Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses 

used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such 

antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is in

be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific bo

number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were bein

Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yello

required fields. Green highlighted cells should be filled using the drop-down boxes, included. Gray fields are aut

filled from other fields.

Please name each resulting spreadsheet with the following naming convention: 

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksh

2. Please enter the test date on the Boiler Information worksheet.

3. Please choose the type of fuel being sampled using the drop-down in the fuel column of the Boiler Informatio

worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column.

4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "A

04".

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If t

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange 

highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksh

6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (orange highlighted cell)

7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a min

composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you ha

more.

8. Provide the results of the analyses for each constituent requested. Use the drop-down boxes to fill in the unit

measure.
Information

ormation about chemical analyses of fuels 

hlorine, fluorine, and metals, such as 

 selenium. This spreadsheet is intended to 

) fuel analyses at that specific boiler. This 

or all 4 HAP surrogates were being tested. 

Fields that are highlighted in yellow are 

xes, included. Gray fields are automatically 

 on the Boiler Information worksheet.

el column of the Boiler Information 

e Other Fuel Description column.

hods worksheet. For example: "ASTM D5865-

cklist worksheet (orange tab). If the units of

ease fill them in the blank, orange 

n the Fuels Sample Results worksheet.

range highlighted cell).

orksheet. You must provide a minimum of 3 

t limited to that number if you have collected 

down boxes to fill in the units of 
EIA Facility Code Facility Name Boiler ID Fuel Type 1

4125 Manitowoc Public Utilities B09 bituminous
Fuel Type 2 Fuel Type 3 Other Fuel Description
EIA Facility Code Facility Name Boiler ID Basis Analyte

4125 Manitowoc Public Utilities B09 As Received Higher Heating Value

4125 Manitowoc Public Utilities B09 As Received % Moisture

4125 Manitowoc Public Utilities B09 As Received % Ash

4125 Manitowoc Public Utilities B09 As Received % Sulfur

4125 Manitowoc Public Utilities B09 Dry basis Higher Heating Value

4125 Manitowoc Public Utilities B09 Dry basis % Ash

4125 Manitowoc Public Utilities B09 Dry basis % Sulfur

4125 Manitowoc Public Utilities B09 Dry basis Antimony

4125 Manitowoc Public Utilities B09 Dry basis Arsenic

4125 Manitowoc Public Utilities B09 Dry basis Beryllium

4125 Manitowoc Public Utilities B09 Dry basis Cadmium

4125 Manitowoc Public Utilities B09 Dry basis Chlorine

4125 Manitowoc Public Utilities B09 Dry basis Chromium

4125 Manitowoc Public Utilities B09 Dry basis Cobalt

4125 Manitowoc Public Utilities B09 Dry basis Fluorine

4125 Manitowoc Public Utilities B09 Dry basis Lead

4125 Manitowoc Public Utilities B09 Dry basis Manganese

4125 Manitowoc Public Utilities B09 Dry basis Mercury

4125 Manitowoc Public Utilities B09 Dry basis Nickel

4125 Manitowoc Public Utilities B09 Dry basis Selenium
Analysis Method for each Analyte 

(example: ASTM D5865-04)

ASTM D5373-02

ASTM D5373-02

ASTM D5373-02

ASTM D5373-02

ASTM D5373-02

ASTM D5373-02

ASTM D5373-02

EPA-SW-846, Method 3030B

EPA-SW-846, Method 3030B

EPA-SW-846, Method 3030B

EPA-SW-846, Method 3030B

USGS Bulletin 1823

EPA-SW-846, Method 3030B

EPA-SW-846, Method 3030B

ASTM 3761-96

EPA-SW-846, Method 3030B

EPA-SW-846, Method 3030B

ASTM 6722

EPA-SW-846, Method 3030B

EPA-SW-846, Method 3030B
EIA Facility Code Facility Name Boiler ID HAPs Test Group

4125 Manitowoc Public Utilities B09 Non-dioxin/furan organic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

% Moisture

(as 

received)

3 4/20/2010 4/20/2010 11930.00 BTU/lb 11.04

4 4/21/2010 4/21/2010 12858.00 Btu/lb 12.07

 Fuel Testing Results


% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

Mercury

(Dry Basis)

