## EMISSIONS TEST REPORT FELMANPRODUCTION, INC. FURNACE #2 BAGHOUSE (ID# 001-01) WVDEP DAQ PERMIT # R30-0530004-2007 PLANT ID# 03-54-05300004 LETART, WEST VIRGINIA MARCH2013

TI-1550

# ~~·TEST, Inc. • www.testincorp.com 

## TechnicalEnvironmentalServices Team

Route 2, Box 33-B, Poca, West Virginia 25159 Ph: (304) 755-1077Fx: (304) 755-1099

## TABLE OF CONTENTS
Introduction Summary ofResults Discussion ofResults Sampling and Analytical Procedures Sampling Location
Appendixes A - Computer Data and Example Calculations B -Pre-flowData C- Analytical Data D - Field Data Sheets E- Calibration Data F - Chain ofCustody

List ofTables Table 1 Summary ofResults HCl Table 2 Summary ofResults Particulate Matter Table 2a Summary ofResults Metals Table 3 Summary ofResults Mercury Table 4 Dioxins/Furans/PCBs Sampling Data Table 4a Summary ofResults PCBs Table 4b Summary ofResults PCBs (cont.) Table 4c Summary ofResults PCBs (cont.) Table 4d Summary ofResults PCBs (cont.) Table 4e Summary ofResults Dioxins Table 4f Summary ofResults Dioxins (cont.) Table 4g Summary ofResults Furans Table 4h Summary ofResults Furans (cont.) Table 5 PAHs Sampling Data Table 5a Summary ofResults PAHs Table 5b Summary ofResults PAHs (cont.) Table 5c Summary ofResults PAHs (cont.) Table 5d Summary ofResults PAHs (cont.) 1 1 20 22 27

29

2 3 4 5 6 7 8 9 10 11 

### 12 13 14 15 16 17 18 19

### INTRODUCTION 

## Emissions TestReport FelmanProduction, Inc. Furnace #2 Baghouse (ID#OO 1-01) WVDEP DAQPermit# R30-0530004-2007 Plant ID# 03-54-05300004 Letart, West Virginia TI-1550

Emission testing was conducted at FelmanProduction, Inc. located 

### inLetart, West Virginia on March 18, 19, and 20, 2013, byTEST, Incorporated, Charleston, West Virginia, underthe direction ofPaul Chinuntdet. Thepurpose ofthese tests was to determine the concentrations of particulate matter, hydrogen chloride, arsenic, cadmium, chromium, lead, manganese, nickel, mercury, dioxins/furans, polychlorinated biphenyls, and polycyclic aromatic hydrocarbons being emitted into the atmosphere viathe Furnace #2 Baghouse. Mr. John Konrady ofFelman Productions, LLC. coordinated the testing withplant operations.

The testing followed the procedures inthe Appendix to the Code ofFederal Regulations, Title 40, Chapter 1, Part 60, Methods 1, 2, 3A, 4, 5d, 26A, 29, and 30B; and CaliforniaAirResources Board Methods 428 (CARB 428), and 429 (CARB 429).

SUMMARY OF RESULTS

The following tables and graphs provide results for the emission rates measured on the Furnace #2 Baghouse. The emission results are presented 

### in micrograms per dry 

### standard cubic meter (ug/dscm), nanograms per dry 

### standard cubic meter (ng/dscm), pounds per hour (lbs/hr), and pounds pertonproduct (lbs/ton). The lbs/ton were calculatedusingthe following productionrates: March 18,2013 = 

### 7.17 tons/hr, March 19,2013 = 

### 8.38 tons/hr, and March 20,2013 = 

### 8.87 tons/hr.

# SUMMARY OF RESULTS Table 1 HCl Sampling Data Baghouse #2

Run Number 1 2 Date 3/19/13 3/19/13 Time 855

- 1110 1215

- 1425 Carbon Dioxide Cone. - % Vol. 0.40 0.40 Oxygen Concentration

- %Vol. 20.40 20.50 Stack Pressure

- "Hg 29.06 29.05 Area ofStack- Sq. in. 950,400.00 950,400.00 Volume Dry Gas Sampled

- dscf 103.659 102.137 Volume Dry Gas Sampled

- dscm 2.935 2.892 Stack Temperature

- Deg. F 150.30 147.20 Percent Moisture - % 1.39 0.50 Velocity in the Stack

- FPS 1.35 1.30 Volumetric FlowRate- ACFM 534,600 532,620 Volumetric Flow Rate

- DSCFM 442,970 447,432 Isokinetic Sampling Rate - % 104.9 102.3 Hydrogen Chloride Concentrations

- ug 3100.00 2500.00 Hydrogen Chloride Emissions

- ug/dscm 1056.22 864.45 Hydrogen Chloride Emissions

- ppm 0.70 0.57 Hydrogen Chloride Emissions

- lbs/hr 1.753 1.449 Hydrogen Chloride Emissions

- lbs/ton prod. 0.209 0.173 Production Rate (tons/hr) = 

### 8.38

2 

### 3 Average 3/19/13


## ---- 1600

- 1815


## ---- 0.50


## ---- 20.40


## ---- 29.06


## ---- 950,400.00 

### ----

101.876


## ----

2.885


## ---- 157.10


## ----

0.62


## ---- 1.40


## ---- 537,240


## ---- 443,690


## ----

102.9 

# ---- 1900.00 2500.00 658.58 859.75

0.43 0.57 1.095 1.432 0.131 0.171

# SUMMARY OF RESULTS Table 2 Particulate/Metals Sampling Data Baghouse #2

Run Number 1 2 Date 3/20/13 3/20113 Time 900- 1315 900- 1315 Carbon Dioxide Cone. - % Vol. 0.40 0.40 Oxygen Concentration

- %Vol. 20.40 20.40 Stack Pressure

- "Hg 29.16 29.16 Area ofStack

- Sq. in. 950,400.00 950,400.00 Volume Dry Gas Sampled

- dscf 209.472 204.748 Volume Dry Gas Sampled

- dscm 5.932 5.798 Stack Temperature

- Deg. F 145.10 153.20 Percent Moisture - % 0.40 0.62 Velocity in the Stack

- FPS 1.34 1.40 Volumetric Flow Rate

- ACFM 530,640 534,600 Volumetric Flow Rate

- DSCFM 449,461 445,847 Isokinetic Sampling Rate - % 104.4 102.9 Particulate Matter Concentrations- gr/acf 0.0003 0.0003 Particulate Matter Concentrations- gr/dscf 0.0004 0.0003 Particulate Matter Concentrations- ug/dscm 859.74 730.14 Particulate Matter Emissions

- lbs/hr 1.54 1.15 Particulate Matter Emissions

- lbs/ton prod. 0.17 0.13 Production Rate (tons/hr) = 

### 8.87

3 

### 3 Average 3/20113


## ---- 1440

- 1850


## ---- 0.40

---- 20.50


## ---- 29.06

---- 950,400.00

----

213.968

----

6.059


## ---- 142.50


## ----

0.50


## ---- 1.30


## ---- 530,640


## ---- 449,401


## ----

106.7


## ---- 0.0003 0.0003 0.0003 0.0003 792.21 794.03

1.16 1.28 0.13 0.14

# SUMMARY OF RESULTS Table 2a Particulate/Metals Sampling Data Baghouse #2

Run Number 1 2 Arsenic Concentrations

- ug 2.0 2.0 Arsenic Emissions- ug/dscm 0.34 0.34 Arsenic Emissions

- lbslhr 0.0006 0.0006 Arsenic Emissions

- lbs/ton prod. 0.0001 0.0001 Cadmium Concentrations

- ug 0.50 0.50 Cadmium Emissions

- ug/dscm 0.08 0.09 Cadmium Emissions

- lbslhr 0.0001 0.0001 Cadmium Emissions -lbs/tonprod. 1.60E-05 1.62E-05 Chromium Concentrations

- ug 3.90 11.40 Chromium Emissions- ug/dscm 0.66 1.97 Chromium Emissions -lbslhr 0.0011 0.0033 Chromium Emissions

- lbs/ton prod. 0.0001 0.0004 Lead Concentrations- ug 50.00 25.00 Lead Emissions

- ug/dscm 8.43 4.31 Lead Emissions -lbslhr 0.0142 0.0072 Lead Emissions

- lbs/ton prod. 0.0016 0.0008 Manganese Concentrations- ug 3370.00 976.00 Manganese Emissions

- ug/dscm 568.11 168.33 Manganese Emissions

- lbslhr 0.9567 0.2812 Manganese Emissions

- lbs/ton prod. 0.1079 0.0317 Nickel Concentrations- ug 4.70 11.10 Nickel Emissions- ug/dscm 0.79 1.91 Nickel Emissions

- lbslhr 0.0013 0.0032 Nickel Emissions

- lbs/ton prod. 0.0002 0.0004 Production Rate (tonslhr) = 

### 8.87 3 Average 2.0 2.0 0.33 0.34 0.0006 0.0006 0.0001 0.0001

0.50 0.50 0.08 0.08 0.0001 0.0001 1.57E-05 1.60E-05 6.50 7.27 1.07 1.23 0.0018 0.0021 0.0002 0.0002 28.30 34.43 4.67 5.80 0.0079 0.0098 0.0009 0.0011 1280.00 1875.33 211.26 315.90 0.3557 0.5312 0.0401 0.0599

9.10 8.30 1.50 1.40 0.0025 0.0024 0.0003 0.0003Vl 

# SUMMARY OF RESULTS

Time Run Trap 1128

- 1328 1 A 156034 B 

### 156058 Average % 

### Relative Deviation

Time Run Trap 1355

- 1555 2 A 156069 B 

### 150824 Average % 

### Relative Deviation

Time Run Trap 1615

- 1815 3 A 156006 B 

### 156057 Average % 

### Relative Deviation 

# * Spiked Production Rate (tons/hr) 

### = 7.17 

## Table 3 Vapor Stage Mercury Test Results Baghouse 2 Sample Sample Volume Volume Flow (1) 

### (dscm) (dscfm) ug 50.177 0.050 397,005 0.0200 50.562 0.051 397,005 0.0180 50.370 0.050 397,005 0.0190
Sample Sample Volume Volume Flow (1) 

### (dscm) (dscfm) ug 51.755 0.052 394,798 0.0232 52.627 0.053 394,798 0.0257 52.191 0.052 394,798 0.0244
Sample Sample Volume Volume Flow (1) 

### (dscm) (dscfm) ug 52.902 0.053 392,228 0.0291 52.971 0.053 392,228 0.0268 52.937 0.053 392,228 0.0279 Mercury Emissions ug/dscm lbslhr lbs/ton prod. 0.40 5.94E-04 8.28E-05 0.36 5.29E-04 7.38E-05 0.38 5.62E-04 7.83E-05 5.72 Mercury Emissions ug/dscm lbslhr lbs/ton prod. 0.45 6.64E-04 9.26E-05 0.49 7.21E-04 1.01E-04 0.47 6.93E-04 9.66E-05 4.14 Mercury Emissions ug/dscm lbslhr lbs/tonprod. 0.55 8.08E-04 1.13E-04 0.51 7.43E-04 1.04E-04 0.53 7.75E-04 1.08E-04 4.20

# SUMMARY OF RESULTS Table 4 Dioxin/Furans/PCB's Sampling Data Baghouse #2

Run Number 1 2 Date 3/19/13 3/19/13 Time 855

- 1105 1220

- 1435 Carbon Dioxide Cone. - % Vol. 0.40 0.40 Oxygen Concentration- %Vol. 20.40 20.50 Stack Pressure- "Hg 29.06 29.06 Area ofStack- Sq. in. 950,400.00 950,400.00 Volume Dry Gas Sampled

- dscf 102.868 100.981 Volume Dry Gas Sampled

- dscm 2.913 2.859 Stack Temperature- Deg. F 161.50 147.60 Percent Moisture - % 0.89 0.76 Velocity inthe Stack

- FPS 1.36 1.30 Volumetric FlowRate- ACFM 539,220 533,280 Volumetric Flow Rate

- DSCFM 440,971 446,676 Isokinetic Sampling Rate - % 104.6 101.3

6 

### 3 3/19/13 1555

- 1810 0.50 20.40 29.06 950,400.00

104.844

2.969 165.00

0.79 1.40 540,540 440,019

106.8

### Run Number 33'44'-TetraCB-(77)

344'5-TetraCB-(81)

233'44'-PentaCB-(105)

2344'5-PentaCB-(114)

23'44'5-PentaCB-(118)

23'44'5'-PentaCB-(123) 

# SUMMARY OF RESULTS Table 4a PCB Sampling Data Baghouse #2

1 2 ng 4.3 2.6 ng/dscm 1.48 0.91 lbs/hr 2.44E-06 1.52E-06 lbs/ton 2.91E-07 1.82E-07 ng 0.26 0.15 ng/dscm 0.09 0.05 lbs/hr 1.47E-07 8.78E-08 lbs/ton 1.76E-08 1.05E-08 ng 4.4 2.5 ng/dscm 1.51 0.87 lbs/hr 2.50E-06 1.46E-06 lbs/ton 2.98E-07 1.75E-07 ng 0.36 0.2 ng/dscm 0.12 0.07 lbs/hr 2.04E-07 1.17E-07 lbs/ton 2.44E-08 1.40E-08 ng 12 6.7 ng/dscm 4.12 2.34 lbs/hr 6.81E-06 3.92E-06 lbs/ton 8.12E-07 4.68E-07 ng 0.23 0.11 ng/dscm 0.08 0.04 lbs/hr 1.30E-07 6.44E-08 lbs/ton 1.56E-08 7.68E-09 Production Rate (tons/hr) = 

### 8.38 3 Average 1.5 2.8 0.51 0.96 8.33E-07 1.60E-06 9.94E-08 1.91E-07

0.085 0.17 0.03 0.06 4.72E-08 9.41E-08 5.63E-09 1.12E-08 1.4 2.8 0.47 0.95 7.77E-07 1.58E-06 9.28E-08 1.88E-07 0.12 0.23 0.04 0.08 6.66E-08 1.29E-07 7.95E-09 1.54E-08 3.9 8 1.31 2.59 2.17E-06 4.30E-06 2.58E-07 5.13E-07

0.082 0.14 0.03 0.05 4.55E-08 8.01E-08 5.43E-09 9.56E-09

# SUMMARY OF RESULTS

Run Number 33'44'5-PentaCB-(126)

HexaCB-(156)+(157)

23'44'55'-HexaCB-(167)

33'44'55'-HexaCB-(169)

233'44'55'-HeptaCB-(189)

C13-233'44'55'-HeptaCB-(189) 

## Table 4b PCB Sampling Data Baghouse #2

1 2 ng 0.081 0.048 ng/dscm 0.03 0.02 lbslhr 4.59E-08 2.81E-08 lbs/ton 5.48E-09 3.35E-09 ng 0.46 0.25 ng/dscm 0.16 0.09 lbs/hr 2.61E-07 1.46E-07 lbs/ton 3.11E-08 1.75E-08 ng 0.18 0.11 ng/dscm 0.06 0.04 lbslhr 1.02E-07 6.44E-08 lbs/ton 1.22E-08 7.68E-09 ng 0.033 0.037 ng/dscm 0.01 0.01 lbslhr 1.87E-08 2.17E-08 lbs/ton 2.23E-09 2.58E-09 ng 0.028 0.023 ng/dscm 0.01 0.01 lbs/hr 1.59E-08 1.35E-08 lbs/ton 1.89E-09 1.61E-09 ng 95 97 ng/dscm 32.61 33.93 lbslhr 5.39E-05 5.68E-05 lbs/ton 6.43E-06 6.77E-06 Production Rate (tonslhr) = 

### 8.38 3 Average 0.033 0.05 0.01 0.02 1.83E-08 3.08E-08 2.19E-09 3.67E-09 0.17 0.29 0.06 0.10 9.44E-08 1.67E-07 1.13E-08 2.00E-08

0.068 0.12 0.02 0.04 3.78E-08 6.81E-08 4.51E-09 8.12E-09

0.039 0.04 0.01 0.01 2.17E-08 2.07E-08 2.58E-09 2.47E-09

0.023 0.02 0.01 0.01 1.28E-08 1.40E-08 1.52E-09 1.68E-09 94 95 31.66 32.73 5.22E-05 5.43E-05 6.23E-06 6.48E-06

# SUMMARY OF RESULTS

Run Number C13-233'44'5-HexaCB-(156)

