Based on information and belief formed 

after reasonable inquiry, I certify that the 

statements and information in this test 

report are true, accurate, and complete. 

I 

Permitted Facility Representative I Date 

Name: 

Title: 

Company: 

Sign Date: 

Tuesday, September 07, 2010 

I have reviewed all testing details and 

results in this test report and hereby certify that the test report is authentic 

and accurate. 

q&paS;5,.~~ 

Name: John T. Sutton 

Title: President 

Company: Entec Services, Inc. 

Sign Date: ~ 1 Z..o/10 

Cj /l.o/1 0 

Date 

Page 1 of 37 
Phone: 

Fax: 

Email: 

Phone: (205) 491-6676 

Fax: (205) 491-6614 

Email: jsutton@entecservices.com 

lndustry/SCC/NAIS 327122 AFS#: FRS#: 

Air Permit Number: 

2004-198-TV (M-1) 

Permitted Source 10/Name: 

Dalltalia LLC 

Permitted Maximum Process Rate: Max. Normal Operation Process Rate: Target Process Test Rat 

Attorney Client Priviledge 

SCC I Description 30500850 Industrial Processes - Mineral Products - Ceramic Clay/Tile Manufacture - Firing -

Natural Gas-fired Kiln 

The following state and federal regulations that apply to the proposed testing: 

I 

--

Regulation Description Compound Limit Unit 

Section 114 of the Clean Air Act (CAA) Metals 0 mg/dscm corrected 

Section 114 of the Clean Air Act (CAA) Total Dioxins 0 grainsldscf 

corrected 

Section 114 of the Clean Air Act (CAA) Total Furans 0 grainsldscf 

corrected 

-

Section 114 of the Clean Air Act (CAA) Filterable Particulate 0 mg/dscm corrected 

Section 114 of the Clean Air Act (CAA) 02 0 percent(%) 

Section 114 of the Clean Air Act (CAA) Co2 0 percent(%) Section 114 of the Clean Air Act (CAA) %H20 0 percent(%) 

--

Section 114 of the Clean Air Act (CAA) Total Dioxins 0 ng/dscm corrected 

Section I 14 of the Clean Air Act (CAA) Total Furans 0 mg/dscm corrected 

-

Section 114 of the Clean Air Act (CAA) Total Dioxins 0 mg/dscm 

Section 114 of the Clean Air Act (CAA) Total Furans 0 mg/dscm 

Description of the source (including control equipment). Please see the attachments for source or 

process flow diagram: 

Spray Drying and Prepared Body Storage 

Raw materials were milled to the desired consistency and viscosity creating a mud like slurry called "slip." Upon 

completion of the milling process, the slip was pumped into underground concrete tanks where it was stored before 

spray drying. The slip from underground tanks was pumped under high pressure into spray dryers where it was 

atomized through specially designed nozzles. The nozzles spray the slip upwards while hot air, from natural gasfired burners, flows downward from the top of the spray dryer chamber. During this process, the moisture in the slip 

Tuesday, September 07, 2010 Page 2 of 37 
increase the tile temperature and reduce the moisture content of the pressed tiles to enhance the glazing operation and 

make them suitable for firing in the kilns. Sampling was performed on Vertical Dryer #9 (EPN 32) using Reference 

Test Method 23. 

Glaze Application 

From the vertical dryers, the tiles were conveyed directly to the Glaze Lines for application of various types of 

surface coatings. Each vertical dryer was connected to its own glaze line. In the glazing operations, the tiles passed 

through brush type cabins, spray-nozzle type cabins, and/or various other types of glaze application stations. 

Multiple application stations arranged in series were used to achieve the desired surface effect. For purposes of this 

test, the facility maximized production of products that require spray application of glaze. The spray application 

cabins were connected to one of two baghouses that were designed to capture the dry dust from the brushing as well 

as the airborne glaze particles lfom the wet application processes. Sampling was performed on the dust collector for 

glaze I ines 7-10 (EPN 41 ) using Reference Test Method 2 9. 

Firing 

The dried and glazed tiles were fed into fast-fire roller-hearth kilns. In the kilns, the tile temperature was slowly 

increased to over 2,000 degrees F and then slowly cooled down to less than 150 degrees F at the exit end of the 

kilns. Emissions of gases from the firing zone of the kilns were controlled to two separate caustic wet scrubber 

systems. Under normal operations, Wet Scrubber# 1 controls emission from Kilns I & 2 and Wet Scrubber# 2 

controls emissions from Kilns 3 & 4. Wet Scrubber# 2 was designed to also control emissions from Kilns 2, 3, & 4 

in the event of a malfunction of Wet Scrubber# I. Sampling was performed on Wet Scrubber# 2 (EPN 29) using 

Reference Test Methods 23, 29 and 320. 

Sampling Location Information: 

Round 

Duct Rect.Duct Equiv. Number of 

Traverse Points J Distance from Distance from Location Diam. Length /Width 

Spray Dryer 71 0 0 

Glaze Lines 33 0 0 

Tile Dryer 17 0 0 

Wet Scrubber 72 0 0 

#2 

Test Parameter Information: 

I I Target Location Parameter 

Glaze Lines %H20 Glaze Lines Flowrate Glaze Lines Nickel Glaze Lines rAntimony 

Glaze Lines Arsenic 

Glaze Lines [Beryllium Glaze Lines Cadmium 

Tuesday, September 07, 2010 

Diam upstream dlst. 1 downstream dist. 

0 0 0 0 

Test 

Method 

Method I- 4 

Method I -4 

Method 29 Method 29 

29 

Method 29 Method 29 

400 336 

126 180 144 

I Number of I 

Test Runs 

3 3 

= 

3 3 

-- -

3 

-

3 3 

580 

75 

80 

Test Run 

Duration 

240 240 

--

240 240 240 240 240 

2 20 2 24 

2 8 

2 24 

Sample 

Points Comments 

0 0 I 0 0 0 

-

0 0 

Page 3 of 37 
y 

y

-

%H20 

2,3,7,8-TCDD 

I ,2,3,7,8-PeCDD 

I ,2,3,4, 7 ,8-Hx COD 

I ,2,3,6, 7 ,8-Hx COD 

I ,2,3,7,8,9-HxCDD 

I ,2,3,4,6, 7 ,8-HpCDD 

OCDD 

2,3, 7,8-TCDF 

1,2,3.7,8-PeCDF 

2,3,4, 7 ,8-P eCDF 

1,2,3,4,7,8-HxCDF 

J ,2,3,6,7,8-HxCDF 

2,3,4,6,7,8-HxCDF 

1,2,3,7,8,9-HxCDF 

I ,2,3,4,6, 7,8-HpCDF 

I ,2,3,4,7,8,9-HpCDF 

OCDF 

-

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer ~pray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Spray Dryer 

Tile Dry~ Tile Dryer 

--

Tile Dryer 

Tile Dryer 

Tile Dryer 

Tile Dryer 

Tile Dryer 

Tile Dryer 

Tile Dry'-e_r _ 

Tile Dryer 

Tile Dryer 

Tile Dry.!!: 

Total Dioxins 

Total Furans 

02 

Flowrate 

%H20 

2,3,7,8-TCDD 

1,2,3,7,8-PeCDD 

I ,2,3,4,7,8-HxCDD 

1,2,3,6,7,8-HxCDD 

1,2,3, 7 ,8, 9-Hx COD 

I ,2,3,4,6,7,8-HpCDD 

OCDD 

2,3,7,8-TCDF 

1,2,3,7,8-PeCDF 

2,3,4, 7 ,8-P eCDF 

1,2,3,4, 7,8-HxCDF 

I ,2,3,6,7,8-HxCDF 

Tile Dryer 

_!ile Dryer 

Tile Dryer 

Tile Dryer 

Tile Dryer 

Tile Dryer 

_

2,3,4,6,7,8-HxCDF 

1,2,3,7,8,9-HxCDF 

I ,2,3,4,6, 7 ,8-HpCDF 

-

1,2,3,4, 7 ,8,9-HpCDF 

Tile Dryer OCDF 

Tile D!l:er Total Dioxins 

Tile Dry.!!_ _ 

Tile Dryer 

Total Furans 

02 

Tuesday, September 07, 2010 

Method I- 4 3 240 ! 0 

Method 23 3 240 I 

r 

0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 I 

Method 23 3 240 0 

-

Method 23 3 240 0 

Method 23 

t 

3 240 0 

-

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 I 

Method 23 3 240 0 

Method 23 3 240 

J 

0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 I 

Method 23 3 240 0 

I 

Method3A 02 3 240 0 

Method I- 4 3 240 0 

Method I- 4 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 

I 0 Method 23 3 240 0 

- fMethod 23 3 240 0 

Method 23 3 240 0 

--

Method 23 3 240 o-r 

-

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

Method 23 3 240 0 

- 1-

Method 23 3 240 0 

-

Method 3A 02 3 240 0 

Page4 of37 
#2 

Wet Scrubber 1 ,2,3,6,7,8-HxCDD 

#2 

Wet Scrubber 1 ,2,3,7,8,9-HxCDD 

#2 

Wet Scrubber 1 ,2,3,4,6,7,8-HpCDD 

#2 

Wet Scrubber OCDD 

#2 

Wet Scrubber 2,3,7,8-TCDF 

#2 

Wet Scrubber 1,2,3,7,8-PeCDF 

#2 

Wet Scrubber 2,3,4,7,8-PeCDF 

#2 

Wet Scrubber I ,2,3,4,7,8-HxCDF 

#2 

Wet Scrubber I ,2,3,6,7,8-HxCDF 

#2 

Wet Scrubber 2,3,4,6,7,8-HxCDF 

#2 

!Wet Scrubber 11,2,3,7,8,9-HxCDF 

,#2 I 

!Wet Scrubber 11,2,3,4,6,7,8-HpCDF 

'#2 

Wet Scrubber 11,2,3,4,7,8,9-HpCDF 

#2 I 

Wet Scrubber Dioxins 

#2 

Wet Scrubber jTotal Furans 

#2 I 

Scrubber 

/Wet Scrubber _______ _ 

,#2 I 

Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 Method 23 3 

Method 29 3 Method 29 3 

240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 240 

I_ 0 

0 

0 0 0 0 0 0 0 

0 

0 0 0 

I 0 I o 

I 0 

I 0 I 0 

IWet Arsenic Method 29 I 3 240 l 0 

r: et Scrubber C-o-b-al

_

t _________ ,_M_e-th_o_d_2_9 ____ 1,--3 -- 240 -·--------· 

!#2 

Scrubber 

_

f hromium Method-·29 ____ I 3 _ __1_ ________ , __ 

Scrubber Method 29 I 3 240 I 0 Scrubber Method 29 __! ___ ---· ---240 _ __! ___ ------

Tuesday, September 07, 2010 Page 5 of 37 
I 

#2 

IWet Scrubber r ilterable Particulate Method 5 I 3 240 0 

#2 

The following describes any modifications and/or deviations to the applicable test 

methods. If alternative methods were requested, see the attachments for documentation 

of request AND approval, including dates. 

Tuesday, September 07, 2010 Page 6 of 37 
Run Finish Time 6:26:00 PM 12:07:00 5:01:00 PM 

PM 

Net Run Time, minutes 240 240 240 

Dry Gas Meter Volume Sampled, dscf 177.947 180.417 181.703 180.022 

Moisture Content of Stack Gas, % 2.30 1.93 2.52 2.250 

Moisture Saturation at Stack Gas Temperature, % 2.94 2.80 3.22 2.987 

Carbon Dioxide,% 0.0004 0.0004 0.0004 0.000 

Oxygen,% 20.8 20.8 20.8 20.800 

Average Stack Gas Temperature, °F 75.04 73.92 78.13 75.697 

Dry Volumetric Flow Rate, dry scfin 22,555.8 22,646.1 22,732.8 22,644.900 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 23,504.6 23,180.3 23,586.6 23,423.833 

Percent Isokinetic of Sampling Rate,% 101.3 102.3 102.6 102.067 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 Fe 0 0 0 0.000 

Location Glaze Lines- Method 3A 02 

Avera e 

Run Number I 29 2-29 3-29 

Test Date 5/1312010 511412010 511 4/2010 

Run Start Time 2:36:00 PM 8:17:00 1:11:00 PM 

AM 

Run Finish Time 6:44:00 PM 12:26:00 5:18:00 PM 

PM 

Carbon Dioxide,% 0.1 0.1 0.1 0.100 Oxygen,% 20.8 20.8 20.8 20.800 

Dry Volumetric Flow Rate, dry scfin 22546 22636 22721 22,634.333 

F-Factor, dscfiniMMBtu @ %02 0 0 0 0.000 

Moisture,% 2.3 1.93 2.52 2.250 

Fuel Type Fw 0 0 0 0.000 Fe 0 0 0 0.000 

Tuesday, September 07, 2010 Page 7 of 37 
Dry Gas Meter Volume Sampled, dscf 

Moisture Content of Stack Gas,% 

Moisture Saturation at Stack Gas Temperature, % 

Carbon Dioxide, % 

Oxygen,% 

Average Stack Gas Temperature, °F 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, actin 

Percent lsokinetic of Sampling Rate, % 

F-Factor, dsctin/MMBtu @ %02 

Fw 

Fe 

Location Spray Dryer- Method 23 

Run Number 

Test Date 

Run Start Time 

Run Finish Time 

Net Run Time, minutes 

Dry Gas Meter Volume Sampled, dscf 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature,% 

Carbon Dioxide, % 

Oxygen,% 

Average Stack Gas Temperature, °F 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate. actin 

Percent lsokinetic of Sampling Rate,% 

F-Factor, dscfin/MMBtu @ %02 

Fw 

Fe 

Tuesday, September 07, 2010 

Avera e 

Page 8 of 37 
Carbon Dioxide,% 

Oxygen,% 

Dry Volumetric Flow Rate, dry scfm F-Factor, dscfin!MMBtu@ %02 Moisture,% Fuel Type Fw Fe 

Location Tile Dryer- Method 23 

Run Number 

Test Date 

Run Start Time 

Run Finish Time 

Net Run Time, minutes 

Dry Gas Meter Volume Sampled, dscf 

Moisture Content of Stack Gas,% Moisture Saturation at Stack Gas Temperature, % 

Carbon Dioxide, % 

Oxygen,% 

Average Stack Gas Temperature, "F 

Dry Volumetric Flow Rate, dry scfm 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 

Percent lsokinetic of Sampling Rate, % 

F-Factor, dscfin!MMBtu@ %02 Fw Fe 

Tuesday, September 07, 2010 

2 

18 

49227 

8710 

22.53 

Gas- Natural 

10610 

1040 

PM 

2.5 2 2.167 

18.5 18 18.167 

49672 51396 50,098.333 

8710 8710 8,710.000 

22.75 19.17 21.483 

Gas- Gas- Natural 

Natural 

10610 10610 10,610.000 

1040 1040 1,040.000 

Avera e 

Page 9 of 37 
Carbon Dioxide,% 

Oxygen,% 

Dry Volumetric Flow Rate, dry scfin 

F-Factor, dscfiniMMBtu@ %02 

Moisture,% 

Fuel Type 

Fw 

Fe 

Location Wet Scrubber #2- Method 23 

Run Number 

Test Date 

Run Start Time 

Run Finish Time 

Net Run Time, minutes 

Dry Gas Meter Volume Sampled, dscf 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature, % 

Carbon Dioxide, % 

Oxygen,% 

Average Stack Gas Temperature, °F 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 

Percent lsokinetic of Sampling Rate, % 

F-Factor, dscfiniMMBtu @ %02 

Fw 

Fe 

Tuesday, September 07, 2010 

0.1 

18.9 

3580 

8710 

11.18 

Gas - Natural 

10610 

1040 

PM AM 

0.1 0.1 0.100 

18.8 18.3 18.667 

3516 3559 3,551.667 

8710 8710 8,710.000 

12.79 11.55 11.840 

Gas- Gas - Natural 

Natural 

10610 10610 10,610.000 

1040 1040 1,040.000 

Avera e 

Page 10 of 37 
Dry Gas Meter Volume Sampled, dscf 

Moisture Content of Stack Gas,% 

Moisture Saturation at Stack Gas Temperature,% 

Carbon Dioxide, % 

Oxygen,% 

Average Stack Gas Temperature, °F Method 29 Method 29 Method 29 

Dry Volumetric Flow Rate, dry scfin 0.84 0.84 0.84 0.840 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 0.973 0.973 0.973 0.973 

Percentlsokinetic of Sampling Rate,% 29.79 30.01 30.01 29.937 

F-Factor, dscfin!MMBtu@ %02 148.450 144.974 133.031 142.152 

Fw 141.373 138.518 126.157 135.349 

Fe 81.81 80.88 84.79 82.493 

Location Wet Scrubber #2- Method 3A 02 

Avera e 

Run Number 1-29 2-29 3-29 

Test Date 5fl 3/2010 511412010 5/1512010 

Run Start Time 9:35:00 AM 2:00:00 I 1:43:00 

PM AM 

Run Finish Time 12:05:00 PM 6:14:00 4:33:00 PM 

PM 

Carbon Dioxide,% 2.5 2 1.5 2.000 

Oxygen,% 18.6 19 18.8 18.800 

Dry Volumetric Flow Rate, dry scfin 49845 54349 51296 51,830.000 

F-Factor, dscfiniMMBtu@ %02 8710 8710 8710 8,710.000 

Moisture,% 16.13 16.35 16.57 16.350 

Fuel Type Gas- Natural Gas- Gas - Natural 

Natural 

Fw 10610 10610 10610 10,610.000 

Fe 1040 1040 1040 1,040.000 

Tuesday, September 07, 2010 Page 11 of 37 
PM 

Net Run Time, minutes 156 240 240 

Dry Gas Meter Volume Sampled, dscf 141.373 138.518 126.157 135.349 

Moisture Content of Stack Gas, % 16.13 16.35 16.57 16.350 

Moisture Saturation at Stack Gas Temperature, % 16.35 16.52 16.91 16.593 

Carbon Dioxide,% 2.5 2 1.5 2.000 

Oxygen,% 18.6 19 18.8 18.800 

Average Stack Gas Temperature, °F 132.88 133.54 134.42 133.613 

Dry Volumetric Flow Rate, dry scfin 49,870.7 54,373.1 51,309.8 51,851.200 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 66,992.4 72,777.3 68,960.3 69,576.667 

Percent lsokinetic of Sampling Rate, % 94.9 104.0 100.4 99.767 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Fw 0 0 0 0.000 

Fe 0 0 0 0.000 

Tuesday, September 07, 2010 Page 12 of 37 
mg/dscm 1.72E-04 6.26E-05 5.83E

05 0.000 

m~dscm@7%02 

2.39£-02 8.70E-03 S.IOE-03 0.014 

Compound: Arsenic 

Averal!e 

Run Number M29-1 M29-2 M29-3 

Mass_mg 0.0012 0.0012 0.0012 0.001 

Egfhr 9.13E-03 9.04E-03 9.01E-03 0.009 

mgfdscm 2.38E-04 2.35E-04 2.33E-04 0.000 m~dsc~7~o()2 3.31 E-02 3.27E-02 3.24E-02 0.033 

Compound: Berylliwn 

Averal!e 

Run Number M29-1 M29-2 M29-3 

Mass mg 0.0003 0.0003 0.0003 0.000 

Egfhr 2.28E-03 2.26E-03 2.25E-03 0.002 

mgfdscm 5.95E-05 5.87E-05 5.83E-05 0.000 m~dscm@7 02 8.27E-03 8. 16E-03 8.10E-03 0.008 

Compound: Cadmium 

Averal!e 

Run Number M29-l M29-2 M29-3 

Mass_mg 0.000271 0.000151 0.00015 0.000 

Egfhr 2.06E-03 1.14E-03 1.13E-03 0.001 

mgfdscm 5.38E-05 2.96E-05 2.92E-05 0.000 

mlidscm@7%02 7.48E-03 4.1 IE-03 4.06E-03 0.005 

Compound: Chromium 

Averal!e 

Run Number M29-l M29-2 M29-3 

Mass_mg 0.002393 0.002184 0.001392 0.002 

Eglhr 1.82E-02 1.64E-02 1.04E-02 0.015 

mgldscm 4.75E-04 4.28E-04 2.71E-04 0.000 

m~/dscm@7%02 

6.60E-02 5.95E-02 3.77E-02 0.054 

Compound: Cobalt 

Averal!e 

RunNumbcr M29-l M29-2 M29-3 

Mass_mg 0.0003 0.000464 0.0003 0.000 

Egfhr 2.28E-03 3.49E-03 2.25E-03 0.003 

mg/dscm 5.95£-05 9.08E-05 5.83E-05 0.000 m~d @7%02 8.27E-03 1.26E-02 S.IOE-03 0.010 

Compound: Lead 

Averal!e 

Tuesday, September 07, 2010 Page 13 of 37 
Mass

_mg 0.02202 0.04078 0.00277 0.022 

Eg/hr 1.67E-O 1 3.07E-Ol 2.08E-02 0.165 

mg/dscm 4.37E-03 7.98E-03 5.38E-04 0.004 mg!dscm@7%02 6.07E-01 1.11 E+OO 7.48E-02 0.597 

Compound: Mercury 

Averalle 

Run Number M29-1 M29-2 M29-3 Mass

_mg 0.000432 0.000127 0.000167 0.000 

Eg/hr 3.29E-03 9.56E-04 1.25E-03 0.002 

mg/dscm 8.57E-05 2.49E-05 3.25E-05 0.000 

mg!dscm@7%02 1.19E-02 3.46E-03 4.52E-03 0.007 

Compound: Nickel 

Avera2e 

RunNumber M29-1 M29-2 M29-3 

Mass mg 0.002855 0.007638 0.002378 0.004 

Eg/hr 2.17E-02 5.75E-02 1.79E-02 0.032 

mg/dscm 5.67E-04 l.SOE-03 4.62E-04 0.001 

7.88E-02 2.09E-OI 6.42E-02 0.117 

Compound: Selenium 

Avera2e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.00359 0.003 0.003 0.003 

Eg!hr 2.73E-02 2.26E-02 2.25E-02 0.024 

mg/dscm 7.13E-04 5.87E-04 5.83E-04 0.001 

mg/dscm@7%02 9.91 E-02 8.16E-02 8.10E-02 0.087 

Location: Glaze Lines - Method 5 

Compound: Filterable Particulate 

Averalle 

Run Number M29-l M29-2 M29-3 

Mass

_mg 4.6 3.9 0.9 3.133 

Eg/hr 3.50E+01 2.94E+01 6.76E+OO 23.720 

mg/dscm 9.13E-OI 7.63E-Ol 1.75E-Ol 0.617 

mg/dscm@7%02 1.27E+02 1.06E+02 2.43E+01 85.767 

Location: Spray Dryer - Method 23 

Compound: I ,2,3,4,6,7,8-HpCDD 

Averalle 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.000000285 0.000000261 0.000000299 0.000 

Eg/hr 5.72E-06 5.32E-06 6.43E-06 0.000 

Tuesday, September 07, 2010 Page 14 of 37 
m~dscm@7 02 2.42E-09 1.82E-09 8.96E-10 0.000 

