‐D Critical Value 0.779 90% Percentile 171

K‐S Test Statistic 0.0659 95% Percentile 201

5% K‐S Critical Value 0.118 99% Percentile 228.2

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 180

90% Percentile 161.3   90% Percentile Bootstrap UTL with   90% Coverage 200

95% Percentile 210.7   90% BCA Bootstrap UTL with   90% Coverage 182

99% Percentile 325.9   90% UPL 179

  90% Chebyshev UPL 260.1

   90% WH Approx. Gamma UPL 160.8 Upper Threshold Limit Based upon IQR 220.4

   90% HW Approx. Gamma UPL 167.4

   90% WH Approx. Gamma UTL with   90% Coverage 188.4

   90% HW Approx. Gamma UTL with   90% Coverage 200

Cobalt

General Statistics

Total Number of Observations 5 Number of Distinct Observations 3

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.78 Minimum ‐0.248

Maximum 0.8 Maximum ‐0.223

Second Largest 0.8 Second Largest ‐0.223

First Quartile 0.78 First Quartile ‐0.248

Median 0.79 Median ‐0.236

Third Quartile 0.8 Third Quartile ‐0.223

Mean 0.79 Mean ‐0.236

SD 0.01 SD 0.0127

Coefficient of Variation 0.0127

Skewness 0

Warning:  There are only 3 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 5 may not adequate enough to compute meaningful and reliable test statistics and estimates!

Mass. UPL Results 173
It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.821 Shapiro Wilk Test Statistic 0.821

Shapiro Wilk Critical Value 0.762 Shapiro Wilk Critical Value 0.762

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.817   90% UTL with   90% Coverage 0.818

   90% UPL (t) 0.807   90% UPL (t) 0.807

90% Percentile (z) 0.803 90% Percentile (z) 0.803

95% Percentile (z) 0.806 95% Percentile (z) 0.807

99% Percentile (z) 0.813 99% Percentile (z) 0.814

Gamma Distribution Test Data Distribution Test

k star 3120 Data appear Normal at 5% Significance Level

Theta Star 2.53E‐04

MLE of Mean 0.79

MLE of Standard Deviation 0.0141

nu star 31204

A‐D Test Statistic 0.631 Nonparametric Statistics

5% A‐D Critical Value 0.678 90% Percentile 0.8

K‐S Test Statistic 0.28 95% Percentile 0.8

5% K‐S Critical Value 0.357 99% Percentile 0.8

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.8

90% Percentile 0.808   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 0.813   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 0.823   90% UPL 0.8

  90% Chebyshev UPL 0.823

   90% WH Approx. Gamma UPL 0.807 Upper Threshold Limit Based upon IQR 0.83

   90% HW Approx. Gamma UPL 0.807

   90% WH Approx. Gamma UTL with   90% Coverage 0.818

   90% HW Approx. Gamma UTL with   90% Coverage 0.818

Lead

General Statistics

Total Number of Observations 60 Number of Distinct Observations 46

Raw Statistics Log‐Transformed Statistics

Minimum 2 Minimum 0.693

Maximum 280 Maximum 5.635

Second Largest 240 Second Largest 5.481

First Quartile 9.65 First Quartile 2.267

Median 19 Median 2.944

Third Quartile 48.25 Third Quartile 3.875

Mean 43.75 Mean 3.046

SD 62.33 SD 1.215

Coefficient of Variation 1.425

Skewness 2.402

Mass. UPL Results 174
Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.279 Lilliefors Test Statistic 0.117

Lilliefors Critical Value 0.114 Lilliefors Critical Value 0.114

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 138.9   90% UTL with   90% Coverage 134.4

   90% UPL (t) 125.2   90% UPL (t) 103

90% Percentile (z) 123.6 90% Percentile (z) 99.87

95% Percentile (z) 146.3 95% Percentile (z) 155.3

99% Percentile (z) 188.7 99% Percentile (z) 355.6

Gamma Distribution Test Data Distribution Test

k star 0.78 Data do not follow a Discernable Distribution (0.05)

Theta Star 56.1

MLE of Mean 43.75

MLE of Standard Deviation 49.54

nu star 93.59

A‐D Test Statistic 2.153 Nonparametric Statistics

5% A‐D Critical Value 0.789 90% Percentile 121

K‐S Test Statistic 0.195 95% Percentile 211

5% K‐S Critical Value 0.119 99% Percentile 256.4

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 150

90% Percentile 107   90% Percentile Bootstrap UTL with   90% Coverage 210

95% Percentile 143.2   90% BCA Bootstrap UTL with   90% Coverage 210

99% Percentile 228.9   90% UPL 129

  90% Chebyshev UPL 232.3

   90% WH Approx. Gamma UPL 102.1 Upper Threshold Limit Based upon IQR 106.2

   90% HW Approx. Gamma UPL 100.8

   90% WH Approx. Gamma UTL with   90% Coverage 121.7

   90% HW Approx. Gamma UTL with   90% Coverage 122

Manganese

General Statistics

Total Number of Observations 5 Number of Distinct Observations 5

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 31 Minimum 3.434

Maximum 80 Maximum 4.382

Second Largest 73 Second Largest 4.29

First Quartile 47 First Quartile 3.85

Median 58 Median 4.06

Third Quartile 73 Third Quartile 4.29

Mean 57.8 Mean 4.003

SD 19.74 SD 0.38

Coefficient of Variation 0.342

Skewness ‐0.328

Warning: A sample size of 'n' = 5 may not adequate enough to compute meaningful and reliable test statistics and estimates!

Mass. UPL Results 175
It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 5 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.968 Shapiro Wilk Test Statistic 0.94

Shapiro Wilk Critical Value 0.762 Shapiro Wilk Critical Value 0.762

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 111.9   90% UTL with   90% Coverage 155.2

   90% UPL (t) 90.96   90% UPL (t) 103.7

90% Percentile (z) 83.1 90% Percentile (z) 89.12

95% Percentile (z) 90.27 95% Percentile (z) 102.3

99% Percentile (z) 103.7 99% Percentile (z) 132.5

Gamma Distribution Test Data Distribution Test

k star 3.932 Data appear Normal at 5% Significance Level

Theta Star 14.7

MLE of Mean 57.8

MLE of Standard Deviation 29.15

nu star 39.32

A‐D Test Statistic 0.243 Nonparametric Statistics

5% A‐D Critical Value 0.679 90% Percentile 77.2

K‐S Test Statistic 0.204 95% Percentile 78.6

5% K‐S Critical Value 0.358 99% Percentile 79.72

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 80

90% Percentile 96.87   90% Percentile Bootstrap UTL with   90% Coverage 80

95% Percentile 112.6   90% BCA Bootstrap UTL with   90% Coverage 80

99% Percentile 146.1   90% UPL 80

  90% Chebyshev UPL 122.7

   90% WH Approx. Gamma UPL 97.83 Upper Threshold Limit Based upon IQR 112

   90% HW Approx. Gamma UPL 99.08

   90% WH Approx. Gamma UTL with   90% Coverage 133

   90% HW Approx. Gamma UTL with   90% Coverage 137.4

Mercury

General Statistics

Total Number of Observations 60 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 0.07 Minimum ‐2.659

Maximum 0.58 Maximum ‐0.545

Second Largest 0.35 Second Largest ‐1.05

Mass. UPL Results 176
First Quartile 0.08 First Quartile ‐2.526

Median 0.08 Median ‐2.526

Third Quartile 0.08 Third Quartile ‐2.526

Mean 0.0968 Mean ‐2.445

SD 0.0778 SD 0.362

Coefficient of Variation 0.803

Skewness 5.114

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.502 Lilliefors Test Statistic 0.505

Lilliefors Critical Value 0.114 Lilliefors Critical Value 0.114

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.215   90% UTL with   90% Coverage 0.151

   90% UPL (t) 0.198   90% UPL (t) 0.139

90% Percentile (z) 0.196 90% Percentile (z) 0.138

95% Percentile (z) 0.225 95% Percentile (z) 0.157

99% Percentile (z) 0.278 99% Percentile (z) 0.202

Gamma Distribution Test Data Distribution Test

k star 4.492 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0216

MLE of Mean 0.0968

MLE of Standard Deviation 0.0457

nu star 539

A‐D Test Statistic 18.65 Nonparametric Statistics

5% A‐D Critical Value 0.753 90% Percentile 0.08

K‐S Test Statistic 0.514 95% Percentile 0.129

5% K‐S Critical Value 0.115 99% Percentile 0.444

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.1

90% Percentile 0.158   90% Percentile Bootstrap UTL with   90% Coverage 0.12

95% Percentile 0.182   90% BCA Bootstrap UTL with   90% Coverage 0.08

99% Percentile 0.233   90% UPL 0.08

  90% Chebyshev UPL 0.332

   90% WH Approx. Gamma UPL 0.155 Upper Threshold Limit Based upon IQR 0.08

   90% HW Approx. Gamma UPL 0.151

   90% WH Approx. Gamma UTL with   90% Coverage 0.169

   90% HW Approx. Gamma UTL with   90% Coverage 0.164

Nickel

General Statistics

Total Number of Observations 5 Number of Distinct Observations 2

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.98 Minimum ‐0.0202

Maximum 0.99 Maximum ‐0.0101

Second Largest 0.99 Second Largest ‐0.0101

First Quartile 0.98 First Quartile ‐0.0202

Mass. UPL Results 177
Median 0.98 Median ‐0.0202

Third Quartile 0.99 Third Quartile ‐0.0101

Mean 0.984 Mean ‐0.0161

SD 0.00548 SD 0.00556

Coefficient of Variation 0.00557

Skewness 0.609

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 5 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.684 Shapiro Wilk Test Statistic 0.684

Shapiro Wilk Critical Value 0.762 Shapiro Wilk Critical Value 0.762

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.999   90% UTL with   90% Coverage 0.999

   90% UPL (t) 0.993   90% UPL (t) 0.993

90% Percentile (z) 0.991 90% Percentile (z) 0.991

95% Percentile (z) 0.993 95% Percentile (z) 0.993

99% Percentile (z) 0.997 99% Percentile (z) 0.997

Gamma Distribution Test Data Distribution Test

k star 16159 Data do not follow a Discernable Distribution (0.05)

Theta Star 6.09E‐05

MLE of Mean 0.984

MLE of Standard Deviation 0.00774

nu star 161595

A‐D Test Statistic 1.56 Nonparametric Statistics

5% A‐D Critical Value 0.678 90% Percentile 0.99

K‐S Test Statistic 0.486 95% Percentile 0.99

5% K‐S Critical Value 0.357 99% Percentile 0.99

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.99

90% Percentile 0.994   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 0.997   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 1.002   90% UPL 0.99

  90% Chebyshev UPL 1.002

   90% WH Approx. Gamma UPL 0.993 Upper Threshold Limit Based upon IQR 1.005

   90% HW Approx. Gamma UPL 0.993

   90% WH Approx. Gamma UTL with   90% Coverage 0.999

   90% HW Approx. Gamma UTL with   90% Coverage 0.999

Mass. UPL Results 178
Selenium

General Statistics

Total Number of Observations 5 Number of Distinct Observations 5

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.78 Minimum ‐0.248

Maximum 1 Maximum 0

Second Largest 0.99 Second Largest ‐0.0101

First Quartile 0.79 First Quartile ‐0.236

Median 0.8 Median ‐0.223

Third Quartile 0.99 Third Quartile ‐0.0101

Mean 0.872 Mean ‐0.143

SD 0.113 SD 0.127

Coefficient of Variation 0.129

Skewness 0.595

Warning: A sample size of 'n' = 5 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 5 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.746 Shapiro Wilk Test Statistic 0.75

Shapiro Wilk Critical Value 0.762 Shapiro Wilk Critical Value 0.762

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.181   90% UTL with   90% Coverage 1.226

   90% UPL (t) 1.061   90% UPL (t) 1.072

90% Percentile (z) 1.016 90% Percentile (z) 1.019

95% Percentile (z) 1.057 95% Percentile (z) 1.067

99% Percentile (z) 1.134 99% Percentile (z) 1.163

Gamma Distribution Test Data Distribution Test

k star 30.92 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0282

MLE of Mean 0.872

MLE of Standard Deviation 0.157

nu star 309.2

A‐D Test Statistic 0.771 Nonparametric Statistics

5% A‐D Critical Value 0.678 90% Percentile 0.996

K‐S Test Statistic 0.36 95% Percentile 0.998

5% K‐S Critical Value 0.357 99% Percentile 1

Data not Gamma Distributed at 5% Significance Level

Mass. UPL Results 179
Assuming Gamma Distribution   90% UTL with   90% Coverage 1

90% Percentile 1.078   90% Percentile Bootstrap UTL with   90% Coverage 1

95% Percentile 1.145   90% BCA Bootstrap UTL with   90% Coverage 1

99% Percentile 1.278   90% UPL 1

  90% Chebyshev UPL 1.242

   90% WH Approx. Gamma UPL 1.068 Upper Threshold Limit Based upon IQR 1.29

   90% HW Approx. Gamma UPL 1.069

   90% WH Approx. Gamma UTL with   90% Coverage 1.209

   90% HW Approx. Gamma UTL with   90% Coverage 1.213

Total Metals

General Statistics

Total Number of Observations 60 Number of Distinct Observations 60

Raw Statistics Log‐Transformed Statistics

Minimum 8.01 Minimum 2.081

Maximum 466.4 Maximum 6.145

Second Largest 462.5 Second Largest 6.137

First Quartile 85.93 First Quartile 4.454

Median 141.6 Median 4.953

Third Quartile 275.5 Third Quartile 5.617

Mean 182.4 Mean 4.839

SD 136.1 SD 0.989

Coefficient of Variation 0.747

Skewness 0.739

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.146 Lilliefors Test Statistic 0.113

Lilliefors Critical Value 0.114 Lilliefors Critical Value 0.114

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 390.1   90% UTL with   90% Coverage 571.8

   90% UPL (t) 360.3   90% UPL (t) 460.3

90% Percentile (z) 356.9 90% Percentile (z) 449

95% Percentile (z) 406.3 95% Percentile (z) 643.2

99% Percentile (z) 499.1 99% Percentile (z) 1262

Gamma Distribution Test Data Distribution Test

k star 1.442 Data appear Gamma Distributed at 5% Significance Level

Theta Star 126.4

MLE of Mean 182.4

MLE of Standard Deviation 151.9

nu star 173.1

A‐D Test Statistic 0.384 Nonparametric Statistics

5% A‐D Critical Value 0.769 90% Percentile 391.8

K‐S Test Statistic 0.0782 95% Percentile 460

5% K‐S Critical Value 0.117 99% Percentile 464.1

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 442.1

90% Percentile 383.7   90% Percentile Bootstrap UTL with   90% Coverage 460

Mass. UPL Results 180
95% Percentile 481.3   90% BCA Bootstrap UTL with   90% Coverage 443.9

99% Percentile 702.5   90% UPL 419.9

  90% Chebyshev UPL 594.2

   90% WH Approx. Gamma UPL 385.4 Upper Threshold Limit Based upon IQR 559.8

   90% HW Approx. Gamma UPL 396.1

   90% WH Approx. Gamma UTL with   90% Coverage 441.5

   90% HW Approx. Gamma UTL with   90% Coverage 460

Chloride

General Statistics

Total Number of Observations 20 Number of Distinct Observations 20

Raw Statistics Log‐Transformed Statistics

Minimum 46.6 Minimum 3.842

Maximum 178.4 Maximum 5.184

Second Largest 165 Second Largest 5.106

First Quartile 71 First Quartile 4.262

Median 94.2 Median 4.544

Third Quartile 139.5 Third Quartile 4.937

Mean 104.3 Mean 4.569

SD 41.37 SD 0.411

Coefficient of Variation 0.397

Skewness 0.341

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.929 Shapiro Wilk Test Statistic 0.948

Shapiro Wilk Critical Value 0.905 Shapiro Wilk Critical Value 0.905

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 177.3   90% UTL with   90% Coverage 199.4

   90% UPL (t) 160.6   90% UPL (t) 168.8

90% Percentile (z) 157.3 90% Percentile (z) 163.4

95% Percentile (z) 172.4 95% Percentile (z) 189.8

99% Percentile (z) 200.6 99% Percentile (z) 251.2

Gamma Distribution Test Data Distribution Test

k star 5.61 Data appear Normal at 5% Significance Level

Theta Star 18.59

MLE of Mean 104.3

MLE of Standard Deviation 44.04

nu star 224.4

A‐D Test Statistic 0.434 Nonparametric Statistics

5% A‐D Critical Value 0.744 90% Percentile 156

K‐S Test Statistic 0.121 95% Percentile 165.7

5% K‐S Critical Value 0.194 99% Percentile 175.9

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 165

90% Percentile 163.2   90% Percentile Bootstrap UTL with   90% Coverage 166.3

95% Percentile 185.7   90% BCA Bootstrap UTL with   90% Coverage 166.3

99% Percentile 232.9   90% UPL 164

  90% Chebyshev UPL 231.5

Mass. UPL Results 181
   90% WH Approx. Gamma UPL 164.9 Upper Threshold Limit Based upon IQR 242.3

   90% HW Approx. Gamma UPL 165.7

   90% WH Approx. Gamma UTL with   90% Coverage 188.9

   90% HW Approx. Gamma UTL with   90% Coverage 191.1

Fluoride

General Statistics

Total Number of Observations 30 Number of Distinct Observations 29

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 10.3 Minimum 2.332

Maximum 37.7 Maximum 3.63

Second Largest 33.9 Second Largest 3.523

First Quartile 13.6 First Quartile 2.61

Median 18.05 Median 2.893

Third Quartile 27.48 Third Quartile 3.309

Mean 20.21 Mean 2.932

SD 8.118 SD 0.388

Coefficient of Variation 0.402

Skewness 0.722

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.89 Shapiro Wilk Test Statistic 0.935

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 33.66   90% UTL with   90% Coverage 35.69

   90% UPL (t) 31.03   90% UPL (t) 31.48

90% Percentile (z) 30.61 90% Percentile (z) 30.85

95% Percentile (z) 33.56 95% Percentile (z) 35.53

99% Percentile (z) 39.09 99% Percentile (z) 46.29

Gamma Distribution Test Data Distribution Test

k star 6.226 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 3.246

MLE of Mean 20.21

MLE of Standard Deviation 8.098

nu star 373.5

A‐D Test Statistic 0.789 Nonparametric Statistics

5% A‐D Critical Value 0.746 90% Percentile 32

K‐S Test Statistic 0.136 95% Percentile 33.86

5% K‐S Critical Value 0.16 99% Percentile 36.6

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 33.9

90% Percentile 31.03   90% Percentile Bootstrap UTL with   90% Coverage 33.9

95% Percentile 35.1   90% BCA Bootstrap UTL with   90% Coverage 33.81

99% Percentile 43.63   90% UPL 33.6

  90% Chebyshev UPL 44.96

   90% WH Approx. Gamma UPL 31.21 Upper Threshold Limit Based upon IQR 48.29

   90% HW Approx. Gamma UPL 31.26

Mass. UPL Results 182
   90% WH Approx. Gamma UTL with   90% Coverage 34.72

   90% HW Approx. Gamma UTL with   90% Coverage 34.93

Total Halogens

General Statistics

Total Number of Observations 30 Number of Distinct Observations 29

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 13.3 Minimum 2.588

Maximum 194.6 Maximum 5.271

Second Largest 184.6 Second Largest 5.218

First Quartile 32.3 First Quartile 3.475

Median 84.17 Median 4.433

Third Quartile 141.6 Third Quartile 4.953

Mean 89.75 Mean 4.189

SD 59.62 SD 0.889

Coefficient of Variation 0.664

Skewness 0.26

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.911 Shapiro Wilk Test Statistic 0.882

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 188.5   90% UTL with   90% Coverage 287.8

   90% UPL (t) 169.2   90% UPL (t) 215.8

90% Percentile (z) 166.2 90% Percentile (z) 206.1

95% Percentile (z) 187.8 95% Percentile (z) 284.7

99% Percentile (z) 228.5 99% Percentile (z) 521.9

Gamma Distribution Test Data Distribution Test

k star 1.617 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 55.49

MLE of Mean 89.75

MLE of Standard Deviation 70.57

nu star 97.05

A‐D Test Statistic 0.883 Nonparametric Statistics

5% A‐D Critical Value 0.761 90% Percentile 174.4

K‐S Test Statistic 0.144 95% Percentile 180.4

5% K‐S Critical Value 0.162 99% Percentile 191.7

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 184.6

90% Percentile 183.6   90% Percentile Bootstrap UTL with   90% Coverage 184.6

95% Percentile 228   90% BCA Bootstrap UTL with   90% Coverage 184.6

99% Percentile 327.7   90% UPL 175.2

  90% Chebyshev UPL 271.6

   90% WH Approx. Gamma UPL 187.4 Upper Threshold Limit Based upon IQR 305.6

   90% HW Approx. Gamma UPL 192.3

   90% WH Approx. Gamma UTL with   90% Coverage 226

   90% HW Approx. Gamma UTL with   90% Coverage 236.2

Mass. UPL Results 183
MDL 6/14/2002 7/2/2002 7/16/2002 8/20/2002 10/1/2002 10/25/2002 2/1/2003 2/11/2003 3/31/2003

Components

‐‐ 12.6 3.9 6.5 8.3 15.13 16.6 3.9 22.4 21.7

‐‐ 4.347826087 5.202913632 4.171122995 5.452562704 3.416990692 2.673860911 4.786680541 3.092783505 3.575989783

‐‐ 0.148741419 0.208116545 0.213903743 0.119956379 0.106044539 0.047961631 0.083246618 0.06443299 0.178799489

‐‐ 9330.663616 8455.775234 8308.02139 8095.965104 8707.4349 8383.693046 8328.824142 9292.525773 9206.896552

Metals (mg/kg)

‐‐ 2.288329519 0.104058273 0.983957219 3.947655398 1.767408978 3.717026379 5.202913632 6.443298969 4.853128991

‐‐ 0.343249428 0.1144641 0.171122995 0.14176663 0.353481796 0.035971223 0.020811655 0.180412371 0.217113665

‐‐ 2.860411899 2.185223725 2.780748663 12.54089422 10.01531754 2.877697842 13.94380853 13.65979381 4.980842912

‐‐ 10.64073227 5.93132154 22.99465241 5.997818975 6.480499588 0.839328537 23.30905307 5.927835052 9.45083014

‐‐

Total Metals (mg/kg) ‐‐ 16.1 8.3 26.9 22.6 18.6 7.5 42.5 26.2 19.5

Ions

‐‐ 800.0 1700.0 1400.0 1100.0 1000.0 400.0 1300.0 830.0 1000.0

‐‐

Total Halogens (mg/kg) ‐‐ 800.0 1700.0 1400.0 1100.0 1000.0 400.0 1300.0 830.0 1000.0

* All 90% UPL Results reported as Normal MRL = Method Reporting Limit

** 90% UPL Result reported as Lognormal MDL = Method Detection Limit

*** 90% UPL Result Non‐Parametric HAP = Hazardous Air Pollutant

‐‐ = Non‐Detect OH = Organic Halogen

n.d. = Only 1 Distinct Value, therefore no variance. N = Nitrogenated

Lead  (HAP)

Chromium  (HAP)

Cadmium  (HAP)

Fluorine (mg/kg)

Chlorine (mg/kg)

Mercury  (HAP)

Moisture (wt%)

Arsenic  (HAP)

Heating Value (BTU/lb)

Sulfur (wt%)

Ash (wt%)

NY C&D Summary Table 184
4/15/2003 5/13/2003 6/29/2003 7/15/2003 8/31/2003 9/12/2003 9/16/2003 9/24/2003 10/29/2003 11/21/2003 11/28/2003 12/5/2003 12/11/2003 12/22/2003

12.4 22.5 13.86 6.55 8.6 11.1 13 12.3 13.3 16.9 16.9 18.4 21.8 22.5

4.566210046 5.935483871 4.52751335 4.173354735 3.938730853 13.27334083 9.609195402 4.561003421 9.457900807 3.610108303 7.34055355 3.06372549 3.516624041 10.4516129

0.159817352 0.193548387 0.023218017 0.064205457 0.131291028 0.114942529 0.045610034 0.034602076 0.048134777 0.096269555 0.049019608 0.076726343 0.180645161

9028.538813 8335.483871 9283.72417 8240.770465 8718.818381 7599.550056 7780.45977 8746.86431 8238.754325 8389.891697 8932.611312 9291.666667 8207.161125 8477.419355

2.168949772 1.612903226 0.656455142 18.22272216 37.47126437 6.157354618 82.12226067 2.406738869 12.39470517 12.74509804 4.859335038 6.967741935

0.057077626 0.090322581 0.010448108 0.321027287 0.098468271 0.899887514 0.091954023 0.07981756 0.265282584 0.048134777 0.048134777 0.526960784 0.127877238 0.180645161

