Exhaust Emissions Sampling 

Hanson Brick, Elgin, TX 

Kiln #1 Dry Scrubber Exhaust 

January 27, 2011 

Armstrong Environmental, Inc. 

Project W-2658-11 

Report Prepared For: 

Paul Anderson 

Hanson Brick 

500 NE 14th Avenue 

Mineral Wells, TX 76067 

Report Prepared February 17, 2011 By: 

Armstrong Environmental, Inc. 

1748 Hlavek Rd. 

Decatur, Texas 76234 

(214) 631-0021 
I. Introduction 

II. Summary 

III. Procedures 

N. Appendices 

A. Calculation Summaries 

B. Continuous Emission Monitor Summaries 

C. Field Data Sheets 

D. Equipment Calibrations 

E. Standard Gas Certifications 

F. Production Data 

G. Hydrogen Halides and Chlorine Analysis Summary 

I. Metals Analysis Summary 

1 

2-5 

6-9 

10- 15 

16-29 

30-36 

37-44 

45-46 

47 

48-90 

91 - 104 
Testing followed procedures detailed in Title 40: Code of Federal Regulations ( 40:CFR). 

Sampling was perfom1ed by Lany Whicher and Tom Armstrong of Armstrong Environmental, Inc. using an Apex Method 5 sampling train, and a Teledyne Continuous 02 analyzer. 

Testing was performed according to the following schedule: 

Date Com_ponent Run Duration Start Time Finish Time 

1/27/10 HF, HCl, C12 60 minutes 8:43AM 12:34 PM 

1/27/10 Metals 60 minutes 1:18PM 5:14PM 

1 
Results of this test series are summarized in Tables 1 - 2. 

Production was maintained throughout testing at the following rates: 

1. Brick Weight- 1552 grams/Brick 

2. Brick/car - 5200 

3. Car/day- 18 

2 
STACK GAS 

Temperature, F 342.8 342.3 345.0 

Velocity, fps 19.82 18.99 18.88 

Volume Flow, acfm 19983.4 19139.1 19034.5 

scfm 12399.8 11742.8 11699.4 

scfh 743987 704565 701964 

Moisture, % 5.67% 6.78% 6.30% 

C02, % 3.25 2.75 2.50 

02,% 17.11 17.03 17.52 

SAMPLE 

Start Time, hrs:min 8:43AM 10:06 AM 11:30 AM 

Finish Time, hrs:min 9:47AM 11 :11 AM 12:34 PM 

Sample Volume, scf 42.365 39.019 38.651 

lsokinetic Ratio, % 102.0535 99.2533 98.67915 

HYDROGEN FLUORIDE 

Sample Weight, mg 0.373 0.471 0.491 

Concentration, ppm 0.373908 0.512631 0.539499 

Concentration, ppm@ 7% 02 1.371325 1.841233 2.218652 

Emissions, lbs/hr 0.014444 0.018753 0.019663 

Emissions, gr/hr 12.06552 14.42828 14.98541 

CHLORINE 

Sample Weight, mg (<0.025) (<0.025) (<0.025) 

Concentration, ppm (<0.007) (<0.008) (<0.008) 

Concentration, ppm @ 7% 02 (<0.026) (<0.028) (<0.032) 

Emissions, lbs/hr (<0.001) (<0.001) (<0.001) 

Emissions, gr/hr (<0.439) (<0.451) (<0.454) 

HYDROGEN CHLORIDE 

Sample Weight, mg 0.995 1.183 1.076 

Concentration, ppm 0.546533 0.705514 0.647827 

Concentration, ppm@ 7% 02 2.004435 2.534018 2.66414 

Emissions, lbs/hr 0.038529 0.047101 0.04309 

Emissions, gr/hr 17.47348 21 .36118 19.54213 

3 
STACK GAS 

Temperature, F 350.3 

Velocity, fps 19.88 

Volume Flow, acfm 20042.9 

scfm 12342.6 

seth 740554 

Moisture,% 5.51% 

C02,% 2.50 

02,% 16.85 

SAMPLE 

Start Time, hrs:min 1:18PM 

Finish Time, hrs:min 2:22PM 

Sample Volume, scf 40.867 

lsokinetic Ratio, % 98.90028 

PARTICULATE 

Front Half 

Sample Weight, mg 7.55 

Concentration, gr/scf 0.002851 

Concentration, mg/dscm@ 7% 02 22.38946 

Emissions, lbs/hr 0.301677 

Emissions, gr/hr 136.815 

Antimony 

Sample Weight, ug 6.00 

Concentration, mg/dscm @ 7% 02 0.017793 

Emissions, gr/hr 0.108727 

Arsenic 

Sample Weight, ug (<2.20) 

Concentration, mg/dscm@ 7% 02 (<0.0065) 

Emissions, gr/hr (<0.0399) 

Berylium 

Sample Weight, ug (<1.00) 

Concentration, mg/dscm@ 7% 02 (<0.0030) 

Emissions, gr/hr (<0.0181) 

Cadmium 

Sample Weight, ug (<1.00) 

Concentration, mg/dscm @ 7% 02 <0.0030) 

Emissions, gr/hr (<0.0181) 

350.9 

20.32 

20483.9 

12550.7 

753040 

5.90% 

2.50 

16.98 

2:45PM 

3:49PM 

42.095 

100.1831 

7.55 

0.002767 

22.45713 

0.297814 

135.0632 

(<5.00) 

(<0.0149) 

(<0.0894) 

(<2.1 0) 

(<0.0060) 

(<0.0376) 

(<0.90) 

(<0.0026) 

(<0.0161) 

0.45 

0.001296 

0.00805 

4 

351.0 

19.98 

20143.0 

12414.3 

744859 

5.36% 

2.75 

17.11 

4:10PM 

5:14PM 

41.528 

99.91998 

8.94 

0.003322 

27.87901 

0.353572 

160.3501 

(<5.00) 

(<0.0156) 

(<0.0897) 

(<2.20) 

(<0.0069) 

(<0.0395) 

(<1.00) 

(<0.0031) 

(<0.0179) 

0.81 

0.002526 

0.014528 
Emissions, gr/hr (<0.0181) 

Lead 

Sample Weight, ug 2.50 

Concentration, mg/dscm @ 7% 02 0.007414 

Emissions, gr/hr 0.045303 

Manganese 

Sample Weight, ug 226.60 

Concentration, mg/dscm @ 7% 02 0.67198 

Emissions, gr/hr 4.106261 

Nickel 

Sample Weight, ug 5.70 

Concentration, mg/dscm @ 7% 02 0.016903 

Emissions, gr/hr 0.103291 

Selenium 

Sample Weight, ug 4.10 

Concentration, mg/dscm @ 7% 02 0.012159 

Emissions, gr/hr 0.074297 

Mercury 

Sample Weight, ug 17.22 

Concentration, mg/dscm@ 7% 02 0.051066 

Emissions, gr/hr 0.312047 

2 

5 

0.007513 

2.10 

0.006046 

0.037567 

7.80 

0.022456 

0.139535 

7.40 

0.021304 

0.13238 

2.30 

0.006622 

0.041145 

32.10 

0.092415 

0.574242 

(<0.0179) 

2.30 

0.007172 

0.041253 

35.00 

0.109146 

0.627769 

3.80 

0.01185 

0.068158 

3.20 

0.009979 

0.057396 

19.82 

0.061808 

0.355497 
2 

3 

3A 

4 

5 

26A 

29 

p

y 

ary Sources 

Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

Gas Analysis for C02, 02, Excess Air and Dry Molecular Weight 

Determination of Oxygen and Carbon Dioxide Concentrations in 

Emissions from Stationary Sources (Instrumental Analyzer Procedure) 

Determination ofMoisture Content in Stack Gas 

Determination ofParticulate Emissions from Stationary Sources 

Determination ofHydrogen Halides and Halogen Emissions from 

Stationary Sources 

Determination of Metals Emissions from Stationary Sources 

C02 was determined using PyRite Analyzers. 

Method 26A sampling was performed for 5 minutes at each of 12 points, 6 points per 

traverse, making a total run duration of 60 minutes. The sampling train was configured as follows: 

Glass Sample Nozzle 

Heated Glass lined probe 

Heated Teflon filter 

Impinger #1 - 100 mls 0.1 N H2S04 

Impinger #2 - 100 mls 0.1 N H2S04 

Impinger #3 - 100 m~s 0.1 N NaOH 

Impinger#4- 100 mls 0.1 NNaOH 

Impinger #5 - 200 grams silica Gel 

Analysis for HF and HCl was perfom1ed on the solution from the 1st and 2nd impingers. 

Analysis for Cl2 ,;r,,as perfonned on the solution from 3rd and 4th impingers. Analysis 

was perfom1ed using a Dionex LC20 HPLC/Ion Chromatograph by Am1strong 

Environnmeta1, Inc. 

6 
Impinger #1- 100 mls 5% HN03110% H202 

Impinger #2 - 100 mls 5% HN0311 0% H202 

Impinger #3- 100 mls 4% K.Mn04110% H2S04 

Impinger #4 - 100 mls 4% K.Mn04/1 0% H2S04 

Impinger #5 - 200 grams silica Gel 

The probe was washed with acetone and recovered, then washed with 0.1 N HN03, 

recovered separately. PM was determined from the probe wash and filter, then both were 

digested and analyzed for metals. Metals and mercury was determined from the probe wash, filter, and the solution from the 1st and 2nd impingers. Mercury was also analyzed in the solution from the 3rd and 4th impingers. 

Metals analyzed for were beryllium, antimony, arsenic, cadmium, chromium, cobalt, 

manganese, mercury, selenium and nickel. 

02 was determined using a Teledyne continuous 02 analyzer. The analyzer was calibrated with 9.01 %, and 20%02 in N2 EPA Protocol! gas standards, zeroed with N2. 

Sampling was perfonned for five minutes at each of 12 points, 6 points per port. 

7 
Figure 1 - Kiln #1 Dry Scrubber Exhaust 

612inches 

() 1h ' 

423inches 

co 

Cyclone 

CEMS and Sampling Traverse Points 

~ 

//// ~\ 

/ \ 

/1 2 3 4 5 6\ 

,// 

,// 

Stack Diameter- 55.5 inches 

Point #1 - 2.4 inches 

Point #2- 8.1 inches 

Point #3- 16.4 inches 

Point #4- 39.1 inches 

Point #5 - 4 7.4 inches 

Point #6- 53.1 inches 
\.0 

Figure 2- GEM Configuration 

Heated Frobg 

Heated Filter 

I 

Heated 

Sample Line 

'------.,r-, 

'._j 

Heated 

Sample 

Pump 

Bias Calibration Span Line 

Processor 

{~' 

\._/ 

Purnp 

02 .1\nalyzer 

Flovvmeter 

:alibration Point 
Appendix A 
NOZZLE DIAMETER (INCH.) : 0.4147 PARTICULATE WEIGHT (Front half mg) : 

METER COEFFICIENT (Y) : 0.995 PARTICULATE WEIGHT (Back half mg): 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 41.652 PERCENT C02 

BAROMETRIC PRESSURE 29.95 PERCENT02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 55.5 STACK LENGTH(inchs): 

STACK AREA (Sq.Ft.) : 16.80016 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000938 STACK AREA (Sq.Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 16.8002 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU. FT.): 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

ISOKINETIC RATIO(%): 

POINTS STACK T. DELTA P SQUAR D.F DELTA H 

deg F 

1 342 0.08 0.28284 1.20 

2 345 0.09 0.3 1. 40 

3 345 0.10 0.31623 1.55 

4 345 0.09 0.3 1. 40 

5 344 0.09 0.3 1.40 

6 336 0.07 0.26458 1.10 

7 335 0.08 0.28284 1.20 

8 347 0.09 0.3 1.40 

g 347 0.08 0.28284 1.20 

10 348 0.08 0.28284 1.20 

11 345 0.08 0.28284 1.20 

12 334 0.05 0.22361 0.78 

342.75 0.2849 1.2525 

42.3652 

2.5465 

0.0567 

79.6400 

29.2044 

28.5691 

29.9228 

19.8246 

19983.4253 

743986.768 

102.0535 

METER T. 

INLET 

46 

59 

62 

64 

65 

66 

56 

68 

69 

71 

72 

73 

64.2500 

METER T. 

OUTLET 

46 

46 

48 

49 

51 

52 

53 

54 

56 

57 

59 

60 

52.5833 

0 

0 

-0.37 

3.25 

17.11 

0 

0 

58.4167 

-- li 

.1. 'J 
NOZZLE DIAMETER (INCH.) : 0.4147 PARTICULATE WEIGHT (Front half mg): 

METER COEFFICIENT (Y) : 0.995 PARTICULATE WEIGHT (Back half mg): PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 39.762 PERCENT C02 

BAROMETRIC PRESSURE 29.95 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 55.5 STACK LENGTH(inches): 

STACK AREA (Sq. Ft.) : 16.80016 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000938 STACK AREA (Sq. Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 16.8002 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

ISOKINETIC RATIO(%): 

POINTS STACK T. DELTAP SQUARD.F DELTAH 

deg F 

1 341. 0.07 0.26458 1..1.0 

2 344 0.08 0.28284 1.20 

3 344 0.08 0.28284 1.20 

4 343 0.28284 1.20 

5 342 0.08 0.28284 1.20 

6 337 0.06 0.24495 0.93 

7 338 0.07 0.26458 1.1.0 

8 345 0.08 0.28284 1.20 9 346 0.08 0.28284 1.20 

10 345 0.08 0.28284 1.20 

11 344 0.07 0.26458 1.10 

12 338 0.06 0.24495 0.93 

342.25 0.2720 1.1300 

39.0194 

2.8383 

0.0678 

80.2200 

29.1212 28.3671 

29.9213 

18.9870 

19139.1067 

704565.453 

99.2533 

METER T. 

INLET 

72 

78 

79 

81 

82 83 

73 

84 

86 86 88 89 

81.7500 

METER T. 

OUTLET 

63 

89 

65 67 69 69 

77 72 

73 

74 76 

77 

72.5833 

0 

0 

-0.39 

2.75 

17.03 

0 

0 

77.1667 
(

) 

(

g)

METER COEFFICIENT (Y) : 0.995 PARTICULATE WEIGHT (Back half mg) : 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 40.057 PERCENT C02 

BAROMETRIC PRESSURE 29.95 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 55.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 16.80016 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000938 STACK AREA (Sq. Ft.): 

ENTER THE STACK AREA SHOWN ABOVE: 16.8002 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULARWT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

ISOKINETIC RATIO(%): 

POINTS STACKT. DELTA P SQUAR D.F DELTA H 

deg F 

1 335 0.07 0.26458 1.10 

2 347 0.08 0.28284 1.20 

3 347 0.08 0.28284 1.30 

4 347 0.08 0.28284 1.30 

5 347 0.07 0.26458 1.10 

6 346 0.06 0.24495 0.97 

7 341 0.08 0.28284 1.30 

8 349 0.08 0.28284 1.30 

9 350 0.08 0.28284 1.30 

10 349 0.08 0.28284 1.30 

11 347 0.07 0.26458 1.10 

12 335 0.05 0.22361 0.81 

345 0.2702 1.1733 

38.6505 

2.5983 

0.0630 

79.9800 

29.1008 

28.4016 

29.9228 

18.8832 

19034.4742 

701964.133 

98.6791 

METER T. 

INLET 

79 

88 

90 

91 

92 

92 

85 

93 

93 

94 

94 

95 

90.5000 

METER T. 

OUTLET 

79 

79 

80 

81 

81 

82 

83 

83 

84 

85 

85 

85 

82.2500 

0 

-0.37 

2.5 

17.52 

0 

0 

86.3750 
METER COEFFICIENT (Y) : 0.995 PARTICULATE WEIGHT (Back half mg): 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 42.282 PERCENT C02 

BAROMETRIC PRESSURE 29.95 PERCENT02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 55.5 STACK LENGTH(inchs): 

STACK AREA (Sq. Ft.) : 16.80016 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000938 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 16.8002 

FLOWS 

SAMPLED VOLUME (STD. CU.FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT(%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (fUsee.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO(%): 

POINTS STACKT. DELTA P SQUAR D.F DELTA H 

deg F 

1 339 0.08 0.28284 1.30 

2 351 0.08 0.28284 1.30 

3 358 0.08 0.28284 1.30 

4 355 0.08 0.28284 1.30 

5 353 0.07 0.26458 1.10 

6 342 0.06 0.24495 0.97 

7 346 0.08 0.28284 1.30 

8 353 0.09 0.3 1.45 9 354 0.09 0.3 1.45 

10 355 0.09 0.3 1.45 

11 356 0.09 0.3 1.45 

12 341 0.08 0.28284 1.30 

350.25 0.2839 1.3058 

40.8667 

2.3817 

0.0551 

80.6500 

29.0740 

28.4641 

29.9221 

19.8837 

20042.9362 

740553.565 

0.0029 

4.07E-07 

0.3017 

98.9003 

METERT. 

INLET 

83 

89 

90 91 91 

91 

88 89 89 88 

88 87 

88.6667 

METER T. 