Compound: 1 ,2,3,4,7,8,9-HpCDF 

Averal!e 

Run Number M23-1 M23-2 M23-3 

Mass mg 0.0000000018 0.0000000017 0.00000000 I 0.000 

Eglhr 3.61 E-08 3.46E-08 2.15E-08 0.000 

mg/dscm 4.32E-10 4.10E-10 2.46E-10 0.000 m~ds m@7 02 2.07E-09 2.37E-09 1.18E-09 0.000 

Compound: 1,2,3,4,7,8-HxCDD 

Averal!e 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.0000000089 0.0000000091 0.000000012 0.000 

Eg/hr 1.79E-07 1.85E-07 2.58E-07 0.000 

mg/dscm 2.14E-09 2.20E-09 2.95E-09 0.000 

m~dscm@7%02 1.03E-08 1.27E-08 1.41 E-08 0.000 

Compound: 1,2,3,4,7,8-HxCDF 

Averal!e 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.00000000095 0.00000000088 0.0000000007 0.000 

Eglhr 1.91 E-08 1.79E-08 1.50E-08 0.000 

mg/dscm 2.28E-IO 2.12E-IO 1.72E-JO 0.000 

m~dscm@7%02 1.09E-09 1.23E-09 8.24E-IO 0.000 

Compound: l ,2,3,6,7,8-HxCDD 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.000000015 0.0000000254 0.0000000 13 0.000 

Eglhr 3.01 E-07 5.17E-07 2.79E-07 0.000 

mg/dscm 3.60E-09 6.13E-09 3.20E-09 0.000 m~dscm 7%02 1.73E-08 3.55E-08 1.53E-08 0.000 

Compound: I ,2,3,6,7,8-HxCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass

_mg 0.00000000086 0.00000000079 0. 00000000041 0.000 

Eglhr 1.73E-08 1.6 1 E-08 8.81 E-09 0.000 

mg/dscm 2.06E-10 1.91E-IO J.OIE-10 0.000 

m!ldscm@7%02 9.87E-IO I. II E-09 4.84E-IO 0.000 

Compound: I ,2,3, 7 ,8,9-HxCDD 

Averal!e 

Run Number M23-1 M23-2 M23-3 

Tuesday, September 07, 2010 Page 15 of 37 
Eglhr 2.21 E-08 2.04E-08 1.12E-08 0.000 

mgldscm 2.64E-10 2.4\E-10 1.28E-10 0.000 

m~dscm@7%02 

1.27E-09 1.40E-09 6.14E-10 0.000 

Compound: 1 ,2,3, 7 ,8-PeCDD 

Avera2e 

RunNumber M23-1 M23-2 M23-3 

Mass_mg 0.0000000384 0.0000000529 0.000000037 0.000 

Eglhr 7.7\E-07 1.08E-06 7.95E-07 0.000 

mg/dscm 9.22E-09 1.28E-08 9.\0E-09 0.000 

m~dscm@7%02 

4.42E-08 7.41 E-08 4.36E-08 0.000 

Compound: 1,2,3,7,8-PeCDF 

Avera2e 

RunNumber M23-l M23-2 M23-3 

Mass mg 0.0000000013 0.00000000099 0.00000000056 0.000 

Eglhr 2.61 E-08 2.02E-08 1.20E-08 0.000 

mgldscm 3.12E-IO 2.39E-10 1.38E-1 0 0.000 

m~dscm@7%02 1.50E-09 1.38E-09 6.61 E-10 0.000 

Compound: 2,3,4,6,7,8-HxCDF 

Avera2e 

Run Number M23-1 M23-2 M23-3 

Mass mg 0.00000000092 0.0000000023 0.00000000044 0.000 

Eglhr 1.85E-08 4.69E-08 9.46E-09 0.000 

mg/dscm 2.2\E-10 5.55E-10 1.08E-IO 0.000 

ms/dscm@7%02 1.06E-09 3.21 E-09 5.18E-IO 0.000 

Compound: 2,3,4, 7 ,8-PeCDF 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass

_ mg 0.0000000015 0.00000000094 0.00000000054 0.000 

Eglhr 3.01 E-08 1.91 E-08 1.16E-08 0.000 

mgldscm 3.60E-IO 2.27E-IO 1.33E-10 0.000 

ms/dscm@7%02 1.73E-09 1.31 E-09 6.37E-10 0.000 

Compound: 2,3,7,8-lrCDD 

Averal!e 

RunNumber M23- l M23-2 M23-3 

Mass_mg 0.0000000593 0.0000000729 0.000000051 0.000 

Eg/hr 1.1 9E-06 1.48E-06 I. IOE-06 0.000 

mgldscm 1.42E-08 1.76E-08 1.25E-08 0.000 

mg/dscm@7%02 6.81 E-08 1.02E-07 5.99E-08 0.000 

Tuesday, September 07, 2010 Page 16 of 37 
p

Run Number M23-l M23-2 M23-3 Mass mg 0.00000726 0.00000654 0.00000991 0.000 

Eg/hr 1.46E-04 1.33E-04 2.13E-04 0.000 

mg/dscm 1.74E-06 1.58E-06 2.44E-06 0.000 

mg/dscm@7%02 8.34E-06 9.15E-06 1.17E-05 0.000 

Compound: OCDF 

Run Number M23-l M23-2 M23-3 Mass_mg 0.000000004 0.0000000023 0.0000000026 0.000 

Eg/hr 8.03E-08 4.69E-08 5.59E-08 0.000 

mg/dscm 9.60E-10 S.SSE-10 6.40E-10 0.000 mg/dscm@7%02 4.60E-09 3.21E-09 3.07E-09 0.000 

Compound: Total Dioxins 

Averal!:e 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.0000077435 0.0000070458 0.0000103&73 0.000 

Eg/hr 1.55E-04 1.44E-04 2.23E-04 0.000 

mg/dscm 1.86E-06 1.70E-06 2.56E-06 0.000 mg/dscm@7%02 &.92E-06 9.&5E-06 1.23E-05 0.000 

Compound: Total Fw-ans 

Averal!:e 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.00000001693 0.0000000141 0.00000000893 0.000 

Eg/hr 3.40E-07 2.87E-07 1.92E-07 0.000 

mg/dscm 4.06E-09 3.40E-09 2.20E-09 0.000 

mg/dscm@7%02 1.95E-08 1.97E-08 1.05E-08 0.000 

Location: Tile Dryer - Method 23 

Compound: I ,2,3,4,6, 7 ,8-HpCDD 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.0000001 0.0000000399 0.0000000594 0.000 

Eg/hr 1.43E-07 5.69E-08 8.63E-08 0.000 

mg/dscm 2.35E-08 9.53E-09 1.43E-08 0.000 mg/dscm@7%02 1.63E-07 6.31E-08 7.65E-08 0.000 

Compound: 1,2,3,4,6,7,8-HpCDF 

Run Number M23-1 M23-2 M23-3 

Mass

_mg 0.000000016 0.0000000016 0.0000000012 0.000 

Tuesday, September 07, 2010 Page 17 of 37 
mgldscm 6.11 E-10 2.20E-l0 3.84E-IO 0.000 m~dscm@7 02 4.25E-09 1.46E-09 2.05E-09 0.000 

Compound: 1,2,3,4,7,8-HxCDD 

Averal!e 

RunNumber M23-3 M23-l M23-2 

Mass_mg 0.0000000051 0.00000000556 0.00000000 I 0.000 

Eg/hr 7.41 E-09 7.94E-09 1.43E-09 0.000 

mgldscm 1.22E-09 1.31 E-09 2.39E-10 0.000 m~dscm@7%02 6.52E-09 9.10E-09 1.58E-09 0.000 

Compound: 1,2,3,4,7,8-HxCDF 

Averal!e 

RunNumber M23-3 M23-1 M23-2 

Mass_mg 0.00000000069 0.0000000068 0. 00000000062 0.000 

Eglhr 1.00E-09 9.72E-09 8.84E-10 0.000 

mg/dscm 1.66£-10 1.60£-09 1.48E-10 0.000 

m~dscm@7%02 8.87E-10 1.11 E-08 9.80E-IO 0.000 

Compound: 1,2,3,6,7,8-HxCDD 

Averal!e 

RunNumber M23-1 M23-2 M23-3 

Mass

_rng 0.00000000522 0.000000002 0.000000003 0.000 

Eglhr 7.46£-09 2.85£-09 4.36£-09 0.000 

mg/dscm 1.23E-09 4.78E-10 7.20£-10 0.000 m~dscm@7 02 8.55E-09 3.16E-09 3.85E-09 0.000 

Compound: 1 ,2,3,6, 7 ,8-HxCDF 

Averal!e 

Run Number M23-3 M23-1 M23-2 

Mass

_mg 0.00000000062 0.0000000025 0.00000000056 0.000 

Eglhr 9.01E-10 3.57E-09 7.99E-IO 0.000 

mg/dscm 1.49E-10 5.87E-10 1.34E-IO 0.000 ~dsc @7%02 7.97E-IO 4.08E-09 8.87E-10 0.000 

Compound: 1,2,3,7,8,9-HxCDD 

Averal!e 

Run Number M23-1 M23-2 M23-3 

Mass

_ mg 0.0000000185 0.0000000069 0.000000012 0.000 

Eg/hr 2.64E-08 9.84E-09 1.74E-08 0.000 

mgldscm 4.35E-09 1.65E-09 2.88E-09 0.000 m~dscm@7 02 3.02E-08 1.09£-08 1.54E-08 0.000 

Compound: I ,2,3,7 ,8,9-HxCDF 

Averal!e 

Tuesday, September 07, 2010 Page 18 of 37 
Mass_mg 0.0000000 II 7 0.00000000914 0.0000000211 0.000 

Eg/hr 1.67E-08 1.30E-08 3.06E-O& 0.000 

mg/dscm 2.75E-09 2.18E-09 5.07E-09 0.000 

1.91 E-08 1.44E-08 2.71 E-0& 0.000 

Compound: 1,2,3,7,8-PeCDF 

Averal!e 

RunNumber M23-3 M23-1 M23-2 

Mass

_mg 0.0000000013 0.0000000041 0.00000000074 0.000 

Eg/hr 1.89E-09 5.86E-09 1.06E-09 0.000 

mg/dscm 3.12E-10 9.63E-10 1.77E-l0 0.000 

1.67E-09 6.69E-09 1.17E-09 0.000 

Compound: 2,3,4,6,7,8-HxCDF 

Averal!e 

Run Number M23-3 M23-l M23-2 

Mass

_mg 0. 00000000066 0.00000000082 0. 0000000006 0.000 

Eg/hr 9.59E-1 0 1.17E-09 8.56E-10 0.000 

mg/dscm 1.5&E-IO 1.93E-10 1.43E-IO 0.000 

m£::dscm@7%02 8.45E-IO 1.34E-09 9.47E-10 0.000 

Compound: 2,3,4,7,8-PeCDF 

Averal!e 

RunNumber M23-3 M23-l M23-2 

Mass_mg 0.000000002 0.0000000018 0.00000000\9 0.000 

Eg/hr 2.91 E-09 2.57E-09 2.71 E-09 0.000 

mg/dscm 4.80E-10 4.23E-10 4.54E-IO 0.000 mg/dscm@7%02 2.57E-09 2.94E-09 3.0\E-09 0.000 

Compound: 2,3,7,8-TCDD 

Averal!e 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.000000028 0.000000026 0.0000000699 0.000 

Eg!hr 4.00E-O& 3.71 E-08 1.02E-07 0.000 

mg/dscm 6.58E-09 6.21E-09 1.68E-O& 0.000 

mg/dscm@7%02 4.57E-08 4.11E-08 8.98E-08 0.000 

Compound: 2,3,7,8-TCDF 

Averal!e 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.00000000079 0.00000000083 0.00000000 I 0.000 

Eg/hr 1.13E-09 1.1 &E-09 1.45E-09 0.000 

mg/dscm 1.86E-IO 1.98E-IO 2.40E-10 0.000 mg!dscm@7%02 1.29E-09 1.31 E-09 l.28E-09 0.000 

Tuesday, September 07, 2010 Page 19 of 37 
Co

pou

d: OC

Avera!!e 

Run Number M23-l M23-2 M23-3 Mass_mg 0.0000000416 0.00000000134 0.0000000028 0.000 

Eg/hr 5.94E-08 1.91 E-09 4.07E-09 0.000 

mg/dscm 9.77E-09 3.20E-\O 6.72E-\O 0.000 mg/dscm@7%02 6.79E-08 2.12E-09 3.59E-09 0.000 

Compound: Total Dioxins 

Avera!!e 

Run Number M23-1 M23-2 M23-3 

Mass_mg 0.000001919 0.0000009269 0.00000 l 0695 0.000 

Eg/hr 2.74E-06 1.32E-06 1.55E-06 0.000 

mg/dscm 4.51E-07 2.21 E-07 2.57E-07 0.000 

3.13E-06 1.46E-06 1.37E-06 0.000 

Compound: Total Furans 

Averalle 

Run Number M23-l M23-2 M23-3 Mass

_ mg 0.00000007743 0.0000000098 0.00000001265 0.000 

Eg/hr l.\1 E-07 1.40E-08 1.84E-08 0.000 

mg/dscm 1.82E-08 2.34E-09 3.04E-09 0.000 

mg/dscm@7%02 1.26E-07 1.55E-08 1.63E-08 0.000 

Location: Wet Scrubber #2- Method 23 

Compound: 1 ,2,3,4,6, 7 ,8-HpCDD 

Averalle 

Run Number M23-l M23-2 M23-3 

Mass mg 0.00000415 0.00000336 0.00000587 0.000 

Eg/hr 8.53E-05 6.39E-05 1.11 E-04 0.000 

mg/dscm 9.99E-07 7.34E-07 1.27E-06 0.000 mg/dscm@7%02 6.04E-06 5.37E-06 8.41 E-06 0.000 

Compound: I ,2,3,4,6, 7 ,8-HpCDF 

Avera!!e 

RunNumber M23-l M23-2 M23-3 Mass

_mg 0.0000000057 0.0000000059 0.0000000045 0.000 

Eg/hr l.\7E-07 1.12E-07 8.52E-08 0.000 

mg/dscm 1.37E-09 1.29E-09 9.76E-10 0.000 

8.28E-09 9.44E-09 6.46E-09 0.000 

Compound: I ,2,3,4, 7 ,8,9-HpCDF 

Avera!!e 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.00000000 19 0.000000002 0.00000000066 0.000 

Tuesday, September 07, 2010 Page 20 of 37 
mgfdscm 8.3\E-08 5.92E-08 7.59E-08 0.000 

5.02E-07 4.33E-07 5.02E-07 0.000 

Compound: 1 ,2,3,4, 7 ,8-HxCDF 

Avera2e 

Run Number M23-l M23-2 M23-3 Mass mg 0.0000000027 0.0000000025 0.0000000017 0.000 

Eg/hr 5.55E-08 4.75E-08 3.22E-08 0.000 

mg/dscm 6.50E-10 5.46E-10 3.69E-10 0.000 

rn&ldscm@7%02 3.93E-09 3.99E-09 2.44E-09 0.000 

Compound: 1,2,3,6,7,8-HxCDD 

Averal!e 

Run Number M23-I M23-2 M23-3 

Mass_mg 0.000000414 0.000000377 0.000000473 0.000 

Eg/hr 8.51 E-06 7.17E-06 8.95E-06 0.000 

mg/dscm 9.97E-08 8.23E-08 1.03E-07 0.000 mg/dscm@7%02 6.03E-07 6.02E-07 6.82E-07 0.000 

Compound: I ,2,3,6,7,8-HxCDF 

Avera2e 

Run Number M23-l M23-2 M23-3 

Mass_mg 0. 0000000046 0.0000000055 0.0000000041 0.000 

Eg/hr 9.46E-08 1.05E-07 7.76E-08 0.000 

mg/dscm I. II E-09 1.20E-09 8.89E-10 0.000 

mg/dscm@7%02 6.71 E-09 8.78E-09 5.88E-09 0.000 

Compound: 1 ,2,3,7,8,9-HxCDD 

Avera2e 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.000000908 0.000000834 0.00000105 0.000 

Eg/hr 1.87E-05 1.59E-05 1.99E-05 0.000 

mg/dscm 2.19E-07 1.82E-07 2.28E-07 0.000 

mg/dscm@7%02 1.32E-06 1.33E-06 1.5 I E-06 0.000 

Compound: 1,2,3,7,8,9-HxCDF 

Avera2e 

Run Number M23-1 M23-2 M23-3 

Mass

_ mg 0.00000000 14 0.00000000227 0. 00000000099 0.000 

Eg/hr 2.88E-08 4.31 E-08 1.87E-08 0.000 

mg/dscm 3.37E-10 4.96E-IO 2.15E-IO 0.000 

mg/dscm@7%02 2.04E-09 3.63E-09 1.42E-09 0.000 

Compound: 1,2,3,7,8-PeCDD 

Averal!e 

Tuesday, September 07, 2010 Page 21 of 37 
Mass mg 0.000000004 7 0.00000000752 0.0000000046 0.000 

Eglhr 9.66E-08 1.43E-07 8.71 E-08 0.000 

mgldscm 1.13E-09 1.64E-09 9.97E-IO 0.000 

mgldscm@7%02 6.83E-09 1.20E-08 6.60E-09 0.000 

Compound: 2,3,4,6, 7 ,8-HxCDF 

Averaee 

Run Number M23-l M23-2 M23-3 

Mass

_mg 0.000000002 0.00000000267 0.0000000021 0.000 

Eglhr 4.11 E-08 5.08E-08 3.98E-08 0.000 

mgldscm 4.81E-IO 5.83E-IO 4.55E-IO 0.000 

m!ldscm@7%02 2.91 E-09 4.27E-09 3.01E-09 0.000 

Compound: 2,3,4,7,8-PeCDF 

Avera2e 

Run Number M23-l M23-2 M23-3 

Mass_mg 0.0000000051 0.00000000726 0.00000000842 0.000 

Eg/hr 1.05E-07 1.38E-07 1.59E-07 0.000 

mg/dscm 1.23E-09 1.59E-09 1.83E-09 0.000 

m~dscm@7%02 7.43E-09 1.16E-08 1.21 E-08 0.000 

Compound: 2,3,7,8-TCDD 

Averaee 

RunNumber M23-l M23-2 M23-3 

Mass_mg 0.000000768 0.000000744 0.00000109 0.000 

Eg/hr 1.58E-05 1.41 E-05 2.06E-05 0.000 

mgldscm 1.85E-07 1.62E-07 2.36E-07 0.000 

mgldscm@7%02 1.12E-06 1.19E-06 1.56E-06 0.000 

Compound: 2,3,7,8-TCDF 

Averaee 

Run Number M23-l M23-2 M23-3 

Mass mg 0.0000000138 0.0000000076 0.0000000123 0.000 

Eg/hr 2.84E-07 1.44E-07 2.33E-07 0.000 

mgldscm 3.32E-09 1.66E-09 2.67E-09 0.000 

mg/dscm@7%02 2.01 E-08 1.21 E-08 1.77E-08 0.000 

Compound: OCDD 

Averaee 

Run Number M23-1 M23-2 M23-3 

Mass mg 0.0000393 0.0000324 0.0000434 0.000 

Eg/hr 8.08E-04 6.16E-04 8.22E-04 0.001 

mgldscm 9.46E-06 7.08E-06 9.41E-06 0.000 

mg/dscm@7%02 5.72E-05 5.l8E-05 6.23E-05 0.000 

Tuesday, September 07, 2010 Page 22 of 37 
p

Run Number M23-1 M23-2 M23-3 

Mass

_mg 0.00004659 0.000038766 0.000053174 0.000 

Eg/hr 9.58E-04 7.37E-04 1.01E-03 0.001 

mg/dscm 1.12E-05 8.47E-06 1.15E-05 0.000 mg/dscm@7%02 6.77E-05 6.20E-05 7.61E-05 0.000 

Compound: Total Furans 

Run Number M23-1 M23-2 M23-3 Mass

_mg 0.0000000497 0.00000004702 0.0000000454 7 0.000 

Eg/hr 1.02E-06 8.94E-07 8.61 E-07 0.000 

mg/dscm 1.20E-08 1.D3E-08 9.86E-09 0.000 mg/dscm@7%02 7.25E-08 7.54E-08 6.53E-08 0.000 

Location: Wet Scrubber #2- Method 29 

Compound: Antimony 

Avera2e 

Run Number M29-1 M29-2 M29-3 Mass

_mg 0.00128 0.00147 0.00129 0.001 

Eg/hr 2.71 E-02 3.46E-02 3.15E-02 0.031 

mg/dscm 3.20E-04 3.75E-04 3.61E-04 0.000 mg/dscm@7%02 1.93E-03 2.74E-03 2.39E-03 0.002 

Compound: Arsenic 

Averal!e 

RunNumber M29-\ M29-2 M29-3 

Mass_mg 0.0116 0.00997 0.00947 0.010 Eg/hr 2.46E-01 2.35E-01 2.31 E-01 0.237 

mg/dscm 2.90E-03 2.54E-03 2.65E-03 0.003 

m£::dscm@7%02 1.75E-02 1.86E-02 1.75E-02 0.018 

Compound: Beryllium 

Averal!e 

RunNumber M29-1 M29-2 M29-3 

Mass_mg 0.0003 0.0003 0.0003 0.000 Eg/hr 6.35E-03 7.07E-03 7.32E-03 0.007 

mgldscm 7.50E-05 7.65E-05 8.40E-05 0.000 mg/dscm@7%02 4.53E-04 5.60E-04 5.56E-04 0.001 

Compound: Cadmium 

Averal!e 

Run Number M29-1 M29-2 M29-3 Mass mg 0.00134 0.00119 0.00138 0.001 

Tuesday, September 07, 2010 Page 23 of 37 
mg/dscm 4.32E-02 4.56E-02 5.91E-02 0.049 

2.61 E-01 3.34E-OI 3.91E-Ol 0.329 

Compound: Cobalt 

Averal!e 

Run Number M29-l M29-2 M29-3 Mass

_mg 0.000479 0.000553 0.001047 0.001 

Eg/hr 1.01 E-02 1.30E-02 2.55E-02 0.016 

mg/dscm 1.20E-04 1.41 E-04 2.93E-04 0.000 

7.25E-04 l.OJE-03 1.94E-03 0.001 

Compound: Lead 

Averal!e 

Run Number M29-l M29-2 M29-3 Mass_mg 0.13 0.115 0.0844 0.110 Eg/hr 2.75E+OO 2.71 E+OO 2.06E+OO 2.507 

mg/dscm 3.25E-02 2.93E-02 2.36E-02 0.028 

mg/dscm@7%02 1.96E-OI 2.14E-01 I. 56 E-O 1 0.189 

Compound: Manganese 

Averal!e 

Run Number M29-l M29-2 M29-3 

Mass

_mg 0.0163 0.0359 0.128 0.060 

Eg/hr 3.45E-OI 8.46E-Ol 3.12E+OO 1.437 

mg/dscm 4.07E-03 9.15E-03 3.58E-02 0.016 

mg/dscm@7%02 2.46E-02 6.69E-02 2.37E-Ol 0.110 

Compound: Mercury 

Averal!e 

RunNumber M29-l M29-2 M29-3 

Mass

_mg 0.0625 0.061 [ 0.0443 0.056 

Eg/hr l.32E+OO 1.44E+OO 1.08E+OO 1.280 

mg/dscm 1.56E-02 1.56E-02 1.24E-02 0.015 

mg/dscm@7%02 9.43E-02 l.14E-Ol 8.21 E-02 0.097 

Compound: Nickel 

Averal!e 

Run Number M29-l M29-2 M29-3 

Mass

_mg 0.00351 0.00265 0.00337 0.003 

Eg/hr 7.43E-02 6.24E-02 8.22E-02 0.073 

mg/dscm 8.77E-04 6.76E-04 9.43E-04 0.001 mgldscm@7%02 5.30E-03 4.95E-OJ 6.24E-03 0.005 