5.479452055 4.116129032 7.778035756 21.08079187 3.938730853 41.73228346 0.574712644 7.753705815 76.93194925 2.767749699 6.618531889 16.05392157 5.115089514 11.48387097

2.96803653 7.870967742 3.830972835 2.140181915 5.689277899 19.91001125 5.977011494 4.104903079 21.22260669 3.128760529 22.38267148 5.637254902 0.511508951 19.22580645

10.7 13.7 11.6 23.5 10.4 80.8 44.1 18.1 180.5 8.4 41.4 35.0 10.6 37.9

1400.0 1500.0 1300.0 600.0 700.0 1100.0 1300.0 1100.0 600.0 1000.0 700.0 500.0

1400.0 1500.0 1300.0 600.0 700.0 1100.0 1300.0 1100.0 600.0 1000.0 700.0 500.0

NY C&D Summary Table 185
12/26/2003 1/2/2004 1/23/2004 1/30/2004 2/6/2004 2/13/2004 3/8/2004 3/19/2004 3/26/2004 4/2/2004 4/23/2004 4/30/2004 5/7/2004 5/14/2004

22.2 5.5 17.9 16.6 19.2 15.1 14.3 10.7 19.2 15.4 19.8 15.4 12.2 15.9

5.912596401 9.312169312 4.263093788 2.997601918 3.465346535 6.360424028 7.584597433 9.070548712 6.559405941 7.446808511 4.613466334 2.836879433 6.378132118 3.210463734

0.115681234 0.105820106 0.097442144 0.131894484 0.123762376 0.176678445 0.233372229 0.235162374 0.198019802 0.141843972 0.124688279 0.082742317 0.148063781 0.118906064

8962.724936 8271.957672 10669.91474 11699.04077 9297.029703 8935.217903 7987.164527 7573.348264 9017.326733 8034.27896 8284.289277 8427.895981 8690.205011 8694.411415

3.084832905 4.973544974 27.77101096 2.398081535 13.73762376 0.11778563 4.434072345 1.231802912 4.702970297 26.8321513 18.82793017 2.836879433 3.758542141 4.042806183

0.28277635 0.126984127 0.146163216 0.095923261 0.061881188 0.23557126 0.058343057 1.11982E‐06 0.04950495 1.773049645 0.049875312 0.165484634 0.148063781 0.344827586

7.197943445 10.05291005 44.94518879 11.99040767 12.9950495 10.83627797 12.25204201 12.87793953 9.034653465 37.35224586 20.69825436 5.319148936 8.54214123 7.372175981

7.326478149 33.22751323 6.577344702 16.30695444 6.559405941 14.01648999 12.48541424 12.87793953 13.36633663 31.32387707 5.236907731 5.082742317 19.36218679 6.420927467

17.9 48.4 79.4 30.8 33.4 25.2 29.2 27.0 27.2 97.3 44.8 13.4 31.8 18.2

1800.0 2100.0 800.0 600.0 800.0 1100.0 1600.0 1700.0 1200.0 1100.0 1100.0 800.0 900.0 900.0

1800.0 2100.0 800.0 600.0 800.0 1100.0 1600.0 1700.0 1100.0 1100.0 800.0 900.0 900.0

NY C&D Summary Table 186
6/11/2004 6/19/2004 7/2/2004 7/16/2004 8/6/2004 8/15/2004 9/10/2004 9/17/2004 9/25/2004 10/8/2004 10/16/3453 10/29/2004 11/5/2004 11/12/2004

14.8 13.8 13.9 17 16.6 14.5 15.3 16 15 10.7 10.2 11 15.7 15.6

2.816901408 2.900232019 2.555168409 2.168674699 2.637889688 9.941520468 2.609208973 2.142857143 2.117647059 1.903695409 1.781737194 2.808988764 10.6405694 14.69194313

0.082159624 0.023201856 0.104529617 0.084337349 0.035971223 0.128654971 0.070838253 0.05952381 0.058823529 0.055991041 0.04454343 0.02247191 0.09489917 0.130331754

8816.901408 8800.464037 8577.235772 8530.120482 9224.220624 7857.309942 9213.695396 8267.857143 9077.647059 9359.462486 9230.512249 9165.168539 8465.005931 8581.753555

0.117370892 2.784222738 8.943089431 12.28915663 29.13669065 19.76608187 4.604486423 9.285714286 4 15.6774916 10.91314031 4.606741573 2.384341637 2.725118483

0.14084507 0.35962877 0.301974448 0.192771084 0.20383693 0.807017544 1.074380165 0.05952381 0.105882353 0.134378499 0.178173719 0.078651685 0.403321471 0.248815166

4.225352113 19.37354988 12.77584204 17.22891566 42.92565947 28.65497076 8.854781582 14.16666667 11.17647059 17.46920493 22.04899777 18.87640449 70.22538553 127.014218

9.154929577 81.67053364 7.317073171 7.951807229 8.872901679 44.32748538 5.430932704 3.80952381 10 176.9316909 15.14476615 3.483146067 15.18386714 39.21800948

13.6 104.2 29.3 37.7 81.1 93.6 20.0 27.3 25.3 210.2 48.3 27.0 88.2 169.2

600.0 700.0 700.0 700.0 700.0 700.0 1100.0 1100.0 1100.0 1700.0 700.0 700.0 794.0 856.0

600.0 700.0 700.0 700.0 700.0 700.0 1100.0 1100.0 1100.0 1700.0 700.0 700.0 794.0 856.0

NY C&D Summary Table 187
11/19/2004 2/11/2005 2/18/2005 2/25/2005 5/6/2005 5/21/2005 5/27/2005 6/19/2005 9/9/2005 9/23/2005 1/29/2006 2/11/2006 2/17/2006 2/24/2006

16.4 23.7 18.2 9.1 22.6 11.5 13 15.9 13.9 15.8 12.5 24.3 33 21.2

3.349282297 2.621231979 2.811735941 8.03080308 6.072351421 2.033898305 2.298850575 1.664684899 7.200929152 4.86935867 3.12 10.33025099 20 6.472081218

0.107655502 0.131061599 0.097799511 0.154015402 0.19379845 0.09039548 0.057471264 0.047562426 0.034843206 0.059382423 0.022857143 0.026420079 0.029850746 0.025380711

9232.057416 9251.63827 9172.371638 7388.338834 8727.390181 8700.564972 9174.712644 9199.762188 7620.209059 8072.446556 8352 7552.179657 6662.686567 8220.812183

32.41626794 0.655307995 0.855745721 3.740374037 2.842377261 1.355932203 0.689655172 5.469678954 3.948896632 29.57244656 17.37142857 18.09775429 7.611940299 3.807106599

0.825358852 0.01310616 0.097799511 0.231023102 0.103359173 0.011299435 0.068965517 0.011890606 0.081300813 0.106888361 0.331428571 0.066050198 0.208955224 0.025380711

58.73205742 4.98034076 4.88997555 13.09130913 11.24031008 6.327683616 7.126436782 10.22592152 16.37630662 42.75534442 49.6 44.64993395 31.64179104 23.73096447

3.468899522 1.31061599 4.645476773 17.16171617 10.85271318 1.242937853 2.988505747 1.070154578 11.96283391 14.60807601 2.857142857 18.09775429 12.3880597 4.822335025

95.4 7.0 10.5 34.2 25.0 8.9 10.9 16.8 32.4 87.0 70.2 80.9 51.9 32.4

900.0 1600.0 1000.0 1500.0 1900.0 1600.0 800.0 600.0 900.0 1600.0 1500.0 1500.0 900.0 900.0

900.0 1600.0 1000.0 1500.0 1900.0 1600.0 800.0 600.0 900.0 1600.0 1500.0 1500.0 900.0 900.0

NY C&D Summary Table 188
3/3/2006 3/13/2006 3/24/2006 3/31/2006 5/17/2006 6/17/2006 6/24/2006 11/28/2006 10/30/2006 12/23/2006 11/28/2006 10/30/2006 12/23/2006 5/2/2007

24.3 29.1 25.7 21.54 11.3 10.8 13.3 30 24.3 27.9 26.34 21.52 22.91 20.34

4.227212682 10.86036671 8.748317631 5.9010961 9.24464487 5.829596413 3.921568627 6.171428571 9.64332893 5.131761442 13.30437144 4.689092762 13.52964068 3.288978157

0.026420079 0.028208745 0.040376851 0.038236044 0.033821871 0.044843049 0.023068051 0.071428571 0.264200793 0.041608877 0.054303557 0.0509684 0.038915553 0.037660055

8441.215324 7296.191819 7858.681023 8130.257456 7597.519729 8041.479821 8126.874279 8040 8025.099075 7593.619972 7097.474885 8019.877676 7745.492282 8306.55285

22.06076618 4.019746121 4.710632571 2.803976549 14.65614431 15.80717489 11.64936563 7.5 6.869220608 12.20527046 10.72495248 2.53567788 3.982358283 3.803665579

0.488771466 0.112834979 0.349932705 0.522559266 0.225479143 0.67264574 0.080738178 0.071428571 0.079260238 0.097087379 0.067879446 0.089194699 0.285380724

56.40686922 72.07334274 126.6487214 29.1868468 34.38556933 32.84753363 24.79815456 29.71428571 16.38044914 59.50069348 68.55824056 21.50866463 35.54287197 8.084358524

4.227212682 3.223856538 26.9179004 14.52969666 21.64599775 132.8475336 7.843137255 16.85714286 24.57067371 10.5409154 36.11186533 23.99337411 31.32702037 13.73336681

0.007000

83.2 79.4 158.6 47.0 70.9 182.2 44.4 54.1 47.9 82.3 115.5 48.1 71.1 25.6

800.0 1000.0 600.0 6460.0 900.0 800.0 600.0 900.0 900.0 800.0 900.0 700.0 737.0 600.0

155.7142857 658.8072122 418.137388 212.7930683 406.0189389 37.66005523

800.0 1000.0 600.0 6460.0 900.0 800.0 600.0 1055.7 900.0 1458.8 1318.1 912.8 1143.0 637.7

New York C&D SUMMARY

NY C&D Summary Table 189
5/3/2007 5/11/2007 10/21/2007 11/17/2007 11/29/2007 12/28/2007 1/4/2008 1/13/2008 1/26/2008 2/15/2008 2/29/2008 3/14/2008 5/16/2008 6/7/2008

21.93 19.16 11.3 15.9 16.6 14.8 28.8 30.8 32.7 38 29.1 23.6 20.9 21.9

8.991930319 2.684314696 9.131905299 12.960761 6.954436451 7.511737089 16.99438202 7.225433526 14.48736999 6.290322581 6.064880113 8.376963351 9.102402023 8.706786172

0.05123607 0.037110341 0.1578354 0.035671819 0.215827338 0.058685446 0.224719101 0.144508671 0.044576523 0.032258065 0.042313117 0.078534031 0.02528445 0.038412292

7735.365697 8313.953488 7942.502818 7626.634958 8173.860911 8071.596244 7008.426966 8109.82659 7292.719168 8151.612903 7902.679831 7727.748691 8040.45512 8088.348271

18.53464839 13.33498268 52.64937993 21.75980975 3.717026379 2.112676056 20.92696629 5.057803468 10.54977712 55.16129032 6.064880113 7.19895288 42.09860936 3.969270166

34.90457282 19.56952004 98.30890643 74.31629013 15.58752998 24.76525822 48.03370787 26.15606936 24.21991085 64.67741935 9.873060649 20.02617801 9.102402023 25.60819462

37.82502882 16.5759525 27.28297632 36.74197384 12.82973621 62.44131455 39.04494382 28.03468208 77.86032689 43.22580645 34.69675599 35.60209424 7.079646018 86.6837388

0.035000 0.016000 0.051000 0.049000 0.035000 0.096000 0.080000 0.060000 0.010000 0.008000 0.010000 0.100000 0.130000 0.140000

91.3 49.5 178.3 132.9 32.2 89.4 108.1 59.3 112.6 163.1 50.6 62.9 58.4 116.4

1900.0 900.0 653.0 640.0 895.0 1000.0 970.0 900.0 1115.0 800.0 800.0 900.0 1200.0 1400.0

256.180351 123.7011381

2156.2 1023.7 653.0 640.0 895.0 1000.0 970.0 900.0 1115.0 800.0 800.0 900.0 1200.0 1400.0

NY C&D Summary Table 190
9/26/2008 11/23/2008 12/19/2008 1/11/2009 2/1/2009 2/13/2009 3/13/2009 3/20/2009 4/25/2009 5/1/2009 8/18/2009 8/30/2009 11/13/2009 11/20/2009

30.8 15.5 18.16 16.1 24.2 29.2 32.7 30.3 21.6 25.29 14.18 19.3 15.33 16.18

9.176300578 5.727810651 3.103616813 8.057210965 7.519788918 3.531073446 9.955423477 3.299856528 4.655612245 6.960246286 2.854812398 2.688971499 4.806897366 4.533524219

0.187861272 0.071005917 0.097751711 0.10727056 0.105540897 0.056497175 0.14858841 0.086083214 0.114795918 0.174006157 0.069913773 0.074349442 0.035431676 0.035790981

7955.202312 8285.207101 8583.822092 7938.021454 8307.387863 8435.028249 7989.598811 8358.680057 8321.428571 8064.516129 8606.385458 8731.10285 8505.964332 8569.553806

51.01156069 4.118343195 3.164711632 110.0595948 15.96306069 42.94205052 16.92969871 18.1122449 10.97577299 1.246795619 2.09417596 1.936931617 1.562872823

64.45086705 6.343195266 7.221407625 110.977354 10.81794195 60.77265973 31.56384505 44.13265306 29.58104671 0.69913773 4.708798017 1.440888154 1.562872823

82.51445087 26.37869822 13.36754643 14.97020262 8.311345646 70.43090639 14.63414634 63.52040816 98.7819569 2.913073876 2.726146221 0.649580725 0.978286805

0.052000 0.048000 0.028000 0.077000 0.009000 0.013000 0.026000 0.076000 0.307000 0.026000 0.012000 0.080000 0.053000

198.0 36.9 23.8 236.1 35.1 174.2 63.2 125.8 139.6 4.9 9.5 4.1 4.2

820.0 760.0 675.0 9940.0 640.0 2200.0 1300.0 1800.0 1300.0 1500.0 900.0 980.0 1000.0 1000.0

820.0 760.0 675.0 9940.0 640.0 2200.0 1300.0 1800.0 1300.0 1500.0 900.0 980.0 1000.0 1000.0

NY C&D Summary Table 191
12/12/2009 12/18/2009 2/15/2010 3/14/2010 3/21/2010 3/29/2010 4/26/2010 4/30/2010 8/15/2010 8/17/2010 8/27/2010 10/12/2010 10/22/2010 10/27/2010

15.8 18 20.2 23.8 22.4 23.2 20.2 23.93 13.8 17.16 21.88 16.4 20.03 22.37

3.491686461 3.536585366 5.263157895 5.118110236 3.608247423 2.473958333 4.260651629 4.206651768 3.480278422 4.73201352 4.838709677 6.722488038 8.078029261 7.175061188

0.035629454 0.109756098 0.288220551 0.052493438 0.038659794 0.065104167 0.062656642 0.144603655 0.046403712 0.060357315 0.038402458 0.179425837 0.200075028 0.141697797

8578.384798 8363.414634 8746.867168 8625.984252 8487.113402 8196.614583 8397.243108 6969.896148 8561.484919 8611.781748 8475.422427 8234.449761 8623.233713 8478.680922

15.91448931 30.24390244 27.56892231 10.76115486 10.69587629 5.338541667 2.882205514 7.098724859 8.816705336 5.359729599 12.41679467 14.19856459 11.92947355 8.823908283

12.82660333 29.87804878 23.55889724 13.12335958 12.88659794 7.552083333 4.761904762 11.17391876 12.6450116 7.436021246 18.68919611 18.39712919 16.74377892 13.7189231

23.63420428 27.31707317 18.29573935 38.58267717 14.04639175 23.828125 18.42105263 35.62508216 15.19721578 18.50555287 92.67793139 50.89712919 115.0306365 139.1730001

0.100000 0.260000 0.005000 0.005000 0.005000 0.005000 0.076000 0.220000 0.170000 0.135000 0.160000 0.130000 0.212000 0.127000

52.5 87.7 69.4 62.5 37.6 36.7 26.1 54.1 36.8 31.4 123.9 83.6 143.9 161.8

2000.0 2100.0 1300.0 600.0 500.0 900.0 700.0 2200.0 300.0 857.0 820.0 692.0 645.0 569.0

2000.0 2100.0 1300.0 600.0 500.0 900.0 700.0 2200.0 300.0 857.0 820.0 692.0 645.0 569.0

NY C&D Summary Table 192
12/31/2010 1/31/2011 2/20/2011 4/13/2011 4/8/2011 4/22/2011 5/21/2011 5/27/2011 6/4/2011 8/12/2011 9/30/2011 10/21/2011 11/15/2011 1/29/2012

26.6 30.23 33.39 28.4 31.18 28.81 21.64 29.22 38.5 32.27 28.12 21.8 28.93 18.27

7.820163488 5.145477999 11.57483861 6.075418994 8.660273176 4.677623262 3.177641654 5.495902797 3.821138211 6.0239185 16.16583194 10.2685422 15.46362741 4.649455524

0.190735695 0.214992117 0.165140369 0.083798883 0.087183958 0.04214075 0.063808065 0.127154563 0.146341463 0.132880555 0.083472454 0.051150895 0.126635711 0.159060321

8782.016349 9217.428694 8455.186909 8593.575419 8204.010462 8502.59868 8786.370597 8506.640294 8497.560976 8290.27019 7591.819699 8135.549872 8262.276629 8557.445247

3.514986376 1.662605704 4.023419907 25.89385475 26.30049404 1.23612867 0.280755487 6.357728172 13.39837398 12.10689502 23.12186978 17.03324808 2.72970311 13.83824789

8.147138965 2.508241364 7.236150728 36.22905028 40.39523394 5.183312263 0.204185809 15.28680418 27.41463415 17.17112063 9.59933222 20.97186701 5.895595891 17.44769363

34.60490463 10.69227462 12.70079568 22.5 261.4065679 21.99747155 0.382848392 26.9991523 135.5772358 41.50302672 20.67334446 14.34782609 21.79541297 43.65594029

0.026000 0.036000 0.045000 0.146000 0.229000 0.128000 0.076000 0.154000 0.156000 0.089000 0.062000 0.097000 0.146000 0.079000

46.3 14.9 24.0 84.8 328.3 28.5 0.9 48.8 176.5 70.9 53.5 52.4 30.6 75.0

586.0 374.0 500.0 584.0 482.0 656.0 460.0 500.0 1870.0 514.0 310.0 341.0 145.0 400.0

586.0 374.0 500.0 584.0 482.0 656.0 460.0 500.0 1870.0 514.0 310.0 341.0 145.0 400.0

NY C&D Summary Table 193
*all results reported as moisture free

*all results pooled from all 7 samples

2/9/2012 3/2/2012 4/21/2012 4/27/2012 5/4/2012 Non‐

Detect Average StandardDeviation Low High

27.2 20.16 38.5 23.35 34.01 0 19.68 7.29 3.90 38.5 31.26**

1.373626374 2.830661323 11.90243902 1.604696673 7.440521291 0 6.11 3.57 1.37 20 10.84**

0.151098901 0.175350701 0.097560976 0.039138943 0.106076678 1 0.10 0.06 0.02 0.288 0.191***

8336.538462 8772.54509 8211.382114 8468.362688 8140.627368 0 8408.87 632.47 6662.69 11699.041 9213***

2.678571429 14.95490982 7.154471545 6.484018265 23.3065616 3 11.94 15.18 0.10 110.06 31.64**

62 0.23 0.28 0.00 1.77 0.523***

3.626373626 28.54458918 46.50406504 12.00260926 40.44552205 1 23.47 24.05 0.20 127.01 58.44**

4.162087912 21.54308617 18.37398374 22.30919765 22.47310199 1 26.23 36.09 0.4 261.4 63.52***

0.054000 0.063000 0.300000 0.070000 0.161000 79 0.09 0.07 0.005 0.31 0.204***

10.5 65.1 72.3 40.9 86.4 ‐‐ 61.63 54.8 0.94 328 145**

508.0 460.0 400.0 1100.0 4290.0 2 1097.30 1029.38 145 9940 1710***

132 283.63 200.73 38 659 584.9*

508.0 460.0 400.0 1100.0 4290.0 ‐‐ 1113.12 1033.60 145.00 9940.0 1720***

Range 90% UPL

Results*

NY C&D Summary Table 194
Moisture (wt%) Ash (wt%) Sulfur (wt%) Heating Value (BTU/lb) Arsenic  (HAP) Cadmium  (HAP)

140 140 139 140 137 78

12.6 4.347826087 0.148741419 9330.663616 2.288329519 0.343249428

3.9 5.202913632 0.208116545 8455.775234 0.104058273 0.1144641

6.5 4.171122995 0.213903743 8308.02139 0.983957219 0.171122995

8.3 5.452562704 0.119956379 8095.965104 3.947655398 0.14176663

15.13 3.416990692 0.106044539 8707.4349 1.767408978 0.353481796

16.6 2.673860911 0.047961631 8383.693046 3.717026379 0.035971223

3.9 4.786680541 0.083246618 8328.824142 5.202913632 0.020811655

22.4 3.092783505 0.06443299 9292.525773 6.443298969 0.180412371

21.7 3.575989783 0.178799489 9206.896552 4.853128991 0.217113665

12.4 4.566210046 0.159817352 9028.538813 2.168949772 0.057077626

22.5 5.935483871 0.193548387 8335.483871 1.612903226 0.090322581

13.86 4.52751335 0.023218017 9283.72417 0.010448108

6.55 4.173354735 0.064205457 8240.770465 0.321027287

8.6 3.938730853 0.131291028 8718.818381 0.656455142 0.098468271

11.1 13.27334083 7599.550056 18.22272216 0.899887514

13 9.609195402 0.114942529 7780.45977 37.47126437 0.091954023

12.3 4.561003421 0.045610034 8746.86431 6.157354618 0.07981756

13.3 9.457900807 0.034602076 8238.754325 82.12226067 0.265282584

16.9 3.610108303 0.048134777 8389.891697 2.406738869 0.048134777

16.9 7.34055355 0.096269555 8932.611312 12.39470517 0.048134777

18.4 3.06372549 0.049019608 9291.666667 12.74509804 0.526960784

21.8 3.516624041 0.076726343 8207.161125 4.859335038 0.127877238

22.5 10.4516129 0.180645161 8477.419355 6.967741935 0.180645161

22.2 5.912596401 0.115681234 8962.724936 3.084832905 0.28277635

5.5 9.312169312 0.105820106 8271.957672 4.973544974 0.126984127

17.9 4.263093788 0.097442144 10669.91474 27.77101096 0.146163216

16.6 2.997601918 0.131894484 11699.04077 2.398081535 0.095923261

19.2 3.465346535 0.123762376 9297.029703 13.73762376 0.061881188

15.1 6.360424028 0.176678445 8935.217903 0.11778563 0.23557126

14.3 7.584597433 0.233372229 7987.164527 4.434072345 0.058343057

10.7 9.070548712 0.235162374 7573.348264 1.231802912 1.11982E‐06

19.2 6.559405941 0.198019802 9017.326733 4.702970297 0.04950495

15.4 7.446808511 0.141843972 8034.27896 26.8321513 1.773049645

19.8 4.613466334 0.124688279 8284.289277 18.82793017 0.049875312

15.4 2.836879433 0.082742317 8427.895981 2.836879433 0.165484634

12.2 6.378132118 0.148063781 8690.205011 3.758542141 0.148063781

15.9 3.210463734 0.118906064 8694.411415 4.042806183 0.344827586

14.8 2.816901408 0.082159624 8816.901408 0.117370892 0.14084507

13.8 2.900232019 0.023201856 8800.464037 2.784222738 0.35962877

13.9 2.555168409 0.104529617 8577.235772 8.943089431 0.301974448

17 2.168674699 0.084337349 8530.120482 12.28915663 0.192771084

16.6 2.637889688 0.035971223 9224.220624 29.13669065 0.20383693

14.5 9.941520468 0.128654971 7857.309942 19.76608187 0.807017544

15.3 2.609208973 0.070838253 9213.695396 4.604486423 1.074380165

16 2.142857143 0.05952381 8267.857143 9.285714286 0.05952381

15 2.117647059 0.058823529 9077.647059 4 0.105882353

10.7 1.903695409 0.055991041 9359.462486 15.6774916 0.134378499

10.2 1.781737194 0.04454343 9230.512249 10.91314031 0.178173719

11 2.808988764 0.02247191 9165.168539 4.606741573 0.078651685

15.7 10.6405694 0.09489917 8465.005931 2.384341637 0.403321471

15.6 14.69194313 0.130331754 8581.753555 2.725118483 0.248815166

16.4 3.349282297 0.107655502 9232.057416 32.41626794 0.825358852

23.7 2.621231979 0.131061599 9251.63827 0.655307995 0.01310616

18.2 2.811735941 0.097799511 9172.371638 0.855745721 0.097799511

9.1 8.03080308 0.154015402 7388.338834 3.740374037 0.231023102

22.6 6.072351421 0.19379845 8727.390181 2.842377261 0.103359173

11.5 2.033898305 0.09039548 8700.564972 1.355932203 0.011299435

13 2.298850575 0.057471264 9174.712644 0.689655172 0.068965517

15.9 1.664684899 0.047562426 9199.762188 5.469678954 0.011890606

NY ProUCL Entry 195
13.9 7.200929152 0.034843206 7620.209059 3.948896632 0.081300813