OUTLET 

83 

84 84 84 84 

83 

88 81 

81 

80 80 

79 

82.5833 

0 

-0.38 

2.5 

16.85 

0 

0 

85.6250 

1 '') 

• .!,.. .J 
METER COEFFICIENT (Y) : 0.995 PARTICULATE WEIGHT (Back half mg): 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20): 

GAS METER VOL.(Cu.Ft.) : 43.165 PERCENT C02 

BAROMETRIC PRESSURE 29.95 PERCENT02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 55.5 STACK LENGTH(inches): 

STACKAREA(Sq.Ft.): 16.80016 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000938 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 16.8002 

FLOWS 

SAMPLED VOLUME (STD. CU. FT.): 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (ACFM): 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (LBS/HR): 

ISOKINETIC RATIO (%): 

POINTS STACKT. DELTA P SQUAR D.F DELTA H 

deg F 

1 349 0.08 0.28284 1.30 

2 357 0.09 0.3 1.45 

3 356 0.09 0.3 1. 45 

4 355 0.09 0.3 1. 45 

5 353 0.09 0.3 1.45 

6 344 0.07 0.26458 1.10 

7 349 0.08 0.28284 1.30 

8 353 0.09 0.3 1. 45 

9 355 0.09 0.3 1.45 

10 354 0.09 0.3 1.45 

11 353 0.08 0.28284 1. 30 

12 333 0.07 0. 26458 1.10 

350.916667 0.2898 1.3542 

42.0948 

2.6406 

0.0590 

80.5200 

29.0792 

28.4252 29.9213 20.3212 

20483.9251 

753040.244 

0.0028 

3.95E-07 

0.2978 

100.1831 

METER T. 

INLET 

74 

84 85 

86 

87 87 82 

87 

88 

87 

87 87 

85.0833 

METER T. 

OUTLET 

74 

75 75 

76 76 

77 77 77 

78 78 78 78 

76.5833 

0 

-0.39 

2.5 

16.98 

0 

0 

80.8333 

-< ' ' 1_ 4 
METER COEFFICIENT (Y) 

PITOT COEFFICIENT (Cp) 

GAS METER VOL. (Cu.Ft.) 

BAROMETRIC PRESSURE 

0.84 

42.391 

29.95 

(

g) 

STATIC PRESSURE (in. H20) 

PERCENT C02 

PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK 

STACK DIAMETER (inch) : 

STACK AREA (Sq. Ft . ) 

NOZZLE AREA (feet): 

55.5 

16.8002 

0. 00094 

FOR RECTANGULAR STACK 

STACK LENGTH(inchs) 

STACK WIDTH(inchs) 

STACK AREA (Sq. Ft. ) 

ENTER THE STACK AREA SHOWN ABOVE: 16.8002 

FLOWS 

S}I.MPLED VOLUHE (STD. CU. FT . ) : 

VOLUME OF WATER VAPOR (STD. CU.FT.): 

FRACTIONAL MOISTURE CONTENT (%): 

DRY BASE: 

MOLECULAR WT. OF STACK GAS (DRY BASE): 

MOLECULAR WT. OF STACK GAS (WET BASE): 

STACK PRESSURE (inch Hg): 

STACK GAS VELOCITY (ft/sec.): 

ACTUAL STACK GAS FLOW RATE (AC:FM) : 

STANDARD STACK GAS FLOW RATE (SCFH): 

PARTICULATE 

FRONT HALF 

PARTICULATE CONCENTRATION (GR./SCF): 

PARTICULATE CONCENTRATION (LBS/SCF): 

PARTICULATE EMISSION (I,BS/HR): 

ISOKINETIC RATIO (%): 

POINTS STACK T. DELTA P SQUAR D.P DELTA H 

deg F 

1 345 0.08 0.28284 1. 30 

2 354 0.09 0.3 1. 45 

3 354 0.08 0.28284 1. 30 

4 354 0.08 0.28284 1. 30 

5 353 0.08 0.28284 1. 30 

6 354 0.07 0. 26458 1.10 

7 344 0.08 0.28284 1.30 

8 356 0.09 0.3 1. 45 

9 356 0.09 0.3 1.45 

1 0 356 0.09 0.3 1. 45 

11 355 0.08 0.28284 1. 30 

12 331 0.07 0 . 26458 1.10 

351 0.2855 1. 31 67 

41.5281 

2.3535 

0.0536 

80.1400 

29.1244 

28.5278 

29.9287 

19.9830 

20143.007 

744859.17 

0.0033 

4.75E-07 

0.3536 

99.9200 

METER T. 

INLET 

74 

83 

83 

83 

84 

84 

79 

84 

84 

84 

85 

85 

82.6667 

HETER T. 

OUTLET 

74 

74 

74 

74 

74 

74 

74 

74 

74 

74 

74 

74 

74.0000 

-0.29 

2.75 

17.11 

0 

0 

78.3333 

15 
Appendix B 
Value Response Difference 

Zero Gas 0 0.05 0.05 0.25 

Low Range 9.01 9.08 0.07 0.35 

Mid Range 20 20.13 0.13 0.65 

System Calibration Bias and Drift Data 

Analyzer Initial Values Final Values Drift Average 

Calibration System System System System Calibration 

Response Calibration Calibration Calibration Calibration Values 

Response Bias Response Bias 

Run #1 Zero Gas 0.05 0.44 1.95 0.37 1.6 -0.35 0.405 

Upscale 9.08 9.15 0.35 9.28 1 0.65 9.215 

Average 02 Concentration: 17.14 

Corrected 02 Concentration: 17.11491 

Run #2 Zero Gas 0.05 0.37 1.6 0.31 1.3 -0.3 0.34 

Upscale 9.08 9.28 1 9.29 1.05 0.05 9.285 

Average 02 Concentration: 17.25 

Corrected 02 Concentration: 17.03288 

Run #3 Zero Gas 0.05 0.31 1.3 0.31 1.3 0 0.31 

Upscale 9.08 9.29 1.05 9.35 1.35 0.3 9.32 

Average 02 Concentration: 17.83 

Corrected 02 Concentration: 17.52 

Run#4 Zero Gas 0.05 0.31 1.3 0.34 1.45 0.15 0.325 

Upscale 9.08 9.35 1.35 9.16 0.4 -0.95 9.255 

Average 02 Concentration: 17.03 

Corrected 02 Concentration: 16.85465 

Run#5 Zero Gas 0.05 0.34 1.45 0.34 1.45 0 0.34 

Upscale 9.08 9.16 0.4 9.14 0.3 -0.1 9.15 

Average 02 Concentration: 16.94 

Corrected 02 Concentration: 16.97684 

Run#6 Zero Gas 0.05 0.34 1.45 0.44 1.95 0.5 0.39 

Upscale 9.08 9.14 0.3 9.08 0 -0.3 9.11 

Average 02 Concentration: 16.95 

Corrected 02 Concentration: 17.11073 

Page 1 if .L I 
01/27/11 07:47:06 0.06 

01/27/11 07:48:06 5.79 

01/27/11 07:49:06 9.16 

01/27/11 07:50:06 9.08 9.0T% 02 

01/27/11 07:51:06 12.91 

01/27/11 07:52:06 20.26 

01/27/11 07:53:06 20.13 20%02 

01/27/11 07:54:06 20.28 

01/27/11 07:55:06 20.93 

01/27/11 07:56:06 19.52 

01/27/11 07:57:06 2.71 

01/27/11 07:58:06 0.54 

01/27/11 07:59:06 0.45 

01/27/11 08:00:06 0.44 Zero N2 Bias 

01/27/11 08:01:06 1.57 

01/27/11 08:02:06 10.45 

01/27/11 08:03:06 9.15 9.0f% 02 Bias 

01/27/11 08:04:06 9.23 

Page 1 

(\ .... . 17 
01/27/11 08:46:06 

01/27/11 08:47:06 

01/27/11 08:48:06 

01/27/11 08:49:06 

01/27/11 08:50:06 

01/27/11 08:51 :06 

01/27/11 08:52:06 

01/27/11 08:53:06 

01/27/11 08:54:06 

01/27/11 08:55:06 

01/27/11 08:56:06 

01/27/11 08:57:06 

01/27/11 08:58:06 

01/27/11 08:59:06 

01/27/11 09:00:06 

01/27/11 09:01 :06 

01/27/11 09:02:06 

01/27/11 09:03:06 

01/27/11 09:04:06 

01/27/11 09:05:06 

01/27/11 09:06:06 

01/27/11 09:07:06 

01/27/11 09:08:06 

01/27/11 09:09:06 

01/27/11 09:10:06 

01/27/11 09:11:06 

01/27/11 09:12:06 

Port Change 

01/27/11 09:13:06 

01/27/11 09:14:06 

01/27/11 09:15:06 

01/27/11 09:16:06 

Resume 

01/27/11 09:17:06 

01/27/11 09:18:06 

01/27/11 09:19:06 

01/27/11 09:20:06 

01/27/11 09:21:06 

01/27/11 09:22:06 

01/27/11 09:23:06 

01/27/11 09:24:06 

01/27/11 09:25:06 

01/27/11 09:26:06 

16.80 

17.19 

17.15 

16.99 

17.10 

18.07 

18.63 

17.68 

16.57 

16.50 

16.72 

16.78 

16.65 

16.64 

16.55 

16.70 

16.70 

16.67 

16.59 

16.48 

16.57 

16.66 

16.72 

16.73 

16.88 

16.77 

17.26 

20.48 

20.65 

17.54 

17.23 

17.40 

17.54 

17.57 

17.47 

17.55 

17.85 

17.72 

17.56 

17.38 

17.05 

Page 1 1 0 0 
01/27/11 09:35:06 16.97 

01/27/11 09:36:06 17.26 

01/27/11 09:37:06 17.23 

01/27/11 09:38:06 17.18 

01/27/11 09:39:06 17.01 

01/27/11 09:40:06 17.09 

01/27/11 09:41:06 17.02 

01/27/11 09:42:06 17.11 

01/27/11 09:43:06 16.86 

01/27/11 09:44:06 16.74 

01/27/11 09:45:06 16.79 

01/27/11 09:46:06 16.96 

Stop Run #1 17.14 

01/27/11 09:47:06 16.96 

01/27/11 09:48:06 19.71 

01/27/11 09:49:06 3.63 

01/27/11 09:50:06 0.51 

01/27/11 09:51:06 0.37 Zero N2 

01/27/11 09:52:06 2.09 

01/27/11 09:53:06 9.51 

01/27/11 09:54:06 9.28 9.01%02 

Page 2 19 
01/27/1110:09:06 17.19 

01/27/1110:10:06 17.11 

01/27/1110:11:06 18.32 

01/27/1110:12:06 18.86 

01/27/11 10:13:06 17.86 

01/27/1110:14:06 16.82 

01/27/1110:15:06 16.88 

01/27/1110:16:06 16.89 

01/27/1110:17:06 17.04 

01/27/1110:18:06 16.94 

01/27/1110:19:06 16.89 

01/27/11 10:20:06 16.86 

01/27/11 10:21 :06 16.80 

01/27/11 10:22:06 16.78 

01/27/11 10:23:06 16.77 

01/27/11 10:24:06 16.83 

01/27/11 1 0:25:0~ 16.84 

01/27/11 10:26:06 16.78 

01/27/1110:27:06 16.70 

01/27/1110:28:06 16.79 

01/27/11 10:29:06 16.89 

01/27/1110:30:06 16.91 

01/27/11 10:31 :06 16.68 

01/27/1110:32:06 16.62 

01/27/1110:33:06 16.82 

01/27/1110:34:06 17.06 

01/27/1110:35:06 17.10 

Port Change 

01/27/11 10:36:06 17.51 

01/27/11 10:37:06 21 .13 

01/27/1110:38:06 21.28 

01/27/1110:39:06 18.52 

Resume 

01/27/11 10:40:06 17.50 

01/27/1110:41:06 17.20 

01/27/11 10:42:06 17.19 

01/27/11 10:43:06 17.33 

01/27/11 10:44:06 17.53 

01/27/11 1 0:45:06 17.51 

01/27/1110:46:06 17.22 

01/27/1110:47:06 17.25 

01/27/11 10:48:06 17.39 

01/27/11 10:49:06 17.75 

Page 1 
01/27/11 10:58:06 17.46 

01/27/11 10:59:06 17.27 

01/27/1111:00:06 17.23 

01/27/11 11:01:06 16.87 

01/27/11 11:02:06 17.03 

01/27/11 11 :03:06 17.14 

01/27/1111:04:06 17.27 

01/27/11 11 :05:06 17.25 

01/27/11 11:06:06 17.21 

01/27/11 11 :07:06 16.99 

01/27/11 11:08:06 17.12 

01/27/11 11:09:06 17.30 

01/27/1111:10:06 17.14 

Stop Run #2 17.25 

01/27/11 11:11:06 17.10 

01/27/1111:12:06 20.73 

01/27/1111:13:06 11.12 

01/27/1111:14:06 0.64 

01/27/11 11:15:06 0.31 Zero N2 

01/27/1111:16:06 2.16 

01/27/11 11:17:06 10.51 

01/27/1111:18:06 10.03 

01/27/1111:19:06 9.29 9.01% 02 

Page 2 
01/27/11 11:33:06 18.71 

01/27/1111:34:06 17.58 

01/27/11 11:35:06 17.38 

01/27/1111:36:06 17.55 

01/27/11 11:37:06 17.50 

01/27/11 11 :38:06 17.53 

01/27/11 11:39:06 17.40 

01/27/1111:40:06 17.26 

01/27/11 11:41:06 17.45 

01/27/11 11:42:06 17.46 

01/27/11 11:43:06 17.50 

01/27/1111 :44:06 17.49 

01/27/11 11:45:06 17.41 

01/27/11 11:46:06 17.41 

01/27/1111 :47:06 17.57 

01/27/11 11:48:06 17.42 

01/27/11 11:49:06 17.45 

01/27/11 11:50:06 17.32 

01/27/11 11:51:06 17.42 

01/27/11 11:52:06 17.54 

01/27/11 11 :53:06 17.68 

01/27/11 11:54:06 17.80 

01/27/11 11:55:06 17.99 

01/27/11 11 :56:06 17.97 

01/27/11 11 :57:06 18.03 

01/27/1111:58:06 18.17 

01/27/1111 :59:06 18.17 

Port Change 

01/27/11 12:00:06 20.90 

01/27/11 12:01 :06 21.95 

01/27/11 12:02:06 20.00 

01/27/11 12:03:06 18.29 

Resume 

01/27/11 12:04:06 18.04 

01/27/11 12:05:06 17.98 

01/27/11 12:06:06 18.30 

01/27/11 12:07:06 18.28 

01/27/11 12:08:06 18.35 

01/27/11 12:09:06 18.14 

01/27/1112:10:06 18.01 

01/27/11 12:11 :06 18.90 

01/27/11 12:12:06 19.79 

01/27/1112:13:06 19.10 

P!:ll1P 1 

I 

-;::,~ I C l ·.,. 1 
01/27/11 12:22:06 17.74 

01/27/11 12:23:06 17.54 

01/27/11 12:24:06 17.40 

01/27/11 12:25:06 17.47 

01/27/1112:26:06 17.56 

01/27/11 12:27:06 17.50 

01/27/1112:28:06 17.41 

01/27/11 12:29:06 17.59 

01/27/11 12:30:06 17.43 

01127/11 12:31:06 17.55 

01/27/11 12:32:06 17.72 

01/27/1112:33:06 17.75 

Stop Run #3 17.83 

01/27/11 12:34:06 17.52 

01/27/11 12:35:06 17.49 

01/27/11 12:36:06 9.81 

01/27/11 12:37:06 1.15 

01/27/11 12:38:06 0.53 

01/27/11 12:39:06 0.39 

01 t?7t11 1 ?·A.n·nR 0.31 7P.rn N? 