Compound: Selenium 

Avera!!e 

Tuesday, September 07, 2010 Page 24of37 
Avera2e 

Run Number M29-l M29-2 M29-3 

Mass

_mg 84.1 73.5 75.6 77.733 

Eg/hr 1.78E+03 1.73E+03 1.84E+03 1,783.333 

mg/dscm 2.10E+Ol 1.87E+Ol 2. 12E+Ol 20.300 m~d cm ?%02 1.27E+02 1.37E+02 1.40E+02 134.667 

Tuesday, September 07, 2010 Page 25of 37 
Run Name 

Spray Dryer Fabric Filter Due>t Collector 

Glaze Lines Dust Collector 

Tile Dryer (Vertical No Control 

Wet Scrubber #2 (Kilns 2, 3 & 4) 

Process Lab Run Data 

Run Name 

None 

Tuesday, September 07, 2010 

Value 

0 0 

0 0 

UOM 

Value UOM 

0 

a

get 

Value 

0 0 0 0 

Comments 

Comments 

Page 26 of 37 
Net Traversing Points 24 24 24 

Net Run Time, minutes 240 240 240 

Nozzle Diameter, inches 0.188 0.188 0.188 0.188 

Pi tot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 1.017 1.017 1.017 1.017 Barometric Pressure, inches of Mercury 29.79 30.16 30.16 30.037 

Average Orifice Meter Differential, inches H20 1.77 1.75 1.79 1.770 

Dry Gas Meter Volume Sampled, cubic teet 176.642 176.762 180.234 177.879 

Average Dry Gas Meter Temperature, "F 73.04 72.58 79.25 74.957 

Dry Gas Meter Volume Sampled, dscf 177.947 180.417 181.703 180.022 

Total Moisture Liquid collected, g 88.8 75.4 99.8 88.000 

Volume of Water Vapor, standard cubic feet 4.18 3.55 4.70 4.143 

Moisture Content of Stack Gas, % 2.30 1.93 2.52 2.250 

Moisture Saturation at Stack Gas Temperature, % 2.94 2.80 3.22 2.987 

Dry Mole Fraction 0.977 0.9807 0.9748 0.978 

Carbon Dioxide,% 0.0004 0.0004 0.0004 0.000 

Oxygen,% 20.8 20.8 20.8 20.800 

Carbon Monoxide & Nitrogen, % 79.1996 79.1996 79.1996 79.200 

Fuel Factor 250.00 250.00 250.00 

Dry Molecular Weight, lb!lb-Mole 28.83 28.83 28.83 28.830 Wet Molecular weight, lb/lb-Mole 28.58 28.62 28.56 28.587 

Flue Gas Static Pressure, inches of H20 -0.15 -0.25 -0.12 -0.173 

Absolute Flue Gas Pressure, inches of Mercury 29.78 30.14 30.15 30.023 

Average Stack Gas Temperature, °F 75.04 73.92 78.13 75.697 

Average Velocity Head, inches of H20 1.3417081248 1.325476742 1.358854617 1.342 

9698 69772 34006 

Average Stack Gas Velocity, feet/second 65.95 65.04 66.18 65.723 

Stack Cross-Sectional Area, square feet 5.940 5.940 5.940 5.940 

Dry Volumetric Flow Rate, dry scfin 22,555.8 22,646.1 22,732.8 22,644.900 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 23,504.6 23,180.3 23,586.6 23,423.833 

Percent lsokinetic of Sampling Rate, % 101.3 102.3 102.6 102.067 

Percent Excess Air, % 19,136.2 19,136.2 19,136.2 19,136.200 

F-Factor, dscfiniMMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 33 33 33 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 Fw 0 0 0 0.000 Fe 0 0 0 0.000 

Tuesday, September 07, 2010 Page 27 of 37 
Fuel Factor l 

Dry Volumetric Flow Rate, dry scfin 22546 22636 22721 22,634.333 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Moisture,% 2.3 1.93 2.52 2.250 

Analyzer Make Analyzer Model Analyzer Serial Number 

Operating Range 25 25 25 25.000 

Operating Units % % % 

No. Readings/Avg. 0 0 0 0.000 

Calibration Set I 1.000 

Calibration Pre Zero Cylinder ID Nitrogen l Nitrogen I Nitrogen I 

Calibration Pre Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Pre Zero Cylinder Bias 0 0 0 0.000 

Calibration Pre Zero Cylinder Drift 0 0 0 0.000 

Calibration Pre High Cylinder ID ambient air ambient air ambient air 

Calibration Pre High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Pre High Cylinder Bias -0.4 -0.4 -0.4 -0.400 

Calibration Pre High Cylinder Drift 0 0 0 0.000 

Calibration Post Zero Cylinder lD Nitrogen 1 Nitrogen I Nitrogen I 

Calibration Post Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Post Zero Cylinder Bias 0 0 0 0.000 

Calibration Post Zero Cylinder Drift 0 0 0 0.000 

Calibration Post High Cylinder lD ambient air ambient air ambient air 

Calibration Post High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Post High Cylinder Bias -0.4 -0.4 -0.4 -0.400 

Calibration Post High Cylinder Drift 0.4 0 0 0.133 Cavg 20.8 20.8 20.8 20.800 Cavg Units %vd %vd %vd 

Cgas 20.9 20.9 20.9 20.900 

Cgas Units %vd %vd %vd 

Fuel Type 

Fw 0 0 0 0.000 Fe 0 0 0 0.000 

Cgasw 0 0 0 0.000 

Cgasw Units 

Tuesday, September 07, 2010 Page 28 of 37 
Nozzle Diameter, inches 

Pitot Tube Coefficient 

Dry Gas Meter Calibration Factor 

Barometric Pressure, inches ofMercury 

Average Orifice Meter Differential, inches H20 

Dry Gas Meter Volume Sampled, cubic feet 

Average Dry Gas Meter Temperature, °F 

Dry Gas Meter Volume Sampled, dscf 

Total Moisture Liquid collected, g 

Volume of Water Vapor, standard cubic feet 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction 

Carbon Dioxide,% 

Oxygen,% Carbon Monoxide & Nitrogen, % 

Fuel Factor 

Dry Molecular Weight, lb/lb-Mole 

Wet Molecular weight, lb/lb-Mole 

Flue Gas Static Pressure, inches of H20 

Absolute Flue Gas Pressure, inches of Mercury 

Average Stack Gas Temperature, °F Average Velocity Head, inches of H20 

Average Stack Gas Velocity, feet/second 

Stack Cross-Sectional Area, square feet 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, actin 

Percent lsokinetic of Sampling Rate, % 

Percent Excess Air,% 

F-Factor, dscfin/MMBtu@ %02 Round Duct Diameter, inches Rectangular Duct Width, inches 

Rectangular Duct Length, inches Fw Fe 

Tuesday, September 07, 2010 

Page 29 of 37 
Nozzle Diameter, inches 

Pitot Tube Coefficient 

Dry Gas Meter Calibration Factor 

Barometric Pressure, inches of Mercury 

Average Orifice Meter Differential, inches H20 

Dry Gas Meter Volume Sampled, cubic feet 

Average Dry Gas Meter Temperature, eF 

Dry Gas Meter Volume Sampled, dscf 

Total Moisture Liquid collected, g 

Volume of Water Vapor, standard cubic feet 

Moisture Content of Stack Gas,% 

Moisture Saturation at Stack Gas Temperature,% Dry Mole Fraction 

Carbon Dioxide, % 

Oxygen,% Carbon Monoxide & Nitrogen, % 

Fuel Factor Dry Molecular Weight, lb/lb-Mole 

Wet Molecular weight, lb/lb-Mole 

Flue Gas Static Pressure, inches of H20 

Absolute Flue Gas Pressure, inches of Mercury 

Average Stack Gas Temperature, °F 

Average Velocity Head, inches of H20 

Average Stack Gas Velocity, feet/second 

Stack Cross-Sectional Area, square feet 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 

Percent lsokinetic of Sampling Rate,% 

Percent Excess Air, % F-Factor, dscfiniMMBtu@ %02 Round Duct Diameter, inches Rectangular Duct Width, inches 

Rectangular Duct Length, inches Fw Fe 

Tuesday, September 07, 2010 

Page 30 of 37 
Oxygen,% 18 18.5 18 18.167 

Fuel Factor 1.45 0.96 1.45 

Dry Volumetric Flow Rate, dry scfin 49227 49672 51396 50,098.333 

F-Factor, dscfin!MMBtu@ %02 8710 8710 8710 8,710.000 

Moisture,% 22.53 22.75 19.17 21.483 

Analyzer Make Analyzer Model Analyzer Serial Number 

Operating Range 25 25 25 25.000 

Operating Units % % % 

No. Readings/ A vg. 0 0 0 0.000 

Calibration Set 1.000 

Calibration Pre Zero Cylinder ID Nitrogen I Nitrogen I Nitrogen I 

Calibration Pre Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Pre Zero Cylinder Bias 0 0 0 0.000 Calibration Pre Zero Cylinder Drift 0 0 0 0.000 Calibration Pre High Cylinder ID ambient air ambient air ambient air 

Calibration Pre High Cylinder Instrument Response 20.8 20.8 20.8 20.800 Calibration Pre High Cylinder Bias -0.4 -0.4 -0.4 -0.400 

Calibration Pre High Cylinder Drift 0 0 0 0.000 

Calibration Post Zero Cylinder ID Nitrogen I Nitrogen 1 Nitrogen 1 

Calibration Post Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Post Zero Cylinder Bias 0 0 0 0.000 Calibration Post Zero Cylinder Drift 0 0 0 0.000 Calibration Post High Cylinder ID ambient air ambient air ambient air 

Calibration Post High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Post High Cylinder Bias -0.4 -0.4 -0.4 -0.400 

Calibration Post High Cylinder Drift 0 0 0 0.000 

Cavg 18 18.5 18 18.167 

Cavg Units %vd %vd %vd Cgas 18.0865 18.5889 18.0865 18.254 

Cgas Units %vd %vd %vd 

Fuel Type Gas - Natural Gas - Natural Gas- Natural 

Fw 10610 10610 10610 10,610.000 Fe 1040 1040 1040 1,040.000 

Cgusw 0 0 0 0.000 Cgasw Units 

Tuesday, September 07, 2010 Page 31 of 37 
Nozzle Diameter, inches 

Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, in(;hes of Mercury 

Average Orifice Meter Differential, inches H20 

Dry Gas Meter Volume Sampled, cubic feet 

Average Dry Gas Meter Temperature, 

Dry Gas Meter Volume Sampled, dscf 

Total Moisture Liquid collected, g 

Volume of Water Vapor, standard cubic feet 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature, % 

Dry Mole Fraction 

Carbon Dioxide, % 

Oxygen,% Carbon Monoxide & Nitrogen, % 

Fuel Factor Dry Molecular Weight, lbJib-Mole 

Wet Molecular weight, lb/lb-Mole 

Flue Gas Static Pressure, inches of H20 

Absolute Flue Gas Pressure, inches of Mercury 

Average Stack Gas Temperature, °F 

Average Velocity Head, inches of H20 

Average Stack Gas Velocity, feet/second 

Stack Cross-Sectional Area, square feet 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 

Percent lsokinetic of Sampling Rate, % 

Percent Excess Air, % F-Factor, dscfiniMMBtu@ %02 

Round Duct Diameter, inches Rectangular Duct Width, inches 

Rectangular Duct Length, inches Fw Fe 

Tuesday, September 07, 2010 

Page 32 of37 
Fuel Factor 20 21 26 

Dry Volumetric Flow Rate, dry scfin 3580 3516 3559 3,551.667 

F-Factor, dscfin/MMBtu@ %02 8710 8710 8710 8,710.000 

Moisture, % 11.18 12.79 11 .55 11 .840 

Analyzer Make 

Analyzer Model 

Analyzer Serial Number 

Operating Range 25 25 25 25.000 

Operating Units % % % 

No. Readings!Avg. 0 0 0 0.000 

Calibration Set 1.000 

Calibration Pre Zero Cylinder ID Nitrogen I Nitrogen I Nitrogen l 

Calibration Pre Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Pre Zero Cylinder Bias 0 0 0 0.000 

Calibration Pre Zero Cylinder Drift 0 0 0 0.000 

Calibration Pre High Cylinder ID ambient air ambient air ambient air 

Calibration Pre High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Pre High Cylinder Bias -0.4 -0.4 -0.4 -0.400 

Calibration Pre High Cylinder Drift 0 0 0 0.000 

Calibration Post Zero Cylinder ID Nitrogen I Nitrogen I Nitrogen I 

Calibration Post Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Post Zero Cylinder Bias 0 0 0 0.000 

Calibration Post Zero Cylinder Drift 0 0 0 0.000 

Calibration Post High Cylinder ID ambient air ambient air ambient air 

Calibration Post High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Post High Cylinder Bias -0.4 -0.4 -0.4 -D.400 

Calibration Post High Cylinder Drift 0 0 0 0.000 

Cavg 18.9 18.8 18.3 18.667 

Cavg Units %vd %vd %vd 

Cgas 18.9909 18.8904 18.388 18.756 

Cgas Units %vd %vd %vd 

Fuel Type Gas- Natural Gas - Natural Gas - Natural 

Fw 10610 10610 10610 10,610.000 

Fe 1040 1040 1040 1,040.000 

Cgasw 0 0 0 0.000 

Cgasw Units 

Tuesday, September 07, 2010 Page 33 of 37 
Nozzle Diameter, inches 

Pitot Tube Coefficient 

Dry Gas Meter Calibration Factor 

Barometric Pressure, inches of Mercury 

Average Orifice Meter Differential, inches H20 

Dry Gas Meter Volume Sampled, cubic feet 

Average Dry Gas Meter Temperature, °F 

Dry Gas Meter Volume Sampled, dscf 

Total Moisture Liquid collected, g 

Volume of Water Vapor, standard cubic feet 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature, % 

Dry Mole Fraction 

Carbon Dioxide,% 

Oxygen,% 

Carbon Monoxide & Nitrogen,% 

Fuel Factor 

Dry Molecular Weight, Jb/lb-Mole 

Wet Molecular weight, lb/lb-Mole 

Flue Gas Static Pressure, inches of H20 

Absolute Flue Gas Pressure, inches of Mercury 

Average Stack Gas Temperature, °F 

Average Velocity Head, inches of H20 

Average Stack Gas Velocity, feet/second 

Stack Cross-Sectional Area, square feet 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 

Percentlsokinetic of Sampling Rate, % 

Percent Excess Air, % 

F-Factor, dscfiniMMBtu@ %02 

Round Duct Diameter, inches 

Rectangular Duct Width, inches 

Rectangular Duct Length, inches 

Fw 

Fe 

Tuesday, September 07, 2010 

Page 34of37 
Nozzle Diameter, inches 

Pitot Tube Coefficient 

Dry Gas Meter Calibration Factor 

Barometric Pressure, inches of Mercury 

Average Orifice Meter Differential, inches H20 

Dry Gas Meter Volume Sampled, cubic feet 

Average Dry Gas Meter Temperature, "F 

Dry Gas Meter Volume Sampled, dscf 

Total Moisture Liquid collected, g 

Volume of Water Vapor, standard cubic feet 

Moisture Content of Stack Gas, % 

Moisture Saturation at Stack Gas Temperature, % 

Dry Mole Fraction 

Carbon Dioxide, % 

Oxygen,% Carbon Monoxide & Nitrogen,% 

Fuel Factor Dry Molecular Weight, lb/lb-Mole 

Wet Molecular weight, lb/lb-Mole 

Flue Gas Static Pressure, inches of H20 

Absolute Flue Gas Pressure, inches of Mercury 

Average Stack Gas Temperature, oF 

Average Velocity Head, inches of H20 

Average Stack Gas Velocity, feet/second 

Stack Cross-Sectional Area, square feet 

Dry Volumetric Flow Rate, dry scfin 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 

Percent Isokinetic of Sampling Rate,% 

Percent Excess Air, % F-Factor, dscfin/MMBtu@ %02 Round Duct Diameter, inches Rectangular Duct Width, inches 

Rectangular Duct Length, inches Fw Fe 

Tuesday, September 07, 2010 

Wet Scrubber 

#2 

5/13/2010 

Method 29 

M29-l 

9:35:00 AM 

0.315 

0.84 

0.973 

29.79 

3.54 

148.450 

12:05:00 PM 

16 

156 

141.373 

81.81 

Wet 

Scrubber#2 

5/14/2010 

Method 29 

M29-2 

2:00:00 PM 

0.23 0.84 

0.973 

30.01 

1.19 

144.974 

5:50:00 PM 

24 

240 

138.518 

80.88 

Wet 

Scrubber#2 

5/15/2010 

Method 29 

M29-3 

11:43:00 AM 

0.23 0.84 

0.973 

30.01 

1.07 

133.031 

3:33:00 PM 

24 

240 

126.157 

84.79 

0.258 0.840 0.973 

29.937 

1.933 

142.152 135.349 

82.493 

Page 35 of 37 
Fuel Factor 0.92 0.95 1.4 

Dry Volumetric Flow Rate, dry scfin 49845 54349 51296 51,830.000 

F-Factor, dscfin!MMBtu@ %02 8710 8710 8710 8,710.000 

Moisture,% 16.13 16.35 16.57 16.350 

Analyzer Make 

Analyzer Model 

Analyzer Serial Number 

Operating Range 25 0 0 8.333 

Operating Units % 

No. Readings/Avg. 0 0 0 0.000 

Calibration Set 1.000 

Calibration Pre Zero Cylinder ID Nitrogen I Nitrogen I Nitrogen 1 

Calibration Pre Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Pre Zero Cylinder Bias 0 0 0 0.000 

Calibration Pre Zero Cylinder Drift 0 0 0 0.000 

Calibration Pre High Cylinder ID ambient air ambient air ambient air 

Calibration Pre High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Pre High Cylinder Bias -0.4 -0.4 -0.4 -0.400 

Calibration Pre High Cylinder Drift 0 0 0 0.000 

Calibration Post Zero Cylinder ID Nitrogen I Nitrogen 1 Nitrogen 1 

Calibration Post Zero Cylinder Instrument Response 0 0 0 0.000 

Calibration Post Zero Cylinder Bias 0 0 0 0.000 

Calibration Post Zero Cylinder Drift 0 0 0 0.000 

Calibration Post High Cylinder ID ambient air ambient air ambient air 

Calibration Post High Cylinder Instrument Response 20.8 20.8 20.8 20.800 

Calibration Post High Cylinder Bias -0.4 -0.4 -0.4 -D.400 

Calibration Post High Cylinder Drift 0 0 0 0.000 

Cavg 18.6 19 18.8 18.800 

Cavg Units %vd %vd %vd 

Cgas 18.6894 19.0913 18.8904 18.890 

Cgas Units %vd %vd %vd 

Fuel Type Gas - Natural Gas - Natural Gas- Natural 

Fw 10610 10610 10610 10,610.000 

Fe 1040 1040 1040 1,040.000 

Cgasw 0 0 0 0.000 

Cgasw Units 

Tuesday, September 07, 2010 Page 36 of 37 
Nozzle Diameter, inches 0.315 0.23 0.23 0.258 

Pitot Tube Coefficient 0.84 0.84 0.84 0.840 

Dry Gas Meter Calibration Factor 0.973 0.973 0.973 0.973 Barometric Pressure, inches of Mercury 29.79 30.01 30.01 29.937 

Average Orifice Meter Differential, inches H20 3.54 1.19 1.07 1.933 

Dry Gas Meter Volume Sampled, cubic teet 148.450 144.974 133.031 142.152 

Average Dry Gas Meter Temperature, °F 81.81 80.88 84.79 82.493 

Dry Gas Meter Volume Sampled, dscf 141.373 138.518 126.157 135.349 

Total Moisture Liquid collected, g 577.4 575 532.2 561.533 

Volume of Water Vapor, standard cubic feet 27.18 27.07 25.05 26.433 

Moisture Content of Stack Gas, % 16.13 16.35 16.57 16.350 

Moisture Saturation at Stack Gas Temperature,% 16.35 16.52 16.91 16.593 

Dry Mole Fraction 0.8387 0.8365 0.8343 0.837 

Carbon Dioxide, % 2.5 2 1.5 2.000 

Oxygen,% 18.6 19 18.8 18.800 

Carbon Monoxide & Nitrogen, % 78.9 79 79.7 79.200 

Fuel Factor 0.92 0.95 1.40 Dry Molecular Weight, lb/lb-Mole 29.14 29.08 28.99 29.070 

Wet Molecular weight, lb/lb-Mole 27.34 27.27 27.17 27.260 

Flue Gas Static Pressure, inches of H20 0.37 0.45 0.45 0.423 Absolute Flue Gas Pressure, inches of Mercury 29.82 30.04 30.04 29.967 

Average Stack Gas Temperature, °F 132.88 133.54 134.42 133.613 

Average Velocity Head, inches of H20 0.41586036 72 0.492525984 0.440052402 0.449 

80145 662171 483229 

Average Stack Gas Velocity, feet/second 39.49 42.90 40.65 41.013 

Stack Cross-Sectional Area, square teet 28.274 28.274 28.274 28.274 

Dry Volumetric Flow Rate, dry scfi11 49,870.7 54,373.1 51,309.8 51,851.200 

Actual Wet Volumetric Flue Gas Flow Rate, acfin 66,992.4 72,777.3 68,960.3 69,576.667 

Percent lsokinetic of Sampling Rate, % 94.9 104.0 100.4 99.767 

Percent Excess Air, % 834.2 1,023.7 839.0 898.967 

F-Factor, dscfin/MMBtu@ %02 0 0 0 0.000 

Round Duct Diameter, inches 72 72 72 

Rectangular Duct Width, inches 0 0 0 

Rectangular Duct Length, inches 0 0 0 Fw 0 0 0 0.000 Fe 0 0 0 0.000 

Tuesday, September 07, 2010 Page 37 of 37 
SOURCE(S) NAME(S): SOURCE(S) CONDITION: SOURCE(S) SHAPE: 

TEST PERFORMED: 

REFERENCE METHOD TESTS: ENTEC PROJECT MANAGER (PM) 

Wet Scrubber 2 

Normal Conditions-Tile MACT 

Circular 

Flow and FTIR 

Sample Test Points at Location 

Volumetric Flow and Gas Velocity 

Molecular Weight Moisture Content 

Hydrogen Chloride Hydrogen Fluoride 

Lynn Beane 

ENVIRONMENTAL ANALYST (Team Leader) Erik Groth ENVIRONMENTAL ANALYST (Assistants) John Drienzo 

OWNER'S REPRESENTATIVE(s): Mr. Bob Hurt and Mr. Steve Willis 

ENTEC PROJECT NUMBER: 210155 

DATES TESTS CONDUCTED: Trav/Prep 

05/13/10 

Thursday 

Run 1 

05/14/10 

Friday 

Run2 

05/14/10 

Friday 

EPA Method EPA Method EPA Method EPA Method EPA Method EPA Method 

Run 3 

05/14/10 

Friday 

1 

2 

3/3A 

4 

320 

320 
Source(s) Tested: 

Test Condition: Test(s) Performed: 

Run Number 

Date of Run 

Times, Pollutant Runs (Began- Ended) Times, Flow Runs (Began- Ended) 

Oxygen Cone., 

Carbon Dioxide Cone. 