15.8 4.86935867 0.059382423 8072.446556 29.57244656 0.106888361

12.5 3.12 0.022857143 8352 17.37142857 0.331428571

24.3 10.33025099 0.026420079 7552.179657 18.09775429 0.066050198

33 20 0.029850746 6662.686567 7.611940299 0.208955224

21.2 6.472081218 0.025380711 8220.812183 3.807106599 0.025380711

24.3 4.227212682 0.026420079 8441.215324 22.06076618 0.488771466

29.1 10.86036671 0.028208745 7296.191819 4.019746121 0.112834979

25.7 8.748317631 0.040376851 7858.681023 4.710632571 0.349932705

21.54 5.9010961 0.038236044 8130.257456 2.803976549 0.522559266

11.3 9.24464487 0.033821871 7597.519729 14.65614431 0.225479143

10.8 5.829596413 0.044843049 8041.479821 15.80717489 0.67264574

13.3 3.921568627 0.023068051 8126.874279 11.64936563 0.080738178

30 6.171428571 0.071428571 8040 7.5 0.071428571

24.3 9.64332893 0.264200793 8025.099075 6.869220608 0.079260238

27.9 5.131761442 0.041608877 7593.619972 12.20527046 0.097087379

26.34 13.30437144 0.054303557 7097.474885 10.72495248 0.067879446

21.52 4.689092762 0.0509684 8019.877676 2.53567788 0.089194699

22.91 13.52964068 0.038915553 7745.492282 3.982358283 0.285380724

20.34 3.288978157 0.037660055 8306.55285 3.803665579

21.93 8.991930319 0.05123607 7735.365697 18.53464839

19.16 2.684314696 0.037110341 8313.953488 13.33498268

11.3 9.131905299 0.1578354 7942.502818 52.64937993

15.9 12.960761 0.035671819 7626.634958 21.75980975

16.6 6.954436451 0.215827338 8173.860911 3.717026379

14.8 7.511737089 0.058685446 8071.596244 2.112676056

28.8 16.99438202 0.224719101 7008.426966 20.92696629

30.8 7.225433526 0.144508671 8109.82659 5.057803468

32.7 14.48736999 0.044576523 7292.719168 10.54977712

38 6.290322581 0.032258065 8151.612903 55.16129032

29.1 6.064880113 0.042313117 7902.679831 6.064880113

23.6 8.376963351 0.078534031 7727.748691 7.19895288

NY ProUCL Entry 196
20.9 9.102402023 0.02528445 8040.45512 42.09860936

21.9 8.706786172 0.038412292 8088.348271 3.969270166

30.8 9.176300578 0.187861272 7955.202312 51.01156069

15.5 5.727810651 0.071005917 8285.207101 4.118343195

18.16 3.103616813 0.097751711 8583.822092 3.164711632

16.1 8.057210965 0.10727056 7938.021454 110.0595948

24.2 7.519788918 0.105540897 8307.387863 15.96306069

29.2 3.531073446 0.056497175 8435.028249

32.7 9.955423477 0.14858841 7989.598811 42.94205052

30.3 3.299856528 0.086083214 8358.680057 16.92969871

21.6 4.655612245 0.114795918 8321.428571 18.1122449

25.29 6.960246286 0.174006157 8064.516129 10.97577299

14.18 2.854812398 0.069913773 8606.385458 1.246795619

19.3 2.688971499 0.074349442 8731.10285 2.09417596

15.33 4.806897366 0.035431676 8505.964332 1.936931617

16.18 4.533524219 0.035790981 8569.553806 1.562872823

15.8 3.491686461 0.035629454 8578.384798 15.91448931

18 3.536585366 0.109756098 8363.414634 30.24390244

20.2 5.263157895 0.288220551 8746.867168 27.56892231

23.8 5.118110236 0.052493438 8625.984252 10.76115486

22.4 3.608247423 0.038659794 8487.113402 10.69587629

23.2 2.473958333 0.065104167 8196.614583 5.338541667

20.2 4.260651629 0.062656642 8397.243108 2.882205514

23.93 4.206651768 0.144603655 6969.896148 7.098724859

13.8 3.480278422 0.046403712 8561.484919 8.816705336

17.16 4.73201352 0.060357315 8611.781748 5.359729599

21.88 4.838709677 0.038402458 8475.422427 12.41679467

16.4 6.722488038 0.179425837 8234.449761 14.19856459

20.03 8.078029261 0.200075028 8623.233713 11.92947355

22.37 7.175061188 0.141697797 8478.680922 8.823908283

26.6 7.820163488 0.190735695 8782.016349 3.514986376

30.23 5.145477999 0.214992117 9217.428694 1.662605704

33.39 11.57483861 0.165140369 8455.186909 4.023419907

28.4 6.075418994 0.083798883 8593.575419 25.89385475

31.18 8.660273176 0.087183958 8204.010462 26.30049404

28.81 4.677623262 0.04214075 8502.59868 1.23612867

21.64 3.177641654 0.063808065 8786.370597 0.280755487

29.22 5.495902797 0.127154563 8506.640294 6.357728172

38.5 3.821138211 0.146341463 8497.560976 13.39837398

32.27 6.0239185 0.132880555 8290.27019 12.10689502

28.12 16.16583194 0.083472454 7591.819699 23.12186978

21.8 10.2685422 0.051150895 8135.549872 17.03324808

28.93 15.46362741 0.126635711 8262.276629 2.72970311

18.27 4.649455524 0.159060321 8557.445247 13.83824789

27.2 1.373626374 0.151098901 8336.538462 2.678571429

20.16 2.830661323 0.175350701 8772.54509 14.95490982

38.5 11.90243902 0.097560976 8211.382114 7.154471545

23.35 1.604696673 0.039138943 8468.362688 6.484018265

34.01 7.440521291 0.106076678 8140.627368 23.3065616

NY ProUCL Entry 197
Chromium  (HAP) Lead  (HAP) Mercury  (HAPTotal Metals (mg/kg) Chlorine (mg/kg) Fluorine (mg/kg) Total Halogens (mg/kg)

139 139 61 139 138 8 137

2.860411899 10.64073227 16.13272311 800 800

2.185223725 5.93132154 8.335067638 1700 1700

2.780748663 22.99465241 26.93048128 1400 1400

12.54089422 5.997818975 22.62813522 1100 1100

10.01531754 6.480499588 18.61670791 1000 1000

2.877697842 0.839328537 7.470023981 400 400

13.94380853 23.30905307 42.47658689 1300 1300

13.65979381 5.927835052 26.21134021 830 830

4.980842912 9.45083014 19.50191571 1000 1000

5.479452055 2.96803653 10.67351598 1400 1400

4.116129032 7.870967742 13.69032258 1500 1500

7.778035756 3.830972835 11.6194567 1300 1300

21.08079187 2.140181915 23.54200107 600 600

3.938730853 5.689277899 10.38293217 700 700

41.73228346 19.91001125 80.76490439

0.574712644 5.977011494 44.11494253 1100 1100

7.753705815 4.104903079 18.09578107 1300 1300

76.93194925 21.22260669 180.5420992 1100 1100

2.767749699 3.128760529 8.351383875 600 600

6.618531889 22.38267148 41.44404332 1000 1000

16.05392157 5.637254902 34.96323529 700 700

5.115089514 0.511508951 10.61381074 500 500

11.48387097 19.22580645 37.85806452

7.197943445 7.326478149 17.89203085 1800 1800

10.05291005 33.22751323 48.38095238 2100 2100

44.94518879 6.577344702 79.43970767 800 800

11.99040767 16.30695444 30.79136691 600 600

12.9950495 6.559405941 33.3539604 800 800

10.83627797 14.01648999 25.20612485 1100 1100

12.25204201 12.48541424 29.22987165 1600 1600

12.87793953 12.87793953 26.98768309 1700 1700

9.034653465 13.36633663 27.15346535 1200

37.35224586 31.32387707 97.28132388 1100 1100

20.69825436 5.236907731 44.81296758 1100 1100

5.319148936 5.082742317 13.40425532 800 800

8.54214123 19.36218679 31.81093394 900 900

7.372175981 6.420927467 18.18073722 900 900

4.225352113 9.154929577 13.63849765 600 600

19.37354988 81.67053364 104.187935 700 700

12.77584204 7.317073171 29.33797909 700 700

17.22891566 7.951807229 37.6626506 700 700

42.92565947 8.872901679 81.13908873 700 700

28.65497076 44.32748538 93.55555556 700 700

8.854781582 5.430932704 19.96458087 1100 1100

14.16666667 3.80952381 27.32142857 1100 1100

11.17647059 10 25.28235294 1100 1100

17.46920493 176.9316909 210.212766 1700 1700

22.04899777 15.14476615 48.28507795 700 700

18.87640449 3.483146067 27.04494382 700 700

70.22538553 15.18386714 88.19691578 794 794

127.014218 39.21800948 169.2061611 856 856

58.73205742 3.468899522 95.44258373 900 900

4.98034076 1.31061599 6.959370904 1600 1600

4.88997555 4.645476773 10.48899756 1000 1000

13.09130913 17.16171617 34.22442244 1500 1500

11.24031008 10.85271318 25.03875969 1900 1900

6.327683616 1.242937853 8.937853107 1600 1600

7.126436782 2.988505747 10.87356322 800 800

10.22592152 1.070154578 16.77764566 600 600

NY ProUCL Entry 198
16.37630662 11.96283391 32.36933798 900 900

42.75534442 14.60807601 87.04275534 1600 1600

49.6 2.857142857 70.16 1500 1500

44.64993395 18.09775429 80.91149273 1500 1500

31.64179104 12.3880597 51.85074627 900 900

23.73096447 4.822335025 32.3857868 900 900

56.40686922 4.227212682 83.18361955 800 800

72.07334274 3.223856538 79.42978037 1000 1000

126.6487214 26.9179004 158.6271871 600 600

29.1868468 14.52969666 47.04307928 6460 6460

34.38556933 21.64599775 70.91319053 900 900

32.84753363 132.8475336 182.1748879 800 800

24.79815456 7.843137255 44.37139562 600 600

29.71428571 16.85714286 54.14285714 900 155.7142857 1055.714286

16.38044914 24.57067371 47.8996037 900 900

59.50069348 10.5409154 82.34396671 800 658.8072122 1458.807212

68.55824056 36.11186533 115.4629378 900 418.137388 1318.137388

21.50866463 23.99337411 48.12691131 700 212.7930683 912.7930683

35.54287197 31.32702037 71.13763134 737 406.0189389 1143.018939

8.084358524 13.73336681 0.007 25.62839091 600 37.66005523 637.6600552

34.90457282 37.82502882 0.035 91.29925003 1900 256.180351 2156.180351

19.56952004 16.5759525 0.016 49.49645522 900 123.7011381 1023.701138

98.30890643 27.28297632 0.051 178.2922627 653 653

74.31629013 36.74197384 0.049 132.8670737 640 640

15.58752998 12.82973621 0.035 32.16929257 895 895

24.76525822 62.44131455 0.096 89.41524883 1000 1000

48.03370787 39.04494382 0.08 108.085618 970 970

26.15606936 28.03468208 0.06 59.30855491 900 900

24.21991085 77.86032689 0.01 112.6400149 1115 1115

64.67741935 43.22580645 0.008 163.0725161 800 800

9.873060649 34.69675599 0.01 50.64469676 800 800

20.02617801 35.60209424 0.1 62.92722513 900 900

NY ProUCL Entry 199
9.102402023 7.079646018 0.13 58.4106574 1200 1200

25.60819462 86.6837388 0.14 116.4012036 1400 1400

64.45086705 82.51445087 0.052 198.0288786 820 820

6.343195266 26.37869822 0.048 36.88823669 760 760

7.221407625 13.36754643 0.028 23.78166569 675 675

110.977354 14.97020262 0.077 236.0841514 9940 9940

10.81794195 8.311345646 0.009 35.10134828 640 640

2200 2200

60.77265973 70.43090639 0.013 174.1586166 1300 1300

31.56384505 14.63414634 0.026 63.1536901 1800 1800

44.13265306 63.52040816 0.076 125.8413061 1300 1300

29.58104671 98.7819569 0.307 139.6457766 1500 1500

0.69913773 2.913073876 0.026 4.885007224 900 900

4.708798017 2.726146221 0.012 9.541120198 980 980

1.440888154 0.649580725 0.08 4.107400496 1000 1000

1.562872823 0.978286805 0.053 4.15703245 1000 1000

12.82660333 23.63420428 0.1 52.47529691 2000 2000

29.87804878 27.31707317 0.26 87.69902439 2100 2100

23.55889724 18.29573935 0.005 69.4285589 1300 1300

13.12335958 38.58267717 0.005 62.4721916 600 600

12.88659794 14.04639175 0.005 37.63386598 500 500

7.552083333 23.828125 0.005 36.72375 900 900

4.761904762 18.42105263 0.076 26.14116291 700 700

11.17391876 35.62508216 0.22 54.11772578 2200 2200

12.6450116 15.19721578 0.17 36.82893271 300 300

7.436021246 18.50555287 0.135 31.43630372 857 857

18.68919611 92.67793139 0.16 123.9439222 820 820

18.39712919 50.89712919 0.13 83.62282297 692 692

16.74377892 115.0306365 0.212 143.915889 645 645

13.7189231 139.1730001 0.127 161.8428315 569 569

8.147138965 34.60490463 0.026 46.29302997 586 586

2.508241364 10.69227462 0.036 14.89912169 374 374

7.236150728 12.70079568 0.045 24.00536631 500 500

36.22905028 22.5 0.146 84.76890503 584 584

40.39523394 261.4065679 0.229 328.3312958 482 482

5.183312263 21.99747155 0.128 28.54491249 656 656

0.204185809 0.382848392 0.076 0.943789689 460 460

15.28680418 26.9991523 0.154 48.79768466 500 500

27.41463415 135.5772358 0.156 176.5462439 1870 1870

17.17112063 41.50302672 0.089 70.87004237 514 514

9.59933222 20.67334446 0.062 53.45654647 310 310

20.97186701 14.34782609 0.097 52.44994118 341 341

5.895595891 21.79541297 0.146 30.56671197 145 145

17.44769363 43.65594029 0.079 75.02088181 400 400

3.626373626 4.162087912 0.054 10.52103297 508 508

28.54458918 21.54308617 0.063 65.10558517 460 460

46.50406504 18.37398374 0.3 72.33252033 400 400

12.00260926 22.30919765 0.07 40.86582518 1100 1100

40.44552205 22.47310199 0.161 86.38618563 4290 4290

NY ProUCL Entry 200
General Background Statistics for Full Data Sets

User Selected Options

From File    WorkSheet.wst

Full Precision    OFF

Confidence Coefficient    90%

Coverage    90%

Different or Future K Values    1

Number of Bootstrap Operations   2000

Moisture

General Statistics

Total Number of Observations 140 Number of Distinct Observations 112

Raw Statistics Log‐Transformed Statistics

Minimum 3.9 Minimum 1.361

Maximum 38.5 Maximum 3.651

Second Largest 38.5 Second Largest 3.651

First Quartile 14.8 First Quartile 2.695

Median 18.78 Median 2.933

Third Quartile 23.83 Third Quartile 3.171

Mean 19.68 Mean 2.902

SD 7.292 SD 0.418

Coefficient of Variation 0.371

Skewness 0.376

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.0934 Lilliefors Test Statistic 0.0693

Lilliefors Critical Value 0.0749 Lilliefors Critical Value 0.0749

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 30.15   90% UTL with   90% Coverage 33.19

   90% UPL (t) 29.1   90% UPL (t) 31.26

90% Percentile (z) 29.02 90% Percentile (z) 31.12

95% Percentile (z) 31.67 95% Percentile (z) 36.22

99% Percentile (z) 36.64 99% Percentile (z) 48.15

Gamma Distribution Test Data Distribution Test

k star 6.492 Data appear Gamma Distributed at 5% Significance Level

Theta Star 3.031

MLE of Mean 19.68

MLE of Standard Deviation 7.724

nu star 1818

A‐D Test Statistic 0.546 Nonparametric Statistics

5% A‐D Critical Value 0.754 90% Percentile 30.02

K‐S Test Statistic 0.0558 95% Percentile 32.7

5% K‐S Critical Value 0.0792 99% Percentile 38.31

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 30.8

90% Percentile 30   90% Percentile Bootstrap UTL with   90% Coverage 30.84

95% Percentile 33.86   90% BCA Bootstrap UTL with   90% Coverage 30.84

99% Percentile 41.93   90% UPL 30.21

  90% Chebyshev UPL 41.63

NY UPL Results 201
   90% WH Approx. Gamma UPL 30.02 Upper Threshold Limit Based upon IQR 37.38

   90% HW Approx. Gamma UPL 30.26

   90% WH Approx. Gamma UTL with   90% Coverage 31.5

   90% HW Approx. Gamma UTL with   90% Coverage 31.83

Ash

General Statistics

Total Number of Observations 140 Number of Distinct Observations 140

Raw Statistics Log‐Transformed Statistics

Minimum 1.374 Minimum 0.317

Maximum 20 Maximum 2.996

Second Largest 16.99 Second Largest 2.833

First Quartile 3.4 First Quartile 1.224

Median 5.125 Median 1.634

Third Quartile 8.037 Third Quartile 2.084

Mean 6.11 Mean 1.652

SD 3.572 SD 0.565

Coefficient of Variation 0.585

Skewness 1.271

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.129 Lilliefors Test Statistic 0.0643

Lilliefors Critical Value 0.0749 Lilliefors Critical Value 0.0749

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 11.24   90% UTL with   90% Coverage 11.75

   90% UPL (t) 10.73   90% UPL (t) 10.84

90% Percentile (z) 10.69 90% Percentile (z) 10.77

95% Percentile (z) 11.98 95% Percentile (z) 13.23

99% Percentile (z) 14.42 99% Percentile (z) 19.44

Gamma Distribution Test Data Distribution Test

k star 3.266 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 1.871

MLE of Mean 6.11

MLE of Standard Deviation 3.381

nu star 914.5

A‐D Test Statistic 0.882 Nonparametric Statistics

5% A‐D Critical Value 0.758 90% Percentile 10.47

K‐S Test Statistic 0.0772 95% Percentile 13.32

5% K‐S Critical Value 0.0796 99% Percentile 16.67

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 11.9

90% Percentile 10.64   90% Percentile Bootstrap UTL with   90% Coverage 12.01

95% Percentile 12.52   90% BCA Bootstrap UTL with   90% Coverage 12.01

99% Percentile 16.56   90% UPL 10.62

  90% Chebyshev UPL 16.86

   90% WH Approx. Gamma UPL 10.62 Upper Threshold Limit Based upon IQR 14.99

   90% HW Approx. Gamma UPL 10.65

   90% WH Approx. Gamma UTL with   90% Coverage 11.34

NY UPL Results 202
   90% HW Approx. Gamma UTL with   90% Coverage 11.41

Sulfur

General Statistics

Total Number of Observations 139 Number of Distinct Observations 138

Number of Missing Values 1

Raw Statistics Log‐Transformed Statistics

Minimum 0.0225 Minimum ‐3.795

Maximum 0.288 Maximum ‐1.244

Second Largest 0.264 Second Largest ‐1.331

First Quartile 0.0452 First Quartile ‐3.096

Median 0.0835 Median ‐2.483

Third Quartile 0.137 Third Quartile ‐1.986

Mean 0.0975 Mean ‐2.532

SD 0.0608 SD 0.661

Coefficient of Variation 0.623

Skewness 0.814

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.127 Lilliefors Test Statistic 0.078

Lilliefors Critical Value 0.0751 Lilliefors Critical Value 0.0751

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.185   90% UTL with   90% Coverage 0.205

   90% UPL (t) 0.176   90% UPL (t) 0.187

90% Percentile (z) 0.175 90% Percentile (z) 0.185

95% Percentile (z) 0.197 95% Percentile (z) 0.236

99% Percentile (z) 0.239 99% Percentile (z) 0.37

Gamma Distribution Test Data Distribution Test

k star 2.551 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0382

MLE of Mean 0.0975

MLE of Standard Deviation 0.061

nu star 709.3

A‐D Test Statistic 1.356 Nonparametric Statistics

5% A‐D Critical Value 0.762 90% Percentile 0.188

K‐S Test Statistic 0.0809 95% Percentile 0.214

5% K‐S Critical Value 0.0801 99% Percentile 0.253

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.198

90% Percentile 0.179   90% Percentile Bootstrap UTL with   90% Coverage 0.198

95% Percentile 0.215   90% BCA Bootstrap UTL with   90% Coverage 0.198

99% Percentile 0.292   90% UPL 0.191

  90% Chebyshev UPL 0.28

   90% WH Approx. Gamma UPL 0.179 Upper Threshold Limit Based upon IQR 0.275

   90% HW Approx. Gamma UPL 0.18

   90% WH Approx. Gamma UTL with   90% Coverage 0.193

   90% HW Approx. Gamma UTL with   90% Coverage 0.195

NY UPL Results 203
Heating Value

General Statistics

Total Number of Observations 140 Number of Distinct Observations 140

Raw Statistics Log‐Transformed Statistics

Minimum 6663 Minimum 8.804

Maximum 11699 Maximum 9.367

Second Largest 10670 Second Largest 9.275

First Quartile 8072 First Quartile 8.996

Median 8374 Median 9.033

Third Quartile 8710 Third Quartile 9.072

Mean 8409 Mean 9.034

SD 632.5 SD 0.0737

Coefficient of Variation 0.0752

Skewness 1.004

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.0871 Lilliefors Test Statistic 0.0794

Lilliefors Critical Value 0.0749 Lilliefors Critical Value 0.0749

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 9317   90% UTL with   90% Coverage 9322

   90% UPL (t) 9226   90% UPL (t) 9224

90% Percentile (z) 9219 90% Percentile (z) 9216

95% Percentile (z) 9449 95% Percentile (z) 9466

99% Percentile (z) 9880 99% Percentile (z) 9954

Gamma Distribution Test Data Distribution Test

k star 179.8 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 46.77

MLE of Mean 8409

MLE of Standard Deviation 627.1

nu star 50341

A‐D Test Statistic 1.423 Nonparametric Statistics

5% A‐D Critical Value 0.75 90% Percentile 9208

K‐S Test Statistic 0.0773 95% Percentile 9284

5% K‐S Critical Value 0.0789 99% Percentile 10159

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 9231

90% Percentile 9222   90% Percentile Bootstrap UTL with   90% Coverage 9231

95% Percentile 9466   90% BCA Bootstrap UTL with   90% Coverage 9231

99% Percentile 9936   90% UPL 9213

  90% Chebyshev UPL 10313

   90% WH Approx. Gamma UPL 9223 Upper Threshold Limit Based upon IQR 9667

   90% HW Approx. Gamma UPL 9223

   90% WH Approx. Gamma UTL with   90% Coverage 9319

   90% HW Approx. Gamma UTL with   90% Coverage 9319

Arsenic

NY UPL Results 204
General Statistics

Total Number of Observations 137 Number of Distinct Observations 136

Number of Missing Values 3

Raw Statistics Log‐Transformed Statistics

Minimum 0.104 Minimum ‐2.263

Maximum 110.1 Maximum 4.701

Second Largest 82.12 Second Largest 4.408

First Quartile 3.085 First Quartile 1.126

Median 6.443 Median 1.863

Third Quartile 15.68 Third Quartile 2.752

Mean 11.94 Mean 1.849

SD 15.18 SD 1.242

Coefficient of Variation 1.271

Skewness 3.345

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.218 Lilliefors Test Statistic 0.0672

Lilliefors Critical Value 0.0757 Lilliefors Critical Value 0.0757

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 33.78   90% UTL with   90% Coverage 37.9