01/27/11 12:41:06 5.36 

01/27/11 12:42:06 9.35 9.01%02 

Page 2 

2 •") ,., ,j 
01/27/1113:21:06 16.86 

01/27/1113:22:06 17.02 

01/27/1113:23:06 17.16 

01/27/11 13:24:06 17.07 

01/27/11 13:25:06 16.98 

01/27/11 13:26:06 16.94 

01/27/1113:27:06 16.93 

01/27/11 13:28:06 17.32 

01/27/1113:29:06 17.16 

01/27/11 13:30:06 16.89 

01/27/1113:31:06 17.47 

01/27/1113:32:06 18.55 

01/27/1113:33:06 18.15 

01/27/1113:34:06 17.16 

01/27/1113:35:06 16.81 

01/27/11 13:36:06 16.96 

01/27/11 13:37:06 16.80 

01/27/11 13:38:06 16.95 

01/27/11 13:39:06 16.83 

01/27/11 13:40:06 16.87 

01/27/1113:41:06 16.47 

01/27/11 13:42:06 16.53 

01/27/11 13:43:06 16.83 

01/27/11 13:44:06 16.80 

01/27/1113:45:06 16.60 

01/27/11 13:46:06 16.43 

01/27/11 13:47:06 16.68 

Port Change 

01/27/11 13:48:06 18.89 

01/27/11 13:49:06 20.97 

01/27/11 13:50:06 19.32 

01/27/11 13:51 :06 16.75 

Resume 

01/27/1113:52:06 16.70 

01/27/11 13:53:06 17.00 

01/27/11 13:54:06 16.98 

01/27/1113:55:06 16.82 

01/27/1113:56:06 16.56 

01/27/1113:57:06 17.04 

01/27/11 13:58:06 17.22 

01/27/11 13:59:06 17.32 

01/27/11 14:00:06 17.20 

01/27/11 14:01:06 16.64 

Page 1 
01/27/1114:10:06 17.10 

01/27/1114:11:06 17.50 

01/27/1114:12:06 18.60 

01/27/1114:13:06 18.12 

01/27/11 14:14:06 16.88 

01/27/1114:15:06 16.58 

01/27/11 14:16:06 16.64 

01/27/1114:17:06 16.68 

01/27/1114:18:06 16.64 

01/27/1114:19:06 16.80 

01/27/1114:20:06 16.81 

01/27/11 14:21:06 16.75 

01/27/11 14:22:06 16.89 

Stop Run #4 17.03 

01/27/1114:23:06 19.93 

01/27/11 14:24:06 20.95 

01/27/11 14:25:06 14.82 

01/27/1114:26:06 1.67 

01/27/11 14:27:06 0.44 

01/27/1114:28:06 0.39 

01/27/11 14:29:06 0.34 Zero N2 

01/27/11 14:30:06 4.51 

01/27/1114:31:06 9.11 

01/27/11 14:32:06 9.16 9.01% 02 

Page 2 
01/27/1114:48:06 17.06593 

01/27/1114:49:06 17.19923 

01/27/11 14:50:06 17.25489 

01/27/11 14:51 :06 17.43946 

01/27/11 14:52:06 18.60792 

01/27/1114:53:06 18.21339 

01/27/11 14:54:06 17.21388 

01/27/11 14:55:06 16.65333 

01/27/11 14:56:06 16.66114 

01/27/1114:57:06 16.80323 

01/27/1114:58:06 16.81056 

01/27/1114:59:06 16.72804 

01/27/11 15:00:06 16.65285 

01/27/11 15:01 :06 16.6216 

01/27/1115:02:06 16.66456 

01/27/1115:03:06 16.74415 

01/27/11 15:04:06 16.82568 

01/27/11 15:05:06 16.98193 

01/27/11 15:06:06 16.70166 

01/27/11 15:07:06 16.86377 

01/27/11 15:08:06 16.93799 

01/27/1115:09:06 16.97315 

01/27/1115:10:06 16.94531 

01/27/1115:11:06 16.93946 

01/27/1115:12:06 17.06543 

01/27/1115:13:06 17.13721 

01/27/1115:14:06 17.23096 

Port Change 

01/27/11 15:15:06 17.16309 

01/27/11 15:16:06 19.96045 

01/27/1115:17:06 20.87842 

01/27/1115:18:06 18.98292 

Resume 

01/27/11 15:19:06 16.91309 

01/27/11 15:20:06 16.73633 

01/27/1115:21:06 16.79005 

01/27/11 15:22:06 16.8418 

01/27/11 15:23:06 16.85352 

01/27/11 15:24:06 16.98096 

01/27/1115:25:06 16.78272 

01/27/11 15:26:06 16.75147 

01/27/11 15:27:06 16.84864 

01/27/11 15:28:06 17.07667 

Page 1 ~, ., l; ,26 
01/27/11 15:37:06 

01/27/11 15:38:06 

01/27/1115:39:06 

01/27/11 15:40:06 

01/27/1115:41:06 

01/27/1115:42:06 

01/27/11 15:43:06 

01/27/1115:44:06 

01/27/11 15:45:06 

01/27/11 15:46:06 

01/27/1115:47:06 

01/27/1115:48:06 

Stop Run #5 

01/27/11 15:49:06 

01/27/11 15:50:06 

01/27/11 15:51 :06 

01/27/1115:52:06 

01/27/11 15:53:06 

01/27/11 15:54:06 0~ !27!~ 5:55:06 

01/27/11 15:56:06 

01/27/1115:57:06 

16.67384 

16.51416 

16.63281 

16.72217 

16.63916 

16.61768 

16.52637 

16.61963 

16.64404 

16.6626 

16.67969 

16.56153 

16.94583 

16.66651 

18.86329 

6.239015 

0.77652 

0.411285 

0.3432 377~98 8.896732 

9.1379 

Zero N2 

9.01% 02 

Page 2 ~~~'I u • 2 ,, ~ I 
01/27/1116:13:06 18.32 

01/27/11 16:14:06 17.38 

01/27/1116:15:06 16.57 

01/27/11 16:16:06 16.63 

01/27/11 16:17:06 16.69 

01/27/1116:18:06 16.64 

01/27/11 16:19:06 16.68 

01/27/11 16:20:06 16.73 

01/27/11 16:21 :06 16.55 

01/27/11 16:22:06 16.61 

01/27/1116:23:06 16.82 

01/27/11 16:24:06 16.90 

01/27/11 16:25:06 16.70 

01/27/11 16:26:06 16.60 

01/27/11 16:27:06 16.70 

01/27/11 16:28:06 16.80 

01/27/11 16:29:06 17.02 

01/27/11 16:30:06 17.01 

01/27/11 16:31:06 16.91 

01/27/11 16:32:06 16.97 

01/27/11 16:33:06 17.18 

01/27/11 16:34:06 17.44 

01/27/11 16:35:06 17.19 

01/27/1116:36:06 16.97 

01/27/11 16:37:06 17.02 

01/27/11 16:38:06 17.43 

01/27/11 16:39:06 17.35 

Port Change 

01/27/11 16:40:06 18.51 

01/27/11 16:41:06 20.58 

01/27/11 16:42:06 20.21 

01/27/11 16:43:06 17.60 

Resume 

01/27/11 16:44:06 17.12 

01/27/1116:45:06 17.34 

01/27/11 16:46:06 16.91 

01/27/11 16:47:06 16.93 

01/27/11 16:48:06 17.00 

01/27/11 16:49:06 17.15 

01/27/11 16:50:06 17.15 

01/27/1116:51:06 17.05 

01/27/11 16:52:06 18.14 

01/27/11 16:53:06 18.29 

Page 1 ,. : u ... ~ 2 gr "' 
01/27/1117:02:06 16.52 

01/27/1117:03:06 16.66 01/27/1117:04:06 16.71 01/27/11 17:05:06 16.57 

01/27/11 17:06:06 16.58 01/27/11 17:07:06 16.41 01/27/11 17:08:06 16.56 

01/27/11 17:09:06 16.59 

01/27/1117:10:06 16.64 

01/27/11 17:11:06 16.62 

01/27/11 17:12:06 16.49 

01/27/11 17:13:06 16.89 

Stop Run #6 16.95 

01/27/11 17:14:06 16.95 

01/27/11 17:15:06 19.37 

01/27/1117:16:06 20.77 

01/27/1•1 17:17:06 11.02 

01/27/1117:18:06 1.57 01/27/1117:19:06 0.58 

01/27111 17:20:06 0_44 Zer0 "!2 

01/27/1117:21:06 1.93 01/27/1117:22:06 8.83 

01/27/11 17:23:06 9.01%02 

Page 2 :,.., ' 29 
Appendix C 
·.~ 

8 arometric Pressure: 2 'i · "i 0 1 Ambient Temperature: 'l/ 1 I d ' . yt, :~ssume. "1mstun;.:._ . 1,f /)}-, f,l 1 , ~~"f.-"' ,_1 :)tack Drameter: 5;.2.- : I· ~,} 1r r ;#. (J ),.....: 7 ~lfpt·e,· H· 1 ,.., ~ .L . ' . . 1• ('0" ''•v ' .. I' '"I/ ; \ . k ( Factor: '•1 "( I ' .2: Y0 '2- C" () ~ ;!t () • • ..,) ; ..J ~vleter Co-Effiecent: (} . c{ '7 r;- ! ), i: ,r; •. ~ f : I '7/3 Nozzle Diameter.: ,. q1;,--, • ti,r.r, • 't!t.( ('irv,~ ) / '1 "" ·· ' 0 Probe Length: {:;; 0 (,. "" I j Filter Number: ,p · be 0 y ~ 7f?) ·~·"- Pretest Leak Check . . } Post Test Leak Check_ Meter 0 ;;:::.{! c'J~~-@ _l$}r1.Hg y----· Meter<)-~· tCu.ft{CY_. ~ in.Hg P1tots.. v @ .:,:r..~ m. H20 . P1tots c- @ ;.ajn 0 

~-

_ 

-·····

-~ 

. 

______ _______ 

=-=~-

..:._ _ __________ 

L : -· · , -~: -!~-~~ T - --~--~:t·= ===~ ~-==::·t----= , =-=L ....~.. __ ___ ___ .•.. ___ __ _ t__ _ ____ __ _ j_____ .... _l _____ ___ ~---- ___ L ___ __ _________ __j __ ___ ______ __ -~

_______ . ____ ...;._ ____ __ __ _ _ __ 

~; , 

C:- ~I ! ~·:. () , .. v ·.. ,, 
Baromen-ic Pressure: 2 q-'7 s-

 

Ambient Temperature: 5'2... 

Assumed Moisture: >? 

StCJ,ck Diameter: !,-s'. Sl'---lcter H (. 1./7 ·1. 

<i Factor , S Vi 

Meter Co-Effiecent O·<i'?s 

'!'Jozzle Diameter: 1 '-f 1 '{ 7 

Probe Length: (, 0 

Filter Number: 

#5 'l. .... c~, 1 

#6 

.,.o 

Pretest Leak Check ./ Post 'I est Leak Check Meter() ,ooc cu.ft~i), IS. in.Hg Meter cu.ft@ in.Hg Pitots !:;::" 0J. $."·~n H20 Pitots c in.E2C 

., ~I;;~~~~ ~~f:~~,w~ ,;_ if: <~~ rW; :~B.~~;\' E~ ~~ . -- .,. -:~~-~\!l7i};*; \6 £~E:--:1~· }\';; :: :·~; r.- ·~·~·.<,.- ,(~-=-:2.·~=-:- . ,~- ~::'!:'" . ~~~.··.~~~-:-~~i_ ... "--·:. ;_~~cE=,~ ~-t"'~:~ :-;. ~::-:-ca:-c-~ C; :---. ._ 5" .' 1-G _ Jifz.._j___Q