2.51 3.71 13409 Btu/lb 2.82 4.17

1.45 4.7 14623 Btu/lb 1.65 5.35


Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

Cadmium 

Units


Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

Selenium 

(Dry Basis)


Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID HAPs Test Group

4125 Manitowoc Public Utilities B09 Dioxin/furan HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

3 4/20/2010 4/20/2010 11930.00 BTU/lb

4 4/21/2010 4/21/2010 12858.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

11.04 2.51 3.71 13409 Btu/lb 2.82 4.17

12.07 1.45 4.7 14623 Btu/lb 1.65 5.35


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units


EIA Facility Code Facility Name Boiler ID HAPs Test Group

4125 Manitowoc Public Utilities B09 Mercury and non-mercury metalic HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher 

Heating 

Value (HHV)

(as 

received) HHV Units

1 5/18/2010 5/18/2010 12181.00 Btu/lb

2 5/19/2010 5/19/2010 12658.00 Btu/lb

3 5/20/2010 5/20/2010 11930.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

10.53 3.51 3.88 13615 Btu/lb 3.92 4.33 290 mg/kg

9.22 1.9 4.4 13943 Btu/lb 2.09 4.84 4080 mg/kg

11.04 2.51 3.71 13409 Btu/lb 2.51 3.71 379 mg/kg


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.017 mg/kg 0 mg/kg 9.45 mg/kg 0.03 mg/kg 0.03

0.01 mg/kg 0 mg/kg 9.14 mg/kg 0.02 mg/kg 0.03


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/kg 0.67 mg/kg 0.68 mg/kg 1.77 mg/kg 154.03 mg/kg

mg/kg 0.73 mg/kg 0.79 mg/kg 2.2 mg/kg 114.15 mg/kg


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

0.18 mg/kg 15 mg/kg 0.63 mg/kg

0.23 mg/kg 24 mg/kg 0.51 mg/kg


EIA Facility Code Facility Name Boiler ID HAPs Test Group

4125 Manitowoc Public Utilities B09 Acid gas HAPs

Sample Number 

(minimum of 3 

composite 

samples)

Test Start Date

(MM/DD/YYYY)

Test Stop Date

(MM/DD/YYYY)

Higher Heating 

Value (HHV)

(as received) HHV Units

2 5/19/2010 5/19/2010 12658.00 Btu/lb

3 5/20/2010 5/20/2010 11930.00 Btu/lb

 Fuel Testing Results


% Moisture

(as 

received)

% Ash

(as 

received)

% Sulfur

(as 

received)

Higher 

Heating 

Value (HHV)

(Dry Basis) HHV Units

% Ash

(Dry Basis)

% Sulfur

(Dry Basis)

Chlorine

(Dry Basis)

Chlorine 

Units

9.22 1.9 4.4 13943 Btu/lb 2.09 4.84 4080 mg/kg

11.04 2.51 3.71 13409 Btu/lb 2.51 3.71 379 mg/kg


Mercury

(Dry Basis)

Mercury

Units

Antimony

(Dry Basis)

Antimony

Units

Arsenic (Dry

Basis)

Arsenic 

Units

Beryllium 

(Dry Basis)

Beryllium 

Units

Cadmium 

(Dry Basis)

0.017 mg/kg 0 mg/kg 9.45 mg/kg 0.03 mg/kg 0.03

0.01 mg/kg 0 mg/kg 9.14 mg/kg 0.02 mg/kg 0.03


Cadmium 

Units

Chromium 

(Dry Basis)

Chromium 

Units

Lead (Dry

Basis) Lead Units

Manganese 

(Dry Basis)

Manganese 

Units

Nickel (Dry

Basis) Nickel Units

mg/kg 0.67 mg/kg 0.68 mg/kg 1.77 mg/kg 154.03 mg/kg

mg/kg 0.73 mg/kg 0.79 mg/kg 2.2 mg/kg 114.15 mg/kg


Selenium 

(Dry Basis)

Selenium 

Units

Fluoride 

(Dry Basis)

Fluoride 

Units

Cobalt (Dry

Basis) Cobalt Units

0.18 mg/kg 15 mg/kg

0.23 mg/kg 24 mg/kg