   90% UPL (t) 31.57   90% UPL (t) 31.64

90% Percentile (z) 31.4 90% Percentile (z) 31.21

95% Percentile (z) 36.92 95% Percentile (z) 49

99% Percentile (z) 47.26 99% Percentile (z) 114.2

Gamma Distribution Test Data Distribution Test

k star 0.908 Data appear Lognormal at 5% Significance Level

Theta Star 13.15

MLE of Mean 11.94

MLE of Standard Deviation 12.53

nu star 248.8

A‐D Test Statistic 1.107 Nonparametric Statistics

5% A‐D Critical Value 0.787 90% Percentile 27.13

K‐S Test Statistic 0.0915 95% Percentile 38.4

5% K‐S Critical Value 0.0825 99% Percentile 72.42

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 29.57

90% Percentile 28.16   90% Percentile Bootstrap UTL with   90% Coverage 29.84

95% Percentile 37.02   90% BCA Bootstrap UTL with   90% Coverage 29.57

99% Percentile 57.75   90% UPL 27.61

  90% Chebyshev UPL 57.66

   90% WH Approx. Gamma UPL 27.11 Upper Threshold Limit Based upon IQR 34.57

   90% HW Approx. Gamma UPL 27.34

   90% WH Approx. Gamma UTL with   90% Coverage 30.27

   90% HW Approx. Gamma UTL with   90% Coverage 30.87

Cadmium

General Statistics

NY UPL Results 205
Total Number of Observations 78 Number of Distinct Observations 77

Raw Statistics Log‐Transformed Statistics

Minimum 1.12E‐06 Minimum ‐13.7

Maximum 1.773 Maximum 0.573

Second Largest 1.074 Second Largest 0.0717

First Quartile 0.0732 First Quartile ‐2.615

Median 0.131 Median ‐2.032

Third Quartile 0.278 Third Quartile ‐1.279

Mean 0.225 Mean ‐2.143

SD 0.277 SD 1.688

Coefficient of Variation 1.229

Skewness 3.162

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.208 Lilliefors Test Statistic 0.196

Lilliefors Critical Value 0.1 Lilliefors Critical Value 0.1

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.639   90% UTL with   90% Coverage 1.459

   90% UPL (t) 0.586   90% UPL (t) 1.054

90% Percentile (z) 0.58 90% Percentile (z) 1.02

95% Percentile (z) 0.681 95% Percentile (z) 1.884

99% Percentile (z) 0.87 99% Percentile (z) 5.953

Gamma Distribution Test Data Distribution Test

k star 0.87 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.259

MLE of Mean 0.225

MLE of Standard Deviation 0.242

nu star 135.7

A‐D Test Statistic 1.123 Nonparametric Statistics

5% A‐D Critical Value 0.786 90% Percentile 0.499

K‐S Test Statistic 0.114 95% Percentile 0.81

5% K‐S Critical Value 0.105 99% Percentile 1.235

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.673

90% Percentile 0.537   90% Percentile Bootstrap UTL with   90% Coverage 0.673

95% Percentile 0.709   90% BCA Bootstrap UTL with   90% Coverage 0.673

99% Percentile 1.114   90% UPL 0.523

  90% Chebyshev UPL 1.062

   90% WH Approx. Gamma UPL 0.51 Upper Threshold Limit Based upon IQR 0.586

   90% HW Approx. Gamma UPL 0.523

   90% WH Approx. Gamma UTL with   90% Coverage 0.587

   90% HW Approx. Gamma UTL with   90% Coverage 0.611

Chromium

General Statistics

Total Number of Observations 139 Number of Distinct Observations 139

Number of Missing Values 1

NY UPL Results 206
Raw Statistics Log‐Transformed Statistics

Minimum 0.204 Minimum ‐1.589

Maximum 127 Maximum 4.844

Second Largest 126.6 Second Largest 4.841

First Quartile 7.653 First Quartile 2.035

Median 14.17 Median 2.651

Third Quartile 29.8 Third Quartile 3.394

Mean 23.47 Mean 2.672

SD 24.05 SD 1.08

Coefficient of Variation 1.025

Skewness 2.115

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.18 Lilliefors Test Statistic 0.0544

Lilliefors Critical Value 0.0751 Lilliefors Critical Value 0.0751

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 58.03   90% UTL with   90% Coverage 68.31

   90% UPL (t) 54.55   90% UPL (t) 58.44

90% Percentile (z) 54.29 90% Percentile (z) 57.77

95% Percentile (z) 63.03 95% Percentile (z) 85.52

99% Percentile (z) 79.42 99% Percentile (z) 178.5

Gamma Distribution Test Data Distribution Test

k star 1.153 Data Follow Appr. Gamma Distribution at 5% Significance Level

Theta Star 20.36

MLE of Mean 23.47

MLE of Standard Deviation 21.86

nu star 320.5

A‐D Test Statistic 0.795 Nonparametric Statistics

5% A‐D Critical Value 0.779 90% Percentile 56.87

K‐S Test Statistic 0.0762 95% Percentile 70.41

5% K‐S Critical Value 0.0814 99% Percentile 120.7

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 64.45

90% Percentile 52.18   90% Percentile Bootstrap UTL with   90% Coverage 64.5

95% Percentile 66.89   90% BCA Bootstrap UTL with   90% Coverage 64.5

99% Percentile 100.7   90% UPL 58.73

  90% Chebyshev UPL 95.88

   90% WH Approx. Gamma UPL 51.1 Upper Threshold Limit Based upon IQR 63.01

   90% HW Approx. Gamma UPL 51.72

   90% WH Approx. Gamma UTL with   90% Coverage 56.47

   90% HW Approx. Gamma UTL with   90% Coverage 57.68

Lead

General Statistics

Total Number of Observations 139 Number of Distinct Observations 139

Number of Missing Values 1

Raw Statistics Log‐Transformed Statistics

Minimum 0.383 Minimum ‐0.96

NY UPL Results 207
Maximum 261.4 Maximum 5.566

Second Largest 176.9 Second Largest 5.176

First Quartile 6.451 First Quartile 1.864

Median 15.14 Median 2.718

Third Quartile 27.3 Third Quartile 3.307

Mean 26.23 Mean 2.62

SD 36.09 SD 1.208

Coefficient of Variation 1.376

Skewness 3.464

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.243 Lilliefors Test Statistic 0.0776

Lilliefors Critical Value 0.0751 Lilliefors Critical Value 0.0751

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 78.08   90% UTL with   90% Coverage 77.9

   90% UPL (t) 72.86   90% UPL (t) 65.42

90% Percentile (z) 72.48 90% Percentile (z) 64.58

95% Percentile (z) 85.59 95% Percentile (z) 100.2

99% Percentile (z) 110.2 99% Percentile (z) 228.2

Gamma Distribution Test Data Distribution Test

k star 0.888 Data do not follow a Discernable Distribution (0.05)

Theta Star 29.53

MLE of Mean 26.23

MLE of Standard Deviation 27.83

nu star 246.9

A‐D Test Statistic 1.749 Nonparametric Statistics

5% A‐D Critical Value 0.788 90% Percentile 62.66

K‐S Test Statistic 0.104 95% Percentile 93.29

5% K‐S Critical Value 0.082 99% Percentile 162.6

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 81.67

90% Percentile 62.18   90% Percentile Bootstrap UTL with   90% Coverage 81.67

95% Percentile 81.95   90% BCA Bootstrap UTL with   90% Coverage 81.84

99% Percentile 128.3   90% UPL 63.52

  90% Chebyshev UPL 134.9

   90% WH Approx. Gamma UPL 59.33 Upper Threshold Limit Based upon IQR 58.57

   90% HW Approx. Gamma UPL 59.3

   90% WH Approx. Gamma UTL with   90% Coverage 66.28

   90% HW Approx. Gamma UTL with   90% Coverage 66.94

Mercury

General Statistics

Total Number of Observations 61 Number of Distinct Observations 48

Number of Missing Values 79

Raw Statistics Log‐Transformed Statistics

Minimum 0.005 Minimum ‐5.298

Maximum 0.307 Maximum ‐1.181

Second Largest 0.3 Second Largest ‐1.204

NY UPL Results 208
First Quartile 0.028 First Quartile ‐3.576

Median 0.076 Median ‐2.577

Third Quartile 0.13 Third Quartile ‐2.04

Mean 0.0879 Mean ‐2.907

SD 0.0744 SD 1.137

Coefficient of Variation 0.847

Skewness 1.139

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.149 Lilliefors Test Statistic 0.127

Lilliefors Critical Value 0.113 Lilliefors Critical Value 0.113

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.201   90% UTL with   90% Coverage 0.309

   90% UPL (t) 0.185   90% UPL (t) 0.241

90% Percentile (z) 0.183 90% Percentile (z) 0.234

95% Percentile (z) 0.21 95% Percentile (z) 0.354

99% Percentile (z) 0.261 99% Percentile (z) 0.769

Gamma Distribution Test Data Distribution Test

k star 1.143 Data appear Gamma Distributed at 5% Significance Level

Theta Star 0.0769

MLE of Mean 0.0879

MLE of Standard Deviation 0.0822

nu star 139.4

A‐D Test Statistic 0.484 Nonparametric Statistics

5% A‐D Critical Value 0.775 90% Percentile 0.17

K‐S Test Statistic 0.0782 95% Percentile 0.229

5% K‐S Critical Value 0.117 99% Percentile 0.303

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.22

90% Percentile 0.196   90% Percentile Bootstrap UTL with   90% Coverage 0.229

95% Percentile 0.251   90% BCA Bootstrap UTL with   90% Coverage 0.22

99% Percentile 0.379   90% UPL 0.204

  90% Chebyshev UPL 0.313

   90% WH Approx. Gamma UPL 0.196 Upper Threshold Limit Based upon IQR 0.283

   90% HW Approx. Gamma UPL 0.203

   90% WH Approx. Gamma UTL with   90% Coverage 0.228

   90% HW Approx. Gamma UTL with   90% Coverage 0.239

Total Metals

General Statistics

Total Number of Observations 139 Number of Distinct Observations 139

Number of Missing Values 1

Raw Statistics Log‐Transformed Statistics

Minimum 0.944 Minimum ‐0.0579

Maximum 328.3 Maximum 5.794

Second Largest 236.1 Second Largest 5.464

First Quartile 25.24 First Quartile 3.229

Median 44.81 Median 3.802

NY UPL Results 209
Third Quartile 82.76 Third Quartile 4.416

Mean 61.63 Mean 3.729

SD 54.84 SD 0.965

Coefficient of Variation 0.89

Skewness 1.791

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.166 Lilliefors Test Statistic 0.0617

Lilliefors Critical Value 0.0751 Lilliefors Critical Value 0.0751

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 140.4   90% UTL with   90% Coverage 166.7

   90% UPL (t) 132.5   90% UPL (t) 145

90% Percentile (z) 131.9 90% Percentile (z) 143.5

95% Percentile (z) 151.8 95% Percentile (z) 203.8

99% Percentile (z) 189.2 99% Percentile (z) 393.5

Gamma Distribution Test Data Distribution Test

k star 1.393 Data appear Gamma Distributed at 5% Significance Level

Theta Star 44.25

MLE of Mean 61.63

MLE of Standard Deviation 52.22

nu star 387.2

A‐D Test Statistic 0.45 Nonparametric Statistics

5% A‐D Critical Value 0.772 90% Percentile 140.5

K‐S Test Statistic 0.058 95% Percentile 176.7

5% K‐S Critical Value 0.081 99% Percentile 226.3

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 163.1

90% Percentile 130.8   90% Percentile Bootstrap UTL with   90% Coverage 164.3

95% Percentile 164.6   90% BCA Bootstrap UTL with   90% Coverage 163.3

99% Percentile 241.4   90% UPL 143.9

  90% Chebyshev UPL 226.7

   90% WH Approx. Gamma UPL 129.3 Upper Threshold Limit Based upon IQR 169

   90% HW Approx. Gamma UPL 131.1

   90% WH Approx. Gamma UTL with   90% Coverage 141.8

   90% HW Approx. Gamma UTL with   90% Coverage 144.9

Chloride

General Statistics

Total Number of Observations 138 Number of Distinct Observations 52

Number of Missing Values 2

Raw Statistics Log‐Transformed Statistics

Minimum 145 Minimum 4.977

Maximum 9940 Maximum 9.204

Second Largest 6460 Second Largest 8.773

First Quartile 679.3 First Quartile 6.521

Median 900 Median 6.802

Third Quartile 1200 Third Quartile 7.09

Mean 1097 Mean 6.818

NY UPL Results 210
SD 1029 SD 0.545

Coefficient of Variation 0.938

Skewness 5.964

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.232 Lilliefors Test Statistic 0.0993

Lilliefors Critical Value 0.0754 Lilliefors Critical Value 0.0754

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2577   90% UTL with   90% Coverage 2002

   90% UPL (t) 2428   90% UPL (t) 1850

90% Percentile (z) 2417 90% Percentile (z) 1839

95% Percentile (z) 2790 95% Percentile (z) 2241

99% Percentile (z) 3492 99% Percentile (z) 3249

Gamma Distribution Test Data Distribution Test

k star 2.843 Data do not follow a Discernable Distribution (0.05)

Theta Star 386

MLE of Mean 1097

MLE of Standard Deviation 650.8

nu star 784.7

A‐D Test Statistic 4.15 Nonparametric Statistics

5% A‐D Critical Value 0.76 90% Percentile 1700

K‐S Test Statistic 0.152 95% Percentile 2015

5% K‐S Critical Value 0.0802 99% Percentile 5657

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1870

90% Percentile 1970   90% Percentile Bootstrap UTL with   90% Coverage 1870

95% Percentile 2339   90% BCA Bootstrap UTL with   90% Coverage 1800

99% Percentile 3141   90% UPL 1710

  90% Chebyshev UPL 4197

   90% WH Approx. Gamma UPL 1930 Upper Threshold Limit Based upon IQR 1981

   90% HW Approx. Gamma UPL 1899

   90% WH Approx. Gamma UTL with   90% Coverage 2067

   90% HW Approx. Gamma UTL with   90% Coverage 2039

Fluoride

General Statistics

Total Number of Observations 8 Number of Distinct Observations 8

Number of Missing Values 73

Raw Statistics Log‐Transformed Statistics

Minimum 37.66 Minimum 3.629

Maximum 658.8 Maximum 6.49

Second Largest 418.1 Second Largest 6.036

First Quartile 147.7 First Quartile 4.99

Median 234.5 Median 5.453

Third Quartile 409 Third Quartile 6.014

Mean 283.6 Mean 5.367

SD 200.7 SD 0.892

Coefficient of Variation 0.708

NY UPL Results 211
Skewness 0.839

Warning:  There are only 8 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.941 Shapiro Wilk Test Statistic 0.944

Shapiro Wilk Critical Value 0.818 Shapiro Wilk Critical Value 0.818

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 729   90% UTL with   90% Coverage 1552

   90% UPL (t) 584.9   90% UPL (t) 817.3

90% Percentile (z) 540.9 90% Percentile (z) 672.1

95% Percentile (z) 613.8 95% Percentile (z) 929.5

99% Percentile (z) 750.6 99% Percentile (z) 1708

Gamma Distribution Test Data Distribution Test

k star 1.289 Data appear Normal at 5% Significance Level

Theta Star 220

MLE of Mean 283.6

MLE of Standard Deviation 249.8

nu star 20.63

A‐D Test Statistic 0.171 Nonparametric Statistics

5% A‐D Critical Value 0.725 90% Percentile 490.3

K‐S Test Statistic 0.153 95% Percentile 574.6

5% K‐S Critical Value 0.298 99% Percentile 642

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 658.8

90% Percentile 613.4   90% Percentile Bootstrap UTL with   90% Coverage 658.8

95% Percentile 777.7   90% BCA Bootstrap UTL with   90% Coverage 658.8

99% Percentile 1152   90% UPL 658.8

  90% Chebyshev UPL 922.3

   90% WH Approx. Gamma UPL 662.8 Upper Threshold Limit Based upon IQR 801.1

   90% HW Approx. Gamma UPL 687.4

   90% WH Approx. Gamma UTL with   90% Coverage 977.2

   90% HW Approx. Gamma UTL with   90% Coverage 1057

Total Halogens

General Statistics

Total Number of Observations 137 Number of Distinct Observations 59

Number of Missing Values 3

Raw Statistics Log‐Transformed Statistics

Minimum 145 Minimum 4.977

Maximum 9940 Maximum 9.204

Second Largest 6460 Second Largest 8.773

First Quartile 675 First Quartile 6.515

NY UPL Results 212
Median 900 Median 6.802

Third Quartile 1300 Third Quartile 7.17

Mean 1113 Mean 6.832

SD 1034 SD 0.549

Coefficient of Variation 0.929

Skewness 5.895

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.222 Lilliefors Test Statistic 0.0933

Lilliefors Critical Value 0.0757 Lilliefors Critical Value 0.0757

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2599   90% UTL with   90% Coverage 2043

   90% UPL (t) 2449   90% UPL (t) 1886

90% Percentile (z) 2438 90% Percentile (z) 1875

95% Percentile (z) 2813 95% Percentile (z) 2289

99% Percentile (z) 3518 99% Percentile (z) 3328

Gamma Distribution Test Data Distribution Test

k star 2.835 Data do not follow a Discernable Distribution (0.05)

Theta Star 392.6

MLE of Mean 1113

MLE of Standard Deviation 661.1

nu star 776.8

A‐D Test Statistic 3.674 Nonparametric Statistics

5% A‐D Critical Value 0.76 90% Percentile 1700

K‐S Test Statistic 0.145 95% Percentile 2100

5% K‐S Critical Value 0.0805 99% Percentile 5679

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1870

90% Percentile 1999   90% Percentile Bootstrap UTL with   90% Coverage 1880

95% Percentile 2374   90% BCA Bootstrap UTL with   90% Coverage 1800

99% Percentile 3190   90% UPL 1720

  90% Chebyshev UPL 4225

   90% WH Approx. Gamma UPL 1960 Upper Threshold Limit Based upon IQR 2238

   90% HW Approx. Gamma UPL 1931

   90% WH Approx. Gamma UTL with   90% Coverage 2101

   90% HW Approx. Gamma UTL with   90% Coverage 2074

NY UPL Results 213
MDL

Metals (mg/kg)

‐‐ 5.4 11.8 6.8 47.0 19.4 47 19.4

‐‐

‐‐ 206 119 250 32 141 32 141 161 451

‐‐

‐‐

Total Metals (mg/kg) ‐‐ 211.4 130.8 256.8 79.0 160.4 79.0 160.4 161.0 451.0

* All 90% UPL Results reported as Normal MRL = Method Reporting Limit

** 90% UPL Result reported as Lognormal MDL = Method Detection Limit

*** 90% UPL Result Non‐Parametric HAP = Hazardous Air Pollutant

‐‐ = Non‐Detect OH = Organic Halogen

n.d. = Only 1 Distinct Value, therefore no variance. N = Nitrogenated

Lead  (HAP)

Mercury  (HAP)

Arsenic  (HAP)

Chromium  (HAP)

Selenium  (HAP)

Maine C&D Summary Table 214
10.4 1.2 10.1

2 2 231

50 41 237 34 29 170 393 188 28 33 214 34 10 3

0.02 0.06 0.08

0.8 0.5 0.6

50.0 41.0 237.0 34.0 29.0 170.0 393.0 188.0 28.0 33.0 214.0 47.2 13.8 244.8

Maine C&D SUMMARY

Maine C&D Summary Table 215
Non‐

Detect Average StandardDeviation

7.1 55 9.9 70 5 10.8 51 3 37 2 6.9 2.5 13.0 19.94 20.82

198 52 142 8 2 76 311 14 67 47 14 66 20 82.13 95.72

391 7 260 225 150 228 80 27 44 2 16 10 0 126.77 122.81

0.09 0.05 0.27 0.26 0.24 0.04 0.20 0.19 0.24 0.04 0.08 0.10 21.00 0.14 0.09

0.8 0.7 0.8 1.3 1.2 0.7 1 0.6 0.7 0.5 0.8 0.4 20 0.76 0.25

597.0 114.8 413.0 304.6 158.4 315.5 443.2 44.8 148.9 51.5 37.8 79.0 ‐‐ 174.89 146.5

Maine C&D Summary Table 216
*all results reported as moisture free

*all results pooled from all 7 samples

Low High

1.20 70.00 53.86**

2.00 311.00 352.4**

2.0 451.0 312.4***

0.040 0.27 0.31**

0.40 1.3 1.107

13.76 597 426.9**

Range 90% UPL

Results*

Maine C&D Summary Table 217
Arsenic  (HAP) Chromium  (HAP) Lead  (HAP) Mercury  (HAP) Selenium  (HAP) Total Metals (mg/kg)

22 15 35 14 15 35

5.4 206 211.4

11.8 119 130.8

6.8 250 256.8

47 32 79

19.4 141 160.4

47 32 79

19.4 141 160.4

161 161

451 451

50 50

41 41

237 237

34 34

29 29

170 170

393 393

188 188

28 28

33 33

214 214

10.4 2 34 0.02 0.8 47.2

1.2 2 10 0.06 0.5 13.76

10.1 231 3 0.08 0.6 244.78

7.1 198 391 0.09 0.8 596.99

55 52 7 0.05 0.7 114.75

9.9 142 260 0.27 0.8 412.97

70 8 225 0.26 1.3 304.56

5 2 150 0.24 1.2 158.44

10.8 76 228 0.04 0.7 315.54

51 311 80 0.2 1 443.2

3 14 27 0.19 0.6 44.79

37 67 44 0.24 0.7 148.94

2 47 2 0.04 0.5 51.54

6.9 14 16 0.08 0.8 37.78

2.5 66 10 0.1 0.4 79

Maine ProUCL Entry 218
General Background Statistics for Full Data Sets

User Selected Options

From File    WorkSheet_a.wst

Full Precision    OFF

Confidence Coefficient    90%

Coverage    90%

Different or Future K Values    1

Number of Bootstrap Operations   2000

Arsenic

General Statistics

Total Number of Observations 22 Number of Distinct Observations 20

Number of Missing Values 13

Raw Statistics Log‐Transformed Statistics

Minimum 1.2 Minimum 0.182

Maximum 70 Maximum 4.248

Second Largest 55 Second Largest 4.007

First Quartile 5.75 First Quartile 1.744

Median 10.25 Median 2.327

Third Quartile 32.6 Third Quartile 3.45

Mean 19.94 Mean 2.419

SD 20.82 SD 1.159

Coefficient of Variation 1.044

Skewness 1.181

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.794 Shapiro Wilk Test Statistic 0.957

Shapiro Wilk Critical Value 0.911 Shapiro Wilk Critical Value 0.911

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 56.1   90% UTL with   90% Coverage 84.05

   90% UPL (t) 48.11   90% UPL (t) 53.86

90% Percentile (z) 46.62 90% Percentile (z) 49.59

95% Percentile (z) 54.18 95% Percentile (z) 75.54

99% Percentile (z) 68.37 99% Percentile (z) 166.4

Gamma Distribution Test Data Distribution Test

k star 0.899 Data appear Gamma Distributed at 5% Significance Level

Theta Star 22.19

MLE of Mean 19.94

MLE of Standard Deviation 21.04

nu star 39.54

A‐D Test Statistic 0.692 Nonparametric Statistics

5% A‐D Critical Value 0.771 90% Percentile 50.6

K‐S Test Statistic 0.191 95% Percentile 54.8

5% K‐S Critical Value 0.191 99% Percentile 66.85

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 55

90% Percentile 47.14   90% Percentile Bootstrap UTL with   90% Coverage 55

95% Percentile 62.05   90% BCA Bootstrap UTL with   90% Coverage 54.6

99% Percentile 96.95   90% UPL 53.8

Maine UPL Results 219
  90% Chebyshev UPL 83.8

   90% WH Approx. Gamma UPL 48.16 Upper Threshold Limit Based upon IQR 72.88

   90% HW Approx. Gamma UPL 48.84

   90% WH Approx. Gamma UTL with   90% Coverage 63.48

   90% HW Approx. Gamma UTL with   90% Coverage 66.29

Chromium

General Statistics

Total Number of Observations 15 Number of Distinct Observations 12

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 2 Minimum 0.693

Maximum 311 Maximum 5.74

Second Largest 231 Second Largest 5.442

First Quartile 11 First Quartile 2.359

Median 52 Median 3.951

Third Quartile 109 Third Quartile 4.643

Mean 82.13 Mean 3.426

SD 95.72 SD 1.756

Coefficient of Variation 1.165

Skewness 1.353

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.812 Shapiro Wilk Test Statistic 0.902

Shapiro Wilk Critical Value 0.881 Shapiro Wilk Critical Value 0.881

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 260.8   90% UTL with   90% Coverage 815.4