_i~ 

~I· 0 

~ ~ LJ :. 23 · · 

~~~ YJo cO :l_j .SJ1 L.LQ (ol_eji 'Z!!J.. .. 9 23 G _bG i <:/.£ ., 8:1 1--=--f-- ~ ,,td I -,. 7 ,yo ··_ f1!___mlL1t a! (._d~z. q o o, I ?3 7'7 2 42- 2:0'-J_& 'Ll >-<> 

~I · .')~ i~ rt~t~.:~~u~~ : Y~ ~ $~ .. ~ r ~~ 4~ J :: i ~1+-~-~ 

i-i

__Qfij,]_ l £7· ~ I [(;. I ] i.{ I 21.f!.( i 2:_5"L' 2i l ~ . .'P s11 u .c{) r l4.:u__,_Q'ifl ;, r "'l ... o I 8 ~ I J'=--t- 2Hs1_ __ lli s.Yll_r b lE_ ~ I 3 ~3. .L~zh.L_£__:/J I /4 . 2- I 85 I -Z2i Vt

c;j_

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1---

---+ (~ :'*--

__ I_J=+ l '(NilL I __ l_j ___ ~- ~~-±~:-+--=-

__ I · _I - - i 

·-t- 1 C),'7? 1/ t· j--- : +------"- --i---- 1 ·-+ 

--~-

:--- · -+----1----------1--- ----r 1 

:----

--~ --- --:-· ---- -~ B--r--=+ --: __ -t::__ ·=r= -:---=-T·-- : -=~+ ~-= =:r · -1 

~-~--

~-----i-

----+--·-~--- -- ---

-~--- --;- ---:- --;--·---: -l 

I 

t-

-=~· ~ i ~~=~~~~~=~-~ ' : -:-~ ~~---~::~:-~ ~--~~~: _~ -:·--] r---- --. ---t------.:.------- - I 7- ··· · --- ·· ---

---'---·--

----

·-----------·-------------- -·-- · ------ · · i l 

_______ •-----'-· ----·-----L ... _ __ ___ _ _ . . ............... ------ -- ·--· ... 

__ 

·- ·-'··--- ------·-'-· ..... 

___ _ 

--'--- -· 

_ .. J 

r) ·; 

l'l , v L• .,r .l. 
Barometric Pressure: 2.--

1 ,Cj (' 

Ambieni Temperature: 

Assumed Moisture: ~ Stack Diameter: :)~. S 

:·vJo-tn H I .41 

<~ 

r co2 02 

J '('3" . ~ .?.-' 7/ j) 

Post Test Leak Check 

Meter & .&.:.of'cu ftWl 

.~~ 

.. .._-

I 

1 

I 

I 

! 

I 

; 

i 

-I 

I 

I ~ r;: 

... 

''· 
Barometric Pressure: 2--'1 .'1 5 

Ambient Temperature: & ~ 

Assumed Moisture: (? 

Stack Diameter: .)5· , J 

\J~

1er H: i. 4 7 -z__ 

(' Factor , j 0 f 

Meter Co-Effiecent: () .cici 5' 

Nozzle Diameter: , 

Probe Length: G() 

Filter Number: 

';.fl 1..( 7 

Pr.etest Leak Check .. / 

Meter 0 

-C~u.f£ (,.~ /$ in.Hg 

P!tots ;,.;-(cU ,:,~ 1 nL H20 

#4 tcc3l<'.L!t\ j'CO 

#5 'Z.-'-'t: S(.:.. 2o?. 6 #Q ~ 

C02 

1?: 

~'1 z. 

s" 

Post 1 est Leak Check 

StJ./o 

Meter cu.ft@ in.Hg 

Pitots @ in.H20 
#5-t,CQ 

#6 ),.IC · i__... 

5"0. l 

.. . 
#4 wo) 'f 

#5 :Wl. ·io 

#6. 

)~0 

.2-(L

~ 

~ 

:>o, o 

"l ,_ . 

. :;. ~~ 
2.... ~i ..... -- 1..5 

3 '?>2 .. '1 

i.( 3 !7lf ,-

:J 335' ~ 3U 

\? ( ~ :z,?, 

2.-- 32.5' ~ "3L) 

v 2.% ' ~ ~~i 

b 32-'7 

AVE. 

? I ~ - •, .. "" D v '~ f'.- C./. ! i .._) ~, • .: .. ) ~\. k._ I l LOCATION (~Q.\~RCE #): ~7 r · t ~-'~ ' 

OPERA TOR: / J1 i 

; .• j 

AiviBIENT TEIVf.PERATURE: '-f f 

BAROl\-fETRIC PRESSURE: ;£1. '7~ 

ASSUMED MOISTURE: 

STACK DIAMETER: ~~;5_ ._;-

C FACTOR: , '/.,:...( . 

v i 

CO IvfTvfENTS: 

t O 

if 

• o'1 

; c c., 

~oS' ~ c -7 

.6-G, 

of 

O'"J 

,. (; c, 

c "1 

o0 

(l. .I/. q 

. I 

<.:fo 

G~ 10 

Cjo 

'7o 

So 

'io 

'1D 

'1o 

'7o 

Cfo 

'1o 

I 

.. 

I 

I 

t--... --

1 

') "• -t; 
Appendix D 
ter Box#: 3 

rial#: AR3 

!!!!! 

Armstrong Environmental Inc. 

EPA Method 5 

522 Series Meter Box Calibration 

Pre-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date: ------------------------> 

Barometric Pressure: ----------> 

Theoretical Critical Vacuum:--> 

01/04/11 

29.40 (in. Hg) 

13.87 (in. Hg) 

~ORTANT For valid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critical Vacuum shown above, 

~ORTANT The Critical Orifice Coefficient, K', must be entered in English units, (ft)'3.(deg R)'0.5/((in.Hg)'(min)). !I!!! 

--------------- DRY GAS METER READINGS ---------------- -CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. Orifice K' Orifice Actual --Ambient Temperature --

H20) 

tlH Time Initial Final Total Inlet Outlet Inlet Oullet Serial# Coefficient Vacuum Initial Final Average (min) (cu ft) (cu II) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) 0.25 5.00 998.871 1000.420 1.549 65.0 65.0 65.0 65.0 0.52 5.00 0.420 2.658 2.238 65.0 65.0 66.0 65.0 0.96 5.00 2.658 5.696 3.038 66.0 66.0 67.0 66.0 1.50 5.00 5.696 9.588 3.892 67.0 66.0 68.0 66.0 2.95 5.00 9.588 14.971 5.383 68.0 66.0 71.0 66.0 

, ............. ,..*"'*""*""*••*..~~**"'*•••••*•**••••••••*•"'•* RESULTS ********"'*•**"'******"'*****'********•••••*••••••••••• 

DRY GAS METER ---

LUME VOLUME 

·RRECTE[ CORRECTED 

Vm(std) Vm(std) 

(cu fl) (liters) 

1.531 0.1 

2.213 0.1 

3.001 0.1 

3.846 0.2 

5.329 0.2 

--------- ORIFICE---------

VOLUME VOLUME VOLUME 

CORRECTED CORRECTED NOMINAL 

Vcr(std) Vcr(std) Vcr 

(cu ft) (liters) (cu ft) 

1.553 0.1 1.581 

2.203 0.1 2.242 

2.968 0.1 3.021 

3. 796 0.1 3.865 

5.270 0.2 5.365 

Average Y -----> 

-- DRY GAS METERCALIBRATION FACTOR 

y 

Value Variation 

(number) (number) 

1.014 0.019 

0.995 0.001 

0.989 -0.006 

0.987 -0.008 

0.989 -0.006 

0.995 

e: For Calibration FactorY, the ratio of the reading of the calibration meter to the dry gas meter, 

acceptable tolerance of individual values from the average is +-0.02. 

(..1,) 

.-..: 

40 

48 

55 

63 

73 

0.243 22.0 68.0 

0.344 21.0 68.0 

0.464 19.0 68.0 

0.593 17.5 68.0 

0.824 14.0 68.0 

--------- ORIFICE---------

CALIBRATION FACTOR 

dH@ 

Value 

(in H20) 

1.441 

1.490 

1.512 

1.444 

1.473 

Variation 

(in H20) 

-0.0307 

0.018 

0.040 

-0.028 

0.001 

68.0 68.0 

68.0 68.0 

68.0 68.0 

68.0 68.0 

68.0 68.0 

1.472 <---Average dH@ 

Date / /•f( /; / 

t I 

CONVERSION FACTORS 

1 mm Hg' 0.13330 kPa 

1 em = 0.39370 inch 

1 mm = 0.03937 inch 

1 cu ft = 28.32 liters 

-Average Temperatures--

DGM DGM Ambient 

Oullet Overall Temp 

(deg R) (deg R) (deg R) 

525.0 525.0 528.0 

525.0 525.3 528.0 

526.0 526.3 528.0 

526.0 526.8 528.0 

526.0 527.8 528.0 
Point 2 212 210 210 211 211 211 

Point 3 752 751 751 751 751 751 

Degrees R 

Point 1 492 490 490 490 490 490 

Point 2 672 670 670 671 671 671 

Point 3 1212 1211 1211 1211 1211 1211 

Percent Difference 

Point 1 -0.4065 -0.4065 -0.4065 -0.4065 -0.4065 

Point 2 -0.29762 -0.29762 -0.14881 -0.14881 -0.14881 

Point 3 -0.08251 -0.08251 -0.08251 -0.08251 -0.08251 

•

. 

' li 38 
er Box#: 3 

ial#: AR3 

!!II 

Armstrong Environmental Inc. 

EPA Method 5 

522 Series Meter Box Calibration 

Pre-Test Orifice Method 

English Meter Box Units, English K' Factor 

Date: ----------------:> 

Barometric Pressure: ---> 

Theoretical Critical Vacuum:---> 

02/08/11 

29.43 (in. Hg) 

13.88 (in, Hg) 

'ORTANT For valid test results, the Actual Vacuum should be 1 to 2 in, Hg greater than the Theoretical Critical Vacuum shown above. 

'ORTANT The Critical Orifice Coefficient, K', must be entered in English units, (ft)"3*(deg R)'0.5/((in.Hg)'(min)). 

1111 

- ------ DRY GAS METER READINGS------- -CRITICAL ORIFICE READINGSVolume Volume Volume Initial Temps. Final Temps. Orifice K' OrifiCe Actual --Ambient Temperature-- dH Time lniUal Final Total Inlet Outlet Inlet Outlet Serial# Coefficient Vacuum Initial Final Average -120) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) 0.25 5.00 265.800 267.334 1.534 61.0 61 .0 62.0 61 .0 

0.52 5.00 267.334 269.560 2.226 62.0 62.0 66.0 63.0 

0.95 5.00 269.660 272.580 3.020 65.0 63.0 67.0 64.0 

1.50 5.00 272.580 276.467 3.887 66.0 65.0 69.0 65.0 

2.95 5.00 276.467 281 .834 5.367 68.0 66.0 73.0 67.0 

.,'frllrllll .., ,oll' ll! -.t-• "''**••* •" *"""'l'l'a"" '* ""'*-"" -**•~•.._. RESULTS **"'*"'"'***'**"~~"*"'***•**"'***•***"'""***"**.,•*•*••-•***"'* 

JRY GAS METER -

LUME VOLUME 

RRECTECCORRECTED 

Vm(std) Vm(std) 

(cu ft) (liters) 

1.529 0.1 

2.212 0.1 

2.995 0.1 

3.849 0.2 

5.311 0.2 

---ORIFICE----

VOLUME VOLUME VOLUME 

CORRECTED CORRECTED NOMINAL 

Vcr(std) Vcr(std) Vcr 

(cu ft) (liters) (cu ft) 

1.551 0.1 1.584 

2.201 0.1 2.247 

2.965 0.1 3.027 

3.793 0.1 3.872 

5.266 0.2 5.376 

Average Y -----> 

- DRY GAS METERCALIBRATION FACTOR 

y 

Value Variation 

(number) (number) 

1.015 0.019 

0.995 -0.001 

0.990 -0.005 

0.985 -0.010 

0.991 -0.004 

0.995 

e: For Calibration Factor Y. the ratio of the reading of the calibration meter to the dry gas meter, 

acceptable tolerance of Individual values from the average is +-0.02. 

SIGN EO :~,... -;r I _,/V .,.. -_1 

~).) 

CJ:) 

40 

48 

55 

63 

73 

0.243 22.0 70.0 

0.344 21.0 70.0 

0.464 19.0 70.0 

0.593 17.5 70.0 

0.824 14.0 70.0 

----ORIFICE ---

CALIBRATION FACTOR 

dH@ 

Value Variation 

(in H20) (in H20) 

1.456 -0.0219 

1.501 0.023 

1.507 0.029 

1.450 -0.028 

1.476 -0.002 

70.0 70.0 

70.0 70.0 

70.0 70.0 

70.0 70.0 

70.0 70.0 

1.478 <---Average dH@ 

Date: z[ f (II f I 

CONVERSION FACTORS 

1 mm Hg' 

1 em = 

1 mm = 

1 cuft= 

0.13330 kPa 

0.39370 inch 

0.03937 inch 

28.32 liters 

-Average Temperatures--

DGM DGM Ambient 

Outlet Overall Temp 

(degR) (deg R) (deg R) 

521 .0 521.3 530.0 

522.5 523.0 530.0 

523.5 524.8 630.0 

525.0 526.3 530.0 

526.5 528.5 530.0 
Point2 212 210 210 210 210 210 

Point 3 752 750 750 750 750 750 

Degrees R 

Point 1 492 490 490 490 490 490 

Point 2 672 670 670 670 670 670 

Point 3 1212 1210 1210 1210 1210 1210 

Percent Difference 

Point 1 -0.4065 -0.4065 -0.4065 -0.4065 -0.4065 

Point2 -0.29762 -0.29762 -0.29762 -0.29762 -0.29762 

Point 3 -0.16502 -0.16502 -0.16502 -0.16502 -0.16502 

40 
De damaged? j/Jo 

C) -, oo < Cll < + l 0() () 

2. -10° < a, < +10° 2--

2- ,..0 < sl < +50 :2 -::J 

0 •o < Pz· < +50 I 0 -~ , Ku.tr I•IC"I.TIC ltft:'l 

_ \ ,..n1• '" ecu ... •••• • r ' y ./ 

0 . . ; e 0 

o.ch (,' A /17~ ' &· qg~ 1. 05 Dt < Pa < 1.5 Dt , :I l(fb. 

()·lf']V 1. 05 Dt < P~ ·< l . 5 Dt ..'f]o 

WCMi l .. IC . .I.llt!C l.(liC'- ,..,,11. ,..,. t.t:n•,••• ~-370 · 3/16 11 "< Dt '< 3/811 [), 370-"-- . 

.. 

-

.. .·. ~ ~ ·-~ . 3y.;,_~ 

·- --~ : 

Corrrnents: 

Jr•<t",I.C[ ,1 -..cCATUII( U'r'tl "MIT I .. 

Pta KH .... •I""- ...,... .. , 

&.ooo -

(J 

.v 

A tan 'Y < 0.125 11 0·~170 A tan 8 < 0.03125 11 .o 

I P a .. , . v = Pts ± 0.053 11 

Pitot tube/ probe number bt;' 6- meets or- exceeds all _s pee i fica tions 

criteria and/or applicab1e design features*daand is hereby assigned a 

pitot tube calibration factor of 0.84. •· . ·· · ' · 

. . 

Signature · 'VI · 

•Set '0 UR 60, Voi. ~2. Ko. 160, .~~h oci 2. Y•rily :he r.ir,i= 

2 Inch Htt:.ad of t..lot ~her.>:>c::.uplt tnc :he r.ini= 3/~ incn 

st;:.<rtt1M bet~tn th~ p1~t :..:.:~ tnd th~ nozzlr ~s ~~It the top' of thl~ p..191. 

.. ,, 41 

I 

I 

i 

I 
rn

Comments: 

~fCiiiU IIIIIOic.i.TI...;. L.!~L 

POSITIC. JO&. ::lC:'r•,., ... ..: 

Gq-.:.o 1 

Kt..lH l lltltC"'"'< t{T(L 

~ITIO. JOA ;.(JI""IWI~ t 

DC::;..tt .•.w•c.-.r•....: Uvt.L re11t1ao. 

'Qa 01(~[-1•1"" ;:, .....,.. lr 

I 

~ 

I 

I 

I 

obstructions? 

damaged? 

-1 0° < Cl) < + l 0° 

-10° < Clz < +10° 

-so < 81 < +50 

I -o -;, < 82 < +50 

y 

e 

A 

1.05 Dt < Pa < 1.5 

I 1. OS Dt < pb < 1. 5 

3/16"-< Dt '< 3/8" 

A tan y < 0.125" 

A tan 9 < 0.03125" 

j Pa = Pb ± 0.063" 

/..} f) 

/Jo 

0 

I 2-

'2. 

0 

( 

0 

.97

~ 

Dt! tWto 

o ... ~q'to 

\.. 

~?,37~ 

(].vt? 

() 

v/ 

Pitot tube/probe number bU G- meets or exceeds all spec;ncanons 

c~1t:ria 

p1'o'" tube 

and/o~ 

ca1lbration 

app~ica~le 

ToCL.Or 

... desi~n 

01 0.84. 

features~""and is ~" ~zi#a 

/ /' 

1 

Sig:.aturo ~111 VU 

.,.See ';Q : .... ~50, Vo1. ~2. No. 150, H~t~oC 2. V~rify th~ 

r.:inimu~ 2 inch se:.back cf the ~he1"7.10c~up1e and the mini~ 

3/~ inch separl:ion b~:we~r. ~he ;>i :ct :.:.tbe end !h~ ~:z::ie as sho\o'T': !!'":: 

~~e 

~~P of :~is page. 

Date /2{n/l1 

•. ,. u ,. 

I 

I 

I ' 

I 

j 

I 

I 

I 

I 

I 

I 
• ~.,.. ., c:, ,_ •• u- ._,,_c:C'f .l I "':~-7 I - .T· ....... -); J{; lff (i I i V• l~ {L.;'D Pt .!---1 tJ 

. .... : .·1 f -c,. · .. ..,_ ', Q. .!".J.-i ~-a ! u I ~ U __ ) 

(JJ L'Jir JO 1' '3S( 

C?!'tlin l! /7 

b?r I 2cz. 2-- J 2<7. 2 -- I - TiT 

H8 2<t .. n ! Z-'7-S- - I 17l 

ID ..;( l )_.~ .tr-1 ~-IS- - I u 

I I 

r I I 

i I . 

I 

\. - l I 

i 

I " '!} I I ' j i 

I ! . 

I 

f 

I 

! 
.Presamole Inspection 

I hereby certify that the above referenced nozzle appears to round, sharp-edged, free of nicks and dents and is ju for use at this time. 

Last Previously Measu~d Nozzle Area 

.~o~37~ ft2 

Date Measured lfl-/1 f date ~~t 1 U I 

Postsamole Measurement 

Measure three diameters as shown; measurement is in inches; record belo\'J; perfonn calculations. • 

1._, l.f--'t ...... s-__ 2. '~t£ 3. I l.f/ Lj 

Ave rage D i amet er _ ._i.f.:..:t;_tf...;....;. l ___ _ 

Area = '11' o2 

4 X 144 = 

data reduction. 

-·· 

• Maximum allowable difference between largest diameter and smallest diameter is 0.004 inches 

., 'I li ; 

n_., o 
Appendix E 
P.O. Number: 

Item Number: 

Notes: 

Assay Date: 

31522 

9-Apr-09 

Component 

Oxygen 

Nitrogen 

Reference Standard(s) Employed For Analysis: 

Std name Std II GMIS~21 GMIS~21 Analysis Information: 

Componont 1: Oxvoen 

Anatvzer Information 

ManufaciiKer: Teledyne 

Model Number: 3000PA Zero 

Serial Number: 1862 Reference 

Analytical Principle: Para mag, Candidate 

MPC Calibrated: 03127109 Result 

Analyst Signature: '-~~~ 

'""-

U~ 

= 

Mix Assayed At: Air Liquide America 

Cone. 

21 .9 

Expiration Date: 8-Apr-12 

Unit s 

% 

Requested 

Concentration 

9% 

Balance 

Std. Error Comp. 

0.1 02 

-

32935988 

LPX250323 

CGA590 

1900psig 

Transfer#: 

LOT#: 

Valve 

Cyl. Pressure:• 

*Cylind er should no1 be used when gas 

pressure is below 150 psig 

Assay 

Concentration 

9.01 ±0.07% 

Balance 

Balance CVI. No. Exp. Date Sample No. 

N2 cc178365 3/27/2011 N.A 

First Triad Anal sJs On: 4/912009 Second Triad Analysis On: 

Trlal1 Trlal2 Trial3 Units Trial 1 Tnal2 Trial 3 Units 

0.80 0.77 0.76 Zero 

21.60 21.58 21.49 Reference 

9.26 9.36 9.36 candidate 

8.94 9.05 9.05 % Result 

Mean Result 9.01 % Mean Result: 

Debra Jackson Calculated by: -~-"'-------=1...:::9_ _ ____ __ Debra Jackson 

" .... li ·,,', 4 5 

11426 Fairmont Pkwy, La Porte, TX, 77571 Phone:(281)474-8400 Fax: (281)474-8419 
P.O. Number: 

Item Number: 

Notes: 

Assay Date: 

31522 

9-Apr-09 

Component 

Oxygen 

Nitrogen 

Reference Standard(s) Employed For Analysis: 

Std name Std # 

GMIS421 GMIS421 

Analysis Information: 

Component 1: Oxvoon 

Analyzer lnfo.-malion 

Manufacli.Xer; Teledyne 

Model Number: 3000PA Zero 

Serial Number: 1862 Reference 

Analytical Principle: Paramag, Candidate 

MPC Calibcated: 03/27/09 Result 

Cone. 

21 .9 

Expiration Date: 8-Apr-12 

Units 

% 

Requested 

Concentration 

20% 

Balance 

Std. Error Como. 

0.1 02 

32935988 

LPX250321 

CGA590 

1900psig 

Transfer#: 

LOT#: 

Valve 

Cyl. Pressure:• 

•cylinder should not be used when gas 

pressure is be\ow 150 psig 

Assay 

Concentration 

20.0 ±0.1% 

Balance 

Balance Cyl. No. Exp. Date Sampje No. 

N2 cc178365 3/27/2011 N.A 

Firs t Triad Analysis On: 419120()9 Se<:ond Triad Analygs On: 

Trial1 Trial2 Trial3 UnitS Trial 1 Triai2 Trial3 

0.80 0.77 0.76 Zero 

21.60 21 .58 21.49 Reference 

19.79 19.73 19.71 Candidate 

20.04 19.97 19.95 % Result 

Mean Res\M: 19.99 % Mean ResLAt: 

Calculated by: ~~ 

Urits 

Debra Jackson 

..... u d ~ 6 

