Final Test Report for Dal Italia LLC Based on information and belief formed after reasonable inquiry,

I certify that the statements and information

in this test report are true, accurate, and complete.

I Permitted Facility Representative

I Date Name: Title: Company: Sign Date: Tuesday, September 07, 2010

I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate. **q&paS;5,.~~** Name: John T. Sutton Title: President Company

: Ent ec Services

, Inc. Sign Date: **~**
1 Z..o/ 10

Cj /l.o/1

0 Date Page

1 of 37FacilityInformation:DalltaliaLLC380IDaltileRoadMuskogeeContact:Mr.BobHurtPhone:Fax:Email:OK74401DalItaliaLLCTestingCompany:EntecServicesInc.16DConunerceAvenueHueytownContact:Mr.JohnSuttonPhone:(205)491-6676Fax:(205)491-6614AL35023Email:jsutton@entecservices.comAFS#:FRS#:lndustry/SCC/NAIS327122AirPermitNumber:2004-198-TV(M-1)PermittedSource10/Name:DalltaliaLLCPermittedMaximumProcessRate:Max.NormalOperationProcessRate:TargetProcessTestRatAttorneyClientPriviledgeSCCIDescription30500850IndustrialProcesses-MineralProducts-CeramicClay/TileManufacture-Firing-NaturalGas-firedKilnThefollowingstateandfederalregulationsthatapplytotheproposedtesting:I--RegulationDescriptionCompoundLimitUnitSection114oftheCleanAirAct(CAA)Metals0mg/dscmcorrectedSection114oftheCleanAirAct(CAA)TotalDioxins0grainsldscfcorrectedSection114oftheCleanAirAct(CAA)TotalFurans0grainsldscfcorrected-Section114oftheCleanAirAct(CAA)FilterableParticulate0mg/dscmcorrectedSection114oftheCleanAirAct(CAA)020percent(%)Section114oftheCleanAirAct(CAA)Co20percent(%)Section114oftheCleanAirAct(CAA)%H200percent(%)--Section114oftheCleanAirAct(CAA)TotalDioxins0ng/dscmcorrectedSectionI14oftheCleanAirAct(CAA)TotalFurans0mg/dscmcorrected-Section114oftheCleanAirAct(CAA)TotalDioxins0mg/dscmSection114oftheCleanAirAct(CAA)TotalFurans0mg/dscmDescriptionofthesource(includingcontrolequipment).Pleaseseetheattachmentsforsourceorprocessflowdiagram:SprayDryingandPreparedBodyStorageRawmaterialsweremilledtothedesiredconsistencyandviscositycreatingamudlikeslurrycalled"slip."Uponcompletionofthemillingprocess,theslipwaspumpedintoundergroundconcretetankswhereitwasstoredbeforespraydrying.Theslipfromundergroundtankswaspumpedunderhighpressureintospraydryerswhereitwasatomizedthroughspeciallydesignednozzles.Thenozzlesspraytheslipupwardswhilehotair,fromnaturalgasfiredburners,flowsdownwardfromthetopofthespraydryerchamber.Duringthisprocess,themoistureintheslipTuesday,September07,2010Page2of37DalltaliaLLCwasreducedtolessthanI0%andformsbodypowdergranulessuitableforpressingintovarioustileshapes.Duringoperation,thegranulescontinuouslyexitthebottomofthespraydryersandwereconveyedtobodypowderstoragesilos.Thehotairfromthespraydryerswasexhaustedthroughfabricfilterdustcollectors(EPN05andEPN36).SamplingwasperformedonSprayDryer#I(EPN05)usingReferenceTestMethod23.TileDryingThebodypowderfromthespraydryerswereformedintovarioustileshapesbymeansofhydraulicpresses.Whenpressed,thetileswereconveyeddirectlytoandthroughVerticalTheverticalfiredbynaturalgas,increasethetiletemperatureandreducethemoisturecontentofthepressedtilestoenhancetheglazingoperationandmakethemsuitableforfiringinthekilns.SamplingwasperformedonVerticalDryer#9(EPN32)usingReferenceTestMethod23.GlazeApplicationFromtheverticaldryers,thetileswereconveyeddirectlytotheGlazeLinesforapplicationofvarioustypesofsurfacecoatings.Eachverticaldryerwasconnectedtoitsownglazeline.Intheglazingoperations,thetilespassedthroughbrushtypecabins,spray-nozzletypecabins,and/orvariousothertypesofglazeapplicationstations.Multipleapplicationstationsarrangedinserieswereusedtoachievethedesiredsurfaceeffect.Forpurposesofthistest,thefacilitymaximizedproductionofproductsthatrequiresprayapplicationofglaze. Thesprayapplicationcabinswereconnectedtooneoftwobaghousesthatweredesignedtocapturethedrydustfromthebrushingaswellastheairborneglazeparticleslfomthewetapplicationprocesses.SamplingwasperformedonthedustcollectorforglazeIines7-10(EPN41)usingReferenceTestMethod29.FiringThedriedandglazedtileswerefedintofast-fireroller-hearthkilns.Inthekilns,thetiletemperaturewasslowlyincreasedtoover2,000degreesFandthenslowlycooleddowntolessthan150degreesFattheexitendofthekilns.Emissionsofgasesfromthefiringzoneofthekilnswerecontrolledtotwoseparatecausticwetscrubbersystems.Undernormaloperations,WetScrubber#1controlsemissionfromKilnsI&2andWetScrubber#2controlsemissionsfromKilns3&4.WetScrubber#2wasdesignedtoalsocontrolemissionsfromKilns2,3,&4intheeventofamalfunctionofWetScrubber#I.SamplingwasperformedonWetScrubber#2(EPN29)usingReferenceTestMethods23,29and320.SamplingLocationInformation:RoundDuctRect.DuctEquiv.NumberofTraversePointsJDistancefromDistancefromLocationDiam.Length/WidthSprayDryer7100GlazeLines3300TileDryer1700WetScrubber7200#2TestParameterInformation:IITargetLocationParameterGlazeLines%H20GlazeLinesFlowrateGlazeLinesNickelGlazeLinesrAntimonyGlazeLinesArsenicGlazeLines[BerylliumGlazeLinesCadmiumTuesday,September07,2010Diamupstreamdlst.1downstreamdist.0000TestMethodMethodI-4MethodI-4Method29Method2929Method29Method29400336126180144INumberofITestRuns33=33---3-335807580TestRunDuration240240--24024024024024022022428224SamplePointsComments0I0000-00Page3of37Glaze Lines Glaze Line
s Glaze Line
s Chromium Cobalt Lead -- Glaze Lines Glaze Lines Glaze Lines Glaze Lines Glaze Lines .--- . spray Dryer Mercury Selenium Manganese 02 Filterable Particulate Flowrate - %H20 2,3,7,8-TCDD I ,2,3,7,8-PeCDD I ,2,3,4,
7 ,8-Hx COD I , 2,3

, 6, 7 ,8-Hx COD I ,2
, 3,7

, 8,9-HxCDD I , 2 , 3 , 4 , 6, 7 , 8-HpCDD OCDD 2 , 3, 7,8- TCDF 1,2,3.7,8-PeCDF 2 , 3,4, 7 ,8-P eCDF 1,2,3,4,7,8-HxCDF J ,2,3

, 6,7,8-HxCDF 2,3,4,6,7,8-HxCDF 1,2,3,7,8,9-HxCDF I ,2,3,4,6, 7,8-HpCDF I ,2,3,4,7,8,9-HpCDF OCDF

- Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer **~pray** Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Spray Dryer Tile **Dry ~**  Tile Dryer
-- Tile Dryer Tile Dryer Tile Dryer Tile Dryer Tile Dryer Tile Dryer Tile Dry '- e _ r _ Tile Dryer Tile Dryer Tile Dry .!!: Total Dioxins Total Furans 02 Flowrate %H20 2 , 3,7,8

- TCDD 1 , 2 , 3,7,8-PeCDD I ,2,3,4,7,8-HxCDD 1,2,3,6,7,8-HxCDD 1,2,3, 7 ,8, 9-Hx COD I ,2,3,4,6,7,8-HpCDD OCDD 2,3

, 7,8-TCDF 1,2,3,7,8-PeCDF 2,3,4,
7 ,8-P eCDF 1 , 2 , 3,4, 7,8-HxCDF I , 2 , 3,6,7

, 8-HxCDF Tile Dryer _! ile Dryer Tile Dryer Tile Dryer Tile Dryer Tile Dryer

_ 2 , 3 , 4,6

, 7 , 8-HxCDF 1 , 2,3,7

, 8 , 9-HxCDF I , 2 , 3,4

, 6, 7 ,8-HpCDF - 1,2,3,4,

7 ,8,9-HpCDF Tile Dryer OCDF Tile D !l: er Total Dioxins Tile Dry .!!_

_ Tile Dryer Total Furans 02 Tuesday, September 07, 2010

Dal ItaUa LLC M ethod 29

3 240

0 Method 29

3 240

0 - Method 29

3 240

0 Method 29

3 240

0 Method 29

3 240

i 0 Method 29

3 240

I 0 Method 3A 02

3 240

0 M ethod
5

3 240

1 0 Meth od I -4

3 240

I 0 Meth od I- 4

3 240

! 0 Method 23

3 240

I r 0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0

I Method 23

3 240

0 - Me
t hod 23

3 240

0 Method 23

t

3 240

0 - Method 23

3 240

0 Meth
o d 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0

I Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

J 0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 I Method 23

3 240

0 I Method3A 02

3 240

0 Method I- 4

3 240

0 Method I- 4

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

I 0 Method 23

3 240

0 -

f Method 23

3 240

0 Method 23

3 240

0 --

o -r Method 23

3 240

- Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Method 23

3 240

0 Meth
o d 23

3 240

0 - 1- Method 23

3 240

0

- Method 3A 02

3 240

0 Page4 of37WetScrubberFlowrate#2WetScrubber%H20#2WetScrubber2,3,7,8-TCDD#2WetScrubber1,2,3,7,8-PeCDD#2WetScrubberI,2,3,4,7,8-HxCDD#2WetScrubber1,2,3,6,7,8-HxCDD#2WetScrubber1,2,3,7,8,9-HxCDD#2WetScrubber1,2,3,4,6,7,8-HpCDD#2WetScrubberOCDD#2WetScrubber2,3,7,8-TCDF#2WetScrubber1,2,3,7,8-PeCDF#2WetScrubber2,3,4,7,8-PeCDF#2WetScrubberI,2,3,4,7,8-HxCDF#2WetScrubberI,2,3,6,7,8-HxCDF#2WetScrubber2,3,4,6,7,8-HxCDF#2!WetScrubber11,2,3,7,8,9-HxCDF,#2I!WetScrubber11,2,3,4,6,7,8-HpCDF'#2WetScrubber11,2,3,4,7,8,9-HpCDF#2IWetScrubberDioxins#2WetScrubberjTotalFurans#2IScrubber/WetScrubber________,#2IDalltaliaLLCMethod1-43MethodI-43Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method233Method293Method293120120240240240240240240240240240240240240240240240240240240240240240I0I0I0I01-0-I_0000000000000I0IoI0I0I0IWetArsenicMethod29I3240l0r:etScrubberC-o-b-al_t_________,_M_e-th_o_d_2_9____1,--3--240-·--------·!#2Scrubber_fhromiumMethod-·29____I3___1_________,__ScrubberMethod29I3240I0ScrubberMethod29__!___---·---240___!___------Tuesday,September07,2010Page5of37DalItaliaLLCjWetScrubberMethod29I32400!#2!WetScrubberMethod29I324001#2IWet ScrubberMethod29I32400,#2IWet ScrubberCadmiumMethod29I32400t#2IWetScrubber02Method3A02I32400#2IWetScrubberrilterableParticulateMethod5I32400#2Thefollowingdescribesanymodificationsand/ordeviationstotheapplicabletestmethods.Ifalternativemethodswererequested,seetheattachmentsfordocumentationofrequestANDapproval,includingdates.Tuesday, September07,2010Page6of37DalltaliaLLCSamplingIStackDataResultsSummaryLocationGlazeLines-Method29AveraeRunNumberM29-1M29-2M29-3TestDate5/13/20105/14/20105/15/2010RunStartTime2:36:00PM8:17:00I:II:OOPMAMRunFinishTime6:26:00PM12:07:005:01:00PMPMNetRunTime,minutes240240240DryGasMeterVolumeSampled,dscf177.947180.417181.703180.022MoistureContentofStackGas,%2.301.932.522.250MoistureSaturationatStackGasTemperature,%2.942.803.222.987CarbonDioxide,%0.00040.00040.00040.000Oxygen,%20.820.820.820.800AverageStackGasTemperature,°F75.0473.9278.1375.697DryVolumetricFlowRate,dryscfin22,555.822,646.122,732.822,644.900ActualWetVolumetricFlueGasFlowRate,acfin23,504.623,180.323,586.623,423.833PercentIsokineticofSamplingRate,%101.3102.3102.6102.067F-Factor,dscfin/MMBtu@%020000.000Fw0000.000Fe0000.000LocationGlazeLines-Method3A02AveraeRunNumberI292-293-29TestDate5/13120105114120105114/2010RunStartTime2:36:00PM8:17:001:11:00PMAMRunFinishTime6:44:00PM12:26:005:18:00PMPMCarbonDioxide,%0.10.10.10.100Oxygen,%20.820.820.820.800DryVolumetricFlowRate,dryscfin22546226362272122,634.333F-Factor,dscfiniMMBtu@%020000.000Moisture,%2.31.932.522.250FuelTypeFw0000.000Fe0000.000Tuesday,September07,2010Page7of37Location Glaze Lines

- Method

5 Run Number Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas,% Moisture Saturation

at Stack Gas Temperature

, % Carbon Dioxide,
% O x ygen ,% Average Stack Gas Temperature

, °F Dry Volumetric Flow Rate, dry scfin Actual Wet Volumetric Flue Gas Flow Rate

, actin Percent lsokinetic of Sampling Rate

, % F-Factor, dsctin/MMBtu

@ % 02 Fw Fe Location Spray Dryer- Method 23 Run Number Test Date Run Start Time Run Finish Time Net Run Time

, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation

at Stack Gas Temperature,% Carbon Dioxide,
% Oxygen,% Average Stack Gas Temperature,

°F Dry Volumetric Flow Rate, dry scfin Actual Wet Volumetric Flue Gas Flow Rate

. ac tin Percent lsokinetic of Sampling Rate,% F-Factor, dscfin/MMBtu

@ %02 Fw Fe Tuesday, September 07, 2010

Dal Ualia LLC

Avera

e Avera

e Page
8 of 37LocationSprayDryer-Method3A02RunNumberTestDateRunStartTimeRunFinishTimeCarbonDioxide,%Oxygen,%DryVolumetricFlowRate,dryscfmF-Factor,dscfin!MMBtu@%02Moisture,%FuelTypeFwFeLocationTileDryer-Method23RunNumberTestDateRunStartTimeRunFinishTimeNetRunTime,minutesDryGasMeterVolumeSampled,dscfMoistureContentofStackGas,%MoistureSaturationatStackGasTemperature,%CarbonDioxide,%Oxygen,%AverageStackGasTemperature,"FDryVolumetricFlowRate,dryscfmActualWetVolumetricFlueGasFlowRate,acfinPercentlsokineticofSamplingRate,%F-Factor,dscfin!MMBtu@%02FwFeTuesday,September07,2010DalltaliaLLC1-235110/20109:05:00AM1:19:00PM21849227871022.53Gas-Natural106101040Averae2-233-235/11/20105/12/201010:57:007:55:00AMAM3:09:002:33:00PMPM2.522.16718.51818.167496725139650,098.333871087108,710.00022.7519.1721.483Gas-Gas-NaturalNatural106101061010,610.000104010401,040.000AveraePage9of37

### Location Tile Dryer- Method 3A 02 Run Number Test Date Run Start Time Run Finish Time Carbon Dioxide,% Oxygen,% Dry Volumetric Flow Rate, dry scfin F-Factor, dscfiniMMBtu@ %02 Moisture,% Fuel Type Fw Fe 

### Location Wet Scrubber #2- Method 23 Run Number Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Conte nt of Stack Gas, % Moisture Saturation

at Stack Gas Temperature,

% Carbon Dioxide,
% Oxygen,% Average Stack Gas Temperature,

°F Dry Volumetric Flow Rate, dry scfin Actual Wet Volumetric Flue Gas Flow Rate, acfin Percent lsokinetic of Sampling Rate, % F-Factor, dscfiniMMBtu

@ %02 Fw Fe 

### Tuesday, September 07, 2010 

### Dalltalia LLC 1-23 511512010 8:43:00 AM 12:50:00 PM 0.1 18.9 3580 8710 11.18 Gas

- Natural 10610 1040


### Avera

e 2-23 3-23 5 fl 512010 5116

/ 20 10 1:40:00 7:50:00 AM PM 6:12:00

11 :5 2:00 PM AM 0.1

0.1 0.100 18.8 18.3 18.667 3516 3559 3,551.667 8710 8710 8,710. 000 12.79 11.55

11. 84 0 Gas- Ga s - Natural Natural 10610 10610 10,610 .000 1040 1040 1,040.000 

### Avera

e Page 10 of 37

### Dalltalia LLC Location Wet Scrubber #2
- Method 29



### Avera

e Run Number Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas,% Moisture Saturation

at Stack Gas Temperature,% Carbon Dioxide,
% Oxygen,% Average Stack Gas Temperature,

° F Method 29 Method 29 Method 29 Dry Volumetric Flow Rate, dry scfin

0 .8 4

0 .8 4

0
. 84

0 .8 40 Actual Wet Volumetric Flue Gas Flow Rate, acfin 0.973 0.973

0
. 973 0.973 Percentlsokinetic

of Sampling Rate ,%
29.79 30.01 30.01 29.937 F-Factor, dscfin!MMBtu@ %02
148.450 144.974 133.031 142.152 Fw

141.373 138.518 126.157 135.349 Fe

81.81 80.88 84.79 82.493 

### Location Wet Scrubber #2- Method 3A 02



### Avera

e Run Number

1-29 2-29 3-29 Test Date

5 f l 3 / 2010 511412010 5/1512010 Run Start Time

9:35:00 AM

2
: 00

: 00

I 1: 43:00 PM AM Run Finish Time

12 :05: 00 PM 6:14:00 4:33:00 PM PM Carbon Dioxide,%

2.5

2

1.5 2.0 00 Oxygen ,%

18.6

19 18.8

18 .8 00 Dry Volumetric Flow Rate, dry scfin
49845 54349 51296 51,830.000 F-Factor

, dscfiniMMBtu@ %02

8710 8710 8710 8,710.000 Moisture ,%

16.13 16.35

16 .57 16.350 Fuel Type

Gas- Natural Gas- Gas

- Natural Natural Fw

10610 106 10 10610
10 ,6 10 .000 Fe

1040 1040 1040 1,040.000 

### Tuesday, September 07, 2010

Page 11 of 37

### Dalltalia LLC Location Wet Scrubber #2- Method

5

Avera

e Run Number

M29-l M29-2 M29-
3 Te s t Date

5 1 13 / 2010

5 / 14 / 2010

5 11 5 J 2010 Run Start Time

9:35:00 AM 2:00:00

11

: 43 :00 PM AM Run Finish Time

12:05:00 PM 5:50:00 3:33:00 PM PM N et Run Time, minutes

156 240 240 Dry Gas Meter Volume Sampled, dscf 141.373 138.518

126 .157 135

. 349 Moi

s ture Content of Stack Gas, %

16.13 16.35 16.57 16.350 Moi

s ture Saturation

at Stack Gas Temperature,

%

16 .3 5 16.52

16

. 91

16

. 593 Ca rbon Dioxide ,%

2.5

2

1.5 2.000 Oxygen,%

18

. 6

19 18.8

18 .800 Average Stack Gas Temperature

, ° F

132 .88 133.54 134.42

1 33.6 13 Dry Volumetric Flow Rate

, dry scfin 49,870.7 54,373.1 51,309.8 51,851.200 Actual Wet Volumetric Flue Gas Flow Rate, acfin 66,992.4 72,777.3 68,960

. 3 69,576.667 Percent lsokinetic of Sampling Rate, %

94.9 104.0 100.4 99.767 F-Factor, dscfin/MMBtu@ %02

0

0

0 0.000 Fw

0

0

0 0.000 Fe

0

0

0

0
. 000 

### Tuesday, September 07, 2010

Page 12 of 37

### Dalltalia LLC Emissions Summary 

### Location

: Glaze Lines- Method 29 Compound

: Antimony



### Averal!e Run Number

M29

- l M29-2 M29-3 Mass _ mg 0.000869 0.00032 0.0003
0.000 Eglhr

6.61 E-03 2.41E-03 2.25E-03
0.004 mg/dscm
1.72E-04 6.26E-05 5.83E-05
0.000 **m~dscm@7%02**

2
. 39£ -0 2

8
. 70E-03 S.IOE-03

0
. 014 

### Compound: Arsenic



### Averal!e Run Number

M29-1 M29-2 M29-3 Mass_mg

0.0012 0.0012

0 .0012

0
. 001 Egfhr 9.13E-03 9.04E-03 9.01E-03

0 .009 mgfd sc m 2.38E-04 2.35E-04 2.33E-04

0
. 000 **m~d sc~7~**  **o()2**

3
. 31 E-02 3.27E-02 3.24E-02

0
. 033 

### Compound: Berylliwn



### Averal!e Run Number

M29-1 M29-2 M29-3 Mass mg
0.0003 0.0003 0.0003
0.000 Egfhr 2.28E-03 2.26E-03 2.25E-03
0.002 mgfdscm 5.95E-05 5.87E-05 5.83E-05
0.000 **m~dscm@7**
**02** 8.27E-03

