InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.ThisInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.lhl id hi hhf ll iiiInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1PleaseentertheEIAFacilityCodeFacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheetInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMInstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.SelecttheHAPsTestGroup(i.e.,HAPsurrogate)forwhichthetab'sdatareflects(orangehighlightedcell).InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.SelecttheHAPsTestGroup(i.e.,HAPsurrogate)forwhichthetab'sdatareflects(orangehighlightedcell).7.ProvidetheSampleNumberandSampleDateontheFuelsSampleResultsworksheet.Youmustprovideaminimumof3compositesamplesconsistingof3combinedgrabsampleseach,butyouarenotlimitedtothatnumberifyouhavecollectedmore.8.Providetheresultsoftheanalysesforeachconstituentrequested.Usethedrop‐downboxestofillintheunitsofmeasure.InstructionsforcompletingtheFuelMaterialAnalysisInformationThisInformationCollectionRequest(ICR)spreadsheetisintendedtocollectinformationaboutchemicalanalysesoffuelsusedfossilfuelburningpowerplants.Constituentsofconcernare:mercury,chlorine,fluorine,andmetals,suchasantimony,beryllium,cadmium,chromium,cobalt,lead,manganese,nickel,andselenium.Thisspreadsheetisintendedtobeusedforoneboilerofonefacilitybutisdesignedtoallowmultiple(upto4)fuelanalysesatthatspecificboiler.Thisnumberofanalyseswouldcoincidewithoneboilerwhereemissionstestingforall4HAPsurrogateswerebeingtested.Dataformultipleboilersshouldbehandledbyusingseparatespreadsheets.Fieldsthatarehighlightedinyellowarerequiredfields.Greenhighlightedcellsshouldbefilledusingthedrop‐downboxes,included.Grayfieldsareautomaticallyfilledfromotherfields.Pleasenameeachresultingspreadsheetwiththefollowingnamingconvention:[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls(example:8100_Unit_2_Fuels_Testing.xls).Pleaserefertothefollowingstepswhenusingthesespreadsheets.1.PleaseentertheEIAFacilityCode,FacilityNameandBoilerIDofyourboilerontheBoilerInformationworksheet.2.PleaseenterthetestdateontheBoilerInformationworksheet.3.Pleasechoosethetypeoffuelbeingsampledusingthedrop‐downinthefuelcolumnoftheBoilerInformationworksheet.Ifyouchoose"other",pleaseprovideadescriptionofthefuelintheOtherFuelDescriptioncolumn.4.PleaseprovidetheanalysismethodforeachconstituentintheAnalysisMethodsworksheet.Forexample:"ASTMD5865‐04".5.PleasechecktheUnitsofMeasuretablesforHHV,Metals,andCl/FlinthePicklistworksheet(orangetab).Iftheunits ofmeasurethatyouplantoreportarenotfoundintheUnitsofmeasuretable,pleasefillthemintheblank,orangehighlighted,cellineachtable.ThisallowsyoutochoosetheunitsofmeasureintheFuelsSampleResultsworksheet.6.SelecttheHAPsTestGroup(i.e.,HAPsurrogate)forwhichthetab'sdatareflects(orangehighlightedcell).7.ProvidetheSampleNumberandSampleDateontheFuelsSampleResultsworksheet.Youmustprovideaminimumof3compositesamplesconsistingof3combinedgrabsampleseach,butyouarenotlimitedtothatnumberifyouhavecollectedmore.8.Providetheresultsoftheanalysesforeachconstituentrequested.Usethedrop‐downboxestofillintheunitsofmeasure.

# EIA Facility Code Facility Name Boiler ID Fuel Type 1

10151 American Bituminous Units 1/2 

# coal refuse (culm or gob)

# Fuel Type 2 Fuel Type 3 Other Fuel Description

# EIA Facility Code Facility Name Boiler ID Basis Analyte



# 10151 American Bitumin o Units 1/2 As Received Higher Heating Value



# 10151 American Bitumin o Units 1/2 As Received % Moisture



# 10151 American Bitumin o Units 1/2 As Received % Ash



# 10151 American Bitumin o Units 1/2 As Received % Sulfur



# 10151 American Bitumin o Units 1/2 Dry basis Higher Heating Value



# 10151 American Bitumin o Units 1/2 Dry basis % Ash



# 10151 American Bitumin o Units 1/2 Dry basis % Sulfur



# 10151 American Bitumin o Units 1/2 Dry basis Antimony



# 10151 American Bitumin o Units 1/2 Dry basis Arsenic



# 10151 American Bitumin o Units 1/2 Dry basis Beryllium



# 10151 American Bitumin o Units 1/2 Dry basis Cadmium



# 10151 American Bitumin o Units 1/2 Dry basis Chlorine



# 10151 American Bitumin o Units 1/2 Dry basis Chromium



# 10151 American Bitumin o Units 1/2 Dry basis Cobalt



# 10151 American Bitumin o Units 1/2 Dry basis Fluorine



# 10151 American Bitumin o Units 1/2 Dry basis Lead



# 10151 American Bitumin o Units 1/2 Dry basis Manganese



# 10151 American Bitumin o Units 1/2 Dry basis Mercury



# 10151 American Bitumin o Units 1/2 Dry basis Nickel



# 10151 American Bitumin o Units 1/2 Dry basis Selenium

# A na l ys i s M e th o d f or eac h A na l y t e

(example: ASTM D5865-04)

Modified ASTM D2961 & D3302

ASTM D3180

ASTM D3174 &/or D5142

ASTM D4239

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6357

ASTM D6721

ASTM D6357

ASTM D6357

ASTM D3761

ASTM D6357

ASTM D6357

ASTM D6722

ASTM D6357

ASTM D4606EIA Facility Code Facility Name Boiler IDHAPs Test Group10151 AmericanBituminous Units1/2 Mercuryandnon‐mercurymetalicHAPsSample Number(minimum of 3compositesamples)Test Start Date(MM/DD/YYYY)Test Stop Date(MM/DD/YYYY)Higher Heating Value(HHV)(as received) HHV Units% Moisture(as received)% Ash(as received)% Sulfur(as received)HigherHeatingValue (HHV)(Dry Basis)HHV Units16/8/2010 6/8/2010 7518.00 Btu/lb 13.76 33.28 2.12 8718 Btu/lb2 6/9/2010 6/9/2010 7619.00 Btu/lb 13.12 34.45 2.44 8770 Btu/lb3 6/10/2010 6/10/2010 7527.00 Btu/lb 11.92 35.13 2.31 8546 Btu/lbFuel Testing Results% Ash(Dry Basis)% Sulfur(Dry Basis)Chlorine(Dry Basis)ChlorineUnitsMercury(Dry Basis)MercuryUnitsAntimony(Dry Basis)AntimonyUnitsArsenic (DryBasis)ArsenicUnitsBeryllium(Dry Basis)BerylliumUnitsCadmium(Dry Basis)CadmiumUnitsChromium(Dry Basis)ChromiumUnits38.59 2.46 424 ppm 0.262 ppm 2.657 ppm 23.712 ppm 1.264 ppm 0.243 ppm 39.128 ppm39.66 2.81 378 ppm 0.263 ppm 2.48 ppm 24.756 ppm 1.341 ppm 0.224 ppm 40.65 ppm39.88 2.63 327 ppm 0.274 ppm 2.2 ppm 27.495 ppm 1.426 ppm 0.244 ppm 41.976 ppmNote the Proximate/Ultimate data belowLead (DryBasis) Lead UnitsManganese(Dry Basis)ManganeseUnitsNickel (DryBasis) Nickel UnitsSelenium(Dry Basis)SeleniumUnitsFluorine(Dry Basis)FluorineUnitsCobalt (DryBasis) Cobalt UnitsTotal Moisture Volatiles Ash Fixed Carbon13.55 ppm 96.892 ppm 21.866 ppm 2.93 ppm 9.067 ppm 13.76 25.77 38.5912.886 ppm 86.89 ppm 23.272 ppm 2.333 ppm 9.492 ppm 13.12 26.19 39.6612.587 ppm 75.927 ppm 22.994 ppm 3.346 ppm 9.47 ppm 11.92 26.32 39.88Proximate Analyses, % by wtwshould be recorded on a dry basis (including ash).Carbon Hydrogen Nitrogen Total Sulfur Oxygen45.93 3.16 1 2.46 8.8648.55 3.34 1.06 2.81 4.5847.03 3.26 1.06 2.63 6.14Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler IDHAPs Test Group10151 AmericanBituminous Units1/2 Non‐dioxin/furanorganicHAPsSample Number(minimum of 3compositesamples)Test Start Date(MM/DD/YYYY)Test Stop Date(MM/DD/YYYY)Higher HeatingValue (HHV)(as received) HHV Units% Moisture(as received)% Ash(as received)% Sulfur(as received)HigherHeatingValue (HHV)(Dry Basis)HHV Units% Ash(Dry