Mix Assayed At: Air Liquidc America 11426 Fairmont PJ..·wy, La Porte, TX, 77571 Phone:(281)474-8400 Fax:(281)474-8419 
Appendix F 
Torn: The production information for the Elgin stack test is below. If you need 

any thing els let me know. 

Thanks for your help. 

Push rate: 

Car count: 

Brick Wt.: 

Paul Anderson 

Group Assets & Eng Mgr 

Hanson Brick 

500 NE 14th Ave. 

Mineral Wells, TX 76067 

Cell: 817 690 8132 

Fax: 940 325 9788 

paul.anderson@hanson.biz 

Hansonbrick.corn 

18 cars/day 

5200 brick/car 

1552 grams/brick 

http://webmail.c.earthlink.net/wam/printable.jsp?msgid=4743&x=-260784951 

.. ·•vu 47 

1/28/2011 
Appendix G 
Run# 

11 &2 

11&2 

11&2 

11&2 

11&2 

Imp# 

13&4 

13&4 

21&2 

2 1 &2 

31&2 

31 &2 

300 

Average 

300 

300 

Average 

300 

300 

Average 

Volume Dilution 

250 

250 

Average 

250 

250 

Average 

250 

250 

Average 

1 1.14 0.07 0;360126 

0.372762 

1 1.47 0.07 0.464373 

1 1.51 0.07 0.477009 

0.470691 

1 1.54 0.07 0.486486 

1 1.57 0.07 0.495963 

0.491225 

Cl-, ug/ml MDL, ug/ml Cl2, mg 

1 <0.1 0.1 <0.025 

1 <0.1 0.1 <0.025 

<0.025 

1 <0.1 0.1 <0.025 

1 <0.1 0.1 <0.025 

<0.025 

1 <0.1 0.1 <0.025 

1 <0.1 0.1 <0.025 

<0.025 

3.24 0.1 0.999216 

0.99459 

3.71 0.1 1.144164 

3.96 0.1 1.221264 

1.182714 

3.46 0.1 1.067064 

3.52 0.1 1.085568 

1.076316 

•• y '-' 4 8 
FlClFlCl

I ,? l 1 !''''''''' \ ........... ,,.,,., .. :::::::.: ::::;::::::::::~~mu:.!!tm: !!!!u:tmm::=:s::· 1. os3l t··················- 1 I .. t' :\ 1. 9so 1........ . •· .. ··:·::.:::::::··: .... ::"'''"'"""'"'"·· 1 2j (.. I I i I i Jl......... ! i i ! ! I . I I i I 4,....... i ' I j I i I sj....... J I ' ! ........ 61 I L. ....................... : ........................................................................... _ .................................................. _ ................................................................................................................ _ .......... .J Component Number Retention Area External Units 

2 

1 

2 

1.083 

1.950 

337.50 M 

252.20 M 

589.70 

3.98 ug/ml 

3.46 ug/ml 

7.45 

337.50 M 3.98 

252.20 M 3.46 

49 
FlCl

i ·:~. 1 j"'"'"'" =::.·~:: :::::::::::::~:::::::::.::::: ~:.: :::: ::::::::mu::: tn=::l:~m~· 1.1001 , .. 

!- 1 \ 

1. 933!, . '· : ··": :::~ ::::::: ::::-:ll Tll!' t"""" ,_ ....... 

I I 

31···· .. ! 

I 

I 

L ...... 

41 

sl····· 

I 6, ....... .. 

I ' . I 

1 ................... : ...................................................................... _ .. ,_ ............................................ _.__ ............................................................................................................ ...1 

Component Number Retention Area External units 

Fl- 1 1.100 335.00 ~'i 3.95 ug/ml Cl- 2 1.933 2.59 .10 ~1 4.12 ug/ml 

2 594.10 8.07 

335.00 M 3.95 

259.10 M 4.12 

50 
FlCl

1,......... < 1 . 0 8 3! I 516 . 8 0 M 6 • 0 2 I '• I 1 . 9 5 j......... : \;· .::::::::::::c.::::::::::::::::::::::::::::::::::::" i 3 6 9 . 50 M 5 . 76 I c --- - - -- ------- ----- - ---- --- --1 

3,......... I 

i 

4f---

l 

l"" 

i 

61""""""""" 

I . . 

I : ! 

.................. ....... : ........................................... ................................. -...................................................................................................................................................................................... .J 

Component Number Retention Area External Units 

Fl- 1 1.08:3 516 .. 80 6.02 ug/ml Cl- 2 1.950 369.50 f"l 5.76 ug/rnl 

2 886.30 11.78 

5.1 
FlClFlCl- 

1!......... < I 1 • 0 8 31 :;: :: :::::: :::::::::: :::::::: ::: ::::::":::~"'" '""'""'"' ""'' "'"" '" """"""'""""" ,. 

I I, 

1.9331 :\...... ! 2!......... : r ... ::.:::::::::::::.o:·:: :.:""''' :::::: :··~··· I ~ ·· ! 

I ! ! 

41 ....... .. 

! 

i 

I 5j· ······ 

I 

I 

61······... II i 

r 

! ......................... : .......................................................................... -........................................................................................................... ........................................................................... ..! 

Component Number Retention Area External Units 

2 

1 

2 

1.083 

1.933 

520.30 M 

366.75 1'1 

887.05 

6. Of3 ug/ml 

5.94 ug/ml 

12.02 

520.30 M 6.08 

366.75 M 5.94 

... ;. 52 
FlCl

£ J;: ~•'""" I!• 1.1 oof ··;;:::::::::.~:::::: ::::.:::::::::::::::::::::: ::::: :::::::"'""'"'""''"''"" '"'·' "'"'"""'""'''""''"'""""'""''·"'"'" ............ . 

I t I i:, 

1. 966! 

2l"""'" 

! 

i 

! ~~ ~r ........ 

i 

j 

i 

! 

4!""'"" 

I 

. ·:l 

: ~~:::::::::::~::~:::: :::::~~: 7-·.:~:::::::::~~:~~~~:::::l~~ ~~:::~:tt~lt!IW.~ 

. 

·' ' .~ ! I i l 

r 1 

61......... I 

l . l 

L. ..................... : ...................................................................... ,_, ................ _,_ ................................................................................................................................. _ ........................ ...l 

Component Number Retention Area External Units 

FlC.l2 1 2 1 .. 100 1.966 759.10 M 474.05 f1 1233.15 8 .. 02 u.g/ml 7.42 ug/ml 15.44 

759.10 M 8.02 

474 .05 M 7.42 

53 
FlClFlCl

I ) l 11""""' ·z, , l ............ ::::: :::::: :~::;;:::::::::::::::::-.:~:::: :·.1\u~nm:nm~murltlllllll' 1 ,1 001 ' I ! (' ! 1 . 9661 : ........ . ·.:·:". ":::·::·::·:.::.:·:·:·:::·:c .. .. , ... 21' "'""' ' 'r".''""' : t 3/ ........ I I 1·-""" 41 ! i 51"""'" ; Component Number Retention Area· External Units 

2 

1 

2 

1.100 

1.966 

699.30 M 

479.20 M 

1178.50 

7.56 ug/ml 

8.08 ug/ml 

15.63 

699.30 M 7.56 

479.20 M 8.08 

54 
FlClFlCl

1. oall ];

:= '"' "'"'""" ' " " • · 1,. ! I i \, ' 1. 933i : \ ....... ._....... .... I zr------- _j· __ _ .............. I .I i i 3j""'"" i I i i Component Number Retention Area Ext.er nal Units 

2 

1 

2 

1.083 

:1..933 

205.25 1'1 

129.50 M 

334.75 

2 .. 43 ug/ml 

1.71 ug/ml 

4.13 

205.25 M 2.43 

129.50 M 1.71 

s·s 
FlClFlCl

i jr' 1 0 8; ]"""'" ::· .. :::::::::::":::::::::::·.:·"''·""'""·"'"'"' . if I \1 1. 91~1....... : '}::::::::::::"'"""' I I ,! .Ji"'""" I ! l 41" ....... I sr-"· I [ ......... 6, I I . I l ........................ ............................................................................................................................................................................................................................................................. J Component Number Retention Area External Units 1 1 .. 083 201 .. 80 M 2 .. 38 ug/ml 2 1.916 123 .. 20 ~'1 1.63 ug/m.l 

2 325.00 4.01 

201.80 M 2.38 

123.20 M 1.63 

56 
\_ 

'· . 

... 

·.\._ 

·

., 

'• .. 

. \ 

'•,\ 

······•··· .... 

\ .... _ 

............ , 

t •••• 

i ·· .. 

L;l 7 9 0< 1 ;2 

Avg slope of curve: 60.04 Y-axis intercept: 0.00 Coeff of lin regr : 0.95 

f\1() . Ar·ea P1mount 

0 . 0 . 000 0 " 000 

1 ; 126 . '/ <-- . 000 

"' ,,;::::, " 250 650 3 990 " . 

..... , ,:.'\ ; 368 . 1::::5 5 990 

4 479 12;5 7 980 

C':F 

0.000 

63.175 

62 2320 

t<L .. ·457 

60.041 

2 

3 

5 

.. • .. 

'

. 
i 

.\ I 

.......... . I 

.\ 

· .. 

·...... ..... I 

I .... ..., I 

7 2 9 . 2 C) 0 !... ......................................................................................................................................... >::..! 

Avg slope of curve: 90.48 

Y-axis intercept: 0.00 

Coeff of lin regr: 0.87 

f\j() ' Area. Amount. 

():: 0.000 0.000 

CF" 

0 .000 

j . .. 20:3.525 2.010 1.01 .256 

2: 341 .660 4.,030 84.779 3~ 518.550 6.040 es .. 853 

4: 729.200 8.060 90.4/:i. 

2 

4 

5 

58 
1.......... 

 II, i j;: I 

,. 

1 :\1 

,........ . :!. 

21 I' I I ................................................................ _ ....... -................................................................. -................................................................................................. 1 

. I I I 3!'"""" i 

i I I : 

. I 

41......... I 

I ! 

51""""' ! 

I I 

I I 

I I 

6r--""" l 

l ! 

-I ....................... : .................................................................. ..................................................................................................................................................................................... J 

Component Number Retention Area External Units 

0 0.00 0 . 00 
11

 

j 

L ....... 

21 

' j 

i 

3J ......... 

' i 

i 

! 

41"'""" 

' 

i 

I Si ........ 

! 

! 

I 

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I 

! 

' , , .,., ' ' ''' • •0' ' UOo-o • • -•oO•o•''' - '' ' ' " - ' '' OOoO , _ ,_, " ' ' '''"" oO oomo n "' OO OO OUO" ... oO Om ,o "'' ' OOnO OO O "''"' " UO .. UUOO OOOUU • onoo nn " OO OOO UO .. O O ... ONUo " ' 

i 

i 

i 

i 

! 

I 

j 

i 

i 

I 

i 

i 

61......... I 

' i l : . I 

i.. ....................... : .................. ................................................................................................................................................................................................................................................. .J 

Component Number Retention Area External Units 

0 0.00 0.00 

.. . \..' ·. s 0 
FlClFlCl-

I .::J r if........ ··:., 

1. 0831 123. SO M 1. 22 

i \. 

1. 9661 . ''· 

2

11

......... : i::::::::::::::::::::,;:::: ••• ,........ 202 .1 0 M 3 • 21 

I 

31 ......... 

! 

I 41""'"" 

i 

I 

! 

s!... ..... 

I 

! 

i·-""" 61 

I 

: : tOOO O OU OOO 000 0000• " ' 0000 00 0 0 O OO OO OO OOOOU - 00 OOUOOOU O OOOOO O no .. O OOO>OOU O .. MO OOO OOOMO .... O O OUOO ... OMY OO n .. o ... O OO OOOO O ..... ,.,,,, , ,, ,,, , , , ,MOONO 00 "0-0 0 .... 0 0 00 00 0 

!O OOMON OOOO OOOO N OO O.OO O O: OO OO OO O OOOO OM- OOOOOO- OO OOOOOO OO OO UOOOOOO OO U OO OOOOO MOO,O OOO .. OOOOOO OOOO OM OO oO OO OONN oOM o0 00 00 00·0 - 00 000 0 0 00o OO ... O OOO .. OO .. MoOo> OO.O NOO OW .. O'o•O • .. 

Component Number Retention Area External Units 

2 

1 

2 

1 .. 083 

:1..966 

123.80 M 

202 "10 

325.90 

1 .. 22 u.g/ml 

3.2:L u.g/ml 

4.44 

... , '-' ._'. 6.1 
FlClFlCl

I .,).:! I 1. 8~ ---- ::::::,, ~, ....... ,. 1 115.90 fl 1 .14 :· .. ,1 1 . 950i......... : t:::::::::::::::"""'"'"""'""""""'' 203.90 M 3. 24 21 : ;I I 3:·---- 1 ! ......... 4: I sl -j 61""""' I . I i ........................ : .................................................................................................................................................................................................................................................................... .J Component Number Retention Area External Units 

2 

1 

2 

1.083 

1.950 

115.90 1"1 

203.90 M 

319.80 

1.14 ug/ml 

3.24 ug/rnl 

4.39 

62 
FlClFlCl- 

I :i I ·' i 1 .1 o&l....... 'f::::::::::::::::'''"'""' I ···. I , :·;1, I 1 . 9 6 J········· ! :::~~·: ~:::·:::·::: :·:::: .............................................................................................................................................................. -......................... 1 J....... l ! I I I ~ I 41 ! sf........ I II i ! I 6, ......... i I 1... .................. : ......................................................... -........................................................................................................................................ _ ............................... ..! Component Number Retention Area External Units 

2 

1 

2 

1.100 

1.966 

148.45 M 

233.20 M 

381.65 

1.47 ug/ml 

3. 71 ug/rnl 

148.45 M 1.47 

233.20 M 3.71 

63 
FlClFlCl-

r :1 I : . : I 

.. ! l 1.1oM........ :;• ......... :::::::::'"'""'"""". I 

I f"' i! • 

. 966; :·· .. ,,.1 i 

1. 21:......... : ,:.:::::::::::::::::::::::::::""'"::::::::::::..... .li 

. :1 

i i I I 

i I 

31""""' II 

I 

I 

4l'"""" 

I 

I 

sl. ........ 

t 

j 

I 

1 ......... 6, 

I 

' !.. ....................... : .................................................................................... . 

Component Number Retention Area External Units 

2 

1 

2 

1.100 

1.966 

152.70 M 

248.70 M 

401.40 

1.51 ug/ml 3.96 ug/ml 

5.47 

152.70 M 1.51 

248.70 M 3.96 

•• v · .' 64 
FlClFlCl- 

1

:1: I ' •·! ' ~- ~ i 1 . 0 s 31 :::::::::::::::,::,::::::"'""'""' I 15 5 . 50 M 1 . 54 

! ... i J ! 1.9661 . h I 217.80 M 3.46 

2 j"'""" : .t::.:·:=.·:·::·::::·::::· .. ::·:·:· ... : ................................. -............................ ""' '"'"'"' "'""'""""""'"'"""'""""""""'""""""' ........................ _, ................................. ..! I . 1 

I I 3\......... I 

! i I i I 

4! - I 

! 

i sj ....... 

I 

! 

6, ......... 

I 

!.. ....................... : .................................. .................................................................................................................................................. ............................................................................... ...! 

Component Number Retention Area External Units 

2 

1 

2 

1.083 

1.966 

155.50 M 

217.80 M 

373.30 

1 .. 54 ug/ml 3.46 ug/ml 

5.00 

" .. ·. . 65 
FlCl

I :;· I .-:. ; I ~~ 1·······-· ,I ....... , ___ ,,.,. ........ UIIUI\11111'!' I I 1 '0831 :ii:......................... 1,' I' .r11 \ ,! 1. 950! : '\ 2,......... : :. :::::~::: :""":: ::::::::::: """ II_ : .i' 

I! 

. 

·; 

I I 1 3 ! ......... 

I 

Ii I 

4,......... I 

I 

I! I I · 51 ! ~- 6! ......... 

I 

I : i 1.. ....................... : ............................ ..................................................................................................................................................................................... ,_, ___________ ,__,.,_,.,.,. ................. ..! 

Component Number Retention Area External Units 

2 

1 

2 

1 .. 083 

1 .. 950 

159 .. 00 ~1 221.10 M 

380.10 

1 .. 57 ug/ml 3.52 ug/m1 

5.09 

159.00 M 1.57 

221.10 M 3.52 

\} 66 
FlClFlCli :.1 

_,.1

1 

r i:·· ) 08; t""''" -; .,,.,. ;;; :: :: ::: :::::: ::::mn=u~""' ""•" - "I i, .... --- · I __ 

l :'\., 

L 9511 ' ' r:::;: ~'"''""' I 

3!......... 

I 

4,........ I ~1- I 

6r- 1 

L ..................... : ................................. -................................................................................................................................................................................................................... ..J 

Component Number Retention Area External Units 

2 

1 

2 

1.083 

1.950 

339.90 M 

247.40 M 

587.30 

4 .. 00 ug/ml 3.94 ug/ml 

7.94 

339.90 M 4.00 

247.40 M 3.94 

67 
FlCl

I ) . li: 

1 . 08 ~ ["""" :}; ;::~::::: :~::~ ::::::::: :::::: :: ::::::::::::·~~'""""""""'" 

I' 1:, . !. 

1. 91 ~~.. ....... : \:~::

::::::::::

::::::::

::::"'"" ! ~ I Jr ........ 

J___ 

I . 

! 

s ........ 

I j ......... 6• ! 

I . L. ..................... : ................................................................................................................. , ................................................................................................................................................. ..l 

354.25 M 4.17 

252.00 M 4.01 

Component Number Retention Area Externa.l Units 

Fl ·-

Cl2 1 2 1.083 1.916 354.25 M 252.00 M 606.25 4.17 ug/ml 4.01 ug/ml 8.19 

.. . 

•!: 6 8 
(unknown) 

Cl

1. 416 ;:: :;::.:· 

1. 96~r::::: :--· :·:-· --· .. :·:::::::::::::::c:: ............... . 

j ~ I . 

31 ......... 

J. 

I 

sl.. ....... 

I 

j ....... .. 6. 

I : I 

1.. ....................... : .......................................................................... _ ............................................................................................................... -...................................................................... ..i 

Component Number Retention Area External Units 

Cl- 2 1.966 209 .. 25 M 2.00 ug/ml 

1 209.25 2.00 

266.10 N/A 

209.25 M 2.00 

69 
( unkno~m) 

Cl

! 

 

.: ............... .. I ,,:;·· .. '"', 1. 4161 . ' · ...... :: :::::: .... 1 • 9 6 :~~ ::: ;~· .. · .. j;:::::;;;;;;:::::nnnmn"""'' 

! ~ l :l 

3! ......... 

i 

j 

I 

I 

4j"""'" 

I 

! 

Stl 

' 

61""'"" 

I : i !.. ...................... : .................................................................................................................................................................................................................................................. -............ ..! 

Component Number Retention Area External Units 

2 1..966 212,8.5 M 2 .. 1.7 ug/ml 

1 212.85 2.17 

(' ,. ~-· .. 

278.10 N/A 

212.B5 M 2.17 

70 
(unknown) 

Cl-

N/ A 

1 • 4 3 31 , <:~::::::::::;~::::· ! 2 8 3 . 7 0 N I A 

v I 2 . 

zf::::::·:"'"'·:":"·~:: :: ::::::::::: :;nn mUO<OOOOO<oo n"" ""'" I 332 . 70 M 3 . 99 

i ·i i I 3i"" I "'" i I 

! i 

i i i I 

~ 

! 

4! l i 

I Sj ........ 

I 

61'"'""' 

! . I : : I I ........................ : ..................................................................... 

_ ............... ...................................................................................................................................................................... ...J 

Component Number Retention Area External Units 

Cl- 2 2.000 332.70 M 3.99 ug/ml 

1 332M70 3.99 

., y v \· 71 
(unknown) 

Cl

1·'"'"', 1 4161 ,. ( ......... ~ .... . L:.:: .... ........... : ..···· 1 . 96~r::: ::: .. : ...... ·:· :~:: =~ :::::::::::::;, :· ··· ...................... _ 

' :I I 

3J'"""" 

I 

I 

41""'"" 

I 

! 

i 

5r··· 

I 

6!"""'" 

I 

I 

L ....................... : ..................................................................................................................................................................................................................................................... .. 

Component Number Retention Area External Units 

Cl- 2 1.966 332 "80 1"1 4.00 u.g/m.l 

1 332.80 4.00 

256.60 N/A 

332.80 M 4.00 

·

,. 72 
(unknown) 

1 , 416! . ' 1: ...... :::m ~ L:.: .............. : 

Cl- 1 . 2r:::::, .. :-.. ··:·:· .. -~;:::::::::::::::::::::,:: :":::::: :>::::::::: ::::::"

::::: : .. ,, .... 

I ::: 

3~ I 

I 4,......... I I 

sl- I I I 

r I : I 

L ..................... : ........................ I ................................................. -.......................................... -............................................................................................................................... 

_ ..... ...1 

Component Number Retention Area. ExteTna.l Units 

Cl- 2 1 .. 983 481.40 M 5.99 ug/ml 

1 481.40 5.99 

269.70 N/A 

481.40 M 5.99 

73 
(unknown) 

Cl

1.416 ;.::;::1 ,1· _ 1 . 2(::::::": .. ·-·,: ..~;i: -: ~:: ::: ::: :: :;,:::: :: :: ::::' """ "' """ "" ""'"' "" ' I ... 

3i"""'" 

I 

I 

I 

! 

4t"""" 

~- I 

L 6; i I I 

I ! ' ! I : 

!... ...................... : .............................................................. I ........... , .. ,_ .... , .............................................................................................................................................................................. ..1 

Component Number Retention Area External Units 

Cl- 2 1.983 475.50 M 5.9 1. u.g / ml 

1 475.50 5.91 

247.85 N/A 

475.50 M 5.91 

74 
(unknown) 

Cl

1 . 3831 ,• ,• :::~ +::. ! 1 , ..... • • 

1 . 9 6 ~ :~:··:··:··--· ·:~::::~~ :::::: :: :::::::~'"" '"'"""''""'""''"'""""''"""''"' "''"'" !} I ·;· 

i 

3L ...... 

i 

I '

i 

! 

41""""' 

i 

sl ......... 

I 

I 

I 

I 

61""""' 

I 

i I i . 

l ................... -.. L .. ........................ ............................ ........ .. ........ ........ ........ " ................. ... ..... ....................................................................... ..... ..... ...... ............... -........................... 1 

Component Number Retention Area External Units 

Cl-- 2 1.966 554.40 1"1 7.98 ug/ml 

1 554.40 7.98 

253.20 N/A 

554.40 M 7.98 

75 
(unknown) 

Cl-

1 4 0 0:1 .• ": .......... :::: .. , 

1: 9s~f;;::F=--=-~~~-·

--

J_! 

i 

i 

I 

L ...... 41 

I s1 ........ 

! 

I 

61........ : I 

I 

[,.,,.,,,,,,,,,,, ,, .... , • • 

: 

: . .. _0o0 0 .. 00M- OOO" " ''''"''"''"''I'00 .... 0000000HOOm00 0 0 0 0 0 .. 00-000oOo00' .. 000 .. 0 0000 0 " 0 0 0" 0 H OOM-.. MoOoOoOo0 .. 0 .. 0 .. 0 0 M OO OOHOOHOM00 00 .... 00 ............ . ......

I 

. , , N, , .,,, ,, .... , , , , ,, ........ ,,, ,,,,.,, .,NN' 0"0_0_''''"y'"'0000'.0N .. 

Component Number Retention Area External Units 

Cl- 2 1.950 575.50 t"' 8.53 u.g /ml 

1 575.50 8.53 

258.40 N/A 

575.50 M 8.53 

76 
I

':, I \. 

I \ .......... 

·· .... 

*

· ••. 

······•····· ..... 

\ . 

.. 

··:· ... 

'·.\. 

I 

.................... 

I ··-................ I 

I ~ 56 4 .. 9 50 1... .............................................................................................................................................. 

:·:~:::~ J Avg slope of curve: 70.75 

Y-axis intercept: 0.00 Coeff of lin regr: 0.67 

No. Area Amount 

o: 0.000 0.000 

CF 

0.000 

1 : 211.050 2.000 105.525 

2: 332.700 3.990 83.383 

3: 478.450 5.990 79.875 

4~ 564.950 7.980 70.796 

2 

3 

4 

5 

... ,_: 7 7 
(unknown) 

;

l.4lk:::T· 

21 '\ 

; 1,! ! 'j: I :.• 

31......... ' 

I 

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I 

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I 

61"'""" 

i 

I . 

,,, ................................... ~ .................... ~ ............................................ ~ ........... ~ ................................................. ~ ..................................................................................... ,_ .... , .................... ..-.: 

Component Number Retention Area External Units 

0 0.00 0.00 

266.40 N/A 

18 
( un kn01~n) 

i

..... ,,.:: .. :

... 

...

I l r ! 1.433\ .... ··::::::::: =·· 1 1:::::: :~~-,, .. , ... ,: I 21 1: I I i; I I .. 

3j ........ . 

I 

I 

:t 

I 

6!'"""" 

I 

I 

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l... ............... , .... : ............................................................................................................................................................................................................................................................ ..i 

Component Number Retention Area External Units 

0 0.00 0.00 

261.30 

... ;_; 79 

N/A 
(unknown) 

0 • as:f.... _-::_L::::::::::: ccccc:::"""'"'"'""''"''" I 

Ill ................... ... \ . 

2......... . :' .. 

: •" :·~·~ .... ,~· II ·· ....... til" :it"··-··· 

I 3["""" 

I 

L. .... 41 

I s, ......... 

I 

I 

61'"...... I 

: : I '''''' ''~~''"~'~' "''"~ 'u u~o• ••• ~'"''''''·"' mo ooo oNOoOoO ""'"''"'' '''' ''H' ''' ''''''' '''''''''' ""'',. "'"' .. ' ''''''''"''"''' ''"'"N"' ' ' '''''''''"''''' ' .. '''''" "" '''''''''' '''''''''' .,''' ''' ''' uooooo~o.,>o ooo Oooo"''"''''"''''"l 

Component Number Retention Area External Units 

0 0.00 0.00 

f . . ... "'·' ~ ~ 

786.10 N/A 80 
(unknown) o. aso11 1 ) .......................................................... ,,",., ... , ... "."'''""'·~·=-""·'"""''' · I 800.30 .,,,. ,,' '"",.u,,"'"'''' '' "''"'" '' ' 

Component 

0 

'

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, ......... 2· ! 

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' J.••'"' .. ' 

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! 6t· ·~-... I I ! : I I . I . , I : 

...................................... ~··· ··-~·-········"'''•"•······· .. 

--·~ .................... - ......................................................................................................................................................................................... 1 

Number Retention Area External Units 

0.00 0.00 

N/A 
(unknown) 

(unkmn) 

j :: ' 0 . 8 5 L...... I:· t ........ ~: ::::: ·~ :::::: :·:::::·::::·:·::::.::::::::::·" :·.::.:=::::::::::::: 

"'"'"'" '·' ·" '""~ I 8 51 . 45 N/ A I 

~···:: .. ··:·........... I J. .,_ \ . 

f : ,j•l" :.:!n· 

2.4661 : .:::::::.:

::~::: · 116.40 M N/A ?I ~f "" , ......... 

4, 

L 

I_ 

6i I : 1 I : : L ..................... : .......................................................................... .................................................................................................................................................. 

_ ....................... _ ... _ ....... J 

Component Number Retention Area External Units 

0 0.00 0.00 

,,·u~: 82 
(unkmn) 

1 :.r 1 o . 8 s ~ r....... ., ..... :::::::::::::::::::::~====: :::: :::: ::::: :;: ::::: ,,,, ................ ., .... .,........................ I 8 4 o .1 o 

.

1

1 t·: .... ,...... I 

·· ....... ; ...... , 

- • 1: 

• I \ i 

2,......... . .... ,\... I 

. : (: ........ ~ I : ~:·""'"""''"''' II 

31 ......... 

I I 

I I r 1 

sl......... I I 

I I r . 

1 l ......................... : ................................................................................................................................................. 

_ .................................................................................................................. ..l 

Component Number Retention Area External Units 

0 0.00 0.00 

.. .. ·.I . 83 

N/A 
( unkno~m) 

' I ~ 0 ' . 1 r· -· 

"d~:::::::.:::::: ::::: ::c:::c--· ---···--·-"'"............... I 

I : r=\,!: 

!......... I :,, 2, .\ I . .. , ........ w I : ~~: :::::~::::m· 

l . ,1 ,,, ............... ...... .... ~ .... . 3 ....... 

I 

! 4, ......... 

L 

I 

I 

61""""' 

I 

i I ......................... : ....................................................................................................... -........................................................................................................................................................ ....1 

Component Number Retention Area External Units 

0 0.00 0.00 

656.80 

·; ·,; 

tt ... u •) 

N/A 

·84 

I 

I
(unknown) 

( unkno~m) 

i ! :1 i 0 , 8 5 ~ ~-........ :· ..... :~:::::: :::: : :·::·:· ~ .. :·:::::::::::·.c.:o:: ::::::oc:::·•···""''''''""'""''""" """"'' I 

i.~.~ ' 

· .... : ... ;. .. ,, ! ! .... 

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21 ""'"' :., I , ........ ,. 

2 . 4 661 :. r:::::::cmr 

I 3j"'""" 

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I 

41""""' 

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I 

51"""'" 

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6, ~ I I I 

. 

I 

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1.. ....................... : .................................................................... ,_ .................................................................................................................................................. - ...................... ..i 

Component Numbe1 Retention Exte1nal Units 

0 0.00 o_oo 

.. ,. u 

820.40 N/A 

125.83 M N/A 

85 
( unkno~m) 

Cl

o . 8 s ~ 1......... ,,_:_: -~: ::~~~::::::=== ::::: ::::::: ::: :::::: :::::::::::::::: :::: ::::: := :~::: ::::: :: ;,:::::::::::........... ...................... I ! •• I 1. 416j_ .. :. :.::: ::::: ::::::•"' l 1. zll':::~::::··c:· .. ···~-:~:::::::::;~::::::::::: :o:::: :::::::•m"''"''"' i 

._, I ., 

J; I ....... 

I 

41"'""' 

I 

sL.. ..... 

J_ I 

II: 

• 

! ........................ 1 :............................................................................................................................................................................................. . ................................. ! 

Component Number Retention Area External Units 

Cl- 2 1.983 327.40 ~1 3.90 u.g/rnl 

1 327.40 3.90 

985.40 N/A 

256.15 N/A 

327.40 M 3.90 

y . • 86 
(unknown) 

Cl

o . a 5 ~~!........ , .: :t. ....................... :::~:~ :::::::~: ::: ::: ::::::::::::: :::::""''"''''"'" ''"'::":::: ::::: """""'''"""""' ~ ~_:: .... : ..·-····" ........ , ....... . i r 1. 416l:::::::: :~::~-~ ;:. ·: .:· .......................... ,,..,,., .. ,.,,., .. ,.,,. 1' 2)""'"" ' .:, .. ........................... . 

! ·:· I . :·; 

I 

3j"""'" 

I 

I 

i 

4i"""'" 

l 

I 

I 

sl ......... 

! 

i I 

I L I ~ I 

I l l ....................... : .. -. ........................................................ , .... _, .. , ......................................................................................................................................................... ,,_,,.,, ............. _ .. ..1 

Component Number Retention Area External Units 

Cl- 2 1.983 342 "90 1'1 4.13 u.g/ml 

1 342.90 4.13 

938.55 N/A 

254.30 M N/A 

342.90 M 4.13 
.. ms1. v .. g Et,vw\mmenral, Inc. 

17 48 Hlavek Rd 

Decatur, TX 76234 

P II 0 N E N 0 • ( 2 1 4) ' 6 3 -~ -. 0 0 2. ·1 

( P....J:l\,~ u1 ~I Uni\ nnd 1\s,'dloss.: --------~ - ·r 

CHAIN OF .CUSTODY . R~·CORD . 

Ef·-/tOt Jl ;4-r JM.~·f§2 :·x: , r~elco,~ t .• c.orn 

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~owv~v" ~ N-J_~ g(~ :}:.p 

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nonwrlls 

S!)111plo Doln Tirno l) ·'I· 1 S 1 

Hurnbor Sornplod Sarnplod oscnp lOll O <trnp os -;---{- --r-~ ----· -- - ·-.-_ -"ii1- l+2_-- . - - ·-··- .. ·.{ I 

~-- ~\1-- _~~- ____ l).l k.J ~1-,..Soy · , I KH~,"f!.H., l<' ._· .. _ _ _ __ __ ll~ LGLt,~ ~ __ 

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Copy ·lo Clioni!Projcc;l Co(iidinalor 

·---· ·------------------------·-------~--------------,-·-- . - ------------------..... 

llolirlquished by; (Sign<liUro) . Dalu Tirno I nocoivod by; (Siom.\luro) 

---·--·----------------------..,.-.. -

. ···------------------...- .. -..... ·-·· ·-·----
Expiration of Certification 

February 2011 

The Chloride Standard was developed to aid the analysis of anions by Jon Chromatography (I C). 

The single-ion standard was prepared by the dissolution of high-purity salt in ~18.2 megohm 