   90% UPL (t) 215.1   90% UPL (t) 352.4

90% Percentile (z) 204.8 90% Percentile (z) 291.7

95% Percentile (z) 239.6 95% Percentile (z) 552.1

99% Percentile (z) 304.8 99% Percentile (z) 1826

Gamma Distribution Test Data Distribution Test

k star 0.545 Data appear Gamma Distributed at 5% Significance Level

Theta Star 150.8

MLE of Mean 82.13

MLE of Standard Deviation 111.3

nu star 16.34

A‐D Test Statistic 0.344 Nonparametric Statistics

5% A‐D Critical Value 0.784 90% Percentile 217.8

K‐S Test Statistic 0.136 95% Percentile 255

5% K‐S Critical Value 0.232 99% Percentile 299.8

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 311

90% Percentile 218.2   90% Percentile Bootstrap UTL with   90% Coverage 279

95% Percentile 306   90% BCA Bootstrap UTL with   90% Coverage 279

99% Percentile 520.2   90% UPL 263

  90% Chebyshev UPL 378.7

   90% WH Approx. Gamma UPL 233.1 Upper Threshold Limit Based upon IQR 256

Maine UPL Results 220
   90% HW Approx. Gamma UPL 245.9

   90% WH Approx. Gamma UTL with   90% Coverage 347

   90% HW Approx. Gamma UTL with   90% Coverage 389.2

Lead

General Statistics

Total Number of Observations 35 Number of Distinct Observations 31

Raw Statistics Log‐Transformed Statistics

Minimum 2 Minimum 0.693

Maximum 451 Maximum 6.111

Second Largest 393 Second Largest 5.974

First Quartile 30.5 First Quartile 3.417

Median 80 Median 4.382

Third Quartile 210 Third Quartile 5.347

Mean 126.8 Mean 4.162

SD 122.8 SD 1.404

Coefficient of Variation 0.969

Skewness 1.038

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.854 Shapiro Wilk Test Statistic 0.922

Shapiro Wilk Critical Value 0.934 Shapiro Wilk Critical Value 0.934

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 324.8   90% UTL with   90% Coverage 618.2

   90% UPL (t) 289.6   90% UPL (t) 413

90% Percentile (z) 284.2 90% Percentile (z) 388.2

95% Percentile (z) 328.8 95% Percentile (z) 646.7

99% Percentile (z) 412.5 99% Percentile (z) 1684

Gamma Distribution Test Data Distribution Test

k star 0.809 Data appear Gamma Distributed at 5% Significance Level

Theta Star 156.8

MLE of Mean 126.8

MLE of Standard Deviation 141

nu star 56.6

A‐D Test Statistic 0.702 Nonparametric Statistics

5% A‐D Critical Value 0.782 90% Percentile 256

K‐S Test Statistic 0.135 95% Percentile 391.6

5% K‐S Critical Value 0.154 99% Percentile 431.3

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 391

90% Percentile 307.5   90% Percentile Bootstrap UTL with   90% Coverage 392.2

95% Percentile 409.7   90% BCA Bootstrap UTL with   90% Coverage 391

99% Percentile 650.8   90% UPL 312.4

  90% Chebyshev UPL 500.4

   90% WH Approx. Gamma UPL 311.1 Upper Threshold Limit Based upon IQR 479.3

   90% HW Approx. Gamma UPL 323.3

   90% WH Approx. Gamma UTL with   90% Coverage 387.4

   90% HW Approx. Gamma UTL with   90% Coverage 414.1

Maine UPL Results 221
Mercury

General Statistics

Total Number of Observations 15 Number of Distinct Observations 12

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.02 Minimum ‐3.912

Maximum 0.27 Maximum ‐1.309

Second Largest 0.26 Second Largest ‐1.347

First Quartile 0.055 First Quartile ‐2.905

Median 0.09 Median ‐2.408

Third Quartile 0.22 Third Quartile ‐1.518

Mean 0.131 Mean ‐2.313

SD 0.0911 SD 0.821

Coefficient of Variation 0.698

Skewness 0.429

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.862 Shapiro Wilk Test Statistic 0.921

Shapiro Wilk Critical Value 0.881 Shapiro Wilk Critical Value 0.881

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.301   90% UTL with   90% Coverage 0.458

   90% UPL (t) 0.257   90% UPL (t) 0.31

90% Percentile (z) 0.247 90% Percentile (z) 0.283

95% Percentile (z) 0.281 95% Percentile (z) 0.382

99% Percentile (z) 0.343 99% Percentile (z) 0.669

Gamma Distribution Test Data Distribution Test

k star 1.602 Data appear Gamma Distributed at 5% Significance Level

Theta Star 0.0816

MLE of Mean 0.131

MLE of Standard Deviation 0.103

nu star 48.05

A‐D Test Statistic 0.575 Nonparametric Statistics

5% A‐D Critical Value 0.748 90% Percentile 0.252

K‐S Test Statistic 0.185 95% Percentile 0.263

5% K‐S Critical Value 0.224 99% Percentile 0.269

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.27

90% Percentile 0.268   90% Percentile Bootstrap UTL with   90% Coverage 0.266

95% Percentile 0.333   90% BCA Bootstrap UTL with   90% Coverage 0.266

99% Percentile 0.479   90% UPL 0.264

  90% Chebyshev UPL 0.413

   90% WH Approx. Gamma UPL 0.278 Upper Threshold Limit Based upon IQR 0.468

   90% HW Approx. Gamma UPL 0.284

   90% WH Approx. Gamma UTL with   90% Coverage 0.362

   90% HW Approx. Gamma UTL with   90% Coverage 0.378

Maine UPL Results 222
Selenium

General Statistics

Total Number of Observations 15 Number of Distinct Observations 8

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.4 Minimum ‐0.916

Maximum 1.3 Maximum 0.262

Second Largest 1.2 Second Largest 0.182

First Quartile 0.6 First Quartile ‐0.511

Median 0.7 Median ‐0.357

Third Quartile 0.8 Third Quartile ‐0.223

Mean 0.76 Mean ‐0.323

SD 0.25 SD 0.321

Coefficient of Variation 0.329

Skewness 0.875

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.919 Shapiro Wilk Test Statistic 0.965

Shapiro Wilk Critical Value 0.881 Shapiro Wilk Critical Value 0.881

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.227   90% UTL with   90% Coverage 1.318

   90% UPL (t) 1.107   90% UPL (t) 1.131

90% Percentile (z) 1.081 90% Percentile (z) 1.093

95% Percentile (z) 1.171 95% Percentile (z) 1.228

99% Percentile (z) 1.342 99% Percentile (z) 1.528

Gamma Distribution Test Data Distribution Test

k star 8.445 Data appear Normal at 5% Significance Level

Theta Star 0.09

MLE of Mean 0.76

MLE of Standard Deviation 0.262

nu star 253.3

A‐D Test Statistic 0.35 Nonparametric Statistics

5% A‐D Critical Value 0.737 90% Percentile 1.12

K‐S Test Statistic 0.193 95% Percentile 1.23

5% K‐S Critical Value 0.221 99% Percentile 1.286

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.3

90% Percentile 1.108   90% Percentile Bootstrap UTL with   90% Coverage 1.26

95% Percentile 1.235   90% BCA Bootstrap UTL with   90% Coverage 1.26

99% Percentile 1.496   90% UPL 1.24

  90% Chebyshev UPL 1.535

   90% WH Approx. Gamma UPL 1.118 Upper Threshold Limit Based upon IQR 1.1

   90% HW Approx. Gamma UPL 1.12E+00

   90% WH Approx. Gamma UTL with   90% Coverage 1.275

   90% HW Approx. Gamma UTL with   90% Coverage 1.284

Maine UPL Results 223
Total Metals

General Statistics

Total Number of Observations 35 Number of Distinct Observations 32

Raw Statistics Log‐Transformed Statistics

Minimum 13.76 Minimum 2.622

Maximum 597 Maximum 6.392

Second Largest 451 Second Largest 6.111

First Quartile 48.6 First Quartile 3.883

Median 158.4 Median 5.065

Third Quartile 240.9 Third Quartile 5.484

Mean 174.9 Mean 4.769

SD 146.5 SD 0.972

Coefficient of Variation 0.838

Skewness 1.125

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.878 Shapiro Wilk Test Statistic 0.952

Shapiro Wilk Critical Value 0.934 Shapiro Wilk Critical Value 0.934

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 411.2   90% UTL with   90% Coverage 564.4

   90% UPL (t) 369.1   90% UPL (t) 426.9

90% Percentile (z) 362.7 90% Percentile (z) 409.1

95% Percentile (z) 415.9 95% Percentile (z) 582.2

99% Percentile (z) 515.8 99% Percentile (z) 1129

Gamma Distribution Test Data Distribution Test

k star 1.306 Data appear Gamma Distributed at 5% Significance Level

Theta Star 133.9

MLE of Mean 174.9

MLE of Standard Deviation 153

nu star 91.45

A‐D Test Statistic 0.467 Nonparametric Statistics

5% A‐D Critical Value 0.768 90% Percentile 405

K‐S Test Statistic 0.131 95% Percentile 445.5

5% K‐S Critical Value 0.152 99% Percentile 547.4

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 443.2

90% Percentile 377   90% Percentile Bootstrap UTL with   90% Coverage 443.2

95% Percentile 477.4   90% BCA Bootstrap UTL with   90% Coverage 447.9

99% Percentile 706.1   90% UPL 425.1

  90% Chebyshev UPL 620.7

   90% WH Approx. Gamma UPL 381.3 Upper Threshold Limit Based upon IQR 529.3

   90% HW Approx. Gamma UPL 388.3

   90% WH Approx. Gamma UTL with   90% Coverage 457.9

   90% HW Approx. Gamma UTL with   90% Coverage 474.4

Maine UPL Results 224
*all results reported as moisture free

*all results pooled from all 7 samples

Average Standard Deviation Low High

Components

19.20 6.95 3.90 38.5 29.7**

4.99 3.86 0.49 20 10.02***

81.14 0.31 80.57 81.44 81.6118.22 0.31 17.85 18.78 18.69

6.00 0.05 5.95 6.12 6.12***

50.51 0.16 50.20 50.72 50.75

0.24 0.25 0.08 1.26 0.644***

42.60 0.23 42.36 43.08 43.08

0.13 0.11 0.01 0.731 0.202***

8091 864 5468 11699 9167***

Metals (mg/kg)

2.60 3.56 0.17 16.6 6.942**

26.12 39.55 0.10 220 67.06**0.088 0.080 0.008 0.2 0.2***

0.27 0.23 0.00 1.773 0.401***

39.01 49.86 0.20 311 99.97**

0.90 0.41 0.38 1.63 1.527**

44.01 69.95 0.4 451.0 103.1**65.89 29.50 31.0 156 103.6**

0.09 0.76 0.005 0.580 0.182***2.47 2.44 0.98 12.2 4.789***0.65 0.28 0.27 1.3 1.0

Total Metals (mg/kg) 111.0 111.5 0.94 597 278.2***

Formaldehyde (g/kg)

48841.00 36196.00 9300 130000 107423**

Ions

6.14 0.38 6 7 7***

933 990 47 9940 1640***

64.58 124.60 5 659 212.8***

Total Halogens (mg/kg) 899 987 13.3 9940 1600***

Volatile Compounds (g/kg)

Chlorobenzene (HAP/OH)Selenium (HAP)

1,1,2‐Trichloroethane (HAP/OH)

1,1,2,2‐Tetrachloroethane (HAP/OH)Fluorine (mg/kg)

Chlorine (mg/kg)

Fixed Carbon (wt%)

Hydrogen (wt%)Bromoform (HAP/OH)Benzene (HAP)Allyl chloride (HAP/OH)

Acrylonitrile (HAP/N)

Lead (HAP)

Cobalt (HAP)1,4‐Dichlorobenzene(p) (HAP/OH)

1,2,4‐Trichlorobenzene (HAP/OH)Bromine (mg/kg)FormaldehydeAcrolein (HAP)

Acetonitrile (HAP/N)Nickel (HAP)Chromium (HAP)

Cadmium (HAP)Beryllium (HAP)Arsenic (HAP)Mercury (HAP)

Manganese (HAP)

Heating Value (BTU/lb)

Antimony (HAP)

Range 90% UPL

Results*

Sulfur (wt%)

Oxygen (wt%)Nitrogen (wt%)Carbon (wt%)

Ash (wt%)Volatile Matter (wt%)Moisture (wt%)

Complete C&D Summary Table 225
Vinyl chloride

Ethyl benzene (HAP)Chloroprene (HAP/OH)

Chloroform (HAP/OH)

Methyl methacrylate (HAP)m,p‐Xylenes (HAP)Isopropylbenzene (HAP)

Hexachlorobutadiene (HAP/OH)

Toluene (HAP)Tetrachloroethylene (HAP/OH)Styrene (HAP)o‐Xylenes (HAP)

n‐Hexane (HAP)

Naphthalene (HAP)Methylene chloride (HAP/OH)Methyl tert butyl ether (HAP)

Complete C&D Summary Table 226
Total Volatile Compounds (g/kg)

Semi‐Volatile Compounds (g/kg)

Total Semi‐Volatile Compounds (g/kg)

* All 90% UPL Results reported as Normal MRL = Method Reporting Limit

** 90% UPL Result reported as Lognormal MDL = Method Detection Limit

*** 90% UPL Result Non‐Parametric HAP = Hazardous Air Pollutant‐‐ = Non‐Detect OH = Organic Halogenn.d. = Only 1 Distinct Value, therefore no variance. N = NitrogenatedPyrenePhenolPhenanthrenePentachlorophenol (HAP/OH)

Nitrobenzene (HAP/N)

Naphthalene (HAP)Benzo(a)pyreneBenzo(a)anthraceneChryseneBis(2‐ethylhexyl)phthalate (HAP)

Biphenyl (HAP)Benzo(k)fluorantheneBenzo(g,h,i)peryleneBenzo(b)fluorantheneIndeno(1,2,3‐cd)pyrene

HexachloroethaneDimethyl phthalate (HAP)

Dibenzofurans (D/F)

Dibenz(a,h)anthraceneHexachlorocyclopentadiene (HAP/OH)

Hexachlorobutadiene (HAP/OH)

Hexachlorobenzene (HAP/OH)

FluoreneFluoranthene1,2,4‐Trichlorobenzene (HAP/OH)

2‐MethylnaphthaleneAnthraceneAnilineAcetophenoneAcenaphthyleneAcenaphthene4‐Nitrophenol (HAP/N)

3,3‐Dichlorobenzidene (HAP/OH/N)2,4‐Dinitrotoluene (HAP/N)2,4‐Dinitrophenol (HAP/N)

2,4,6‐Trichlorophenol (HAP/OH)2,4,5‐Trichlorophenol (HAP/OH)1‐Methylnaphthalene1,4‐Dichlorobenzene (HAP/OH)

Complete C&D Summary Table 227
Complete C&D Summary Table 228
Complete C&D Summary Table 229
Complete C&D Summary Table 230
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ABCDE FGH I

Moisture (wAsh (wt%) Volatile MaFixed CarboHydrogen ( Carbon (wt Nitrogen (wOxygen (wtSulfur (wt%

177 177 7 7 7 7 47 7 186

12.05 0.64 81.24 18.13 6.12 50.56 0.25 42.41 0.018

13.03 0.65 80.57 18.78 6 50.57 0.2 42.58 0.01

15.2 0.7 80.89 18.42 5.99 50.5 0.22 42.57 0.015

14.91 0.68 81.37 17.96 6 50.72 0.23 42.36 0.009

14.1 0.7 81.44 17.85 5.98 50.53 0.19 42.57 0.021

13.87 0.63 81.24 18.13 5.99 50.48 0.29 42.6 0.014

13.45 0.52 81.24 18.24 5.95 50.2 0.23 43.08 0.018

0.77 0.455

1.26 0.516

0.7 0.608

0.76 0.625

0.55 0.486

0.39 0.394

0.27 0.136

0.42 0.731

0.63 0.61

0.55 0.355

15.87 0.55 0.09 0.18

19.63 0.57 0.14 0.17

18.47 1.5 0.09 0.17

14.88 0.58 0.09 0.18

30.34 0.53 0.11 0.15

23 0.74 0.16 0.16

13.3 0.67 0.09 0.18

16.6 0.76 0.09 0.18

15.1 0.6 0.16 0.18

15.75 0.89 0.09 0.18

19.6 1.06 0.15 0.17

22.7 0.67 0.08 0.16

14.5 0.52 0.09 0.18

13.94 0.71 0.12 0.18

28.3 0.96 0.11 0.15

20.82 0.68 0.08 0.17

21.4 1.22 0.08 0.17

20.3 0.99 0.15 0.17

22 0.87 0.08 0.16

16.86 0.65 0.09 0.17

Complete ProUCL Entry 231
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ABCDE FGH I

9.12 0.76 0.2 0.19

31.9 0.9 0.08 0.14

18.87 1.09 0.21 0.17

11.4 0.56 0.09 0.19

15.7 0.6 0.09 0.18

18.6 0.66 0.09 0.17

14 0.55 0.09 0.18

12.78 0.82 0.14 0.18

12.7 0.76 0.09 0.18

17.5 0.49 0.09 0.17

12.6 4.347826 0.148741

3.9 5.202914 0.208117

6.5 4.171123 0.213904

8.3 5.452563 0.119956

15.13 3.416991 0.106045

16.6 2.673861 0.047962

3.9 4.786681 0.083247

22.4 3.092784 0.064433

21.7 3.57599 0.178799

12.4 4.56621 0.159817

22.5 5.935484 0.193548

13.86 4.527513 0.023218

6.55 4.173355 0.064205

8.6 3.938731 0.131291

11.1 13.27334

13 9.609195 0.114943

12.3 4.561003 0.04561

13.3 9.457901 0.034602

16.9 3.610108 0.048135

16.9 7.340554 0.09627

18.4 3.063725 0.04902

21.8 3.516624 0.076726

22.5 10.45161 0.180645

22.2 5.912596 0.115681

5.5 9.312169 0.10582

Complete ProUCL Entry 232
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ABCDE FGH I

17.9 4.263094 0.097442

16.6 2.997602 0.131894

19.2 3.465347 0.123762

15.1 6.360424 0.176678

14.3 7.584597 0.233372

10.7 9.070549 0.235162

19.2 6.559406 0.19802

15.4 7.446809 0.141844

19.8 4.613466 0.124688

15.4 2.836879 0.082742

12.2 6.378132 0.148064

15.9 3.210464 0.118906

14.8 2.816901 0.08216

13.8 2.900232 0.023202

13.9 2.555168 0.10453

17 2.168675 0.084337

16.6 2.63789 0.035971

14.5 9.94152 0.128655

15.3 2.609209 0.070838

16 2.142857 0.059524

15 2.117647 0.058824

10.7 1.903695 0.055991

10.2 1.781737 0.044543

11 2.808989 0.022472

15.7 10.64057 0.094899

15.6 14.69194 0.130332

16.4 3.349282 0.107656

23.7 2.621232 0.131062

18.2 2.811736 0.0978

9.1 8.030803 0.154015

22.6 6.072351 0.193798

11.5 2.033898 0.090395

13 2.298851 0.057471

15.9 1.664685 0.047562

13.9 7.200929 0.034843

15.8 4.869359 0.059382

12.5 3.12 0.022857

24.3 10.33025 0.02642

33 20 0.029851

21.2 6.472081 0.025381

24.3 4.227213 0.02642

29.1 10.86037 0.028209

25.7 8.748318 0.040377

21.54 5.901096 0.038236

11.3 9.244645 0.033822

10.8 5.829596 0.044843

13.3 3.921569 0.023068

30 6.171429 0.071429

24.3 9.643329 0.264201

27.9 5.131761 0.041609

26.34 13.30437 0.054304

21.52 4.689093 0.050968

Complete ProUCL Entry 233
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ABCDE FGH I

22.91 13.52964 0.038916

20.34 3.288978 0.03766

21.93 8.99193 0.051236

19.16 2.684315 0.03711

11.3 9.131905 0.157835

15.9 12.96076 0.035672

16.6 6.954436 0.215827

14.8 7.511737 0.058685

28.8 16.99438 0.224719

30.8 7.225434 0.144509

32.7 14.48737 0.044577

38 6.290323 0.032258

29.1 6.06488 0.042313

23.6 8.376963 0.078534

20.9 9.102402 0.025284

21.9 8.706786 0.038412

30.8 9.176301 0.187861

15.5 5.727811 0.071006

18.16 3.103617 0.097752

16.1 8.057211 0.107271

24.2 7.519789 0.105541

29.2 3.531073 0.056497

32.7 9.955423 0.148588

30.3 3.299857 0.086083

21.6 4.655612 0.114796

25.29 6.960246 0.174006

14.18 2.854812 0.069914

19.3 2.688971 0.074349

15.33 4.806897 0.035432

16.18 4.533524 0.035791

15.8 3.491686 0.035629

18 3.536585 0.109756

20.2 5.263158 0.288221

23.8 5.11811 0.052493

22.4 3.608247 0.03866

23.2 2.473958 0.065104

20.2 4.260652 0.062657

23.93 4.206652 0.144604

13.8 3.480278 0.046404

17.16 4.732014 0.060357

21.88 4.83871 0.038402

16.4 6.722488 0.179426

20.03 8.078029 0.200075

22.37 7.175061 0.141698

26.6 7.820163 0.190736

30.23 5.145478 0.214992

33.39 11.57484 0.16514

28.4 6.075419 0.083799

31.18 8.660273 0.087184

28.81 4.677623 0.042141

21.64 3.177642 0.063808

29.22 5.495903 0.127155

Complete ProUCL Entry 234
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ABCDE FGH I

38.5 3.821138 0.146341

32.27 6.023918 0.132881

28.12 16.16583 0.083472

21.8 10.26854 0.051151

28.93 15.46363 0.126636

18.27 4.649456 0.15906

27.2 1.373626 0.151099

20.16 2.830661 0.175351

38.5 11.90244 0.097561

23.35 1.604697 0.039139

34.01 7.440521 0.106077

Complete ProUCL Entry 235
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J K LMNO P Q R S

Heating Va Antimony   Arsenic  (HABeryllium  (Cadmium  (Chromium Cobalt  (HALead  (HAP)ManganeseMercury  (H

187 22 236 22 125 231 22 251 22 152

8644 0.59 65.7 0.008 0.25 73.2 0.38 96.8 41.5 0.049

8254 0.18 2.21 0.008 0.18 4.1 0.41 41.3 55.3 0.04

8423 0.37 16.9 0.008 0.14 21.2 0.46 12.5 39.4 0.017

8624 0.17 1.95 0.008 0.13 3.01 0.51 34.6 44.1 0.032

8624 0.41 11.2 0.008 0.14 14 0.41 8.78 38.6 0.015

8033 0.35 13.8 0.008 0.13 16.2 0.62 15.7 39.1 0.02

8805 0.43 50.4 0.008 0.14 60.1 1.52 22 156 0.027

7600 16.6 8.2 0.03 0.26 12.3 0.83 26 54.6 0.143

7620 3.6 6.8 0.03 0.27 10.2 0.77 10.6 62.6 0.0188

7310 4.2 8.9 0.17 0.31 10.8 1.37 5.5 79.3 0.0778

7140 2.9 3.6 0.08 0.33 5.51 1.34 12.2 69.4 0.0284

6820 2.4 14.3 0.11 0.51 46 1.63 11.6 78.3 0.051

7170 1.8 11.6 0.04 0.34 14.4 1.18 7.8 65.5 0.0468

7920 0.6 6.3 0.07 0.18 6.86 0.67 3.8 56.3 0.0367

6460 3.5 26.2 0.17 0.33 34.3 1.58 13.2 127 0.0632

6770 7.4 5.1 0.13 0.32 7.2 1.45 7 90.5 0.0733

7900 1.7 13.2 0.05 0.26 15.1 0.78 8.3 63.1 0.0614

7157 57 0.4 60 20 0.08

6702 100 0.4 100 60 0.08

6900 80 0.4 80 210 0.08

7172 2 22 0.2 0.4 26 0.8 17 73 0.3

5587 11 0.4 13 61 0.08

6617 6.3 0.39 8.2 18 0.08

7434 44 0.39 59 71 0.08

7059 2 92 0.2 0.39 130 0.79 130 31 0.08

7243 210 0.4 240 9.5 0.08

7022 4 0.4 4 15 0.1

6872 150 0.4 180 19 0.08

6251 2 37 0.2 0.39 43 0.78 8.5 47 0.07

6444 47 0.39 50 8.9 0.07

6568 210 0.4 220 32 0.08

6035 13 0.4 16 26 0.08

6763 2 180 0.2 0.39 180 0.78 21 80 0.08

6608 110 0.39 120 230 0.08

6676 140 0.39 170 17 0.08

6481 21 0.39 28 110 0.08

6947 2 52 0.2 0.4 68 0.8 240 58 0.08

66 83 37 0.08

64 68 56 0.08

95 100 33 0.08

27 30 47 0.08

42 48 19 0.08

7.5 8.5 23 0.08

45 53 16 0.08

15 20 52 0.08

120 130 16 0.08

32 37 17 0.08

40 50 13 0.08

50 56 5 0.08

47 50 6.6 0.08

Complete ProUCL Entry 236
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J K LMNO P Q R S