Molecular Weight Of Stack Gas 

Molecular Weight Of Stack Gas 

Hydrogen Chloride Hydrogen Fluoride 

Stack Temperature 

Moisture Content 

Average Stack Gas Velocity 

Stack Gas Flow @ Actual Conditions 

Stack Gas Flow @ STP 

Stack Gas Flow @ Dry Standard Conditions 

Hydrogen C hlorlde Cone. @ STP 

Hydrogen Fluoride Cone. @ STP 

Hydrogen Chloride Cone @ 7% 02 Hydrogen Fluoride Cone @ 7% 02 Hydrogen Chloride Mass Emissions 

Fluoride Mass Emissions 

Wet Scrubber 2 

Normal Conditions-Tile MACT 

Flows, Moistures, HCI and HF 

2 

5/14/10 5/14/10 

1403-1504 1527-1630 1403-1504 1527-1630 

%(dry basis) 19.0 19.0 % (dry basis) 2.0 2.0 % (dry basis) 29.08 29.08 

% (wet basis) 27.27 27.27 

ppm, v/ v, d 9.40 15.10 ppm, v/ v, d 10.66 12.62 

oc 56.4 56.4 

%, vlv 16.13 16.35 

m/s 13.07 13.07 

acmm 2,061 2,061 

scmm 1,840 1,840 

dscmm 1,539 1,539 

mg /dscm 14.22 22.84 mg /dscm 8.85 10.47 

mg/dscm. 85.92 167.10 mg/dscm. 53.49 76.62 

kg I hr 1.313 2.109 

kg/ hr 0.817 0.967 

••Flow testing was performed for this source in conjunction with the Method 29 Testing, Run 2. 

[NOTE - Run 4 Flow was completed as a Post-ICR flow run to bracket the 3 ICR runs.] 

Project Manager: 

Lynn Beane 

3 4 Average 

5/14/10 5/14/10 3Runs 

1655-1758 1655-1758 1800-1814 

19.0 19.0 19.0 

2.0 2.0 2.0 

29.08 29.08 29.07 

27.27 27.27 27.26 

5.96 10.16 

6.77 10.02 

56.4 56.4 56.4 

16.57 16.35 16.35 

13.07 13.07 13.07 

2,061 2,061 2061 

1,840 1,840 1840 1,539 1,539 1539 

9.02 15.36 

5.62 8.32 

59.71 104.24 

37.21 55.77 

0.833 1.418 0.519 0.768 
Source: Wet Scrubber 2 Input By: Erik Groth 

Type of Traverse: Velocity (V) or Particulate (P): 

Stack Diameter, Inches: 72 

Stack Height, feet: 50.0 

Stack Properties: Inches 

'After' Flow Disturbance, Distance (A): 80.0 

'Before' Flow Disturbance, Distance (B): 144.0 

72.0 INCHES 

80.0 INCHES 

0 

144.0 INCHES 

y Port Type Nipple Port Diameter 4 

Stack Area, Ft2: 28.274 

Number of Ports: 2 

Length of Port, inches: 15.00 

1.11 Total Number of Traverse Points: 16 

2.00 Number of Points per port I traverse: 8 

Inside Stack Outside Nipple 

Point No. Inches Inches 

2.3 17.3 

2 7.6 22.6 

3 14.0 29.0 

4 23.3 38.3 

5 48.7 63.7 

6 58.0 73.0 

7 64.4 79.4 

8 69.7 84.7 

• Adjusted points diameter> 24" no point closer than 1.0 Inch 

• Adjusted points 24M no point closer than 0.5 Inch 

Stack Diameters between 12·24 inches minimum points are 8 ; 

4 points per port if the 8 I 2 diameters downstream and 

upstream criteria Is met. 

I QC'd by: JRF I 

8 
Traverse Point Delta P Sq. Rt. Delta P Null Reading (Angle) Stack Temp. (°F) 

1-1 0.0000 

1-2 0.0000 1-3 0.0000 1-4 0.0000 1-5 0.0000 1-6 0.0000 1-7 0.0000 1-8 0.0000 

2-1 0.0000 2-2 0.0000 2-3 0.0000 2-4 0.0000 2-5 0.0000 2-6 0.0000 2-7 0.0000 2-8 0.0000 

Average #DIVIOI 0.0000 #DIVIO! 

QC"dby:JRF 

Note: Mlcro-monometer required based on preliminary low flows. 

Note: The cyclonic flows were not tested based on the absence of cyclonic flow from previous test results. 
Client: Dalltalia Location: Muskogee, Oklahoma 

Source: Wet Scrubber 2 Job Number: 210155 

Meter Box: NC-2 Original Delta H @: 1.986 

Calibration Date: 9/29/2009 Original Y Factor: 0.987 

Initial Volume: 87.200 Initial Meter Temperature: 88.0 

Final Volume: 94.875 Final Meter Temperature: 86.0 

Meter Volume: 7.675 Average Temperature: 87.0 

Deg.R 547.0 

Barometric Pressure: 29.30 

Yo = 1.005 

Y 0 Equation: 10 I (Volume) X SQRT ((0.0319 * (Tm/Pbar)) 

Y0 Result: 1.303 X 0.772 I QC'd by: JRF 

Meter Calibration o/o Difference = -1.87% 

Signature: Date: 
Run Date 

1 05/14/10 

2 05/14/10 

3 05/14/10 

FTIR Raw Input 

Results Summary (from FTIR Output) 

See Raw Results from FTIR Data Set 

Time (24-hr) Measured Concentration, ppm (wet, v/v) 

Start Run End Run Hydrogen Chloride Hydrogen Fluoride 

HCI HF 

14:03:00 15:04:00 7.88 8.94 

15:27:00 16:30:00 12.63 10.55 

16:55:00 17:58:00 4.98 5.65 
Run Number . - 1 2 3 AVERAGE 

Test Date - - 05114/10 05/14110 05114/10 05/14110 All Runs 

Times, Pollutant Runs (Began - Ended) - Military Time 1403-1504 1527-1630 1655-1758 -

Times, Flow Runs (Began - Ended) - Military Time 1403-1504 1527-1630 1655-1758 1800-1814 

Sampling Time 8 minutes 60.0 60.0 60.0 - 60.0 Stack Area A. Ft' 28.27 28.27 28.27 28.27 -

Barometric Pressure p,_ in.Hg 29.79 30.01 30.01 30.01 29.96 

Stack Static Pressure Po in. H20 0.37 0.45 0.45 0.45 0.43 

Oxygen Concentration,% (dry basis) o, % 19.0 19.0 19.0 19.0 19.00 Carbon Dioxide Concentration,% (dry basis) co, % 2.0 2.0 2.0 2.0 2.00 

Avg. Sq. Rl. of Delta P sqrt6P (in. H20)1 /2 0.702 0.702 0.702 0.702 0.702 

Stack Temperature .. "F 133.5 133.5 133.5 133.5 133.5 

Hydrogen Chloride (FTIR), ppm, wet HCI ppm, wet 7.884 12.634 4.976 8.498 Hydrogen Fluoride {FTIR), ppm, wet HF ppm, wet 8.944 10.555 5.651 8.383 

Hydrogen Chloride (FTIR), ppm, dry HCI ppm, d, V IV 9.400 15.103 5.965 10.156 Hydrogen Fluoride {FTIR), ppm, dry HF ppm, d, vI v 10.664 12.618 6.773 10.018 
Test Date(s) - 05114110 051H/10 05114110 05114/10 3Runs Times, Pollutant Runs (Began - Ended) - Military Time 1403-1504 1527-1630 1655-1758 0 . Times, Flow Runs (Began - Ended) - Military Time 1403-1504 1527·1630 1655-1758 1600·1815 

1. Stack Pressure P.., + P1 /13.6 P, in. Hg 29.82 30.04 30.04 30.04 29.97 

2. Meter Pressure Pw + AH !13.6 in.Hg 29.79 30.01 30.01 29.94 

3. Standard Meter Volume 17.&.4' Y' fV.JT (P.., + 411 /13.6) viii( .... dstl 0.000 0.000 0.000 0.00 

4a. Standard Volume of Water Vapor Condensed -o.04706'W, .. v'«(.hll sci 0.000 0.000 0.000 0.00 4b. Standard Volume of Water Collected in Silica Gel ..0.04715'W., v .... sci 0.000 0.000 0.000 0.00 

5. Moisture Fraction :rv_,., .... _ .... wrv_ ......... _, ..... B" fraction 0.1613 0.1635 0.1657 0.1635 0.16 

9. Molecular Weight of Stack Gas (dry basis) • 0.32'(0,)+ 0.44'(CO:I+0.28'(101l-(O,HCO,I) M, g lg-mole 29.144 29.080 28.992 29.072 29.07 

10. Molecular Weight of Stack Gas (wet basis) • M,'(1·B-1+18.0'(B.J M, gig-mole 27.347 27.268 27.171 27.262 27.26 

11 . Average Stack Gas Velocity • B5.49'C,.'(sqrt 6PI..,'SQRT((T ,1 I (P,"Mwll v, ftls 42.89 42.89 42.89 42.89 42.89 

12. Stack Gas Flow @ Actual Condnlons = 60'v,'A, a, ac;fm 72.766 72.766 72,766 72,766 72766 13. Stack Gas Flow @ STP " Q. "(T .,.IT ,)'(P JP ,..) a, serm 64,971 64,971 64,971 64,971 64971 14. Stack Gas Flow @ STP, dry = a, '(1·B-I'(T ...IT ,I'(P ,11',.) a., dstfm 54,349 54,349 54,349 54,349 54349 15. Hydrogen Chloride Cone.@ Std.Conditions =(0.01543'HCI,..JN- HCica gr/dsef 0.00621 0.00998 0.00394 . 0.01 15. Hydrogen Auoride Cone.@ =(0.01543'HF,..JN_, HFcs gr/dscf 0.00387 0.00458 0.00246 - 0.00 

21. Hydrogen Chloride Mass Emissions "(6017000I'HCics'O... HCIIbs/ hr lbslhr 2.89 4.65 1.84 . 3.13 

32. Hydrogen Auoride Mass Emissions "(6017000)'HFcs•a.. HF ·lbslhr lbs /hr 1.80 2.13 1.14 . 1.69 

CALCULATED TEST DATA· Metric Units 

Deacrtptton I Fonnulas Syn'Col Units Calculated Data QC'dby,JRF 

Run Number 1 2 3 4 AVERAGE 

Test Date - 05114110 05114/10 05114110 05114/10 3Runs Times, Pollutant Runs (Began - Ended) Mllilary Time 1403-1504 1527-1630 1655-1758 . . 

1. Stack Pressure = P,'25.4 P, mm.Hg 757.36 763.09 763.09 763.09 761.66 

5. Moisture Fraction =tv .... .., .. v_,..,)l(v...,,,., + v_ ... , + v ...... a_ fraction 0.161 0.163 0.166 0.163 0.163 

9. Molecular Weight of Stack Gas, dry basis = 0.32'(02)+ 0.44'(C0,)+0.28'(100oj0,)1CO,)) M, g/g·mole 29.144 29.080 28.992 29.072 29.072 

10. Molecular Weight of Stack Gas, wet basis = M,'(1·B,.,)+18.0'(B,.,) M, g/g·mole 27.347 27.268 27.171 27.262 27.262 

11. Average Stack Gas Velocity = 85.49'C,'(sqrl AI').,. 'SQRT((T ,) I (P, 'M,.)) v, m/s 13.07 13.07 13.07 13.07 13.07 

12. Stack Gas Flow @ Actual Conditions =eo•v:A. a, acmm 2,061 2,061 2,061 2,061 2.061 

13. Stack Gas Flow @ STP = Q.'(T,1,1T,)'(P,IP,.,) a, stmm 1,840 1,840 1,840 1,840 1,840 14. Stack Gas Flow@ STP (dry) = Q.'(1·B-)'(T,1,1T,)'(P ,/P,,.) a.,, dscmm 1,539 1,539 1,539 1,539 1,539 

15. Hydrogen Chloride Cone.@ Std.Conditions ( FTIR) mg/dstm 14.217 22.841 9.021 - 15.360 

15. Hydrogen Fluoride Cone.@ Std.Conditions (FTIR) Hfcs mgldscm 8.851 10.473 5.622 - 8.3154 

15. Hydrogen Chloride Cone @ 7% 02 =C,' ((20.9·7)/(20.9-%02)1 c...,, mglds<m. 85.92 167.10 59.71 . 104.24 15. Hydrogen Fluoride Cone @ 7% 02 •• ((20.9· 7)1(20.9-%02)) c.,, mgldscm. 53.49 76.62 37.21 - 55.77 

21. Hydrogen Chloride Mass Emissions =(6017000)'HCics•o,.. HCI kg I hr kg/lv 1.3128 2.1091 0.8330 - 1.4183 21. Hydrogen Fluoride Mass Emissions •(6017000)'HFcs•a.. HCII<g/ 1v kg/hf 0.8173 0.9671 0.5191 0.7678 
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0.0001 O.CM ~ 

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S/14/2010 11:15:01 :\C•k:mot~s\20155 cbl tilt\20100514\ HI cts scon BdO<o Run 1_03130.SPE 

S/14/2010 11:15:19 C:\CalunctS~\201SS d>llilo\20100514\ HI cts sc.on Bolon Run 1_03131.SPE 

5/14/2010 11:15:22 C:\Cil<metSamplts\201SS dol tilt\20100514\ HI cts scon klort Run 1_03132-SPE 

AVG 

Water "• Unil 

0 ..... " 

0 ""'"" 0 vol·" 

com~ns.a bs~ Myckocen chbidtt ttd Unit 

- 0.0016 0 ppm 

wtl 0.0007 0.06 ppm 

Ml O.OOil 0.03 ppm 

Roslclual Hydrocon fkl«ide Hf Urit 

0.0008 2U.71 """ 

0.0001 21l.89 ppm 

0.0004 212.13 ppm 

212.60 

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0.004 

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Unit 

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Re~ 

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0.0013 

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S/14/2010 

S/14/2010 

S/14/2010 

r.m~ SpectrUI"'I\File 

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11:19:22 :\~IS.mples\201SS dollilt\20100514\ Sf6 ,,. «M!Borort Run l_OllOUPE 

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AVG 

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0 vol·" 

Com pen~ Residua& Hydfoten chkN'HS. HCI Un._ Reslduol Hyd<ocen fluotide HF UniC 

wt1 

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0.0001 

0

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w•1 0.0015 0 ppm 

0

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0

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O.OJR.-.a Sf6 u ... Resi<kl .. o.oozz 9.9 ppm 0.0016 0.0018 9.!1 ppm 0.0018 

0.0043 10.1 ppm 

o.oozs 

9

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HCL Dalllalla 

Sm -&pllood Oalo 

Dolt 

S/14/1010 

5/14/1010 

S/1.,-2010 

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320 

320 

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S/14/2010 IUI3:S6 C:\(olanttS...pios\20155 doltllt\2010DSU\Wtt su-. 2 Sf6 ... bolo<t '"" 1_03S 1U5vol-" 

S/14/2010 

S/14/2010 ll:OC:02 

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Hati" Data HCI-~16 

Doto nmt •cuumftlt Wlltr vapc UrMI Compen~ion Resictull 

S/14/2010 12:11:17 C:\Calc:I!'NtS..-npt.s\20155 dal tile\20100514\Wtl S<t*r l before run l_Ol300.Sf'[ t•.n vol·" Wtl 

5/14/1010 12:n :• 3 C:\CakrMtSMriPfi\10155 ctal tile\2010051•\Wet Sallber 2 Mfore run l_0330l.SPE JC.I? ....,.." 

5/14/2010 12:32:49 C:\c.krnt~\201S~ dol tilt\20100S14\Wot ~r 2 btforo run 1_03302.SP£ ••. 65 val-~ --

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0.0022 0.99 PfN" 0.0004 9.91 ppm 0.0044 0.!141- 0.0021 

0.0021 l.42 ppm 0.0004 11.16- 0.000 .. , ..... 0.0011 

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0.0041 24.31 ppm 0.000< 1U7p""' 0.0067 D ppm 0.0031 

0.00!8 29. 13 ppm O.OOOJ " .53 ppm 0.005 0.01 ppm o.ooza 

Hydroc;f:'n c:hlorUnit Residual Hvdroc:en ftu.Un6t Re sidual Sf6 Uait "tsidu~l 

O.OOll i.53 PPM o.oooe 11.]3 "'"' 0.(1(1)7 0.03 ppm 0.001. 

0.0035 , ,65,. 0.0007 12.17 PCif11 0.0057 O.OJ ppm 0.0026 

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S/14/lOlO 12:32:0 C:\c.km.ttSampiH\lOlS!.dal Ule\2:010DS14\Wet S<ru~rl Mfort run I_Ol301.SP£ 14.67 \IOI•" w•t 

S/14/lOlO l2:Jl:.t9 C:\CJicmct.S•mpltt\201S!tdal Ule\20100U4\Wt'l Scru~r l: ~fort tuft l_DJlOl.SP£ 14.6S vol-" w•• 

~ ........ HydfOJHIUr'li( Rnld•l Hy4ro&M tluot1dt HF Unit Rcstdwl Sf6 UM Residual 

0.0024 1.73 p,_ o.ooos 9.19 ppm 0.0002 0.99 liP"' 0.0024 

0.0022 0.99""' 0.0000 ..,,,... 0.0004 0.91 .. ,. 0.0021 

O.OOl l '2~ 0.0000 ll.K,..., 0.004J ... _ O.OOIJ 

··- Hy4toaen tUM ~~ tfVdlOftft..,..Hf Unl< RtsWIHI Sf6 ...... ......... 0.0024 S.lppm OA>DOJ JO.J6.pprr'l 0.0047 o,... 0.0017 

0.0021 S.16ppm 0.0000 JUt- 0.0006 0.01 PP"' 0.0016 

0 .0021 2., "'"' o.oooJ JO.S' '~"" o.ooos Oppm 0.0017 

Resldull ttvdrocen cUnit Rnldual Hydroatn nuQflcft HF Unit lesidwl Sf6 Unit Residual 

0.00>2 l!i.Slppm O.O!XIt n.u ppm 0.00~7 0.0) ;rrpm 0.0024 

O.OOJS UiS PP11 0.0007 12.17 ppm D.DOS7 0.0) ppm 0.0026 

0.00]1 7 ,11 ppm 0.0009 U .J6 ppm 0.0019 o..,m 0.0025 
D1t~ 

S/14/2010 

5/14/2010 

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Time SpectrumFife 

14:03:10 C:\CokmetS.mplos\20155 dol tile\20100514\Wot 5crubor 2 rvn 1_03781.SPE 

14:04:11 C:\CokmotS.mplos\20155 dal tile\20100514\Wot 5cruber 2 run 1_03782.SPE 

14:05:11 C:\Cokmot5amplos\20155 dol t~e\20100514\Wet 5cruber 2 rvn 1_03783.5PE 

14:06:11 C:\CalcmotSomplos\10155 dal Ulo\20100514\Wet Scruber 2 run 1_03784.SPE 

14:07:13 C:\CakmotSomplos\20155 doltilo\20100514\Wot Scrvber 2 run 1_0378S.SPE 

14:08:13 C:\CokmotSomc>los\20155 dol t;r.\20100S14\Wot Scrvber 2 rvn 1_03786.SPE 

14:09:14 C:\CokmotSomc>los\20155dol tilo\20100S14\Wet Scrvber 2 run 1_03787.SPE 

14:10:15 C:\CokmotS.mc>los\20155 dol tilo\20100S14\Wet Scruber 2 run 1_03788.SPE 

14:11:16 C:\CokmetSomplos\20155 doltilo\20100514\Wet Scruber 2 run 1_03789.5PE 

14:12:16 C:\CokmetSompl«s\20155 dol tilo\20100514\Wet Scn~bor 2 run 1_03790.5PE 

14:13:17 C:\CokmetSomplos\20155 dol tilo\20100514\Wet ScNbor 2 run 1_0379l.SPE 

14:14:18 C:\CokmotS.mples\20155 d•l tile\20100SI4\Wot Scrubor 2 "'" 1_03792.5PE 

14:15:19 C:\CokmetS.mplos\20155 dol tile\20100514\Wet Scrvbor 2 rvn 1_03793.5PE 

14:16:19 C:\CokmetS.mplos\20155 dal tilo\20100514\Wet 5cruber 2 run 1_03794.SPE 

14:17:20 C:\Colcmet5amplos\20155 dol tUo\20100514\Wet 5trubor 2 rvn 1_03795.SPE 

14:18:21 C:\CokmotSamplos\20155 d•l tije\20100514\Wot Scrubor 2 rvn 1.03796.5PE 

14:19:21 C:\Colcmet5ompl«s\20155 doltile\20100514\Wet Scrvber 2 run 1_03797.5PE 

14:20:12 C:\CaltmotS.mplos\20155 dol tile\20100S14\Wet Scrvber 2 run 1.03798.5PE 

14:21:22 C:\CokmetS.mc>los\20155 dol tilt\20100S14\Wet Scnsber 2 run 1.03799.SPE 

14:22:23 C:\CalcmotS.mc>los\20155 dol tilo\20100S14\Wet Scnsber 2 run 1_03800.SPE 

14:23:24 C:\ColcmetS.mc>los\20155 dol tilo\20100S14\Wet Scnsber 2 run 1.0JI01.SPE 

14:14:14 C:\Cakmot5omc>los\10155 dol tile\20100514\Wet Scrvber 2 run I.OJI02.SPE 

14:25:25 c:\C•Icmet5omplos\20155 dol tilo\20100514\Wet ScflJbor 2 run I.OJI03.SPE 