C13-233'44'5'-HexaCB-(157)

C13-233'44'-PentaCB-(105)

C13-23'44'55'-HexaCB-(167)

CB-2344'5-PentaCB-(114)

C13-23'44'5-PentaCB-(118) 

## Table 4c PCB Sampling Data Baghouse #2

1 2 ng 109 110 ng/dscm 37.42 38.47 lbs/hr 6.18E-05 6.44E-05 lbs/ton 7.38E-06 7.68E-06 ng 109 110 ng/dscm 37.42 38.47 lbs/hr 6.18E-05 6.44E-05 lbs/ton 7.38E-06 7.68E-06 ng 114 113 ng/dscm 39.13 39.52 lbs/hr 6.47E-05 6.61E-05 lbs/ton 7.72E-06 7.89E-06 ng 107 106 ng/dscm 36.73 37.08 lbs/hr 6.07E-05 6.20E-05 lbs/ton 7.24E-06 7.40E-06 ng 118 113 ng/dscm 40.51 39.52 lbs/hr 6.69E-05 6.61E-05 lbs/ton 7.99E-06 7.89E-06 ng 116 113 ng/dscm 39.82 39.52 lbs/hr 6.58E-05 6.61E-05 lbs/ton 7.85E-06 7.89E-06 Production Rate (tons/hr) 

### = 8.38 3 Average 102 107 34.36 36.75 5.66E-05 6.09E-05 6.76E-06 7.27E-06 102 107 34.36 36.75 5.66E-05 6.09E-05 6.76E-06 7.27E-06 109 112 36.71 38.46 6.05E-05 6.38E-05 7.22E-06 7.61E-06 100 104 33.68 35.83 5.55E-05 5.94E-05 6.63E-06 7.09E-06 106 112 35.70 38.58 5.89E-05 6.40E-05 7.02E-06 7.63E-06 105 Ill 35.37 38.24 5.83E-05 6.34E-05 6.96E-06 7.57E-06

# SUMMARY OF RESULTS

Run Number C13-2'344'5-PentaCB-(123)

C13-33'44'55'-HexaCB-(169)

C13-33'44'5-PentaCB-(126)

C13-33'44'-TetraCB-(77)

C13-344'5-TetraCB-(81) 

## Table 4d PCB Sampling Data Baghouse #2

1 2 ng 115 111 ng/dscm 39.48 38.82 lbslhr 6.52E-05 6.50E-05 lbs/ton 7.78E-06 7.75E-06 ng 106 106 ng/dscm 36.39 37.08 lbslhr 6.01E-05 6.20E-05 lbs/ton 7.17E-06 7.40E-06 ng 117 117 ng/dscm 40.16 40.92 lbs/hr 6.64E-05 6.85E-05 lbs/ton 7.92E-06 8.17E-06 ng 121 115 ng/dscm 41.54 40.22 lbslhr 6.86E-05 6.73E-05 lbs/ton 8.19E-06 8.03E-06 ng 115 115 ng/dscm 39.48 40.22 lbs/hr 6.52E-05 6.73E-05 lbs/ton 7.78E-06 8.03E-06 Production Rate (tonslhr) 

### = 8.38

10 

### 3 Average 103 110 34.69 37.66 5.72E-05 6.25E-05 6.82E-06 7.45E-06 90 101 30.31 34.59 5.00E-05 5.74E-05 5.96E-06 6.85E-06 113 116 38.06 39.72 6.27E-05 6.59E-05 7.49E-06 7.86E-06 110 115 37.05 39.60 6.11E-05 6.57E-05 7.29E-06 7.84E-06 111 114 37.39 39.03 6.16E-05 6.47E-05 7.35E-06 7.72E-06

### Run Number 2,3,7,8-Tetra CDD 

# *

1,2,3,7,8-Penta CDD

1,2,3,4,7,8-Hexa CDD

1,2,3,6,7,8-Hexa CDD

1,2,3,7,8,9-Hexa CDD 

# SUMMARY OF RESULTS Table 4e Dioxins Sampling Data Baghouse #2

1 2 ng 3.3 3.7 ng/dscm 1.13 1.29 lbslhr 1.87E-06 2.17E-06 lbs/ton 2.23E-07 2.58E-07 ng 3.5 3.6 ng/dscm 1.20 1.26 lbslhr 1.98E-06 2.11E-06 lbs/ton 2.37E-07 2.51E-07 ng 4.9 3.6 ng/dscm 1.68 1.26 lbslhr 2.78E-06 2.11E-06 lbs/ton 3.32E-07 2.51E-07 ng 4.8 3.4 ng/dscm 1.65 1.19 lbslhr 2.72E-06 1.99E-06 lbs/ton 3.25E-07 2.37E-07 ng 4.8 3.5 ng/dscm 1.65 1.22 lbs/hr 2.72E-06 2.05E-06 lbs/ton 3.25E-07 2.44E-07 Production Rate (tonslhr) = 

### 8.38

11 

### 3 Average 4.1 3.7 1.38 1.27 2.28E-06 2.10E-06 2.72E-07 2.51E-07 4.1 3.7 1.38 1.28 2.28E-06 2.12E-06 2.72E-07 2.53E-07 3.9 4.1 1.31 1.42 2.17E-06 2.35E-06 2.58E-07 2.80E-07 3.8 4.0 1.28 1.37 2.11E-06 2.27E-06 2.52E-07 2.71E-07 3.8 4.0 1.28 1.38 2.11E-06 2.29E-06 2.52E-07 2.74E-07

### RunNumber 1,2,3,4,6,7,8-HeptaCDD

1,2,3,4,6,7,8,9-0cta CDD 

# SUMMARY OF RESULTS Table 4f Dioxins SamplingData Baghouse #2

1 2 ng 15.8 3.5 ng/dscm 5.42 1.22 1bslhr 8.96E-06 2.05E-06 lbs/ton 1.07E-06 2.44E-07 ng 30.4 12.3 ng/dscm 10.44 4.30 lbslhr 1.72E-05 7.20E-06 lbs/ton 2.06E-06 8.59E-07 Production Rate (tonslhr) = 

### 8.38

12 

### 3 Average 3.2 7.5 1.08 2.58 1.78E-06 4.26E-06 2.12E-07 5.09E-07 7.7 16.8 2.59 5.78 4.28E-06 9.57E-06 5.10E-07 1.14E-06

### Run Number 2,3,7,8-Tetra CDF 

# **

1,2,3,7,8-Penta CDF

2,3,4,7,8-Penta CDF

1,2,3,4,7,8-Hexa CDF

1,2,3,6,7,8-Hexa CDF 

# SUMMARY OF RESULTS Table 4g Furans Sampling Data Baghouse #2

1 2 ng 190 53 ng/dscm 65.22 18.54 lbs/hr 1.08E-04 3.10E-05 lbs/ton 1.29E-05 3.70E-06 ng 21.2 5.9 ng/dscm 7.28 2.06 lbs/hr 1.20E-05 3.45E-06 lbs/ton 1.43E-06 4.12E-07 ng 23.4 6 ng/dscm 8.03 2.10 lbs/hr 1.33E-05 3.51E-06 lbs/ton 1.58E-06 4.19E-07 ng 33.3 8 ng/dscm 11.43 2.80 lbs/hr 1.89E-05 4.68E-06 lbs/ton 2.25E-06 5.59E-07 ng 15.1 3.2 ng/dscm 5.18 1.12 lbs/hr 8.56E-06 1.87E-06 lbs/ton 1.02E-06 2.23E-07 Production Rate (tons/hr) = 

### 8.38

13 

### 3 Average 78 107 26.27 36.68 4.33E-05 6.07E-05 5.17E-06 7.24E-06 9.7 12.3 3.27 4.20 5.39E-06 6.95E-06 6.43E-07 8.30E-07 12.6 14.0 4.24 4.79 7.00E-06 7.93E-06 8.35E-07 9.46E-07 13 18.1 4.38 6.20 7.22E-06 1.03E-05 8.61E-07 1.22E-06 5.2 7.8 1.75 2.68 2.89E-06 4.44E-06 3.45E-07 5.30E-07

### Run Number 2,3,4,6,7,8-Hexa CDF

1,2,3,7,8,9-HexaCDF

1,2,3,4,6,7,8-Hepta CDF

1,2,3,4,7,8,9-HeptaCDF

1,2,3,4,6,7,8,9-0ctaCDF 

# SUMMARY OF RESULTS Table 4h Furans SamplingData Baghouse #2

1 2 ng 12.2 4.1 ng/dscm 4.19 1.43 lbslhr 6.92E-06 2.40E-06 lbs/ton 8.26E-07 2.86E-07 ng 4.4 4.5 ng/dscm 1.51 1.57 lbslhr 2.50E-06 2.63E-06 lbs/ton 2.98E-07 3.14E-07 ng 25.7 5.9 ng/dscm 8.82 2.06 lbslhr 1.46E-05 3.45E-06 lbs/ton 1.74E-06 4.12E-07 ng 4.6 3.1 ng/dscm 1.58 1.08 lbslhr 2.61E-06 1.81E-06 lbs/ton 3.11E-07 2.16E-07 ng 16.1 5.3 ng/dscm 5.53 1.85 lbs/hr 9.13E-06 3.10E-06 lbs/ton 1.09E-06 3.70E-07 Production Rate (tons/hr) = 

### 8.38

14 

### 3 Average 4.1 6.800 1.38 2.33 2.28E-06 3.86E-06 2.72E-07 4.61E-07 4.5 4.467 1.52 1.53 2.50E-06 2.54E-06 2.98E-07 3.03E-07 7.2 12.9 2.43 4.44 4.00E-06 7.34E-06 4.77E-07 8.76E-07 4 3.9 1.35 1.34 2.22E-06 2.21E-06 2.65E-07 2.64E-07 5.3 8.9 1.79 3.06 2.94E-06 5.06E-06 3.51E-07 6.04E-07

# SUMMARY OF RESULTS Table 5 

## PAH Sampling Data Baghouse #2

Run Number 1 Date 3/18113 Time 955

- 1225 Carbon Dioxide Cone. - % Vol. 0.40 Oxygen Concentration

- %Vol. 20.40 Stack Pressure

- "Hg 28.96 Area ofStack

- Sq. in. 950,400.00 Volume Dry Gas Sampled

- dscf 84.585 Volume Dry Gas Sampled

- dscm 2.395 Stack Temperature- Deg. F 166.80 Percent Moisture - % 1.37 Velocity in the Stack

- FPS 1.25 Volumetric FlowRate

- ACFM 493,680 Volumetric Flow Rate

- DSCFM 397,005 Isokinetic Sampling Rate - % 95.5

15 

### 2 3/18/13 1255

- 1505 0.40 20.40 28.91 950,400.00 84.44 2.391 166.80

1.88 1.20 494,340 394,798

95.9 3 3/18/13 1545

- 1800 0.40 20.50 28.76 950,400.00 86.56 2.451 179.90

1.15 1.30 500,280 392,228

98.9

### Run Number Naphthalene

2-Methylnaphthalene

Acenaphthylene

Acenaphthene

Fluorene

Phenanthrene 

# SUMMARY OF RESULTS Table Sa PAH Sampling Data Baghouse #2

1 2 ng 27400 48800 ng/dscrn 11440.50 20409.87 lbslhr 0.0170 0.0302 lbs/ton 0.0020 0.0036 ng 21700 42900 ng/dscrn 9060.54 17942.28 lbs/hr 0.0135 0.0265 lbs/ton 0.0016 0.0032 ng 2600 3060 ng/dscrn 1085.59 1279.80 lbslhr 0.0016 0.0019 lbs/ton 0.0002 0.0002 ng 1730 2230 ng/dscrn 722.34 932.66 lbs/hr 0.0011 0.0014 lbs/ton 0.0001 0.0002 ng 2230 3290 ng/dscrn 931.11 1375.99 lbslhr 0.0014 0.0020 lbs/ton 0.0002 0.0002 ng 13400 25100 ng/dscrn 5594.99 10497.70 lbslhr 0.0083 0.0155 lbs/ton 0.0010 0.0019 Production Rate (tonslhr) = 

### 8.38 3 Average 43800 40000 17870.26 16573.54

0.0263 0.0245 0.0031 0.0029 29700 31433 12117.50 13040.11

0.0178 0.0193 0.0021 0.0023

4570 3410 1864.55 1409.98 0.0027 0.0021 0.0003 0.0002

2520 2160 1028.15 894.38 0.0015 0.0013 0.0002 0.0002

3480 3000 1419.83 1242.31 0.0021 0.0018 0.0002 0.0002 22400 20300 9139.13 8410.61 0.0134 0.0124 0.0016 0.0015

### Run Number Anthracene

Fluoranthene

Pyrene

Benzo(a)anthracene

Chrysene

Benzo(b)fluoranthene 

# SUMMARY OF RESULTS Table 5b PAH Sampling Data Baghouse #2

1 2 ng 1040 1180 ng/dscm 434.24 493.52 lbs/hr 0.0006 0.0007 lbs/ton 0.0001 0.0001 ng 11100 73500 ng/dscm 4634.66 30740.28 lbs/hr 0.0069 0.0455 lbs/ton 0.0008 0.0054 ng 5200 42700 ng/dscm 2171.19 17858.64 lbs/hr 0.0032 0.0264 lbs/ton 0.0004 0.0032 ng 618 3260 ng/dscm 258.04 1363.45 lbs/hr 0.0004 0.0020 lbs/ton 0.0000 0.0002 ng 3660 29000 ng/dscm 1528.18 12128.82 lbs/hr 0.0023 0.0179 lbs/ton 0.0003 0.0021 ng 503 3320 ng/dscm 210.02 1388.54 lbs/hr 0.0003 0.0021 lbs/ton 0.0000 0.0002 Production Rate (tons/hr) = 

### 8.38 3 Average 1630 1283 665.03 530.93 0.0010 0.0008 0.0001 0.0001 15100 33233 6160.75 13845.23 0.0091 0.0205 0.0011 0.0024

7790 18563 3178.29 7736.04 0.0047 0.0114 0.0006 0.0014

672 1517 274.17 631.89 0.0004 0.0009 0.0000 0.0001

3830 12163 1562.63 5073.21 0.0023 0.0075 0.0003 0.0009

902 1575 368.01 655.52 0.0005 0.0010 0.0001 0.0001

### Run Number Benzo(k)fluoranthene

Benzo(e)pyrene

Benzo(a)pyrene

Perylene

Indeno(1,2,3-cd)pyrene

Dibenz(a,h)anthracene 

# SUMMARY OF RESULTS Table 5c PAH Sampling Data Baghouse #2

1 2 ng 172 1310 ng/dscm 71.82 547.89 lbslhr 1.07E-04 8.10E-04 lbs/ton 1.27E-05 9.67E-05 ng 364 1950 ng/dscm 151.98 815.56 lbs/hr 0.0002 0.0012 lbs/ton 2.70E-05 1.44E-04 ng 37 60 ng/dscm 15.45 25.09 lbslhr 2.30E-05 3.71E-05 lbs/ton 2.74E-06 4.43E-06 ng 33 55 ng/dscm 13.78 23.00 lbslhr 2.05E-05 3.40E-05 lbs/ton 2.45E-06 4.06E-06 ng 27.7 71.3 ng/dscm 11.57 29.82 lbslhr 1.72E-05 4.41E-05 lbs/ton 2.05E-06 5.26E-06 ng 4.7 9.6 ng/dscm 1.96 4.02 lbslhr 2.92E-06 5.94E-06 lbs/ton 3.48E-07 7.09E-07 Production Rate (tons/hr) 

### = 8.38 3 Average 246 576.0 100.37 240.02 1.47E-04 3.55E-04 1.76E-05 4.23E-05 519 944 211.75 393.10 0.0003 0.0006 3.71E-05 6.93E-05 21 39 8.57 16.37 1.26E-05 2.42E-05 1.50E-06 2.89E-06 15 34.3 6.12 14.30 8.99E-06 2.12E-05 1.07E-06 2.53E-06 52.4 50 21.38 20.92 3.14E-05 3.09E-05 3.75E-06 3.69E-06 9.6 8 3.92 3.30 5.76E-06 4.87E-06 6.87E-07 5.81E-07

### RunNumber Benzo(g,h,i)perylene 

# SUMMARY OF RESULTS Table 5d 

## PAH Sampling Data Baghouse #2

1 2 ng 36.4 81.5 ng/dscm 15.20 34.09 lbslhr 2.26E-05 5.04E-05 lbs/ton 2.70E-06 6.02E-06 Production Rate (tonslhr) = 

### 8.38

19 

### 3 Average 64.5 60.8 26.32 25.20 3.87E-05 3.72E-05 4.61E-06 4.44E-06

### DISCUSSION OF RESULTS

Three tests for particulate matter, hydrogen chloride, arsenic, cadmium, chromium, lead, manganese, nickel, mercury, dioxins/:furans, polychlorinated biphenyls, and polycyclic aromatic hydrocarbons were performed onthe Furnace #2 Baghouse. The results ofthe tests appear to be an accurate and valid representation ofthe actual emissions ofthe stack. Leak checks were performed
onthe sampling systems to maintain the integrity ofthe samples and no leaks were detected.
Hydrogen Chloride 

### The moisture percentages were consistent with the largest variation being 66.1 percent from the
mean value of0.84 percent. The flow rates were consistent with the largest variation being 0.61 percent from the mean value of444,697 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 

### % isokinetic) with the largest variation being 4.9 percent from 100 percent.

Particulate/Metals 

### The moisture percentages were consistent with the largest variation being 22.37 percent from the
mean value of0.51 percent. The flow rates were consistent with the largest variation being 0.53 percent from the mean value of448,236 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % 

### isokinetic) with the largest variation being 6.7 percent from 100 percent. Mercury 

### Paired samples for mercury were taken simultaneously for eachrun. The relative deviation percentages were within the allowable limits ofthe method for eachrun.