65 86 8.8 0.08

29 32 20 0.08

89 100 12 0.08

76 82 20 0.08

46 52 9.7 0.08

34 37 18 0.08

54 62 56 0.08

7655 170 0.4 200 2.2 0.08

5468 16 0.4 9.6 26 0.07

6427 54 0.39 99 150 0.35

7713 140 0.4 150 18 0.08

6541 110 0.39 120 10 0.08

6935 14 0.39 16 19 0.07

7159 18 0.41 34 90 0.08

7435 2.7 0.4 2 120 0.08

6918 15 0.4 19 280 0.08

6875 0.94 0.4 0.49 6.1 0.08

150 170 2 0.08

22 21 5.4 0.08

177 30 35 0.58

43 52 2.5 0.08

220 220 2 0.08

9.7 9.7 12 0.08

18 18 20 0.08

1.2 0.9 6.9 0.08

5.9 6.4 6.5 0.12

6.1 5.3 2.4 0.08

9330.664 2.28833 0.343249 2.860412 10.64073

8455.775 0.104058 0.114464 2.185224 5.931322

8308.021 0.983957 0.171123 2.780749 22.99465

8095.965 3.947655 0.141767 12.54089 5.997819

8707.435 1.767409 0.353482 10.01532 6.4805

8383.693 3.717026 0.035971 2.877698 0.839329

8328.824 5.202914 0.020812 13.94381 23.30905

9292.526 6.443299 0.180412 13.65979 5.927835

9206.897 4.853129 0.217114 4.980843 9.45083

9028.539 2.16895 0.057078 5.479452 2.968037

8335.484 1.612903 0.090323 4.116129 7.870968

9283.724 0.010448 7.778036 3.830973

8240.77 0.321027 21.08079 2.140182

8718.818 0.656455 0.098468 3.938731 5.689278

7599.55 18.22272 0.899888 41.73228 19.91001

7780.46 37.47126 0.091954 0.574713 5.977011

8746.864 6.157355 0.079818 7.753706 4.104903

8238.754 82.12226 0.265283 76.93195 21.22261

8389.892 2.406739 0.048135 2.76775 3.128761

8932.611 12.39471 0.048135 6.618532 22.38267

9291.667 12.7451 0.526961 16.05392 5.637255

8207.161 4.859335 0.127877 5.11509 0.511509

8477.419 6.967742 0.180645 11.48387 19.22581

8962.725 3.084833 0.282776 7.197943 7.326478

8271.958 4.973545 0.126984 10.05291 33.22751

Complete ProUCL Entry 237
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J K LMNO P Q R S

10669.91 27.77101 0.146163 44.94519 6.577345

11699.04 2.398082 0.095923 11.99041 16.30695

9297.03 13.73762 0.061881 12.99505 6.559406

8935.218 0.117786 0.235571 10.83628 14.01649

7987.165 4.434072 0.058343 12.25204 12.48541

7573.348 1.231803 1.12E‐06 12.87794 12.87794

9017.327 4.70297 0.049505 9.034653 13.36634

8034.279 26.83215 1.77305 37.35225 31.32388

8284.289 18.82793 0.049875 20.69825 5.236908

8427.896 2.836879 0.165485 5.319149 5.082742

8690.205 3.758542 0.148064 8.542141 19.36219

8694.411 4.042806 0.344828 7.372176 6.420927

8816.901 0.117371 0.140845 4.225352 9.15493

8800.464 2.784223 0.359629 19.37355 81.67053

8577.236 8.943089 0.301974 12.77584 7.317073

8530.12 12.28916 0.192771 17.22892 7.951807

9224.221 29.13669 0.203837 42.92566 8.872902

7857.31 19.76608 0.807018 28.65497 44.32749

9213.695 4.604486 1.07438 8.854782 5.430933

8267.857 9.285714 0.059524 14.16667 3.809524

9077.647 4 0.105882 11.17647 10

9359.462 15.67749 0.134378 17.4692 176.9317

9230.512 10.91314 0.178174 22.049 15.14477

9165.169 4.606742 0.078652 18.8764 3.483146

8465.006 2.384342 0.403321 70.22539 15.18387

8581.754 2.725118 0.248815 127.0142 39.21801

9232.057 32.41627 0.825359 58.73206 3.4689

9251.638 0.655308 0.013106 4.980341 1.310616

9172.372 0.855746 0.0978 4.889976 4.645477

7388.339 3.740374 0.231023 13.09131 17.16172

8727.39 2.842377 0.103359 11.24031 10.85271

8700.565 1.355932 0.011299 6.327684 1.242938

9174.713 0.689655 0.068966 7.126437 2.988506

9199.762 5.469679 0.011891 10.22592 1.070155

7620.209 3.948897 0.081301 16.37631 11.96283

8072.447 29.57245 0.106888 42.75534 14.60808

8352 17.37143 0.331429 49.6 2.857143

7552.18 18.09775 0.06605 44.64993 18.09775

6662.687 7.61194 0.208955 31.64179 12.38806

8220.812 3.807107 0.025381 23.73096 4.822335

8441.215 22.06077 0.488771 56.40687 4.227213

7296.192 4.019746 0.112835 72.07334 3.223857

7858.681 4.710633 0.349933 126.6487 26.9179

8130.257 2.803977 0.522559 29.18685 14.5297

7597.52 14.65614 0.225479 34.38557 21.646

8041.48 15.80717 0.672646 32.84753 132.8475

8126.874 11.64937 0.080738 24.79815 7.843137

8040 7.5 0.071429 29.71429 16.85714

8025.099 6.869221 0.07926 16.38045 24.57067

7593.62 12.20527 0.097087 59.50069 10.54092

7097.475 10.72495 0.067879 68.55824 36.11187

8019.878 2.535678 0.089195 21.50866 23.99337

Complete ProUCL Entry 238
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7745.492 3.982358 0.285381 35.54287 31.32702

8306.553 3.803666 8.084359 13.73337 0.007

7735.366 18.53465 34.90457 37.82503 0.035

8313.953 13.33498 19.56952 16.57595 0.016

7942.503 52.64938 98.30891 27.28298 0.051

7626.635 21.75981 74.31629 36.74197 0.049

8173.861 3.717026 15.58753 12.82974 0.035

8071.596 2.112676 24.76526 62.44131 0.096

7008.427 20.92697 48.03371 39.04494 0.08

8109.827 5.057803 26.15607 28.03468 0.06

7292.719 10.54978 24.21991 77.86033 0.01

8151.613 55.16129 64.67742 43.22581 0.008

7902.68 6.06488 9.873061 34.69676 0.01

7727.749 7.198953 20.02618 35.60209 0.1

8040.455 42.09861 9.102402 7.079646 0.13

8088.348 3.96927 25.60819 86.68374 0.14

7955.202 51.01156 64.45087 82.51445 0.052

8285.207 4.118343 6.343195 26.3787 0.048

8583.822 3.164712 7.221408 13.36755 0.028

7938.021 110.0596 110.9774 14.9702 0.077

8307.388 15.96306 10.81794 8.311346 0.009

8435.028

7989.599 42.94205 60.77266 70.43091 0.013

8358.68 16.9297 31.56385 14.63415 0.026

8321.429 18.11224 44.13265 63.52041 0.076

8064.516 10.97577 29.58105 98.78196 0.307

8606.385 1.246796 0.699138 2.913074 0.026

8731.103 2.094176 4.708798 2.726146 0.012

8505.964 1.936932 1.440888 0.649581 0.08

8569.554 1.562873 1.562873 0.978287 0.053

8578.385 15.91449 12.8266 23.6342 0.1

8363.415 30.2439 29.87805 27.31707 0.26

8746.867 27.56892 23.5589 18.29574 0.005

8625.984 10.76115 13.12336 38.58268 0.005

8487.113 10.69588 12.8866 14.04639 0.005

8196.615 5.338542 7.552083 23.82813 0.005

8397.243 2.882206 4.761905 18.42105 0.076

6969.896 7.098725 11.17392 35.62508 0.22

8561.485 8.816705 12.64501 15.19722 0.17

8611.782 5.35973 7.436021 18.50555 0.135

8475.422 12.41679 18.6892 92.67793 0.16

8234.45 14.19856 18.39713 50.89713 0.13

8623.234 11.92947 16.74378 115.0306 0.212

8478.681 8.823908 13.71892 139.173 0.127

8782.016 3.514986 8.147139 34.6049 0.026

9217.429 1.662606 2.508241 10.69227 0.036

8455.187 4.02342 7.236151 12.7008 0.045

8593.575 25.89385 36.22905 22.5 0.146

8204.01 26.30049 40.39523 261.4066 0.229

8502.599 1.236129 5.183312 21.99747 0.128

8786.371 0.280755 0.204186 0.382848 0.076

8506.64 6.357728 15.2868 26.99915 0.154

Complete ProUCL Entry 239
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J K LMNO P Q R S

8497.561 13.39837 27.41463 135.5772 0.156

8290.27 12.1069 17.17112 41.50303 0.089

7591.82 23.12187 9.599332 20.67334 0.062

8135.55 17.03325 20.97187 14.34783 0.097

8262.277 2.729703 5.895596 21.79541 0.146

8557.445 13.83825 17.44769 43.65594 0.079

8336.538 2.678571 3.626374 4.162088 0.054

8772.545 14.95491 28.54459 21.54309 0.063

8211.382 7.154472 46.50407 18.37398 0.3

8468.363 6.484018 12.00261 22.3092 0.07

8140.627 23.30656 40.44552 22.4731 0.161

5.4 206

11.8 119

6.8 250

47 32

19.4 141

47 32

19.4 141

161

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10.4 2 34 0.02

1.2 2 10 0.06

10.1 231 3 0.08

7.1 198 391 0.09

55 52 7 0.05

9.9 142 260 0.27

70 8 225 0.26

5 2 150 0.24

10.8 76 228 0.04

51 311 80 0.2

3 14 27 0.19

37 67 44 0.24

2 47 2 0.04

6.9 14 16 0.08

2.5 66 10 0.1

Complete ProUCL Entry 240
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T U V W X Y Z AA AB AC

Nickel  (HA Selenium  ( FormaldehyBromine (mChlorine (mFluorine (mg/kg) Total Meta Total Halogens

22 30 17 7 175 49 251 184

2.44 0.29 15000 6 110 25 281.207 141

2.34 0.27 34000 6 95 24 106.338 125

1.2 0.27 18000 6 90 5 92.465 101

1.31 0.27 16000 7 110 25 86.09 142

1.35 0.27 17000 6 90 6 75.183 102

1.06 0.31 9300 6 90 6 87.298 102

5.05 0.27 110000 6 130 25 295.945 161

2.65 49000 1120 121.613 1120

1.26 130000 797 96.1488 797

2.93 0.6 46000 660 37 114.1578 697

2.16 46000 1340 97.5484 1340

12.2 0.6 29000 1960 47 167.701 2007

2.78 0.6 60000 1530 106.0868 1530

1.29 35000 179 76.1067 179

4.18 44000 516 47 210.5232 563

2.74 62000 597 42 121.9133 639

2.49 110000 385 105.0414 385

99 11.9 137.48 110.9

130 13.5 260.48 143.5

165 10.3 370.48 175.3

0.99 0.8 79.5 23.1 143.49 102.6

124 19.5 85.48 143.5

62 18.4 32.97 80.4

53.7 29.3 174.47 83

0.98 0.79 60.6 12.5 388.23 73.1

154 20.3 459.98 174.3

155 29.6 23.5 184.6

86.9 18.7 349.48 105.6

0.98 0.78 72.3 12.1 140.7 84.4

89.4 17.7 106.36 107.1

150 13.9 462.48 163.9

104.1 31.8 55.48 135.9

0.98 0.99 72.73 11.2 466.42 83.93

46.6 11.37 460.47 57.97

178.4 16.2 327.47 194.6

67.1 19.4 159.47 86.5

0.99 1 136 37.7 423.47 173.7

186.08

188.08

228.08

104.08

109.08

39.08

114.08

87.08

266.08

86.08

103.08

111.08

103.68

Complete ProUCL Entry 241
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T U V W X Y Z AA AB AC

159.88

81.08

201.08

178.08

107.78

89.08

172.08

23.2 372.68 23.2

14.1 52.07 14.1

33.9 303.74 33.9

13.3 308.48 13.3

28.9 240.47 28.9

14.9 49.46 14.9

16.6 142.49 16.6

17.2 125.18 17.2

33.8 314.48 33.8

31.8 8.01 31.8

322.08

48.48

242.58

97.58

442.08

31.48

56.08

9.08

18.92

13.88

800 16.13272 800

1700 8.335068 1700

1400 26.93048 1400

1100 22.62814 1100

1000 18.61671 1000

400 7.470024 400

1300 42.47659 1300

830 26.21134 830

1000 19.50192 1000

1400 10.67352 1400

1500 13.69032 1500

1300 11.61946 1300

600 23.542 600

700 10.38293 700

80.7649

1100 44.11494 1100

1300 18.09578 1300

1100 180.5421 1100

600 8.351384 600

1000 41.44404 1000

700 34.96324 700

500 10.61381 500

37.85806

1800 17.89203 1800

2100 48.38095 2100

Complete ProUCL Entry 242
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T U V W X Y Z AA AB AC

800 79.43971 800

600 30.79137 600

800 33.35396 800

1100 25.20612 1100

1600 29.22987 1600

1700 26.98768 1700

1200 27.15347

1100 97.28132 1100

1100 44.81297 1100

800 13.40426 800

900 31.81093 900

900 18.18074 900

600 13.6385 600

700 104.1879 700

700 29.33798 700

700 37.66265 700

700 81.13909 700

700 93.55556 700

1100 19.96458 1100

1100 27.32143 1100

1100 25.28235 1100

1700 210.2128 1700

700 48.28508 700

700 27.04494 700

794 88.19692 794

856 169.2062 856

900 95.44258 900

1600 6.959371 1600

1000 10.489 1000

1500 34.22442 1500

1900 25.03876 1900

1600 8.937853 1600

800 10.87356 800

600 16.77765 600

900 32.36934 900

1600 87.04276 1600

1500 70.16 1500

1500 80.91149 1500

900 51.85075 900

900 32.38579 900

800 83.18362 800

1000 79.42978 1000

600 158.6272 600

6460 47.04308 6460

900 70.91319 900

800 182.1749 800

600 44.3714 600

900 155.7143 54.14286 1055.714

900 47.8996 900

800 658.8072 82.34397 1458.807

900 418.1374 115.4629 1318.137

700 212.7931 48.12691 912.7931

Complete ProUCL Entry 243
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T U V W X Y Z AA AB AC

737 406.0189 71.13763 1143.019

600 37.66006 25.62839 637.6601

1900 256.1804 91.29925 2156.18

900 123.7011 49.49646 1023.701

653 178.2923 653

640 132.8671 640

895 32.16929 895

1000 89.41525 1000

970 108.0856 970

900 59.30855 900

1115 112.64 1115

800 163.0725 800

800 50.6447 800

900 62.92723 900

1200 58.41066 1200

1400 116.4012 1400

820 198.0289 820

760 36.88824 760

675 23.78167 675

9940 236.0842 9940

640 35.10135 640

2200 2200

1300 174.1586 1300

1800 63.15369 1800

1300 125.8413 1300

1500 139.6458 1500

900 4.885007 900

980 9.54112 980

1000 4.1074 1000

1000 4.157032 1000

2000 52.4753 2000

2100 87.69902 2100

1300 69.42856 1300

600 62.47219 600

500 37.63387 500

900 36.72375 900

700 26.14116 700

2200 54.11773 2200

300 36.82893 300

857 31.4363 857

820 123.9439 820

692 83.62282 692

645 143.9159 645

569 161.8428 569

586 46.29303 586

374 14.89912 374

500 24.00537 500

584 84.76891 584

482 328.3313 482

656 28.54491 656

460 0.94379 460

500 48.79768 500

Complete ProUCL Entry 244
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T U V W X Y Z AA AB AC

1870 176.5462 1870

514 70.87004 514

310 53.45655 310

341 52.44994 341

145 30.56671 145

400 75.02088 400

508 10.52103 508

460 65.10559 460

400 72.33252 400

1100 40.86583 1100

4290 86.38619 4290

211.4

130.8

256.8

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0.8 47.2

0.5 13.76

0.6 244.78

0.8 596.99

0.7 114.75

0.8 412.97

1.3 304.56

1.2 158.44

0.7 315.54

1 443.2

0.6 44.79

0.7 148.94

0.5 51.54

0.8 37.78

0.4 79

Complete ProUCL Entry 245
General Background Statistics for Full Data Sets

User Selected Options

From File    WorkSheet_a.wst

Full Precision    OFF

Confidence Coefficient    90%

Coverage    90%

Different or Future K Values    1

Number of Bootstrap Operations   2000

Moisture

General Statistics

Total Number of Observations 177 Number of Distinct Observations 144

Number of Missing Values 40

Raw Statistics Log‐Transformed Statistics

Minimum 3.9 Minimum 1.361

Maximum 38.5 Maximum 3.651

Second Largest 38.5 Second Largest 3.651

First Quartile 14.3 First Quartile 2.66

Median 18 Median 2.89

Third Quartile 22.91 Third Quartile 3.132

Mean 19.2 Mean 2.884

SD 6.946 SD 0.393

Coefficient of Variation 0.362

Skewness 0.53

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.104 Lilliefors Test Statistic 0.0622

Lilliefors Critical Value 0.0666 Lilliefors Critical Value 0.0666

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 29.05   90% UTL with   90% Coverage 31.24

   90% UPL (t) 28.16   90% UPL (t) 29.7

90% Percentile (z) 28.1 90% Percentile (z) 29.6

95% Percentile (z) 30.62 95% Percentile (z) 34.15

99% Percentile (z) 35.35 99% Percentile (z) 44.63

Gamma Distribution Test Data Distribution Test

k star 7.153 Data appear Gamma Distributed at 5% Significance Level

Theta Star 2.684

MLE of Mean 19.2

MLE of Standard Deviation 7.178

nu star 2532

A‐D Test Statistic 0.739 Nonparametric Statistics

5% A‐D Critical Value 0.754 90% Percentile 29.21

K‐S Test Statistic 0.0591 95% Percentile 31.97

5% K‐S Critical Value 0.0696 99% Percentile 38.12

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 30.34

90% Percentile 28.78   90% Percentile Bootstrap UTL with   90% Coverage 30.5

95% Percentile 32.32   90% BCA Bootstrap UTL with   90% Coverage 30.34

99% Percentile 39.7   90% UPL 29.38

Complete UPL Results 246
  90% Chebyshev UPL 40.09

   90% WH Approx. Gamma UPL 28.78 Upper Threshold Limit Based upon IQR 35.83

   90% HW Approx. Gamma UPL 28.96

   90% WH Approx. Gamma UTL with   90% Coverage 29.99

   90% HW Approx. Gamma UTL with   90% Coverage 30.23

Ash

General Statistics

Total Number of Observations 177 Number of Distinct Observations 168

Number of Missing Values 40

Raw Statistics Log‐Transformed Statistics

Minimum 0.49 Minimum ‐0.713

Maximum 20 Maximum 2.996

Second Largest 16.99 Second Largest 2.833

First Quartile 2.143 First Quartile 0.762

Median 4.227 Median 1.442

Third Quartile 7.201 Third Quartile 1.974

Mean 4.987 Mean 1.237

SD 3.857 SD 0.96

Coefficient of Variation 0.773

Skewness 1.127

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.122 Lilliefors Test Statistic 0.109

Lilliefors Critical Value 0.0666 Lilliefors Critical Value 0.0666

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 10.46   90% UTL with   90% Coverage 13.45

   90% UPL (t) 9.963   90% UPL (t) 11.89

90% Percentile (z) 9.93 90% Percentile (z) 11.8

95% Percentile (z) 11.33 95% Percentile (z) 16.72

99% Percentile (z) 13.96 99% Percentile (z) 32.17

Gamma Distribution Test Data Distribution Test

k star 1.475 Data do not follow a Discernable Distribution (0.05)

Theta Star 3.38

MLE of Mean 4.987

MLE of Standard Deviation 4.106

nu star 522.3

A‐D Test Statistic 1.568 Nonparametric Statistics

5% A‐D Critical Value 0.771 90% Percentile 9.947

K‐S Test Statistic 0.0845 95% Percentile 13.02

5% K‐S Critical Value 0.0709 99% Percentile 16.36

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 10.64

90% Percentile 10.43   90% Percentile Bootstrap UTL with   90% Coverage 10.64

95% Percentile 13.06   90% BCA Bootstrap UTL with   90% Coverage 10.64

99% Percentile 19.01   90% UPL 10.02

  90% Chebyshev UPL 16.59

   90% WH Approx. Gamma UPL 10.4 Upper Threshold Limit Based upon IQR 14.79

Complete UPL Results 247
   90% HW Approx. Gamma UPL 10.62

   90% WH Approx. Gamma UTL with   90% Coverage 11.27

   90% HW Approx. Gamma UTL with   90% Coverage 11.6

Volatile Matter

General Statistics

Total Number of Observations 7 Number of Distinct Observations 5

Raw Statistics Log‐Transformed Statistics

Minimum 80.57 Minimum 4.389

Maximum 81.44 Maximum 4.4

Second Largest 81.37 Second Largest 4.399

First Quartile 81.07 First Quartile 4.395

Median 81.24 Median 4.397

Third Quartile 81.31 Third Quartile 4.398

Mean 81.14 Mean 4.396

SD 0.306 SD 0.00377

Coefficient of Variation 0.00377

Skewness ‐1.317

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.844 Shapiro Wilk Test Statistic 0.844

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 81.85   90% UTL with   90% Coverage 81.86

   90% UPL (t) 81.61   90% UPL (t) 81.61

90% Percentile (z) 81.53 90% Percentile (z) 81.53

95% Percentile (z) 81.64 95% Percentile (z) 81.65

99% Percentile (z) 81.85 99% Percentile (z) 81.86

Gamma Distribution Test Data Distribution Test

k star 46893 Data appear Normal at 5% Significance Level

Theta Star 0.00173

MLE of Mean 81.14

MLE of Standard Deviation 0.375

nu star 656499

A‐D Test Statistic 0.858 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 81.4

Complete UPL Results 248
K‐S Test Statistic 0.351 95% Percentile 81.42

5% K‐S Critical Value 0.311 99% Percentile 81.44

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 81.44

90% Percentile 81.62   90% Percentile Bootstrap UTL with   90% Coverage 81.44

95% Percentile 81.76   90% BCA Bootstrap UTL with   90% Coverage 81.44

99% Percentile 82.02   90% UPL 81.44

  90% Chebyshev UPL 82.12

   90% WH Approx. Gamma UPL 81.61 Upper Threshold Limit Based upon IQR 81.67

   90% HW Approx. Gamma UPL 81.61

   90% WH Approx. Gamma UTL with   90% Coverage 81.86

   90% HW Approx. Gamma UTL with   90% Coverage 81.86

Fixed Carbon

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 17.85 Minimum 2.882

Maximum 18.78 Maximum 2.933

Second Largest 18.42 Second Largest 2.913

First Quartile 18.05 First Quartile 2.893

Median 18.13 Median 2.898

Third Quartile 18.33 Third Quartile 2.909

Mean 18.22 Mean 2.902

SD 0.309 SD 0.0169

Coefficient of Variation 0.017

Skewness 0.955

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.939 Shapiro Wilk Test Statistic 0.942

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 18.94   90% UTL with   90% Coverage 18.95

   90% UPL (t) 18.69   90% UPL (t) 18.69

90% Percentile (z) 18.61 90% Percentile (z) 18.61

95% Percentile (z) 18.72 95% Percentile (z) 18.73

99% Percentile (z) 18.94 99% Percentile (z) 18.94

Complete UPL Results 249
Gamma Distribution Test Data Distribution Test

k star 2327 Data appear Normal at 5% Significance Level

Theta Star 0.00783

MLE of Mean 18.22

MLE of Standard Deviation 0.378

nu star 32584

A‐D Test Statistic 0.317 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 18.56

K‐S Test Statistic 0.218 95% Percentile 18.67

5% K‐S Critical Value 0.311 99% Percentile 18.76

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 18.78

90% Percentile 18.7   90% Percentile Bootstrap UTL with   90% Coverage 18.78

95% Percentile 18.84   90% BCA Bootstrap UTL with   90% Coverage 18.78

99% Percentile 19.11   90% UPL 18.78

  90% Chebyshev UPL 19.21

   90% WH Approx. Gamma UPL 18.69 Upper Threshold Limit Based upon IQR 18.76

   90% HW Approx. Gamma UPL 18.69

   90% WH Approx. Gamma UTL with   90% Coverage 18.94

   90% HW Approx. Gamma UTL with   90% Coverage 18.94

Hydrogen

General Statistics

Total Number of Observations 7 Number of Distinct Observations 5

Raw Statistics Log‐Transformed Statistics

Minimum 5.95 Minimum 1.783

Maximum 6.12 Maximum 1.812

Second Largest 6 Second Largest 1.792

First Quartile 5.985 First Quartile 1.789

Median 5.99 Median 1.79

Third Quartile 6 Third Quartile 1.792

Mean 6.004 Mean 1.792

SD 0.0538 SD 0.0089

Coefficient of Variation 0.00896

Skewness 2.051

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Complete UPL Results 250
Shapiro Wilk Test Statistic 0.741 Shapiro Wilk Test Statistic 0.743

