### Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. This number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being Fields that are highlighted in down boxes, included. Gray fields are

[FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM

5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Test Date

Tri-Stete G&T Nucla Generating Station 1 5/10/2010Fuel Type 1 Fuel Type 2 Fuel Type 3

bitum inousOther Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis

0 Tri-Stete G&T Nucla Generating Station 1 As Received 0 Tri-Stete G&T Nucla Generating Station 1 As Received 0 Tri-Stete G&T Nucla Generating Station 1 As Received 0 Tri-Stete G&T Nucla Generating Station 1 As Received 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basis 0 Tri-Stete G&T Nucla Generating Station 1 Dry basisAn alyte An alysis M ethod for each Analyte (example: ASTM D5865-04) Higher Heating Value ASTM D5865 % Moisture ASTM D3302 % Ash ASTM D3174 % Sulfur ASTM D4239 Method B Higher Heating Value ASTM D5865 % Moisture ASTM D3302 % Ash ASTM D3174 % Sulfur ASTM D4239 Method B Antim ony ASTM D3683 (Mod) Arsenic ASTM D3683 Beryllium ASTM D3683 (Mod) Cadmium ASTM D3683 (Mod) Chlorine ASTM D4208 Chromium ASTM D3683 (Mod) Cobalt ASTM D3683 (Mod) Fluorine Lead ASTM D3683 (Mod) Manganese ASTM D3683 (Mod) Mercury ASTM D6722 Nickel ASTM D3683 (Mod) Selenium ASTM D3683EIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 0 Tri-Stete G&T Nucla Generating Station 1 M30B, M29, M5B/OTM28

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) TSMC01 5/13/2010 10684.00 Btu/lb 6.34 TSMC02 5/13/2010 10252.00 Btu/lb 6.77 TSMC03 5/15/2010 10144.00 Btu/lb 6.51 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 19.79 0.64 11407 Btu/lb N/A 21.13 0.68 21.86 0.65 10997 Btu/lb N/A 23.44 0.69 22.7 0.67 10850 Btu/lb N/A 24.28 0.71Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis) 0.02 % 0.05 μg/g 2 ug/g 2 ug/g <1 0.02 % 0.03 μg/g 2 ug/g 2 ug/g <1 0.02 % 0.05 μg/g 3 ug/g 2 ug/g <1Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel Units ug/g 9 ug/g 11 ug/g 50 ug/g 7 ug/g ug/g 11 ug/g 12 ug/g 19 ug/g 8 ug/g ug/g 9 ug/g 12 ug/g 37 ug/g 7 ug/gSelenium

(Dry Basis) Selenium

Units Cobalt (Dry

Basis) Cobalt Units 1 ug/g 2 ug/g 1 ug/g 3 ug/g 4 ug/g 2 ug/gEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 0 Tri-Stete G&T Nucla Generating Station 1 0010, 0011, 0031, 10, 25A, 18

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) NDFN01 5/14/2010 10441.00 Btu/lb 5.62 NDFN02 5/14/2010 10697.00 Btu/lb 5.42 NDFN03 5/14/2010 10361.00 Btu/lb 5.22 Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis) 21.43 0.69 11063 Btu/lb N/A 22.7 0.73 19.87 0.69 11310 Btu/lb N/A 21.01 0.73 21.99 0.75 10931 Btu/lb N/A 23.2 0.79EIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 0 Tri-Stete G&T Nucla Generating Station 1

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6260B) 0 Tri-Stete G&T Nucla Generating Station 1

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals synfuel mg/g petroleum coke μg/g other mg/KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm