# TECa LaboratoryServices

'Af'¥1PA ELECTRIC 5012 

### Causeway Blvd * 

### Tampa FI. 33619 * Ph (813)630-7490 * 

### Fax (813)630-7360 * DOH #E54272 

## Report For: Ray McOarby 

# ReportDate: 8/31/2010 

# U/i1:-t**~I** 

# Laboratory 10: AB06224 Location Code: 

# TE_BBJCR_STUDY Sample Information Description: 

## Big Bend ICRTests-Method 26a Sampled 

## By: ProjectAccountCode: Date and Time Collected: 

## 3/10/201012:00:00AM Sample Collection Method: DateofSample Receipt: 

## 3/1212010 

## Laboratory Results Qualifier Test Analysis Lower Upper Violation PARAMETER Result Units MOL Code Method**Anal~st** 

### Date &

### Time Limit Limit Check Chloride Duplicate result, Run 1 a 34,752 uglmL 0,05 Method26a KASZS 3/23120102:23:00 PM Chloride Duplicate result, Run 1b 12.701 uglmL 0,05 Method 26a KASZS 3/23120102:23:00 PM Chloride Duplicate result, Run 2a 39,385 uglmL 0,05 Method26a KASZS 3123120102:2300 PM Chloride Duplicate result, Run 2b 7,880 uglmL 0,05 Method 26a KASZS 3124120102:23:00 PM Chloride Duplicate result Run 3a 33567 ug/mL Method26a KASZS 3123120102:23:00 PM Chloride Duplicate result, Run 3b 9,952 uglmL Method 26a KASZS 3/24/20102:23:00 PM Chloride result, Run 1 a 35,519 uglmL 0,05 Method 26a KASZS 3/23/20102:23:00 PM Chloride result Run 1 b 12,686 uglmL 0,05 Method 26a KASZS 3/23/20102:23:00 PM Chloride result, Run 2a 40,146 uglmL 0,05 Method26a KASZS 3/2312010 2:23:00 PM Chloride result, Run 2b 7,855 uglmL 0,05 Method 26a KASZS 3/24120102:2300 PM Chloride result, Run 3a 33.756 uglmL 0,05 Method 26a KASZS 312312010 2:23:00 PM Chloride result, Run 3b 9,911 ug/mL 0,05 Method 26a KASZS 3124120102:23:00 PM Chloride, Duplicate Blank result 0041 ug/mL EPA Method26a KASZS 3/24120102:23:00 PM Final Sample Volume, Run 1 a 320 mL EPA Method 26a KASZS 3124/2010 2:23:00 PM Final SampleVolume, Run 1 b 410 mL EPA Method 26a KASZS 3/2412010 2:23:00 PM Final Sample Volume, Run 2a 460 mL EPA Method 26a KASZS 3/24/201022300 PM Final Sample Volume, Run 2b 380 ml EPA Method 26a KASZS 3124120102:23:00 PM Final SampleVolume, Run 3a 440 ml EPA Method26a KASZS 3/24/20102:23:00 PM Final Sample Volume, Run 3b 360 mL EPA Method 26a KASZS 3/24/20102:23:00 PM Fluoride Duplicate result, Run 1a 0.403 uglmL 0,05 Method26a KASZS 3/24120102:23:00 PM Fluonde Duplicate result, Run 1b 0.125 ug/mL 0.05 Method26a KASZS 3/24120102:23:00 PM Fluoride Duplicate result, Run 2a 0,481 ug/mL 0,05 Method 26a KASZS 3124120102:23:00 PM Fluoride Dupiicate result, Run 2b 0148 ug/mL 0.05 Method 26a KASZS 3/24/20102:23:00 PM Fluoride Duplicate result, Run 3a 0.620 ug/mL 0.05 Method 26a KASZS 3/24/20102:23:00 PM Fluoride Duplicate result, Run 3b 0.239 ug/mL 0.05 Method26a KASZS 3/24/20102:23:00 PM

Laboratory Services certifiesthatthe test results in this report meet all requirements ofthe NELAC standards, unless indicated otherwise in the body ofthe report. Unless otherwise noted, all methodsfollowed are perthe most current published version of40CFR Part 136, Table B, Results reported on this report pertain to the above referenced sampleonly,

Report Number. AB06224-083110-09 

### , Page I of2 "GeneralReport'

# "TEca LaboratoryServices

T,A

....... FlA EL_ECTRIC 5012 Causeway Blvd • Tampa 

### FI. 33619 

# . Ph (813)630-7490 

# . Fax (813)630-7360 

# . DOH #E54272 

### Qualifier Test Analysis Lower Upper Violation PARAMETER Result Units MOL Code Method Anallst Date&Time Limit Limit Check Fluoride, Duplicate Blank result < uglmL U EPA Method 26a 

## KASZS 3124120102:23:00 PM HCL result. Run 1 a 11545 ug Method 26a 

## KASZS 3124/20102:23:00PM HCL result, Run 1 b 5333 ug Method 26a 

## KASZS 3/24/20102:23:00PM HCL result, Run 2a 18785 ug Method 26a 

## KASZS 3124120102:23:00 PM HCL result, Run 2b 3057 ug Method26a 

## KASZS 3/24/20102:23:00 PM HCL result. Run 3a 15207 ug Method 26a 

## KASZS 3124120102:23:00 PM HCL result. Run 3b 3660 ug Method26a 

## KASZS 3/24/20102:23:00PM HF result. Run 1a 134.8 ug Method26a 

## KASZS 3124120102:23:00 PM HF result. Run 1 b 53.8 ug Method 26a 

## KASZS 3/24/20102:23:00PM HF result. Run2a 232 ug Method26a 

## KASZS 3124120102:23:00 PM HF result, Run2b 58.8 ug Method 26a 

## KASZS 3/24/20102:23:00PM H Fresult, Run3a 285 ug Method26a 

## KASZS 3/24/20102:23:00 PM HF result, Run3b 90,0 ug Method26a 

## KASZS 3124/20102:23:00 PM 

## Comments All results calculated on awetto wet basis, unlessotherwise indicated, 

### Data QualifierCodes Explanation: U Indicates that the compound was analyzed for but not detected. I The reported value is between the laboratory method detection limit (MDl)and the laboratory practical quantitation limit (Pal). pal

## = 4 x MDL. 

### Should there be any questions regarding this report, please contact:

Cheryl Howard, Designee for Peggy Penner, Manager, Laboratory Services (813) 630-7490

Laboratory Services certifies thatthetest results in this report meetall requirements ofthe NELAC standards, unless indicated otherwise in the bodyofthe report, Unless otherwise noted, all methods followed are perthe mostcurrent published version of40CFR Part 136, Table S, Results reported on this report pertain tothe above referenced sampleonly,

Report Number: "GeneralReport" AB06224-083110·09 

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