8
. 16E-03 8.10E-03

0 .0 08 

### Compound: Cadmium



### Averal!e Run Number

M29-l M29-2 M29-3 Mass_mg

0 .00027

1

0 .000 151 0.00015
0.000 Egfhr 2.06E-03 1.14E-03 1.13E-0

3 0.001 mgfdscm 5.38E-05 2.96E-05 2.92E-05
0.000 m lids cm@7 % 02 7.48E-03

4.1 IE-03 4.06E-03
0.005 

### Compound: Chromium



### Averal!e Run Number

M29-l M29-2 M29-3 Mass_mg 0.002393 0.002184

0
. 001392
0.002 Eglhr
1.82E-02 1.64E-02

1 . 04E-02
0.015 mgldscm 4.75E-04

4
. 28E-04

2
. 71E-04

0
. 000 **m~/dscm@7%02**

6 .60 E-02

5
. 95E-02 3.77E-02

0
. 054 

### Compound: Cobalt



### Averal!e RunNumbcr

M2 9- l M29-2 M29-3 Ma ss _mg
0.0003

0 .0 00464 0.0003
0.000 Egfhr 2.28E-03 3.49E-03 2.25E-03
0.003 m g/dsc m 5.95£-05 9.08E-05 5.83E-05
0.000 **m~d @7%**  **02** 8.27E-03

1 .2 6E-02 S.IOE-03
0.010 

### Compound: Lead



### Averal!e Tuesday, September 07, 2010

Page 13 of 37DalltaliaLLCRunNumberM29-1M29-2M29-3Mass_mg0.0015250.0015720.0010330.001Eg/hr1.16E-021.18E-027.75E-030.010mg/dscm3.03E-043.08E-042.01E-040.000mg/dscm@7%024.21E-024.28E-022.79E-02O.D38Compound:ManganeseAveralleRunNumberM29-1M29-2M29-3Mass_mg0.022020.040780.002770.022Eg/hr1.67E-O13.07E-Ol2.08E-020.165mg/dscm4.37E-037.98E-035.38E-040.004mg!dscm@7%026.07E-011.11E+OO7.48E-020.597Compound:MercuryAveralleRunNumberM29-1M29-2M29-3Mass_mg0.0004320.0001270.0001670.000Eg/hr3.29E-039.56E-041.25E-030.002mg/dscm8.57E-052.49E-053.25E-050.000mg!dscm@7%021.19E-023.46E-034.52E-030.007Compound:NickelAvera2eRunNumberM29-1M29-2M29-3Massmg0.0028550.0076380.0023780.004Eg/hr2.17E-025.75E-021.79E-020.032mg/dscm5.67E-04l.SOE-034.62E-040.0017.88E-022.09E-OI6.42E-020.117Compound:SeleniumAvera2eRunNumberM29-1M29-2M29-3Mass_mg0.003590.0030.0030.003Eg!hr2.73E-022.26E-022.25E-020.024mg/dscm7.13E-045.87E-045.83E-040.001mg/dscm@7%029.91E-028.16E-028.10E-020.087Location:GlazeLines-Method5Compound:FilterableParticulateAveralleRunNumberM29-lM29-2M29-3Mass_mg4.63.90.93.133Eg/hr3.50E+012.94E+016.76E+OO23.720mg/dscm9.13E-OI7.63E-Ol1.75E-Ol0.617mg/dscm@7%021.27E+021.06E+022.43E+0185.767Location:SprayDryer-Method23Compound:I,2,3,4,6,7,8-HpCDDAveralleRunNumberM23-lM23-2M23-3Mass_mg0.0000002850.0000002610.0000002990.000Eg/hr5.72E-065.32E-066.43E-060.000Tuesday,September07,2010Page14of37Dalltalia LLC mg/dscm

6
. 84E-08

6
. 30E-08

7
. 36E-08

0
. 000 **m~dscm@7%02**

3
. 28E-07

3
. 65E-07

3
. 53E-07

0
. 000 Compound:

l ,2,3,4,6,

7 ,8-HpCDF

Averal!e RunNumb

e r
M23-l M23-2 M23-3 Mas

s _ mg 0.0000000021 0.0000000013 0.00000000076

0.000 Eg/hr 4.22E-08 2.65E-08 1.63E-08
0.000 mg/dscm 5.04E-IO

3
. 14E-1
0 1.87E-1

0 0.000 **m~dscm@7**
**02** 2.42E-09 1.82E-09

8 .96E -10 0.000 Compound

:
1 , 2 , 3,4,7,8,9-HpCDF

Averal!e Run Numb

e r
M23-1 M23-2 M23-3 Ma ss mg 0.0000000018

0
. 0000000017

0
. 00000000

I

0
. 000 Eglhr

3
. 61 E-08 3.46E-08

2
. 15E-08

0 .00 0 mg/dscm

4
. 32E-10

4
. 10E-10 2.46E-10
0.000 **m~ds m@7**  **02**

2

. 07E -0 9 2.37E-09

1 . 18E -09

0
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: 1,2

, 3,4,7 ,8 -HxCDD

Averal!e RunNumb

e r
M23-l M23-2 M23-3 Ma ss_m
g 0.00000000
89 0.0000000091

0 .0 00000012
0.000 Eg/hr 1.79E-07

1 .8 5E-07 2.58E-07
0.000 mg/dscm 2.14E-09 2.20E-09

2 .95 E-09 0.000 **m~dscm@7%02** 1.03E-08 1.27E-08

1.41 E-08 0.000 Compound

: 1,2,3,4

, 7,8-HxCDF

Averal!e Run Number

M23-1 M23-2 M23-3 Mass_mg 0.00000000095 0.00000000088

0
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1.91 E-08 1.79E-08

1 . 50E-08

0
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2
. 28E-IO 2.12E-IO 1.72E-JO

0
. 000 **m~dscm@7%02** 1.09E-09 1.23E-09

8
. 24E-IO
0.000 Compound:

l ,2,3

, 6 , 7,8-HxCDD

Averal!e RunNumber

M23-1 M23-2 M23-3 M ass _mg

0
. 000000015 0.0000000254 0.0000000

13 0.000 Eglhr

3.01 E-07 5.17E-07 2.79E-07
0.000 mg/dscm 3.60E-09 6.13E-09 3.20E-09
0.000 **m~dscm 7%02** 

1 . 73E-08 3.55E-08 1.53E-08

0
. 000 Compound:

I ,2, 3,6

, 7,8-HxCDF

Averal!e RunNumber

M23-1 M23-2

M 23 -3 Ma ss _ mg

0
. 00000000086 0.00000000079

0 . 00000000041
0.000 Eglhr
1.73E-0

8

1 .6 1 E-08

8.8 1 E-09 0.000 mg/dscm 2.06E-10 1.91E-IO J.OIE-10
0.000 m!ld sc m @7%02

9 .8 7E-IO

I. II E-09

4 .84 E-IO 0.000 Compound:

I ,2,3, 7 ,8,9-HxCDD

Averal!e Run Number

M23-1 M23-2 M23-3 Tuesday, September 07, 2010

Page 15 of 37

### Dal ltalia LLC Mass_mg 0.0000000769 0.0000000845 0.0000000653

0.000 Eglhr 1.54E-06 1.72E-06

1 .40E -0 6 0.000 mgldscm

1. 85E-08
2.04 E-0 8
1.61 E-08 0.000 ms/dscm@7%02 8.87E-08

1.1 8 E-07
7.72 E-08

0
. 000 

### Compound:



### 1 ,2,3, 7 ,8,9- HxCDF

Avera2e RunNumbcr

M23-l M23-2 M23-3 Ma ss _mg 0.0000000011

0. 00000000

I 0.00000000052

0.000 Eglhr

2.21 E-08 2.04E-08 1.12E-08
0.000 mgldscm 2.64E-10 2.4\E-10 1.28E-10
0.000 **m~dscm@7%02**
1.27E-09 1.40E-09 6.14E-10
0.000 

### Compound:



### 1 ,2,3, 7 ,8-PeCDD

Avera2e RunNumber

M23-1 M23-2 M23-3 Mass_mg 0.0000000384 0.0000000529 0.000000037
0.000 Eglhr

7
. 7\E-07 1.08E-06

7.95 E-0 7 0.000 mg/dscm 9.22E-09 1.28E-08 9.\0E-09

0
. 000 **m~dscm@7%02** 4.42E-08

7.41 E-08

4 .36E -08 0.000 

### Compound:



### 1 ,2, 3 , 7 , 8-PeCDF

Avera2e RunNumber

M23-l M23-2 M23-3 Mass mg 0.0000000013 0.00000000099 0.00000000056

0.000 Eglhr

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1.20E

- 08 0.000 mgldscm 3.12E-IO 2.39E-10 1.38E-1

0 0.000 **m~dscm@7%02** 1.50E-09

1 . 38E-09

6.61 E-10 0.000 

### Compound: 

### 2,3,4,6,7,8-HxCDF

Avera2e Run Number

M23-1 M23-2 M23-3 Mass mg 0.00000000092

0
. 0000000023 0.00000000044

0
. 000 Eglhr

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4
. 69E-08 9.46E-09
0.000 mg / dscm

2
. 2\E-10 5.55E-10 1.08E-IO

0
. 000 ms /dsc m @7%02

1 .06 E-09
3.21 E-09 5.18E-IO
0.000 

### Compound: 

### 2,3,4,
7 , 8-PeCDF

Averal!e RunNumber

M2 3 -1 M23-2
M23

- 3 Mass _ mg 0.0000000015

0
. 00000000094 0.00000000054

0.000 Eglhr

3.01 E-08

1.91 E-08 1.16E- 08 0.000 mgldscm 3.60E-IO

2
. 27E-IO 1.33E-10
0.000 ms/dscm@7%02

1.73E

- 09
1.31 E-09

6
. 37E-10
0.000 

### Compound: 

### 2,3,7

, 8-lrCDD

Averal!e RunNumber

M23

- l M23-2 M23-3 Mass_mg 0.0000000593

0
. 0000000729 0.000000051

0
. 000 E g/ hr

1.1 9E-06 1.48E-06

I. IOE- 06 0.000 mgldscm
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8

1 . 76E-08 1.25E-08
0.000 mg/dscm@7%02

6 .8 1 E-08

1 .02E-07 5.99E-08
0.000 

### Tuesday, September 07, 2010

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2.29£

- 08

2
. 28E-09 1.74E-09

0
. 000 mg/dscm

3
. 76E-09

3
. 82E-10 2.88E-10

0
. 000 **m~ /dscm~**  **%02**

2
. 61 E-08 2.53E-09 1.54E-09
0.000 Compound

:

l , 2,3

, 4,7 ,8,9-HpCDF

Averal!e Run Number

M23-l M23-2 M23-3 Mass _ mg

0 .0 000000026 0.00000000092

0 .00 00000016
0.000 Eg/hr 3.72E-09

1.31 E-09 2.32E-09
0.000 mgldscm

6.11 E-10 2.20E-l0

3
. 84E-IO 0.000 **m~dscm@7**
**02** 4.25E-09 1.46E-09 2.05E-09
0.000 Compound:

1,2

, 3,4

, 7,8-HxCDD

Averal!e RunNumber

M23-3 M23-l M23-2 Mass_mg

0
. 0000000051

0
. 00000000556 0.00000000

I 0.000 Eg/hr

7.41 E-09

7
. 94E-09 1.43E-09
0.000 mgld sc m

1.22E

- 09

1 . 31 E-09

2
. 39E-10

0
. 000 **m~d scm@7%02**  6.52E-09

9
. 10E-09 1.58E-09

0
. 000 Compound:

1 ,2, 3,4

, 7 , 8-HxCDF

Averal!e RunNumber

M23-3 M23-1 M23-2 Mass_mg 0.00000000069 0.0000000068

0. 00000000062
0.000 Eglhr 1.00E-09

9
. 72E-09 8.84E-10
0.000 mg/dscm

1 . 66£-10 1.60£-09 1.48E-10
0.000 **m~dscm@7%02** 8.87E-10

1.11 E-08 9.80E-IO
0.000 Compound:

1,2

, 3,6,7,8-HxCDD

Averal!e RunNumber

M23-1 M23-2

M2 3- 3 Mass _ rng

0
. 00000000522

0
. 000000002

0
. 000000003

0
. 000 Eglhr 7.46£-09 2.85£-09

4
. 36£-09

0
. 000 mg / d scm 1.23E-09

4
. 78E-10

7
. 20£-10

0
. 000 **m~dscm@7**
**02**

8.55 E-09 3.16E-09

3
. 85E-09 0.000 Compound:

1 ,2,3,6,
7 ,8-HxCDF

Averal!e Run Number
M23-3 M23-1 M23-2 Mass _ mg 0.00000000062 0.0000000025 0.00000000056

0.000 Eglhr 9.01E-10 3.57E-09 7.99E-IO
0.000 mg/dscm 1.49E-10

5 .87 E-10 1.34E-IO
0.000 **~dsc @7%**  **02**

7
. 97E-IO

4
. 08E-09 8.87E-10
0.000 Compound:

1,2

, 3 , 7,8,9-HxCDD

Averal!e Run Number

M23-1 M23-2 M23-3 Ma ss _ mg

0
. 0000000185

0
. 0000000069

0
. 000000012

0
. 000 Eg / hr

2
. 64E-08

9
. 84E-09 1.74E-08
0.000 mgld

s cm

4
. 35E-09 1.65E-09

2 .8 8E-09

0
. 000 **m~dscm@7**
**02**

3
. 02E-08

1 . 09£-08 1.54E-08
0.000 Compound:

I ,2,3,7 ,8,9-HxCDF

Averal!e Tuesday, September 07, 2010

Page 18 of 37DalItaliaLLCRunNumberM23-3M23-lM23-2Mass_mg0.000000000780.000000000420.000000000710.000Eg/hr1.13E-096.00E-IO\.OIE-090.000mg/dscm1.87E-IO9.86E-11l.70E-100.000mg/dscm@7%021.00E-096.&5E-10l.I3E-090.000Compound:1,2,3,7,8-PeCDDAveral!eRunNumberM23-lM23-2M23-3Mass_mg0.0000000II70.000000009140.00000002110.000Eg/hr1.67E-081.30E-083.06E-O&0.000mg/dscm2.75E-092.18E-095.07E-090.0001.91E-081.44E-082.71E-0&0.000Compound:1,2,3,7,8-PeCDFAveral!eRunNumberM23-3M23-1M23-2Mass_mg0.00000000130.00000000410.000000000740.000Eg/hr1.89E-095.86E-091.06E-090.000mg/dscm3.12E-109.63E-101.77E-l00.0001.67E-096.69E-091.17E-090.000Compound:2,3,4,6,7,8-HxCDFAveral!eRunNumberM23-3M23-lM23-2Mass_mg0.000000000660.000000000820.00000000060.000Eg/hr9.59E-101.17E-098.56E-100.000mg/dscm1.5&E-IO1.93E-101.43E-IO0.000m£::dscm@7%028.45E-IO1.34E-099.47E-100.000Compound:2,3,4,7,8-PeCDFAveral!eRunNumberM23-3M23-lM23-2Mass_mg0.0000000020.00000000180.00000000\90.000Eg/hr2.91E-092.57E-092.71E-090.000mg/dscm4.80E-104.23E-104.54E-IO0.000mg/dscm@7%022.57E-092.94E-093.0\E-090.000Compound:2,3,7,8-TCDDAveral!eRunNumberM23-lM23-2M23-3Mass_mg0.0000000280.0000000260.00000006990.000Eg!hr4.00E-O&3.71E-081.02E-070.000mg/dscm6.58E-096.21E-091.68E-O&0.000mg/dscm@7%024.57E-084.11E-088.98E-080.000Compound:2,3,7,8-TCDFAveral!eRunNumberM23-lM23-2M23-3Mass_mg0.000000000790.000000000830.00000000I0.000Eg/hr1.13E-091.1&E-091.45E-090.000mg/dscm1.86E-IO1.98E-IO2.40E-100.000mg!dscm@7%021.29E-091.31E-09l.28E-090.000Tuesday,September07,2010Page19of37DalltaliaLLCCompound:OCDDAvera2eRunNumberM23-3M23-lM23-2Mass_mg0.0000008990.000001750.0000008420.000Eg/hr1.31E-062.50E-06l.20E-060.000mg/dscm2.16E-074.1\E-072.01E-070.000mg/dscm@7%02l.\5E-062.86E-061.33E-060.000Compound:OCDFAvera!!eRunNumberM23-lM23-2M23-3Mass_mg0.00000004160.000000001340.00000000280.000Eg/hr5.94E-081.91E-094.07E-090.000mg/dscm9.77E-093.20E-\O6.72E-\O0.000mg/dscm@7%026.79E-082.12E-093.59E-090.000Compound:TotalDioxinsAvera!!eRunNumberM23-1M23-2M23-3Mass_mg0.0000019190.00000092690.00000l06950.000Eg/hr2.74E-061.32E-061.55E-060.000mg/dscm4.51E-072.21E-072.57E-070.0003.13E-061.46E-061.37E-060.000Compound:TotalFuransAveralleRunNumberM23-lM23-2M23-3Mass_mg0.000000077430.00000000980.000000012650.000Eg/hrl.\1E-071.40E-081.84E-080.000mg/dscm1.82E-082.34E-093.04E-090.000mg/dscm@7%021.26E-071.55E-081.63E-080.000Location:WetScrubber#2-Method23Compound:1,2,3,4,6,7,8-HpCDDAveralleRunNumberM23-lM23-2M23-3Massmg0.000004150.000003360.000005870.000Eg/hr8.53E-056.39E-051.11E-040.000mg/dscm9.99E-077.34E-071.27E-060.000mg/dscm@7%026.04E-065.37E-068.41E-060.000Compound:I,2,3,4,6,7,8-HpCDFAvera!!eRunNumberM23-lM23-2M23-3Mass_mg0.00000000570.00000000590.00000000450.000Eg/hrl.\7E-071.12E-078.52E-080.000mg/dscm1.37E-091.29E-099.76E-100.0008.28E-099.44E-096.46E-090.000Compound:I,2,3,4,7,8,9-HpCDFAvera!!eRunNumberM23-lM23-2M23-3Mass_mg0.00000000190.0000000020.000000000660.000Tuesday,September07,2010Page20of37DalltaliaLLCEg/hr3.9\E-083.80E-081.25E-080.000mg/dscm4.57E-IO4.37E-IO1.43E-IO0.000mg/dscm@7%022.76E-093.20E-099.47E-100.000Compound:1,2,3,4,7,8-HxCDDAvera2eRunNumberM23-IM23-2M23-3Mass_mg0.0000003450.0000002710.000000350.000Eg/hr7.09E-065.15E-066.63E-060.000mgfdscm8.3\E-085.92E-087.59E-080.0005.02E-074.33E-075.02E-070.000Compound:1,2,3,4,7,8-HxCDFAvera2eRunNumberM23-lM23-2M23-3Massmg0.00000000270.00000000250.00000000170.000Eg/hr5.55E-084.75E-083.22E-080.000mg/dscm6.50E-105.46E-103.69E-100.000rn&ldscm@7%023.93E-093.99E-092.44E-090.000Compound:1,2,3,6,7,8-HxCDDAveral!eRunNumberM23-IM23-2M23-3Mass_mg0.0000004140.0000003770.0000004730.000Eg/hr8.51E-067.17E-068.95E-060.000mg/dscm9.97E-088.23E-081.03E-070.000mg/dscm@7%026.03E-076.02E-076.82E-070.000Compound:I,2,3,6,7,8-HxCDFAvera2eRunNumberM23-lM23-2M23-3Mass_mg0.00000000460.00000000550.00000000410.000Eg/hr9.46E-081.05E-077.76E-080.000mg/dscmI.IIE-091.20E-098.89E-100.000mg/dscm@7%026.71E-098.78E-095.88E-090.000Compound:1,2,3,7,8,9-HxCDDAvera2eRunNumberM23-lM23-2M23-3Mass_mg0.0000009080.0000008340.000001050.000Eg/hr1.87E-051.59E-051.99E-050.000mg/dscm2.19E-071.82E-072.28E-070.000mg/dscm@7%021.32E-061.33E-061.5IE-060.000Compound:1,2,3,7,8,9-HxCDFAvera2eRunNumberM23-1M23-2M23-3Mass_mg0.00000000140.000000002270.000000000990.000Eg/hr2.88E-084.31E-081.87E-080.000mg/dscm3.37E-104.96E-IO2.15E-IO0.000mg/dscm@7%022.04E-093.63E-091.42E-090.000Compound:1,2,3,7,8-PeCDDAveral!eTuesday,September07,2010Page21of37Dal Italia LLC RunNumb
er
M23-1 M23-2 M23-3 Mass mg 0.000000705 0.00000078 0.000000941
0.000 Eglhr