deionized water, which was tested by IC for ionic contaminants. The bottle label states the 

nominal concentration value of the ionic component for informational purposes only. The ion 

concentration value was determined by Ion Chromatography. The system was standardized using 

the National Institute of Standards & Technology (NIST), Standard Reference Material, SRM 

3182 (Chloride Standard Solution). The actual concentration value determined for the single-ion 

is listed below. 

Chloride Standard 

Component 

Chloride 

Concentration 

(mg/L) 

998 ± 3 

The concentration value is based on proven reliable methods of analysis. The estimated 

uncertainties are two standard deviations of the concentration values. The concentration value is 

warranted to be stable for three months from the date of shipment. 

The preparation and analyses of the Chloride Standard was performed with extreme care by the 

DIONEX Corporation Consumables Manufacturing Department. 

Document No. 034184-25 20 May 1998 89 

Dian ex Corporation 

1226 Titan way P.O. Box3603 

Sunnyvale, CA 

94066-3603 

(406) 737-0100 

North America 

U.SJCanada (641) 295-1500 

South America 

Brazil (55) 11 31315140 

Europe 

Austria (43) 1 616 51 25 Benelux (31) 20 683 9766(32) 3 353 4294 Denmark (45) 36 36 90 90 

France (33) 1 39 30 0110 Germany (49) 6126 991 0 Ireland (353) 1 6M 0064 Italy (39) 02 51 621267 

Sweden (46)8 479 3380 Switzerland (41) 62 205 9965 United Kingdom (44) 1276 691722 

www.dionex.com 

Asia Pacific 

Auslralia (61) 2 9420 5233 China (852) 2428 3282 India (91) 22 2764 2135 

Japan (81) 6 66651213 Korea (82) 2 2653 2580 Singapore (65) 62891190 

Taiwan (886) 2 8751 6655 

LPN 031316-ll610M 03109 
Expiration of Certification 

December 2011 

The Fluoride Standard was developed to aid the analysis of anions by Ion Chromatography (IC). The single-ion standard was prepared by the dissolution of high-purity salt in ;:::18.2 megohm deionized water, which was tested by IC for ionic contaminants. The bottle label states the 

nominal concentration value of the ionic component for informational purposes only. The ion concentration value was determined by Ion Chro,matography. The system was standardized using the National Institute of Standards & Technology (NIST), Standard Reference Material, SRM 

3183 (Fluoride Standard Solution). The actual concentration value dete1mined for the 

component ion is listed below. 

Fluoride Standard 

Component 

Fluoride 

Concentration 

(mg/L) 

1007 ±3 

The concentration value is based on proven reliable methods of analysis. The estimated uncertainties are two standard deviations of the concentration values. The concentration value is 

warranted to be stable for three months from the date of shipment. 

The preparation and analyses of the Fluoride Standard was performed with extreme care by DIONEX Corporation Consumables Manufacturing Department. 

Docum~nt No. 0341 !!3-18 13-Dec-02 

Oionex Corporation 

1228 Tiian Way 

P.O. Box3003 

Sunnyvale, CA 

9406&-3503 

(408) 737·0700 

NorthAmerice 

U.S/Canada (847) 295-7500 

South America 

Br.!zll (55) 1137315140 

Europe 

Auslrla (43) 1616 51 25 B<lnelux (31) 20 583 9763(32)3 353 4294 Oenmark(45) 3636 90 90 France (33) 139 30 0110 e~many (49) 6126 991 0 Ireland (353) 1644 OO&t Italy (391 02 51 621267 SWeden (46)8 479 3360 Switnrland (41) 62 205 9956 Uniled Kinodorn (44) 1276 691722 

www.dionex.com 

Asio Pacific us~a ia (61) 2 9420 5233 China (852) 2428 3282 India (91) 22 2764 2735 

Japan (81) 6 68851213 Korea (82) 2 2853 2580 Singapore (65) 62891190 

Taiwan (886) 2 8751 6655 

90 

LPN 031311Hl610M ll3i1l9 
Appendix I 
Antimony, ug (<2.00) 6.00 6.00 

Arsenic, ug (<0.90) (<1.30) (<2.20) 

Berylium, ug (<0.40) (<0.60) (<1.00) 

Cadmium, ug (<0.40) (<0.60) (<1.00) 

Chromium, ug 3.20 2.60 5.80 

Cobalt, ug (<0.40) (<0.60) (<1.00) 

Lead,ug 1.40 1.10 2.50 

Manganese, ug 4.20 222.40 226.60 

Nickel, ug 3.40 2.30 5.70 

Selenium, ug 2.50 1.60 4.10 

Mercury, ug 0.120 12.90 4.20 17.22 

Run#S 

PW & Filter Imps 1 & 2 Imps 3 &4 Total 

Antimony, ug (<2.00) <3.00) (<5.00} 

Arsenic, ug (<0.90) (<1.20) (<2.10) 

Berylium, ug (<0.40) <0.50} (<0.90) 

Cadmium, ug 0.45 <0.50) 0.45 

Chromium, ug 5.10 2.50 7.60 

Cobalt, ug 0.42 (<0.50) 0.42 

Lead,ug 1.20 0.90 2.10 

Manganese, ug 4.40 3.40 7.80 

Nickel, ug 5.20 2.20 7.40 

Selenium, ug 2.30 (<1.00) 2.30 

Mercury, ug (<0.01) 15.90 16.20 32.10 

Run#6 

PW & Filter Imps 1 & 2 Imps 3 &4 Total 

Antimony, ug (<2.00} (<3.00) (<5.00) 

Arsenic, ug (<0.90) (<1.30) (<2.20) 

Berylium, ug (<0.40) {<0.60) (<1.00) 

Cadmium, ug 0.81 (<0.60) 0.81 

Chromium, ug 3.40 3.00 6.40 

Cobalt, ug (<0.40) (<0.60) (<1.00) 

Lead, ug 1.00 1.30 2.30 

Manganese, ug 12.90 22.10 35.00 

Nickel, ug 2.10 1.70 3.80 

Selenium, ug 2.20 1.00 3.20 

Mercury, ug 0.02 15.20 

4.6 19.82 

.. ._; 91 
g 

Phone: 1-214-631.0021 

Email: armst@ix.netcom.com 

david.mckeown@hanson.biz 

CHEMTEXID Sample 10 

?11010758 Quartt Fiber Filter 

P11010759 Acetone 

P11010760 0.1N HN03 

P11010763 Quartz Fiber Filter 

P11010764 Acetone 

P11010765 0.1N HN03 

MDL: Method Detection Limit. 

Sample 

Volume 

(ml) 

190 

100 

155 

100 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgin,TX 

Date Received: 

01/28/11 

Time Received: 01 :OOpm 

CHEMTEX File#: P11 010758 

Results' MDL 

Paramat&r mg/t. mg/sample mg/L mg/sample 

Antimony <0.02 <0.002 0.02 0.002 

Arsenic <0.009 <0.0009 0.009 0.0009 

Beryllium <0.004 <0.0004 0.004 0.0004 

Cadmium <0.004 <0.0004 0.004 0.0004 

Chromium 0.032 0.0032 0.004 0.0004 

Cobalt <0.004 <0.0004 0.004 0.0004 

Lead 0.014 0.0014 0.004 0.0004 

Manganese 0.042 0.0042 0.004 0.0004 

Nickel 0.034 0.0034 0.004 0.0004 

Selenium 0.025 0.0025 0.007 0.0007 

Mercury 0.0012 0.00012 0.0001 0.00001 

Antimony <0.02 <0.002 0.02 0.002 

Arsenic <0.009 <0.0009 0.009 0.0009 

Beryllium <0.004 <0.0004 0.004 0.0004 

Cadmium 0.0045 0.00045 0.004 0.0004 

Chromium 0.051 0.0051 0.004 0.0004 

Cobalt 0.0042 0.00042 0.004 0.0004 

Lead 0.012 0.0012 0.004 0.0004 

Manganese 0.044 0.0044 0.004 0.0004 

Nickel 0.052 0.0052 0.004 0.0004 

Selenium 0.023 0.0023 0.007 0.0007 

Mercury <0.0001 <0.00001 0.0001 0.00001 

CHEMTEX, Port Arthur Is not NELAP accredited for the above anaiyte(s). Anatysis was subcontracted to another 

NELAP accredited laboratory. Report Is generated at CHEMTEX, Port Arthur, TX. 

• :See Case Narration 

NOTICE/DISCLAIMER: The snslytic:af tesulls., opinions or lnt@rpretatlons contain~ In this report ere bued upon lnfomatlon end ml!lteriell!lupplted by the Client for Whose QXC/uslvc and conlldentrar usc lhh!l report hee been m11dra . No por&on or entity other lh<'n Dle client may reley on this report.. Any s.uc:h reliance .....tw be unjuaUOed. An'/ penson other \har. the t ti&n\, \ha\ reeos thl5 report does so at his orh&r QIM'\ rl&~ The eniJiytlcal resull5, opinions end/or interpri!laUons expressed herein represent tile 'best JrJdgemenl ol Chemlex. based on lhelnformaUon end in•trucUons received lrom lhe client Chemlex makes no wammtyorrepresentaUon, express at implied, or any ~ope. and exp,.ssly disclaims 

~:srne This report ahall not be reprvduced, ln whole or In pert, \'ftthout the Wt1tten approVDI of Cheml~ In no event ahl'll Chemlex b& re~:.pon51b1t for eny darnltge greeter than the amount that II recalved for tt'le enelysis per fonned. 

1 of 11 

Qual 

,, . ., u : 92 
Mr. Tom Armstrong 

Phone: 1-214-631-0021 

Email: armst@ix.netcom.com 

david.mckeown@hanson.biz 

CHEMTEX 10 Sample ID 

P11010768 Quartz Fiber Filter 

P11010769 Acetone 

P11010770 0.1N HN03 

P11010773 Quartz Fiber Filter 

P11010774 Acetone 

P11010775 0.1N HN03 

MDL: Method Detection limit. 

Sample 

Volume 

(ml) 

175 

100 

285 

320 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgin,TX 

Date Received: 

01/28/11 

Time Received: 01:OOpm 

CHEMTEX File#: P11 010758 

Results* MDL 

Parameter mg/L mg/sample mg/L mglsample 

Antimony <0.02 <0.002 0.02 0.002 

Arsenic <0.009 <0.0009 0.009 0.0009 

Beryllium <0.004 <0.0004 0.004 0.0004 

Cadmium 0.0081 0.00081 0.004 0.0004 

Chromium 0.034 0.0034 0.004 0.0004 

Cobalt <0.004 <0.0004 0.004 0.0004 

Lead 0.010 0.0010 0.004 0.0004 

Manganese 0.129 0.0129 0.004 0.0004 

Nickel 0.021 0.0021 0.004 0.0004 

Selenium 0.022 0.0022 0.007 0.0007 

Mercury 0.0002 0.00002 0.0001 0.00001 

Antimony <0.02 <0.002 0.02 0.002 

Arsenic <0.009 <0.0009 0.009 0.0009 

Beryllium <0.004 <0.0004 0.004 0.0004 

Cadmium <0.004 <0.0004 0.004 0.0004 

Chromium 0.014 0.0014 0.004 0.0004 

Cobalt <0.004 <0.0004 0.004 0.0004 

Lead 0.024 0.0024 0.004 0.0004 

Manganese 0.545 0.0545 0.004 0.0004 

Nickel 0.008 0.0008 0.004 0.0004 

Selenium <0.007 <0.0007 0.007 0.0007 

Mercury <0.0001 <0.00001 0.0001 0.00001 

CHEMTEX, Port Arthur is not NELAP accredited for the above analyte(s). Analysis was subcontracted to another 

NELAP accredited laboratory. Report is generated at CHEMTEX, Port Arthur, TX. 

• :See Case Narration 

NOTICE/DISCLAIMER: The enalyticel re&ulle, opinions or lntorprelotiorts contlllned In lhts tepgrt ere ba•ed upon 1nrormat1on ;nd malarial .supplied by lhe client ror v.hose I!Xdusive and ctmrtdenial uae lhis r&pol1 hes been made. No person or ontlty other then the client may rala.y on lhlS report, Any 11uch ~llance wtn be u~u~Uried. Any pe~on olher than the client the I read& this roport does 50 al his or hero~ risk . The analytical results, opk"'lons ancVor interpretstfons expressed her(lln representlhe bestfudgement or Chemlex. based on the k'lfOnn,uon end lnsiNc.tlons received 1mm the cJie:nl. Chemtex ma"e5 no waFTBnty ot raprASet'119llon, axpress or Implied. or any type, end expressly ~Jsc m;. sama ih/s report shall nol be reproduced, In whole or ln pl!lrt, wilhoullhe W'l'lltan approval of Chemtex. In no event ehell Chemtex be rt~&ponstble for any dam ego grealer ttlM lhe omoun! lhellt received for lhe analysl6 per formed. 

2 of 11 

Qual 

'·' 93 
Email: armst@lx.netcom.com 

david.mckeown@hanson.biz 

CHEMTEXID 

P11010761 

P11010766 

Sample 10 

5% HN0;/10% H202 

MDL: Method Detection Limit. 

Time Received: 

CHEMTEX File#: 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgin,TX 

Sample 

Volume Results• 

Parameter (ml) mg/L mg/sample 

Antimony 340 0.042 0.006 

Arsenic 340 <0.009 <::0.0013 

Beryllium 340 <0.004 <0.0006 

Cadmium 340 <0.004 <o.ooos 

Chromium 340 0.018 0.0026 

Cobalt 340 <0.004 <0.0006 

Lead 340 0.0081 0.0011 

Manganese 340 1.570 0.2224 

Nickel 340 0.016 0.0023 

Selenium 340 0.011 0.0016 

Mercury 340 0.038 0.0129 

Antimony 370 <0.02 <0.003 

Arsenic 370 <0.009 <0.0012 

Beryllium 370 <0.004 <0.0005 

Cadmium 370 <0.004 <0.0005 

Chromium 370 0.018 0.0025 

Cobalt 370 <0.004 <0.0005 

Lead 370 0.0067 0.0009 

Manganese 370 0.025 0.0034 

Nickel 370 0.016 0.0022 

Selenium 370 <0.007 <0.0010 

Mercury 370 0.043 0.0159 

CHEMTEX, Port Arthur is not NELAP accredited for the above analyte(s). Analysis was subcontracted to another 

NELAP accredited laboratory. Report is generated at CHEMTJ:::X, Port Arthur, TX. 

• :See Case Narration 

01:OOpm 

P11010758 

mg/L 

0.02 

0.009 

0.004 

0.004 

0.004 

0.004 

0.004 

0.004 

0.004 

0.007 

0.0001 

0.02 

0.009 

0.004 

0.004 

0.004 

0.004 

0.004 

0.004 

0.004 

0.007 

0.0001 

NOTICE/DISCLAIMER: The analytical re5uiiS, opinion:~ or lnterpretstion;: conLalned In lhis ~por1e.re based upon informslion end material supplied by the cUent lor whose exclusive and confidenUal use flle: Ulport has been mOO e. No person or entity ottlt!l' then the client may relay on tt\ts repcul·Any tuch ~ance ..WI be un}u&\lned. Any person o\hM lhan the client. U'lBt read9 lhle rtJPQrt does so ot nts or herO'MI risk. The analyticsl re5ull$, opinions and/or lnlerprfltation!l expressed herein 1eprnsenl tho best judgement or Chemte11:, based on lhe information end in51nteUomll received from tie dlont. Chern lox makes no W;.lrranty or repr•s&nlalon, exprass or lmplt&d,of any type, and expressly disdaims nme. This reports hell nol be reproduced, In y,.hole or In par1, without the writien approval or Chemtox. In no evenlshall Chemlex be rotpons\ble for gny damage grealer than the 

~mounllhal II received ior lhe onely!lls per fonntd. 

3 of 11 

MDL 

mg/sample 

0.003 

0.0013 

0.0006 

0.0006 

0.0006 

0.0005 

0.0006 

0.0006 

0.0006 

0.0010 

0.00003 

0.003 

0.0012 

0.0005 

0.0005 

0.0005 

0.0005 

0.0005 

0.0005 

0.0005 

0.0010 

0.00004 

Qual 

94 
Time Received: 01:00pm Email: armst@ix.netcom.com CHEMTEX File#: P11010758 

david .mckeown@hanson. biz 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgin,TX 

Sam piA 

Volume Results* 

CHEMTEX ID Sample ID Parameter (ml) mg/L mglsample mg/L P11010771 5% HN03/10% HP2 Antimony 345 <0.02 <0.003 0.02 

Arsenic 345 <0.009 <0.0013 0.009 

Beryllium 345 <0.004 <0.0006 0.004 

Cadmium 345 <0.004 <0.0006 0.004 

Chromium 345 0.021 0.0030 0.004 

Cobalt 345 <0.004 <0.0006 0.004 

Lead 345 0.009 0.0013 0.004 

Manganese 345 0.157 0.0221 0.004 

Nickel 345 0.012 0.0017 0.004 

Selenium 345 <0.007 <0.0010 0.007 

Mercury 345 0.044 0.0152 0.0001 

P11010776 5% HNOa/1 0% H20 2 Antimony 390 <0.02 <0.003 O.Q2 

Arsenic 390 <0.009 <0.0012 0.009 

Beryllium 390 <0.004 <0.0005 0.004 

Cadmium 390 <0.004 <0.0005 0.004 

Chromium 390 0.03 0.004 0.004 

Cobalt 390 <0.004 <0.0005 0.004 

Lead 390 0.0046 0.0006 0.004 

Manganese 390 0.012 0.0016 0.004 

Nickel 390 0.0098 0.0013 0.004 

Selenium 390 0.007 0.0010 0.007 

Mercury 390 <0.0001 <0.00001 0.0001 

MDL: Method Detection Limit. 

CHEMTEX, Port Arthur is not NELAP accredited for the above analyte(s}. Analysis was subcontracted to another 

NELAP accredited laboratory. Report is generated at CHEMTEX, Port Arthur, TX. 

• :See Case Narration 

NOTICE/DISCLA.IMER: The Zlnalytleal re:~ult:~, oplnkme or lnterpretstiom; corUalned In this A!port are bit:~ed upon inrorrneUon end matettal supplied by the client ror v.hoee exduslve and conlldenUal use: this report hes been made. No pol'$on or entity othl!r than th~ cllet'lt may reley on this reporl Any s~.H;h re6anoe will be unjusUned. Any person oth~ lhan lhe cllenl.lhel ""'ds lhls report does so 81 h/6 or hera>w! rtsk. The onolytlcal result., opinions and/or Jnlerprelillons expressed ho~Jn '"P'"""IIht boSIJudgemenl of 

Chemle.~~. based on the ln(onn&Uon and lnstrvcGons rec~ved rrom Ute cllenl Chrmtex mekea nowarrentyorreprasentalion, e>cpress or\mpHed. of enytype, and exprteQiydl,dalm' eame. This repon shall nol be lllproducad, Ill whole or In part. wiU1oullhe wrillen epproval or Chemlmt. In no ev~nt shall Chemtex ba responsible for any dam~ge areeler thtm the emovnt lhetll received tor the analy&ls per formed. 

4 of 11 

MDL 

mglsample 

0.003 

0.0013 

0.0006 

0.0006 

0.0006 

0.0006 

0.0006 

0.0006 

0.0006 

0.0010 

0.00003 

0.003 

0.0012 

0.0005 

0.0005 

0.0005 

0.0005 

0.0005 

0.0005 