20

### Dioxins!Furans/PCBs The moisture percentages were consistent with the largest variation being 9.42 percent from the
mean value of0.81 percent. The flow rates were consistent with the largest variation being 0.93 percent from the mean value of442,555 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % 

### isokinetic) with the largest variation being 6.8 percent from 100 percent. Polycyclic Aromatic Hydrocarbons (PAH) 

### The moisture percentages were consistent with the largest variation being 28.18 percent from the
mean value of 1.47 percent. The flow rates were consistent with the largest variation being 0.62 percent from the mean value of394,677 DSCFM. The isokinetic sampling rates were within the specified limits (90 to 110 % 

### isokinetic) with the largest variation being 4.5 percent from 100 percent.

21

### SAMPLINGAND ANALYTICAL PROCEDURES

The testing followed the procedures inthe Appendix to the Code ofFederal Regulations, Title 40, Chapter 1, Part 60, Methods 1, 2, 3A, 4, 5d, 26A, 29, and 30B; and CaliforniaAirResources BoardMethods 428 (CARB 428), and 429 (CARB 429). Threetests wereperformed for each pollutant. The manometer was zeroed and leakchecks were performedbefore eachtest. Leak checks wereperformedonthe sampling systems to maintainthe integrity ofthe samples andno leaks were detected.

A velocity traverse was performed onthe inlettothe baghousepriortothetesting according to EPA Method 5D. The inletvelocity wasused to calculatethe isokinetic setup and determine the velocity in the outlet ofthe baghouse for each test. Once the preliminary inlet velocity was determined, Equation 5D-3 from Method 5D was used to determine the dilution air flow rate ofthe baghouse and applied to thebaghouse velocity.


### Hydrogen Chloride The hydrogen chloride samples were taken accordingto EPAMethods 5D and 26A. Foreachrun, samples offive minute duration were taken isokinetically from each ofthe twenty-four traverse points for a total sampling time of 120 minutes. Blank samples were collected for each reagent used during sampling and analyzed for contamination.

The "front-half'' ofthe sampling train consisted of a glass nozzle, heated glass probe (248op 

### + 25°F), and heated Teflon filter support with a quartz fiber filter (248op 

## +25op). The "back-half'' of the sampling

### train containedthe following impingers: lm:Qinger Contents 1 0.1 N. H2S04 2 0.1 N. H2S04 3 Empty 4 SilicaGel Amount 100ml 100ml
400g

22 

### Parameter HCI HCl Moisture Moisture

### The impingers were measured to determine moisture content and then rinsed and recovered using de-ionized water into a leak-free amber glass samplejarwith a Teflon lid.

The samples were analyzed using ion chromatography by Maxxam Analytics, Inc located in Mississauga, Ontario.



### Particulate Matter/Multiple Metals The particulate matter and multiple metals samples were taken according to EPA Methods 5D and 29. For eachrun, samples oftenminute duration were taken isokinetically from each ofthe twentyfour traverse points for a total sampling time of240 minutes. Data was recorded in five minute intervals. 

### Blank samples were collected for each reagent used during sampling and analyzed for contamination.

The "front-half' of the sampling train consisted of a glass nozzle, heated glass probe (248°F 

### + 25°F), and heated Teflon filter support with a quartz fiber filter (248°F 

### +25°F). The "back-half' of the samplingtrain containedthe following impingers: Impinger 1 2 

### 3 

### 4 Contents 5%HN03/lO%H202 5%HN03/lO%H202 Empty Silica Gel Amount lOOml lOOml

400 g Parameter Metals Metals Metals Moisture

The filter was recovered and collected in a sealed petri dish. The "front-half' ofthe sampling train (nozzle, probe, and front-halffilter holder) was rinsed with acetone and collected in a leak-free amber glass sampling bottle with teflon lid. The "front-half' ofthe sampling train (nozzle, probe, and front-half offilter holder) was then rinsed three times with a total of 1 OOml of0.1 N HN03 and collected in a leak-free amber glass sample bottle with Teflon lid. The impinger contents
were measured to determine the moisture content and then collected in a leak-free amber glass sample bottle with teflon lid. The back-half of the filter holder, impingers, and connecting 23

### glassware were then rinsed with three times with a total of 1 OOml of0.1 N HN03 and collected into the same sample bottle as the impinger contents.

The metals samples were analyzed by ICP-MS and ICP-AES according to EPA Method 29, by Maxxam Analytics, Inc located in Mississauga, Ontario. The particulate samples were analyzed using gravimetric analysis byTEST, Incorporated locatedinPoca, WestVirginia. 

### Mercury The mercury samples were taken according to EPA Methods 30B. Samples ofeighteen minute duration were taken from each of the seven traverse points for a total sampling time of 126 minutes on each stack. Each run consisted ofpaired samples. Blank and spiked samples were taken, recovered, and analyzed for contamination. The sampling train consisted ofa two stage sorbent trap, heated probe, sample line, and gas meter and pump. The paired sorbent traps were contained withinthe heatedprobe.

The samples were analyzed for mercury by Ohio Lumex, Twinsburg, Ohio. 

### Dioxins/Furans/Polychlorinated Biphenyls The dioxins/furans/PCBs samples were taken according to EPA Method 5D and CARB 428. For eachrun, samples offive minute duration were taken isokinetically from each ofthe twenty-four traverse points for a total samplingtime of 120 minutes. Datawasrecorded infive minute intervals. Blank samples were collected for eachreagent used during sampling and analyzed for contamination. A trainblankwas also performed and analyzed for contamination.

The "front-half' ofthe sampling

### train consisted ofa glassnozzle, heated glassprobe (248op

## ± 25op), andheated Teflonfilter support with a quartz fiber filter (248op

## ±25op). The "back-half' of the sampling train contained the following impingers:

24

### lmQinger Contents Amount Parameter Water-cooled condenser coil Water-cooled XAD-2 adsorbenttube 1 Empty



### --------- Dioxins/Furans/PCBs 2 De-ionized water 100m1 Dioxins/Furans/PCBs 

### 3 empty Dioxins/Furans/PCBs 4 Silica Gel 400g Moisture
The filter wasrecovered and collected ina sealedpetri dish. The "front-half' ofthe sampling train (nozzle, probe, and front-halfoffilter holder) was rinsed and brushedthree times with methanol, benzene, and methylene chloride and collected in a leak-free amber glass sampling bottle withteflon lid. The impinger contents were measuredto determine the moisture content and then collected ina leak-free amber glass sample bottle withteflon lid. The "back-half' of the filter holder, connecting glassware before the condenser, andthe condenserwas rinsed with methanol, benzene, and methylene chloride and collected ina leak-free amberglass sampling bottle withteflonlid. The XAD-2 trap wasrecovered, covered with aluminum foil and refrigerated.
The dioxins/furans/PCBs samples were analyzed byhighresolution mass spectrometry according to CARB 428, by MaxxamAnalytics, Inc located inMississauga, Ontario. 

### PolycyclicAromatic Hydrocarbons Thepolycyclic aromatic hydrocarbon samples were taken according to CARB 429. Foreachrun, samples offive minute duration were takenisokineticallyfrom each ofthetwenty-fourtraverse points for a total samplingtime of 120minutes. Datawasrecorded infive minute intervals. Blank samples were collected for eachreagentused during sampling andanalyzed for contamination.

The "front-half' ofthe samplingtrainconsisted ofa glass nozzle, heated glassprobe (248<>p 

## ± 25<>p), andheated Teflon filter supportwith a quartz fiber filter (248<>p

# ±25°F). The "back-half' of the sampling train containedthe following impingers: 25

### Im,ninger Contents Amount Parameter Water-cooled condenser coil Water-cooled XAD-2 adsorbent tube 1 

### Empty



### --------- PAH 2 3mM NaHC03/2.4mMNa2C03 lOOml PAH 3 3mM NaHC03/2.4mMNa2C03 lOOml PAH 4 empty PAH 5 

### Silica Gel 400 g Moisture

The filter was recovered and collected in a sealed petri dish. The impinger contents were measured to determine the moisture content and then collected in a leak-free amber glass sample bottle with Teflon lid. The "front-half' and "back-half' ofthe sampling train (nozzle, probe, and front and back-halfoffilter holder, connecting glassware, and condenser) were rinsed three times each with acetone, hexane, and methylene chloride and collected in a leak-free amber glass sample bottle with Teflon lid. The impingers and connecting glassware were then rinsed three times each with acetone, hexane, and methylene chloride and collected into the same sample bottle as the impinger contents. The XAD-2 trap was recovered, covered with aluminum foil and refrigerated.

The PAH samples were analyzed according to CARB 429 by Maxxam Analytics, Inc located in Mississauga, Ontario.

26

### Baghouse 2

N -...] 

### Baghouse 2

40' Duct Dimensions = 

### 40' x 165' Area OfDuct = 

### 950,400.0 sq. inches

Drawings Notto Scale 165' 

# • • • 

# •
• • 

# • 

# •
• 

# • • •
• • • •

-**~** .... ""'1 

# • • • 

# •

- -**~- -~**  .. -**~ -~** **.~** 

### - "" .. 

# • • • •
• • • • 

# • • • • 

# • • 

# • •

-------**--~----** ------L ··----**--~---** -- 

# • •

Traverse

Points 1 2 

### 3 4 

# •


# • • •

I**----------~-** ---·· I 

# •

Feet from Stack Wall 

### 5 15 25 35 

# •

### Furnace #2 Baghouse Inlet



# -- Gas Flow 

# - 

# 5

# I

.N 

### 696" 144"

Traverse Percent of Inches From Points Diameter Stack Wall 1 2.1 3 3/16 2 6.7 10 2/16 3 11.8 1714/16 4 17.7 26 13/16 5 25.0 37 14116 Inside Diameter ofStack = 

### 12 ft. 7.5 

### m. 6 35.5 53 13/16 Port to Upstream Distance = 

### 12 ft. 0.0 

### m. 7 64.5 97 11116 Portto Downstream Distance = 

### 58 ft. 0.0 in. 8 75.0 113 10/16 Area OfStack = 

### 18,026.7 sq. inches 9 82.3 124 11116 Port to Upstream Distance = 

### 0.95 Stack Diameters 10 88.2 133 10/16 Portto Downstream Distance = 

### 4.59 Stack Diameters 11 93.3 141 6/16 DrawingsNotto Scale 12 97.9 148 5/16

## APPENDIXES

A - ComputerDataand Example Calculations B - Pre-flow Data C - Analytical Data D - Field Data Sheets E - Calibration Data F - Chain ofCustody G - Plant Operational Data

29

### APPENDIX A COMPUTERDATA AND EXAMPLE CALCULATIONS .::.•

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #2 PROJECT#: TI1550

Run Number 1 2 3 Date 3/19/13 3/19/13 3/19/13 Time 855

- 1110 1215

- 1425 1600

- 1815 0 = Sample time 120 120 120 minutes Pb = Barometric Pressure at Port Elevation 29.05 29.05 29.05 in. Hg Vm =Vol. ofMetered Gas- meter cond., cal corr. 108.701 107.025 101.416 cu. ft. Tm =Meter Temperature 80.8 80.4 53.0 Farenheit Tm =MeterTemperature 540.8 540.4 513.0 Rankine Po = Meter Orifice Pressure 2.30 2.30 2.00 in. H20 Pma =MeterPressure Absolute 29.22 29.22 29.20 in. Hg Vtwet =Sampled Gas Volume Wet 125.080 121.557 123.337 cu. ft. Vtstd = Sampled Gas Volume at Stand. Cond., dry 103.659 102.137 101.876 cu.ft Vtstd = Sampled Gas Volume at Stand. Cond., dry 2.935 2.892 2.885 cu. Meter C02 =% C02, dry 0.40 0.40 0.50 % 02 =% 02, dry 20.40 20.50 20.40 %
co =%co, dry 0.00 0.00 0.00 % N2 = %N2,dry (N2+CO) = 1 OO-(C02+02) 79.20 79.10 79.10 % EA =Excess Air 3,469.4 4,442.0 3,633.1 % Vw =Volume Water 31.0 10.8 13.5 grams H20 =mgas 1.39 0.50 0.62 % H20 = Moisture in Gas at Saturation 26.07 24.14 30.78 % Md = Dry Molecular Weight ofStack Gas 28.88 28.88 28.90 Mw =Wet Molecular Weight ofStack Gas 28.73 28.83 28.83 Psg = Stack Pressure, gauge - measured 0.10 0.00 0.10 in. H20 Psa = Stack Pressure, absolute 29.06 29.05 29.06 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #2 PROJECT#: TI1550

Run Number 1 2 3 Ts =Stack Temperature 150.30 147.20 157.10 Farenheit Ts = Stack Temperature 338.72 337.00 342.50 Kelvin Ts =Stack Temperature 610.3 607.2 617.1 Rankine 

# \I L1 

### P = Avg. Sum. ofPressure Square Root 0.022 0.022 0.022

Vs = Velocity in the Stack 81.0 80.7 81.4 ft/min Vs = Velocity inthe Stack 1.35 1.30 1.40 ft/sec As = Effective Stack Area 950,400.0 950,400.0 950,400.0 sq. m. Qa =Volumetric Flow Rate at stack cond. 534,600 532,620 537,240 acfm Qs = Volumetric Flow Rate, stand. cond., dry 442,970 447,432 443,690 dscfm IR = Isokinetic Ratio (Vn/Vs)* 100 104.9 102.3 102.9 

### %

# TEST, Inc. 

# romments: HCI Sampling Data Project# TI1550 Meter Box# 2010 %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0203 %02 20.40 1 705.2 693.2 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 710.3 722.7

Operator br Nozzle# %N2 79.20 3 599.1 606.9 Run# 1 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 872.3 895.1

Date 3/19/13 Stack Dia.(in.) Final Moist. % 1.39 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic % 104.9 6 Min/pt 5 Bar. Press. ("Hg) 29.05 Initial Leak Rate 

### 0.001 cfm@ 10 "Hg Filter# Leak Check Vol. Final Leak Rate 0.001 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 855 898.665 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 11-6 900 903.210 0.0005 2.30 0.864 5.0 138 246 252 68 77 76

5 905 907.007 0.0005 2.30 0.864 5.0 138 247 251 65 

### 80 78 4 910 911.502 0.0005 2.30 0.864 5.0 143 252 251 67 82 80 3 915 918.908 0.0005 2.30 0.864 5.0 142 252 249 66 85 82 2 920 920.502 0.0005 2.30 0.864 5.0 146 249 251 66 89 87 1 925 924.975 0.0005 2.30 0.864 5.0 155 251 251 63 82 80 10-6 935 929.403 0.0005 2.30 0.864 5.0 143 241 250 58 87 86

