### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

4125 Manitowoc Public Utilities B09 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 4125 Manitowoc Public Utilities B09 As Received Higher Heating Value 

### 4125 Manitowoc Public Utilities B09 As Received % Moisture 

### 4125 Manitowoc Public Utilities B09 As Received % Ash 

### 4125 Manitowoc Public Utilities B09 As Received % Sulfur 

### 4125 Manitowoc Public Utilities B09 Dry

basis Higher Heating Value 

### 4125 Manitowoc Public Utilities B09 Dry

basis % Ash 

### 4125 Manitowoc Public Utilities B09 Dry

basis % Sulfur 

### 4125 Manitowoc Public Utilities B09 Dry

basis Antim ony 

### 4125 Manitowoc Public Utilities B09 Dry

basis Arsenic 

### 4125 Manitowoc Public Utilities B09 Dry

basis Bery llium 

### 4125 Manitowoc Public Utilities B09 Dry

basis Cadmium 

### 4125 Manitowoc Public Utilities B09 Dry

basis Chlorine 

### 4125 Manitowoc Public Utilities B09 Dry

basis Chromium 

### 4125 Manitowoc Public Utilities B09 Dry

basis Cobalt 

### 4125 Manitowoc Public Utilities B09 Dry

basis Fluorine 

### 4125 Manitowoc Public Utilities B09 Dry

basis Lead 

### 4125 Manitowoc Public Utilities B09 Dry

basis Manganese 

### 4125 Manitowoc Public Utilities B09 Dry

basis Mercury 

### 4125 Manitowoc Public Utilities B09 Dry

basis Nickel 

### 4125 Manitowoc Public Utilities B09 Dry

basis SeleniumAn alysis M ethod for each Analyte

(example: ASTM D5865-04) 

### ASTM D5373-02 ASTM D5373-02 ASTM D5373-02 ASTM D5373-02 ASTM D5373-02 ASTM D5373-02 ASTM D5373-02 EPA-SW-846, Method 3030B EPA-SW-846, Method 3030B EPA-SW-846, Method 3030B EPA-SW-846, Method 3030B USGS Bulletin 1823 EPA-SW-846, Method 3030B EPA-SW-846, Method 3030B ASTM 3761-96 EPA-SW-846, Method 3030B EPA-SW-846, Method 3030B ASTM 6722 EPA-SW-846, Method 3030B EPA-SW-846, Method 3030BEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 4125 Manitowoc Public Utilities B09 Non-dioxin/furan organic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher

Heating Value (HHV) (as received) HHV Units % Moisture (as received) 3 

### 4/20/2010 4/20/2010 11930.00 BTU/lb 11.04 4 4/21/2010 4/21/2010 12858.00 Btu/lb 12.07 Fuel Testing Results% A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) 

### 2.51 3.71 13409 Btu/lb 2.82 4.17 1.45 4.7 14623 Btu/lb 1.65 5.35Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) Cadmium

UnitsChromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units Selenium (Dry Basis)Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 4125 Manitowoc Public Utilities B09 Dioxin/furan HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 3 

### 4/20/2010 4/20/2010 11930.00 BTU/lb 4 4/21/2010 4/21/2010 12858.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 11.04 2.51 3.71 13409 Btu/lb 2.82 4.17 12.07 1.45 4.7 14623 Btu/lb 1.65 5.35Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 4125 Manitowoc Public Utilities B09 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 

### 5/18/2010 5/18/2010 12181.00 Btu/lb 2 5/19/2010 5/19/2010 12658.00 Btu/lb 3 5/20/2010 5/20/2010 11930.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 10.53 3.51 3.88 13615 Btu/lb 3.92 4.33 290 mg/kg 9.22 1.9 4.4 13943 Btu/lb 2.09 4.84 4080 mg/kg 11.04 2.51 3.71 13409 Btu/lb 2.51 3.71 379 mg/kgMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis)



### 0.017 mg/kg 0 mg/kg 9.45 mg/kg 0.03 mg/kg 0.03 0.01 mg/kg 0 mg/kg 9.14 mg/kg 0.02 mg/kg 0.03Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units



### mg/kg 0.67 mg/kg 0.68 mg/kg 1.77 mg/kg 154.03 mg/kg mg/kg 0.73 mg/kg 0.79 mg/kg 2.2 mg/kg 114.15 mg/kgSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units



### 0.18 mg/kg 15 mg/kg 0.63 mg/kg 0.23 mg/kg 24 mg/kg 0.51 mg/kgEIA

Facility Code Facility

Name Boiler ID HAPs Test Group 

### 4125 Manitowoc Public Utilities B09 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 2 

### 5/19/2010 5/19/2010 12658.00 Btu/lb 3 5/20/2010 5/20/2010 11930.00 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units 

### 9.22 1.9 4.4 13943 Btu/lb 2.09 4.84 4080 mg/kg 11.04 2.51 3.71 13409 Btu/lb 2.51 3.71 379 mg/kgMercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 

### 0.017 mg/kg 0 mg/kg 9.45 mg/kg 0.03 mg/kg 0.03 0.01 mg/kg 0 mg/kg 9.14 mg/kg 0.02 mg/kg 0.03Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units 

### mg/kg 0.67 mg/kg 0.68 mg/kg 1.77 mg/kg 154.03 mg/kg mg/kg 0.73 mg/kg 0.79 mg/kg 2.2 mg/kg 114.15 mg/kgSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units 

### 0.18 mg/kg 15 mg/kg 0.23 mg/kg 24 mg/kg