1 .4 5E-05 1.48E-05 1.78E-05
0.000 mgldscm

1 .70 E-07 1.70E-07 2.04E-07

0
. 000 **m~ /dscm@7%02**  1.03E-06

1 . 24E-06 1.35E-06
0.000 Compound

: 1,2,3,7 ,8- PeCDF

Averaee RunNumb
er
M23-l M23-2 M23-3 Mass mg 0.000000004

7 0.00000000752 0.0000000046

0.000 Eglhr 9.66E-08 1.43E-07

8.71 E-08 0.000 mgld scm 1.13E-09 1.64E-09 9.97E-IO
0.000 mgldscm@7%02 6.83E-09

1 .20 E - 08 6.60E-09
0.000 Compound

: 2,3,4,6,

7 ,8-HxCDF

Averaee Run Number

M 2 3-l M23-2 M23-3 Mass _ mg 0.000000002

0 .0000 0000267

0 .000000 0021 0.000 Eglhr

4.11 E-08 5.08E-08

3.98 E-08 0.000 mgld sc m

4
. 81E-IO 5.83E-IO 4.55E-IO

0 .000 m!ldscm
@ 7 %02

2.91 E-09 4.27E-09 3.01E-09

0
. 000 Compound: 2,3,4,7,8-PeCDF

Avera2e Run Number

M23-l M23-2 M23-3 M ass_ mg 0.0000000051

0 .00000000726

0 .000000008

4 2

0
. 000 Eg / hr 1.05E-07

1.3 8E -07

1 .59 E-07 0.000 m g/ ds c m

1 .23E- 09

1 .59E- 09

1 .83E -09

0
. 000 **m~dscm@7%02**

7 .43 E-09

1 . 16E -08
1.21 E-0 8

0
. 000 Compound: 2,3,7,8-TCDD

Averaee RunNumber

M23-l M23-2 M23-3 Mass_mg 0.000000768

0
. 000000744 0.00000109
0.000 Eg/hr
1.58E-05

1.41 E-05

2
. 06E-05
0.000 m gldsc m 1.85E-07

1 . 62E-07 2.36E-07

0
. 000 mgld scm@7% 02

1 . 12E-06

1 . 19E-06 1.56E-06
0.000 Compound: 2,3,7,8-TCDF

Averaee Run Number

M23-l M23-2 M23-3 Mass m g

0 .0000000
13 8

0
. 0000000076 0.0000000123

0.000 Eg/hr

2 .8 4E-07 1.44E-07 2.33E- 07 0.000 mgldscm 3.32E-09

1 . 66E-09

2
. 67E-09

0
. 000 m g/ d sc m @7%02

2.0 1 E-08

1 .21 E-08

1 . 77E-08
0.000 Compound: OCDD

Averaee Run Number

M23-1 M23-2
M23-
3 Ma ss mg 0.0000393 0.0000324 0.0000434

0 .00 0 Eg/hr
8.08E-0

4 6.16E-04 8.22E- 04

0
. 001 mgld sc m 9.46E-06 7.08E-06

9
. 41E-06

0
. 000 m g/dsc m @7%02 5.72E-05

5
. l8E-05

6 .2 3E-05

0
. 000 Tuesday, September
07, 2010

Page 22 of 37DalltaliaLLCCompound:OCDFRunNumberM23-1M23-2M23-3Mass_mg0.00000000780.00000000380.00000000610.000Eg/hr1.60E-077.22E-081.15E-070.000mg/dscm1.88E-098.30E-101.32E-090.000m£::dscm@7%021.14E-086.07E-098.74E-090.000Compound:TotalDioxinsRunNumberM23-1M23-2M23-3Mass_mg0.000046590.0000387660.0000531740.000Eg/hr9.58E-047.37E-041.01E-030.001mg/dscm1.12E-058.47E-061.15E-050.000mg/dscm@7%026.77E-056.20E-057.61E-050.000Compound:TotalFuransRunNumberM23-1M23-2M23-3Mass_mg0.00000004970.000000047020.000000045470.000Eg/hr1.02E-068.94E-078.61E-070.000mg/dscm1.20E-081.D3E-089.86E-090.000mg/dscm@7%027.25E-087.54E-086.53E-080.000Location:WetScrubber#2-Method29Compound:AntimonyAvera2eRunNumberM29-1M29-2M29-3Mass_mg0.001280.001470.001290.001Eg/hr2.71E-023.46E-023.15E-020.031mg/dscm3.20E-043.75E-043.61E-040.000mg/dscm@7%021.93E-032.74E-032.39E-030.002Compound:ArsenicAveral!eRunNumberM29-\M29-2M29-3Mass_mg0.01160.009970.009470.010Eg/hr2.46E-012.35E-012.31E-010.237mg/dscm2.90E-032.54E-032.65E-030.003m£::dscm@7%021.75E-021.86E-021.75E-020.018Compound:BerylliumAveral!eRunNumberM29-1M29-2M29-3Mass_mg0.00030.00030.00030.000Eg/hr6.35E-037.07E-037.32E-030.007mgldscm7.50E-057.65E-058.40E-050.000mg/dscm@7%024.53E-045.60E-045.56E-040.001Compound:CadmiumAveral!eRunNumberM29-1M29-2M29-3Massmg0.001340.001190.001380.001Tuesday,September07,2010Page23of37DalItaliaLLCEg/hr2.84E-022.80E-023.37E-020.030mg/dscm3.35E-043.03E-043.86E-040.000mg/dscm@7%022.02E-032.22E-032.55E-030.002Compound:ChromiumAveral!eRunNumberM29-1M29-2M29-3Mass_mg0.1730.1790.2110.188Eg/hr3.66E+OO4.22E+OO5.15E+OO4.343mg/dscm4.32E-024.56E-025.91E-020.0492.61E-013.34E-OI3.91E-Ol0.329Compound:CobaltAveral!eRunNumberM29-lM29-2M29-3Mass_mg0.0004790.0005530.0010470.001Eg/hr1.01E-021.30E-022.55E-020.016mg/dscm1.20E-041.41E-042.93E-040.0007.25E-04l.OJE-031.94E-030.001Compound:LeadAveral!eRunNumberM29-lM29-2M29-3Mass_mg0.130.1150.08440.110Eg/hr2.75E+OO2.71E+OO2.06E+OO2.507mg/dscm3.25E-022.93E-022.36E-020.028mg/dscm@7%021.96E-OI2.14E-01I.56E-O10.189Compound:ManganeseAveral!eRunNumberM29-lM29-2M29-3Mass_mg0.01630.03590.1280.060Eg/hr3.45E-OI8.46E-Ol3.12E+OO1.437mg/dscm4.07E-039.15E-033.58E-020.016mg/dscm@7%022.46E-026.69E-022.37E-Ol0.110Compound:MercuryAveral!eRunNumberM29-lM29-2M29-3Mass_mg0.06250.061[0.04430.056Eg/hrl.32E+OO1.44E+OO1.08E+OO1.280mg/dscm1.56E-021.56E-021.24E-020.015mg/dscm@7%029.43E-02l.14E-Ol8.21E-020.097Compound:NickelAveral!eRunNumberM29-lM29-2M29-3Mass_mg0.003510.002650.003370.003Eg/hr7.43E-026.24E-028.22E-020.073mg/dscm8.77E-046.76E-049.43E-040.001mgldscm@7%025.30E-034.95E-OJ6.24E-030.005Compound:SeleniumAvera!!eTuesday,September07,2010Page24of37Dalltalia LLC Run Numb

e r
M29-l M29-2 M29-3 Mass _ mg
0.1058 0.0927 0.0712
0.090 Eg/hr

2
. 24E+OO 2.18E+OO 1.74E+OO

2 . 053 mg/d

s cm

2
. 64E-02

2
. 36E-02 1.99E-02
0.023 m g/ d s cm@7 % 02

1 . 60E-OI 1.73E-OI

1 .32 E-Ol

0
. 15 5 Location: Wet Scrubber #2- Method

5 Compound: Filterable Particulate

Avera2e Run Numb

e r
M29-l M29-2 M29-3 Mass _ mg

84.1

73

. 5
75.6

77

. 733 Eg/hr 1.78E+03 1.73E+03

1 . 84E+03

1 , 783

. 333 mg/d

s cm

2
. 10E+Ol 1.87E+Ol

2. 12E+Ol

20

. 300 **m~d cm**  **?%02** 1.27E+02 1.37E+02 1.40E+02

134

. 667 Tuesday, September 07, 2010

Page 25of 37ProcessRunDataRunNameProductProducedAPCDRunDataRunNameSprayDryerFabricFilterDue>tCollectorGlazeLinesDustCollectorTileDryer(VerticalNoControlWetScrubber#2(Kilns2,3&4)ProcessLabRunDataRunNameNoneTuesday,September07,2010DalItaliaLLCValue0Value0000UOMTonslhrUOMValueUOM0TargetValueTargetValue0000CommentsCommentsCommentsPage26of37DalItaliaLLCSamplingIStackDataResultsDetailLocationGlazeLines-Method29AveraeRunNumberM29-lM29-2 M29-3TestDate51131'20105114120105/1512010RunStartTime2:36:00PM8:17:00AM1:11:00PMRunFinishTime6:26:00PM12:07:00PM5:01:00PMNetTraversingPoints242424NetRunTime,minutes240240240NozzleDiameter,inches0.1880.1880.1880.188PitotTubeCoefficient0.840.840.840.840DryGasMeterCalibrationFactor1.0171.0171.0171.017BarometricPressure,inchesofMercury29.7930.1630.1630.037AverageOrificeMeterDifferential,inchesH201.771.751.791.770DryGasMeterVolumeSampled,cubicteet176.642176.762180.234177.879AverageDryGasMeterTemperature,"F73.0472.5879.2574.957DryGasMeterVolumeSampled,dscf177.947180.417181.703180.022TotalMoistureLiquidcollected,g88.875.499.888.000VolumeofWaterVapor,standardcubicfeet4.183.554.704.143MoistureContentofStackGas,%2.301.932.522.250MoistureSaturationatStackGasTemperature,%2.942.803.222.987DryMoleFraction0.9770.98070.97480.978CarbonDioxide,%0.00040.00040.00040.000Oxygen,%20.820.820.820.800CarbonMonoxide&Nitrogen,%79.199679.199679.199679.200FuelFactor250.00250.00250.00DryMolecularWeight,lb!lb-Mole28.8328.8328.8328.830WetMolecularweight,lb/lb-Mole28.5828.6228.5628.587FlueGasStaticPressure,inchesofH20-0.15-0.25-0.12-0.173AbsoluteFlueGasPressure,inchesofMercury29.7830.1430.1530.023AverageStackGasTemperature,°F75.0473.9278.1375.697AverageVelocityHead,inchesofH201.34170812481.3254767421.3588546171.34296986977234006AverageStackGasVelocity,feet/second65.9565.0466.1865.723StackCross-SectionalArea,squarefeet5.9405.9405.9405.940DryVolumetricFlowRate,dryscfin22,555.822,646.122,732.822,644.900ActualWetVolumetricFlueGasFlowRate,acfin23,504.623,180.323,586.623,423.833PercentlsokineticofSamplingRate,%101.3102.3102.6102.067PercentExcessAir,%19,136.2 19,136.219,136.219,136.200F-Factor,dscfiniMMBtu@%020000.000RoundDuctDiameter,inches333333RectangularDuctWidth,inches000RectangularDuctLength,inches000Fw0000.000Fe0000.000Tuesday,September07,2010Page27of37DalltaliaLLCLocationGlazeLines-Method3A02AveraeRunNumberl292-293-29TestDate5113120105ll4t20105114l2010RunStartTime2:36:00PM8:17:00AM1:11:00PMRunFinishTime6:44:00PM12:26:00PM5:18:00PMCarbonDioxide,%0.10.10.10.100Oxygen,%20.820.820.820.800FuelFactorlDryVolumetricFlowRate,dryscfin22546226362272122,634.333F-Factor,dscfin/MMBtu@%020000.000Moisture,%2.31.932.522.250AnalyzerMakeAnalyzerModelAnalyzerSerialNumberOperatingRange25252525.000OperatingUnits%%%No.Readings/Avg.0000.000CalibrationSetI1.000CalibrationPreZeroCylinderIDNitrogenlNitrogenINitrogenICalibrationPreZeroCylinderInstrumentResponse0000.000CalibrationPreZeroCylinderBias0000.000CalibrationPreZeroCylinderDrift0000.000CalibrationPreHighCylinderIDambientairambientairambientairCalibrationPreHighCylinderInstrumentResponse20.820.820.820.800CalibrationPreHighCylinderBias-0.4-0.4-0.4-0.400CalibrationPreHighCylinderDrift0000.000CalibrationPostZeroCylinderlDNitrogen1NitrogenINitrogenICalibrationPostZeroCylinderInstrumentResponse0000.000CalibrationPostZeroCylinderBias0000.000CalibrationPostZeroCylinderDrift0000.000CalibrationPostHighCylinderlDambientairambientairambientairCalibrationPostHighCylinderInstrumentResponse20.820.820.820.800CalibrationPostHighCylinderBias-0.4-0.4-0.4-0.400CalibrationPostHighCylinderDrift0.4000.133Cavg20.820.820.820.800CavgUnits%vd%vd%vdCgas20.920.920.920.900CgasUnits%vd%vd%vdFuelTypeFw0000.000Fe0000.000Cgasw0000.000CgaswUnitsTuesday,September07,2010Page28of37LocationGlazeLines-Method5RunNumberTestDateRunStartTimeRunFinishTimeNetTraversingPointsNetRunTime,minutesNozzleDiameter,inchesPitotTubeCoefficientDryGasMeterCalibrationFactorBarometricPressure,inchesofMercuryAverageOrificeMeterDifferential,inchesH20DryGasMeterVolumeSampled,cubicfeetAverageDryGasMeterTemperature,°FDryGasMeterVolumeSampled,dscfTotalMoistureLiquidcollected,gVolumeofWaterVapor,standardcubicfeetMoistureContentofStackGas,%MoistureSaturationatStackGasTemperature,%DryMoleFractionCarbonDioxide,%Oxygen,%CarbonMonoxide&Nitrogen,%FuelFactorDryMolecularWeight,lb/lb-MoleWetMolecularweight,lb/lb-MoleFlueGasStaticPressure,inchesofH20AbsoluteFlueGasPressure,inchesofMercuryAverageStackGasTemperature,°FAverageVelocityHead,inchesofH20AverageStackGasVelocity,feet/secondStackCross-SectionalArea,squarefeetDryVolumetricFlowRate,dryscfinActualWetVolumetricFlueGasFlowRate,actinPercentlsokineticofSamplingRate,%PercentExcessAir,%F-Factor,dscfin/MMBtu@%02RoundDuctDiameter,inchesRectangularDuctWidth,inchesRectangularDuctLength,inchesFwFeTuesday,September07,2010DalItaliaLLCAveraePage29of37LocationSprayDryer-Method23RunNumberTestDateRunStartTimeRunFinishTimeNetTraversingPointsNetRunTime,minutesNozzleDiameter,inchesPitotTubeCoefficientDryGasMeterCalibrationFactorBarometricPressure,inchesofMercuryAverageOrificeMeterDifferential,inchesH20DryGasMeterVolumeSampled,cubicfeetAverageDryGasMeterTemperature,eFDryGasMeterVolumeSampled,dscfTotalMoistureLiquidcollected,gVolumeofWaterVapor,standardcubicfeetMoistureContentofStackGas,%MoistureSaturationatStackGasTemperature,%DryMoleFractionCarbonDioxide,%Oxygen,%CarbonMonoxide&Nitrogen,%FuelFactorDryMolecularWeight,lb/lb-MoleWetMolecularweight,lb/lb-MoleFlueGasStaticPressure,inchesofH20AbsoluteFlueGasPressure,inchesofMercuryAverageStackGasTemperature,°FAverageVelocityHead,inchesofH20AverageStackGasVelocity,feet/secondStackCross-SectionalArea,squarefeetDryVolumetricFlowRate,dryscfinActualWetVolumetricFlueGasFlowRate,acfinPercentlsokineticofSamplingRate,%PercentExcessAir,%F-Factor,dscfiniMMBtu@%02RoundDuctDiameter,inchesRectangularDuctWidth,inchesRectangularDuctLength,inchesFwFeTuesday,September07,2010DalltaliaLLCAveraePage30of37DalltaliaLLCLocationSprayDryer-Method3A02AveraeRunNumber1-232-233-23TestDate5/10/20105/11/20105/1212010RunStartTime9:05:00AM10:57:007:55:00AMAMRunFinishTime1:19:00PM3:09:00PM2:33:00PMCarbonDioxide,%22.522.167Oxygen,%1818.51818.167FuelFactor1.450.961.45DryVolumetricFlowRate,dryscfin49227496725139650,098.333F-Factor,dscfin!MMBtu@%028710871087108,710.000Moisture,%22.53 22.7519.1721.483AnalyzerMakeAnalyzerModelAnalyzerSerialNumberOperatingRange25252525.000OperatingUnits%%%No.Readings/Avg.0000.000CalibrationSet1.000CalibrationPreZeroCylinderIDNitrogenINitrogenINitrogenICalibrationPreZeroCylinderInstrumentResponse0000.000CalibrationPreZeroCylinderBias0000.000CalibrationPreZeroCylinderDrift0000.000CalibrationPreHighCylinderIDambientairambientairambientairCalibrationPreHighCylinderInstrumentResponse20.820.820.820.800CalibrationPreHighCylinderBias-0.4-0.4-0.4-0.400CalibrationPreHighCylinderDrift0000.000CalibrationPostZeroCylinderIDNitrogenINitrogen1Nitrogen1CalibrationPostZeroCylinderInstrumentResponse0000.000CalibrationPostZeroCylinderBias0000.000CalibrationPostZeroCylinderDrift0000.000CalibrationPostHighCylinderIDambientairambientairambientairCalibrationPostHighCylinderInstrumentResponse20.820.820.820.800CalibrationPostHighCylinderBias-0.4-0.4-0.4-0.400CalibrationPostHighCylinderDrift0000.000Cavg1818.51818.167CavgUnits%vd%vd %vdCgas18.086518.588918.086518.254CgasUnits%vd%vd %vdFuelTypeGas-NaturalGas-NaturalGas-NaturalFw10610106101061010,610.000Fe1040104010401,040.000Cgusw0000.000CgaswUnitsTuesday,September07,2010Page31of37LocationTileDryer-Method23RunNumberTestDateRunStartTimeRunFinishTimeNetTraversingPointsNetRunTime,minutesNozzleDiameter,inchesPitotTubeCoefficientDryGasMeterCalibrationFactorBarometricPressure,in(;hesofMercuryAverageOrificeMeterDifferential,inchesH20DryGasMeterVolumeSampled,cubicfeetAverageDryGasMeterTemperature,DryGasMeterVolumeSampled,dscfTotalMoistureLiquidcollected,gVolumeofWaterVapor,standardcubicfeetMoistureContentofStackGas,%MoistureSaturationatStackGasTemperature,%DryMoleFractionCarbonDioxide,%Oxygen,%CarbonMonoxide&Nitrogen,%FuelFactorDryMolecularWeight,lbJib-MoleWetMolecularweight,lb/lb-MoleFlueGasStaticPressure,inchesofH20AbsoluteFlueGasPressure,inchesofMercuryAverageStackGasTemperature,°FAverageVelocityHead,inchesofH20AverageStackGasVelocity,feet/secondStackCross-SectionalArea,squarefeetDryVolumetricFlowRate,dryscfinActualWetVolumetricFlueGasFlowRate,acfinPercentlsokineticofSamplingRate,%PercentExcessAir,%F-Factor,dscfiniMMBtu@%02RoundDuct Diameter,inchesRectangularDuctWidth,inchesRectangularDuctLength,inchesFwFeTuesday,September07,2010DalItaliaLLCAveraePage32of37Dal ltalia LLC Location Tile Dryer- Method 3A 02

Avera

e Run Number

1-23 2-23 3-23 Test Date

5 1 1512010

5 11 5 / 2010

5 11 6 / 2010 Run Start Time

8:43:00 AM 1:40:00 PM

7 :50: 00 AM Run Finish Time

12:50:00 PM 6:12:00 PM 11 :52:00 AM Carbon Dioxide,
%

0.1

0.1

0.1 0.100 Oxygen,% 18.9 18.8

18.3 18.667 Fuel Factor

20

21

26 Dry Volumetric Flow Rate, dry scfin

3580 3516 3559 3,551.667 F-Factor

, dscfin/MMBtu@ %02

8710 8710 8710 8,710.000 Moisture

, %

11.18 12.79

11 .55

11 .8 40 Analyzer Make Analyzer Model Analyzer Serial Number Operating Range

25

25

25 25.000 Operating Units

%

%

% No. Reading
s! Avg.