5 940 933.807 0.0005 2.30 0.864 5.0 143 247 250 60 82 80 4 945 938.305 0.0005 2.30 0.864 5.0 147 253 250 63 85 84 3 950 942.801 0.0005 2.30 0.864 5.0 146 250 250 68 82 80 2 955 947.206 0.0005 2.30 0.864 5.0 145 249 250 47 78 77 1 1000 951.406 0.0005 2.30 0.864 5.0 147 248 249 50 78 76 9-6 1010 955.808 0.0005 2.30 0.864 5.0 175 244 250 51 83 80

5 1015 960.305 0.0005 2.30 0.864 5.0 176 248 250 51 81 79 4 1020 964.803 0.0005 2.30 0.864 5.0 178 253 250 53 80 78 3 1025 969.206 0.0005 2.30 0.864 5.0 165 252 249 53 82 80 2 1030 974.002 0.0005 2.30 0.864 5.0 151 249 250 53 81 78 

### 1 1035 978.203 0.0005 2.30 0.864 5.0 152 250 250 54 82 81 8-6 1045 982.706 0.0005 2.30 0.864 5.0 146 249 251 52 77 75

5 1050 987.003 0.0005 2.30 0.864 5.0 146 249 249 56 80 78 4 1055 991.702 0.0005 2.30 0.864 5.0 149 249 249 56 80 79 3 1100 996.103 0.0005 2.30 0.864 5.0 149 252 249 57 83 82 2 1105 1,000.702 0.0005 2.30 0.864 5.0 143 248 251 57 80 80 1 1110 1,005.203 0.0005 2.30 0.864 5.0 145 250 250 58 84 82

## Example Calculations Run Number Pb 29.05 "Hg Barometric Pressure Cp 0.84 Vw 31 Water weight gain Ds 0 Pm 2.3 "H20 Meter pressure As 950,400.0 Avg L1 

### P 0.001 "H20 Differential pressure Dn 1.5 AvgSqrti1 P 0.022 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen

Vm 106.538 acf Ps 0.10 "H20 Tm 80.8 (F) Ts 150.3 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# ~J Tm(R)

Vwgas = 0.0471 * Vw = 0.0471 * %N2 79.20 108.701 (acf* Y) 

### Dry Gas Volume

29.06 "Hg Stack Pressure 540.8 (R) Meter Temperature 610.3 (R) 

### Stack Temperature

# ~ 17.65 

## * 108.701 ' [ 

### 2.30 29.05 

### + 13.6 540.8 

# l

31 1.4601 sft 3 

### Pitot Cal m. Stack Diameter Sq in. Stack Area m Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

103.659 sft j



### 1.728 scfm

Bws= Vwgas Bws*100 = 1.39 %Moist. Md = 28.880 Vmstd 

### + Vwgas

Ts (R) 

### Vs = 5129.4 * Cp * \ Ps * Mw

5129.4 * 0.84 1-Bws = 0.9861

* sqrt L1 

### P 610.3 29.06 * 28.729 * 0.022

ACFM= Vs *As 144 81.0 * 950400.0 144 534,600 ACFM ====== 

### MW = 28.729 =====



### 81.0 fpm 1.35 fps ==== ======



### DSCFM = ACFM * 528 * Ps 

# * (1-Bws) Ts (R) * 29.92 534,600 * 528 * 29.06 * 0.9861 610.3 * 29.92 442,970 DSCFM

0 /o 

### Iso. 

### = 1039 * Vmstd * Ts (R) 

### (1-Bws) * Ps * Tt 

### * Vs * (DnY'2 1,039 * 103.659 0.9861 * 29.06 * 120 

## * 610.3 104.9 % 

## * 81.0 * 2.25000

# TEST, Inc. 

# I Comments: 

### HCI Sampling Data Project# TI1550 MeterBox# 20I0 %C02 0.40 Imp. Initial Final Plant Felman Productions LLC MeterCal. (Y) 1.0203 %02 20.50 1 710 688.9 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 710.1 721.1

Operator br Nozzle# %N2 79.10 3 604.5 609.3 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 895.1 911.2

Date 3/19/13 Stack Dia.(in.) Final Moist. % 0.50 5 Sample Time 120 Static Press.("H20) Final Isokinetic % 102.3 6 

### Min/pt 5 Bar. Press. ("Hg) 29.05 

### Initial Leak Rate 0.001 cfm@ 15 "Hg Filter# Leak CheckVol. Final Leak Rate 0.001 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 1215 9.705 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out

7-8 1220 10.208 0.0005 2.30 0.864 5.0 152 242 246 58 78 76

7 1225 15.718 0.0005 2.30 0.864 5.0 150 249 249 63 76 

## 74 6 1230 19.307 0.0005 2.30 0.864 5.0 149 253 251 66 80 78 5 1235 23.809 0.0005 2.30 0.864 5.0 151 250 254 67 86 84 4 1240 28.400 0.0005 2.30 0.864 5.0 158 251 252 59 82 80 3 1245 32.908 0.0005 2.30 0.864 5.0 162 251 250 61 83 81 2 1250 37.507 0.0005 2.30 0.864 5.0 157 251 249 60 84 82 I 1255 42.105 0.0005 2.30 0.864 5.0 154 250 248 64 80 78 6-8 1305 46.902 0.0005 2.30 0.864 5.0 120 246 248 53 78 76

7 1310 51.203 0.0005 2.30 0.864 5.0 126 251 248 61 77 75 6 1315 55.801 0.0005 2.30 0.864 5.0 128 252 251 61 78 77 5 1320 59.107 0.0005 2.30 0.864 5.0 131 251 252 55 74 72 4 1325 65.506 0.0005 2.30 0.864 5.0 136 252 251 61 78 76 3 1330 69.405 0.0005 2.30 0.864 5.0 136 251 251 65 79 77 2 1335 73.902 0.0005 2.30 0.864 5.0 131 249 249 48 79 78 I 1340 78.505 0.0005 2.30 0.864 5.0 142 251 249 52 83 80 5-8 1350 83.104 0.0005 2.30 0.864 5.0 146 249 249 49 88 86

7 1355 87.502 0.0005 2.30 0.864 5.0 162 249 249 51 89 88 6 1400 91.908 0.0005 2.30 0.864 5.0 158 251 250 51 90 88 5 1405 96.409 0.0005 2.30 0.864 5.0 155 252 250 50 85 82 4 1410 101.003 0.0005 2.30 0.864 5.0 155 250 250 50 79 78 3 1415 105.007 0.0005 2.30 0.864 5.0 156 250 251 53 78 77 2 1420 110.008 0.0005 2.30 0.864 5.0 160 249 251 55 83 82 I 1425 114.601 0.0005 2.30 0.864 5.0 158 247 250 56 85 83

## Example Calculations Run Number 2 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 10.8 Water weight gain Ds 0 in. Stack Diameter Pm 2.3 "H20 Meterpressure As 950,400.0 Sq in. Stack Area Avg!::. P 0.001 "H20 Differential pressure Dn 1.5 in Nozzle Diameter Avg Sqrt!::. P 0.022 "H20 Sqrt Diff. press. Tt 120 min Sample Time %C02 0.40 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.50 Oxygen

Vm 104.896 acf Ps 0.00 "H20 Tm 80.4 (F) Ts 147.2 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm(R) %N2 79.10 107.025 (acf* Y) Dry Gas Volume 29.05 "Hg Stack Pressure 540.4 (R) 

### Meter Temperature 607.2 (R) 

### Stack Temperature



## = 17.65 • 107.025 • [ 

### 2.30 29.05 

### + 13.6 540.4 

# }Nitrogen

102.137 sft 5



### 1.702 scfm

Vwgas = 0.0471 * Vw = 

### 0.0471 * 10.8 0.5087 sft 3



### Bws= Vwgas Vmstd 

### +Vwgas

Vs = 5129.4 *

5129.4 * Ts (R) 

### \Ps 

## * Mw

0.84 Bws* I

### 00 = 0.50 % Moist. Md = 28.884 ===== 

### 1-Bws = 0.9950 MW = 28.830

* sqrt !::. 

### P 607.2 29.05 * 28.830 * 0.022 

## = 80.7 fpm 1.3 ==== =====


### ACFM= Vs *As 144 80.7 * 950400.0 144 532,620 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) 

### * 29.92 532,620 * 528 * 29.05 * 0.9950 607.2 * 29.92 447,432 DSCFM



### % Iso.= 1039 * Vmstd * Ts (R) 

### (1-Bws) * Ps * Tt * Vs * (Dn)"2 1,039 * 102.137 * 607.2 0.9950 * 29.05 * 120 * 80.7 * 2.25000 102.3 %

# TEST, Inc. 

# I Comments: 

### HCI Sampling Data Project# TI1550 Meter Box# 20IOmst %C02 0.50 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.40 I 709.9 756.3 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 710.5 659.6

Operator br Nozzle# %N2 79.10 3 603.5 603.5 Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 896.9 914.9

Date 3/19/13 Stack Dia.(in.) Final Moist. % 0.62 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic % 102.9 6 Min/pt 5 Bar. Press. ("Hg) 29.05 Initial Leak Rate 

### 0 cfm@ 10 "Hg Filter# Leak Check Vol. Final Leak Rate 0 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1600 730.157 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 4-6 1605 734.300 0.0005 2.00 0.814 3.0 155 255 249 61 51 49

5 1610 738.420 0.0005 2.00 0.814 3.0 156 254 250 60 

### 51 49 4 1615 742.600 0.0005 2.00 0.814 3.0 154 247 251 60 54 52 3 1620 746.790 0.0005 2.00 0.814 3.0 154 251 253 64 54 54 2 1625 750.920 0.0005 2.00 0.814 3.0 153 254 252 61 54 52 1 1630 755.075 0.0005 2.00 0.814 3.0 153 262 250 64 54 53 3-6 1640 759.140 0.0005 2.00 0.814 3.0 155 266 254 

### 61 53 49

5 1645 763.300 0.0005 2.00 0.814 3.0 157 262 250 57 52 50 4 1650 767.405 0.0005 2.00 0.814 3.0 156 256 250 58 54 51 3 1655 771.515 0.0005 2.00 0.814 3.0 150 257 250 58 53 51 2 1700 775.645 0.0005 2.00 0.814 3.0 154 260 249 60 54 52 1 1705 779.725 0.0005 2.00 0.814 3.0 153 259 249 60 54 52 2-6 1715 783.850 0.0005 2.00 0.814 3.0 155 268 248 67 56 52

5 1720 787.975 0.0005 2.00 0.814 3.0 156 260 251 58 57 53 4 1725 792.080 0.0005 2.00 0.814 3.0 159 254 250 56 56 53 3 1730 796.245 0.0005 2.00 0.814 3.0 161 256 249 54 55 53 2 1735 800.400 0.0005 2.00 0.814 3.0 156 259 249 55 55 53 1 1740 804.560 0.0005 2.00 0.814 3.0 157 260 250 56 56 54 1-6 1750 808.700 0.0005 2.00 0.814 3.0 160 267 250 64 54 52 5 1755 812.845 0.0005 2.00 0.814 3.0 163 261 251 58 54 52 4 1800 817.000 0.0005 2.00 0.814 3.0 164 258 252 56 54 53 3 1805 821.225 0.0005 2.00 0.814 3.0 164 256 252 54 55 53 2 1810 824.410 0.0005 2.00 0.814 3.0 162 258 251 52 54 53 l 1815 828.600 0.0005 2.00 0.814 3.0 163 260 250 55 54 51

## Example Calculations Run Number 3 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Vw 13.5 Water weight gain Ds 0 Pm 2 "H20 Meter pressure As 950,400.0 Avg**~** 

### P 0.001 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.50 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen

Vm 98.443 acf Ps 0.10 "H20 Tm 53.0 (F) Ts 157.1 (F)

Vmstd = 17.65 *Vm * [ Pb 

### +

# 1~] Tm(R) %N2 79.10 101.416 (acf

## *Y) Dry Gas Volume 29.06 "Hg Stack Pressure

513 (R) 

### Meter Temperature 617.1 (R) 

### Stack Temperature


# = 17.65 * 101.416 * [ 29.05 

### +

# ~~~~ ]= 513.0

Vwgas = 0.0471 *Vw = 0.0471 

## * 13.5 0.6359 sft 3 

### Pitot Cal Ill. 

### Stack Diameter Sq in. Stack Area Ill 

### Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

101.876 sft j



### 1.698 scfm

Bws= Vwgas Bws*100 

### = 0.62 %Moist. Md 

### = 28.896 ===== Vmstd 

### +Vwgas 1-Bws 

### = 0.9938 MW = 28.828

Ts (R) 

### Vs= 5129.4 * Cp * \Ps * Mw * sqrt**~** 

### P 617.1 5129.4 * 0.84 29.06 * 28.828 

## * 0.022 81.4 fipm

ACFM= Vs *As 144 81.4 * 950400.0 144

DSCFM = ACFM * 528 * Ps 

# * (1-Bws) Ts (R) 

### * 29.92

% 

### Iso. 

### = 1039 *Vmstd * Ts (R) 

### (1-Bws) * Ps * Tt 

### * Vs * (DnY'2 1,039 * 101.876 0.9938 * 29.06 * 120 

## * * ==== 537,240 ACFM

537,240 * 528 

## * 29.06 

## * 0.9938 617.1 * 29.92

617.1 102.9 % 81.4 

## * 2.25000 ===1=.4==fps

443,690 DSCFM

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC Baghouse #2 UNIT: PROJECT#: TI1550

Run Number Date Time 0 = Sample time Pb = Barometric Pressure at Port Elevation Vm = Vol. ofMetered Gas

- meter cond., cal corr. Tm = Meter Temperature Tm = Meter Temperature Po = Meter Orifice Pressure Pma = Meter Pressure Absolute Vtwet =Sampled Gas Volume Wet Vtstd = Sampled Gas Volume at Stand. Cond., dry Vtstd = Sampled Gas Volume at Stand. Cond., dry C02 =% C02, dry 02 =% 02, dry 

# co =%CO, dry N2 = %N2,dry (N2+CO) = 1 OO-(C02+02) EA =Excess Air Vw =Volume Water H20 =mgas H20 =Moisture in Gas at Saturation Md = Dry Molecular Weight ofStack Gas Mw = Wet Molecular Weight ofStack Gas Psg = Stack Pressure, gauge - measured Psa = Stack Pressure, absolute 1 3/20/13 900

- 1315 240 29.15 216.202

74.0 534.0 2.22 29.31 247.268 209.472

5.932 0.40 20.40 0.00 79.20 3,469.4

17.9 0.40 22.81 28.88 28.84 0.10 29.16 2 3 3/20113 3/20/13 900- 1315 1440

- 1850 240 240 29.15 29.05 204.513 224.790

56.5 81.8 516.5 541.8 2.00 2.30 29.30 29.22 245.471 252.611 204.748 213.968

5.798 6.059 0.40 0.40 20.40 20.50 0.00 0.00 79.20 79.10 3,469.4 4,442.0

27.2 22.9 0.62 0.50 27.90 21.43 28.88 28.88 28.81 28.83 0.10 0.10 29.16 29.06 minutes in. Hg
cu. ft. Farenheit Rankine in. H20 in. Hg
cu. ft. cu.ft
cu. Meter % % % % % grams % %

in. H20 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #2 PROJECT#: TI1550

Run Number 1 2 3 Ts =StackTemperature 145.10 153.20 142.50 Farenheit Ts =StackTemperature 335.83 340.33 334.39 Kelvin Ts = Stack Temperature 605.1 613.2 602.5 Rankine 

# 'I L1 

### P = Avg. Sum. ofPressure Square Root 0.022 0.022 0.022

Vs = Velocity in the Stack 80.4 81.0 80.4 ft/min Vs = Velocity inthe Stack 1.34 1.40 1.30 ft!sec As = Effective Stack Area 950,400.0 950,400.0 950,400.0 sq.m. Qa = Volumetric Flow Rate at stack cond. 530,640 534,600 530,640 acfm Qs = Volumetric Flow Rate, stand. cond., dry 449,461 445,847 449,401 dscfm IR = Isokinetic Ratio (Vn/Vs)*100 104.4 102.9 106.7 % 

### Mn = Particulate Matter Catch, grams 0.0051 0.0042 0.0048 grams

= Particulate Matter Catch, milligrams 5100.00 4233.33 4800.00 ug Ca = Particulate Matter Cone.