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 6.13   90% UTL with   90% Coverage 6.13

   90% UPL (t) 6.087   90% UPL (t) 6.087

90% Percentile (z) 6.073 90% Percentile (z) 6.073

95% Percentile (z) 6.093 95% Percentile (z) 6.093

99% Percentile (z) 6.129 99% Percentile (z) 6.13

Gamma Distribution Test Data Distribution Test

k star 8374 Data do not follow a Discernable Distribution (0.05)

Theta Star 7.17E‐04

MLE of Mean 6.004

MLE of Standard Deviation 0.0656

nu star 117230

A‐D Test Statistic 2.209 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6.048

K‐S Test Statistic 0.57 95% Percentile 6.084

5% K‐S Critical Value 0.311 99% Percentile 6.113

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 6.12

90% Percentile 6.089   90% Percentile Bootstrap UTL with   90% Coverage 6.12

95% Percentile 6.113   90% BCA Bootstrap UTL with   90% Coverage 6.048

99% Percentile 6.158   90% UPL 6.12

  90% Chebyshev UPL 6.177

   90% WH Approx. Gamma UPL 6.087 Upper Threshold Limit Based upon IQR 6.023

   90% HW Approx. Gamma UPL 6.087

   90% WH Approx. Gamma UTL with   90% Coverage 6.13

   90% HW Approx. Gamma UTL with   90% Coverage 6.13

Carbon

General Statistics

Total Number of Observations 7 Number of Distinct Observations 7

Raw Statistics Log‐Transformed Statistics

Minimum 50.2 Minimum 3.916

Maximum 50.72 Maximum 3.926

Second Largest 50.57 Second Largest 3.923

First Quartile 50.49 First Quartile 3.922

Median 50.53 Median 3.923

Third Quartile 50.57 Third Quartile 3.923

Mean 50.51 Mean 3.922

SD 0.157 SD 0.00311

Coefficient of Variation 0.00311

Skewness ‐1.183

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Complete UPL Results 251
Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.877 Shapiro Wilk Test Statistic 0.876

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data appear Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 50.87   90% UTL with   90% Coverage 50.88

   90% UPL (t) 50.75   90% UPL (t) 50.75

90% Percentile (z) 50.71 90% Percentile (z) 50.71

95% Percentile (z) 50.77 95% Percentile (z) 50.77

99% Percentile (z) 50.87 99% Percentile (z) 50.88

Gamma Distribution Test Data Distribution Test

k star 68974 Data appear Normal at 5% Significance Level

Theta Star 7.32E‐04

MLE of Mean 50.51

MLE of Standard Deviation 0.192

nu star 965640

A‐D Test Statistic 0.862 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 50.63

K‐S Test Statistic 0.315 95% Percentile 50.68

5% K‐S Critical Value 0.311 99% Percentile 50.71

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 50.72

90% Percentile 50.76   90% Percentile Bootstrap UTL with   90% Coverage 50.72

95% Percentile 50.83   90% BCA Bootstrap UTL with   90% Coverage 50.72

99% Percentile 50.96   90% UPL 50.72

  90% Chebyshev UPL 51.01

   90% WH Approx. Gamma UPL 50.75 Upper Threshold Limit Based upon IQR 50.68

   90% HW Approx. Gamma UPL 50.75

   90% WH Approx. Gamma UTL with   90% Coverage 50.88

   90% HW Approx. Gamma UTL with   90% Coverage 50.88

Nitrogen

General Statistics

Total Number of Observations 47 Number of Distinct Observations 23

Number of Missing Values 20

Raw Statistics Log‐Transformed Statistics

Minimum 0.08 Minimum ‐2.526

Maximum 1.26 Maximum 0.231

Second Largest 0.77 Second Largest ‐0.261

First Quartile 0.09 First Quartile ‐2.408

Median 0.14 Median ‐1.966

Complete UPL Results 252
Third Quartile 0.24 Third Quartile ‐1.428

Mean 0.239 Mean ‐1.771

SD 0.245 SD 0.761

Coefficient of Variation 1.025

Skewness 2.339

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.68 Shapiro Wilk Test Statistic 0.848

Shapiro Wilk Critical Value 0.946 Shapiro Wilk Critical Value 0.946

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.621   90% UTL with   90% Coverage 0.559

   90% UPL (t) 0.56   90% UPL (t) 0.463

90% Percentile (z) 0.552 90% Percentile (z) 0.451

95% Percentile (z) 0.641 95% Percentile (z) 0.595

99% Percentile (z) 0.808 99% Percentile (z) 1

Gamma Distribution Test Data Distribution Test

k star 1.535 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.155

MLE of Mean 0.239

MLE of Standard Deviation 0.193

nu star 144.3

A‐D Test Statistic 3.3 Nonparametric Statistics

5% A‐D Critical Value 0.766 90% Percentile 0.582

K‐S Test Statistic 0.19 95% Percentile 0.742

5% K‐S Critical Value 0.131 99% Percentile 1.035

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.7

90% Percentile 0.495   90% Percentile Bootstrap UTL with   90% Coverage 0.724

95% Percentile 0.617   90% BCA Bootstrap UTL with   90% Coverage 0.7

99% Percentile 0.893   90% UPL 0.644

  90% Chebyshev UPL 0.98

   90% WH Approx. Gamma UPL 0.489 Upper Threshold Limit Based upon IQR 0.465

   90% HW Approx. Gamma UPL 0.481

   90% WH Approx. Gamma UTL with   90% Coverage 0.568

   90% HW Approx. Gamma UTL with   90% Coverage 0.564

Oxygen

General Statistics

Total Number of Observations 7 Number of Distinct Observations 6

Raw Statistics Log‐Transformed Statistics

Minimum 42.36 Minimum 3.746

Maximum 43.08 Maximum 3.763

Second Largest 42.6 Second Largest 3.752

First Quartile 42.49 First Quartile 3.749

Median 42.57 Median 3.751

Third Quartile 42.59 Third Quartile 3.752

Mean 42.6 Mean 3.752

SD 0.233 SD 0.00546

Complete UPL Results 253
Coefficient of Variation 0.00547

Skewness 1.731

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Warning:  There are only 7 Values in this data

Note:  It should be noted that even though bootstrap methods may be performed on this data set,

the resulting calculations may not be reliable enough to draw conclusions

The literature suggests to use bootstrap methods on data sets having more than 10‐15 observations.

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.79 Shapiro Wilk Test Statistic 0.792

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 43.14   90% UTL with   90% Coverage 43.14

   90% UPL (t) 42.95   90% UPL (t) 42.95

90% Percentile (z) 42.89 90% Percentile (z) 42.89

95% Percentile (z) 42.98 95% Percentile (z) 42.98

99% Percentile (z) 43.14 99% Percentile (z) 43.14

Gamma Distribution Test Data Distribution Test

k star 22351 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.00191

MLE of Mean 42.6

MLE of Standard Deviation 0.285

nu star 312910

A‐D Test Statistic 2.281 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 42.79

K‐S Test Statistic 0.523 95% Percentile 42.94

5% K‐S Critical Value 0.311 99% Percentile 43.05

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 43.08

90% Percentile 42.96   90% Percentile Bootstrap UTL with   90% Coverage 43.08

95% Percentile 43.07   90% BCA Bootstrap UTL with   90% Coverage 43.08

99% Percentile 43.26   90% UPL 43.08

  90% Chebyshev UPL 43.34

   90% WH Approx. Gamma UPL 42.95 Upper Threshold Limit Based upon IQR 42.74

   90% HW Approx. Gamma UPL 42.95

   90% WH Approx. Gamma UTL with   90% Coverage 43.14

   90% HW Approx. Gamma UTL with   90% Coverage 43.14

Sulfur

General Statistics

Total Number of Observations 186 Number of Distinct Observations 160

Complete UPL Results 254
Number of Missing Values 31

Raw Statistics Log‐Transformed Statistics

Minimum 0.009 Minimum ‐4.711

Maximum 0.731 Maximum ‐0.313

Second Largest 0.625 Second Largest ‐0.47

First Quartile 0.0484 First Quartile ‐3.029

Median 0.107 Median ‐2.238

Third Quartile 0.17 Third Quartile ‐1.772

Mean 0.128 Mean ‐2.379

SD 0.113 SD 0.829

Coefficient of Variation 0.887

Skewness 2.652

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.18 Lilliefors Test Statistic 0.0934

Lilliefors Critical Value 0.065 Lilliefors Critical Value 0.065

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.288   90% UTL with   90% Coverage 0.299

   90% UPL (t) 0.274   90% UPL (t) 0.27

90% Percentile (z) 0.273 90% Percentile (z) 0.268

95% Percentile (z) 0.314 95% Percentile (z) 0.362

99% Percentile (z) 0.391 99% Percentile (z) 0.638

Gamma Distribution Test Data Distribution Test

k star 1.687 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0756

MLE of Mean 0.128

MLE of Standard Deviation 0.0982

nu star 627.6

A‐D Test Statistic 2.047 Nonparametric Statistics

5% A‐D Critical Value 0.769 90% Percentile 0.199

K‐S Test Statistic 0.094 95% Percentile 0.282

5% K‐S Critical Value 0.0684 99% Percentile 0.612

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.216

90% Percentile 0.258   90% Percentile Bootstrap UTL with   90% Coverage 0.216

95% Percentile 0.32   90% BCA Bootstrap UTL with   90% Coverage 0.22

99% Percentile 0.457   90% UPL 0.202

  90% Chebyshev UPL 0.468

   90% WH Approx. Gamma UPL 0.255 Upper Threshold Limit Based upon IQR 0.352

   90% HW Approx. Gamma UPL 0.257

   90% WH Approx. Gamma UTL with   90% Coverage 0.275

   90% HW Approx. Gamma UTL with   90% Coverage 0.278

Heating Value

General Statistics

Total Number of Observations 187 Number of Distinct Observations 186

Number of Missing Values 30

Complete UPL Results 255
Raw Statistics Log‐Transformed Statistics

Minimum 5468 Minimum 8.607

Maximum 11699 Maximum 9.367

Second Largest 10670 Second Largest 9.275

First Quartile 7600 First Quartile 8.936

Median 8241 Median 9.017

Third Quartile 8600 Third Quartile 9.06

Mean 8091 Mean 8.993

SD 864.2 SD 0.11

Coefficient of Variation 0.107

Skewness ‐0.146

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.109 Lilliefors Test Statistic 0.131

Lilliefors Critical Value 0.0648 Lilliefors Critical Value 0.0648

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 9313   90% UTL with   90% Coverage 9396

   90% UPL (t) 9205   90% UPL (t) 9269

90% Percentile (z) 9199 90% Percentile (z) 9260

95% Percentile (z) 9513 95% Percentile (z) 9638

99% Percentile (z) 10102 99% Percentile (z) 10387

Gamma Distribution Test Data Distribution Test

k star 83.9 Data do not follow a Discernable Distribution (0.05)

Theta Star 96.44

MLE of Mean 8091

MLE of Standard Deviation 883.3

nu star 31378

A‐D Test Statistic 3.327 Nonparametric Statistics

5% A‐D Critical Value 0.75 90% Percentile 9113

K‐S Test Statistic 0.124 95% Percentile 9232

5% K‐S Critical Value 0.0668 99% Percentile 9543

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 9207

90% Percentile 9242   90% Percentile Bootstrap UTL with   90% Coverage 9205

95% Percentile 9597   90% BCA Bootstrap UTL with   90% Coverage 9207

99% Percentile 10287   90% UPL 9167

  90% Chebyshev UPL 10691

   90% WH Approx. Gamma UPL 9243 Upper Threshold Limit Based upon IQR 10100

   90% HW Approx. Gamma UPL 9249

   90% WH Approx. Gamma UTL with   90% Coverage 9363

   90% HW Approx. Gamma UTL with   90% Coverage 9371

Antimony

General Statistics

Total Number of Observations 22 Number of Distinct Observations 18

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.17 Minimum ‐1.772

Complete UPL Results 256
Maximum 16.6 Maximum 2.809

Second Largest 7.4 Second Largest 2.001

First Quartile 0.47 First Quartile ‐0.765

Median 2 Median 0.693

Third Quartile 2.775 Third Quartile 1.017

Mean 2.6 Mean 0.318

SD 3.56 SD 1.197

Coefficient of Variation 1.369

Skewness 3.216

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.611 Shapiro Wilk Test Statistic 0.946

Shapiro Wilk Critical Value 0.911 Shapiro Wilk Critical Value 0.911

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 8.784   90% UTL with   90% Coverage 10.99

   90% UPL (t) 7.416   90% UPL (t) 6.942

90% Percentile (z) 7.162 90% Percentile (z) 6.374

95% Percentile (z) 8.456 95% Percentile (z) 9.846

99% Percentile (z) 10.88 99% Percentile (z) 22.26

Gamma Distribution Test Data Distribution Test

k star 0.821 Data appear Gamma Distributed at 5% Significance Level

Theta Star 3.168

MLE of Mean 2.6

MLE of Standard Deviation 2.87

nu star 36.12

A‐D Test Statistic 0.669 Nonparametric Statistics

5% A‐D Critical Value 0.775 90% Percentile 4.14

K‐S Test Statistic 0.138 95% Percentile 7.24

5% K‐S Critical Value 0.191 99% Percentile 14.67

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7.4

90% Percentile 6.283   90% Percentile Bootstrap UTL with   90% Coverage 7.4

95% Percentile 8.357   90% BCA Bootstrap UTL with   90% Coverage 7.4

99% Percentile 13.24   90% UPL 6.44

  90% Chebyshev UPL 13.52

   90% WH Approx. Gamma UPL 6.294 Upper Threshold Limit Based upon IQR 6.233

   90% HW Approx. Gamma UPL 6.323

   90% WH Approx. Gamma UTL with   90% Coverage 8.37

   90% HW Approx. Gamma UTL with   90% Coverage 8.656

Arsenic

General Statistics

Total Number of Observations 236 Number of Distinct Observations 217

Number of Missing Values 16

Raw Statistics Log‐Transformed Statistics

Minimum 0.104 Minimum ‐2.263

Maximum 220 Maximum 5.394

Second Largest 210 Second Largest 5.347

Complete UPL Results 257
First Quartile 4.015 First Quartile 1.39

Median 11.1 Median 2.407

Third Quartile 28.08 Third Quartile 3.335

Mean 26.12 Mean 2.379

SD 39.55 SD 1.418

Coefficient of Variation 1.514

Skewness 2.787

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.255 Lilliefors Test Statistic 0.0343

Lilliefors Critical Value 0.0577 Lilliefors Critical Value 0.0577

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 81.45   90% UTL with   90% Coverage 78.51

   90% UPL (t) 77.06   90% UPL (t) 67.06

90% Percentile (z) 76.81 90% Percentile (z) 66.46

95% Percentile (z) 91.18 95% Percentile (z) 111.3

99% Percentile (z) 118.1 99% Percentile (z) 292.5

Gamma Distribution Test Data Distribution Test

k star 0.68 Data appear Lognormal at 5% Significance Level

Theta Star 38.42

MLE of Mean 26.12

MLE of Standard Deviation 31.68

nu star 320.9

A‐D Test Statistic 4.4 Nonparametric Statistics

5% A‐D Critical Value 0.803 90% Percentile 65.35

K‐S Test Statistic 0.112 95% Percentile 110

5% K‐S Critical Value 0.0622 99% Percentile 199.5

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 82.12

90% Percentile 66.02   90% Percentile Bootstrap UTL with   90% Coverage 81.06

95% Percentile 89.85   90% BCA Bootstrap UTL with   90% Coverage 82.12

99% Percentile 146.9   90% UPL 65.79

  90% Chebyshev UPL 145

   90% WH Approx. Gamma UPL 61.32 Upper Threshold Limit Based upon IQR 64.17

   90% HW Approx. Gamma UPL 60.87

   90% WH Approx. Gamma UTL with   90% Coverage 67.49

   90% HW Approx. Gamma UTL with   90% Coverage 67.66

Beryllium

General Statistics

Total Number of Observations 22 Number of Distinct Observations 10

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.008 Minimum ‐4.828

Maximum 0.2 Maximum ‐1.609

Second Largest 0.2 Second Largest ‐1.609

First Quartile 0.008 First Quartile ‐4.828

Median 0.06 Median ‐2.827

Complete UPL Results 258
Third Quartile 0.17 Third Quartile ‐1.772

Mean 0.088 Mean ‐3.093

SD 0.0799 SD 1.351

Coefficient of Variation 0.908

Skewness 0.417

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.814 Shapiro Wilk Test Statistic 0.82

Shapiro Wilk Critical Value 0.911 Shapiro Wilk Critical Value 0.911

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.227   90% UTL with   90% Coverage 0.474

   90% UPL (t) 0.196   90% UPL (t) 0.282

90% Percentile (z) 0.19 90% Percentile (z) 0.256

95% Percentile (z) 0.219 95% Percentile (z) 0.419

99% Percentile (z) 0.274 99% Percentile (z) 1.052

Gamma Distribution Test Data Distribution Test

k star 0.794 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.111

MLE of Mean 0.088

MLE of Standard Deviation 0.0988

nu star 34.93

A‐D Test Statistic 1.281 Nonparametric Statistics

5% A‐D Critical Value 0.776 90% Percentile 0.2

K‐S Test Statistic 0.21 95% Percentile 0.2

5% K‐S Critical Value 0.192 99% Percentile 0.2

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.2

90% Percentile 0.214   90% Percentile Bootstrap UTL with   90% Coverage 0.2

95% Percentile 0.286   90% BCA Bootstrap UTL with   90% Coverage 0.2

99% Percentile 0.456   90% UPL 0.2

  90% Chebyshev UPL 0.333

   90% WH Approx. Gamma UPL 0.223 Upper Threshold Limit Based upon IQR 0.413

   90% HW Approx. Gamma UPL 0.232

   90% WH Approx. Gamma UTL with   90% Coverage 0.298

   90% HW Approx. Gamma UTL with   90% Coverage 0.322

Cadmium

General Statistics

Total Number of Observations 125 Number of Distinct Observations 91

Number of Missing Values 30

Raw Statistics Log‐Transformed Statistics

Minimum 1.12E‐06 Minimum ‐13.7

Maximum 1.773 Maximum 0.573

Second Largest 1.074 Second Largest 0.0717

First Quartile 0.0985 First Quartile ‐2.318

Median 0.236 Median ‐1.446

Third Quartile 0.39 Third Quartile ‐0.942

Mean 0.27 Mean ‐1.76

Complete UPL Results 259
SD 0.233 SD 1.437

Coefficient of Variation 0.864

Skewness 2.801

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.195 Lilliefors Test Statistic 0.193

Lilliefors Critical Value 0.0792 Lilliefors Critical Value 0.0792

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.606   90% UTL with   90% Coverage 1.373

   90% UPL (t) 0.571   90% UPL (t) 1.103

90% Percentile (z) 0.568 90% Percentile (z) 1.084

95% Percentile (z) 0.653 95% Percentile (z) 1.828

99% Percentile (z) 0.811 99% Percentile (z) 4.865

Gamma Distribution Test Data Distribution Test

k star 1.23 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.219

MLE of Mean 0.27

MLE of Standard Deviation 0.243

nu star 307.4

A‐D Test Statistic 2.284 Nonparametric Statistics

5% A‐D Critical Value 0.777 90% Percentile 0.4

K‐S Test Statistic 0.133 95% Percentile 0.526

5% K‐S Critical Value 0.085 99% Percentile 1.033

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.489

90% Percentile 0.59   90% Percentile Bootstrap UTL with   90% Coverage 0.489

95% Percentile 0.751   90% BCA Bootstrap UTL with   90% Coverage 0.4

99% Percentile 1.12   90% UPL 0.401

  90% Chebyshev UPL 0.971

   90% WH Approx. Gamma UPL 0.571 Upper Threshold Limit Based upon IQR 0.827

   90% HW Approx. Gamma UPL 0.595

   90% WH Approx. Gamma UTL with   90% Coverage 0.63

   90% HW Approx. Gamma UTL with   90% Coverage 0.663

Chromium

General Statistics

Total Number of Observations 231 Number of Distinct Observations 211

Number of Missing Values 21

Raw Statistics Log‐Transformed Statistics

Minimum 0.204 Minimum ‐1.589

Maximum 311 Maximum 5.74

Second Largest 240 Second Largest 5.481

First Quartile 8.945 First Quartile 2.191

Median 19 Median 2.944

Third Quartile 49.8 Third Quartile 3.908

Mean 39.01 Mean 2.977

SD 49.86 SD 1.264

Coefficient of Variation 1.278

Complete UPL Results 260
Skewness 2.503

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.218 Lilliefors Test Statistic 0.0341

Lilliefors Critical Value 0.0583 Lilliefors Critical Value 0.0583

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 108.8   90% UTL with   90% Coverage 115.2

   90% UPL (t) 103.2   90% UPL (t) 99.97

90% Percentile (z) 102.9 90% Percentile (z) 99.15

95% Percentile (z) 121 95% Percentile (z) 157

99% Percentile (z) 155 99% Percentile (z) 371.5

Gamma Distribution Test Data Distribution Test

k star 0.848 Data appear Lognormal at 5% Significance Level

Theta Star 46.02

MLE of Mean 39.01

MLE of Standard Deviation 42.37

nu star 391.6

A‐D Test Statistic 2.509 Nonparametric Statistics

5% A‐D Critical Value 0.791 90% Percentile 99

K‐S Test Statistic 0.0947 95% Percentile 146

5% K‐S Critical Value 0.0622 99% Percentile 227.7

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 120

90% Percentile 93.54   90% Percentile Bootstrap UTL with   90% Coverage 120

95% Percentile 124   90% BCA Bootstrap UTL with   90% Coverage 120

99% Percentile 195.4   90% UPL 99.8

  90% Chebyshev UPL 188.9

   90% WH Approx. Gamma UPL 89.39 Upper Threshold Limit Based upon IQR 111.1

   90% HW Approx. Gamma UPL 89.69

   90% WH Approx. Gamma UTL with   90% Coverage 97.68

   90% HW Approx. Gamma UTL with   90% Coverage 98.87

Cobalt

General Statistics

Total Number of Observations 22 Number of Distinct Observations 18

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.38 Minimum ‐0.968

Maximum 1.63 Maximum 0.489

Second Largest 1.58 Second Largest 0.457

First Quartile 0.633 First Quartile ‐0.459

Median 0.785 Median ‐0.242

Third Quartile 1.3 Third Quartile 0.261

Mean 0.903 Mean ‐0.202

SD 0.408 SD 0.462

Coefficient of Variation 0.452

Skewness 0.558

Complete UPL Results 261
Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.886 Shapiro Wilk Test Statistic 0.923

Shapiro Wilk Critical Value 0.911 Shapiro Wilk Critical Value 0.911

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.612   90% UTL with   90% Coverage 1.824

   90% UPL (t) 1.455   90% UPL (t) 1.527

90% Percentile (z) 1.426 90% Percentile (z) 1.478

95% Percentile (z) 1.574 95% Percentile (z) 1.748

99% Percentile (z) 1.852 99% Percentile (z) 2.396

Gamma Distribution Test Data Distribution Test

k star 4.5 Data appear Lognormal at 5% Significance Level

Theta Star 0.201

MLE of Mean 0.903

MLE of Standard Deviation 0.426

nu star 198

A‐D Test Statistic 0.749 Nonparametric Statistics

5% A‐D Critical Value 0.746 90% Percentile 1.513

K‐S Test Statistic 0.198 95% Percentile 1.577

5% K‐S Critical Value 0.186 99% Percentile 1.62

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.58

90% Percentile 1.473   90% Percentile Bootstrap UTL with   90% Coverage 1.58

95% Percentile 1.697   90% BCA Bootstrap UTL with   90% Coverage 1.58

99% Percentile 2.173   90% UPL 1.562

  90% Chebyshev UPL 2.155

   90% WH Approx. Gamma UPL 1.489 Upper Threshold Limit Based upon IQR 2.301

   90% HW Approx. Gamma UPL 1.496

   90% WH Approx. Gamma UTL with   90% Coverage 1.718

   90% HW Approx. Gamma UTL with   90% Coverage 1.739

Lead

General Statistics

Total Number of Observations 251 Number of Distinct Observations 224

Number of Missing Values 1

Raw Statistics Log‐Transformed Statistics

Minimum 0.383 Minimum ‐0.96

Maximum 451 Maximum 6.111

Second Largest 393 Second Largest 5.974

First Quartile 8.306 First Quartile 2.117

Median 18.37 Median 2.911

Third Quartile 37.41 Third Quartile 3.622

Mean 44.01 Mean 2.937

SD 69.95 SD 1.319

Coefficient of Variation 1.59

Skewness 2.983

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Complete UPL Results 262
Lilliefors Test Statistic 0.292 Lilliefors Test Statistic 0.0544