14:26:26 C:\CaltmetS.mplos\10155 dol tile\20100514\Wet Scrubor 2 run 1_03804.5PE 

14:27:27 C:\ColcmetS.mplu\20155 dol tile\20100514\Wet Scruber 2 run 1_03805.5PE 

14:28:27 C:\CokmetS.mplos\20155 dol tllo\10100514\Wet Scrubor 2 n~n 1_03806.5PE 

14:29:28 C:\CokmotS.mplos\20155 dal tile\20100514\Wot Scruber 2 "'" 1_03807.5PE 

14:30:29 C:\CokmotSamploJ\20155 dol tile\20100514\Wot 5crubor 2 rvn 1_03808.SPE 

14:31:29 C:\CakmetS.mplos\20155 dal tile\10100514\Wet Struber 2 rvn 1_03809.SPE 

14:32:30 C:\C.Icmet5amplos\20155 dol tilt\20100514\Wet Scrvber 2 rvn 1_03810.5PE 

14:33:31 C:\CalcmotS.mplos\20155 dol tilo\20100S14\Wet Scruber 2 run 1.03811.SPE 

14:)4:32 C:\CalcmotS.mc>los\20155 dol tie\20100S14\Wet Scrvber 2 run 1_03812-SPE 

14:35:32 C:\C.IcmotS.mples\20155 dol tilt\20100S14\Wot Scnsber 2 run 1_03813.SPE 

14:36:33 C:\CalcmotS.mplos\20155 dol tilo\20100S14\Wet Scrvber 2 run 1.0381'-SPE 

14:37:33 C:\CakmetSomples\10155 dol tile\20100S14\Wet Scruber 2 "'" 1_03815.5PE 

14:38:34 C:\CalcmetSompl«s\20155 dol tile\20100514\Wet Scn~bor 2 Nn 1_03816.SPE 

14:41:06 C:\CalcmetS.mplts\20155 dol tile\20100514\Wet Scrubor 2 Nn 1_03817.SPE 

14:42:07 C:\C.kmetS.mplos\20155 dollilo\20100514\Wet ScRJbor 2 run 1_03818.SPE 

14:43:08 C:\CokmoiS.mplos\20155 dol tllo\10100514\Wet Scrubor 2 "'" 1_03819.5PE 

14:44:09 C:\CokmotS.mplos\20155 dal tile\20100514\Wot 5cruber 2 run 1_03820.5PE 

14:45:09 C:\CokmotSamplts\20155 dal tilo\20100514\Wot Struber 2 rvn 1_03811.SPE 

14:46:10 C:\CokmetSomples\20155 dol tilo\20100514\Wot ScRiber Z "'" 1.03822.5PE 

14:47:11 C:\Cak;metSomptes\20155 dol tile\20100S14\Wet Scruber 2 rvn 1_03823.5PE 

14:48:12 C:\CaltmetSomplos\20155 dol tilo\20100S14\Wot Scrubef 2 run 1_ 03824-SPE 

14:49:12 C:\CaltmotSamples\20155 dol tile\20100SI4\Wet Scrvber 2 rvn l_03825.SPE 

14:50:13 C:\CaltmotS.mplos\20155 dol tilo\20100SI4\Wot Stnsber 2 ""' I_038~.SPE 

14:51:14 C:\CalcmetS.mplos\10155 d•l tilo\20100S14\Wet Scruber 2 run 1_03827.SPE 

14:52:14 C:\C.IcmotSamples\10155 dol tilo\20100S14\Wet Scrubor 2 run 1_03828.5PE 

14:53:15 C:\Colcmot5amplos\20155 dol tile\20100514\Wot 5crubor 2 run 1_03829.5PE 

14:54:16 C:\Calcmet5omplos\20155 dal tile\20100514\Wet Scrubor 2 "'" 1.03830.SPE 

14:55:16 C:\CalcmetSomplos\10155 dol tilo\20100H4\Wet Scrubor 2 rvn 1_03831.SPE 

14:56:17 C:\Calcmet5amplos\10155 dol tllo\20100514\Wet Scrvber 2 run 1.03832.SPE 

14:57:18 C:\Calcmot5omples\20155 dol tii«\20100514\Wet Scrubor 2 run 1_03833.SPE 

14:51:19 C:\C•Iemet5omplos\20155 dat tlle\20100514\Wet Scruber 2 run 1_038)4.SPE 

14:59:19 C:\Colcmet5omplos\10155 dat tilo\20100514\Wet Scrubor 2 run 1_03835.SPE 

15:00:10 C:\Cakmet5omples\2015S dol tilo\20100S14\Wet ScRiber 2 run 1_03836.SPE 

15:01:21 C:\Calcrnet.SanoPes\20155 dol tile\20100514\Wet Scruber 2 run 1.03837.SPE 

15:02:21 C:\CalcmetSomplos\10155 dol tilo\20100514\Wot ScRJbor 2 run 1_03838.5PE 

15:03:22 C:\CakmetSomc>los\20155 dol t;r.\20100514\Wot Scrubor 2 Nn 1_03839.5PE 

15:04:23 C:\Cokmet5ornjMs\20155 dol tile\10100514\Wet Scrubor 2 run 1_03840.5PE 

AVG 

W1te1 '4'.1PI Unit 

17.37 vol·% 

17.73 VOl·% 

17. 19 VOl·% 

17.45 vol-% 

17.47 val·% 

16.97 val·" 

16.88 \101-% 

17. 28 \101-" 

16.98 \101-% 

16.65 val·% 

16.7 val·" 

16.68 val·% 

16.79 VOl·% 

16.63 1101·" 

16.26 vol·" 

16.25 VOl·" 

17. 19 vol-% 

16.6 VOl·% 

16.7 val·% 

17.19 vol-% 

16.97 val·" 

16.59 val·% 

16.89 val·% 

17.41 1101·% 

17.17 1101·% 

16.48 1101·" 

16.27 vol·% 

16.11 1101·% 

16.23 VOl·% 

16.65 vol·" 

16.08 vol·" 

16.21101-% 

16.56 val·% 

16.5 val·% 

16.59 \101-" 

16.54 vof." 

16.99 1101·% 

16.36 1101·% 

16.74 1101·% 

16.59 vol-% 

16.76 vol·% 

16.74 vol·% 

17.03 val-% 

17.65 1101-% 

17.1 vo~% 

17.35 val·" 

17. 14 vol-" 

17 1110~" 

17.27 1101·" 

16.68 vat-% 

16.53 YOI·" 

16.49 YOI·" 

16.97 vol·" 

17.04 vol·" 

16.89 vof." 

16.75 val·" 

17.29 val·" 

17.4 vol-% 

17.22 val·" 

17.17 vof." 

16.86 

Compenu Rtosidual Hydroten c Unit 

wot 0.0045 2.84 ppm 

wot 

wot 

-· 

-· 

-· 

---lftt 

wot 

wot 

wet 

wot 

wot 

wet 

wot 

wet 

wot 

--

-

wet 

wot 

wet 

wot 

wet 

wot 

wot 

wet 

wet 

wot 

wet 

-wet 

wet 

wot 

wot 

wot 

wot 

wot 

wot 

wot 

wet 

-· 

-

wet 

-· 

wet 

-· 

-· 

-· 

wot 

-· 

wot 

-----· 

0.0047 

0.0045 

0.0045 

0.0046 

0.0045 

0.0044 

0.0046 

0.0044 

0.0043 

0.0044 

0.0042 

0.0043 

0.0042 

0.004 

0.0042 

0.0045 

0.0042 

0.0043 

0.0044 

0.0043 

0.0042 

0.0042 

0.0045 

0.0044 

0.0042 

0.0041 

0.0041 

0.0042 

0.0043 

0.004 

0.004 

0.0042 

0.0042 

0.0042 

0.0042 

0.0043 

0.0042 

0.0043 

0.0042 

0.0043 

0.0043 

0.0044 

0.0045 

0.0043 

0.0045 

0.0045 

0.0044 

0.0044 

0.0043 

0.0042 

0.0041 

0.0044 

0.0044 

0.0043 

0.0043 

0.0046 

0.0045 

0.0044 

0.0045 

2.42 ppm 

2.54 ppm 

2.58 ppm 

1.5 ppm 

2.34 ppm 

2.17 ppm 

2.3-1 ppm 

2.28 ppm 

2.36 ppm 

2.57 ppm 

2. 23 ppm 

1. 15 ppm 

1.87 ppm 

2.8 ppm 

1.71 ppm 

2.47 ppm 

2.27 ppm 

2.17 ppm 

1.9ppm 

1.69 ppm 

2.53 ppm 

2.51 ppm 

3.31 ppm 

2.33 ppm 

1.98 ppm 

2.99 ppm 

2.5 ppm 

1.98 ppm 

1.94 ppm 

1.78 ppm 

1.78 ppm 

2.49 ppm 

2.2 ppm 

2.19 ppm 

1.7 ppm 

18.94 ppm 

17. 16 ppm 

16.86 ppm 

16.3 ppm 

15.38 ppm 

18.25 ppm 

18.94 ppm 

16.3 ppm 

19.66 ppm 

18.46 ppm 

13.77 ppm 

14.14 ppm 

IB2 ppm 

15.64 ppm 

15.03 ppm 

15.14Wm 

17.16 ppm 

19.8wm 

14.47 ppm 

15.19 ppm 

15.27 ppm 

16.87 wm 

13.92 wm 

12.4Swm 

7.88 

Residual Hydtocen f Unit 

0.0004 9.58 ppm 

0.0004 10.9 ppm 

0.0005 8.92 ppm 

0.0004 

0.0004 

0.0004 

0.0004 

0.0005 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0005 

0.0005 

0.0004 

0.0004 

0.0004 

0.0003 

0.0003 

0.0004 

0.0004 

0.0004 

0.0004 

0.0005 

0.0003 

0.0004 

0.0004 

0.0004 

0.0058 

0.0055 

0.00$3 

O.OOS3 

0.0054 

0.0059 

0.0062 

O.OOS7 

0.0062 

0.0061 

O.OOS2 

0.0053 

0.005S 

0 .0052 

o.oos 

0.0051 

0.0062 

0.0066 

0.0052 

0.0053 

O.OOS3 

O.OOS3 

O.OOS1 

o.oos 

10.34 ppm 

9.08 ppm 

9.01 ppm 

8.77 ppm 

9.09 ppm 

8.41 ppm 

8.9ppm 

9.35 ppm 

9.12 ppm 

9.07 ppm 

9.31 ppm 

8.71 ppm 

8.47 ppm 

9.06 ppm 

8.87 ppm 

8.08 ppm 

9.aa ppm 

8.92 ppm 

8.3 ppm 

8.22 ppm 

8.14 ppm 

9.43 ppm 

8.32 ppm 

7.26 ppm 

8.29 ppm 

8 ppm 

9.47 ppm 

8.65 ppm 

9.14 ppm 

8.39 ppm 

1.65 ppm 

8.58 ppm 

8.65 ppm 

7.99 ppm 

8.29 ppm 

8.5 ppm 

9.02 ppm 

8.2 ppm 

8.93 ppm 

1.64 ppm 

10.47 ppm 

9.18 ppm 

9.92 ppm 

10.01 ppm 

9.44 ppm 

8.44 ppm 

9.67 ppm 

9.2 ppm 

7.91 ppm 

9.35 ppm 

8.96 ppm 

8.41 ppm 

10.08 ppm 

9.18 ppm 

9.09 ppm 

8.83 ppm 

8.96 ppm 

8.94 

Residu11 SF6 

0.007 

0.0064 

0.0069 

0.0063 

0.0071 

0.0068 

0 .0068 

0.007 

0.0068 

0.0067 

0.007 

0.006 

0.0071 

0.006 

0.0067 

0.0063 

0.0069 

0.007 

0.0068 

0.0065 

0.0069 

0.0067 

0.0068 

0.007 

0.0068 

0.0065 

0.0066 

0.0064 

0.0066 

0.006 

O.OOS9 

0.006 

0.0068 

0.0069 

0.007 

0.0068 

0.0066 

0.0067 

0.0071 

0.007 

0.007 

0.0069 

0.007 

0.0066 

0.0072 

0.0065 

0.0064 

0.0064 

0.007 

0.0063 

0.0062 

0.0067 

0.0072 

0.0067 

0.0068 

0.0066 

0.0073 

0.0073 

0.0068 

0.0072 

Unit 

Owm 

0 ppm 

owm 

o ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

o ppm 

owm 

0 ppm 

o ppm 

0 ppm 

o ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

o ppm 

0 ppm 

0 ppm 

0 ppm 

owm 

o ppm 

Oppm 

Oppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

o ppm 

o ppm 

owm 

owm 

0 ppm 

Oppm 

Ownn 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

o ppm 

o ppm 

0 ppm 

0 ppm 

o ppm 

o ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0.00 

R~stdu1l 

0.0028 

0.0039 

0 .0029 

0.0038 

0.0032 

0.0033 

0.0033 

0.0031 

0.0033 

0.003 

0.003 

0.0034 

0.003 

0 .0037 

0,0031 

0.0035 

0 .0035 

0.0029 

0.003 

0.003S 

0.0033 

0.0033 

0.0035 

0.0036 

0.0036 

0.003S 

0.0033 

0.0035 

0.0034 

0.0033 

0.0033 

0 .0033 

0.0028 

0.003 

0.003 

0.0027 

0.003 

0.0031 

0.0032 

0.003 

0.003 

0.0031 

0.0029 

0.0035 

0.0029 

0.0037 

0.0035 

0.0034 

0.0031 

0.003-1 

0.0036 

0.003 

0.003-1 

0.0033 

0.0032 

0.0036 

0.0032 

0.0033 

0.0032 

0.0033 
HCL Dalltalia 

Sm~lcodData 

O.tt 

S/14/:010 

S/10/2010 

S/14/2010 

Method 

320 

320 

320 

Filtn_.t HCI{ppmj 

29.53 

21.?6 

30.24 

Ava.Conc.{-1~ 

Sf6 CppmJ 

0.93 

0.99 

o.n I o.t)SI 

s..--Cone. 01 ana¥- o ... 

S/14/2010 

S/14/2010 

5/14/2010 

Stn 

s.. 

Of 

c. 

c. 

Method 

320 

320 

320 

Aei:CWtf'Y(%)• 

c.. Of.,,. Su(l·Df') 

29.51 - 14.0 PPM 

9.4"" 

200.1 ppm 

9.9& ppm 

ll.SS ppm 

Ftlefllam4: 

Sm · So(1·Dfl 

DfxC:. 

ltCICPt>ml 

U5.17 

1).92 

12.48 

SF6 Cppm} 

0 

0 

0 

Ava. Cone. (ppm tO§ I I 

...... cootetllfili<>n ol .,....,.....,... 

Nat• COftCMttalilo.. ol .,~. 

Ditution ~actor (T¥1t' < 1'"'-} 

Cyliftdtf' ol "Piktd I.U 

CyliftdiK oltr•C"ff 1ft• (SF6) 

Elcpected concentration of M•lytt 

Roco .. rv 1'<1! aU%! 70·110" 

s.>ittd«a Sf6 

O.t• limo Spe<uwmJM Wattt ~r~~ap<UI"'II ComP"Hbon ~mu• 

5/14/2010 16:Jl:"S :\Calc.JM~s\lOlSS cbl tilt\20100514\wtC wubbotr2 Sf6 Spikt AMI IbM 2_~ 16.77 .... " 

S/14/2010 

5/IC/2010 

t6;)):SI 

t6:JJ:5\ 

C:\c..k.nMtSamples\201SS 

C:\CJkrntt~\201SS 

dill 

d~ 

tile\20100S14\wet 

tb\20100$14\ ..... t 

su~r2 

urubber2 Sf' 

Sf5SpiU> 

Spa 

After 

AftH...,.. 

R~o~n 2_1)10S 

2_~ li.$2 

16.41..0·

..0·% 

" --

wet 

Spfktdata HCL 

o. .. Tome Sptctrumfilt Walt'tY~Uftit Co"'"nsalion Rt'Mdu .. 

S/14/2010 16:oU:2S C~\CalcmetSamples\20lSSd•l ,.le\20100$1•\wt( Ktubbtrl Hd SpUct Ahef 1\un 2_0U2 16.41 YOI·" 

5/14/2010 \6:41:37 t:\C.IC'Mtt.Sampl~s\20tSSdal tile\20100$14\wtt saubbtrl Hd Sp;kl! After Run z_oe12 11.05 .ol·" -

_, · S/14/2010 16:41:0 C:\C.IC'Mt•Sampl~s\20155 d•l tlle\20100S1•\wtl saubbtrl lid Spike After Run 2_0412 16.33 ""''" 

_, 

"•tiw Oitl HCI·Sf6 

Oalt Time SPtCitumF"• W4Ctt'I~(Vnit Compe nsation llttsid"al 

S/14/2010 15~1;21 C:\c.akm•tSimS)I.s\201SS dolll tile\20100S14\Wt1 SUubtr 2 ntt1 1_03138.S.PE 17.4 Yol·" wet 

S/14/2010 lS-:Ol:ll C:\C..rnt:tSam$>1f1\201SS d~ tilt\20100Sl4\Wt1 Su_..r 2 tttnl_031l'9oSPE 17.22 .... ,. 

S/14/2010 IS:<M:ll C:\ColciTiotS ...... \20155 doi1Jte\2010DSU\W .. Sulll>cr 2 ronl_Cl3140.SI'{ 1717 vol-lt. --

....,.oc .. d\k)fVnic R.tidual Hydroa«n fiMo Unit .. - Sf6 UNI .......... 0.0044 l2.69PfM" 0.0067 12~ 0.0075 o.n,_ O.OOlt 

0.0041 18.06ppm o.oos 1.79- 0.006t O.Hppm 0.00l2 

0.0043 12.62- 0.0049 7.91 Ppia 0.0063 O.llppm O.OOJC 

~oten chtor Onit Re-sidual Kydrocen Ouo U•it Residual Sf' Unit Residu•l 

0.0011 29.SJ ppm 0.0011 2.6 ppm 0.0016 0 ppm D.OODI 

0.0021 21.76 ppm 0.002) 6.42 ppm 0.0052 Oppm o.oon 0.0027 30.24 ppm 0.001-0 41.Uppm 0.0054 0.02 ppm 0.0027 

Hydrocen chlorUnil fltsldu~ H~~n fluo Unil Resklull 5f6 Unit ... sid ... l 

0.0045 )6.87 ppM O.ODS3 ,.09 ppm 0.0071 OppM 0.0033 

0.0044 13.92- 0.0051 

.... _ 0.0061 Opom 0.0032 

0.0045 12 .... PP"' O.ODS ..,,..., 0.0072 0- 0.0033 
HfDaiiUolia 

......... _Dolo 

o ... 

S/lt/2010 

S/IC/2010 

S/14/2010 

...- l20 

l20 

)20 

, ...... IIF""'"'I SF6[pjlm) 

:z:.sa 1.00 

l2.A4 o ... 1:.91 o ... A~J. COAC. tpp,_) c::::::J!EI I 1.0071 

Su -Nathe Cone. Of •n;~lyto 

Date M~hoc:l F .. el'lamto Hl(ppm) $F6[ .... 1 >tt•noto 

~ll•noto 

~n•noto 

Sm 

Su 

Of 

c. 

c. 

JZO 

l20 

)20 

RacOMry f") • 

C. • Df ll Cs • Su(l-Of) 

n.n Plk'n 

..,, ppm 

2u'·"'" .o..,. 

.... ""' 21.76 ,. 

Avc. Conc. (ppm} 

Sm~Of) 

Ofx($ 

9.09 

&.IJ 

~ 

U6 

I 

Mon COftt"tnotion of s,ptlird .N'I.ty\e 

HMNI' conu•ntration of ...e,te 

Oilutla. Fa"Of (TMJet <10M,) 

Cytlftdtto4splle4au 

~oltr.cer1-.ttsf'} 

hp.ectH concentrM10n of Matyte 

............ ~ 10A%j 10 uo" Spike O.ta Sfi 

O.Me "'" sn•noto 

S/l<nGIO 

S/14/2010 

Splk O.ca Nf 

S/14/2010 

snono1o 

S/14/2010 

Hatfve Oeta HF·SFI 

~te nrM 

>t~<noto 

5/14/2010 

5/14/2010 

~ttuMF~ Wet«~ vepc: Unit 

lS:Ol:l& \Ctk~s\lOlSStW t•\l0100S14\W.-t Scnlok1 l Sf6 Spil•Aftet run 1 J6.J9 wol-,.. 

lS:01:2S C:\CikfNtS~s.\20lSSUtilt\20100S14\W'lt~2SfiSpa.Aft., run l J4.l2 \'01-" 

LS:Qt:26 \CtiC11Ml»~s.\201SS dal tlle\20100514\Wet Sct\lbtr 2 Sf6 SpAe After tun I 14.9 Yolo'-

l!'d)::Z2 :\c.lc:,..tS&n.plcs\201~S ct.l tile\2:0100514\Wet Scrultcr :Z Ht $pike Aft•r run 1 

JS:J7:41 C:\C.IcmetS•mplcs\201SS dill tllc\2D1010Slt\W•t ScruMr 2 ttl Spike -'fter run 1. 

tS:J7:$4 C:\CelcmctS•mples\201S51bl tlle\201005)t\Wet $crulter 2 Hf .Spike ~fter run 1. 

tS.S vol·,. 

U .tJ vol·" 

U .07 vot·,_, 

Spe<INiftFile: WatervapcUnlt 

U:02:21 C:\Cik~mpln\201~5 d<ile\20100514\Wel$tf\lbcr 2 run a_omt.SP£ 17.4 vol-% 

1S;01:22 C:\(tkmets.lm~\201SS dal Ule\20100SlC\W~tl Scrvbcr 2 rvn t.OJtJ9.$P( 17.22 vol•" 

lS;C)I:U C:\c.kmetS.Impln\20155 doll ttle\~OlOOSl'\Wcl $(1\1bcr 2 rvn l_OSMIUP! 17.17 v~"" 

(OII'IpeM.Itioab~ 

--.... 

.... 

.... 

w•• 

CCimf)4'nUUOn Rctldull 

.... 

--

o.oo 

0.0) 

0.0) 

o.ml 

0.0041 

0.004 

O.OOJZ 

0.001' 

0.0009 

O.OOSl 

0.004$ 

0.0044 

0.0045 

~enchkKUntt 

16.12""" 

17.11,... 