Basis)16/8/2010 6/8/2010 7387.00 Btu/lb 14.11 34.05 1.97 8601 Btu/lb 39.642 6/10/2010 6/10/2010 7589.00 Btu/lb 11.89 35.02 2.27 8613 Btu/lb 39.743 6/10/2010 6/10/2010 7559.00 Btu/lb 12.39 34.73 2.3 8628 Btu/lb 39.64Fuel Testing Results% Sulfur(Dry Basis)Chlorine(Dry Basis)ChlorineUnitsMercury(Dry Basis)MercuryUnitsAntimony(Dry Basis)AntimonyUnitsArsenic (DryBasis)ArsenicUnitsBeryllium(Dry Basis)BerylliumUnitsCadmium(Dry Basis)CadmiumUnitsChromium(Dry Basis)ChromiumUnits2.32.582.62Note the Proximate/Ultimate dataLead (DryBasis) Lead UnitsManganese(Dry Basis)ManganeseUnitsNickel (DryBasis) Nickel UnitsSelenium(Dry Basis)SeleniumUnitsFluorine(Dry Basis)FluorineUnitsCobalt (DryBasis) Cobalt UnitsTotal Moisture Volatiles Ash Fixed Carbon14.11 25.62 39.6411.89 26.07 39.7412.39 25.92 39.64Proximate Analyses, % by wtabelow should be recorded on a dry basis (including ash).Carbon Hydrogen Nitrogen Total Sulfur Oxygen47.49 3.16 1.05 2.3 6.3646.62 3.23 1.01 2.58 6.8248 3.23 1.11 2.62 5.4Ultimate Analyses, % by wtEIA Facility Code Facility Name Boiler IDHAPs Test Group10151 AmericanBituminous Units1/2 AcidgasHAPsSample Number(minimum of 3compositesamples)Test Start Date(MM/DD/YYYY)Test Stop Date(MM/DD/YYYY)HigherHeatingValue (HHV)(asreceived) HHV Units% Moisture(asreceived)% Ash(asreceived)% Sulfur(asreceived)HigherHeatingValue (HHV)(Dry Basis)HHV Units% Ash(Dry Basis)16/8/2010 6/8/2010 7425.00 Btu/lb 12.86 34.12 2.14 8520 Btu/lb 39.152 6/9/2010 6/9/2010 7224.00 Btu/lb 12.21 36.61 2.34 8228 Btu/lb 41.73 6/10/2010 6/10/2010 7559.00 Btu/lb 12.39 34.73 2.3 8628 Btu/lb 39.64Fuel Testing Results% Sulfur(Dry Basis)Chlorine(Dry Basis)ChlorineUnitsMercury(Dry Basis)MercuryUnitsAntimony(Dry Basis)AntimonyUnitsArsenic (DryBasis)ArsenicUnitsBeryllium(Dry Basis)BerylliumUnitsCadmium(Dry Basis)CadmiumUnitsChromium(Dry Basis)ChromiumUnits2.45 405 ppm2.67 352 ppm2.62 366 ppmNote the Proximate/Ultimate dataLead (DryBasis) Lead UnitsManganese(Dry Basis)ManganeseUnitsNickel (DryBasis) Nickel UnitsSelenium(Dry Basis)SeleniumUnitsFluorine(Dry Basis)FluorineUnitsCobalt (DryBasis) Cobalt UnitsTotal Moisture Volatiles Ash Fixed Carbon120 ppm 12.86 26.6 39.15120 ppm 12.21 26.74 41.792 ppm 12.39 25.92 39.64Proximate Analyses, % by wtabelow should be recorded on a dry basis (including ash).Carbon Hydrogen Nitrogen Total Sulfur Oxygen48.29 3.24 1.13 2.45 5.7444.25 2.93 1.06 2.67 7.3948 3.23 1.11 2.62 5.4Ultimate Analyses, % by wt

# EIA Facility Code Facility Name Boiler ID 

# HAPs Test Group



# 10151 American Bituminous Units 1/2

Sample Number 

# Fuel Testing Results

(minimum of 3

composite

samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV)

(as received) HHV Units

# Higher

% Moisture

(as

received) % Ash

(as

received) % Sulfur

(as

received) Heating

Value (HHV)

(Dry Basis) HHV Units % Ash

(Dry Basis) % Sulfur

(Dry Basis)

# Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Antimony

(Dry Basis) Antimony

Units A rsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) Beryllium

Units

# Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese

(Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units

# Note the Proximate/U

Proximate Analyses, % by w

Selenium

(Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Volatiles Ash

# ltimate data below should be recorded on a dry basis (including ash).

wt Ultimate Analyses, % by wt

Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen

# Units of Measure Tables: Please do not modify these tables, except to add your own unit of measu

Fuel Units of Measure - HHV

anthracite Btu/lb

bituminous Btu/gallon

subbituminous

lignite

coal refuse (culm or gob)

No.2 Fuel Oil (distillate)

No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals

synfuel mg/g

petroleum coke μ g/g

othe r mg/Kg

# re to the orange hightlighted cell, if necessary.

Units of Measure - Cl, Fl

%

ppm