TECa Laboratory Services 'Af'¥1PA ELECTRIC 5012 Causeway Blvd * Tampa FI. 33619 * Ph (813)630-7490 * Fax (813)630-7360 * DOH #E54272 

Report For: Ray McOarby Report Date: 8/31/2010 

U/i1:-t ~I 

Laboratory 10: AB06224 

Location Code: TE_BBJCR_STUDY 

Sample Information 

Description: Big Bend ICR Tests-Method 26a Sampled By: 

Project Account Code: Date and Time Collected: 3/10/201012:00:00 AM 

Sample Collection Method: Date of Sample Receipt: 3/1212010 

Laboratory Results 

Qualifier Test Analysis Lower Upper Violation 

PARAMETER Result Units MOL Code Method Anal~st Date & Time Limit Limit Check 

Chloride Duplicate result, Run 1 a 34,752 uglmL 0,05 Method 26a KASZS 3/23120102:23:00 PM 

Chloride Duplicate result, Run 1b 12.701 uglmL 0,05 Method 26a KASZS 3/23120102:23:00 PM 

Chloride Duplicate result, Run 2a 39,385 uglmL 0,05 Method 26a KASZS 3123120102:2300 PM 

Chloride Duplicate result, Run 2b 7,880 uglmL 0,05 Method 26a KASZS 3124120102:23:00 PM 

Chloride Duplicate result Run 3a 33567 ug/mL Method 26a KASZS 3123120102:23:00 PM 

Chloride Duplicate result, Run 3b 9,952 uglmL Method 26a KASZS 3/24/2010 2:23:00 PM 

Chloride result, Run 1 a 35,519 uglmL 0,05 Method 26a KASZS 3/23/20102:23:00 PM 

Chloride result Run 1 b 12,686 uglmL 0,05 Method 26a KASZS 3/23/20102:23:00 PM 

Chloride result, Run 2a 40,146 uglmL 0,05 Method 26a KASZS 3/2312010 2:23:00 PM 

Chloride result, Run 2b 7,855 uglmL 0,05 Method 26a KASZS 3/24120102:2300 PM 

Chloride result, Run 3a 33.756 uglmL 0,05 Method 26a KASZS 312312010 2:23:00 PM 

Chloride result, Run 3b 9,911 ug/mL 0,05 Method 26a KASZS 3124120102:23:00 PM 

Chloride, Duplicate Blank result 0041 ug/mL EPA Method 26a KASZS 3/24120102:23:00 PM 

Final Sample Volume, Run 1 a 320 mL EPA Method 26a KASZS 3124/2010 2:23:00 PM 

Final Sample Volume, Run 1 b 410 mL EPA Method 26a KASZS 3/2412010 2:23:00 PM 

Final Sample Volume, Run 2a 460 mL EPA Method 26a KASZS 3/24/201022300 PM 

Final Sample Volume, Run 2b 380 ml EPA Method 26a KASZS 3124120102:23:00 PM 

Final Sample Volume, Run 3a 440 ml EPA Method 26a KASZS 3/24/20102:23:00 PM 

Final Sample Volume, Run 3b 360 mL EPA Method 26a KASZS 3/24/20102:23:00 PM 

Fluoride Duplicate result, Run 1a 0.403 uglmL 0,05 Method 26a KASZS 3/24120102:23:00 PM 

Fluonde Duplicate result, Run 1b 0.125 ug/mL 0.05 Method 26a KASZS 3/24120102:23:00 PM 

Fluoride Duplicate result, Run 2a 0,481 ug/mL 0,05 Method 26a KASZS 3124120102:23:00 PM 

Fluoride Dupiicate result, Run 2b 0148 ug/mL 0.05 Method 26a KASZS 3/24/20102:23:00 PM 

Fluoride Duplicate result, Run 3a 0.620 ug/mL 0.05 Method 26a KASZS 3/24/20102:23:00 PM 

Fluoride Duplicate result, Run 3b 0.239 ug/mL 0.05 Method 26a KASZS 3/24/20102:23:00 PM 

Laboratory Services certifies that the test results in this report meet all requirements of the NELAC standards, unless indicated otherwise 

in the body of the report. Unless otherwise noted, all methods followed are per the most current published version of 40 CFR Part 136, Table B, 

Results reported on this report pertain to the above referenced sample only, 

Report Number. AB06224-083110-09 , Page I of2 "General Report' 
"TEca Laboratory Services T,A ....... FlA EL_ECTRIC 
 5012 Causeway Blvd • Tampa FI. 33619 . Ph (813)630-7490 . Fax (813)630-7360 . DOH #E54272 

Qualifier Test Analysis Lower Upper Violation 

PARAMETER Result Units MOL Code Method Anallst Date & Time Limit Limit Check 

Fluoride, Duplicate Blank result < uglmL U EPA Method 26a KASZS 3124120102:23:00 PM 

HCL result. Run 1 a 11545 ug Method 26a KASZS 3124/20102:23:00 PM 

HCL result, Run 1 b 5333 ug Method 26a KASZS 3/24/20102:23:00 PM 

HCL result, Run 2a 18785 ug Method 26a KASZS 3124120102:23:00 PM 

HCL result, Run 2b 3057 ug Method 26a KASZS 3/24/2010 2:23:00 PM 

HCL result. Run 3a 15207 ug Method 26a KASZS 3124120102:23:00 PM 

HCL result. Run 3b 3660 ug Method 26a KASZS 3/24/20102:23:00 PM 

HF result. Run 1a 134.8 ug Method 26a KASZS 3124120102:23:00 PM 

HF result. Run 1 b 53.8 ug Method 26a KASZS 3/24/20102:23:00 PM 

HF result. Run2a 232 ug Method 26a KASZS 3124120102:23:00 PM 

HF result, Run2b 58.8 ug Method 26a KASZS 3/24/20102:23:00 PM 

H F result, Run3a 285 ug Method 26a KASZS 3/24/2010 2:23:00 PM 

HF result, Run3b 90,0 ug Method 26a KASZS 3124/20102:23:00 PM 

Comments 

All results calculated on a wet to wet basis, unless otherwise indicated, 

Data Qualifier Codes Explanation: 

U Indicates that the compound was analyzed for but not detected. 


I The reported value is between the laboratory method detection limit (MDl) and the laboratory practical quantitation limit (Pal). pal =4 x MDL. 


Should there be any questions regarding this report, please contact: 

Cheryl Howard, 


Designee for Peggy Penner, 


Manager, Laboratory Services 


(813) 630-7490 

Laboratory Services certifies that the test results in this report meet all requirements of the NELAC standards, unless indicated otherwise 

in the body of the report, Unless otherwise noted, all methods followed are per the most current published version of 40 CFR Part 136, Table S, 

Results reported on this report pertain to the above referenced sample only, 

Report Number: "General Report" AB06224-083110·09 Page 2 of2