6.9 PPM 

IO.Sippm 

10.25 ppm 

n .u ppm 

Jotydro&~ <hlor Unit 

16.17 ppm 

ll.t:Z ppm 

12.41 ppm 

~~~~ Hvdtoceaftuo~VAil Rt:~ SF6 Unit ........ 0.0017 7.89 ppm 0.00651 1.0) ppM 0.()0)1 

0.0051 '-12 ppm 0.0066 0.9ppm o.oon 0.0046 , ,Uppm o.006S 0.9 PPM O.OOl9 

0 .0046 lJ.U ppm Q.0062 0 ppm 0.0001 

O.OOH 22.1A ppm O.OOSI 0 ppm O.DOOl 

0.0024 22.97 ,..,. 0.0044 0.01 ppm 0.00 .. 

ResMIIuel ttydrocen lluo• Ur~lt lflldiiNI Sf6 Unit "•~Mtu•l 

0.0051 51.09 ppm OOOIJ Oppm 0.001) 

0.0051 I.U I'P"' 0.0068 Oppm O.OOJ2 

0.005 1.96 ppm 0-0012 Oppm 0.00" 
S/1•12010 15:29:01 C:\C•km•t.Sampl~\20155 d•l Ule\20100514\Run 2_DJ!J2UPE 

S/14/2010 15:~:01 C:\C.akmttSamplti\lOlSSd•l tjle\20100514\Run 2 ... 0l!J2UPE 

S/14/2010 15:29:14 C:\Co~~tcm•~mll)lti\20155d•l tile\20100!.141\Rwn l_OJ92•.WE 

5/14/2010 15:29:20 C:\C•kmet.Sampln\2015Sdal ti ... \20100514\ftun l OJ92S.!#t:. 

i/14/2010 15:29:26 C:\C•kmel.Samplft\20155 dil ~tlt\20100514\Run 2-0)9l6.SPt: 

5/14/2010 1S:29:l2 C:\CI&crne-tS..Iimp!M\lOI55d.lllllitlt\20100SI4\aun 2-Ol9l7.SH 

S/14f/l010 1S:l9:ll (:\C.Ikrne~\10155 ~ dlt\10100514\Rvn l .. Oltli.SH 

S/1.V1010 IS:29:.W \C*IM~\l0155U 

rile\l'OlDOS14~un 2-Olllt.SPf 

S/14/lOlO 15·29-.S1 \C*mt~ft\20155 dal rt.\,20100St4VtWft 2:0)9)0.SPf 5/1~1010 15:29:51 \(M.Mt~e:sU0155 d.ll tilt'\20100514\R..-Z ... OH)l.SPt 

5/1<\fl010 15:10.GJ \CtltiN~\lOIS5 d ... tk\201005!4\J\M l ... 0),)2.SP£ 

S/14/2010 15:10;09 C:\c.tcMtt.Sall'ple:s\10155 d.lll tile-\20100514\Run l ... 0)9)).SP[ 

5/14/2010 1!d0::1S C:\CIItMt~llf'.,l~\20155 do~~l tile-\20100514\RYR l_0)9}1$P[ 

S/14/2010 15:30:21 C:\(~et.Sallf',.t!'l\20155 do~~l 1ilt-\20l00514\Ron l_Ol91S.SPE. 

5/14/2010 15:30:27 C:\C*mets..mples,\,20155 d•l 1ilt\201CXl514Vtun 2 ... 0J9li.S~t S/14/~DlO 15:30:33 C:\Cikm•tSatnplcs\20155dll Ule\20100514\ltun Z ... OJ9J7.5P( 

5/14/2010 15:30:39 C:\Co~~lcmetSatnpln\201S5d•l tllt\20100514\lton 2 ... 0JUI.SP( 

5/14/1010 l$:30:46 (:\C•h:mei.Samplft\2DlS5dll Ult'\20100St4~ulll'_OJ9Jt SK 5/14/2010 15:30:52 \Co~~kmetS..mpln\l01SSdill 

tj~\20100514\ftun 1' OJ940.51t:. 

S/1.V201D 15:)0:st (:\C•6cmt'tS.Iimpln\l0155d.al ~llt\20100514\ftun (0)941.511 

S/14/2010 1!di:G4 \CIIC~nU01S5cNI tik\l0100Sl41\Run 2_0l94UPl 

S/1'*11010 15:JI:10 C:\C*~\2<1155dal tA!\ZOl00514"'un 2 .. 0394).SPl 

S/14/2010 l>:ll:IO C:\Coi<MOISamo'nUOISScblllle\l010051 ........ 2_0l'I04.5H 

S/I.nG!O 15:)1·12 \CalcMt~\101SSdaltie:\20100514\Run2 ... 039tS ~ 511~10 l5:ll:21 t:\CKIM~\20155 dal .-e\20l00Slt'\R.,._ 2_03"'-SH 

5/1-t/2010 15:ll:U C:\C.tkMt~UOtSS elM tk\20100514\JIIWII 2:_0lM7.SPf 5/1~10 15:)1 41 C:\C*M~\S.IMI!Ies\2015~ doll t~\20100514\ftvn 2,.0JMI.SP£ 

S/14/1010 15:)1:417 C:\C.II'cm•tS.II"-J'Iti\20155 d•l tllt\20100S14\ft...n 2 .. 0Jt4t.SPE 

S/14/2010 15:)1:5) (:\C.acrneU..mplft\lDlS5 do~~l tilt-\20100S14\IIIun l .. OltsO.SPf 

5/14/2010 15:11:59 C:\CiftmC!tSampl~\20155 d.lll tllt\20100514\~un l_Oltst.SPf 

S/14/2010 15:11:05 (:\C•Icm•ISMiples\2DlS5do~~l til•\l0100S14\Ron l _0)9S2.SPr: 

S/14/2010 15';)1:11 C:\Co~~lemt1S.IImplt1\l01~5do~~ltjlc!-\20100514\Run 2_0)9SUP£ 

S/14/2010 IS:ll:17 C:\C..Icm•Wtnplf1\l01S5d•l ~tle\2011)0514\awn 2 ... 019$4 $~£ 5/14/2010 15:32:2) C:\C.lkm•WmplttU0155dll tj'e\20100'514\Rwn 2_0)9SS.St( 

5/14f/2010 15:31:29 C:\tlkm•tSatnplt"\lOlSSdll t._\2'0100514\ftun 2 .. 0JtS6.51E 

S/14/2010 15:31:31 C:\ti!IC:I'M1S.Irnple..\l01S5dll ~·\20100SI4\Run 2_0J9S1.Sft 

S/14/2010 lNl C:\Cole_,._\XI1SSd" ... \l0100514\0un 2_0,...-SH 

S/14/2010 15:12;41 GIIc:IM~ft\20155d..lll tile:\20100514\J'un 2 .. 03959.SPI 

S/1412010 15:ll."S4 C~~U015S cUt tit'U010CI51t'\Run 2 ... 0l960.SH 

S/14/2010 15:lJ:OO C:\CMMt\Saw.ples\20JS5 dM tie\20100514\RW~l ... 0)"1.sPf: 

S/14/2010 lS:JJ:06 C:\(*"'tCS..piH\l01S5 d.lll tilc\20to0514\R""l ... OU62.SPt 

S/14/lOlO 1'5:J);l1 C:\Co~~tcmt~•.,ln\20155 doll tilr\20100514\RUA 2 ... Dl96U,.t 

S/14/lOlO 15:)):18 (:\C•km•U..Mpi~K\201SS dtl1ilt\20100S14\ft"'" l Olt6UPf 

5/14/2010 15:33:2S C:\Co~~lcrnetSMipiiH\20155 d•l tilt\20100514\ltun 2-OlMS.SPf 

S/1-4/2010 15;)3:)1 (:\CIItmetS.IIntples\lOlSSd.tltii~\20100S14\Itun (03H6.SPf 

S/141/2010 15.:33:11 C:\C•IcmetS.IImpln\2015Sdo~~l 

~1&\20100514\kon Z .. Ol967.S~f S/14/2010 15.:)3:'*3 C:\C.Ic:met.S.IImple~\201S5do~~l Ule\20100514\llon l,.OlMI.SPf 

S/14/2010 1S:ll~419 C:\C.Ic:rn.t.Sampi~\:KI155cWI 

tl~\201005141\fton l_039M.SH 

S/14/.2010 15:ll:SS \C..kmtt$1mpln\201SSd.lti~\20100514\Rwn l ... OJ970.SI't 

S/1.-/2010 15:14:01 C:\C.IIkiMWmpfes\101S5dal t.r.e\20100!114\Run 2_0)971.S'( 

S/141/2010 IS:l4:07 C:\C.IIkMtlSM'nl)lts\201S5daltifll!'\20100!114v-un 2 .. 0J91UI1 

S/U/2010 15:J.4:U C:\CMMC~\20155 d.lll t~\20100514\Run 2_0J97l.SPE 

SIU/1010 15:34::20 \C.IIk~\lOISS chil t~\l(ll005l~un l .. Ol914.$1'E 

S/14/2010 IS:lt::Z6 \C~\10155 cW tle\20100Slof\llt.lft 2_0J91S..SPE 

S/1</2010 15~)2 C:\C*""'-UOlSS ... t .. \20100S1 ...... 1,0lt16_... 

5/1<4/1010 15:Jt:lt C:\CIIcmet~\2D1S5 d.ll tilt\20lCI:IS14\AIIIft l .. Olt77.sH 

S/141/2010 15:34:otol C:\CIIc.rne-tS.Iilnplel\lOlSSd.ll t .. \20100S14\kun l.Olt11 SPf 

'5/14/2010 l5:)4:SO C:\C•Ic:metS.Iin'tplel\20155do~~l tile-\20100514\ltun l .. Olt19.SPf 

5/14/2010 1S:lot:S6 \C.Ic:met.Sam~n\2015Sdo~~l ble\20100514\):un 1 .. 0391CUPf 

5/14/2010 1S:lS:0.2 C:\C.Icrnet.Sempln\20155d•l ble\20100514\Run l . OlMl.SPt 

5/14/2010 15:)5,:01 C:\C..Itrnt~mpln\2015ScWI tlle\20100S141\Run 1_0)91l.5Pt 

S/14/2G10 15:1!1:15 C:\C.IIk.Mt~mpln\20155d•l tik!\20100514\Run l ... Ol913.5Pt 

5114/2010 lS:lS:ll C:\C.IIIuwunS•mpfHU0155dal tile\20100SI4f\Run l_Ol914.SH 

S/14/2010 1S:lS:l7 C:\C.IIkmetS.."'I)IH\20155 dfl tile\20100!114\Rwn l ... Ol98S.SPf 

5/14/2010 15:15;33 C:\CIIC.mtt.sMII)Ies\20155 dal ttle\20100S14\Run 2_0l986.SI'E 

S/14/2010 15:l5:3t C:\Cikmc~\l01SS d.lll tile\l0l00514\,Run 2 ... 0l987.5P( 

S/14/1010 15:JS:45 C:\C·mct~\201SS ct.! tileo\l0100514\ftU~A l_OltN.SI'E 

S/14f/20l0 15:35:51 \CMcmt~\201S5 

dfltM\20100514\R~ l .. Ol919.SPE 

5/l-4'20t0 1~57 C.."\CMC:mt~\201SSd.lllt.i&eU0100514\AUft 1_0lt90.SP£ 

S/14/2010 15:l6.:0J C:\C.IIkmtt~\20155dM lit'\20100'S14\Run Z ... OJ99l.SP( 

5110/2010 IS~10 C:\C~U01SS ... I<Ic:\20100Sl4\ltun 2_01992.SP£ 

5/14/2010 15:36:16 \C.k.IM~\201SSdal tll&\20100514\ltun 2 .. 019tJ.Stt 

5/14/2010 15:36:12 C;\CIJkm~lSMnpiH\2015Scbl 

tlle\l0100Sl41\RU~t l ... OJ9H.St[ 

!t/14/2010 1'5:36:21 C:\CM:m~tSAMple,\lOJSS dM rile\20100514\Run 2 ... 0JttS.SI't 

5/141/2010 15:l6:M C:\Codcm~ts.mple$\20155 dalliiii!'\20100S141\Ron 2_0l996.SH 

5/141/2010 1'5:31:50 C:\CIItmtt$.11Mpl('s\lOISS dal Ult!\.20100514\Run 2 ... 0l997.$1'1 

5/14/lOlD 15:38:51 C:\CIIcmetS..Mplcs\l01SS dllllle\201005141\flu" 2 OJ9ti.SPI 

S/14/2010 15:39:52 C:\CIItrn•ts...m~e-s\20155 del tlle\20lDOS14\Piw" (oJ9tSI.SPE 

5J14hOtO 15:40:!.3 C:\CIIc.met.S.Implts\201S5 del tile-\20100S14V!un 2 040CXUPI 

S/141/2010 15:•41:5'* C:\CIIun•tS.IIMPtti\20155 dll Ule\20100514\Run z:04001.SPE 

S/14/2010 1!1 :4f2:5ot C:\Cak:MetS.IImp~\201SSdlllile\20100514\lt~.~n 2_0400l.SPE 

5/141/2010 15:4):55 C;\CMIIIIetSM'npats\201SScbl tlle\20100514\ltun 2.04003.$Pt 

5/14/2010 1S;44:s6 ( ;\(MtMtSMI'\pft"'\lOlSSd.ll riJe\2010051~"" l 04004 W[ 

S/14/2010 ~:57 C:\C*me~\2015Sd.tllile\10100SI4\IUtll OtOOS Vf 

!l/14f/l010 15:46:57 \C~\20155 diltlt'\20100514\lllun 2_01006.51( 

S/14f/ZOIO 15:41:'5.1 C:\C~\l'OIS5 d.lll tile\20100514\,ltun l_cMCX)1.SH 

17.56-vol""-

11.4 vol·" 

17.4 vol·" 

17.15 VOl·" 17-~vol·" 17.SS 1'01·" 

17.74 .,. 

17.61-.d-" 

17.46\JCII." 

11.21 \do" 

17.29 vof·" 

17.4 1'01·" 

17.14 vol·" 

17.11 vol·" 

17.01 vol·" 

17-04 vol·" 

17.13 VOl·" 

17.04 VOl·" 

17.03 \'OI·" 

16.,1 \'01·" 

16.95 YOI-" 

1'-g vof." 

16.19 -" 16.&svd-" 

15.95 \*Cif." 

11.17 '#01-" 

17.S2 \1101·" 

11.15 ¥011·· 17.gl~·" 11.1 .. YDI·" 

17.75 wf." 

11.72 vol·" 

17.63 vol·" 

17.65 vol·" 

17.83 vol·" 

17,73 vol·" 

U .J&vol-" 17.95~" 17.9YOI-" 

17.1 val-" 

n..tsvof." 

17.36 vd-" 

17-38 \1101·" 

17.16 wei·" 

17.74 vol·" 

11.64 vof·" 

17.1 vol·" 

11.64 vol·'% 

17.7l vol..,.. 

17.99 vol-" 

17.8) vol-" 

17.66'¥0l-" 

l7.6S wt4 

11.06 YoH5 

11.11-..ol-" 

11.-41 .,. 

11.'*1 vol·" 

1&.4g \1101·" 

11.64 ld·" 

18.7 Yd·" 

11.6) vol·" 

18.67 vol·" 

11.65 vol·" 

11.94 wl·" 

1t.1 vol·" 

1g.27 vol·" 

l9.27 '¥01"' 1g.lv~" 19.22-" 

19.18vd-" 

lt.l6 \*Cif." 

11.99¥d·" 

11.91 vol·" 

11.87 YDI·" 

18-85 vol·" 

19.4S vol·" 

22-0Svol·" 

19.Sl VOl·" 

l9.26-vol-% 

1928 vol·" 

19.-46 YDI·" 

1t.21 li'Of." llvol-ll 19.2S tod-" 

19-29 ¥01·" 

1g..l6 YDI·" 

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0.0042 

0.0041 

0.0Gt5 004~ 0.004) 

0.004S 

0,004) 

0.0041' 

0.0041 

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O.O!M 

0.0041 

0.0047 

0.0042 

0.0045 

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0.0046 

0.0046 

o.mn 

0.0046 0.004~ 

0.004A 

0.004S 

0.0046 

0.0046 

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O.O!MS 

0.0047 

0.004A 

0.0046 

0.004) 

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0.0041 

0.0047 

0.0047 

O,OG4S 

0.0044 

O.OG41 

0.0041 

0.0044 

o.D046 

O.O!MS 

0.004) 

0.0006 

O.D049 

0.005 

0.005 

0.0041 

0.005 

0.0046 

0.0047 

0.0041 

0.005 

0.0051 

O.OOS1 

0.0052 

0.0049 

0.0051 

O.OOS1 

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ODDS1 

O.OOSZ: 

0.0049 

0.0051 

O.DDS1 

O.OOS1 

0 .0042 

ODDSl 

O.OOS1 

O.DDS2 

O.OOS2 

00051 

O.OOSJ 

O.OOSZ: 

0.0052 

O.OOS1 

pp

11.19 ppm 

U.4 ppm 

11.13 ppm 

U.24ppm 

11.16 pp~n 1l.07 pPIIt 

U-1SC»P"' )41 41~ ·=- 15.06 PPM 

19.71 PPM 

11.01 ppm 

15.19 ppm 

14.16 ppm 

16.1 ppm 

14.82 PP"' 

U.l? ppm 

17.61 Wfl 

16.66f)pn 

17.9S ppm 

11.llpem 

14.75 ppm 

11.l6pll)m 

14.11 PIW" 

ll.19ppm 

11.69 pPm 

12-93 00. 

9.241 l)l)m 

11.24 ppm 

11.7 ppm 

ll.01 ppm 

11.51 ppm 

11.17 ppm 

10.81 p~ 10.19 ppm 

10-9ol PP"' 

10.51 ppm 

10.44 Pill"' 

l0.16ptWn 

ll.19ppm 

12 ..... 

11.16ppm 

11.()4ppm 

9.27 ppm 

U.S2 PDITI 

11.08 1)1)1"1\ 

12-06 Pt:~m 9.54 PPM 

9.14 ppm 

1.&4 ppm 

8.tl ppm 71~ 

9.) PPII' 

9.0. .... 

ua..., 

t.17 PP"' 

9.99-

1.8611P"' 8.47~ 5.62 ppm 

1.25 ppm 

6.66 ppm 

7.11 ppm 

7.75 ppm 

6.01 PPM 

8.04 ppm 5~ 

9.62 PPI"' 

1.26 ppm 

S.ll ppm 

5.91 ppm 

10.54 pprn 

7 ... ppn 

1.81 ppm 

1.73 ppm 

6.&g ppm 

17.94 ppm 

8.61 ppm 

11.48 ppm 

9.44 ppm S9p~ 

6.42 ppm 

S.l7 ppm 

6.04 ppm 

5.42 PPT' 

7.69 ppm 

pp

O.OOs-4 12.01 pll)fll 

0.005:2 10.6) 11)1)11'1 

0.0049 10.71 pll)lf'l 

0.0049 10.41 ppm 

O.OOH 10.79 ppm 

0.0059 10.t1 PCifl'l 

o.ooe 10.11 ppn 

0.0061 12.2 ppm 

o.001 ua..., 0.0072 11.91 ppm 

0.0(>12 10.62 .... 

0.0069 U .9l ppm 

0 .1)0619 .... , ppn 

0.0011 12.62 ppm 

0.007 11.22 pptn 

0.0061 10.01 ppm 

0.007 Sl.otl """ 

0.006t I .U pp-n 

0.007 11.47 ,_ 

0.0071 JO.O ppm 

0.007) 12.27 .... 

0.0016 11.1. ""' 

0.0013 • .) ... 

0 0071 9.$.4 OOM 

0.0062 10.07 ps0.0057 10.)5 PP"' 

1).01)56 7.99 PP"' 

O.OOSJ U .SI pp~t~ 0.0054 ll.l6 ppm 

0.0051 12.09 PP"' 

0.0053 g,U PP"' 

O.OO!.l: 10.95 p~ D.OOSJ 10.6S ppm 

O.OOS2 U .U ppm 

O.OOS3 1 .12 ppm 

0.00!15 10.71 ppm 

O.OOS2 10.94 ppm 

0.0051 1062 .... 

O.OOSl 12.16 ppm 

O.OOS2 10.61"""' 

0.0054 9.) .... 

0.0049 11.)9 p;wn 

0.00'52 9.4tppm 

O.oo52 11.21 ,.m 

0.005 •. 12 ppm 

0.005 11.0!1 ppm 

O.OOSl 11.12 ppm 

O.OOS2 8.64 ppm 

0.0051 10.11 PPM 

0 .0048 •.• pll)fll 

o..oos 11.$9 .,., .. 

O.oGtl tO.tl .,.,_ 

o.aos 9.07 PCIM 

0.005) 12. 7~ 

0.0052 U.l PP1P1 

0.0054 u ... 1 PP"' 

0.0052 10.76 PP"' 

0.0051 U.57 ppm 

O.OOSl U.&& ppm 

0.00$4 U . 1 ppm 

O.OOS4 11.9 ppm 

o.oosl 1US.pm 

O.OOSl 8.69-

0.00SJ 11.91 ppm 

0.0054 U .419 PP"' 

o.oosa u.24 II)Cin\ 

0.0056 14 11 ppta 

O.OOS1 U.63 .,.... 

O.OOS4 tl.l9ppM 

D.cm5 44~ 

0.0055 U~ 0.0057 1.12 ppm 

0.00!15 11.66 ppm 

O.ODS5 9.71 PPfl"' 

0.0054 U .SI PPfl"' 

O.OOS6 U.64 ppm 

0.0044 7.9-4 ppm 

0.006 U .l1 wn 

0.0062 12.!.1 ppm 

o.oosa tl.l4 ppn 

0.0056 U .61 PPM 

O.OOSl 11.98 PPM 

O.OOS!I 11 14 ppM 

O.OOSS ll.OI PC1M 

0.0051 11.14 ppM 

O.CXM U .Ol pp.-

0.006) 

0.0068 

0.0067 

0.0066 

0.0072 

0.0064 

0.!1069 

0.0061 

0.007 

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0.0009 

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0.0064 

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0.0069 

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0.0067 

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0.0064 

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0.0075 

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0.0066 

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0.0071 

0.0071 

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0.00)'5 

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0.00)6 

0.0042 

0.00)9 

0.00)9 

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0.0011 

0.0041 

0.00)5 

0.00)7 

O.D041 

0.00)7 

0.00)7 

O.DO.JS 

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0.00!1 

0.00411 

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0.0045 

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0.0041 

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0.0009 

0.00:16 

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0.0047 

0.0045 

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0.0042 

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0.004) 

O.D04l 

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0.0041 

0.00 .. 

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0 .0017 

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0.00) 

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0.0047 

0.004) 

0.0042 

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pp

pp

S/14/2010 16~;U C:\l:tt:m•tSaomplts\lOlSS dil tilt\20100514\ltun l_O.Ol7.SPE 22.91 vol-" .... 0.0046 11.99 ,ppm 0.0044 9.01 ppm 0.0061 Oppm O.GOll 