- Stack Cond. 0.0003 0.0003 0.0003 gr/acf Cs = Particulate Matter Cone.

- Dry Std. Cond. 0.0004 0.0003 0.0003 gr/dscf

= Particulate MatterEmissions * 859.74 730.14 792.21 ug/dscm ER = Particulate MatterEmissions 1.54 1.15 1.16 lbs/hr

# TEST, Inc.**~Comments:** Particulate/Metals Sampling Data**~----------------------------------------~** Project# TI1550 Meter Box# 2010 %C02 0.40 Imp. Initial Final



## ------ Plant Felman Productions LLC Meter Cal. (Y) 1.0203 %02 20.40 1 727.1 686.4 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 758.4 776.6



### ----- ------ Operator br Nozzle# %N2 79.20 3 608.8 613.4 Run# I Nozzle Dia. (in.) 1.5 Assumed Moist% 1.17 4 917.7 953.5



## ----- ------ Date 3/20/13 Stack Dia.(in.) Final Moist.% 0.40 5



## ------ Sample Time 240 Static Press.("H20) 0.10 Final Isokinetic % 104.4 6



## ------------- Min/pt 5 Bar. Press. ("Hg) 29.15 

### Initial Leak Rate 0.001 cfm@ 14 "Hg



### --- Filter# 1007 Leak Check Vol. Final Leak Rate 0.001 cfm@ 12 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 900 277.406 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In 

### Out 11-6 905 282.005 0.0005 2.20 0.848 5.0 130 245 250 60 66 64

6 910 286.306 0.0005 2.20 0.848 5.0 130 251 248 66 69 67 5 915 290.507 0.0005 2.20 0.848 5.0 131 250 254 67 76 74 5 920 294.803 0.0005 2.20 0.848 5.0 139 252 251 67 81 80 4 925 299.205 0.0005 2.20 0.848 5.0 133 246 250 68 72 70 4 930 303.601 0.0005 2.20 0.848 5.0 152 243 249 66 70 68 3 935 307.908 0.0005 2.20 0.848 5.0 152 253 251 68 79 77 3 940 312.305 0.0005 2.20 0.848 5.0 149 250 250 55 78 76 2 945 316.705 0.0005 2.20 0.848 5.0 148 250 252 51 65 63 2 950 321.107 0.0005 2.20 0.848 5.0 153 251 250 53 64 63 1 955 325.407 0.0005 2.20 0.848 5.0 139 246 249 50 68 65 1 1000 329.805 0.0005 2.20 0.848 5.0 139 251 249 51 70 68 10-6 1010 334.108 0.0005 2.20 0.848 5.0 139 242 249 51 67 66

6 1015 338.401 0.0005 2.20 0.848 5.0 142 251 250 51 70 68 5 1020 343.103 0.0005 2.20 0.848 5.0 143 251 250 54 69 68 5 1025 347.106 0.0005 2.20 0.848 5.0 141 247 250 53 71 70 4 1030 351.406 0.0005 2.20 0.848 5.0 140 250 251 53 67 65 4 1035 356.609 0.0005 2.20 0.848 5.0 145 251 250 56 71 70 3 1040 360.104 0.0005 2.20 0.848 5.0 140 249 250 58 72 70 3 1045 364.408 0.0005 2.20 0.848 5.0 141 251 250 58 72 71 2 1050 368.805 0.0005 2.20 0.848 5.0 138 247 249 56 73 70 2 1055 373.201 0.0005 2.20 0.848 5.0 148 255 250 56 74 72 1 1100 377.508 0.0005 2.20 0.848 5.0 152 251 251 56 75 73 1 1105 381.909 0.0005 2.20 0.848 5.0 146 247 251 57 75 73 9-6 1115 386.306 0.0005 2.20 0.848 5.0 153 244 250 56 75 73

6 1120 390.703 0.0005 2.20 0.848 5.0 152 248 250 55 75 74 5 1125 395.503 0.0005 2.20 0.848 5.0 160 250 250 55 74 72 5 1130 399.408 0.0005 2.20 0.848 5.0 148 249 250 53 76 74 4 1135 404.508 0.0005 2.20 0.848 5.0 152 252 250 55 76 74 4 1140 408.202 0.0005 2.20 0.848 5.0 148 249 251 55 73 71 3 1145 412.509 0.0005 2.20 0.848 5.0 155 252 250 56 75 74

## Example Calculations Run Number Pb 29.15 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 17.9 Water weight gain Ds 0 in. Stack Diameter Pm 2.22 "H20 Meter pressure As 950,400.0 Sq in. Stack Area Avg 11 

### P 0.001 "H20 Differential pressure Dn 1.5 in Nozzle Diameter Avg Sqrt 11 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 240 mm Sample Time %C02 0.40 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.40 Oxygen

Vm 211.9 acf Ps 0.10 "H20 Tm 74.0 (F) Ts 145.1 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm(R) 216.202 29.16

534 605.1

:::::: 17.65 %N2 79.20 Nitrogen (acf* Y) Dry Gas Volume "Hg Stack Pressure (R) Meter Temperature (R) Stack Temperature

• 216.202 • [ 2.22 29.15 

### + 13.6 534.0 ] = 209.472 sft j 

### 3.491 scfm

Vwgas=0.0471*Vw= 0.0471 * 17.9 0.8431 sft 3



### Bws= Vwgas Vmstd 

### + Vwgas

Ts (R) 

### Vs=5129.4*Cp* \Ps*Mw

5129.4 * 0.84 Bws*100 = 0.40 %Moist. Md = 28.880 ===== 

### 1-Bws = 0.9960 MW = 28.836 =====



### * sqrt 11 

### P 605.1 29.16 * 28.836 * 0.022 = 80.4 fpm 1.34 :tips ==== =====


### ACFM= Vs *As 144 80.4 * 950400.0 144

DSCFM = ACFM * 528 * Ps 

# *(1-Bws) Ts (R) * 29.92

%Iso.= 1039 * Vmstd 

## * Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (Dn)"2 1,039 * 209.472 530,640 ACFM

530,640 * 528 

## * 29.16 

## * 0.9960 605.1 * 29.92

* 605.1 104.4 % 0.9960 * 29.16 * 240 * 80.4 * 2.25000 449,461 DSCFM

# TEST, Inc. 

# I Comments: 

## Particulate/Metals Sampling Data Project# TI1550 MeterBox# 20IOmst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.40 1 709.1 667.4 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 692.8 719.1

Operator csm Nozzle# %N2 79.20 3 600.2 610.6 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % 1.80 4 913.4 945.6

Date 3/20113 Stack Dia.(in.) Final Moist. % 0.62 5 Sample Time 240 Static Press.("H20) 0.10 Final Isokinetic % 102.9 6 Min/pt 5 Bar. Press. ("Hg) 29.15 Initial Leak Rate 

### 0 cfm@ 12 "Hg Filter # I006 Leak Check Vol. Final Leak Rate 0 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 900 881.892 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 4-6 905 886.015 0.0005 2.00 0.814 4.0 151 256 244 66 49 47

6 910 889.995 0.0005 2.00 0.814 4.0 155 258 247 66 

### 48 45 5 915 893.990 0.0005 2.00 0.814 4.0 156 261 251 65 55 50 5 920 898.065 0.0005 2.00 0.814 4.0 159 263 250 64 55 51 4 925 902.140 0.0005 2.00 0.814 4.0 156 264 249 65 55 50 4 930 906.255 0.0005 2.00 0.814 4.0 154 259 250 62 58 48 3 935 910.380 0.0005 2.00 0.814 4.0 153 257 250 62 57 48 3 940 914.500 0.0005 2.00 0.814 4.0 151 263 251 60 57 49 2 945 918.585 0.0005 2.00 0.814 4.0 152 255 2479 60 56 49 2 950 922.707 0.0005 2.00 0.814 4.0 156 258 250 60 57 49 1 955 926.815 0.0005 2.00 0.814 4.0 160 259 252 61 57 50 1 1000 830.957 0.0005 2.00 0.814 4.0 161 262 250 61 57 50 3-6 1010 935.080 0.0005 2.00 0.814 4.0 161 257 250 65 54 49

6 1015 939.215 0.0005 2.00 0.814 4.0 160 256 250 63 547 49 5 1020 943.400 0.0005 2.00 0.814 4.0 163 255 250 60 55 50 5 1025 947.435 0.0005 2.00 0.814 4.0 156 261 251 59 56 50 4 1030 951.550 0.0005 2.00 0.814 4.0 150 265 250 59 57 50 4 1035 955.660 0.0005 2.00 0.814 4.0 151 258 251 58 57 50 3 1040 959.770 0.0005 2.00 0.814 4.0 153 259 250 59 55 49 3 1045 963.880 0.0005 2.00 0.814 4.0 155 259 250 60 56 50 2 1050 968.090 0.0005 2.00 0.814 4.0 152 259 250 59 57 50 2 1055 972.125 0.0005 2.00 0.814 4.0 154 261 250 61 58 51 I 1100 976.250 0.0005 2.00 0.814 4.0 156 265 250 64 56 50 I 1105 980.395 0.0005 2.00 0.814 4.0 156 258 248 65 56 51 2-6 1115 984.580 0.0005 2.00 0.814 4.0 151 261 250 67 51 49

6 1120 988.700 0.0005 2.00 0.814 4.0 153 260 251 63 53 49 5 1125 992.830 0.0005 2.00 0.814 4.0 154 261 250 62 52 49 5 1130 996.965 0.0005 2.00 0.814 4.0 156 260 249 63 

### 53 49 4 1135 1,001.105 0.0005 2.00 0.814 4.0 151 261 251 56 51 49 4 1140 1,005.325 0.0005 2.00 0.814 4.0 150 260 251 55 52 49 3 1145 1,009.500 0.0005 2.00 0.814 4.0 150 258 249 55 53 49

## Example Calculations Run Number 2 Pb 29.15 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 27.2 Water weight gain Ds 0 in. Stack Diameter Pm 2 "H20 Meter pressure As 950,400.0 Sq in. Stack Area Avg!::. P 0.001 "H20 Differential pressure Dn 1.5 in Nozzle Diameter Avg Sqrt!::. P 0.022 "H20 Sqrt Diff. press. Tt 

### 240 mm Sample Time %C02 0.40 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.40 Oxygen

Vm 198.518 acf Ps 0.10 "H20 Tm 56.5 (F) Ts 153.2 (F)

Vmstd

## = 17.65 * Vm * [ Pb 

### + :] Tm(R) 204.513 (acf* Y) 29.16 "Hg 516.5 (R) 

### 613.2 (R)



### = 17.65 * 204.513 %N2 79.20 Dry Gas Volume Stack Pressure Meter Temperature Stack Temperature

* [ 29.15 

### +

# ~~~~ ]= 516.5 Nitrogen

204.748 sft j



### 3.412 scfm

Vwgas = 0.0471 * Vw = 0.0471 * 27.2 1.2811 sft 3



### Bws= Vwgas Vmstd 

### +Vwgas

Vs = 5129.4 *

5129.4 * Ts (R) 

### \Ps 

## *Mw

0.84 Bws* 100 = 0.62 % Moist. Md = 28.880 ===== 

### 1-Bws = 0.9938 MW = 28.813

* sqrt !::. 

### P 613.2 29.16 * 28.813 * 0.022 81.0 fpm 1.4 ==== =====


### ACFM= Vs *As 144 81.0 * 950400.0 144 534,600 ACFM fps

DSCFM = ACFM * 528 * Ps 

# *(1-Bws) Ts (R) * 29.92 534,600 * 528 * 29.16 * 0.9938 613.2 * 29.92 445,847 DSCFM

% 

### Iso. 

## = 1039 * Vmstd * Ts (R) 

### (1-Bws) *Ps * Tt * Vs * (DnY'2 1,039 * 204.748 * 613.2 0.9938 * 29.16 * 240 * 81.0 * 2.25000 102.9 %

# TEST, Inc. 

# I Comments: 

## Particulate/Metals Sampling Data Project# TI1550 MeterBox# 2010 %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0203 %02 20.50 1 714.2 640.5 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 718.1 675.2

Operator csm Nozzle# %N2 79.10 3 595 698.1 Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist % 2.00 4 881.1 917.5

Date 3/20/13 Stack Dia.(in.) Final Moist. % 0.50 5 Sample Time 240 Static Press.("H20) 0.10 Final Isokinetic% 106.7 6 Min/pt 5 Bar. Press. ("Hg) 29.05 Initial Leak Rate 

### 0 cfm@ 15 "Hg Filter# 1005 Leak CheckVol. Final Leak Rate 0.001 cfm@ 15 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1440 489.889 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out

5-8 1445 494.400 0.0005 2.30 0.868 5.0 149 266 237 46 81 86

8 1450 499.150 0.0005 2.30 0.868 5.0 150 256 239 42 

### 80 86 7 1455 503.705 0.0005 2.30 0.868 5.0 155 246 258 42 80 86 7 1500 508.500 0.0005 2.30 0.868 5.0 152 250 261 41 81 86 6 1505 513.125 0.0005 2.30 0.868 5.0 148 256 258 42 78 86 6 1510 517.720 0.0005 2.30 0.868 5.0 147 252 251 42 76 84 5 1515 522.215 0.0005 2.30 0.868 5.0 150 249 250 

### 44 81 86 5 1520 526.900 0.0005 2.30 0.868 5.0 151 249 251 43 81 85 4 1525 531.500 0.0005 2.30 0.868 5.0 154 248 250 44 78 86 4 1530 536.100 0.0005 2.30 0.868 5.0 157 250 249 46 80 86 3 1535 540.650 0.0005 2.30 0.868 5.0 155 249 250 45 80 85 3 1540 545.120 0.0005 2.30 0.868 5.0 155 251 252 46 74 83 2 1545 549.805 0.0005 2.30 0.868 5.0 153 249 248 48 81 86 2 1550 554.350 0.0005 2.30 0.868 5.0 150 250 250 51 83 87 1 1555 558.900 0.0005 2.30 0.868 5.0 150 250 249 51 85 88 I 1600 563.573 0.0005 2.30 0.868 5.0 148 251 250 52 85 88 6-8 1610 567.865 0.0005 2.30 0.868 5.0 140 249 248 63 84 87

8 1615 572.450 0.0005 2.30 0.868 5.0 140 249 249 60 82 87 7 1620 577.000 0.0005 2.30 0.868 5.0 141 251 250 61 81 87 7 1625 581.500 0.0005 2.30 0.868 5.0 139 249 250 65 81 87 6 1630 586.285 0.0005 2.30 0.868 5.0 140 251 253 56 72 84 6 1635 590.750 0.0005 2.30 0.868 5.0 139 250 252 55 70 83 5 1640 595.395 0.0005 2.30 0.868 5.0 140 251 250 54 77 84 5 1645 600.010 0.0005 2.30 0.868 5.0 141 250 248 55 75 83 4 1650 604.400 0.0005 2.30 0.868 5.0 139 250 252 54 79 84 4 1655 609.075 0.0005 2.30 0.868 5.0 142 251 249 55 80 85 3 1700 613.670 0.0005 2.30 0.868 5.0 141 251 250 50 79 84 3 1705 618.000 0.0005 2.30 0.868 5.0 141 251 251 55 80 86 2 1710 622.850 0.0005 2.30 0.868 5.0 142 250 252 55 80 86 2 1715 627.400 0.0005 2.30 0.868 5.0 140 251 249 59 79 85 I 1720 632.035 0.0005 2.30 0.868 5.0 140 250 251 62 79 86

## Example Calculations Run Number 3 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Vw 22.9 Water weight gain Ds 0 Pm 2.3 "H20 Meter pressure As 950,400.0 Avg 1'1 

### P 0.001 "H20 Differential pressure Dn 1.5 AvgSqrti'1 P 0.022 "H20 Sqrt Diff. press. Tt 

### 240 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.50 Oxygen

Vm 220.318 acf Ps 0.10 "H20 Tm 81.8 (F) Ts 142.5 (F)

Vmstd = 17.65 *Vm * [ Pb+

# 1~] Tm(R) %N2 79.10 224.79 (acf* Y) Dry Gas Volume 29.06 "Hg Stack Pressure 541.8 (R) 

### Meter Temperature 602.5 (R) 

### Stack Temperature



### = 17.65 * 224.790 * [ 29.05 +

# ~:~ ]= 541.8

Vwgas = 0.0471 * Vw = 0.0471 * 22.9 1.0786 sft 3 

### Pitot Cal m. Stack Diameter Sq in. Stack Area m Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

213.968 sft 5



### 3.566 scfm

Bws= Vwgas Bws*100 

### = 0.50 %Moist. Md = 28.884 Vmstd + Vwgas

Ts (R) 