0.0005 

0.0009 

0.00004 

Qual 

95 
63

00

Time Received: 

Email: armst@ix.netcom.com CHEMTEX File#: 

david.mckeown@hanson.biz 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgin,TX 

Sample 

Volume Results• 

CHEMTEXID SampleiD Parameter (ml) mg/1. mg/samplt 

P11010762 4% KMn04/1 0% H2S04 Mercury 300 0.0140 0.00420 

P11010767 4% KMnOJ10% H2S04 Mercury 300 0.0054 0.00162 

P11010772 4% KMnOJ10% H2S04 Mercury 290 0.0046 0.00133 

P11010777 4% KMn04/10% H2S04 Mercury 350 <0.0001 <0.00002 

MDL: Method DetecUon Limit. 

CHEMTEX, Port Arthur is not NELAP accredited for the above analyte(s). Analysis was subcontracted to another 

NELAP accredited laboratory. Report is generated at CHEMTEX, Port Arthur. TX. 

• :See Case Narration 

01:00pm 

P11010758 

mg/1. 

0.0001 

0.0001 

0.0001 

0.0001 

NOTICE/DISCLAIMER: The enalyticl!l ~sul18, opinions or lnlerpretellons oontalnQd In ltlls report are bl'&~ upon informslion and mattrlalsupplied by the client Tor Y.tloSC! 

axclu&lve 11"16 conflde:nlilll use lhi~ rtJ)or1 h86 been me~o. No person or entity othef than the client mfl.y relay on lhls report Any such reliMce wUI be unjusiJned. Any petllon o\h•r 

than the t:llent, th11t rea.:b this report does so el his or h~r own rtsk. The analytical resulls, opinions and/or lnterprelldons expressed herein represent the be.stjl.dgemenl or 

Chemtex, based on the lnformallon and lnslrnctlons received from the client. Ch.:mle1i. mekee no warranty or representation, exprcs:s or Implied, of BfiY type, cand expressly disclaims 

sllm&. This ~port shall not be reproduced, ln whole or in part, without the 'Mitten approval of Chemtex. In no event &hell Chomtex be responsible for .any dem9Q& gra"ler than lhe 

amount thalll receiYed (or the snelysis per ronned. 

5 of 11 

MDL Qual 

mg/sample 

0.00003 

0.00003 

0.00003 

0.00004 

._; 96 
Phone: 1-214-631-0021 

Email: armst@ix.netcom.com 

david.mckeown@hanson.biz 

CHEMTEXID Sample 1D 

P11010759 Acetone 

P11010764 Acetone 

P11010769 Acetone 

P11010774 Acetone 

MDL: Method Detection Limit. 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgln,TX 

Time Received: 

CHEMTEX File#: 

Results' 

Parameter mg/kg mg/sample Particulate Matter 49.2 7.3 

Particulate Matter 55.4 6.8 

Particulate Matter 50.6 6.9 

ParticLJiate Matter 24.7 5.6 

• Analysis performed and report generated at CHEMTEX, Port Arthur, TX 

Qualifier Definition: 

Parameter 

Particulate Matter 

LABORATORY QUALITY CONTROL DATA 

Method Blank (mg/sample) 

Result 

< 0.1 

MDL 

0.1 

01:00pm 

P11010758 

MDL. 

mg/sample 

0.1 

0.1 0.1 

0.1 

Qual 

Parameter 

Particulate Matter 

LABORATORY QUALITY CONTROL DATA 

Method References/Analysis Dates & Analysts 

Method Reference 

PM Methos 5 (NIOSH Method 0500} 

Date Analyzed/Analyzed By 

02/03/11 TRS 

NOTICE/01 SCLAIMER: The analytical "'"utts. oplnloos or lnlerpreta.Uons contained In lhls report ere besed upon Jnlonnalion end ml!lteriel by the client for 'Mlose 

exclusive and conndenllal use this report has beoen made. No or entity other than tne client mayTt!lay on lhls 1'4tport. Any such reliance \IIIII be unjuatllled. Any person other 

than lhe climl, thet reeds this report does so et his or her own risk. The enetytical results, opinions 1!nd/or rucprened herein repreun\ lhe bes1 judgement ol 

Chemlex, based on the infonnallon and Instructions received rrom the cuenL Chcml.ex makes no warr.anty or representeHon, express or implied, of any I).'PEI. and eKpressly disdelms 

same. This report shall not be reproduced, In wholl'l or in pert wilhoullhe written approvZII or Chem\ex, In no event &hetl Ch(lmiBX he responsible for pny dem39e gre9ter the 

amounllhat it received ror tie pn&ly&is pM tonned. 

6 of 11 

Qual 

97 
Email: armst@ix.netcom.com 

david. mckeown@hanso n. biz 

CHEMTEXID Sample ID 

P11010756 Quartz Fiber Filter P11010763 Quartz Fiber Filter 

P11010768 Quartz Fiber Filter P11010773 Quartz Fiber Filter 

MDL: Method Detection Limit. 

RESULTS OF ANALYSIS 

PROJECT LOCATION: Elgin,TX 

Parameter 

Particulate Matter 

(Total dust) 

Particulate Matter 

(Total dust) 

Particulate Matter 

(Total dust) 

Particulate Matter 

(Total dust) 

CHEMTEX File#: 

Results* 

mg/sample 

0.25 0.75 

2.04 

<0.01 

*Analysis performed and report generated at CHEMTEX, Port Arthur, TX. 

Parameter 

Total Dust 

Qualifier Definition: 

LABORATORY QUALITY CONTROL DATA 

Method Blank (mg/sample) 

Result 

<0.01 

MDL 

O.D1 

P11010758 

MDL Qual 

mg/sample 

0.01 0.01 0.01 

0.01 

Qual 

Parameter 

Total Dust 

LABORATORY QUALITY CONTROL DATA 

Method References/Analysis Dates & Analysts 

Method Reference Date Analyzed! Analyzed By 

PM Method 5 (NIOSH Method 0500) 02/02/11 TRS 

NOTiCE/DISCLAIMER: The enelytlcpl re.$ulls, oplnkms or lnlerpretaUons c;onlalncd in thl& report ere based upOn lnformauon ond eupplled bylhe client 

C'!Xcluslve conflden11al use this report ha.a been m&de. No per:wn or enUty other than lhe client mey relay on lhi& report. Any such relicm;e v.ill be unjuGtiRecl. Any per.oon olhet' 

lhan the client. that reBds this ll!port does so at his: or her o'Ml riak. The anelyUcsl results, opinions sndlor lnterprelalions expressed herein represMt the bes1 Judgement of 

Chemlex, based on the inrorm.ellon and Instructions received from tho cUenl. Chemtex. meke& no warranty or representation, express or Implied, o( any type, end expressly disclaims 

sAme. Thl.s report shall not be reproduced, in "-"ole or in pert, without the written Dpprov(ll or Chamtex.ln no event shall Chemtex be responsible for eny damage greater than fhe 

amount that it received ror lhe enelysls per farmed. 7 of 11 98 
Method Blank (mg/L) 

QC Batch ID Parameter Result MDL 

Qb11021122 Antimony <0.02 0.02 

Arsenic <0.009 0.009 

Beryllium <0.004 0.004 

Cadmium <0.004 0.004 

Chromium <0.004 0.004 

Cobalt <0.004 0.004 

Lead <0.004 0.004 

Manganese <0.004 0.004 

Nickel <0.004 0.004 

Selenium <0.007 0.007 

LABORATORY QliALITY CONTROL DATA 

LCS and LCSD (mg/1) 

QC BatchiD Parameter Spk LCS LCS LCSO LCSD RPD RPD 

Added Result % Rec Result "IoRee Limit 

Ob11021122 Antimony 1.000 0.980 98 1.005 101 3 20 

Arsenic 1.000 1.029 103 1.037 104 20 

Beryllium 1.000 1.024 102 1.027 103 0.3 20 

Cadmium 1.000 1.017 102 1.020 102 0.3 20 

Chromium 1.000 1.018 102 1.021 102 0.3 20 

Cobalt 1.000 1.013 101 1.017 102 0.4 20 

Lead 1.000 1.019 102 1.028 103 1 20 

Manganese 1.000 1.020 102 1.024 102 0.4 20 

Nickel 1.000 1.020 102 1.023 102 0.3 20 

Selenium 1.000 1.036 104 1.044 104 20 

Qualifier Definition: 

NOTICE/DISCLAIMER: The Mllly\ical resulls, opinions orlnlerpnoiOUons conlaW.ed in lhis r<opo~""' b.,Gd upon lnfomoaUonand melerialsuppll«< by lho cllonl lorv.llose ~txtluSive an<f oonncten\Jal uoe !hi' report has been made. No pe:Boo or entity other lh81'\ the cllenl may r~ayon this reporl Any such rananc• -Mil be unJustmed. Any pet~on olher 

than the cllont, that ~ads: tills report does so al his or her o'Ml risk. The snalyttcal resutls, opfnions and/or lnl&rl)r9tallons expressed hertln represent the best Judgement or 

Chcmtex, based on the rnronnetloo end lntllllcliona received rrom the clienL Chemtax makes no w.rranty or represenlstion, expr99; or Implied, ol any type, and expre!sly d~claims same. ThiS repof'\ tlheU not be reproduced, In Yttlole or In pZirt, without the written approval of Chemlex. In no DV11nt shall Chemtex be reepoMible for sny damage Qrt:atar th:en the 

amount thalli received for the anaiY8i' per formed. 

8 of 11 

"IoRee 

Limit 

80-120 

80-120 

80-120 

80-120 

80-120 

80-120 

80-120 

80-120 

80-120 

80-120 

Qual 

Qual 

. : 99 
Method Blank (mg/L) 

QC Batch ID Parameter Result MDL 

Qb11021123 Antimony <0.02 0.02 

Arsenic <0.009 0.009 

Beryllium <0.004 0,004 

Cadmium <0.004 0.004 

Chromium <0.004 0.004 

Cobalt <0.004 0.004 

Lead <0.004 0.004 

Manganese <0.004 0.004 

Nickel <0.004 0.004 

Selenium <0.007 0.007 

LABORATORY QUALITY CONTROL DATA 

LCS and LCSD (mg/1) 

QC Batch ID Parameter Spk LCS LCS LCSD LSCSD RPD RPD 

Added Result % Rec Result %Rec Limit 

Qb11021123 Antimony 1.000 1.004 100 1.052 105 5 20 

Arsenic 1.000 1.038 104 1.059 106 2 20 

Beryllium 1.000 1.035 104 1.045 105 20 

Cadmium 1.000 1.031 103 1.079 108 5 20 

Chromium 1.000 1.031 103 1.045 105 1 20 

Cobalt 1.000 1.025 103 1.046 105 2 20 

Lead 1.000 1.030 103 1.021 102 1 20 

Manganese 1.000 1.031 103 1.033 103 0.2 20 

Nickel 1.000 1.033 103 1.049 105 2 20 

Selenium 1.000 1.050 105 1.057 106 20 

Qualifier Definition: 

NOTICEJDISCLAIMER: The anelytlc&lrt!!!JUIIJ. oplnk>na or Interpretations conlained In this report ere bZI!Jcd upon lnforma•on and matlt1191 .supplied by tho client torwho&e 

cxc:ILI!.Ive and ccnftdential use !his report has been mllde. No person or entity olher than the ciiMI may relay on this report Any such rt~ll~~.nce will be unjustined. Any person ou-.er 

than lh& client, thai re9d& 1hl& report does so at his or her own rtsk.. The analyiical resvlls, opinions and/or lnterprelallona fl)(preu9d he~n represC!nl !he bestjudgemenl or 

Chemtex. baaed on the lt'lfonnellon and lnstruc.llons recl!lved from f'le dlon!. Chern lex mak&S no warranty or re~.sentaUon, express or Implied. or any type. 8ftd expressly disclaims 

same. This report shall nol ba reproduced, in whole or In p8rt, -Mihoullhe wrltton opproval of Chemtex. In no event ehall ChemliX be responsible for 11ny d.,mege grealer then the 

amount thalli receive.d for the anelysifi par fonned. 

9 of 11 

%Rec 

Llmlt 

80-120 

80-120 

80-120 

80·120 

80·120 

80-120 

80-120 

80-120 

80-120 

80-120 

Qual 

Qual 

100 
QC Bacth 10 

Qb11020924 

QC Bacth ID 

Qb11020924 

Parameter 

QC Bacth ID: 

QC Sample ID: 

Mercury 

Parameter 

Mercury 

Parameter 

Mercury 

Sample 

Result 

Qb11020924 

11020241.04 

<0.0001 

Qualifier Definition: 

Spk 

LABORATORY QUALITY CONTROL DATA 

Method Blank (mgll) 

Result 

<0.0001 

LCS 

MDL 

0.0001 

Qual 

LCS and LCSD (mg/L) 

LCS LCSD LCSO 

Added Result "IoRee Result %Ret 

0.0050 0.0049 9B 0.0050 100 

MS and MSD (mg/L) 

MS Spk MS MS MSO MSO 

Added Result 'lo Rec Result %Ret 

0.005 0.0050 100 

Method References/Analysis Dates & Analysts 

RPO RPO 

Limit 

2.4 20 

RPD RPD 

Limit 

"lo Rec 

Limit 

B0-120 

o/o Rec 

Limit 

75-125 

Qual 

Qual 

' Parameter Method Reference Date Analyzed/Analyzed By 

Antimony Method 29 I EPA 6010C 02/10/11 

Arsenic Method 29/ EPA 6010C 02/10/11 

Beryllium Method 29 I EPA 601 OC 02/10/11 

Cadmium Method 29 I EPA 6010C 02/10111 

Chromium Method 29/ EPA 6010C 02/10/11 

Cobalt Method 29/ EPA 6010C 02/10/11 

Lead Method 29 I EPA 6010C 02/10/11 

Manganese Method 29/ EPA 601 DC 02/10/11 

Nickel Method 29/ EPA 6010C 02/10/11 

Selenium Method 29/ EPA 6010C 02/10/11 

Mercury Method 29/ EPA 7470A 02/08/11 

NOTICE/DJSCLAIMER: The analytical rosuiLs, opinions or Interpretations contained In this report are based upon rnronnatlon end mBterial suppned by lhe cllent ror v.hose 

exclusive and confidential use thl& report hae been mede. No person or enllty otner than the client may relay on \his repon. Any such reV.ance vAll be unjustified. Any pen;on other 

then the client. thet r&eds this report does so at his or her oVwn r1sk. The un"lyUcal mull&, opinion a and/or lnterpratallons expressed herein repreaentlhe best Jvd'oement of 

Chemtex, based on tho lnformejon end inan.cttone receiYed from the clit~nl Chemtex mattes no wammty or repreeentation, axpNJu or lmpllad, of any type, end expre~aly di&cleims 

same. This report ehsn not be reproduced, In tM\ole: orin pBrl wlthov1 W"le wrltten approve! or ChemleK. In no evenl shall Chemtax be recponslble for eny dtJmf'De prtl&ter then lt'le 

amount !hal II received for lhe analysis per formed. 

10 of 11 

sc 

sc 

sc 

sc 

sc 

sc 

sc 

sc 

sc 

sc 

ss 

101 
Case Narration 

a) Ref:P11 010758+759+760.P11 01763+764+765,P11010768+769+770,P1 1010773+774+775. 

1. Samples are digested and made to 1 OOmL volume. This volume is used for metals analysis including mercury. 

2. Results and Reporting Limits expressed in mg/L are reported as such. 

3. Results and Reporting Limits expressed in mg/sample are calculated from above mg/l values 

based on the sample volume 100ml (which is the volume after digestion). 

Ex: For the sample P11 01 0758+759+760, Mn-0.042mg/L for which 

mg/Sample value would be =0.042.100=0.0042 

1000 

b) Ref:P11 01 0761.P11 01 0766.P11 01 0771.P11 010776. 

1. A 100mL of sample is separated for the mercury analysis and the remaining sample is digested, made to 1 OOmL volume. 

This volume is used for metals analysis. 

2. Results and Reporting Limits expressed In mg/L are reported as such. 

3. Results and Reporting Limits expressed in mg/sample are calculated from above mg/L values 

based on the total sample volume. 

Ex: For the sample P11010761, Mn=1.57mg/L for which 

mg/Sample value would be =1.57*340*1 00 = 0.2224 

1000*240 

cl Ref:P11Q10762.P1101 0767.P11010772.P1101 0777. 

1. Samples are digested and volume is made up to original volume. It Is then analyzed for mercury. 

2. Results and Reporting Limits expressed in mg/L are reported as such. 

3. Results and Reporting Limits expressed in mg/sample are calculated from above mg/L values 

based on the total sample volume. 

Ex: For the sample P11 010762, Hg=0.014mg/L for which 

mg/Sample value would be =0.014*300 = 0.0042. 

1000 

rs*/CNR 

Dr. C. N. Reddy, Ph.D, CIH, ASP 

Director 

NOTICE/DISCLAIMER: The anely1ical restdlsi, oplnlons: or lnterpllillotlons contained In lhl1 reporl we based upon information and materi111l supplied by the clienl rorv..tlose~: 

exclusive and corildtnlfal Ule thl:s repor1 hal been m&de. No p11rcon or enUty othti1rthan lhR client may relpY on thle: report Any sueh renance W\11 be unjudOed. Any person other 

than lh~ client. thai reeds lhls report does so at his or her O'M'I rfsk. The anal)'11ca1 results, opinions and/or lnt-:rpretations expressed Mreh1 te:pn=sent th·e be•l Judgement of 

ChemtelC, besecl on the lntonnatlon and lnstruction6 reeeived from tie cllenl ChamhiiX me'<es no wam~ntv or rept'eZ!enlellon, txpreu orknplied, or any type, and expressly disclaims 

uma. This rl!port shalt ncl be reproduced, In ~ole or In part, wilhcullhe wrillen approv&l of Chemtex. In no evenl ~htth Chemtex be responalblo 1or any damage g~aier than \he 

amounl thzt It received for the EmBiysl& per formed. 

11 of 11 

J 02 
~· -: .. -' 

Ar·mstrortg Environmental, Inc. 

17 48 Hlavek Rd 

PHONE ·No. (214-)'631-:0021. 

Decatur, TX 76234 t:S -JA..~: t - Arm 5t ~ >-t i n.e.k.oWL • cOM. 

·cHAIN OF .CU~TODV RECORD 

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Arm!rtrong Environmental, Ihc. 

PIIONE-:NO. (214)'631~0021 

:ff-M.'l- Arh1st~ 'II ,ne.b~ .c~ ' 1748 Hlavek Rd 

Decatur, TX 76234 ·cHAIN OF CU~TODY RECORD •,.. 

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