0

0

0 0.000 Calibration Set

1 .000 Calibration Pre Zero Cylinder ID Nitrogen

I Nitrogen

I Nitrogen

l Calibration Pre Zero Cylinder Instrument Response

0

0

0 0.000 Calibration Pre Zero Cylinder Bias

0

0

0

0
. 000 Calibration Pre Zero Cylinder Drift

0

0

0

0
. 000 Calibration Pre High Cylinder ID ambient air ambient air ambient air Calibration Pre High Cylinder Instrument Response

20.8 20.8 20.8 20.800 Calibration Pre High Cylinder Bias

-0.4 -0.4 -0.4 -0.400 Calibration Pre High Cylinder Drift

0

0

0 0.000 Calibration Post Zero Cylinder ID Nitrogen

I Nitrogen

I Nitrogen

I Cal

i bration Post Zero Cylinder Instrument Respons

e

0

0

0

0
. 000 Calibration Post Zero Cylinder Bias

0

0

0 0.000 Calibration Post Zero Cylinder Drift

0

0

0 0.000 Calibration
Po st High Cylinder ID ambient air ambient air ambient air Calibration Post High Cylinder Instrument Response

20.8 20.8 20.8 20.800 Calibration Post High Cylinder Bias

-0.4 -0.4 -0.4 -D.400 Calibration Post High Cylinder Drift

0

0

0

0
. 000 Cavg

18.9 18.8

18 .3 18.667 Cavg Units

%vd %vd %vd Cga
s

18.9909 18.8904

18

. 388

18

. 756 Cgas Unit
s

%vd %vd %vd Fuel Typ e

Gas- Natural Gas

- Natural Gas

- Natural Fw

10610 10610 10610 10,610.000 Fe

1040 1040 1040 1,040.000 Cgasw

0

0

0 0.000 Cgasw Units Tuesday, September 07, 2010

Page 33 of 37Location Wet Scrubber #2
- Method 23 Run Number T e st Date Run Start Time Run Finish Time Net Traversing Points N e t Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury A v erage Orifice Meter Differential, inche

s H20 Dry G as Meter Volume Sampled, cubic feet Av e rag e Dry Gas Meter Temperature

, ° F Dry G as Meter Volume Sampled

, ds c f Total Moisture Liquid collected,

g Volume of Water Vapor

, standard cubic feet Moisture Content of Stack Gas

, % Moisture Saturation

at Stack Gas Temperature,

% Dry Mole Fraction Carbon Dioxide,% Oxygen,% Carbon Monoxide

& Nitrogen,% Fuel Factor Dry Molecular Weight, Jb/lb-Mole Wet Molecular weight,
lb / lb-Mole Flue Gas Static Pressure, inches of H20 Ab s ol u te Flue Ga s Pressure, inches of Mercury Average Stack Gas Temperature

, ° F Averag

e V e locity Head

, inches of H20 Average Sta c k Gas Velocity

, feet/second Sta c k Cro ss -Sectional Area, square feet Dry Volumetric Flow Rate

, dry scfin Actual Wet Volumetric Flue Gas Flow Rate,

a c fin Percentlsokinetic

of Sampling Rate, % P e r c ent Excess Air

, % F-Factor

, dscfiniMMBtu@ %02 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length

, inches Fw F e Tuesday, September 07, 2010

Dal ltalia LLC

Avera

e Page 34of37LocationWetScrubber#2-Method29RunNumberTestDateRunStartTimeRunFinishTimeNetTraversingPointsNetRunTime,minutesNozzleDiameter,inchesPitotTubeCoefficientDryGasMeterCalibrationFactorBarometricPressure,inchesofMercuryAverageOrificeMeterDifferential,inchesH20DryGasMeterVolumeSampled,cubicfeetAverageDryGasMeterTemperature,"FDryGasMeterVolumeSampled,dscfTotalMoistureLiquidcollected,gVolumeofWaterVapor,standardcubicfeetMoistureContentofStackGas,%MoistureSaturationatStackGasTemperature,%DryMoleFractionCarbonDioxide,%Oxygen,%CarbonMonoxide&Nitrogen,%FuelFactorDryMolecularWeight,lb/lb-MoleWetMolecularweight,lb/lb-MoleFlueGasStaticPressure,inchesofH20AbsoluteFlueGasPressure,inchesofMercuryAverageStackGasTemperature,oFAverageVelocityHead,inchesofH20AverageStackGasVelocity,feet/secondStackCross-SectionalArea,squarefeetDryVolumetricFlowRate,dryscfinActualWetVolumetricFlueGasFlowRate,acfinPercentIsokineticofSamplingRate,%PercentExcessAir,%F-Factor,dscfin/MMBtu@%02RoundDuctDiameter,inchesRectangularDuctWidth,inchesRectangularDuctLength,inchesFwFeTuesday,September07,2010DalltaliaLLCWetScrubber#25/13/2010Method29M29-l9:35:00AM0.3150.840.97329.793.54148.45012:05:00PM16156141.37381.81WetScrubber#25/14/2010Method29M29-22:00:00PM0.230.840.97330.011.19144.9745:50:00PM24240138.51880.88WetScrubber#25/15/2010Method29M29-311:43:00AM0.230.840.97330.011.07133.0313:33:00PM24240126.15784.79Averae0.2580.8400.97329.9371.933142.152135.34982.493Page35of37Dalltalia LLC Location Wet Scrubber #2- Method 3A 02

Avera

e Run Number

1-29 2-29 3-29 Test Date

5 fl312 010 5/14/2010

5 11 5 /2 010 Run Start Time

9
: 35

: 00 AM

2
: 00:00 PM 11

: 43

: 00 AM Run Finish Time

12

: 05:00 PM

6
: 14:00 PM

4

: 33

: 00 PM Carbon Dioxide ,%

2.5

2
1.5 2.000 Oxyg
e n,%

18.6

19

18

. 8 18

. 800 Fuel Factor

0.92 0.95

1.4 Dry Volumetric Flow Rate, dry scfin
49845 54349 51296 51,830.000 F-Factor

, dscfin!MMBtu@ %02

8710 8710 8710

8 , 710

. 000 Moisture ,%

16

. 13 16.35

16

. 57 16.350 Analyzer
M a ke Anal yze
r Model Analyzer Serial Number Operating

R a nge

25

0

0

8
. 333 Operating Units

% No

. Readings/Avg.

0

0

0 0.000 Ca
l ibration Set

1 . 000 Calibration Pre Zero Cylinder ID Nitrogen

I Nitrogen

I Nitrogen

1 Calibration Pre Zero Cylinder Instrument Re s ponse

0

0

0

0
. 000 Calibration Pre Zero Cylinder Bias

0

0

0 0.000 Calibration Pre Zero Cylinder Drift

0

0

0

0
. 000 Calibration Pre High Cylinder ID ambient air ambient air ambient air Calibration Pre High Cylinder Instrument Response

20.8 20.8

20

. 8 20.800 C a libration Pre High Cylinder Bias

-0.4 -0.4

-0

. 4 -0.400 Calibration Pre High Cylinder Drift

0

0

0

0
. 000 C a libration Post Zero Cylinder ID Nitrogen

I Nitrogen

1 Nitrogen

1 Calibra

t ion Post Zero Cylinder Instrument
Re s pon
s e

0

0

0

0
. 000 C alibration Post Zero Cylinder Bia s

0

0

0

0
. 000 Calibrat

i on Post Zero Cylinder Drift

0

0

0

0
. 000 C a libration Po s t High Cylinder ID ambient air amb

i en t air ambient air Calibration
Po s t High Cylinder Instrument Response

20

. 8
20

. 8
20

. 8 20

. 800 Calibration Post High Cylinder Bias

-0.4

- 0
. 4

-0

. 4 -D.400 Calibration Post High Cylinder Drift

0

0

0

0
. 000 C av g

18.6

19

1 8 .8 18.800 Cavg Unit
s

%vd %vd

% vd Cga
s

18.6894 19.0913 18.8904 18.890 Cgas Units

%vd %vd %vd Fuel Type

Gas

- Natural Gas

- Natural Gas- Natural Fw

10610 10610 10610 10

, 610.000 F e

1040 1040 1040

1 , 040

. 000 Cgasw

0

0

0

0
. 000 Cga

s w Units Tuesday, September 07, 2010

Page 36 of 37DalltaliaLLCLocationWetScrubber#2-Method5AveraeRunNumberM29-lM29-2M29-3TestDate5/13120105/14120105/1512010RunStartTime9:35:00AM2:00:00PM11:43:00AMRunFinishTime12:05:00PM5:50:00PM3:33:00PMNetTraversingPoints162424NetRunTime,minutes156240240NozzleDiameter,inches0.3150.230.230.258PitotTubeCoefficient0.840.840.840.840DryGasMeterCalibrationFactor0.9730.9730.9730.973BarometricPressure,inchesofMercury29.7930.0130.0129.937AverageOrificeMeterDifferential,inchesH203.541.191.071.933DryGasMeterVolumeSampled,cubicteet148.450144.974133.031142.152AverageDryGasMeterTemperature,°F81.8180.8884.7982.493DryGasMeterVolumeSampled,dscf141.373138.518126.157135.349TotalMoistureLiquidcollected,g577.4575532.2561.533VolumeofWaterVapor,standardcubicfeet27.1827.0725.0526.433MoistureContentofStackGas,%16.1316.3516.5716.350MoistureSaturationatStackGasTemperature,%16.3516.5216.9116.593DryMoleFraction0.83870.83650.83430.837CarbonDioxide,%2.521.52.000Oxygen,%18.61918.818.800CarbonMonoxide&Nitrogen,%78.97979.779.200FuelFactor0.920.951.40DryMolecularWeight,lb/lb-Mole29.1429.0828.9929.070WetMolecularweight,lb/lb-Mole27.3427.2727.1727.260FlueGasStaticPressure,inchesofH200.370.450.450.423AbsoluteFlueGasPressure,inchesofMercury29.8230.0430.0429.967AverageStackGasTemperature,°F132.88133.54134.42133.613AverageVelocityHead,inchesofH200.41586036720.4925259840.4400524020.44980145662171483229AverageStackGasVelocity,feet/second39.4942.9040.6541.013StackCross-SectionalArea,squareteet28.27428.27428.27428.274DryVolumetricFlowRate,dryscfi1149,870.754,373.151,309.851,851.200ActualWetVolumetricFlueGasFlowRate,acfin66,992.472,777.368,960.369,576.667PercentlsokineticofSamplingRate,%94.9104.0100.499.767PercentExcessAir,%834.21,023.7839.0898.967F-Factor,dscfin/MMBtu@%020000.000RoundDuctDiameter,inches727272RectangularDuctWidth,inches000RectangularDuctLength,inches000Fw0000.000Fe0000.000Tuesday,September07,2010Page37of37EntecServices,Inc.SOURCEOWNER:PLANTLOCATION:SOURCE(S)NAME(S):SOURCE(S)CONDITION:SOURCE(S)SHAPE:TESTPERFORMED:REFERENCEMETHODTESTS:ENTECPROJECTMANAGER(PM)SOURCEOVERVIEWDalltaliaMuskogee,OklahomaWetScrubber2NormalConditions-TileMACTCircularFlowandFTIRSampleTestPointsatLocationVolumetricFlowandGasVelocityMolecularWeightMoistureContentHydrogenChlorideHydrogenFluorideLynnBeaneENVIRONMENTALANALYST(TeamLeader)ErikGrothENVIRONMENTALANALYST(Assistants)JohnDrienzoOWNER'SREPRESENTATIVE(s):Mr.BobHurtandMr.SteveWillisENTECPROJECTNUMBER:210155DATESTESTSCONDUCTED:Trav/Prep05/13/10ThursdayRun105/14/10FridayRun205/14/10FridayEPAMethodEPAMethodEPAMethodEPAMethodEPAMethodEPAMethodRun305/14/10Friday123/3A4320320TestPerformedFor:Source(s)Tested:TestCondition:Test(s)Performed:RunNumberDateofRunTimes,PollutantRuns(Began-Ended)Times,FlowRuns(Began-Ended)OxygenCone.,CarbonDioxideCone.MolecularWeightOfStackGasMolecularWeightOfStackGasHydrogenChlorideHydrogenFluorideStackTemperatureMoistureContentAverageStackGasVelocityStackGasFlow@ActualConditionsStackGasFlow@STPStackGasFlow@DryStandardConditionsHydrogenChlorldeCone.@STPHydrogenFluorideCone.@STPHydrogenChlorideCone@7%02HydrogenFluorideCone@7%02HydrogenChlorideMassEmissionsFluorideMassEmissionsTable2-6EmissionsSummaryDalltaliaMuskogee,OklahomaWetScrubber2NormalConditions-TileMACTFlows,Moistures,HCIandHF25/14/105/14/101403-15041527-16301403-15041527-1630%(drybasis)19.019.0%(drybasis)2.02.0%(drybasis)29.0829.08%(wetbasis)27.2727.27ppm,v/v,d9.4015.10ppm,v/v,d10.6612.62oc56.456.4%,vlv16.1316.35m/s13.0713.07acmm2,0612,061scmm1,8401,840dscmm1,5391,539mg/dscm14.2222.84mg/dscm8.8510.47mg/dscm.85.92167.10mg/dscm.53.4976.62kgIhr1.3132.109kg/hr0.8170.967••FlowtestingwasperformedforthissourceinconjunctionwiththeMethod29Testing,Run2.[NOTE-Run4FlowwascompletedasaPost-ICRflowruntobracketthe3ICRruns.]TestingPerformedBy:BirminghamDivisionProjectManager:LynnBeane34Average5/14/105/14/103Runs1655-17581655-17581800-181419.019.019.02.02.02.029.0829.0829.0727.2727.2727.265.9610.166.7710.0256.456.456.416.5716.3516.3513.0713.0713.072,0612,06120611,8401,84018401,5391,53915399.0215.365.628.3259.71104.2437.2155.770.8331.4180.5190.768Client:DalltaliaFigure4-1EntecServices,Inc16DCommerceAve.Hueytown,AL35023STACKDRAWING&TRAVERSEPOINTLOCATIONJobNo.:210155Source:WetScrubber2InputBy:ErikGrothTypeofTraverse:Velocity(V)orParticulate(P):StackDiameter,Inches:72StackHeight,feet:50.0StackProperties:Inches'After'FlowDisturbance,Distance(A):80.0'Before'FlowDisturbance,Distance(B):144.072.0INCHES80.0INCHES0144.0INCHESyPortTypeNipplePortDiameter4StackArea,Ft2:28.274NumberofPorts:2LengthofPort,inches:15.001.11TotalNumberofTraversePoints:162.00NumberofPointsperportItraverse:8InsideStackOutsideNipplePointNo.InchesInches2.317.327.622.6314.029.0423.338.3548.763.7658.073.0764.479.4869.784.7•Adjustedpointsdiameter>24"nopointcloserthan1.0Inch•Adjustedpoints24Mnopointcloserthan0.5InchStackDiametersbetween12·24inchesminimumpointsare8 ;4pointsperportifthe8I2diametersdownstreamandupstreamcriteriaIsmet.IQC'dby:JRFI8ENTECServices,Inc.16DCommerceAve.Hueytown,Al35023PreliminaryTraverse&CyclonicFlowVerificationClient:DalltaliaTestDate:05113110Source:WetScrubber2RunNo.:PreliminaryTestTraversePointDeltaPSq.Rt.DeltaPNullReading(Angle)StackTemp.(°F)1-10.00001-20.00001-30.00001-40.00001-50.00001-60.00001-70.00001-80.00002-10.00002-20.00002-30.00002-40.00002-50.00002-60.00002-70.00002-80.0000Average#DIVIOI0.0000#DIVIO!QC"dby:JRFNote:Mlcro-monometerrequiredbasedonpreliminarylowflows.Note:Thecyclonicflowswerenottestedbasedontheabsenceofcyclonicflowfromprevioustestresults.ENTECServices,Inc.16-DCommerceAve.Hueytown,Alabama35023InitialMeterBox10MinuteCalibrationClient:DalltaliaLocation:Muskogee,OklahomaSource:WetScrubber2JobNumber:210155MeterBox:NC-2OriginalDeltaH@:1.986CalibrationDate:9/29/2009OriginalYFactor:0.987InitialVolume:87.200InitialMeterTemperature:88.0FinalVolume:94.875FinalMeterTemperature:86.0MeterVolume:7.675AverageTemperature:87.0Deg.R547.0BarometricPressure:29.30Yo=1.005Y0Equation:10I(Volume)XSQRT((0.0319*(Tm/Pbar))Y0Result:1.303X0.772IQC'dby:JRFMeterCalibrationo/oDifference=-1.87%Signature:Date:

# Run Date 1 05/14/10 2 05/14/10 

# 3 05/14/10 

# FTIR Raw Input Results Summary (from FTIR Output) See Raw Results from FTIR Data Set 

# Time (24-hr) Measured Concentration, ppm (wet, v/v) Start Run End Run Hydrogen Chloride Hydrogen Fluoride HCI HF 14:03:00 15:04:00 7.88 8.94 15:27:00 16:30:00 

# 12.63 10.55 16:55:00 17:58:00 4.98 5.65ENTECServices,Inc.16-DCommerceAve.Hueytown,Alabama35023INPUTTESTDATAClient:DalltallaJobNo.:210155Source:WetScrubber2DataInputBy:LynnBeaneFieldDataSymbolUnitsTestDataOC'dby:JRFRunNumber.-123AVERAGETestDate- -05114/1005/1411005114/1005/14110AllRunsTimes,PollutantRuns(Began-Ended)-MilitaryTime1403-15041527-16301655-1758-Times,FlowRuns(Began-Ended)-MilitaryTime1403-15041527-16301655-17581800-1814SamplingTime8minutes60.060.060.0-60.0StackAreaA.Ft'28.2728.2728.27 28.27-BarometricPressurep,_in.Hg29.7930.0130.0130.0129.96StackStaticPressurePoin.H200.370.450.450.450.43OxygenConcentration,%(drybasis)o,%19.019.019.019.019.00CarbonDioxideConcentration,%(drybasis)co,%2.02.02.02.02.00Avg.Sq.Rl.ofDeltaPsqrt6P(in.H20)1/20.7020.7020.7020.7020.702StackTemperature.."F133.5 133.5133.5133.5133.5HydrogenChloride(FTIR),ppm,wetHCIppm,wet7.88412.6344.9768.498HydrogenFluoride{FTIR),ppm,wetHFppm,wet8.94410.5555.6518.383HydrogenChloride(FTIR),ppm,dryHCIppm,d,VIV9.40015.1035.96510.156HydrogenFluoride{FTIR),ppm,dryHFppm,d,vIv10.66412.6186.77310.018ENTECServices,Inc.16-0CommerceAve.HUB)'Iown.Alabama35023CALCULATEDTESTDATA·EnglishUnitsClient:DalltallaJobNo.:210155Source:WetScrubber2DataInputBy:LynnBeaneDescriptionIFonnulasSymbolUnitsCalculatedDataQC'dby:JRFRunNumbers-1234AVERAGETestDate(s)-05114110051H/100511411005114/103RunsTimes,PollutantRuns(Began-Ended)-MilitaryTime1403-15041527-16301655-17580.Times,FlowRuns(Began-Ended)-MilitaryTime1403-15041527·16301655-17581600·18151.StackPressureP..,+P1/13.6P,in.Hg29.8230.0430.0430.0429.972.MeterPressurePw+AH!13.6in.Hg29.7930.0130.0129.943.StandardMeterVolume17.&.4'Y'fV.JT(P..,+411/13.6)viii(....dstl0.0000.0000.0000.004a.StandardVolumeofWaterVaporCondensed-o.04706'W,..v'«(.hllsci0.0000.0000.0000.004b.StandardVolumeofWaterCollectedinSilicaGel..0.04715'W.,v....sci0.0000.0000.0000.005.MoistureFraction:rv_,.,...._....wrv_........._,.....B"fraction0.16130.16350.16570.16350.169.MolecularWeightofStackGas(drybasis)•0.32'(0,)+0.44'(CO:I+0.28'(101l-(O,HCO,I)M,glg-mole29.14429.08028.99229.07229.0710.MolecularWeightofStackGas(wetbasis)•M,'(1·B-1+18.0'(B.JM,gig-mole27.34727.26827.17127.26227.2611.AverageStackGasVelocity•B5.49'C,.'(sqrt6PI..,'SQRT((T,1I(P,"Mwllv,ftls42.8942.8942.8942.8942.8912.StackGasFlow@ActualCondnlons=60'v,'A,a,ac;fm72.76672.76672,76672,7667276613.StackGasFlow@STP"Q."(T.,.IT,)'(PJP,..)a,serm64,97164,971 64,97164,9716497114.StackGasFlow@STP,dry=a,'(1·B-I'(T...IT,I'(P,11',.)a.,dstfm54,34954,34954,34954,3495434915.HydrogenChlorideCone.@Std.Conditions=(0.01543'HCI,..JN-HCicagr/dsef0.006210.009980.00394.0.0115.HydrogenAuorideCone.@=(0.01543'HF,..JN_,HFcsgr/dscf0.003870.004580.00246-0.0021.HydrogenChlorideMassEmissions"(6017000I'HCics'O...HCIIbs/hrlbslhr2.894.651.84.3.1332.HydrogenAuorideMassEmissions"(6017000)'HFcs•a..HF·lbslhrlbs/hr1.802.131.14.1.69CALCULATEDTESTDATA·MetricUnitsDeacrtpttonIFonnulasSyn'ColUnitsCalculatedDataQC'dby,JRFRunNumber1234AVERAGETestDate-0511411005114/100511411005114/103RunsTimes,PollutantRuns(Began-Ended)MllilaryTime1403-15041527-16301655-1758. .1.StackPressure=P,'25.4P,mm.Hg757.36763.09763.09763.09761.665.MoistureFraction=tv......,..v_,..,)l(v...,,,.,+v_...,+v......a_fraction0.1610.1630.1660.1630.1639.MolecularWeightofStackGas,drybasis=0.32'(02)+0.44'(C0,)+0.28'(100oj0,)1CO,))M,g/g·mole29.14429.08028.99229.07229.07210.MolecularWeightofStackGas,wetbasis=M,'(1·B,.,)+18.0'(B,.,)M,g/g·mole27.34727.26827.17127.26227.26211.AverageStackGasVelocity=85.49'C,'(sqrlAI').,.'SQRT((T,)I(P,'M,.))v,m/s13.0713.0713.0713.0713.0712.StackGasFlow@ActualConditions=eo•v:A.a,acmm2,0612,0612,0612,0612.06113.StackGasFlow@STP=Q.'(T,1,1T,)'(P,IP,.,)a,stmm1,8401,8401,8401,8401,84014.StackGasFlow@STP(dry)=Q.'(1·B-)'(T,1,1T,)'(P,/P,,.)a.,,dscmm1,5391,5391,539 1,5391,53915.HydrogenChlorideCone.@Std.Conditions(FTIR)mg/dstm14.21722.8419.021-15.36015.HydrogenFluorideCone.@Std.Conditions(FTIR)Hfcsmgldscm8.85110.4735.622-8.315415.HydrogenChlorideCone@7%02=C,'((20.9·7)/(20.9-%02)1c...,,mglds<m.85.92167.1059.71.104.2415.HydrogenFluorideCone@7%02••((20.9·7)1(20.9-%02))c.,,mgldscm.53.4976.6237.21-55.7721.HydrogenChlorideMassEmissions=(6017000)'HCics•o,..HCIkgIhrkg/lv1.31282.10910.8330-1.418321.HydrogenFluorideMassEmissions•(6017000)'HFcs•a..HCII<g/1vkg/hf0.81730.96710.51910.7678"in }ooo **~Hi !~~** 