### Vs= 5129.4*Cp* \Ps*Mw

5129.4 * 0.84 1-Bws 

### = 0.9950

* sqrt 1'1 

### P 602.5 29.06 * 28.830 * 0.022

ACFM= Vs *As 144 80.4 * 950400.0 144 530,640 ACFM ===== 

### MW = 28.830 =====



### fpm ==== 

### 80.4 ===1=.3==fps

DSCFM 

### = ACFM * 528 * Ps 

# * (1-Bws) Ts (R) * 29.92 530,640 * 528 * 29.06 * 0.9950 449,401 DSCFM

% 

### Iso. 

### = 1039 *Vmstd * Ts (R) 

### (1-Bws) * Ps * Tt 

### * Vs * (Dn)'"'2 1,039 * 213.968 602.5 * 29.92



## * 602.5 0.9950 * 29.06 * 240 * 80.4 * 2.25000 106.7 %

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC Baghouse #2 UNIT: 

## PROJECT#: TI1550

Run Number Date Time 0 = Sample time Pb = Barometric Pressure at Port Elevation Vm =Vol. ofMetered Gas- meter cond., cal corr. Tm =MeterTemperature Tm =MeterTemperature Po = Meter Orifice Pressure Pma = Meter Pressure Absolute Vtwet =Sampled Gas Volume Wet Vtstd = Sampled Gas Volume at Stand. Cond., dry Vtstd = Sampled Gas Volume at Stand. Cond., dry 

### C02 =% C02, dry 02 =% 02, dry
co =%co, dry N2 =%N2,dry (N2+CO) = 1 OO-(C02+02) EA =Excess Air Vw = Volume Water H20 =in gas H20 = Moisture in Gas at Saturation Md =DryMolecular Weight ofStack Gas Mw =WetMolecular Weight ofStack Gas Psg = Stack Pressure, gauge - measured Psa =StackPressure, absolute 1 3/19113 855

- 1105 120 29.05 102.044

51.2 511.2 2.00 29.20 125.766 102.868 2.913 0.40 20.40 0.00 79.20 3,469.4

19.6 0.89 34.20 28.88 28.78 0.10 29.06 2 3 3/19/13 3/19/13 1220- 1435 1555

- 1810 120 120 29.05 29.05 99.957 110.187

50.1 82.0 510.1 542.0 2.00 2.30 29.20 29.22 120.540 128.773 100.981 104.844

2.859 2.969 0.40 0.50 20.50 20.40 0.00 0.00 79.10 79.10 4,442.0 3,633.1

16.4 17.7 0.76 0.79 24.37 37.15 28.88 28.90 28.80 28.81 0.10 0.10 29.06 29.06 minutes in. Hg
cu. ft. Farenheit Rankine in. H20 in. Hg
cu. ft. cu.ft
cu. Meter % % % % % grams % %

in. H20 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC Baghouse #2 UNIT: PROJECT#: TI1550

Run Number Ts =StackTemperature Ts =StackTemperature Ts =StackTemperature

### 'I~ P = Avg. Sum. ofPressure Square Root Vs = Velocity in the Stack Vs = Velocity inthe Stack As =Effective Stack Area Qa =Volumetric Flow Rate at stack cond. Qs = Volumetric Flow Rate, stand. cond., dry IR = Isokinetic Ratio (VnNs)*lOO 1 161.50 344.94 621.5 0.022 81.7 1.36 950,400.0

539,220 440,971

104.6 2 3 147.60 165.00 337.22 346.89 607.6 625 0.022 0.022 80.8 81.9 1.30 1.40 950,400.0 950,400.0

533,280 540,540 446,676 440,019

101.3 106.8 Farenheit Kelvin Rankine

ft/min ft/sec sq.m. acfm dscfm %

# TEST, Inc.**~Comments:** Dioxin/Furans/PCB's Sampling Data**~----------------------------------------~** 

### Project# TI1550 Meter Box# 2010 mst %C02 0.40 Imp. Initial Final



### ------ Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.40 1 344.5 353.7 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 713.5 700



## ------ ------ Operator csm Nozzle# %N2 79.20 3 593.3 595 Run# 1 Nozzle Dia. (in.) 1.5 Assumed Moist% 2.00 4 869.6 891.8



### ------ 

## ------ Date 3/19/13 Stack Dia.(in.) Final Moist.% 0.89 5



## ------ Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 104.6 6



### -------------- 

## ------ Min/pt 5 Bar. Press. ("Hg) 29.05 

### Initial Leak Rate 0.005 cfm@ 11 "Hg



### --- Filter#

---- Leak Check Vol. Final Leak Rate 0.001 cfm@ 11 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 855 531.635 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out 7-8 900 535.805 0.0005 2.00 0.814 5.0 151 262 232 51 52 50

7 905 540.005 0.0005 2.00 0.814 5.0 157 260 249 47 

### 54 51 6 910 544.015 0.0005 2.00 0.814 5.0 159 263 249 45 54 52 5 915 548.175 0.0005 2.00 0.814 5.0 160 262 252 47 59 52 4 920 552.320 0.0005 2.00 0.814 5.0 166 259 250 52 60 52 3 925 556.470 0.0005 2.00 0.814 5.0 166 264 251 53 55 52 2 930 560.545 0.0005 2.00 0.814 5.0 164 261 251 55 55 52 1 935 564.700 0.0005 2.00 0.814 5.0 161 260 251 52 52 50 6-8 945 568.830 0.0005 2.00 0.814 5.0 160 253 250 60 52 49

7 950 572.980 0.0005 2.00 0.814 5.0 163 260 251 57 53 50 6 955 577.055 0.0005 2.00 0.814 5.0 163 258 249 52 52 50 5 1000 581.190 0.0005 2.00 0.814 5.0 164 259 251 50 51 49 4 1005 585.265 0.0005 2.00 0.814 5.0 169 258 251 51 50 48 3 1010 589.400 0.0005 2.00 0.814 5.0 170 256 250 52 50 48 2 1015 593.540 0.0005 2.00 0.814 5.0 161 257 250 56 51 49 1 1020 597.695 0.0005 2.00 0.814 5.0 159 258 249 58 51 49 5-8 1030 601.835 0.0005 2.00 0.814 5.0 161 266 249 58 50 48

7 1035 605.800 0.0005 2.00 0.814 5.0 163 257 251 58 52 50 6 1040 609.925 0.0005 2.00 0.814 5.0 165 257 250 56 51 48 5 1045 614.050 0.0005 2.00 0.814 5.0 164 262 251 56 52 47 4 1050 618.195 0.0005 2.00 0.814 5.0 163 259 250 57 52 49 3 1055 622.350 0.0005 2.00 0.814 5.0 159 258 249 56 52 50 2 ] 100 626.575 0.0005 2.00 0.814 5.0 158 257 250 56 52 50 1 

### 1105 630.688 0.0005 2.00 0.814 5.0 151 260 251 57 52 49

## Example Calculations Run Number Pb 29.05 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 19.6 Water weight gain Ds 0 m. Stack Diameter Pm 2 "H20 Meter pressure As 950,400.0 Sq in. Stack Area Avg**~** P 0.001 "H20 Differential pressure Dn 1.5 in Nozzle Diameter Avg Sqrt**~** P 0.022 "H20 Sqrt Diff. press. Tt 120 mm Sample Time %C02 0.40 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.40 Oxygen %N2 79.20 Nitrogen

Vm 99.053 acf 102.044 (acf* Y) Dry Gas Volume Ps 0.10 "H20 29.06 "Hg Stack Pressure Tm 51.2 (F) 511.2 (R) Meter Temperature Ts 161.5 (F) 621.5 (R) Stack Temperature

Vmstd = 17.65 * Vm *

# ~ Pb 

### +

# 1~] LTm (R)

# ~ 17.65 ' 102.044 ' [ 2.00 29.05 

### + 13.6 511.2 ] = 102.868 sft j 1.714 scfm

Vwgas = 0.0471 * Vw = 0.0471 * 19.6 0.9232 sft 3

Bws= Vwgas Bws*100 = 0.89 %Moist. Vmstd 

### + Vwgas

Ts (R) Vs= 5129.4 * Cp * \ Ps * Mw

5129.4 * 0.84 1-Bws = 0.9911



## * sqrt**~** P 621.5 29.06 * 28.783 * 0.022

ACFM= Vs *As 144 81.7 * 950400.0 144 539,220 ACFM Md = 28.880 ===== MW = 28.783 =====

81.7 fpm 1.36 tips 

## ==== =====

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 539,220 * 528 * 29.06 * 0.9911 440,971 DSCFM

0 /o Iso. 

### = 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt * Vs * (DnY'2 1,039 * 102.868 0.9911 * 29.06 * 120 621.5 * 29.92



## * 621.5 104.6 % 

## * 81.7 * 2.25000

# TEST, Inc. IComments: 

## Dioxin!Furans/PCB's Sampling Data Project # TI1550 Meter Box# 2010 mst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.50 1 335.1 374.9 Unit/Stack Baghouse #5 Pitot Cal. (Cp) 0.84 %CO 2 725.6 681.2

Operator csm Nozzle# %N2 79.10 3 609.6 612.8 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % 0.94 4 899 916.8

Date 3119/13 Stack Dia.(in.) Final Moist.% 0.76 5 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 101.3 6 

### Min/pt 5 Bar. Press. ("Hg) 29.05 

### Initial Leak Rate 0.001 cfm@ 12 "Hg Filter#

---- Leak CheckVol. Final Leak Rate 0.001 cfm@ 12 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter(CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 1220 632.460 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out 4-6 1225 636.365 0.0005 2.00 0.814 5.0 139 263 233 67 49 48

5 1230 640.300 0.0005 2.00 0.814 5.0 143 269 232 49 

### 52 48 4 1235 644.410 0.0005 2.00 0.814 5.0 149 258 239 49 52 49 3 1240 648.530 0.0005 2.00 0.814 5.0 150 256 243 49 52 50 2 1245 652.645 0.0005 2.00 0.814 5.0 151 264 249 45 52 49 1 1250 656.830 0.0005 2.00 0.814 5.0 149 259 251 43 52 50 3-6 1300 661.005 0.0005 2.00 0.814 5.0 145 263 249 47 52 49

5 1305 665.160 0.0005 2.00 0.814 5.0 147 260 251 45 52 50 4 1310 669.305 0.0005 2.00 0.814 5.0 144 258 250 48 52 50 3 1315 673.510 0.0005 2.00 0.814 5.0 143 256 249 47 51 49 2 1320 677.700 0.0005 2.00 0.814 5.0 150 259 251 49 51 49 1 1325 681.845 0.0005 2.00 0.814 5.0 151 261 249 50 51 49 2-6 1335 685.000 0.0005 2.00 0.814 5.0 153 259 253 47 50 49

5 1340 689.135 0.0005 2.00 0.814 5.0 150 258 250 49 50 48 4 1345 693.290 0.0005 2.00 0.814 5.0 150 259 250 50 51 48 3 1350 697.415 0.0005 2.00 0.814 5.0 149 255 249 52 51 49 2 1355 701.590 0.0005 2.00 0.814 5.0 140 260 250 52 51 49 1 1400 709.710 0.0005 2.00 0.814 5.0 146 257 250 52 50 49 1-6 1410 708.850 0.0005 2.00 0.814 6.0 153 261 249 64 51 49 5 1415 712.970 0.0005 2.00 0.814 6.0 151 260 252 54 51 48 4 1420 717.200 0.0005 2.00 0.814 6.0 151 259 249 52 51 48 3 1425 721.305 0.0005 2.00 0.814 6.0 148 259 250 54 51 49 2 1430 725.400 0.0005 2.00 0.814 6.0 144 261 251 56 52 50 1 1435 729.487 0.0005 2.00 0.814 6.0 147 259 249 56 52 50

## Example Calculations Run Number 2 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 16.4 Water weight gain Ds 0 in. Stack Diameter Pm 2 "H20 Meter pressure As 950,400.0 Sq in. Stack Area Avg**~** 

### P 0.001 "H20 Differential pressure Dn 1.5 m 

### Nozzle Diameter Avg Sqrt**~** 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 120 min Sample Time %C02 0.40 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.50 Oxygen

Vm 97.027 acf Ps 0.10 "H20 Tm 50.1 (F) Ts 147.6 (F)

Vmstd 

## = 17.65 *Vm * [ Pb+

# 1~] Tm(R) %N2 79.10 Nitrogen 99.957 (acf* Y) Dry Gas Volume 29.06 "Hg Stack Pressure 510.1 (R) Meter Temperature 607.6 (R) Stack Temperature

# ~ 17.65 • 99.957 • [ 

### 2.00 29.05 + 13.6 510.1 

### ] = 100.981 sft _j 

### 1.683 scfm

Vwgas 

## = 0.0471 * Vw 

## = 0.0471 * 16.4 0.7724 sft 3



### Bws= Vwgas Vmstd + Vwgas

Vs 

### = 5129.4 *

5129.4 * Ts (R) 

### \Ps 

## *Mw

0.84 Bws*100 

### = 0.76 %Moist. Md 

### = 28.884 ==== ===== 1-Bws 

### = 0.9924 MW = 

### 28.801

* sqrt**~** 

### P 607.6 29.06 * 28.801 * 0.022 1.3 ==8=0.=8=fpm ======


### ACFM= Vs *As 144 80.8 * 950400.0 144 533,280 ACFM fps

DSCFM = ACFM * 528 * Ps * (1-Bws) Ts (R) * 29.92 533,280 * 528 * 29.06 * 0.9924 607.6 * 29.92 446,676 DSCFM

% 

### lso. 

## = 1039 * Vmstd * Ts (R) (1-Bws) *Ps * Tt * Vs * (Dn)"2 1,039 * 100.981 * 607.6 0.9924 * 29.06 * 120 * 80.8 * 2.25000 101.3 %

# TEST, Inc. !Comments: 

## Dioxin/Furans/PCB's Sampling Data**~--------------------------------------~** 

### Project# TI1550 Meter Box# 2010 %C02 0.50 Imp. Initial Final



# --- Plant Felman Productions LLC Meter Cal. (Y) 1.0203 %02 20.40 1 340.9 339.8 Unit/Stack Baghouse #2 Pitot Cal. (Cp)_0_.8_4___ %CO

__ _ 2 679.2 680.5 Operator br Nozzle# %N2 79.10 3 609.6 609.6



## ----- Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist% 2.00 4 891.8 909.3



# ----- --- Date 3/19/13 Stack Dia.(in.) Final Moist.% 0.79 5



# --- Sample Time 120 Static Press.("H20)_0_.1_0

___ Final Isokinetic % 106.8 6 Min/pt 

### 5 Bar. Press. ("Hg) 29.05 Initial Leak Rate 

### 0.001 cfm@ 10 "Hg Filter# Leak Check Vol. Final Leak Rate 0.001 cfm@ 10 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 1555 115.208 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In Out 11-6 1600 119.607 0.0005 2.30 0.864 6.0 153 248 259 56 88 86

5 1605 124.106 0.0005 2.30 0.864 6.0 151 247 252 52 

### 84 82 4 1610 128.703 0.0005 2.30 0.864 6.0 139 248 249 52 82 81 3 1615 132.306 0.0005 2.30 0.864 6.0 153 249 252 56 81 80 2 1620 137.806 0.0005 2.30 0.864 6.0 164 251 252 60 83 81 1 1625 142.209 0.0005 2.30 0.864 6.0 154 251 250 59 83 80 10-6 1635 146.707 0.0005 2.30 0.864 6.0 157 249 250 

### 61 86 84

5 1640 151.307 0.0005 2.30 0.864 6.0 160 249 249 60 85 83 4 1645 155.804 0.0005 2.30 0.864 6.0 157 251 250 61 84 82 3 1650 160.305 0.0005 2.30 0.864 6.0 156 250 251 61 84 82 2 1655 164.808 0.0005 2.30 0.864 6.0 156 248 250 60 81 79 1 1700 169.305 0.0005 2.30 0.864 6.0 166 251 251 63 83 82 9-6 1710 173.803 0.0005 2.30 0.864 6.0 176 254 251 60 84 82

5 1715 178.304 0.0005 2.30 0.864 6.0 175 249 250 57 83 81 4 1720 182.805 0.0005 2.30 0.864 6.0 174 250 250 56 84 82 3 1725 187.308 0.0005 2.30 0.864 6.0 171 250 249 55 80 81 2 1730 191.806 0.0005 2.30 0.864 6.0 170 251 250 53 81 80 1 1735 196.308 0.0005 2.30 0.864 6.0 169 250 251 52 80 79 8-6 1745 200.708 0.0005 2.30 0.864 6.0 172 249 251 53 84 82

5 1750 205.208 0.0005 2.30 0.864 6.0 178 251 250 53 83 81 4 1755 209.707 0.0005 2.30 0.864 6.0 177 251 251 55 83 80 3 1800 214.205 0.0005 2.30 0.864 6.0 174 249 250 56 80 78 2 1805 218.705 0.0005 2.30 0.864 6.0 179 250 250 61 80 78 1 1810 223.203 0.0005 2.30 0.864 6.0 178 250 250 65 83 82

## Example Calculations Run Number 3 Pb 29.05 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 17.7 Water weight gain Ds 0 in. Stack Diameter Pm 2.3 "H20 Meter pressure As 950,400.0 Sq in. Stack Area Avg !}. 