5114/2010 16.-09:U C:\Calcm•tSaompiH\201SS dillilt\20100S1~un l_040li.SPE ll.2 vol-" wot 0.0046 11.77 PSlM 0.0045 9.98 ppm 0.0061 Oppm 0.0018 

S/14/2010 16:10:14 C:\t.llcm•~mrift\l015S d•l \fle\20100514\Run 2_(H029.SPf :ZJ.U¥01·"- .... 0.0047 14.0S PP"" 0.00ol8 10.17 ppm 0.006ol Oppm 0.004 

5114/2010 16:11:1• C:\Calcmt\Sallftple-s\l01S5 dal tlle\20100S14\Run l _01030.$Pt: 13.44 "0'·" ""t 0.00ol8 17.11ppm 0.005 10,17 ppm 0.0064 o..,. O.OOI'l 

5/14/1010 16:1l:lS C:\c.tcm•t.S.I...P4:S\l0155 ~ tiltUOI<0$14\Itun 2_1)10ll.SPt: 23.49 VOl•" ... t O.OOota 11.07 PPM O.ClOM 9.16ppm 0.006 Oppm O.OOll 

S/14/2010 16:13:16 \(.Mm~~t.S.I,..P4:'1\101SSdal tMe\10100S14\Run 2_0oi0Jl.$Pt: 12.91vol-" ... t 0.00ol6 10.59 PP"' O.ClOM 8,63 pt)lll O.OOEa o .... O.OOlS 

S/14/1010 16.:1~17 C:\C.acrNt.Sa~\lOIS!.ct~ Cile\10l<IOS14-Vtun l_o.o.n.sn 22.UYOI·" 

- 0.00ol6 15.91 PP'I- 0.~ t.ll- 0.0063 0- O.f0l2 

5/14/1010 16:tS;1S \CMIM~U01ss clll t~~eUOl<IOS14\Il"" z_C)t())ot sn 21.1.2: 1101·" 

- 0.00ol6 16.19 PP't .. ~ t.lS- 0.0069 o .... 0 ... 37 

5114/2010 16:16:11 C:\Cak:Mtt$.tMp&e1\l01SS ~ tk\l0100514~WA l_CMOl\ SH 11.98-

- 0.0006 1S.24 PP" o.ooso t .41 PP"t ...... 0- O.OOol 

5114/2010 16:17:19 ~Mt~\20155 dill ttle\20100S14\AVIA2_040)6.5P£ 2286-

- o ..... 16.11 ppill 0.005) 9.ll PP"' G.006II o .... o.eo)ol 

5114/2010 16:11::10 C!\Cak:Mtt~\201SS d.e tlle\20100Sle\ltwn 2.040l7.SI't 22.58 '"""' 

- 0.0006 14.74 PP"' 0.005 ....... 0.0064 OppM o.eo:u 

5/14/2010 16:19:21 C:\CH:Mt\Sirnplt1\201SS d~ tlleUOJOOS14\I'un l . 04011.5Pl 2286vol·!l -· 0,0045 16.39 PP"' 0.005 9.11 ppnll 0 .0061 0 ppm 0.00}1 5/14/1010 1':20:.U C:\CakmotS-amplti\201SS d~ tiiii!'\2:0100514\Jiun l)MOlSI.Sf( ~~. ...... " -· 0 .004S 1S.69 ppm O.OOS4 1.7) ppm 0.0064 0 ppm 0.00!1 5/14/1010 :21:2 C:\Ca1C:meW.mplt1\l0lSS dJJ tH11!\l0100S14\I!:"n l_04040,SI( 22!9 vol·!l -· 0.004S 16-76 ppm O.OOS4 I .J PP" 0.0066 0 ppm 0.00)5 S/14/2010 16:22:23 C:\Calcme tSampln\l015S dill tilt\2G100S14\ftun l _Oo1D41.Sfll ll.16YOI-" ... t 0.00ol5 14.41 ppm 0.005! 1.05 ppm 0.0064 0 ppm 0.0012 

5/14/2010 16:21:23 C:\C•tmets.ampln\20155 dill tilt\20100514\Run 2:,.041042.Sfll 11.51 val-" .... 0.0045 15.4 ppm 0.005) 9.1 pl)m 0.0066 0 ppm 0.0015 

5114/2010 16:24:241 C:\CJfcmet.S.empln\20155 dill tilt\20100S141\Run 2_040U.Sf'l 22.37 .at-" wet 0.0044 16.5 ppm O.OOS) 1.)1 ppM 0.0066 0 PPM O,OOll 

5/14/1010 l6:1S:25 C:\C•Itmll!'t.Simplts\20155 diilllilt\20100514\Run l_0404C.SPI 22.07 voi-'K wtt 0.0044 15.47 ppm 0.0049 9.06 Pt>M 0.0067 0 ..... 0.00!1 

5114/2010 16:16:26 C:\CakmetSample-s\20155 dallilt\20100514\Run 2_010-tS.SPI!! 22.04 wl-" Wtl 0.0044 14.75 ppm 0.0051 1 .2 .... 00065 0 ppm 0.00)ol 

S/14/1010 17~26 C:\C.tc:m• t.S.I"'plft\20155 dal ti!e-\l0100S14\Run l_OI046.SPt: 12.0) wi·'K Wtl O.OOoll 14. 14 ppm O.OOSl 7.)5- 0.0062 0 ppm 0.00)) 

5114/2010 l~l7 \C.kmtts.•Pe-s\201SSct.~•\20100514\lltun z_o.on.m 21.61 wa-• w•t 0-) 15.8 pcwn 0.0051 7.tJwn 0.0064 Oppm 0.00)2 

S/14/2010 16:lt-21 "*~\lOISScbl ftle\lOt<IOSt~ 2_040d.SPf l,.S6vof-." -t 00054 ).19ppm 0.006 u. .. wn 0.0071 Oppm 0.00ol5 

5/14/2010 100:11 ,'ttok~\lOIS5dollifo\lOIOO>lol'"'"' l_OOOoi9.SH 19.18 ... ,. -· 0 .0051 .t.7Soom 0.0051 11.16wn 0 .007 Oppm O.OOrU 

AI/G 19-15 11.6) 10.55 000 
HCLDaJ-. 

Sm...s,IMdOMa 

O.Cc 

5/14/2010 

S/14/2010 

5/14/2010 

-hod 

320 

)20 

320 

FiltMmt HCI(-1 

2J.04 

lJ.7J 

n .69 

A"8-Cooc.(pl"")~ 

$<5 (ppm) 

o ... 

0.96 

o.,J 

I unl 

Su - Natift Cone. ot an•lyte 

Date 

5/14/2010 

S/14/2010 

5/14/2010 

Sm 

.. 

Of 

c. 

Cc 

Method 

J20 

no 

120 

Recowry "") • 

Ct • OF • Cs • SuCl·Of) 

U .lS ppm 

8.16 """ 

9.5"" 

200.8 ppm 

9.98 ppm 

u .•J PP"' 

Filename 

Sm • Su{l•Df) 

Of JCCs 

~CI(ppm) 

lS.I 

U9 

4.78 

Ava. COnt. {ppm)~ 

Sf& (ppm) 

0 

I . J 

MtiA COIKtftlf~tion of spik.cl .-llylt 

k•tiw conceatr•tion ol ~· 

Dilution Fector (T•1et < 10%) 

Cyl;odet<ll~ ,., 

Cykckf ol tfiCfl' liS (Sf6t 

bpec\H coaceau~tion o4 Matytto 

Rcc.....,!"'! 1ae.O?q 70 ·130" 

Spite dM.I SF6 

O.te llf'l'lt 

S/14/2010 

5/14/2010 

5/14/2010 

Spike d1t11 HCl 

04itc Timt 

5/14/2010 

5/14/2010 

5/14/2010 

N•tfw 0.111 HCI·.SF6 

D•t• nme 

S/14/2010 

5/14/2010 

S/14/2010 

SpecerumFtle: Wittr vapc Umt CoiRI)fl'sation Res•du•f 

16:14:21 C.:\CakmetS•mptes\10155 dal tik\20100514\wel scr..tt1Mr2 Sf6 Spike After Au-.:_~ \&.46 Vol·" wet 

16::W:27 C:\CflcmttSarnptn\2:01SS dM tH\20100514\Mtl scrutiiMrl SF6 Splitt Alter Avn 2_060f 16.48 vol·" ... 16:14;33 C:\CilcmetSa.rn.,les\20155 d-' tie~\20100514\wcl s.ctubberZ SF5 Spit(e Aher Run 2_0406 16.lS vo4·" ••• 

SputrumFile Witer ViP( Unit Compens.~tion Rcs.du•l 

16:ll:ll C:\C•IunetSamples\201SS dal tile\20100514\wet suubbtrl Hcl S,.ke After Run 1_040S 17.49 .... " ... 16:ll:l9 C:\C-iil(mttSJmples\201S5 dil ti1e\20100Sol4\wtt s.crubbefl Hcl $pikt Ahtr Run 2_040S 17.Z vol·" w•l 

16:ll:4S C:\C...IcmetS.ampJes\20155 dal tile\20100514\wet saubberl Hcl Sptke After fll.un 2_040S 16.77 vol-" wei 

Sptttrumfile W• ler VIP< Unit Co.m~n'l-llion Rnfdual 

16:lt:l1 C:\C.IcmtlSimple~oUOlSS del Ult\20100S14\Run 2_04047.SPE 21.61 vol-" wet 

16:29:21 C:\Calcme~mplts\201SS del rtle\20100!t14\Run 2_040U.SPE 

16:!0:21 C:\c.lcmets.atnples.\20155 dal tNe\20100Sl4\Run 2_00049.SPE 1U&¥01·" 

19.56 ""'·"' 

--· 

H~rocen d\lor Ul'lil Aa-sidull Hv*ocu nuori Ufliit "-achllll Sf6 Un~ Rasedwal 

0.004 ).5 ~,.. 0.0049 7.94 ppm 0.0059 O.t!. p,n 0.0042 

0.0041 s.•a P~ 0.0040 10.05- ppm 0.0057 0.96 ppm O.OOJI 

0.0041 6.95 PI"" 0.0048 9.2J ppm 0.0054 O.!Jl ppm 0.002& 

Hydrocen chlor Unh Rtsiduil 11vdroctn nuori Untt R.eiidull SF6 \Jnh 1\ntd ... l 

0.000 21.04 ppm 0.0051 9.7& ppm 0.007 Oppm 0.004 

0.004& 2t.7J ppm 0.0054 11.81 ppm 0.0066 O.OJ ppm 0.0044 

0.0044 ll.Upttm 0.0067 1.12 ppm 0.0075 0.13 ppm 0.0011 

Hydroctn <hfOrUnlt ~idu.l Hydroten fluoriUnit Res.idu•l Sf5 Unit Rtsidufl 

0.0043 15.1 ppm 0.0052 7;93 ppm 0.0054 Oppm O.OOJl 

0.0054 l .lt ppm 0.006 12 .... ppm 0.0073 Oppm 0.0045 

0.0051 4.71 ppm 0.005& U.Ui ppm 0.007 Oppm 0.0043 
HFOalbtlo 

Sm-$plllod0... 

Oot• 

S/14/2010 

5/14/2010 

5/14/2010 

Mol hod 

120 

320 

320 

Su - hlative COftc. Of an:a~ 

Dote 

S/14/2010 

S/14/2010 

S/14/2010 

Sm 

w 

Of 

(> 

c. 

Me thad 

120 

uo 

320 

FWcowry ('%) • 

Ce • OF,. Cs + SuCl-Of) 

23.5* l)l)m 

10.64 ppm 

U li li 

212.0 ptllm 

t .tl ~ 

29.47""" 

Ao<ovtry(li)c:: 

Sp bO~aSF6 

~ 

Filt,.~t 

Filtniome 

Sm • Su(t-1)1) 

OF.IICS 

A"'-COIIC. (ppm) 

Ave. Cone. {ppm) 

HF(ppm} Sf6 (ppm) 

21.23 o.n 22.1 0.99 

lO.•t o.u 

I 23.s.l I o.m I 

I 

Hf(ppm) 5" (ppm) 

7.91 

1U4 

1U~ 

10,UJ I 

Mun concenuation of sP'ked ~n~y1e 

Native contenlr41tion of ~n.alyt~ 

Oilutton Fact« CT1r1tt < 10%) 

o,tiftder ot ~piked cas 

Cybd<tt Qf tr~ ps (Sf6) 

Etpeaed COftCtfttution of anM,\e 

70· BOli 

0 

I 

Dot• Tom• ~cu~Ftle Water vapc. Untl Compensation Rtsi4u,l 

5/14/2010 16:U :-4S C:\c.kmet.Samplts\20155 dit tile\20100514\we' scrubkrl Sf& 5pikt After Run 2_040! 16.77 viM-% wet 0.00ol4 

5/1</2010 16:)1:51 C:\Calcm•tSamples\20155 d .. t"e\20100514\wetsttubMrl SF6 Spikt Afttr lun 2_0405 16.52 vol-% w•t O.OOtl 

5/14/2010 16:ll:S8 C:\Citcmet$ample~\..l01SS dal tilt\20100514\wtt scrubbcrl Sf' Spike Aher Jl:un 2_040! 16 ... ... ~."' w•t O.OOtl 

Spikt 0•~ HF 

5/14/2010 16:42:)2 C:\C..kmetSampiH\201SS dal titt\20100514\wet "crubbcrl HF Spike Ahtr R1.11"11 ,2:_0'J.U 25.77 vol·% w•t 0.0052 

S/14/2010 16:42:38 C:\CakmetSamples\101$$ d,-lil~\20100514\wet scrubbcrl Hf Spib After Aun J_04U· 2U~vol·li w•t 0.0051 

S/14/2010 16:42:.t4 C:\CalanetS..mples\201SS d.ttilt\2010051.\Wtt SC/IIbber2 HF 5pikt After Runl.04US 21.12 vol·" wtt 0.0052 

Native 0.11 Hf.SF6 

Date Time ~pectrumfil• W•ltt YiiiP< U•it Compen'Salion Re~dual 

S/1012010 16:2&:21 C:\CalcmttS-ilmptes\2015Sdal Ule\2010()5;14\Run 2_04047.SPl 21.61 VCJI·" wet 0.0041 

S/14/2010 16:29:28 C:\C.Icmei.S.JmplesU01SS dal tile\20LOOS14\Ru" 2_04048.SPE 19.!.6 \1'01·" .... 0.0054 

S/14/2010 1':30:2$ C:\C.Ic:meiSampfes\20155 dal tile\20100$14\Run 2 0404,.SPE 19.1& vol·" 

- 0.0051 

Hydroctn chlor Unit Res~ Hydroc~ fluor Unit Rtstd.wal SF& UM Rutctua• 

32.69 ppm 0.0067 1.12 ppm 0 .0075 0.9) ppm 0.00)8 

18.o& ppm 0.005 a.19 ppm 0.005, 0." ppm 0.0012 

U .6J ppm 0.00t9 7.91 ppm 0.0063 0.81 ppm 0.00) .. 

17.09 ppm 0.0056 28.23 ppm 0.0075 Oppm O.OOtl 

1S.2J ppm o.ooss 22.1 ppm 0.0067 0.02 ppm 0.004& 

11.6! ppm 0.0054 20.41 ppm 0.0072 Oppm 0.0044 

Hydro1en chlot Uni1 -.sidual HydtGit" Ruor U"it Rltsidual SF6 Unit Residual 

1$.1 ppm 0.0052 7.93 ppm 0.0064 Oppm 0.0012 

l.l' ppm 0.006 12.14 ppm 0.0073 Oppm 0.0045 

4.78 ppm 0.0058 11.16 ppm 0.007 Oppm 0.004J 
Dat~ 

S/14/2010 

5/14/2010 

5/10/2010 

S/14/2010 

5/14/2010 

S/14/2010 

S/14/2010 

S/14/ 2010 

5/14/2010 

s/1•/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

S/14/2010 

5/10/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/1./2010 

5/14/2010 

5/14/2010 

5/14/2010 

S/14/2010 

S/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

5/14/2010 

Time SpcQ,.urn~•le 

16:55:50 C:\Cokme<Somples\20155 dol <ilo\20100514lwe! stfubber 2 Run 3_04U6.SPE 

16:56:51 C:ICokme<Son.plesl20155 dol <llel20100114l..e< SO'ubber 2 Run s_04137.SPE 

16:S7:Sl' C:\C.Icmet~mples\201SS dJ~It ile\2 0100514\wet suubber 2 Run 3_04Ua.SPIE 

16:58:52 C:\Colcme<Sompl .. \20155 dol l~e\20100514lwel se.ubber 2 Run 3_04U9.SPE 

16:!.9:53 C:\Cakmct~mples\20155 d•ltil•\l0100S14\wet saubbet 2 Run l_04140.SPE. 

17:00:54 C:\Cokmnlomples\20155 dol l~e\20100514\we< oc:rubber 2 llun 3_04141.SPE 

17:01:54 C:\Cokme<Somplesi2015Sdol Ule\20100514\we< scrubber 2 11un 3_04142.SPE 

11:02:55 C:\Cokme<Sompios\20115 dol dle\20100514\wol scrubber 21tun J_04143.SPE 

17:03:56 C:\Cokme<Sompl.,l20155 dol <~120100514\-t 1CNbbef 21tun 3_04144.SPE 

17:04:57 C:\Cokme<Sompies\20155 dol <ile\201005141-• scrubber 2 Run 3_04141.SPE 

17:0S:SI C:IC.IO'ne<l....,.es\20155 dol Ulel20100514\wol Krubber 2 ~un 3_04146.1PE 

17:06:59 C:\CIIcme•Sample~\2015Sdallile\20100S14\wet scrubber l Run 3_04147.SPE 

17:07:59 C:\C.J,cme•Sample~\20155 daltlla\20100S14\wel scrubber l Run l_04141.SPl: 

17:09:00 C:\C.JicmelS.Jmples\20155 dal tile\20100514\wet scrubber 2 Run 3_04149.SPE 

17:10:01 C:\CakmetS.Jmples\20155 dal tilt\201005.14\wet scrubber l Run 3_041SO.SPE 

17:11:02 C:\CakmetS.JmP'es\20155 dal lil•\20100514\wel saubber 2 Run l_04151.SPE 

17:12:02 C:\CakmetSamptn\20155 d&llitl\20100514\wel suubber 2 1\un 3_~1S2 SPE 

17:13:03 C:\Cokmellompl .. \20155d•l dle\20100514lwel K<Ubbor 2 Run 3_04153.SPE 

17:14:03 C:\Cokme<S.mplu\20155 dol tile\20100514\we< saubber 2 R"" 3_04154.SPE 

17:15:04 C:\CokrMlSomplti\20155 dol <~\20100514\we< S<Nbller 2 R.., 3_04155.SP£ 

17:16:05 C:IC.kme<Somplesl20155 dol t~\20100514lwe< scrubbe< 2 R.., 3_041S6.SPE 

17:17:05 C:\Cokme<Sompiesl20155 dol <ilel20100514\we< >«ubber 2 Run 3_04157.SPE 

17:11:06 C:\Cokmell....,.es\20111 dol lllel20100514\we< S<Nbller l Run l_041SS.SPE 

17:19:07 C:\C•tcmetSan.ples\2015S d.al tile\2010051.\WH scrubber l Run l_041S9.SPE 

17:20:08 C:\Ca,cme1Simple~\201S5 daltilt\20100514\wet scrubber l Run 3_0U60.SPf 

17:21:08 C:\CalcmetS.Jmples\20155 dallilto\20100SU\wel saubber 2 Run 3_04161.SP£ 

17:22:09 C:\CakmetSampln\20155 dallile\20100514\wet scrubber 2 flun )_CM162.SPE 

17:23:09 C:\C.JkmetSamples\20155 dal Ule\10100514\wel sctubber 2 Run 3_0416.tSPf: 

17:24:10 C:\Cokme<Somplesl20155 dol lile\20100514lwel strubbor 2 Run 3_04164.SPE 

17:25:11 C:\C.kmetSo.!mples\201SSdalti'*\lOlOOS14\wltl S(l'ubber 2 kun 3_0C16S.SPE 

l 7:M:U C:\Cak:mel$;1mpln\201SS dll tife\20100514\wtl scrubber 2 k~ S_011166.SPE 

17:27:12 C:ICokme<S....plesl20155 dol <~\20100514lwe< oc:rubber 2 R.., 3_04167.SPE 

17:21:13 C:\Cokmn5omplesl20115dol <ile\20100514'\we< wubbor 2 Run 3_0416&.SPE 

17:29:13 C:\Cokme<Sompies\20155 dol 1~120100514\we< ouubber 21tun 1_04169.1PE 

17:30:14 C:\C.kme<Somples\20155 dol <~120100514\-• wubber 2 Run 3_04170.SPE 

17:31:15 C:\Cokme<Sompies\20155 dallile\20100514\we< saubber 2 Run 3_04171.SPE 

17:32:16 C:\CalcmetSamples\20155 dat tile\2010051•\wet scr~r 2 ~un J_04172.SPE 

17:33:17 C:\~lanetS.amples\2015S dal tile\20100514\wet scrubbet2 ftun l_0417).SPE 

17:34:1? C:\CalcmetS.Jmples\20155 dal tlla\20100514\wet Krubbtt 2 Run 3_0.174.SPE 

17:U:18 C:\Calc:met$,mples\201SS dal tilt\2010051•\wet st:rub~t 2 R~o~n J_0417S.SPf 

17:36:19 C:\Colcme<S•mplo•\2015S dol llltl20100514\wet s.:rub~r 2 Run 3_04176.SPE 

17:37:20 C:\Calc:metSampl~s\20155 dal tlle\20lll!Y..U\YIIL scrubber l Run 3_0.177.SPE 

17:11:20 C:\C.Icme<Somples\20155 dol tile\201005141-• s.:rub~r 2 Run 3_04171.1PE 

17:39:21 C:\CalcmetS~es\20155 daltile\2010051•\wel scrubbe, 2 Run 3_04179.SPI 

17:40:22 C:\C-<So"'PPes\20155 dal lile\20100514\wel St<ub~r 2 ~un l_04110.SPE 

17:41:22 C:\Colcnoe<So,.ples\20155 dol <ile\20100514\-• scrub~r 2 Run l_04111.5Pf 

17:42:23 C:\C-tSomples\20115 dol !~\201005141- scrubber 2 Run l_04182.SPE 

17:43:24 C:\C-tSomples\20155dol tile\20100514\- oc:rub~r 2 Run 3_04183.5Pf 

17:44:24 C:\Colc ... <Somplt$120155 dol <~\201005141.,., scrubber 2 Run 3_041U.SPf 

17:45:25 C:\Colcme<S.mplesl20155dollilel20100514lwel sa-ubber 2 Run 3_0411S.S'E 

17;46:26 C:\C::akmetS.mples\2015$ dalllle\20100S14\wet setubber 2 R.un 3.,.04le6.SPE 

17:47:27 C:ICokmolS.mpt.,I201SS dll <lle\20100514\wet scrubber 2 Run 3_04117.SP£ 

17;4.1:28 C:\C.Jkmet5.Jmpl~ts\201S5 da.l tilt\20100514\wet suubber 2 Run 3.,.04UI8.5PE 

17:49:21 C:\C31cm~tSimples\201SS d.JI Ule\20100514\we:t scrubber 2 ~n 3_04189.$PE 

l7;S0:29 C:\Oicme1S..mpl•s\201SS dal tlle\l0100SJC\wet sccubbet 2 Rvn 3_04190.SPE 

17:51:30 C:\Calcme<S.mples\20155 dol tilt\20100514\we< scrubber 2 Run 3_04191.1PE 

17:52:31 C:\Colcme<S....plos\20155 dol tilo\20100514\we< scrubber 2Run 3_04192.SPE 

17:53:31 C:\C.kme<Somples\20155 dol <~\20100514\wel scrubbe< 2 llun 3_04193.SPE 

17:54:32 C:\C.kme<Somples\20155 dol <~\20100514lwe< wubber 21tun 3_04194.1PE 

17:55:33 C:\Cokme<Somples\20155 dol tile\20100514\wet 1CNbbef 2 Runl_04195.SPE 

17:56:34 C:ICokme<Somplesi201SS dal tilo\20100514\wo< scrubber 2 Run1_041!16.SPE 

17:57:14 C:\C.kmel~$\20155 dol lilol20100514lwe< ..:rubber 2 R'"' )_04197.SPE 

AVG 

W.Jler Vi1p1UnJt 

19.S4 vol-% 

19.86 vol·" 

19.78 vol-% 

19.56 vol·ll 

19.28 vol·" 

19.77vol·ll 

19.46vol-ll 

19.47 ..... ,. 

20.03 ..... ,. 

19.91vol-% 

19.81 vol-"' 

19.72'1oJ·" 

19.77'4'ol·% 

19.83vol·" 

19.71 vel-% 

20.12 ..... ,. 

20.46 vol·ll 

20.26 vol""' 

20.3vol-% 

20.4 vol-!1 

20.54 vol-!1 

20.67 ..... ,. 

20.5.6 vol·" 

2'0.65 vol-" 

20.51 vol-" 

Z1 vol-% 

20.9 vcl4 

20.86 vol-% 

20.7 vol•" 

20.77 ..... ,. 

20.84 vol·" 

20.9vol·" 

20.94-..ol·" 

20.11 ..... ,. 

20.54 ..... ,. 

20.65 ..... ,. 

20.4& vol-" 

20.19 vol-" 

19.99 vol·" 

19.avol-" 

19.57 'f'Ol·" 

19.95 .... ,. 

19.7Zvol-!1 

19.94 vol-!1 

19.91 vol·" 

19.78 Yol·% 

19.82 vol·" 

19.65 vol·ll 

19.41 vol4 

19.17 vol-% 

19.23 Vol•" 

19.25 vol·" 

19.01vol·" 

18.85 vol-!1 

19.•6 vol·" 

20.36 ..... ,. 

20.51 ..... ,. 

20.19 ..... ,. 

20.19 ..... ,. 

20.12 .... ,. 

19.71 .... ,. 

19.67 vol-" 

20.05 

Compenn Residu.JI Hydropn thloride HCI Untt 

w.t 0.007 4.4S ppm 

we t 0.0072 S.33 pe~m 

wet 0.0072 4.67 pe~m 

w.t 0.007 •.68 ppm 

wet 0.0069 4.55 ppm 

..... 0.0071 5.02 ppt'A 

.,., 

-· 

--· .... 

wet 

we< 

wOl 

.... 

wo< 

.,., 

.,., 

-· 

--

--· 

-.,., 

we< 

Wtl 

.,., 

.... 

-· .,., 

.,., 

.,., -· .,., 

-· 

-· 

wet 

.,., 

.,., 

w•• .,., 

we< 

w•• 

-· .,., -· .... .,., 

wt< 

.,., 

.,., 

wet 

wet 

-· 

.,., 

-· .,., 

.,., 

.,., 

.,., 

.,., 

0.0071 

0.0071 

0.0072 

o.oorz 

0.0073 

0.0071 

0.0071 

0.0072 

0.0072 

0.0073 

0.0075 

0.0075 

0.0075 

0.0076 

0.0075 

0.0075 

0.0075 

0.0076 

0.0076 

0.0077 

0.0077 

0.0077 

0.0078 

0.0077 

0.0077 

0.0076 

0.0076 

0.0075 

0.0075 

0.0075 

0.0074 

0.0073 

0.0072 

0.0071 

0.0072 

0.0072 

0.0073 

0.0072 

0.0072 

0.0072 

0.0072 

0.0071 

0.0061 

0.0069 

0.0069 

0.0069 

0.0068 

0.0066 

0.007 

0.0074 

0.0074 

0.0074 

0.0073 

0.0072 

0.0071 

0.007 

5.19ppra 

4.13ppra 

5.7 ...... 

4.98 ppm 

S.ll ppm 

1.18 ppm 

5 ... ppm 

4.75 ppm 

4.69 ppm 

5.31 ppm 

5.42 ppm 

5.13 ppm 

53ppra 

5.13 ...... 

S.l2ppra 

6.31ppra 

5.64 ppm 

S.l ppm 

S . .J ppm 

4.91 ppm 

5.21 ppm 

6.17 ppm 

5.44 pe~m 

5.29 ppm 

5.52 PPft' 

5.21ppra 

5.15 ...... 

4.73 ...... 

4.91 ...... 

4.5 ...... 

5.05 ppm 

4,93 ppm 

4.7 ppm 

5.!7 ppm 

5.02 ppm 

~ ppm 

5.06 ppm 

5.06 ppm 

5.4ppm 

t.Uppm 

4.76 ppm 

4.09 ppm 

3.62 ppm 

S.Uppm 

3.57 ppm 

3.91 ppm 

•.09 ppm 

).24 ppm 

•.16 ppm 

5.06ppm 

5.3 ppm 

5.S1ppno 

5.15ppno 

5.01ppra 

S.51ppra 

• . 24 PP"' 

4.91 

Rn4du~l Hydroeen fluorid• HF Unit 

0.0003 5.5 ppm 

0.0004 5.97 ppm 

0.0004 

0.0004 

0.0004 

0.0003 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

o.ooo• 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0005 

0.0004 

0.0004 

0.0004 

0.0005 

0.0004 

0.0005 

0.0005 

0.0004 

0.000• 

0.0004 

0.0004 

0.0004 

0.0004 

0.0004 

0.0005 

0.0004 

0,0004 

0.0004 

0.0005 

0.0004 

0.0004 

0.0005 

0.0004 

0.0004 

0.0004 

o.ooos 

0.0004 

0.0004 

0.0005 

5.65 ppm 

7 ppm 

4.11 ppm 

6.83 ppm 

4.97 ppm 

5.73 ppm 

4.95 ppm 

6.31 ppm 

5.59 ppm 

15.41 ppm 

S.J-4 ppm 

6.4ppm 

6.05 ppm 

6.14 pprn 

6 ppm 

6.46 ppm 

6.04 ppm 

4.12ppm 

7.06 ppm 

5.76 ppm 

5.61 ppm 

1.02 ppm 

6.6tppm 

5.16 ppm 

6.02 ppm 

7.14 ppm 

6.68ppm 

5.&5 ppm 

6 .•7 ppm 

1.•2 ppm 

5.45 ppm 

S.'-4 ppm 

6.01 ppm 

6.11 ppm 

5.96 ppm 

5.56 ppm 

5.07 ppm 

S.46 ppm 

4.S4 ppm 

5.83 ppm 

5.16 ppm 

5.71 ppm 

S.9ppra 

us,... 

4.15 ...... 

4.51,... 

4.l7ppra 

4,37-

4.6 ppm 

4.42 ppm 

4.29 ppm 

l .S ppm 

4.17ppm 

5.59 ppm 

6 ppm 

5.71 ppm 

4.73 ppm 

5.25 ppm 

5.01 ppm 

5.21 ppm 

5.65 

1\esiduil SF6 

0.0048 

0.0049 

0.0049 

0.0049 

0.0041 

0.005 

0.0051 

0.005 

0.0051 

0.005 

0.005 

0.005 

0.005 

0.0052 

0.0051 

0.0051 

o.0054 

0.0054 

O.OOS4 

O.OOS4 

O.OOS4 

O.OOS4 

o.ooss 

0.0053 

0.0054 

0.0054 

0.0055 

0.0055 

0.0055 

0.0055 

0.0056 

0.0057 

0.0054 

0.0056 

0.0053 

O.OOS4 

O.OOS4 

0.0054 

0.0051 

0.0052 

0.0051 

0.005 

o.oos 

0.0049 

0.005 

0.005 

0.0051 

0.005 

0.0049 

0.0048 

0.0049 

0.0048 

0.0046 

0.0047 

0.0049 

0.0051 

0.0052 

0.0051 

0.0051 

0.0052 

0.005 

0.005 

Unft 

Oppm 

Oppm 

Oppm 

Oppm 

Oppm 

o,... 

Oppm 

Oppm 

Oppm 

Oppm 

Oppm 

0 ppm 

0 ppm 

0 ppm 

Oppm 

Oppm 

Oppm 

Oppm 

Oppra 

Oppra 

Oppm 

Oppm 

Oppm 

Oppm 

0 ppm 

0 ppm 

0 ppm 

Oppm 

Oppm 

Oppm 

Oppm 

Oppm 

Oppn~ 

Oppm 

Oppm 

Oppm 

Oppm 

o ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

0 ppm 

Oppm 

Oppm 

Oppm 

Oppm 

Oppm 

o ppm 

0 ppm 

Oppm 

Oppm 

Oppra 

o,... 

Oppm 

Oppm 

Oppm 

0 ppm 

0.00 

anidual 

0.0059 

0.0058 

0.0051 

0.006 

0.0057 

0.0051 

0.0056 

0.0057 

0.0051 

0.006 

0.0051 

0.0059 

O.OOS7 

0.0057 

0.0059 

0.0061 

0.0058 

0.0062 

0.0059 

0.0061 

0.0061 

0.0057 

00057 

0.0057 

0.0061 

0.0063 

0.0063 

0.0061 

0.0061 

0.0062 

0.006 

0.0059 

0.006 

0.0051 

0.0051 

0.0051 

0.0059 

o.005a 

0.005a 

0.0058 

o.o05a 

0.0058 

0.0058 

0.006 

0.0058 

0.006 

0.0059 

0.0057 

0.0056 

0.0058 

0.0058 

0.006 

0.0061 

0.0058 

0.0061 

0.0064 

0.0061 

0.0061 

0.0059 

00059 

0.006 

0.006 
HC~ Oalltalia 

Sm -SpUcod Data 

Oatt 

S/14/2010 

S/14/2010 

S/14/2010 

Method 

no 

320 

3~ 

f~ifn.tm• ~·pm) 

24.11 

24.62 

l4.lt 

sF6 (ppm) 

0.517 

0.96 

O.t7 

..... c-. """'lc:::::E!!] I o.ae11 

s..--co... 01.....,.. Date 

5/14/~10 

5/14/2010 

5/14/l010 

......... 3~ 

320 

320 

Fitltn..at HCI-) 

5.01 

S.S1 

2~ 

SF6 (.,...) 

0 

0 

0 

AVI. Conc. lppm}c::::::::!!!J I · I 

... 

s. 

DF 

c. 

c. 

~OW'!Y(%)• 

Ce • Of • Ci • Su(L·OJ) 

24.l2 ppm 

... 92 ppm 

200··""'" .8 ppm 

9.91 ppm 

23.19 ppm 

Sm·Sull·Ofl 

Ofl(s 

Rccowrvi"JI -~ 

SIH•tdata ... p, .. Ti<M 5~cttYMFM 

5/14/~10 l&ill:11 C:\(•kiMtS,...,...\20155o.l tio\201DOSI'\wtl scr..._l SF6 ..,.., - 3_04122.5'1 

S/14n010 11:02:33 C:\CaktMtSa•plln\201SS cW tH\ZOlOOS14\W'tt Ktubb« 2 SF5 ahH RUlli l_GUU.Sft 

S/14/2010 18:02:39 C:\CakrM~s\201SS dal tile\20100S14\wtt wubb« 2 SF6 HIH ltuA 3_0ot224.SPE 

Spikelata HCL 

Dole lii'N SpecUVMF'i~ 

S/1'/1010 18:0C:O' C;\C.tc:metSamples\20US ct.lt,.e\20100514\w.' Kl'\lbbtr 2 hclltter Run 3_04243.SP£ 

5/14/2010 18;~ 40 C':\C•IautSample:•\20155 da' c;ae\2:0100514\wtt wubbtr l hclllter Ruft l_04244.SPt: 

S/14/2010 11:04:~2 C:\CikJutSamples\201SS dallilt\20100514\wtl wubbltr 2 hcl alter lun 3_042n.SPE 

Nal~~ta, HCI-SF6 

Datt Tftt p•c:lrumfl~ 

S/14/2010 17:5S:l3 C:\C .. cmed.llrft~\20155 hlti'*\20100Slol\wtt scrubbtf 2 lun l_GU9S.SP£ 

S/14n010 11:$6:)4 \Calc.mttSa"'pln\lOlSSd~ tilc'\20100514\wt« u:rubbef l Awl l_ot19f.SP£ 

S/14/2010 17:57:14 \C~IaMtS•rRPIHU01SS d~ tM\2010051,\wtC scrubb4f 2 twn l_CM 197 .SPf 

..... coac:ftltration of~ ~Ntytt 

Mati¥91t0ft<alrJbon of .-n•fvl• 

Dilwfion hctor (hraet < 10.) 

Cyliftct.,ofspikl'dcas 

Cylinder of trKer aas.tSFf) 

hpecttd conctnlratlon ol ana~• 

70·130% 

WMttvapoo.t C~ns.a tion lll:t~ 

1U4vol·" .... 11.44 wd·" 11.42 tt~Gt·" 

-- Wattf v.poUnit C:o-pe.-wtion Atsidnl 

17.01 WI·" 

17.04 ¥01·" -... , 17.09 vol·" ... , 

Wlttr Vlpc:J Unit Compenution Rtttdual 

20.12 vot-" .... 1,,71 woa-" .... 1'.67 YO!~" 

-

ttydros:et~~ chkw \Mit "-sidual Hvdros:en ftuori Un" ~u~ SJ6 Un• Resiclu& 

O.OOS2 u .... o.ooos 2.95 ..... 0.00)1 0.97 ..... 0.0044 

0.0049 ).59 .... 0.0006 t.9ot PJft 0.0034 O.K ppra 0 .0047 

O.ocMt 2.5! .... o.ooos 2.95 ..... 0.0037 0.17 ppra 0.004 

Hvdrotcr. chlor Unie ~idu.. Hydroce• Auori Unit Rcsid<oal SF6 Unit Rc•ict.al 

O.DOS2 24.14 ppm 0.0011 1.93 ppm o.oon o..., .. 0.0067 

0.0055 24.,2 ppm 0.0029 3.87 ppm 0.0007 0 ppm 0.0071 

0.005) 24.1' PPM 0.0007 3.98 ppm O.OOS6 0 p;pm 0.0035 

Hydro1en chlof un•t R-u•• tfvdro&en fluori Unil ...,_idual SF' Urlil Rnldual 

0.001Z S.01 ~POl 0.0004 5.25 ppm 0.0052 0 pt>m 0.0059 

0.0071 S.SIPPOI 0.0004 S.08..,... 0.005 0..,... 0-

0.007 •.z• PP"' o.ooos .5.21 ppm 0.005 0..,... 0-
HF Dalltalia 

s .. -.sP'IIIed DMa 

.,.,. MtthOd ' icrtf,.., 5/14/2010 SlO 

S/14/2010 520 

5/14/2010 320 

AVI- COftL (ppm) 

s" - Natiw Con4;. Of •n.etvW 

.,.,. 

ou~ wchod 

5/14/2010 uo S/1'12010 120 

S/14/2010 320 

.... 

•• 

., 

,, 

c. 

a.eccwt"fy l"tt = 

Ce•Pf~tCJ•SYll-of) 

22.11 ppm 

s.ta ppm 

9-"'" 

21'2.0 ppm 

9.9a IDPM 

25.21 DPffl 

........ 11'11 ....... SplhD.ItiSI• 

Tinoe Spi!CtrumFfle 

-- Ayt. CoM. (ppm) 

ko~ 

111 • <-l 

5/1.!/2010 11:02~1& C:\Cetcmei.Satlq)lt'l\lGlSS d&l t.at-\20100514\w•t "'vbber 2 516 atter Run :t_04l22.SPE 

S/14/2010 18:02;)) C:\Cikmets.ampln\20155 dal tle\'20100S14\wtt .crubbtr 1 Sf' a.rttt Rvn 3_ou:a.SPf 

S/14/2010 11:02:l9 C:\Citcmn5arnpln\20as dill tlle\20100514\wtt "rubber 2 SF6 after Run J_04224.SII'f 

Spt.Ut>at~~ 

S/l4/l010 "' 18:00:56 C.:\Calcmc1$1n'l.,.fl\20US d1l tlle\lOlOOSl.t\""t suubba- l hf i!ftet ftun l_04209.SPE 

S/1.11/1010 1*:00 $~ C:\CIIkrM\SIMCiitS\20l~S dl4 titi!!'U<Il00$14\wc~ SCNbber 2 hf lfttt Jtvn )_Oi1210.SPE 

S/14/2010 18!01:01 ;\CIIIcnM:tSa~s\20JS5 dill t ... \20100$141\~c wubbll!t2hf~er 11Wn3_0llt1.SI't 

Nat""'* Data Hf·Sf6 

0111C r .... SptttJvmfNt 

5/t4noJo 17:55:lJ C;\Calemet.Sel'f\PIH\la155 dal tilt\20JDOS14\~Jrtrlt sc:t .. bbtt 2 Rul"'l_04195.SPf 

S/14/2010 17:56:34 C:\Caktntl.Samplfl\10155 dal tle\20i00Sl4\wtt scrubber 2 Run l_0419&.511'E 

S/14/l()ID 17:57;34 c·\QkmetSamptts\lOlSSdal tllt\20100514\wtt s.crubbtr :Z Run l_Odl97 ~PE 

HFtppm) Sf& (ppm} 

2).62 0.,7 

20.14 .... 22.SG 0.97 

c:=JmJ I Q.H7j 

... , .... , ... (Will 

s.n 

.... 

5.21 

c:::::::EJ I 

Mten concmtr1t1on of sp1led tnelyte 

Nnivtcoi'IUntratiOn of tntl'ytl' 

OlutiOf'l haor [hr&fl c l~) 

cytjndtf of~piked ~' 

CflincMf Of trlcer ps {SF6) 

bpect.-d tonu:nuaclion of en•~• 

70· 1)0" 

WI~VIpciUntt Comp .. nW(ion l!:n'dull 

ll.l-1\10 .. " ... , 11.44 vo~K w<l 

11.42 vol•" WOI 

17.Nvol·" wtl 

t7.0l ¥01·" W<l 

IUhol-" 

- W11tervapoUn.t co.._pensatbn Rts~ ... 

20.12 \10 ... 

19.71 voJ." -· 

WOI 

19." vol-% WOI 

D 

D 

I 

O.OOS2 

0.0049 

0.0049 

0.0064 

0.0041 

O.OOSl 

0.0072 

0.0071 

0.007 

HydfQCeft chiQf Unit 

4.1 PP"' 

"·"ppm 

'2.SJ ppm 

2.)? PP"' 

~ DPflll 

l.ll ""' 

HydrosetJ chlor Unit 

S.Ol PP"' 

5.51 PP"' 

4.24 ppm 

RHidual HrdJOpn tlvo Unit ltnidu .. SF6 """ lltsidual 

O.CXXJS ,.. •• j)no 0.0018 0.97 ppm 0.0044 

O.OD06 1.94p~ 0.0034 0.96 ppm D.oD47 

D.OOOS 2.95 Dpn'l 0.00)7 0,,7 ppm D.OD4 

0.0011 2!.62 ppm O.OOS2 O_ppm 0.0045 

D.OOD7 lO.t• ppm O.OOll o.-m o.ooc, D.ODD9 22-S6 .... 0.00)9 o.- O.OOSI 

Residuel HW"ckopn tluo Unit ltnldt.ial Sfi ""' lle~·· O.ooo4 S.25 ppm O.OOS2 Oppm o.ooso 

0.<>000 5.01Dpm ·- Oppm 

o.ooos 5.21 ppm DDDS Oppm D··-.OD6 
Oate Time Spec.trumFile 

S/14/2010 18:28:34 C:\ColcmeiSomplos\20155 d•l1ilo\20100SI4\ Hf ch sun Allor Run 3_04320.SPE 

5/14/2010 18:29:36 C:\C.Icmo1Somplos\201SS d•l tilo\20100514\ Hf cu sun Alter Run 3_0432t.SPE 

5/14/2010 18:30:25 C:\C.kmotSomplos\201SS d1l tile\20100S14\ Hf <U ..:on Aile< Run 3_0432HPE 

AVG 

Water vapor H20 Unit CompenMtion 

0 vo~% wot 

0 vol-% w.t 

o 1101-% wet 

Rosiduol ~vd<osen chloride HCI Un~ Residual Hvd<ocon fluoride HF Unft 

Oppm 

0 ppm 

0.024 ppm 

0.0014 217 19 ppm 0.0007 

o.ooss 

0 .0037 

216.92 ppm 

216.93 ppm 

217.01 

0.0007 

0.0005 

Residual SF6 Unit Residual 

0.0039 0 ppm 0.001 

0 .0042 0 ppm 0.0014 

0.0023 0 ppm 0.0016 
D<~te Time Spectrumfile 

5/14/2010 18:17:54 C:\C.IcmetS.mples\20155 dol tile\20100514\ HI cu san After Run 3_043U.SPE 

5/14/2010 18:11:57 C:\C.IcmetS.mples\20155 dol tile\20100514\ HI cu saon After Run 3_04312.SPE 

S/14/2010 18:18:14 C:\C.IcmotS.mplts\20155 dal tile\20100514\ HI cu saon Afttr Run 3_04313.SPE 

AVG 

WiitervapcUnit 

0 vol·% 

0 vol·% 

0 vol·% 

CompenS<ll Residual Hydroeen chloricUnit 

wet 0.0003 0.011 ppm 

wet 0.0005 0.016 ppm 

wet 0.0004 0.031 ppm 

Residual Hydrocen fluorid Unit 

0.0005 212.09 ppm 

0.0001 211.74 ppm 

0.0002 212.61 ppm 

212.15 

Residuol SF6 

0.0041 

0.0047 

0.0059 

Unit 

0 ppm 

0 ppm 

0 ppm 

Resi u~l 

0.009 

0.0013 

0.0007 
Date Tim~ SpectrumFil~ Water vapo Unit Compen52 Residual Hydroaen cUnit Residual Hydrogen I Unit Residual SF6 Unit Residual 

5/14/2010 18:10:13 C:\CalcmetSamples\20155 daltile\20100514\ 516 cts scan After Run 3_0427 0 vol·" wet 0.0026 0.02 ppm 0.0003 O.Dl ppm 0.0016 9.98 ppm 0.0027 

5/14/2010 18:11:19 C:\CalcmetSamples\20155 dal tile\20100514\ 516 cts scan After Run 3_042 0 vol·" wet 0.0021 0.04 ppm 0.0007 O.Ql ppm 0.0017 10 ppm 0.0014 

5/14/2010 18:12:24 C:\CalcmetSamples\20155 dal tile\20100514\ 516 cts scan After Run 3_042 0 vol·" wet 0.0028 0.02 ppm 0.0004 0.022 ppm 0.0012 10.06 ppm 0.0024 

AVG 10.01 
o.te Tomo Spt<tn•mfUe Wecerv•Un~ Carnp.ns~ fl:e~ ....,.01 ... chlotiM HCI "'"' Residul tt;cftoc• ftuoride Hf "'"' ... -.. Sf6 S/14/2010 11;07:10 C:\CMUM~\201SS dll \IM\20100S14\~ sattbM' l CTS ZEJIO aft.- Run l_OU6l.SPE 0.01_,. .... 0.0001 0.08"""' 0.0003 o ..... 0.0004 o..,. "'"' 

-o.ooll S/14/lOIO IS:OH6 \C-~\lOUS dol t;jo\20100514\we< .a-.. 2 CTS2£110 olte< .... l_00262.SP( 0.03_,. -· 0.0003 0.05"""' 0.0004 a PP"> 0.0006 Oppm 0.001 S/14/lOIO 18;07:22 C;\C--.tSI,mpJes\201SS dai •ilt\l0100S14\wet scntbMr 2 CUZEAO .t't~ IWn l_CM26l.SPE 0.01 ~ol·" -· 0.0002 .,_ ....... 0.0003 0.11Hm 0.0005 ..... o.oou 

AVO 0.03 0.06 

0

.04