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# flt'PchAI Hyckoc•n 

# <hlof• HCI URiC



# ..... 0.0002 211 . 71 ""'

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# ppm 

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# ........ Hvdroc•n n-ido HF \Mi t 0 . 0001 O . CM

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# O.OOOJ 0.07 

# PfM" 

# 0
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# SF6 

# 0.00)) 

# 0.0031 0
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# Oppm 0.02 

# ppm



# o..,., R"idu.al 0.0014 

# 0
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# O.le TOe Spmrumfite 

# S/14/2010 11 : 15:01

**:\ C•k:mot~s**  **\201 55**  

# cbl 

# t ilt\ 20100514\ HI cts 

# scon BdO< o Run 1_03130.SPE S/14/2010 11:15 : 19

**C:\CalunctS~\201SS** 

# d>llilo\20100514\ HI cts 

# sc.on Bolon Run 1_03131.SPE 5/14/2010 11:15:22 C:\Cil<metSamplts\201SS dol til t\20 100514\ HI cts scon klort 

# Run 1_03132-SPE AVG Water "• 

# Unil 

# 0
..... " 0 ""'"" 

# 0 

# vol·" **com~ns.a bs~**  

# Myckocen 

# chbidtt ttd Unit

- 0.0016 0 

# ppm wtl 0.0007 0.06 ppm 

# Ml O.OOil 

# 0.03 ppm Roslclual Hydrocon 

# fkl«ide Hf Urit 

# 0
. 0008 

# 2U
. 71 """ 0
. 0001 21l
. 89 

# ppm 0.0004 212
. 13 

# ppm 212
. 60 ResHiu•l Sf6 

# 0.0004 0
. 004 

# 0.0025 Unit 

# Oppm 0.02 ppm

0 Pl>ftl **Re~** 

# 0
. 001 0
. 0013 0
. 0011

# Olt~ 

# S/14/2010 S/14/2010 S/14/2010 **r.m~** 

# SpectrUI"'I\File 

# 11:19 :20

**C:\Calc-~\201SS** 

# dol lit\20100514\ Sf6 CIS....., 

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# l_0310.SP£ 11:19:22

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# l_OllOUPE 11:19:25 C : \C•kmeiS.mples\201SS d•llilo\20100514\ Sf6 ,,. .an 

# eorore Run 

# 3_0314S.SPE AVG **Wat•r~apoUrMC** 

# 0\001-% 

# 0 

# vol·" 0 

# vol·" Com

**pen~** 

# Residua& Hydfoten chkN'HS. HCI Un ._ 

# Reslduol Hyd<ocen fluotide 

# HF 

# UniC wt1 

# o . oon o.oe ppm 

# 0
. 0001 0
. 04ppm 

# w•1 0.0015 0 ppm 

# 0
. 0006 0.01-

.... 0.0008 

# o. 71 ppm 

# 0
. 0001 O
. OJR.-.a Sf6 

# u ... Resi<kl

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# o . oozz 9.9 ppm 

# 0
. 0016 0
. 0018 9.!1 ppm 

# 0.0018 0.0043 10.1 

# ppm 

# o . oozs 9
. 97

# HCL Dalllalla

Sm 

# -&pllood 

# Oalo Dolt 

# S/14/1010 5/14/1010 S/1.,-2010 MetM<II 

# 320 320 320 

# f"tn•m• HCI(ppm( 11
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# 2'J,Il Ava.



# Cone.(- **~** $F6

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# 0
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# .. , I O.H7l 

# S..- Hal l ve Cone. 

# 01 onalyOo 

# D•w 5/14/2010 5/14/2010 5/14/2010

Sm 

# Su Df 

# Cs Ct ..... hod 

# 320 

# 320 320

**ftt.<:overv(~);~~** 

# Ct
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# Of II($. 

# Su(l·Of ) 

# 21.31 ..,... 

# 6.77
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# '-4"" zoo.• ppm 

# 9.98 ppm 

# 2US ppm **Fi~ftlmt**

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# OhCJ 

# HCIIPI>"'I 6
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# us 712 AVJ. 

# C:DAc. (ppm,c:::::!ID Sf6 (ppm( 

# 0.03 0
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# 0 

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# - S/14/2010 ll:OC:02

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# S/14/2010 13:04:27

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# -· S/1./1010 U:04:52 C:\CIIcmtLSirnples\20tSS 

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# ~/14/2010 

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# wtt Hati" 

# Data

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# S/14/2010 12:11:17 C:\Calc:I!'NtS..-npt.s\20155 dal 

# tile\20100514\Wtl S<t*r l before run l_Ol300.Sf'[ 

# t• . n vol·" Wtl 

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# - 5/14/2010 12 : 32 : 49

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# 0
. 0004 9
. 91 ppm 

# 0
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. !141- 0.0021 0.0021 l.42 ppm 

# 0.0004 

# 11.16- 0
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# Sf6 Unit

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# 0
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# 0
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# 0.00< O
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# 0.0016 0
. 0041 24.31 ppm 0
. 000< 

# 1U7p""' 0
. 0067 D 

# ppm 0
. 0031 0
. 00!8 29
. 13 ppm 

# O
. OOOJ "
. 53 ppm 

# 0.005 0
. 01 ppm 

# o . ooza Hydroc;f:'n c:hlorUn i t Residual Hvdroc:en ftu.Un 6t R e sidual Sf6 U a i t

**"tsidu~l** 

# O
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# i.53 PPM 

# o.oooe 11
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# 0
. 03 ppm 

# 0.001. 0.0035 

# , , 65,. 0.0007 

# 12
. 17 PCif11 

# 0
. 0057 

# O
. OJ ppm 

# 0.0026 0.0031 7tlppll' 0
. 000!1 

# 13.16 ppm 

# 0.005' 

# o.,.. 0
. 0025

# HF 

# Dolltalia

Sm -$p1Md D.Ua 

# D•t• S/12/lOlO S/12/lOlO Slll/lOlO Method 

# ]20 320 

# l20 

# F._.me HJ(ppml SF6 (ppm) )0 , ), 

# 0
. 99 

# U .l, 

# .... lO

. S7 

# ...

**Aw&.Conc.~~** 

# I 0.11571 

# k-H.ciwConc.OfiNIIy\e Ottt Method Iii<
..... Hf{ppmt 

# SF6 {ppm) 

# SIU/lOIO llO 

# ll
. 3l 0.01 

# S/11/1010 120 

# U
. l7 O.Ol 

# S/12/1010 JZO U
. JI5 

# 0



# A~. Conc.(ppm. 

# t%.2111 

# I o.o:zo 

# I

s-


# ... Df Cs 

# Co R.HcweryC"l* Ce•

**Df•Cl•~t..()F)** 

# ,...,. 

# .... 12..29 ppm 

# ' · ·"" 212.0 ppm 9.98 

# ppm 

# ll.Ol ppm 

# Sm Su(l·OF) 

# Df 

# xes

MMn COM....U.tloft of spi(ecf

**~t** 

# NMM

**tonc:enttat~** 

# al 

# iulft* Dllutloft 

# Factot {hr'e1 

# < tOIK, 

# Cytln
.. of 1.pilH ,., 

# Cylinckf Qf 

# uac« 

# cu [SF6) 

# bpectH con cenlr ae ion of

**an.~Jyte**



# R~onrv 

# C")l M.S'It! 70·130!1

Spike Data SFi 

# .... 

# .... $p«trumfWe 

# Water

**vapo~** 

# ,.On.t

**Com~ns.fiof)** 

# S/l4/l010 lJ:Ol:56 

# C:\(.eknwtS.mpl.n\101SS.daltilt\:20100$14\Wet

**Sc.n~Mr** 

# J SF6 spike IM:fotCI rutt l_OlS 

# U
. 4S vol·% 

# .... S/14/1<110 U:OI : Ol C:\c.lc..UMnPiet\201SS.cW tk\l0100S.l4\Wet ScrvMrl SF6
.... befofe n.tn 

# l_OJS 

# U
. tlvot-" 

# -· S/14/lOlO 

# U : 04:CJI C:\ColktH1.S....,...,\201S!.cNI t•\10100514\Wet Scrwt.l Sl'

**s,~r~ befof~**  tun 

# 1 _o n 1U2vol-!l 

# -

**Sp._~OM~** 

# ... 

# .... ..... StM<trutnF• WMtr Y l pot

**~Untt**



# ~ 

# S/14/lOIO 

# ll:Dl :4 7

**C:\c.k."'CtS ~U01SSct.l**  

# tlle\20100SI4\Wtl $cr'*t 2hf
... INfo« fP.Ml_DJS71 

# u . •s 

# ¥01·" 

# - S/14/lOlO 

# ll:Ol:SJ

**:\C.tc metSao~t\201S~**  

# cW 

# tile\l0100S)4\Wet Sen••' 2:hf tpille befort ,,.. 

# l_OJS7!. 12
. 47 

# \10111·" 

# -· S/14/lOIO 

# U:Ol:St

**!\C kmdS.~tUOlSS** 

**d~** 

# tleUOIOOS14\Wtt Scrubcr 2:hf IP ib bf:tore run 1_0JSIO U
. 48vol"' 

# -· Naliw

**o~••** 

# Hf..SF6 

# .... T.,..

**Spt<~•umfllt** 

# Wattt VlpOr
.. Untt

**Cam~nulion** 

# S/14/lOlO 

# 12;12::37 C:\CekmtUampln\201SSdJitile\20100S14\Wet Scruber 1 

# tMtor• tuft 

# I_OUOO.SP£ 14 , 7)

**O~ "**  

# w .. S/14/lOlO 

# 12:32:0 

# C:\c.km.ttSampiH\lOlS!.dal Ule\2:010DS14\Wet

**S<ru~rl** 

# Mfort run I_Ol301.SP£ 14 .67 \IOI • " 

# w•t S/1 4/lOlO 

# l2:Jl :.t9 C:\CJicmct.S•mpltt\201S!tdal Ule\20100U4\Wt'l

**Scru~r** 

# l:

**~fort** tuft 

# l_DJlOl.SP£ 14 .6S vol-" 

# w•• **~** 

# ........ HydfOJHIUr'li( 

# Rnld•l Hy4ro&M tluot1dt HF Unit 

# Rcstdwl Sf6 UM Residual 

# 0.0024 1.73 

# p,_ 

# o.ooos 9.19 

# ppm 

# 0.0002 0.99 liP"' 0.0024 

# 0.0022 

# 0
. 99""' 0.0000 

# ..,,,... 0
. 0004 0.91
.. ,. 

# 0
. 0021 O.OOl l

**'2~** 

# 0.0000 

# ll
. K,..., 0
. 004J 

# ... 

# _ O.OOIJ 

# ··- Hy4toaen 

# tUM

**~~** 

# tfVdlOftft..,..Hf Unl< RtsWIHI Sf6 

# ...... 

# ......... 0 .002 4 S.lppm OA>DOJ JO.J6.pprr'l 

# 0.0047 

# o,... 0.0017 0
. 0021 

# S.16ppm 0.0000 

# JUt- 0.0006 

# 0.01 PP"' 0.0016 0
. 0021 

# 2., "'"' o.oooJ 

# JO
. S'

**'~""** 

# o.ooos Oppm 

# 0.0017


# Resldull ttvdrocen cUnit 

# Rnldual Hydroatn 

# n u Qflcft HF 

# Unit lesidwl Sf6 Unit 

# Residual 0.00>2 l!i.Slppm 

# O.O!XIt 

# n.u ppm

**0.00~7** 

# 0
. 0) 

# ;rrpm 0
. 0024 O.OOJS UiS PP11 

# 0.0007 

# 12.17 ppm D.DOS7 0
. 0) ppm 0
. 0026 0
. 00]1 7 , 11 ppm 

# 0.0009 

# U
. J6 ppm 

# 0.0019 o..,m 0.0025

# D1t~ 

# S/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 S/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 S/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 Time SpectrumFife 

# 14:03:10 C:\CokmetS.mplos\20155 dol tile\20100514\Wot 5crubor 2 rvn 1_03781.SPE 14:04:11 C:\CokmotS.mplos\20155 dal tile\20100514\Wot 5cruber 2 run 1

_ 03782.SPE 14:05:11 C:\Cokmot5amplos\20155 dol

**t~e\20100514\Wet** 

# 5cruber 2 rvn 1_03783.5PE 14:06:11 C:\CalcmotSomplos\10155 dal Ulo\20100514\Wet Scruber 2 run 1_03784.SPE 14:07:13 C:\CakmotSomplos\20155 doltilo\20100514\Wot Scrvber 2 run 1_0378S.SPE 14:08:13 C:\CokmotSomc>los\20155 dol t;r.\20100S14\Wot Scrvber 2 rvn 1_03786
. SPE 1 4 : 09:14 C : \CokmotSomc>los\20155dol tilo\20100S14\Wet Scrvber 2 

# run 1_03787.SPE 14 : 10 : 15 C : \CokmotS.mc>los\20155 dol tilo\20100S14\Wet Scruber 2 run 1_03788.SPE 14:11:16 C:\CokmetSomplos\20155 doltilo\20100514\Wet Scruber 

# 2 run 1_03789
. 5PE 14:12:16 C:\CokmetSompl«s\20155 dol tilo\20100514\Wet

**Scn~bor** 

# 2 run 1_03790
. 5PE 14:13:17 C:\CokmetSomplos\20155 dol tilo\20100514\Wet ScNbor 2 run 1_0379l.SPE 14:14:18 C:\CokmotS.mples\20155 d•l tile\20100SI4\Wot Scrubor 

# 2 "'" 1_03792.5PE 14:15:19 C:\CokmetS.mplos\20155 dol tile\20100514\Wet Scrvbor 

# 2 rvn 1_03793.5PE 14:16:19 C:\CokmetS.mplos\20155 dal tilo\20100514\Wet 5cruber 2 run 1_03794.SPE 14:17:20 C:\Colcmet5amplos\20155 dol tUo\20100514\Wet 5trubor 

# 2 rvn 1_03795.SPE 14:18:21 C:\CokmotSamplos\20155 d•l tije\20100514\Wot Scrubor 2 rvn 1.03796
. 5PE 14:19:21 C:\Colcmet5ompl«s\20155 doltile\2010051 4\Wet Scrvber 

# 2 run 1 _03797.5 PE 14:20:12 C:\CaltmotS.mplo s\ 20155 dol tile\20100S 1 4\Wet Scrvber 2 

# run 1.03798
. 5PE 14:21:22 C:\CokmetS.mc>los\20155 dol tilt\20100S14\Wet Scnsber 2 run 1.03799 .SPE 14:22:23 C :\ CalcmotS.mc>los\20155 dol tilo\20100S14\Wet Scnsber 2 

# run 1 _03800.SPE 14 : 23 : 24 C : \ColcmetS.mc>los\20155 dol tilo\20100S14\Wet Scnsber 2 

# run 1.0JI01
. SPE 14 : 14 :1 4 C:\Cakmot5omc>los\10155 dol tile\20100514\Wet Scrvber 2 run I.OJI02.SPE 14 : 25:25 c:\C•Icmet5omplos\20155 dol tilo\20100514\Wet ScflJbor 2 run I.OJI03.SPE 14:26:26 C:\CaltmetS.mplos\10155 dol tile\20100514\Wet Scrubor 2 run 1_03804.5PE 14:27:27 C:\ColcmetS.mplu\20155 dol tile\20100514\Wet Scruber 2 run 1_03805.5PE 14:28:27 C:\CokmetS.mplos\20155 dol tllo\10100514\Wet Scrubor 2

**n~n** 

# 1_03806.5PE 14:29:28 C:\CokmotS.mplos\20155 dal tile\20100514\Wot Scruber 2 "'" 1_03807.5PE 14:30:29 C:\CokmotSamploJ\20155 dol tile\20100514\Wot 5crubor 

# 2 rvn 1_03808.SPE 14:31:29 C:\CakmetS.mplos\20155 dal tile\10100514\Wet Struber 

# 2 rvn 1_03809.SPE 14:32:30 C:\C.Icmet5amplos\20155 dol tilt\20100514\Wet Scrvber 2 rvn 1_03810
. 5PE 14:33:31 C:\CalcmotS.mplos\20155 dol tilo\20100S14\Wet Scruber 

# 2 run 1.03811
. SPE 14:)4:32 C:\CalcmotS.mc>los\20155 dol tie\20100S14\Wet Scrvber 2 

# run 1_03812-SPE 14:35:32 C:\C.IcmotS.mples\20155 dol tilt\20100S14\Wot Scnsber 2 

# run 1_03813.SPE 14 : 36:33 C:\CalcmotS.mplos\20155 dol tilo\20100S14\Wet Scrvber 

# 2 

# run 1.0381'-SPE 14 : 37:33 C:\CakmetSomples\10155 dol tile\20100S14\Wet Scruber 

# 2 "'" 1_03815 .5 PE 14 : 38:34 C:\CalcmetSompl«s\20155 dol tile\20100514\Wet

**Scn~bor** 

# 2 Nn 1_03816.SPE 14:41:06 C:\CalcmetS.mplts\20155 dol tile\20100514\Wet Scrubor 2 Nn 1_03817.SPE 14:42:07 C:\C.kmetS.mplos\20155 dollilo\20100514\Wet ScRJbor 

# 2 run 1_03818.SPE 14:43:08 C:\CokmoiS.mplos\20155 dol tllo\10100514\Wet Scrubor 2 "'" 1_03819.5PE 14:44:09 C:\CokmotS.mplos\20155 dal tile\20100514\Wot 5cruber 2 run 1_03820.5PE 14:45:09 C:\CokmotSamplts\20155 dal tilo\20100514\Wot Struber 2 

# rvn 1_03811.SPE 14:46:10 C:\CokmetSomples\20155 dol tilo\20100514\Wot ScRiber 

# Z "'" 1.03822.5PE 14:47:11 C:\Cak;metSomptes\20155 dol tile\20100S 14\Wet Scruber 

# 2 rvn 1_03823.5PE 14:48:12 C : \CaltmetSomplo s\ 20155 dol tilo\20100S14\Wot Scrubef 

# 2 

# run 1_ 03824-SPE 14 :49:12 C:\CaltmotSamples\20155 dol tile\20100SI4\Wet Scrvber 2 rvn l_03825.SPE 14:50:13 C:\CaltmotS.mplos\20155 dol tilo\20100SI4\Wot Stnsber 2 ""'