### P 0.001 "H20 Differential pressure Dn 1.5 m 

### Nozzle Diameter Avg Sqrt !}. 

### P 0.022 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.50 Carbon Dioxide %02 20.40 Oxygen

Vm 107.995 acf Ps 0.10 "H20 Tm 82.0 (F) Ts 165.0 (F)

Vmstd = 17.65 *Vm * [ Pb 

### +

# 1~] Tm(R) 110.187 29.06

542 625

::::: 17.65

Vwgas = 0.0471 *Vw = 0.0471 * 17.7 %CO 0.00 %N2 79.10 (acf* Y) Dry Gas Volume "Hg Stack Pressure (R) 

### Meter Temperature (R) 

### Stack Temperature


## * llO.l87 •[ 2.30 29.05 

### + 13.6 542.0

0.8337 sft 3 

### min Sample Time Carbon Monoxide Nitrogen

] = 104.844 sft j 

### 1.747 scfm

Bws= Vwgas Bws*100 = 0.79 %Moist. Md = 28.896 Vmstd 

### +Vwgas

Ts (R) 

### Vs=5129.4*Cp* \Ps*Mw

5129.4 * 0.84 1-Bws = 0.9921

* sqrt !}. 

### P 625 29.06 * 28.810 * ===== 

### MW = 28.810

0.022 ===8=1.=9=fpm ===== 

### 1.4

ACFM= Vs *As 144 81.9 * 950400.0 144 540,540 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) 

### * 29.92 540,540 * 528 * 29.06 * 0.9921 440,019 DSCFM

% 

### lso.= 1039 * Vmstd * Ts (R) 

### (1-Bws) * Ps * Tt 

### * Vs * (Dn)"2 1,039 * 104.844 625 * 29.92



## * 625 0.9921 * 29.06 * 120 * 81.9 * 2.25000 106.8 %

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC Baghouse #2 UNIT: PROJECT#: TI1550

Run Number Date Time 0 = Sample time Pb = Barometric Pressure at Port Elevation Vm =Vol. ofMetered Gas- meter cond., cal corr. Tm =MeterTemperature Tm =MeterTemperature Po = Meter Orifice Pressure Pma = Meter Pressure Absolute Vtwet =Sampled Gas Volume Wet Vtstd = Sampled Gas Volume at Stand. Cond., dry Vtstd = Sampled Gas Volume at Stand. Cond., dry 

### C02 =%C02,dry 02 =%02,dry 

# co =%CO,dry N2 = %N2,dry (N2+CO) = 1 OO-(C02+02) EA =ExcessAir Vw =Volume Water H20 =ingas H20 = Moisture in Gas at Saturation Md =DryMolecular Weight ofStack Gas Mw =WetMolecular Weight ofStack Gas Psg = Stack Pressure, gauge - measured Psa = Stack Pressure, absolute 1 3/18/13 955

- 1225 120 28.95 86.540

64.9 524.9

1.60 29.07 105.163 84.585 2.395 0.40 20.40 0.00 79.20 3,469.4

24.9 1.37 38.88 28.88 28.73 0.10 28.96 2 3 3/18/13 3/18/13 1255

- 1505 1545

- 1800 120 120 28.90 28.75 86.540 91.444

64.9 78.4 524.9 538.4

1.60 1.70 29.02 28.88 105.711 110.383 84.440 86.560 2.391 2.451 0.40 0.40 20.40 20.50 0.00 0.00 79.20 79.10 3,469.4 4,442.0

34.3 21.3 1.88 1.15 38.94 52.74 28.88 28.88 28.68 28.76 0.10 0.10 28.91 28.76 minutes in. Hg
cu. ft. Farenheit Rankine in. H20 in. Hg
cu. ft. cu.ft
cu. Meter % % % % % grams % %

in. H20 in. Hg

# CALCULATION SUMMARY SHEET
PLANT: Felman Productions LLC UNIT: Baghouse #2 PROJECT#: TI1550

Run Number 1 2 3 Ts = Stack Temperature 166.80 166.80 179.90 Farenheit Ts = Stack Temperature 347.89 347.89 355.17 Kelvin Ts =Stack Temperature 626.8 626.8 639.9 Rankine 

# \I L1 

### P = Avg. Sum. ofPressure Square Root 0.02 0.02 0.02

Vs = Velocity in the Stack 74.8 74.9 75.8 ft/min Vs = Velocity in the Stack 1.25 1.20 1.30 ft/sec As = Effective Stack Area 950,400.0 950,400.0 950,400.0 sq. m. Qa = Volumetric Flow Rate at stack cond. 493,680 494,340 500,280 acfm Qs = Volumetric Flow Rate, stand. cond., dry 397,005 394,798 392,228 dscfm IR = Isokinetic Ratio (Vn/Vs)* 100 95.5 95.9 98.9 

### %

# TEST, Inc.**~Comments:** Trap #5 pah PAH Sampling Data Project# TI1550 Meter Box# 20IOmst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC Meter Cal. (Y) 1.0302 %02 20.40 I 333.3 338.6 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 725.1 723.1

Operator br Nozzle# %N2 79.20 3 746.9 748 Run# I Nozzle Dia. (in.) 1.5 Assumed Moist % 1.22 4 606.5 609.1

Date 3/18/13 Stack Dia.(in.) Final Moist.% 1.37 5 922.5 940.4 Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 95.5 6 

### Minlpt 5 Bar. Press. ("Hg) 28.95 

### Initial Leak Rate 0 cfm@ 12 "Hg Filter#

---- Leak Check Vol. Fina! Leak Rate 0.002 cfm@ 12 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 955 208.905 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out 4-6 1000 212.260 0.0004 1.60 0.746 6.0 171 253 229 55 60 58

5 1005 215.530 0.0004 1.60 0.746 6.0 166 260 242 54 61 60 4 1010 219.102 0.0004 1.60 0.746 6.0 166 259 248 54 61 59 3 1015 222.003 0.0004 1.60 0.746 6.0 169 260 251 54 61 59 2 1020 226.202 0.0004 1.60 0.746 6.0 146 261 251 57 61 60 1 1025 230.108 0.0004 1.60 0.746 6.0 160 265 252 58 62 61 3-6 1035 233.418 0.0004 1.60 0.747 6.0 184 257 250 60 63 61

5 1040 237.014 0.0004 1.60 0.747 6.0 155 256 250 58 64 62 4 1045 241.908 0.0004 1.60 0.747 6.0 156 260 250 60 66 64 3 1050 246.701 0.0004 1.60 0.747 6.0 149 262 250 62 69 67 2 1055 249.309 0.0004 1.60 0.747 6.0 153 260 252 64 68 67 1 1100 253.501 0.0004 1.60 0.747 6.0 159 265 250 65 69 68 2-6 1110 256.403 0.0004 1.60 0.747 6.0 184 254 249 66 70 69

5 1115 260.103 0.0004 1.60 0.747 6.0 184 255 250 66 69 67 4 1120 263.410 0.0004 1.60 0.747 6.0 183 257 249 68 66 65 3 1125 266.570 0.0004 1.60 0.747 6.0 178 267 250 67 64 62 2 1130 269.601 0.0004 1.60 0.748 6.0 172 252 242 60 64 62 1 1135 272.701 0.0004 1.60 0.748 6.0 176 260 250 57 65 63 1-6 1200 276.608 0.0004 1.60 0.748 6.0 180 255 250 57 64 63 5 1205 280.002 0.0004 1.60 0.748 6.0 153 255 250 55 72 70 4 1210 283.807 0.0004 1.60 0.748 6.0 154 258 249 55 70 68 3 1215 286.801 0.0004 1.60 0.748 6.0 168 265 250 57 70 69 2 1220 289.704 0.0004 1.60 0.748 6.0 168 263 251 54 68 66 1 1225 292.908 0.0004 1.60 0.748 6.0 169 264 249 54 69 68

## Example Calculations Run Number Pb 28.95 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 24.9 Water weight gain Ds 0 m. Stack Diameter Pm 1.6 "H20 Meter pressure As 950,400.0 Sq in. Stack Area Avg .!1 P 0.000 "H20 Differential pressure Dn 1.5 m Nozzle Diameter Avg Sqrt .!1 P 0.020 "H20 Sqrt Diff. press. %C02 0.40 Carbon Dioxide %02 20.40 Oxygen

Vm 84.003 acf Ps 0.10 "H20 Tm 64.9 (F) Ts 166.8 (F)

Vmstd=

# 17.65*Vm*[Pb+1~] Tm(R) 86.54 (acf* Y) 28.96 "Hg 524.9 (R) 626.8 (R)

= 17.65 * 86.540 Tt 120 %CO 0.00 %N2 79.20 Dry Gas Volume Stack Pressure Meter Temperature Stack Temperature

[ 1.60 * 28.95 + 13.6 524.9 

# }

Vwgas = 0.0471 * Vw = 0.0471 * 24.9 1.1728 sft 3 mm Sample Time Carbon Monoxide Nitrogen

84.585 sft j

1.410 scfm

Bws= Vwgas Bws*100 = 1.37 %Moist. Md = 28.880 Vmstd + Vwgas

Ts (R) Vs = 5129.4 * Cp * \ Ps * Mw

5129.4 * 0.84 1-Bws = 0.9863

* sqrt .!1 P 626.8 28.96 * 28.731 * 0.020

ACFM= Vs *As 144 74.8 * 950400.0 144 493,680 ACFM ===== MW = 28.731 =====

74.8 fpm 1.25 ==== =====fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 493,680 * 528 * 28.96 * 0.9863 626.8 * 29.92 397,005 DSCFM

% 

### Iso. 

## = 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt * Vs * (Dn)"'2 1,039 * 84.585 0.9863 * 28.96 * 120 

## * 626.8 95.5 % * 74.8 * 2.25000

# TEST, Inc. 

# I Comments: 

## Trap #8 PAH Sampling Data Project# TII550 Meter Box# 20I0 mst %C02 0.40 Imp. Initial Final Plant Felman Productions LLC MeterCal. (Y) I.0302 %02 20.40 I 339.8 350.5 Unit/Stack Baghouse #2 Pitot Cal. (Cp) 0.84 %CO 2 703.4 70I.8

Operator br Nozzle# %N2 79.20 3 707.7 708.7 Run# 2 Nozzle Dia. (in.) 1.5 Assumed Moist % I.80 4 602.3 606.9

Date 3/18/13 Stack Dia.(in.) Final Moist. % I.88 5 9I6.5 936.I Sample Time I20 Static Press.("H20) O.I0 Final Isokinetic% 95.9 6 

### Min/pt 5 Bar. Press. ("Hg) 28.90 

### Initial Leak Rate 0.001 cfm@ II "Hg Filter#

---- Leak Check Vol. Final Leak Rate O.OOI cfm@ II "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 1255 208.905 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In 

### Out

-8 1300 212.260 0.0004 1.60 0.746 6.0 17I 253 229 55 60 58 7 1305 2I5.530 0.0004 1.60 0.746 6.0 I66 260 242 54 

### 61 60 6 1310 2I9.102 0.0004 1.60 0.746 6.0 I66 259 248 54 6I 59 5 13I5 222.003 0.0004 1.60 0.746 6.0 I69 260 25I 54 61 59 4 1320 226.202 0.0004 1.60 0.746 6.0 I46 26I 25I 57 61 60 3 1325 230.I08 0.0004 1.60 0.746 6.0 I60 265 252 58 62 61 2 1330 233.4I8 0.0004 1.60 0.747 6.0 I84 257 250 60 63 61 1 1335 237.014 0.0004 1.60 0.747 6.0 I55 256 250 58 64 62 6-8 1345 241.908 0.0004 1.60 0.747 6.0 I56 260 250 60 66 64

7 1350 246.70I 0.0004 1.60 0.747 6.0 149 262 250 62 69 67 6 1355 249.309 0.0004 1.60 0.747 6.0 I53 260 252 64 68 67 5 1400 253.50I 0.0004 1.60 0.747 6.0 159 265 250 65 69 68 4 1405 256.403 0.0004 1.60 0.747 6.0 I84 254 249 66 70 69 3 1410 260.I03 0.0004 1.60 0.747 6.0 I84 255 250 66 69 67 2 1415 263.4IO 0.0004 1.60 0.747 6.0 I83 257 249 68 66 65 I 1420 266.570 0.0004 1.60 0.747 6.0 I78 267 250 67 64 62 7-8 1430 269.60I 0.0004 1.60 0.748 6.0 I72 252 242 60 64 62

7 1435 272.70I 0.0004 1.60 0.748 6.0 I76 260 250 57 65 63 6 1440 276.608 0.0004 1.60 0.748 6.0 I80 255 250 57 64 63 5 I445 280.002 0.0004 1.60 0.748 6.0 I53 255 250 55 72 70 4 1450 283.807 0.0004 1.60 0.748 6.0 I54 258 249 55 70 68 3 1455 286.80I 0.0004 1.60 0.748 6.0 I68 265 250 57 70 69 2 1500 289.704 0.0004 1.60 0.748 6.0 I68 263 25I 54 68 66 1 1505 292.908 0.0004 1.60 0.748 6.0 169 264 249 54 69 68

## Example Calculations Run Number 2 Pb 28.90 "Hg Barometric Pressure Cp 0.84 Vw 34.3 Water weight gain Ds 0 Pm 1.6 "H20 Meter pressure As 950,400.0 Avg**~** 

### P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** 

### P 0.020 "H20 Sqrt Diff. press. Tt 

### 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.40 Oxygen %N2 79.20

Vm 84.003 acf 86.54 (acf* Y) Dry Gas Volume Ps 0.10 "H20 28.91 "Hg Stack Pressure Tm 64.9 (F) 524.9 (R) Meter Temperature Ts 166.8 (F) 626.8 (R) Stack Temperature

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm(R) = 17.65 * 86.540

# ·[ 1.60 28.90 

### + 13.6 524.9 

# }

Vwgas = 0.0471 * Vw = 0.0471 * 34.3 1.6155 sft 3 

### Pitot Cal 

### m. Stack Diameter Sq in. Stack Area 

### m Nozzle Diameter min Sample Time Carbon Monoxide Nitrogen

84.440 sft j



### 1.407 scfm

Bws= Vwgas Bws* 100 = 1.88 % Moist. Md = 28.880 Vmstd 

### +Vwgas

Vs = 5129.4 *

5129.4 * Ts (R) 

### \Ps 

## *Mw

0.84 1-Bws = 0.9812

* sqrt**~** 

### P 626.8 28.91 * 28.675 * ===== 

### MW = 28.675 =====



### 0.020 ===7=4.=9= fpm ===== 

### 1.2

ACFM= Vs *As 144 74.9 * 950400.0 144 494,340 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 494,340 * 528 * 28.91 * 0.9812 394,798 DSCFM