Lilliefors Critical Value 0.0559 Lilliefors Critical Value 0.0559

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 141.6   90% UTL with   90% Coverage 118.8

   90% UPL (t) 134.1   90% UPL (t) 103.1

90% Percentile (z) 133.7 90% Percentile (z) 102.3

95% Percentile (z) 159.1 95% Percentile (z) 165.1

99% Percentile (z) 206.7 99% Percentile (z) 405.6

Gamma Distribution Test Data Distribution Test

k star 0.706 Data appear Lognormal at 5% Significance Level

Theta Star 62.33

MLE of Mean 44.01

MLE of Standard Deviation 52.37

nu star 354.4

A‐D Test Statistic 7.939 Nonparametric Statistics

5% A‐D Critical Value 0.8 90% Percentile 132.8

K‐S Test Statistic 0.147 95% Percentile 212

5% K‐S Critical Value 0.0602 99% Percentile 335.5

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 150

90% Percentile 110.2   90% Percentile Bootstrap UTL with   90% Coverage 150

95% Percentile 149.3   90% BCA Bootstrap UTL with   90% Coverage 150

99% Percentile 242.6   90% UPL 135

  90% Chebyshev UPL 254.3

   90% WH Approx. Gamma UPL 101.6 Upper Threshold Limit Based upon IQR 81.07

   90% HW Approx. Gamma UPL 99.68

   90% WH Approx. Gamma UTL with   90% Coverage 111.4

   90% HW Approx. Gamma UTL with   90% Coverage 110.2

Manganese

General Statistics

Total Number of Observations 22 Number of Distinct Observations 22

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 31 Minimum 3.434

Maximum 156 Maximum 5.05

Second Largest 127 Second Largest 4.844

First Quartile 44.83 First Quartile 3.802

Median 60.3 Median 4.099

Third Quartile 76.98 Third Quartile 4.343

Mean 65.89 Mean 4.109

SD 29.5 SD 0.393

Coefficient of Variation 0.448

Skewness 1.726

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.841 Shapiro Wilk Test Statistic 0.964

Shapiro Wilk Critical Value 0.911 Shapiro Wilk Critical Value 0.911

Complete UPL Results 263
Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 117.1   90% UTL with   90% Coverage 120.5

   90% UPL (t) 105.8   90% UPL (t) 103.6

90% Percentile (z) 103.7 90% Percentile (z) 100.8

95% Percentile (z) 114.4 95% Percentile (z) 116.2

99% Percentile (z) 134.5 99% Percentile (z) 152

Gamma Distribution Test Data Distribution Test

k star 5.65 Data appear Gamma Distributed at 5% Significance Level

Theta Star 11.66

MLE of Mean 65.89

MLE of Standard Deviation 27.72

nu star 248.6

A‐D Test Statistic 0.444 Nonparametric Statistics

5% A‐D Critical Value 0.746 90% Percentile 89.45

K‐S Test Statistic 0.125 95% Percentile 125.2

5% K‐S Critical Value 0.186 99% Percentile 149.9

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 127

90% Percentile 103   90% Percentile Bootstrap UTL with   90% Coverage 127

95% Percentile 117.1   90% BCA Bootstrap UTL with   90% Coverage 127

99% Percentile 146.8   90% UPL 116.1

  90% Chebyshev UPL 156.4

   90% WH Approx. Gamma UPL 103.7 Upper Threshold Limit Based upon IQR 125.2

   90% HW Approx. Gamma UPL 103.6

   90% WH Approx. Gamma UTL with   90% Coverage 118

   90% HW Approx. Gamma UTL with   90% Coverage 118.5

Mercury

General Statistics

Total Number of Observations 153 Number of Distinct Observations 72

Number of Missing Values 99

Raw Statistics Log‐Transformed Statistics

Minimum 0.005 Minimum ‐5.298

Maximum 0.58 Maximum ‐0.545

Second Largest 0.35 Second Largest ‐1.05

First Quartile 0.051 First Quartile ‐2.976

Median 0.08 Median ‐2.526

Third Quartile 0.08 Third Quartile ‐2.526

Mean 0.0911 Mean ‐2.704

SD 0.0761 SD 0.868

Coefficient of Variation 0.836

Skewness 2.773

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.309 Lilliefors Test Statistic 0.207

Lilliefors Critical Value 0.0716 Lilliefors Critical Value 0.0716

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Complete UPL Results 264
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 0.2   90% UTL with   90% Coverage 0.231

   90% UPL (t) 0.189   90% UPL (t) 0.205

90% Percentile (z) 0.189 90% Percentile (z) 0.203

95% Percentile (z) 0.216 95% Percentile (z) 0.279

99% Percentile (z) 0.268 99% Percentile (z) 0.504

Gamma Distribution Test Data Distribution Test

k star 1.742 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0523

MLE of Mean 0.0911

MLE of Standard Deviation 0.069

nu star 533

A‐D Test Statistic 5.81 Nonparametric Statistics

5% A‐D Critical Value 0.768 90% Percentile 0.168

K‐S Test Statistic 0.217 95% Percentile 0.248

5% K‐S Critical Value 0.077 99% Percentile 0.328

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 0.22

90% Percentile 0.183   90% Percentile Bootstrap UTL with   90% Coverage 0.22

95% Percentile 0.226   90% BCA Bootstrap UTL with   90% Coverage 0.22

99% Percentile 0.321   90% UPL 0.182

  90% Chebyshev UPL 0.32

   90% WH Approx. Gamma UPL 0.181 Upper Threshold Limit Based upon IQR 0.124

   90% HW Approx. Gamma UPL 0.184

   90% WH Approx. Gamma UTL with   90% Coverage 0.196

   90% HW Approx. Gamma UTL with   90% Coverage 0.201

Nickel

General Statistics

Total Number of Observations 22 Number of Distinct Observations 19

Number of Missing Values 15

Raw Statistics Log‐Transformed Statistics

Minimum 0.98 Minimum ‐0.0202

Maximum 12.2 Maximum 2.501

Second Largest 5.05 Second Largest 1.619

First Quartile 1.095 First Quartile 0.0893

Median 1.755 Median 0.535

Third Quartile 2.718 Third Quartile 1

Mean 2.47 Mean 0.649

SD 2.439 SD 0.658

Coefficient of Variation 0.987

Skewness 3.307

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.595 Shapiro Wilk Test Statistic 0.871

Shapiro Wilk Critical Value 0.911 Shapiro Wilk Critical Value 0.911

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 6.706   90% UTL with   90% Coverage 6.001

Complete UPL Results 265
   90% UPL (t) 5.77   90% UPL (t) 4.661

90% Percentile (z) 5.596 90% Percentile (z) 4.447

95% Percentile (z) 6.482 95% Percentile (z) 5.648

99% Percentile (z) 8.143 99% Percentile (z) 8.845

Gamma Distribution Test Data Distribution Test

k star 1.85 Data do not follow a Discernable Distribution (0.05)

Theta Star 1.335

MLE of Mean 2.47

MLE of Standard Deviation 1.816

nu star 81.4

A‐D Test Statistic 1.278 Nonparametric Statistics

5% A‐D Critical Value 0.755 90% Percentile 4.055

K‐S Test Statistic 0.211 95% Percentile 5.007

5% K‐S Critical Value 0.188 99% Percentile 10.7

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 5.05

90% Percentile 4.894   90% Percentile Bootstrap UTL with   90% Coverage 5.05

95% Percentile 6.007   90% BCA Bootstrap UTL with   90% Coverage 5.05

99% Percentile 8.488   90% UPL 4.789

  90% Chebyshev UPL 9.951

   90% WH Approx. Gamma UPL 4.9 Upper Threshold Limit Based upon IQR 5.151

   90% HW Approx. Gamma UPL 4.826

   90% WH Approx. Gamma UTL with   90% Coverage 6.024

   90% HW Approx. Gamma UTL with   90% Coverage 5.991

Selenium

General Statistics

Total Number of Observations 30 Number of Distinct Observations 14

Number of Missing Values 222

Raw Statistics Log‐Transformed Statistics

Minimum 0.27 Minimum ‐1.309

Maximum 1.3 Maximum 0.262

Second Largest 1.2 Second Largest 0.182

First Quartile 0.425 First Quartile ‐0.861

Median 0.65 Median ‐0.434

Third Quartile 0.8 Third Quartile ‐0.223

Mean 0.65 Mean ‐0.535

SD 0.283 SD 0.486

Coefficient of Variation 0.436

Skewness 0.329

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.931 Shapiro Wilk Test Statistic 0.894

Shapiro Wilk Critical Value 0.927 Shapiro Wilk Critical Value 0.927

Data appear Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 1.12   90% UTL with   90% Coverage 1.31

   90% UPL (t) 1.028   90% UPL (t) 1.119

90% Percentile (z) 1.014 90% Percentile (z) 1.092

Complete UPL Results 266
95% Percentile (z) 1.116 95% Percentile (z) 1.303

99% Percentile (z) 1.31 99% Percentile (z) 1.814

Gamma Distribution Test Data Distribution Test

k star 4.467 Data appear Normal at 5% Significance Level

Theta Star 0.146

MLE of Mean 0.65

MLE of Standard Deviation 0.308

nu star 268

A‐D Test Statistic 0.908 Nonparametric Statistics

5% A‐D Critical Value 0.747 90% Percentile 1

K‐S Test Statistic 0.157 95% Percentile 1.11

5% K‐S Critical Value 0.16 99% Percentile 1.271

Data follow Appx. Gamma Distribution at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1.2

90% Percentile 1.063   90% Percentile Bootstrap UTL with   90% Coverage 1.2

95% Percentile 1.225   90% BCA Bootstrap UTL with   90% Coverage 1.02

99% Percentile 1.57   90% UPL 1

  90% Chebyshev UPL 1.515

   90% WH Approx. Gamma UPL 1.072 Upper Threshold Limit Based upon IQR 1.363

   90% HW Approx. Gamma UPL 1.082

   90% WH Approx. Gamma UTL with   90% Coverage 1.212

   90% HW Approx. Gamma UTL with   90% Coverage 1.232

Formaldehyde

General Statistics

Total Number of Observations 17 Number of Distinct Observations 15

Raw Statistics Log‐Transformed Statistics

Minimum 9300 Minimum 9.138

Maximum 130000 Maximum 11.78

Second Largest 110000 Second Largest 11.61

First Quartile 18000 First Quartile 9.798

Median 44000 Median 10.69

Third Quartile 60000 Third Quartile 11

Mean 48841 Mean 10.54

SD 36196 SD 0.761

Coefficient of Variation 0.741

Skewness 1.171

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.854 Shapiro Wilk Test Statistic 0.96

Shapiro Wilk Critical Value 0.892 Shapiro Wilk Critical Value 0.892

Data not Normal at 5% Significance Level Data appear Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 114682   90% UTL with   90% Coverage 150556

   90% UPL (t) 98630   90% UPL (t) 107423

90% Percentile (z) 95228 90% Percentile (z) 100008

95% Percentile (z) 108379 95% Percentile (z) 131865

99% Percentile (z) 133046 99% Percentile (z) 221518

Complete UPL Results 267
Gamma Distribution Test Data Distribution Test

k star 1.755 Data appear Gamma Distributed at 5% Significance Level

Theta Star 27829

MLE of Mean 48841

MLE of Standard Deviation 36868

nu star 59.67

A‐D Test Statistic 0.371 Nonparametric Statistics

5% A‐D Critical Value 0.749 90% Percentile 110000

K‐S Test Statistic 0.133 95% Percentile 114000

5% K‐S Critical Value 0.212 99% Percentile 126800

Data appear Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 110000

90% Percentile 97983   90% Percentile Bootstrap UTL with   90% Coverage 118000

95% Percentile 120806   90% BCA Bootstrap UTL with   90% Coverage 110000

99% Percentile 171832   90% UPL 114000

  90% Chebyshev UPL 160578

   90% WH Approx. Gamma UPL 100629 Upper Threshold Limit Based upon IQR 123000

   90% HW Approx. Gamma UPL 101728

   90% WH Approx. Gamma UTL with   90% Coverage 127788

   90% HW Approx. Gamma UTL with   90% Coverage 131635

Bromide

General Statistics

Total Number of Observations 7 Number of Distinct Observations 2

Raw Statistics Log‐Transformed Statistics

Minimum 6 Minimum 1.792

Maximum 7 Maximum 1.946

Second Largest 6 Second Largest 1.792

First Quartile 6 First Quartile 1.792

Median 6 Median 1.792

Third Quartile 6 Third Quartile 1.792

Mean 6.143 Mean 1.814

SD 0.378 SD 0.0583

Coefficient of Variation 0.0615

Skewness 2.646

Warning:  There are only 2 Distinct Values in this data

There are insufficient Distinct Values to perform some GOF tests and bootstrap methods.

Those methods will return a 'N/A' value on your output display!

It is necessary to have 4 or more Distinct Values to compute bootstrap methods.

However, results obtained using 4 to 9 distinct values may not be reliable.

It is recommended to have 10‐15 or more observations for accurate and meaningful bootstrap results.

Warning: A sample size of 'n' = 7 may not adequate enough to compute meaningful and reliable test statistics and estimates!

It is suggested to collect at least 8 to 10 observations using these statistical methods!

If possible compute and collect Data Quality Objectives (DQO) based sample size and analytical results.

Background Statistics

Complete UPL Results 268
Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.453 Shapiro Wilk Test Statistic 0.453

Shapiro Wilk Critical Value 0.803 Shapiro Wilk Critical Value 0.803

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 7.025   90% UTL with   90% Coverage 7.027

   90% UPL (t) 6.725   90% UPL (t) 6.709

90% Percentile (z) 6.627 90% Percentile (z) 6.609

95% Percentile (z) 6.765 95% Percentile (z) 6.75

99% Percentile (z) 7.022 99% Percentile (z) 7.024

Gamma Distribution Test Data Distribution Test

k star 189.5 Data do not follow a Discernable Distribution (0.05)

Theta Star 0.0324

MLE of Mean 6.143

MLE of Standard Deviation 0.446

nu star 2653

A‐D Test Statistic 2.109 Nonparametric Statistics

5% A‐D Critical Value 0.708 90% Percentile 6.4

K‐S Test Statistic 0.516 95% Percentile 6.7

5% K‐S Critical Value 0.311 99% Percentile 6.94

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 7

90% Percentile 6.721   90% Percentile Bootstrap UTL with   90% Coverage    N/A    

95% Percentile 6.895   90% BCA Bootstrap UTL with   90% Coverage    N/A    

99% Percentile 7.228   90% UPL 7

  90% Chebyshev UPL 7.355

   90% WH Approx. Gamma UPL 6.714 Upper Threshold Limit Based upon IQR 6

   90% HW Approx. Gamma UPL 6.713

   90% WH Approx. Gamma UTL with   90% Coverage 7.026

   90% HW Approx. Gamma UTL with   90% Coverage 7.026

Chloride

General Statistics

Total Number of Observations 175 Number of Distinct Observations 85

Number of Missing Values 42

Raw Statistics Log‐Transformed Statistics

Minimum 46.6 Minimum 3.842

Maximum 9940 Maximum 9.204

Second Largest 6460 Second Largest 8.773

First Quartile 504 First Quartile 6.223

Median 800 Median 6.685

Third Quartile 1100 Third Quartile 7.003

Mean 933.2 Mean 6.461

SD 989.5 SD 0.965

Coefficient of Variation 1.06

Skewness 5.615

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.202 Lilliefors Test Statistic 0.188

Complete UPL Results 269
Lilliefors Critical Value 0.067 Lilliefors Critical Value 0.067

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2337   90% UTL with   90% Coverage 2515

   90% UPL (t) 2210   90% UPL (t) 2221

90% Percentile (z) 2201 90% Percentile (z) 2203

95% Percentile (z) 2561 95% Percentile (z) 3127

99% Percentile (z) 3235 99% Percentile (z) 6034

Gamma Distribution Test Data Distribution Test

k star 1.448 Data do not follow a Discernable Distribution (0.05)

Theta Star 644.3

MLE of Mean 933.2

MLE of Standard Deviation 775.4

nu star 507

A‐D Test Statistic 3.777 Nonparametric Statistics

5% A‐D Critical Value 0.772 90% Percentile 1600

K‐S Test Statistic 0.131 95% Percentile 1918

5% K‐S Critical Value 0.0715 99% Percentile 4854

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1800

90% Percentile 1961   90% Percentile Bootstrap UTL with   90% Coverage 1800

95% Percentile 2460   90% BCA Bootstrap UTL with   90% Coverage 1600

99% Percentile 3587   90% UPL 1640

  90% Chebyshev UPL 3910

   90% WH Approx. Gamma UPL 1924 Upper Threshold Limit Based upon IQR 1994

   90% HW Approx. Gamma UPL 1955

   90% WH Approx. Gamma UTL with   90% Coverage 2086

   90% HW Approx. Gamma UTL with   90% Coverage 2136

Fluoride

General Statistics

Total Number of Observations 49 Number of Distinct Observations 44

Number of Missing Values 109

Raw Statistics Log‐Transformed Statistics

Minimum 5 Minimum 1.609

Maximum 658.8 Maximum 6.49

Second Largest 418.1 Second Largest 6.036

First Quartile 14.1 First Quartile 2.646

Median 23.2 Median 3.144

Third Quartile 37 Third Quartile 3.611

Mean 64.58 Mean 3.346

SD 124.6 SD 1.084

Coefficient of Variation 1.93

Skewness 3.381

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Shapiro Wilk Test Statistic 0.483 Shapiro Wilk Test Statistic 0.867

Shapiro Wilk Critical Value 0.947 Shapiro Wilk Critical Value 0.947

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Complete UPL Results 270
Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 258.4   90% UTL with   90% Coverage 153.3

   90% UPL (t) 228.2   90% UPL (t) 117.8

90% Percentile (z) 224.3 90% Percentile (z) 113.9

95% Percentile (z) 269.6 95% Percentile (z) 168.9

99% Percentile (z) 354.5 99% Percentile (z) 353.6

Gamma Distribution Test Data Distribution Test

k star 0.7 Data do not follow a Discernable Distribution (0.05)

Theta Star 92.26

MLE of Mean 64.58

MLE of Standard Deviation 77.19

nu star 68.59

A‐D Test Statistic 5.573 Nonparametric Statistics

5% A‐D Critical Value 0.794 90% Percentile 167.1

K‐S Test Statistic 0.302 95% Percentile 346.1

5% K‐S Critical Value 0.132 99% Percentile 543.3

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 256.2

90% Percentile 162.1   90% Percentile Bootstrap UTL with   90% Coverage 286.1

95% Percentile 219.8   90% BCA Bootstrap UTL with   90% Coverage 286.1

99% Percentile 357.6   90% UPL 212.8

  90% Chebyshev UPL 442.3

   90% WH Approx. Gamma UPL 146.6 Upper Threshold Limit Based upon IQR 71.35

   90% HW Approx. Gamma UPL 138.1

   90% WH Approx. Gamma UTL with   90% Coverage 179.4

   90% HW Approx. Gamma UTL with   90% Coverage 171.2

Total Metals

General Statistics

Total Number of Observations 251 Number of Distinct Observations 248

Number of Missing Values 1

Raw Statistics Log‐Transformed Statistics

Minimum 0.944 Minimum ‐0.0579

Maximum 597 Maximum 6.392

Second Largest 466.4 Second Largest 6.145

First Quartile 32.68 First Quartile 3.487

Median 79 Median 4.369

Third Quartile 153.7 Third Quartile 5.034

Mean 111 Mean 4.211

SD 111.5 SD 1.084

Coefficient of Variation 1.004

Skewness 1.742

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.174 Lilliefors Test Statistic 0.0641

Lilliefors Critical Value 0.0559 Lilliefors Critical Value 0.0559

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

Complete UPL Results 271
   90% UTL with   90% Coverage 266.6   90% UTL with   90% Coverage 306

   90% UPL (t) 254.6   90% UPL (t) 272.2

90% Percentile (z) 253.9 90% Percentile (z) 270.5

95% Percentile (z) 294.4 95% Percentile (z) 401

99% Percentile (z) 370.4 99% Percentile (z) 839.5

Gamma Distribution Test Data Distribution Test

k star 1.129 Data do not follow a Discernable Distribution (0.05)

Theta Star 98.36

MLE of Mean 111

MLE of Standard Deviation 104.5

nu star 566.7

A‐D Test Statistic 1.24 Nonparametric Statistics

5% A‐D Critical Value 0.781 90% Percentile 266.1

K‐S Test Statistic 0.0652 95% Percentile 371.6

5% K‐S Critical Value 0.0593 99% Percentile 461.5

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 308.5

90% Percentile 248.1   90% Percentile Bootstrap UTL with   90% Coverage 314.5

95% Percentile 318.8   90% BCA Bootstrap UTL with   90% Coverage 308.5

99% Percentile 481.4   90% UPL 278.2

  90% Chebyshev UPL 446.1

   90% WH Approx. Gamma UPL 242.9 Upper Threshold Limit Based upon IQR 335.2

   90% HW Approx. Gamma UPL 245.7

   90% WH Approx. Gamma UTL with   90% Coverage 262

   90% HW Approx. Gamma UTL with   90% Coverage 267

Total Halogens

General Statistics

Total Number of Observations 184 Number of Distinct Observations 104

Number of Missing Values 33

Raw Statistics Log‐Transformed Statistics

Minimum 13.3 Minimum 2.588

Maximum 9940 Maximum 9.204

Second Largest 6460 Second Largest 8.773

First Quartile 400 First Quartile 5.991

Median 800 Median 6.685

Third Quartile 1100 Third Quartile 7.003

Mean 898.5 Mean 6.314

SD 987.4 SD 1.187

Coefficient of Variation 1.099

Skewness 5.447

Background Statistics

Normal Distribution Test Lognormal Distribution Test

Lilliefors Test Statistic 0.188 Lilliefors Test Statistic 0.204

Lilliefors Critical Value 0.0653 Lilliefors Critical Value 0.0653

Data not Normal at 5% Significance Level Data not Lognormal at 5% Significance Level

Assuming Normal Distribution Assuming Lognormal Distribution

   90% UTL with   90% Coverage 2296   90% UTL with   90% Coverage 2962

   90% UPL (t) 2172   90% UPL (t) 2551

Complete UPL Results 272
90% Percentile (z) 2164 90% Percentile (z) 2527

95% Percentile (z) 2523 95% Percentile (z) 3889

99% Percentile (z) 3195 99% Percentile (z) 8733

Gamma Distribution Test Data Distribution Test

k star 1.149 Data do not follow a Discernable Distribution (0.05)

Theta Star 781.7

MLE of Mean 898.5

MLE of Standard Deviation 838

nu star 423

A‐D Test Statistic 3.941 Nonparametric Statistics

5% A‐D Critical Value 0.78 90% Percentile 1600

K‐S Test Statistic 0.14 95% Percentile 1985

5% K‐S Critical Value 0.0695 99% Percentile 4659

Data not Gamma Distributed at 5% Significance Level

Assuming Gamma Distribution   90% UTL with   90% Coverage 1700

90% Percentile 1999   90% Percentile Bootstrap UTL with   90% Coverage 1770

95% Percentile 2563   90% BCA Bootstrap UTL with   90% Coverage 1700

99% Percentile 3861   90% UPL 1600

  90% Chebyshev UPL 3869

   90% WH Approx. Gamma UPL 1957 Upper Threshold Limit Based upon IQR 2150

   90% HW Approx. Gamma UPL 2020

   90% WH Approx. Gamma UTL with   90% Coverage 2133

   90% HW Approx. Gamma UTL with   90% Coverage 2222

Complete UPL Results 273
137.48

260.48

370.48

143.49

85.48

32.97

174.47

388.23

459.98

23.5

349.48

140.7

106.36

462.48

55.48

466.42

460.47

327.47

159.47

423.47

186.08

188.08

228.08

104.08

109.08

39.08

114.08

87.08

266.08

86.08

103.08

111.08

103.68

159.88

81.08

201.08

178.08

107.78

89.08

172.08

372.68

52.07

303.74

308.48

240.47

49.46

142.49

Sheet1 274
125.18

314.48

8.01

322.08

48.48

242.58

97.58

442.08

31.48

56.08

9.08

18.92

13.88

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