**I_038~.SPE** 

# 14:51 : 14 C:\CalcmetS.mplos\10155 d•l tilo\20100S14\Wet Scruber 

# 2 run 1_03827
. SPE 14:52:14 C:\C.IcmotSamples\10155 dol tilo\20100S14\Wet Scrubor 2 

# run 1_03828.5PE 14:53:15 C:\Colcmot5amplos\20155 dol tile\20100514\Wot 5crubor 2 run 1_03829.5PE 14 :54: 16 C:\Calcmet5omplos\20155 dal tile\20100514\Wet Scrubor 2 "'" 1.03830.SPE 14 :55: 16 C:\CalcmetSomplos\10155 dol tilo\20100H4\Wet Scrubor 2 rvn 1_03831.SPE 14 :56: 17 C:\Calcmet5amplos\10155 dol tllo\20100514\Wet Scrvber 2 run 1.03832.SPE 14:57:18 C:\Calcmot5omples\20155 dol tii«\20100514\Wet Scrubor 2 run 1_03833.SPE 1 4 : 51:19 C:\C•Iemet5omplos\20155 dat tlle\20100514\Wet Scruber 2 run 1_038)4.SPE 14 : 59:19 C:\Colcmet5omplos\10155 dat tilo\20100514\Wet Scrubor 2 

# run 1_03835
. SPE 15:00:10 C:\Cakmet5omples\2015S dol tilo\20100S14\Wet ScRiber 2 run 1_03836
. SPE 15 :0 1 : 21 C:\Calcrnet.SanoPes\20155 dol tile\20100514 \Wet Scruber 2 run 1.03837.SPE 15:02:21 C : \CalcmetSomplos\10155 dol tilo\20100514\Wot ScRJbor 

# 2 run 1_03838.5PE 15:03 : 22 C :\ CakmetSomc>los\20155 dol t;r.\20100514\Wot Scrubor 2 

# Nn 1_03839.5PE 15:04:23 C:\Cokmet5ornjMs\20155 dol tile\10100514\Wet Scrubor 2 run 1_03840
. 5PE 

# AVG W1te1 '4'.1PI Unit 

# 17.37 vol·% 17.73 VOl·% 17
. 19 VOl·% 17.45 vol

- % 17.47 val · % 16
. 97 

# val·" 16
. 88 \101-% 17
. 28 \101-" 16.98 \101-% 16.65 val · % 16.7 val·" 16.68 val · % 16.79 VOl·% 16.63 1101 · " 16.26 vol · " 16.25 VOl · " 17
. 19 vol-% 16.6 VOl·% 16 .7 val·% 17
. 19 vol-% 16

. 97 val · " 16.59 val · % 16.89 val·% 17.41 1101·% 17.17 1101·% 16.48 1101·" 16.27 vol·% 16.11 1101 · % 16.23 VOl·% 16.65 vol·" 16.08 vol · " 16
. 21101-% 16

. 56 

# val·% 16.5 val · % 16.59 \101-" 16.54 

# vof." 16.99 1101·% 16.36 1101·% 16.74 1101·% 16.59 vol

- % 16.76 vol·% 16.74 vol ·% 17.03 val

- % 17.65 1101-% 17 .1

**vo~%** 

# 17.35 val·" 17
. 14 vol-"

**17 1110~"**  

# 17.27 1101 · " 16.68 vat-% 16.53 YOI·" 16.49 YOI·" 16 .97 vol · " 17
. 04 vol · " 16 .89 

# vof." 16

. 75 val · " 17.29 val · " 17
. 4 vol-% 17
. 22 val · " 17
. 17 

# vof." 16.86 Co mpenu Rtosidual Hydroten c Unit 

# w o t 0.0045 2.84 ppm 

# wot w o t 

# -· -· 

# -

· 

# - - 

# - lftt 

# wot w ot wet wot 

# wot 

# wet w o t wet wot 

# - - 

# - wet wot 

# wet wot 

# wet wot wot wet 

# wet wot wet 

# - wet wet wot wot wot wot wot wot wot wet 

# -· 

# - wet 

# -· wet 

# -· -· -· wot 

# -· wot 

# - - - - -· 0.0047 0.0045 0.0045 0.0046 0.0045 0
. 0044 0.0046 0.0044 0.0043 0
. 0044 0.0042 0.0043 0.0042 0.004 0.0042 0.0045 0.0042 0.0043 0.0044 0
. 0043 0
. 0042 

# 0.0042 0
. 0045 0.0044 0.0042 0
. 0041 0.0041 0.0042 0.0043 0.004 0
. 004 0.0042 0
. 0042 0
. 0042 0.0042 0.0043 0.0042 0.0043 

# 0.0042 0.0043 0.0043 0.0044 0.0045 0.0043 0.0045 0.0045 0.0044 0.0044 0.0043 0.0042 0
. 0041 0.0044 0.0044 0
. 0043 0
. 0043 0.0046 0
. 0045 0.0044 0
. 0045 2
. 42 pp m 2
. 54 pp m 2
. 58 ppm 1
. 5 ppm 2
. 34 ppm 2
. 17 ppm 2.3-1 ppm 2.28 ppm 2.36 ppm 2
. 57 ppm 2
. 23 ppm 1
. 15 ppm 1.87 ppm 2.8 ppm 1.7 1 ppm 2
. 4 7 ppm 2
. 27 ppm 2.17 ppm 

# 1
. 9ppm 1
. 69 ppm 2 .5 3 ppm 2
. 51 ppm 3
. 31 ppm 2.33 ppm 1 .98 ppm 2.99 ppm 2
. 5 ppm 1
. 98 ppm 1.94 ppm 1
. 78 ppm 

# 1
. 78 ppm 

# 2
. 49 ppm 

# 2.2 ppm 2.19 ppm 1
. 7 ppm 18.94 ppm 17
. 16 ppm 16.86 ppm 16
. 3 ppm 15
. 38 ppm 18
. 25 ppm 18.94 ppm 

# 16.3 ppm 19
. 66 ppm 

# 18
. 46 ppm 

# 13
. 77 ppm 

# 14.14 ppm IB2 ppm 15.64 ppm 15.03 ppm 15.14Wm 17.16 ppm 19.8wm 14.47 ppm 15.19 ppm 15 .27 ppm 16
. 87 wm 13
. 92 wm 12.4Swm 7.88 Residual Hydtocen f Unit 

# 0
. 0004 9
. 58 ppm 0
. 0004 10
. 9 ppm 0
. 0005 8.92 ppm 

# 0
. 0004 0
. 0004 0
. 0004 0
. 0004 0.0005 

# 0.0004 0
. 0004 0.0004 0.0004 0.0004 0.0004 

# 0.0004 0
. 0004 0
. 0004 0
. 0004 

# 0
. 0004 0
. 0004 0.0005 0.0005 0.0004 0
. 0004 0.0004 0.0003 0.0003 0
. 0004 0
. 0004 0
. 0004 

# 0
. 0004 0
. 0005 0
. 0003 

# 0
. 0004 0.0004 0
. 0004 0.0058 0.0055 0
. 00$3 

# O
. OOS3 0
. 0054 0.0059 0
. 0062 

# O .OOS7 0
. 0062 0
. 0061 

# O.OOS2 0.0053 0.005S 0
.

0052 

# o.oos 0
. 0051 0.0062 0
. 0066 0.0052 0
. 0053 

# O
. OOS3 O
. OOS3 O.OOS1 

# o.oos 10
. 34 ppm 9.08 

# ppm 9.01 

# ppm 8
. 77 ppm 

# 9
. 09 ppm 8
. 41 

# ppm 8.9ppm 9
. 35 

# ppm 

# 9.12 ppm 9.07 ppm 9
. 31 ppm 8
. 71 ppm 8.47 ppm 9.06 ppm 8.87 ppm 

# 8.08 

# ppm 

# 9
. aa ppm 8.92 ppm 

# 8.3 

# ppm 8
. 22 

# ppm 8
. 14 ppm 9.43 ppm 8.32 ppm 7
. 26 ppm 8
. 29 ppm



# 8 ppm 9.47 ppm 

# 8.65 

# ppm 9
. 14 ppm 

# 8.39 ppm 1.65 ppm 

# 8.58 ppm 

# 8.65 ppm 7.99 ppm 8.29 ppm 8
. 5 ppm 9
. 02 ppm 8.2 ppm 8.93 ppm 

# 1.64 ppm 

# 10
. 47 ppm 9
. 18 

# ppm 9.92 

# ppm 10.01 ppm 9.44 ppm 8
. 44 ppm 9.67 ppm 9.2 ppm 7.91 ppm 9.35 ppm 8
. 96 ppm 8
. 41 ppm 10
. 08 ppm 9
. 18 ppm 

# 9.09 ppm 8.83 ppm 8.96 ppm 

# 8.94 

# Res i du11 SF6 0
. 007 0
. 0064 0.0069 0.0063 0.0071 0.0068 0
. 0068 0
. 007 0
. 0068 0
. 0067 0
. 007 0.006 

# 0.0071 0.006 0.0067 0.0063 0.0069 0.007 0.0068 0
. 0065 0
. 0069 0
. 0067 0
. 0068 0
. 007 0
. 0068 0 .0065 0
. 0066 0.0064 0.0066 0.006 

# O.OOS9 0
. 006 0
. 0068 0
. 0069 0
. 007 0.0068 0.0066 0
. 0067 0
. 0071 0.00 7 0.007 0.0069 0.007 0
. 0066 0
. 0072 0.0065 0
. 0064 0.0064 0.007 0.0063 

# 0.0062 0.0067 0.0072 0
. 006 7 0
. 0068 0.0066 0
. 0073 0.0073 0.0068 

# 0
. 0072 

# Unit Owm 0 ppm owm 

# o ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# o ppm owm 

# 0 ppm 

# o ppm 

# 0 ppm 

# o pp m 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# o ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm owm 

# o ppm Oppm 

# Oppm 

# 0 ppm 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# o ppm 

# o ppm owm owm 

# 0 ppm 

# Oppm Ownn 0 ppm 0 ppm 0 ppm 

# 0 ppm o ppm 

# o ppm 

# 0 ppm 

# 0 ppm 

# o ppm 

# o ppm 

# 0 

# ppm 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# 0.00 **R~stdu1l** 

# 0
. 0028 0
. 0039 0
.

00 29 0.0038 0.0032 0.0033 0
. 0033 0.0031 0.0033 0
. 003 0.003 0.0034 0
. 003 0
.

0037 0,0031 0.0035 0
.

0035 0.0029 0
. 003 0
. 003S 0
. 0033 0.0033 0
. 0035 0
. 0036 0
. 0036 0
. 003S 0.0033 0.0035 0.0034 0.0033 0.0033 0
. 0033 0.0028 0
. 003 0
. 003 0
. 0027 0.003 0
. 0031 0
. 0032 0.003 0.003 0.0031 0.0029 0.0035 0
. 0029 0
. 0037 0.0035 0.0034 0
. 0031 0.003-1 0
. 0036 0
. 003 0.003-1 0.0033 0.0032 0.0036 0
. 0032 0
. 0033 0
. 0032 0
. 0033

# HCL Dalltalia

**Sm~lcodData** 

# O.tt S/14/:010 S/10/2010 S/14/2010 

# Method 320 320 320 Filtn_.t 

# HCI { ppmj 29
. 53 21
. ?6 

# 30.24



# Ava.Conc.{-1~ Sf6 

# CppmJ 0.93 0.99 

# o . n 

# I o.t)SI 

# s..-- Cone. 01 

# ana¥- o ... S/14/20 10 S/14/2010 5/ 14/2010

Stn 

# s.. Of 

# c. 

# c. Method 

# 320 320 320

Aei:CWtf'Y(%)• 

# c.. 

# Of., ,. Su(l·Df')


# 29.51

- 14 .0 PPM 

# 9.4"" 200.1 ppm 

# 9.9& ppm 

# ll.SS ppm 

# Ftlefllam4:



# Sm · So(1·Dfl

DfxC:. 

# ltCICPt>ml U5
. 17 

# 1).92 

# 12.48 SF6 

# Cppm} 

# 0 

# 0 0 

# Ava. Cone. 

# (ppm 

# tO§ I I

...... cootetllfili<>n 

# ol .,....,.....,... Nat• COftCMttalilo.. 

# ol

**.,~.** 

# Ditution

**~actor** 

# (T¥1t' < 

# 1'"'-} Cyliftdtf' 

# ol "Piktd I.U 

# CyliftdiK oltr•C"ff 1ft• 

# (SF6) Elcpected 

# concentration of M•lytt 

# Roco
.. rv 

# 1'<1! aU%! 

# 70·110"


# s.>ittd«a Sf6 O.t• limo 

# Spe<uwmJM Wat tt

**~r~~ap<UI"'II** 

# ComP"Hbon

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. SPE 5/141/2010

15

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. 0061

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0

. 00}1 5/14/1010

1' :20: .U C
: \CakmotS-amplti\201SS

**d~** tiiii!'\2:0100514\Jiun l)MOlSI

. Sf(
**~~.** ...... " -·

0

. 004S 1S.69 ppm O.OOS4

1
. 7) ppm 0.0064

0 ppm

0
. 00!1 5/14/1010 **:21:2**
C

: \Ca1C:meW.mplt1\l0lSS

dJJ tH11!\l0100S14\I!:"n l_04040 ,SI ( 22!9 vol·!l -·

0

. 004 S 16-76 ppm O.OOS4

I

. J PP" 0.0066

0 ppm

0

. 00)5 S/14/2010 16:22:23

C

: \Calcm

e tSampln\l015S

dill tilt\2G100S14\ftun

l _ Oo1D41.Sfll ll.16YOI-"

... t 0.00ol5 14.41 ppm 0.005! 1.05 ppm 0.0064

0 ppm

0

. 0012 5/14/2010 16:21:23 C:\C•tmets.ampln\20155

dill tilt\20100514\Run 2:,.041042.Sfll 11.51 val-" ....

0

. 0045 15.4 ppm

0
. 005)

9

. 1 pl)m 0.0066

0 ppm 0.0015 5114/2010 16:24:241 C:\CJfcmet.S.empln\20155

dill tilt\20100S141\Run 2_040U

. Sf'l 22.37 .at-" wet

0

. 0044 16.5 ppm O.OOS) 1.)1 ppM 0.0066

0 PPM

O
, OOll 5/14/1010 l6:1S:25 C:\C•Itmll!'t.Simplts\20155 diilllilt\20100514\Run l_0404C

. SPI 22.07 voi-'K wtt

0

. 0044 15.47 ppm 0.0049 9.06 Pt>M 0.0067

0 .....

0

. 00!1 5114/2010 16:16:26 C:\CakmetSample-s\20155 dallilt\20100514\Run 2_010-tS

. SPI!!

22

. 04 wl - " Wtl

0

. 0044 14.75 ppm

0
. 0051

1
. 2 .... 00065

0 ppm 0.00)ol S/14/1010 **17~26** C:\C.tc:m

• t.S.I"'plft\20155
dal ti!e-\l0100S14\Run l_OI046

. SPt: 12.0) wi·'K Wtl

O
. OOoll
14

. 14 ppm

O . OOSl

7
. )5-

0
. 0062

0 ppm

0

. 00)) 5114/2010 **l~l7 \C.kmtts.•Pe-s\201SSct.~•\20100514\lltun** 

z_o.on

. m

21

. 61 wa-• w•t 0-)

15 .8 pcwn

0
. 0051

7 . tJwn 0.0064 Oppm

0

. 00)2 S/14/2010

16

: lt-21 **"*~\lOISScbl** **ftle\lOt<IOSt~** 2_040d

. SPf l,.S6vof-." -t 00054 ).19ppm

0

. 006 u. .. wn

0
. 0071 Oppm 0.00ol5 5/14/2010 100:11
**,'tt ok~\lOIS5dollifo\lOIOO>lol'"'"'**  l_OOOoi9.SH 19.18 ... ,. -·

0

. 0051 .t.7Soom

0
. 0051

11

. 16wn

0

. 007 Oppm

O .O OrU AI/G

19 - 15

11

. 6)

10.55

000

# HCLDaJ-.
Sm...s,IMdOMa O.Cc 

# 5/14/2010 S/14/2010 5/14/2010 

# -hod 320 )20 320 F iltMmt 

# HCI(-1 2J
. 04 lJ.7J 

# n .

69

**A"8-Cooc.(pl"")~** $<5 

# (ppm) 

# o . .. 0.96 

# o.,J 

# I unl Su
- 

# Natift Cone

. ot an•lyte 

# Date 5/14/2010 S/14/2010 5/14/2010



# Sm 

# .. Of 

# c. Cc Method 

# J20 

# no 120

Recowry "") • 

# Ct • OF • Cs • SuCl·Of) 

# U
. lS ppm 

# 8
. 16 """ 9
. 5"" 2 00
. 8 ppm 

# 9.98 ppm 

# u . •J PP"' 

# Filename

Sm • Su{l•Df)



# Of 

# JCC s **~CI(ppm)** 

# lS.I U9 4
. 78 Ava

. COnt.



# {ppm)~ Sf& (ppm) 

# 0 

# I

. 

# J

MtiA

**COIKtftlf~tion** 

# of spik.cl .-llylt 

# k•tiw conceatr•tion ol

**~·** 

# Dilution 

# Fector (T•1et < 

# 10%)

**Cyl;odet<ll~** 

# ,., Cykckf 

# ol tfiCfl' 

# liS (Sf6t bpec\H

**coaceau~tion** 

# o4 Matytto 

# Rcc.....,!"'! 

# 1ae .O?q 7 0 ·1 30"
Spite 

# dM.I SF6 O.te llf'l'lt 

# S/14/2010 5/14/2010 5/14/2010 Spike d1t11 HCl 04itc 

# Tim t 5/14/2010 5/14/2010 5/14/2010 N•tfw 0.111 HCI ·.S F6 

# D•t• 

# nme S/14/2010 5/14/2010 S/14/2010 S pecerumFtle: Wittr vapc Umt 

# CoiRI)fl'sation Res•du•f 16 : 14 : 21 C.:\CakmetS•mptes\10155 dal tik\20100514\wel scr..tt1Mr2 Sf6 Spike After

**Au-.:_~** 

# \&.46 Vol·" 

# wet 16 : :W : 27 C:\CflcmttSarnptn\2:01SS dM tH\20100514\Mtl 

# scrutiiMrl SF6 Splitt Alter 

# Avn 2_060f 16.48 

# vol·" 

# ... 16 : 14 ;33 C:\CilcmetSa.rn.,les\20155 d-'

**tie~\20100514\wcl** 

# s.ctubberZ SF5 Spit(e Aher Run 

# 2 _0406 

# 16.lS 

# vo4·" 

# ••• SputrumFile Witer ViP( Unit

**Compens.~tion** 

# Rcs.du•l 16:ll:ll C:\C•IunetSamples\201SS dal tile\20100514\wet suubbtrl Hcl S,.ke After Run 1_040S 

# 17.49
.... " 

# ... 16 : ll : l9 C:\C-iil(mttSJmples\201S5 dil ti1e\20100Sol4\wtt s.crubbefl Hcl $pikt Ahtr Run 

# 2_040S 17
. Z vol·" 

# w•l 16 :ll:4S C:\C...IcmetS.ampJes\20155 dal 

# tile\20100514\wet saubberl Hcl Sptke After fll.un 

# 2_040S 16.77 vol-" 

# wei
Sptttrumfile W • ler VIP< Unit

**Co.m~n'l-llion** 

# Rnfdual 16:lt:l1

**C:\C.IcmtlSimple~oUOlSS** 

# del Ult\20100S14\Run 2_04047 .SP E 21.61 vol-" 

# wet 16:29 : 21

**C:\Calcme~mplts\201SS** 

# del rtle\20100!t14\Run 2_040U .SP E 

# 19.56 ""'·"' 

# - 16 : !0 :2 1 C : \c.lcmets.atnples.\20155 

# dal tNe\20100Sl4\Run 2_00049.SPE 

# 1U&¥01·" 

# -· **H~rocen** 

# d\lor Ul'lil Aa-sidull Hv*ocu 

# nuor i Ufliit 

# "-achllll Sf6

**Un~** 

# Rasedwal 0 .004 )
. 5

**~,..** 

# 0
. 0049 7.94 ppm 

# 0.0059 O .t!. p,n 0
. 0042 0.0041 

# s .•a

**P~** 

# 0.0040 10.05- ppm 

# 0
. 0057 0.96 ppm 

# O .O OJI 0
. 0041 6.95 PI"" 0
. 0048 9.2J ppm 

# 0
. 0054 O.!Jl ppm 

# 0
. 002& Hydrocen chlor Unh Rtsiduil 11vdroctn nuori Untt 

# R.eiidull SF6 \Jn h 1\ntd
...

l 

# 0.000 21.04 ppm 

# 0
. 0051 9.7& ppm 

# 0.007 Oppm 

# 0.004 0.004& 2t.7J ppm 

# 0
. 0054 11.81 ppm 

# 0.0066 O.OJ ppm 

# 0
. 0044 0.0044 ll.Upttm 0.0067 1.12 ppm 

# 0.0075 0.13 ppm 0
. 0011
Hydroctn 

# <hfOrUnlt

**~idu.l** 

# Hydroten fluoriUnit Res.idu•l Sf5 Unit 

# Rtsidufl 

# 0.0043 15
. 1 ppm 

# 0
. 0052 7;93 ppm 

# 0.0054 Oppm 

# O.OOJl 0.0054 

# l .lt ppm 

# 0
. 006 12
.... ppm 

# 0 .0073 Oppm 

# 0.0045 0.0051 4
. 71 ppm 

# 0
. 005& U.Ui ppm 

# 0.007 

# Oppm 0.0043

# HFOalbtlo Sm-$plllod0... 

# Oot• S/14/2010 5/14/2010 5/14/2010 Mol hod 

# 120 320 320


# Su
- hlative COftc. Of

**an:a~** 

# Dote S/14/2010 S/14/2010 S/14/2010

Sm 

# w Of (> 

# c. Me thad 

# 120 

# uo 320



# FWcowry ('%) • 

# Ce • 

# OF,. Cs + 

# SuCl-Of) 23.5* l)l)m 

# 10.64 ppm 

# U li li 212
. 0 ptllm 

# t
. tl

**~** 

# 29
. 47""" Ao<ovtry(li)c::



# ~

**Sp bO~aSF6**  **Filt,.~t**



# Filtniome

Sm • Su(t-1)1)



# OF.IICS 

# A"'-COIIC
. (ppm)

Ave

. 

# Cone
. {ppm) HF(ppm} 

# Sf6 (ppm) 21
. 23 

# o . n 22.1 0
. 99 

# lO.•t 

# o . u 

# I 23.s.l 

# I o.m 

# I

I Hf(ppm) 

# 5" (ppm) 

# 7.91 1U4

**1U~** 

# 10,UJ 

# I

Mun 

# concenuation of sP'ked

**~n~y1e** 

# Native contenlr41tion 

# of

**~n.alyt~** 

# Oilutton Fact« CT1r1tt 

# < 10%) 

# o,t i ftder 

# ot

**~piked** 

# cas Cybd<tt 

# Qf

**tr~** 

# ps (Sf6) 

# Etpeaed COftCt ftt ution 

# of anM,\e 

# 70 · BOli 0 

# I

Dot• 

# Tom•

**~cu~Ftle** 

# Water vapc. Untl 

# Compensation Rtsi4u,l 5/14/2010 

# 16 : U : -4S C :\ c.kmet.Samplts\20155 dit tile\20100514\we' scru bkrl Sf& 5pikt 

# After Run 2_040! 16
. 77 viM- % 

# wet 0
. 00ol4 5/1</2010 16 : )1 : 51 C:\Calcm•tSamples\20155 d
.. 

# t"e\20100514\wetsttubMrl SF6 

# Sp ikt Afttr lun 2_0405 16.52 vol-% 

# w•t 

# O.OOtl 5/14/2010 16:ll : S8

**C:\Citcmet$ample~\..l01SS** 

# dal tilt\20100514\wtt scrubbcrl 

# Sf' Spike Aher Jl:un 2_040! 16
.. . ...

**~."'** 

# w•t 

# O .OOt l Spikt

**0•~** 

# HF 

# 5/14/2010 16:42 : )2 C:\C..kmetSampiH\201SS dal titt\20100514\wet "crubbcrl HF Spike 

# Ahtr R1.11"11 

# , 2:_0'J.U 25
. 77 vol·% 

# w•t 0
. 0052 S/14/2010 16 : 42:38 C : \CakmetSamples\101$$

**d,-lil~\20100514\wet** 

# scrubbcrl Hf Spib After Aun J_04U ·

**2U~vol·li** 

# w•t 0.0051 S/14/2010 16 : 42 : .t4 C:\CalanetS..mples\201SS d.ttilt\2010051.\Wtt SC/IIbber2 

# HF 5pikt After Runl.04US 21.12 vol·" 

# wtt 0.0052 Native 0.11 

# Hf.SF6 

# Date 

# Time

**~pectrumfil•** 

# W•ltt YiiiP< U•it Compen'Salion

**Re~dual** 

# S/1012010 16 :2 & : 21 C:\CalcmttS-ilmptes\2015Sdal Ule\2010()5;14\Run 2_04047 .S Pl 21
. 61 VCJI·" wet 0.0041 S/14/2010 16 :2 9 :2 8 C:\C.Icmei.S.JmplesU01SS dal tile\20LOOS14\Ru" 2_04048.SPE 19.!.6 

# \1'01·" 

# .... 0.0054 S/14/2010 1' :3 0 :2$ C:\C.Ic:meiSampfes\20155 dal tile\20100$14\Run 2 0404,.SPE 19
. 1& vol·" 

# - 0.0051 Hydroctn chlor Unit

**Res~ Hydroc~**  

# fluor Unit Rtstd.wal SF& 

# UM 

# Rutctua• 32 .6

9 ppm 

# 0.0067 1.12 ppm 

# 0
. 0075 0.9) ppm 

# 0
. 00)8 18
. o& ppm 0
. 005 a.19 ppm 0
. 005, 

# 0." ppm 

# 0
. 0012 U
. 6J ppm 

# 0.00t9 7.91 ppm 0
. 0063 0.81 ppm 0
. 00)
.. 

# 17
.

09 ppm 

# 0
. 0056 28.23 ppm 0.0075 Oppm 

# O
. OOtl 1S.2J ppm 

# o . ooss 22.1 ppm 0.0067 0.02 ppm 0
. 004& 11
. 6! ppm 0.0054 

# 20.41 ppm 0.0072 Oppm 0.0044 Hydro1en chlot Uni1 -.sidual HydtGit" 

# Ruor U"it Rltsidual SF6 Unit Residual 1$

. 1 ppm 0
. 0052 7.93 ppm 0.0064 Oppm 0
. 0012 l.l' ppm 0.006 12.14 ppm 0.0073 Oppm 0
. 0045 4
. 78 ppm 0
. 0058 11.16 ppm 0.007 Oppm 0
. 004J

# Dat~ 

# S/14/2010 5/14/2010 5/10/2010 S/14/2010 5/14/2010 S/14/2010 S/14/2010 S/14

/ 2010 5/14/2010 s/1•/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 S/14/2010 5/10/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/1./2010 5/ 14/2010 5/14/2010 5/14/2010 S/14/2010 S/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 5/14/2010 Time

**SpcQ,.urn~•le** 

# 16 :55:5 0 C:\Cokme<Somples\20155 dol <ilo\20100514lwe! stfubber 2 Run 3_04U6 .S PE 16:56:51 C:ICokme<Son.plesl20155 dol <llel20100114l..e< SO'ubber 2 Run s_04137.SPE 16:S7:Sl'

**C:\C.Icmet~mples\201SS**

**dJ~It ile\2**  **0100514\wet** 

# suubber 2 Run 

# 3_04Ua.SPIE 

# 16:58:52 C:\Colcme<Sompl
.. \20155 dol

**l~e\20100514lwel** 

# se.ubber 2 Run 3_04U9
. SPE 16:!.9:53

**C:\Cakmct~mples\20155** 

# d•ltil•\l0100S14\wet saubbet 2 Run 

# l_04140.SPE. 

# 17 : 00:54 C:\Cokmnlomples\20155 dol

**l~e\20100514\we<** 

# oc:rubber 2 llun 

# 3_04141.SPE 17 : 01:54 C:\Cokme<Somplesi2015Sdol Ule\20100514\we< scrubber 2 11un 

# 3_04142.SPE 11:02:55 C:\Cokme<Sompios\20115 

# dol dle\20100514\wol scrubber 21tun J_04143.SPE 17 : 03:56 C:\Cokme<Sompl.,l20155 dol

**<~120100514\-t** 

# 1CNbbef 21tun 3_04144
. SPE 17 : 04:57 C:\Cokme<Sompies\20155 dol <ile\201005141-• scrubber 2 Run 3_04141
. SPE 17 : 0S:SI C:IC.IO'ne<l....,.es\20155 dol Ulel20100514\wol Krubber 2

**~un** 

# 3_04146.1PE 17:06:59

**C:\CIIcme•Sample~\2015Sdallile\20100S14\wet** 

# scrubber l 

# Run 3_04147.SPE 17:07:59

**C:\C.J,cme•Sample~\20155** 

# daltlla\20100S14\wel scrubber l 

# Run l_04141.SPl: 17:09:00 C:\C.JicmelS.Jmples\20155 dal tile\20100514\wet scrubber 2 Run 3_04149.SPE 17:10:01 C:\CakmetS.Jmples\20155 dal tilt\201005.14\wet scrubber l 

# Run 3_041SO.SPE 17:11:02 C:\CakmetS.JmP'es\20155 dal lil•\20100514\wel saubber 2 Run 

# l_04151.SPE 17:12:02 C:\CakmetSamptn\20155 d&llitl\20100514\wel suubber 2 

# 1\un

**3_~1S2 SPE**  

# 17 : 13:03 C:\Cokmellompl
.. \20155d• l dle\2 0100514lwel K<Ubbor 

# 2 Run 3_04153.SPE 17 : 14:03 C :\ Cokme<S.mplu\20155 dol tile\201005 14 \we< saubber 

# 2 R"" 3_04154
. SPE 17 : 15:04 C:\CokrMlSomplti\20155 

# dol

**<~\20100514\we<** 

# S<Nbller 2 

# R.., 3_04155 .SP £ 17 : 16:05 C:IC.kme<Somplesl20155 dol

**t~\20100514lwe<** 

# scrubbe< 2 

# R.., 3_041S6 .SP E 17 : 17:05 C:\Cokme<Sompiesl20155 dol <ilel20100514\we< >«ubber 2 Run 3_04157
. SPE 17:11:06 C:\Cokmell....,.es\20111 dol lllel20100514\we< S<Nbller l 

# Run l_041SS.SPE 17:19:07 C:\C•tcmetSan.ples\2015S d.al tile\2010051.\WH scrubber l 

# R un l_041S9.SPE 17:20:08

**C:\Ca,cme1Simple~\201S5** 

# daltilt\20100514\wet scrubber l 

# Run 3_0U60.SPf 17:21:08 C:\CalcmetS.Jmples\20155 dallilto\20100SU\wel saubber 

# 2 Run 3_04161.SP£ 17:22:09 C:\CakmetSampln\20155 dallile\20100514\wet scrubber 

# 2 flun )_CM162.SPE 17:23:09 C:\C.JkmetSamples\20155 dal Ule\10100514\wel sctubber 

# 2 Run 3_0416.tSPf: 

# 17 : 24:10 C:\Cokme<Somplesl20155 dol lile\20100 514lwel strubbor 2 Run 3_04164.SPE 17 : 25:11 C:\C.kmetSo.!mples\201SSdalti'*\lOlOOS14\wltl S(l'ubber 2 kun 3_0C16S . SPE l 7:M:U C:\Cak:mel$;1mpln\201SS dll tife\2010051 4 \ wtl scrubber 2

**k~** 

# S_011166.SPE 

# 17 :2 7:12 C:ICokme<S....plesl20155 

# dol

**<~\201005**

**14 lwe<**  

# oc:rubber 2 R.., 3_04167.SPE 1 7:21:13 C:\Cokmn5omplesl20115dol <ile\20100514'\we< wubbor 2 Run 3_0416&.SPE 17 : 29:13 C:\Cokme<Sompies\20155 dol

**1~120100514\we<** 

# ouubber 21tun 1_04169.1PE 17 : 30 : 14 C:\C.kme<Somples\20155 dol

**<~120100514\-•** 

# wubber 2 Run 3

_ 04170.SPE 17 : 31:15 C:\Cokme<Sompies\20155 dallile\20100514\we< saubber 2 Run 

# 3_04171.SPE 17:32:16 C:\CalcmetSamples\20155 dat tile\2010051•\wet

**scr~r** 

# 2

**~un** 

# J_04172.SPE 17:33:17

**C:\~lanetS.amples\2015S** 

# dal tile\20100514\wet scrubbet2 

# ftun l_0417).SPE 17:34:1? C:\CalcmetS.Jmples\20155 dal tlla\20100514\wet Krubbtt 2 Run 

# 3_0.174.SPE 17:U:18 C:\Calc:met$,mples\201SS dal tilt\2010051•\wet

**st:rub~t** 

# 2

**R~o~n** 

# J_0417S.SPf 

# 17:36:19 C:\Colcme<S•mplo•\2015S dol llltl20100514\wet

**s.:rub~r** 

# 2 Run 3_04176.SPE 17:37:20

**C:\Calc:metSampl~s\20155** 

# dal tlle\20lll!Y..U\YIIL scrubber l 

# Run 3_0.177.SPE 

# 17:11:20 C:\C.Icme<Somples\20155 dol tile\201005141-•

**s.:rub~r** 

# 2 Run 3_04171.1PE 17 : 39:21

**C:\CalcmetS~es\20155** 

# daltile\2010051•\wel scrubbe, 2 Run 3_04179.SPI 

# 17:40:22 C:\C-<So"'PPes\20 155 dal lile\201005 14 \wel

**St<ub~r** 

# 2

**~un** 

# l_04110
. SPE 17 :4 1 :22 C:\Colcnoe<So,.ples\20155 dol <ile\2010051 4\ -•

**scrub~r** 

# 2 

# Run l_04111
. 5Pf 17 : 42:23 C:\C-tSomples\20115 dol

**!~\201005141-** 

# scrubber 2 Run l_04182.SPE 17 : 43:24 C:\C-tSomples\20155dol tile\20100514\-

**oc:rub~r** 

# 2 Run 3_04183
. 5Pf 17:44:24 C:\Colc
... <Somplt$120155 dol

**<~\201005141.,.,** 

# scrubber 2 Run 3_041U
. SPf 17:45:25 C:\Colcme<S.mplesl20155d ollilel20100514l wel sa-ubber 

# 2 Run 3_0411S
. S'E 17;46:26 C:\C::akmetS.mples\2015$ dalllle\20100S14\wet setubber 

# 2 R.un 3.,.04le6 . SPE 

# 17:47:27 C:ICokmolS.mpt.,I201SS dll <lle\20100514\wet scrubber 2 Run 3_04117.SP£ 17;4.1:28

**C:\C.Jkmet5.Jmpl~t**

**s\2 01S5**  

# da.l tilt\20100514\wet suubber 

# 2 Run 3.,.04UI8.5PE 17:49:21

**C:\C31cm~tSimples\201SS** 

# d.JI Ule\20100514\we:t scrubber 

# 2

**~n** 

# 3_04189.$PE l7 ;S0:29 

# C:\Oicme1S..mpl•s\201SS dal tlle\l0100SJC\wet sccubbet 2 Rvn 

# 3_04190 . SPE 

# 17:51:30 C:\Calcme<S.mples\20155 dol tilt\20100514\we< scrubber 2 

# Run 3_04191.1PE 17 :52:3 1 C:\Colcme<S....plos\20155 dol tilo\20100514\we< scrubber 2Run 3_04192
. SPE 17 :53:3 1 C:\C.kme<Somples\20155 

# dol

**<~\20100514\wel** 

# scrubbe< 2 llun 

# 3_04193.SPE 17 : 54:32 C :\ C.kme<Somples\20155 dol

**<~\20100514lwe<** 

# wubber 21tun 3_04194
. 1PE 17 : 55:33 C:\Cokme<Somples\20155 dol tile\20100514\wet 

# 1CNbbef 2 Runl_04195
. SPE 

# 17 : 56:34 C:ICokme<Somplesi201SS d al tilo\20100514\wo< scrubber 

# 2 Run1_041!16.SPE 17:57:14

**C:\C.kmel~$\20155** 

# dol lilol20100514lwe< ..:rubber 2 R'"' )_04197.SPE 

# AVG W.Jler Vi1p1UnJt 

# 19.S4 vol-% 19.86 

# vol·" 19.78 vol-% 19.56 vol·ll 19.28 

# vol·" 19
. 77vol·ll 19
. 46vol

- ll 19.47
..... ,. 20.03
..... ,. 19.91vol-% 19.81 vol-"' 19.72'1oJ ·" 19.77'4'ol ·% 19.83vol ·" 19.71 

# vel - % 

# 20.12
..... ,. 20.46 vol·ll 20.26 

# vol""' 20.3vol-% 20.4 vol-!1 20.54 vol-!1 20
. 67
..... ,. 20.5.6 

# vol·" 2'0.65 

# vol-" 20.51 vol-"



# Z1 vol-% 20.9 

# vcl4 20.86 vol-% 20

.7 vol•" 20.77
..... ,. 20.84 

# vol·" 20.9vol · " 20.94-..ol·" 

# 20.11
..... ,. 20.54
..... ,. 20.65
..... ,. 20.4& vol-" 20.19 

# vol-" 

# 19.99 vol·" 19.avol -" 19.57 

# 'f'Ol ·" 19.95
.... ,. 19.7Zvol-!1 19.94 vol-!1 19.91 vol·" 19 . 78 Yol·% 

# 19.82 vol·" 19
. 65 vol·ll 19.41 

# vol4 

# 19.17 vol-% 19.23 

# Vol•" 19.25 vol·" 19.01vol·" 18.85 vol-!1 19.•6 

# vol·" 20.36
..... ,. 20.51
..... ,. 20.19
..... ,. 20.19
..... ,. 20.12
.... ,. 

# 19
. 71
.... ,. 19.67 vol-" 

# 20.05 Compenn Residu.JI Hydropn 

# thloride HCI Untt 

# w.t 

# 0.007 4.4S ppm 

# w e t 

# 0.0072 S.33

**pe~m** 

# wet 

# 0 . 0072 4 . 67

**pe~m** 

# w.t 0.007 

# •.68 ppm wet 

# 0 . 0069 4 . 55 ppm



# .... . 0 . 0071 

# 5 . 02 ppt'A 

# .,., 

# -

· 

# -· 

# - .... wet we< wOl 

# .... wo< 

# .,., 

# .,., 

# -

· 

# - - - -· 

# - .,., we< Wtl 

# .,., 

# .... 

# -· .,., .,., 

# -· .,., .,., 

# -· -· wet 

# .,., .,., w • • 

# .,., we< 

# w•• 

# -· 

# -· .,., 

# .. . . .,., wt< 

# .,., .,., wet wet 

# -· .,., 

# -· .,., .,., .,., .,., .,., 0.0071 0.0071 

# 0.0072 

# o.oorz 0.0073 0.0071 0.0071 0.0072 0 .0072 0.0073 0.0075 0.0075 0
. 0075 0
. 0076 0
. 0075 0.0075 0.0075 0.0076 0.0076 0.0077 0.0077 0.0077 0.0078 0
. 0077 0
. 0077 0
. 0076 0
. 0076 0.0075 0.0075 0.0075 0.0074 

# 0.0073 0.0072 0.0071 0.0072 0.0072 0
. 0073 0
. 0072 0
. 0072 0
. 0072 0.0072 0.0071 0.0061 0.0069 0
. 0069 0
. 0069 

# 0.0068 0
. 0066 

# 0.007 0.0074 0.0074 0.0074 0.0073 

# 0.0072 0
. 0071 0.007 

# 5.19ppra 4
. 13ppra 5.7
...... 4 . 98 ppm 

# S.ll ppm 1.18 ppm 

# 5 ... ppm 

# 4.75 ppm 4.69 ppm 5 . 31 

# ppm 5.42 ppm 

# 5
. 13 ppm 

# 53ppra 5
. 13
...... S
. l2ppra 6
. 31ppra 5.64 ppm S.l ppm 

# S . .J 

# ppm 4 . 91 ppm 

# 5.21 ppm 6.17 ppm 

# 5 . 44

**pe~m** 

# 5.29 ppm 5 .5 2 PPft' 5
. 21ppra 5
. 15
...... 4
. 73
...... 

# 4.91
...... 4
. 5
...... 

# 5
. 05 ppm 4 , 93 ppm 4.7 ppm 

# 5.!7 ppm 

# 5.02 ppm

**~** 

# ppm 

# 5
. 06 ppm 5
. 06 ppm 5
. 4ppm 

# t . Uppm 4.76 

# ppm 4.09 ppm 3.62 ppm S . Uppm 

# 3
. 57 ppm 3
. 91 ppm 

# • . 09 ppm ).24 ppm 

# •.16 ppm 

# 5.06ppm 5.3 ppm 5.S1ppno 5.15ppno 5
. 01ppra S
. 51ppra


# • . 24 PP"' 4
. 91 **Rn4du~l** 

# Hydroeen 

# fluorid• HF Unit 

# 0.0003 5 .5 ppm 0.0004 5.97 ppm 0
. 0004 0
. 0004 0
. 0004 

# 0.0003 0.0004 0.0004 0.0004 0.0004 0.0004 

# 0.0004 0.0004 0.0004 0.0004 0.0004 0
. 0004 0
. 0004 0.0004 0.0004 0.0004 0.0004 0.0004 0.0004 0.0004 

# o . ooo• 0.0004 0.0004 0
. 0004 0.0004 0
. 0004 0
. 0004 

# 0.0005 0.0004 0.0004 

# 0.0004 0.0005 0.0004 0.0005 0.0005 0
. 0004 0
. 000• 0.0004 0.0004 0.0004 0 .0004 0.0004 

# 0.0005 0.0004 0,0004 0.0004 

# 0.0005 0.0004 0.0004 

# 0.0005 0.0004 0.0004 

# 0.0004 

# o.ooos 0.0004 0.0004 

# 0.0005 5.65 ppm 

# 7 ppm 4.11 ppm 

# 6.83 ppm 4.97 ppm 

# 5.73 ppm 4
. 95 ppm 

# 6.31 ppm 

# 5
. 59 ppm 15.41 ppm S.J-4 ppm 

# 6.4ppm 6
. 05 pp m 6.14 pprn

6 ppm 

# 6.46 ppm 6.04 ppm 4.12ppm 

# 7 .06 ppm 

# 5
. 76 ppm 5.61 ppm 1
. 02 ppm 6
. 6tppm 5
. 16 ppm 6
. 02 ppm 7.14 ppm 6.68ppm 

# 5 .&5 ppm 6 . •7 ppm 

# 1 . •2 ppm 

# 5.45 ppm 

# S . '-4 ppm 

# 6
. 01 ppm 6 .1 1 ppm 

# 5.96 ppm 

# 5.56 ppm 

# 5.07 

# ppm S . 46 

# ppm 4 . S4 

# ppm 5.83 ppm 

# 5.16 ppm 5.71 ppm 

# S.9ppra 

# us,... 4
. 15
...... 4
. 51,... 4.l7ppra 4 , 37- 

# 4.6 ppm 

# 4 . 42 ppm 

# 4 . 29 ppm 

# l . S ppm 

# 4.17ppm 

# 5
. 59 ppm



# 6 ppm 5.71 ppm 4
. 73 ppm 

# 5.25 ppm 

# 5.01 ppm 

# 5.21 ppm 

# 5.65 1\esiduil SF6 

# 0.0048 0.0049 0.0049 0.0049 

# 0.0041 0
. 005 0.0051 0.005 0.0051 0.005 0.005 0.005 0.005 0.00 52 0.0051 0.0051 o.0054 0.0054 O.OOS4 O.OOS4 O.OOS4 O
. OOS4 

# o.ooss 0.0053 0.0054 0.0054 0.0055 0.0055 0.0055 0.0055 0.0056 0.0057 0.0054 

# 0
. 0056 0.0053 O.OOS4 O.OOS4 

# 0
. 0054 0.00 51 0
. 0052 0.0051 0.005 

# o . oos 0.0049 0
. 005 0
. 005 0.0051 0
. 005 0.0049 0.0048 0.0049 0.0048 0.0046 0
. 0047 0.0049 0.0051 0
. 0052 0
. 0051 0
. 0051 0.0052 0.005 0.005 Unft Oppm 

# Oppm Oppm Oppm Oppm 

# o,... Oppm 

# Oppm Oppm Oppm Oppm 

# 0 ppm 

# 0 ppm 

# 0 ppm Oppm 

# Oppm Oppm Oppm 

# Oppra Oppra Oppm Oppm 

# Oppm Oppm 

# 0 ppm 

# 0 ppm 0 

# ppm Oppm Oppm Oppm Oppm 

# Oppm

**Oppn~** 

# Oppm Oppm 

# Oppm Oppm 

# o ppm 

# 0 ppm 

# 0 ppm 

# 0 ppm 

# 0 

# ppm 0 ppm 

# 0 ppm 

# 0 ppm 0 ppm 0 ppm Oppm 

# Oppm Oppm Oppm Oppm 

# o ppm 0 ppm 

# Oppm 

# Oppm Oppra 

# o,... Oppm Oppm 

# Oppm 0 ppm 

# 0.00 anidual 

# 0.0059 0 .0058 

# 0
. 0051 0.006 0.0057 0.0051 0.0056 

# 0.0057 0.0051 

# 0
. 006 0.0051 0.0059 O
. OOS7 0.0057 0.0059 0.0061 0.0058 

# 0
. 0062 0.0059 0
. 0061 0.0061 0.0057 00057 0.0057 0.0061 0
. 0063 0 .0063 0.0061 

# 0.0061 

# 0.0062 0.006 0.0059 0.006 0.0051 0.0051 

# 0.0051 0.0059 o . 005a 0.005a 0.0058 o . o05a 0.0058 0.0058 0.006 0
. 0058 

# 0.006 0.0059 0.0057 0.0056 0.0058 0
. 0058 

# 0.006 0.0061 0
. 0058 0.0061 0.0064 

# 0
. 0061 0.0061 0.0059 00059 0.006 0.006

# HC~ 

# Oalltalia

Sm -SpUcod 

# Data 

# Oatt S /14/2010 S/14/2010 S/14/2010 Method 

# no 320

**3~ f~ifn.tm•** 



# ~·pm) 

# 24
. 1 1 

# 24
. 62 l4.lt 

# sF6 (ppm) 0 .5 1

7 

# 0
. 96 O
. t7



# .... . c-. 

# """'lc:::::E!!] I o.ae11 

# s..-- co... 

# 01.....,.. Date

**5/14/~ 10**  

# 5/14/2010 5/14/l010 

# .........

**3~** 

# 320 320 Fitltn..at 

# HCI-) 5.01 

# S.S1

**2~** 

# SF6 (.,...) 0 

# 0 0 AVI. Conc

. lppm}c::::::::!!!J 

# I · I



# ... s. DF 

# c. c. **~OW'!Y(%)•** 

# Ce • Of • 

# Ci • Su(L·OJ) 

# 2 4.l2 ppm

.. . 92 ppm


# · ·""'" 200 .8 ppm 

# 9.91 ppm 23.19 ppm 

# Sm·Sull·Ofl Ofl(s



# Rccowrvi"JI

-

**~**


# SIH•tdata 

# ... p, .. Ti<M

**5~cttYMFM**

**5/14/~10** 

# l&ill:11 C:\(•kiMtS,...,...\20155o.l tio\201DOSI'\wtl 

# scr..._l SF6 ..,.., - 3_04122
. 5'1 S/14n010 11:02 : 33 C:\CaktMtSa•plln\201SS 

# cW tH\ZO lOOS14 \W'tt Ktubb« 

# 2 SF5 ahH 

# RUlli 

# l_GUU
. Sft 

# S/14/2010 18:02:39

**C:\CakrM~s\201SS** 

# dal tile\20100S14\wtt wubb« 2 SF6 HIH ltuA 

# 3_0ot224
. SPE Spikelata 

# HCL Dole 

# lii'N

**SpecUVMF'i~** 

# S/1'/1010 18:0C:O' C;\C.tc:metSamples\20US ct.lt,.e\20100514\w.' Kl'\lbbtr 

# 2 hclltter Run 3_04243.SP£ 5/14/2010

**18;~ 40**  

# C':\C•IautSample:•\20155 da' c;ae\2:0100514\wtt wubbtr l 

# hclllter Ruft l_04244.SPt: S/14/2010

**11:04:~2** 

# C:\CikJutSamples\201SS dallilt\20100514\wtl wubbltr 2 hcl 

# alter lun 3_042n.SPE

**Nal~~ta,** 

# HCI-SF6 

# Datt 

# Tftt

**p•c:lrumfl~** 

# S/14/2010 17 : 5S:l3 C : \C
.. **cmed.llrft~\20155** 

# hlti'*\20100Slol\wtt scrubbtf 2 lun 

# l_GU9S.SP£ S/14n010 11 : $6 :)4

**\C alc.mttSa"'pln\lOlSSd~**  

# tilc'\20100514\wt« u:rubbef l 

# Awl l_ot19f
. SP£ S/14/2010 17:57:14

**\C~IaMtS •rRPIHU01SS** 
**d~** 

# tM\2010051,\wtC scrubb4f 

# 2 

# twn l_CM 197 .SPf ..... coac:ftltr ation

**of~ ~Ntytt**  

# Mati¥91t0ft<alrJbon of 

# .-n•fvl• Dilwfion hctor 

# (hraet 

# < 10.) Cyliftct.,ofspikl'dcas Cylinder of 

# trKer aas.tSFf) 

# hpecttd conctnlratlon ol

**ana~•** 

# 70·130%

WM ttvapoo.t

**C~ns.a tion**  **lll:t~** 

# 1U4vol·" 

# .... 11.44 

# wd·" 

# - 11.42

**tt~Gt·"** 

# - Wattf v.poUnit C:o-pe.-wtion 

# Atsidnl 17
.

01 WI·" 

# - 17.04 ¥01·" 

# ... , 17.09 

# vol·" 

# ... ,

Wlttr Vlpc:J U nit 

# Compenution Rtttdual 

# 20.12 

# vot- " 

# .... 1,,7 1 

# woa-" 

# .... 1'.67

**YO!~"** 

# - **ttydros:et~~** 

# chkw 

# \Mit 

# "-sidual 

# Hvdros:en ftuori Un "

**~u~** 

# SJ6 

# Un• Resiclu& 

# O.OOS2 

# u .... 

# o.ooos 2.95
..... 

# 0
. 00)1 0
. 97
..... 0
. 0044 0.0049 ).59
.... 0
. 0006 

# t.9ot PJft 

# 0
. 0034 O .K ppra 

# 0
. 0047 O.ocMt 

# 2 .5!
.... 

# o.ooos 2.95
..... 0.0037 0.17 ppra 

# 0.004 Hvdrotcr. chlor Unie

**~idu..** 

# Hydroce• Auori Unit 

# Rcsid<o al SF6 Unit 

# Rc•ict.al 

# O
. DOS2 24.14 ppm 

# 0 .0011 1.93 ppm 

# o.oon 

# o..., .. 0.0067 0.0055 24.,2 ppm 

# 0.0029 3.87 ppm 

# 0
. 0007 0 ppm 

# 0.0071 0
. 00 5 ) 

# 24.1' PPM 0
. 0007 3.98 ppm 

# O.OOS6 0 

# p;pm 

# 0
. 0035
Hydro1en c hlof un•t 

# R-u•• tfvdro&en fluori Unil 

# ...,_idual SF' Urlil 

# Rnldual 0
. 001Z S
. 01

**~POl** 

# 0.0004 5.25 ppm 

# 0
. 0052 0 pt>m 

# 0
. 0059 0
. 0071 S
. SIPPOI 0.0004 

# S
. 08..,... 0.005 0..,... 0- 0.007 

# •.z• PP"' 

# o . ooos .5.21 

# ppm 

# 0.005 0..,... 0-

# HF Dalltalia


# s .. -.sP'IIIed DMa 

# .,.,. MtthOd 

# ' icrtf,.., 5/14/2010 SlO 

# S/14/2010 520 5/14/2010 320 AVI- COftL 

# (ppm) 

# s"

- Natiw Con4;. 

# Of 

# •n.etvW



# .,.,. **ou~** 

# wchod 5/14/2010 

# uo S/1'12010 120 S/14/2010 320



# .... 

# •• 

# ., ,, c. a.eccwt"fy 

# l"tt 

# =

**Ce•Pf~tCJ•SYll-of)** 

# 22.11 ppm 

# s.ta ppm 

# 9-"'" 21'2.0 ppm 9.9a IDPM 

# 25

. 21 DPffl



# ........ 11'11
.. . ....

SplhD.ItiSI• Tinoe Spi!CtrumFfle 

# --

Ayt. CoM. (ppm)



# ko~



# 111 • <- l

5/1.!/2010

**11:02~1&** 

# C:\Cetcmei.Satlq)lt'l\lGlSS d&l t.at-\20100514\w•t "'vbber 2 516 atter Run :t_04l22 .S PE 

# S/14/2010 

# 18:02;)) C:\Cikmets.ampln\20155 

# dal tle\'20100S14\wtt .crubbtr 1 

# Sf' a.rttt Rvn 3_ou:a.SPf S/14/2010 11:02:l9 C:\Citcmn5arnpln\20as dill tlle\20100514\wtt "rubber 2 

# SF6 after Run J_04224.SII'f

**Spt.Ut>at~~** 

# "' S/l4/l010 18:00:56 C.:\Calcmc1$1n'l.,.fl\20US d1l tlle\lOlOOSl.t\""t suubba- l hf i!ftet 

# ftun l_04209 .S PE S/1.11/1010

**1*:00** **$~ C:\CIIkrM\SIMCiitS\20l~S**  

# dl4

**titi!!'U<Il00$14\wc~** 

# SCNbber 2 hf 

# lfttt Jtvn )_Oi1210
. SPE S/14/2010 18!01:01

**;\CIIIcnM:tS a~s\20JS5**  

# dill 

# t ... **\20100$141\~c wubbll!t2hf~er**  

# 11Wn3_0llt1
. SI't Nat""'* Data Hf·Sf6 0111C 

# r .... SptttJvmfNt 

# 5/t4noJo 17:55:lJ C;\Calemet.Sel'f\PIH\la155 dal

**tilt\20JDOS14\~Jrtrlt** 

# sc:t .. bbtt 2 Rul"'l_04195.SPf S/14/2010 17:56:34 C:\Caktntl.Samplfl\10155 dal tle\20i00Sl4\wtt scrubber 2 Run l_0419&.511'E S/14/l()ID 17:57;34 c·\QkmetSamptts\lOlSSdal tllt\20100514\wtt s.crubbtr :Z 

# Run

**l_Odl97 ~PE**  HFtppm) 

# Sf& (ppm} 

# 2).62 0
. ,7 20.14 

# .... 22.SG 

# 0
. 97 

# c:=JmJ I Q.H7j



# ... 

# ,



# .... , ... (Will



# s .n 

# .... 5. 21 

# c:::::::EJ I

Mten concmtr1t1on of 

# sp1led tnelyte Nn ivtco i'IUntratiOn of tntl'ytl' 

# OlutiOf'l haor [hr&fl c

**l~)** 

# cytjndtf



# of~piked **~'** 

# Cfl i ncMf Of trlcer ps {SF6) 

# bpect.-d 

# tonu:nuaclion o f

**en•~•** 

# 70 · 1)0"

**WI~VIpciUntt** 

# Comp
.. nW(ion l!:n'dull 

# ll.l-1\10
.. " 

# ... , 11.44

**vo~K** 

# w<l 

# 11.42 vol•" WOI 

# 17.Nvol · " wtl 

# t7
. 0l 

# ¥01 · " W<l 

# IUho l- " 

# - W11tervapoUn.t co.._pensatbn

**Rts~** 

# ... 20.12 \10
... 

# -· 19.71 voJ." WOI 

# 19." vol-% WOI 

# D D 

# I

O
. OOS2 0
. 0049 0.0049 0
. 0064 

# 0
. 0041 O
. OOSl



# 0
. 0072 0
. 0071 0.007 HydfQCeft 

# chiQf Unit 

# 4
. 1 PP"' 

# "·"ppm '2.SJ ppm 

# 2.)? PP"'

**~** 

# DPflll 

# l.ll ""' HydrosetJ chlor Unit 

# S.Ol PP"' 5 .5 1 PP"' 4.24 ppm RHidual HrdJOpn tlvo 

# Unit 

# ltnidu
.. SF6 

# """ lltsidua l O.CXXJS ,.. ••

j)no 

# 0.0018 0.97 

# ppm 0
. 0044 

# O.OD06

**1.94p~** 

# 0
. 0034 

# 0.96 ppm D.oD47 D.OOOS 2

. 95 Dpn'l 

# 0.00)7 0 , ,7 ppm D.OD4 0.0011 

# 2!
. 62 ppm O.OOS2 O_ppm 0.0045 

# D.OOD 7 lO.t• ppm 

# O.OOll 

# o.-m 

# o.ooc, D.ODD9 

# 22-S6
.... 0.00)9 

# o.- O.OOSI
Residuel HW"ckopn tluo Unit ltnldt.ial 

# Sfi 

# ""'

**lle~··**

O.ooo4 

# S.25 ppm O

. OOS2 

# Oppm 

# o.ooso 0.<>000 

# 5
. 01Dpm 

# ·- Oppm 

# ··- o . ooos 5
. 21 ppm DDDS Oppm D
. OD6

# Oate Time Spec.trumFile 

# S/14/2010 18:28:34 C:\ColcmeiSomplos\20155 d•l1ilo\20100SI4\ Hf ch 

# sun Allor Run 3_04320.SPE 5/14/2010 18:29 : 36 C : \C.Icmo1Somplos\201SS d•l tilo\20100514\ Hf 

# cu sun Alter Run 3_0432t.SPE 5/14/2010 18 : 30 : 25 C :\ C.kmotSomplos\201SS d1l tile\20100S14\ Hf <U ..:on Aile< Run 3_0432HPE 

# AVG Water vapor H20 Unit CompenMtion 

# 0

**vo~%** 

# wot 0 vol-% w.t 

# o 1101-% wet Rosiduol

**~vd<osen** 

# chloride HCI

**Un~** 

# Residual Hvd<ocon fluoride HF 

# Unft Oppm 0 

# ppm 0
. 024 ppm 0.0014 217 19 ppm 0.0007 

# o .

ooss 0
.

0037 216.92 ppm 216
.

93 ppm 217.01 0.0007 0
. 0005 Residual SF6 Unit Residual 

# 0.0039 0 ppm 0.001 0
.

0042 0 

# ppm 0.0014 0.0023 0 ppm 

# 0.0016

# D<~te 

# Time Spectrumfile 

# 5/14/2010 18:17:54 C:\C.IcmetS.mples\20155 dol tile\20100514\ HI cu san After 

# Run 3_043U.SPE 5/14/2010 18:11:57 C:\C.IcmetS.mples\20155 dol tile\20100514\ HI cu saon After 

# Run 3_04312.SPE S/14/2010 18:18:14 C:\C.IcmotS.mplts\20155 dal tile\20100514\ HI cu saon Afttr 

# Run 3_04313.SPE AVG Wiitervap c Unit 

# 0 vol·% 0 vol·% 0 vol · % CompenS<ll Residual Hydroeen chlori c Unit 

# wet 0.0003 0
. 011 ppm wet 0.0005 0
. 016 ppm wet 0
. 0004 0.031 ppm Residual Hydrocen fluorid Unit 

# 0.0005 212 .09 

# ppm 0.000 1 2 11
. 74 ppm 0
.

0002 212.61 ppm 212
. 15 Residuol SF6 0.0 0 41 0.0 0 47 0.0059 Unit 

# 0 ppm 0 

# ppm 

# 0 ppm **Resi u~l**  

# 0.009 0
. 0013 0.0007

# Date

**Tim~ SpectrumFil~**  

# Water vapo Unit Compen52 Residual Hydroaen cU n i t Residual Hydrogen I Unit Residual SF6 Unit Residual 5/14/2010 18:10:13 C:\CalcmetSamples\20155 daltile\20100514\ 516 cts scan After Run 3_0427 0 vol·" wet 0.0026 0.02 ppm 0.0003 O.Dl ppm 0.0016 9.98 ppm 0
. 0027 5/14/2010 18:11:19 C:\CalcmetSamples\20155 dal tile\20100514\ 516 cts scan After Run 3_042 0 vol·" wet 0.0021 0
. 04 ppm 0.0007 O.Ql ppm 0.0017 10 ppm 0
. 0014 5/14/2010 18:12:24 C:\CalcmetSamples\20155 dal tile\20100514\ 516 cts scan After Run 3_042 0 vol·" wet 0
. 0028 0.02 ppm 0.0004 0.022 ppm 0.0012 1 0.06 ppm 0.0024 

# AVG 10
. 01

# o.te Tomo 

# Spt<tn•mfUe

**Wecerv•Un~ Carnp.ns~**  **fl:e~** 

# ....,.01 ... chlotiM HCI 

# "'"' Residul 

# tt;cftoc• ftuoride Hf 

# "'"'
... -.. Sf6 

# "'"' 

# - S/14/2010 11 ; 07:10

**C:\CMUM~\201SS** 

# dll

**\IM\20100S14\~** 

# sattbM' l CTS ZEJIO 

# aft.- Run l_OU6l . SPE 

# 0
. 01_,. 

# .... 0.0001 0.08"""' 0
. 0003 

# o ..... 0
. 0004 

# o..,. o . ooll S/14/lOIO IS:OH6

**\C-~\lOUS** 

# dol t;jo\20100514\we< 

# .a-.. 2 CTS2£110 olte<
.... l_00262
. SP( 0.03_,. 

# -· 0.0003 0
. 05"""' 0
. 0004 

# a PP"> 0.0006 Opp m 

# 0 . 001 

# S/14/lOIO 18;07:22 C;\C--.tSI,mpJes\201SS dai •ilt\l0100S14\wet scntbMr 

# 2 CUZEAO

**.t't~** 

# IWn l_CM26l . SPE 0.01

**~ol·"** 

# -· 0.0002 

# .,_ 

# ....... 0.0003 0.11Hm 

# 0
. 0005 

# ..... o.oou AVO 0.03 0.06 

# 0
. 04