% 

### Iso.= 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt 

### * Vs * (DnY'2 1,039 * 84.44 626.8 * 29.92

* 626.8 0.9812 * 28.91 * 120 * 74.9 * 2.25000 95.9 %

# TEST, Inc. PAH Sampling Data Project# TI1550



## ------- Plant Felman Productions LLC Unit/Stack Baghouse #2 

# I Comment.:

Meter Box# 2010 MST Meter Cal. (Y) 1.0302 Pitot Cal. (Cp) 0.84



## --- %C02 0.40



## --- %02 20.50 %CO



## --- Operator csm Nozzle # %N2 79.10



## --- Run# 3 Nozzle Dia. (in.) 1.5 Assumed Moist% 2.00



## --- ---- Date 3/18/13 Stack Dia.(in.) Final Moist.% 1.15



## --- ---- Sample Time 120 Static Press.("H20) 0.10 Final Isokinetic% 98.9



## ------- --- --- Imp. 1 2 3 4 5 6 Min/pt 

### 5 Bar. Press. ("Hg) 28.75 Initial Leak Rate 

### 0.001 cfm@ Filter# Leak Check Vol. Final Leak Rate 0.001 cfm @ Dry Gas Pitot Orifice Vacuu Stack Probe Filter Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Point 1545 401.745 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F)

8-6 1550 405.409 0.0004 1.70 0.760 6.0 194 263 244

5 1555 409.106 0.0004 1.70 0.760 6.0 197 272 250 4 1600 412.809 0.0004 1.70 0.760 6.0 197 263 240 3 1605 416.760 0.0004 1.70 0.760 6.0 195 256 248 2 1610 420.409 0.0004 1.70 0.760 6.0 197 255 250 1 1615 423.995 0.0004 1.70 0.760 6.0 204 258 253 9-6 1625 427.603 0.0004 1.70 0.760 6.0 174 270 248

5 1630 431.201 0.0004 1.70 0.760 6.0 177 272 251 4 1635 434.902 0.0004 1.70 0.760 6.0 178 254 250 3 1640 438.608 0.0004 1.70 0.747 6.0 180 256 250 2 1645 442.406 0.0004 1.70 0.747 7.0 176 255 250 1 1650 446.001 0.0004 1.70 0.747 7.0 172 259 250 10-6 1700 449.809 0.0004 1.70 0.747 7.0 167 258 250

5 1705 453.302 0.0004 1.70 0.747 7.0 180 258 251 4 1710 457.106 0.0004 1.70 0.747 7.0 151 258 251 3 1715 460.804 0.0004 1.70 0.747 7.0 180 260 249 2 1720 464.409 0.0004 1.70 0.747 7.0 180 261 250 1 1725 468.209 0.0004 1.70 0.747 7.0 179 260 251 11-6 1735 471.908 0.0004 1.70 0.747 7.0 171 270 249

5 1740 475.650 0.0004 1.70 0.747 7.0 164 265 249 4 1745 479.303 0.0004 1.70 0.747 7.0 173 258 250 3 1750 483.005 0.0004 1.70 0.747 7.0 175 258 250 2 1755 486.707 0.0004 1.70 0.747 7.0 179 262 251 1 1800 490.508 0.0004 1.70 0.747 7.0 177 261 250 Initial Final 339.4 344.7 725.6 721.8 747.8 746.5 607.8 612.8 940.4 956.5

12 "Hg 14 "Hg Imp. 

### Dry Gas Temp. Temp.

(F) In Out 65 69 68 67 

### 70 70 67 72 70 66 76 74 65 78 77 63 79 78 

### 60 80 78 63 80 77 63 81 80 65 81 79 66 82 80 66 82 81 60 81 80 52 80 78 54 80 78 53 80 79 52 81 80 52 83 81 53 81 80 48 81 79 49 80 78 49 81 80 50 81 78 50 81 80

## Example Calculations Run Number 3 Pb 28.75 "Hg Barometric Pressure Cp 0.84 Vw 21.3 Water weight gain Ds 0 Pm 1.7 "H20 Meterpressure As 950,400.0 Avg**~** P 0.000 "H20 Differential pressure Dn 1.5 Avg Sqrt**~** P 0.020 "H20 Sqrt Diff. press. Tt 120 %C02 0.40 Carbon Dioxide %CO 0.00 %02 20.50 Oxygen

Vm 88.763 acf Ps 0.10 "H20 Tm 78.4 (F) Ts 179.9 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# l~J Tm(R) %N2 79.10 91.444 (acf* Y) Dry Gas Volume 28.76 "Hg Stack Pressure 538.4 (R) Meter Temperature 639.9 (R) Stack Temperature

# ~ 17.65 • 91.444 • [ 

### .L1Q 

# ]= 28.75 

### + 13.6

- 538.4

Vwgas = 0.0471 * Vw = 0.0471 * 21.3 1.0032 sft 3 Pitot Cal m. Stack Diameter Sq in. StackArea m Nozzle Diameter mm Sample Time Carbon Monoxide Nitrogen

86.560 sft j

1.443 scfm

Bws= Vwgas Bws*lOO = 1.15 %Moist. Md = 28.884 ===== Vmstd 

### + Vwgas 1-Bws = 0.9885 MW = 28.759

Ts(R) Vs= 5129.4 * Cp * \Ps * Mw * sqrt**~** P 639.9 5129.4 * 0.84 28.76 * 28.759 * 0.020 ===7=5.=8=fpm

ACFM= Vs *As 144 75.8 * 950400.0 144

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92

% Iso.= 1039 * Vmstd * Ts (R) (1-Bws) * Ps * Tt * Vs * (Dn)l'2 1,039 * 86.56 0.9885 * 28.76 * 120 500,280 ACFM

500,280 * 528 * 28.76 * 0.9885 639.9 * 29.92



## * 639.9 98.9 % 

## * 75.8 * 2.25000 ===1=.3==fps

392,228 DSCFM

# EXAMPLE CALCULATIONS HYDROGEN CHLORIDE

mgHCl 24.04 Hydrogen Chloride ppm = 

### x --- Vmstd (cu.m) 36.45

HCllbslhr = 

### mg HCl x __ l..::g._r- x DSCFM x 60 min llb X 

### Vmstd 64.8 mg 1hr 

### 7,000 gr

36.45 = 

### Molecular Weight ofHydrogen Chloride
24.04 

### =**L~ .?al**  

### G<.'S CoEslant 

### liters/g-mole
DSCFM* = 

### Stack FlowRate

Vmstd* = 

### Volume ofdry 

### gas sampled at standard conditions dry standard cubic feet
Vmstd* (cu.m) = 

### Volume ofdry gas sampled (cubic meters)

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C)

# EXAMPLE CALCULi\TIONS MERCURY

lbs/hr=--m-=g- x -- 1 

### -=g"-r- x DSCFM x Vmstd 64.8 mg

DSCFM* = Stack FlowRate 60min 

## lhr

Vmstd* = Volume ofdry gas sampled at standard conditions dry standard cubic feet

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C) llb 

### x--- 7,000 gr

# EXAMPLE CALCULATIONS 11ULTIPLE**~\1ETALS**



### mg 

### 1 gr lbs/hr = ----"'"- X _ _____,......__ X 

### DSCFM X 

### Vmstd 64.8 mg

DSCFM* = 

### Stack FlowRate 60min lhr

Vmstd* = 

### Volume ofdry gas sampled at standard conditions dry standard cubic feet

* 29.92 "Hg, 68 degrees F (760 mm Hg, 20 degrees C) 1 lb 

### x--- 7,000 gr

### APPENDIXB 

### PRE-FLOW DATA

# TEST, Inc.**~Comments:** Method SD Setup**~----------------------------------------~** 

### Project# Meter Box# 2010 MST %C02 0.01 Imp. Initial Final



## ----- Plant Meter Cal. (Y) 1.0283 %02 20.80 1 703.7 695 Unit/Stack Pitot Cal. (Cp)_0_.8_4

__ %CO



## ----- 2 711.3 723.5

Operator Nozzle# %N2 79.19 3 597.8 601.3



## ---- Run# BH2 Inlet Nozzle Dia. (in.) Assumed Moist% 1.15 4 896.3 908.3



## ----- ----- Date 3/12/13 Stack Dia.(in.) 144 Final Moist.% 1.15 5



## ----- Sample Time 30 Static Press.("H20) -0.40 Final Isokinetic % #REF! 6



## ------------ Min/pt 

### 5 Bar. Press. ("Hg) 28.95 Initial Leak Rate 

### 0.006 cfm @ 14 "Hg Filter# Leak Check Vol. Final Leak Rate 0.006 cfm@ 14 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. Temp. Point 163.555 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) In 

### Out 236.550 0.40 1.20 0.628 2.0 358 40 40 0.42 355 0.45 353 0.45 352 0.40 356 0.38 366 0.35 363 0.33 365 0.32 361 0.28 350 0.26 344 0.25 345 0.50 368 0.52 374 0.53 372 0.53 373 0.50 370 0.46 372 0.45 374 0.40 368 0.30 368 0.27 363 0.24 362 0.22 341

## Example Calculations Run Number BH2 Inlet Pb 28.95 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 19 Water weight gain Ds 144 in. Stack Diameter Pm 1.2 "H20 Meterpressure As 16,286.0 Sq in. Stack Area Avg /'). P 0.384 "H20 Differential pressure Dn 0 m Nozzle Diameter Avg Sqrt /'). P 0.614 "H20 Sqrt Diff. press. Tt 30 min Sample Time %C02 0.01 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.80 Oxygen

Vm 72.995 acf Ps -0.40 "H20 Tm 40.0 (F) Ts 361.4 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm{R)

Vwgas = 0.0471 * Vw = 0.0471 *

Bws= Vwgas Vmstd 

### +Vwgas

Ts (R) Vs = 5129.4 * Cp * \ Ps * Mw

5129.4 * 0.84 75.061 (acf* Y) 28.92 "Hg

500 (R) 821.4 (R)

= 17.65 * 75.061 %N2 79.19 Dry Gas Volume Stack Pressure Meter Temperature Stack Temperature 

# ·[ 1.20 28.95 

### + 13.6 500.0 

# } Nitrogen

76.941 sft 5

1.282 scfm

19 0.8949 sft 3

Bws*100 = 1.15 %Moist. Md = 28.834 ===== 1-Bws = 0.9885 MW = 28.709 =====

* sqrt /'). P
821.4 28.92 * 28.709 * 0.614 

## = 2,631.4 fpm 43.86 ======
ACFM= Vs *As 144 2,631.4 * 16286.0 144 297,604 ACFM fps

DSCFM

### = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 297,604 * 528 * 28.92 * 0.9885 821.4 * 29.92 182,781 DSCFM

# Method 5D Velocity Calculation
Area ofmeasurement site Ao= Temp. at measurement site To= Ambient temp. Tarnb = Inlet temp. Ti = Inlet gas volume flow rate Qi=


### Eq. SD-3 Dilution AirFlow Rate Qd = Qi (Ti-To) To-Tarnb Qd = 

### 5239.722 

### (DSCFS)



### Eq. SD-2 Volumetric Flow Rate Qo = Qi+Qd Qo = 

### 8286.072 

### (DSCFS)


### Eq. SD-1 Average Gas Velocity Qo v 

## =--=:._- Ao

v= 1.255465 

### (FPS) 6600)ft2 155f

### (F) 615 ( 

### R)

35) 

### (F) 495 ( 

### R) 361.4 

### (F) 821.4 

### (R) 182,781 

### (DSCFM) 3046.35 

### (DSCFS)

## ISOKINETIC PRELIMINARY SETUP CALCULATIONS %Moisture 1.15 % Y= 1.0283 Md = 0.9885 ll 

### p = 0.000413 "H20 C02 0.01 % \Ill p = 0.020 "H20

02 20.80 % Pb 28.95 "Hg 

# co = % Cp 0.84 N2 79.19 % Ts 155 OF 615 MWd 28.834 Tm = 40 OF 500

MW 28.709 (28.966) Psa = -0.400 "H20 28.92 AssumedRm

Assumed Tt Assumedcf = 

### Velocity Calculation
Vs =

= \Ill

ll



### Nozzle Diameter Dn =

= 

### MeterRate Rm 0.650 (0.60-0.85) cfm 120 mm 78.0 (scfm * 

### Tt)



### 85.49. Cp.llllP •

# \I(MW.**~:,)** ( 

### 61.8044 *\Ill p ) = 1.2555 fps p = 0.02031 p = 0.000413

Rm 

# *Ts 

# *Y \ 0.33 * Vs * Tm * Md



### Desired 1.397 in 

### Actual 1.500 in

0.33 * (Vs *

### \(A""i>'") * Tm * Md * Dn 2 

### Ts* Y 0.729 cfm cf

# *Tt= 87.42 cf Correction factor = cfm \Ill p 

### 35.865 @ 40



### Rate Correction Multipliers
= Rm(new)= Tm(new) 

### +460 Tm( old) 

### +460 35.865 * \Ill P 

## ®

__ 4_o

__ 36.582 * \Ill P 

## ®

__ 5_o

__ 37.299 * \Ill P 

## ®

__ 6_o

__

# * Rm(old)

°FTm °FTm °FTm OR OR

"Hg

### 38.017 

### *\lAp @ 70 

### °FTm 38.734 

### *\lAp @ 80 

### °FTm 39.451 

### *\lAp @ 90 

### °FTm
40.169 

### *\lAp @ 100 

### °FTm
40.886 

### *\lAp @ 110 

### °FTm

# TEST, Inc. 'Comments: 

## Method 5D Setup Project# Meter Box# 2010 MST %C02 0.01 Imp. Initial Final Plant Meter Cal. (Y) 1.0283 %02 20.80 1 703.7 695 Unit/Stack Pitot Cal. (Cp) 0.84 %CO 2 711.3 723.5

Operator Nozzle# %N2 79.19 3 597.8 601.3 Run # BH2 Inlet Nozzle Dia. (in.) Assumed Moist % 1.15 4 896.3 908.3

Date 3/12/13 Stack Dia.(in.) 144 Final Moist. % 1.15 5 Sample Time 30 Static Press.("H20) -0.40 Final lsokinetic% #REF! 6 

### Min/pt 5 Bar. Press. ("Hg) 28.95 

### Initial Leak Rate 0.006 cfm@ 14 "Hg Filter# Leak Check Vol. Final Leak Rate 0.006 cfm@ 14 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 163.555 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In Out 236.550 0.50 1.20 0.628 2.0 375 40 40 0.50 375 0.52 395 0.52 398 0.50 395 0.45 395 0.42 396 0.43 389 0.43 385 0.42 384 0.37 382 0.26 365 0.55 399 0.50 404 0.47 399 0.44 403 0.43 398 0.44 405 0.40 407 0.32 408 0.30 402 0.28 397 0.26 395 0.26 390

## Example Calculations Run Number BH2 Inlet Pb 28.95 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 19 Water weight gain Ds 144 m. Stack Diameter Pm 1.2 "H20 Meter pressure As 16,286.0 Sq in. Stack Area Avg !). 

### P 0.415 "H20 Differential pressure Dn 0 m Nozzle Diameter Avg Sqrt !). 

### P 0.641 "H20 Sqrt Diff. press. Tt 30 %C02 0.01 Carbon Dioxide %CO 0.00 %02 20.80 Oxygen

Vm 72.995 acf Ps -0.40 "H20 Tm 40.0 (F) Ts 393.4 (F)

Vmstd = 17.65 *Vm * [ Pb 

### + 1r::,J Tm(R)

Vwgas = 0.0471 * Vw = 0.0471 * 75.061 (acf* Y) 28.92 "Hg

500 (R) 853.4 (R)

= 17.65 * 75.061 %N2 79.19 Dry Gas Volume Stack Pressure Meter Temperature Stack Temperature 

# ·[ 1.20 28.95 

### + 13.6 500.0 

# }

19 0.8949 sft 3 

### mm Sample Time Carbon Monoxide Nitrogen

76.941 sft j



### 1.282 scfm

Bws= Vwgas Bws*100 = 1.15 %Moist. Md = 28.834 Vmstd 

### +Vwgas

Ts (R) 

### Vs = 5129.4 * Cp * \ Ps * Mw ==== 

### 1-Bws = 0.9885

* sqrt !). 

### P

5129.4 * 0.84 

# I 853.4 * \ -2-8-.9-2--*--2-8-. 7-0-9 * ===== 

### MW = 28.709 =====



### 0.641 = 2,800.1 fpm 46.67 ======


### ACFM= Vs *As 144 2,800.1 * 16286.0 144 316,684 ACFM fps

DSCFM = ACFM * 528 * Ps 

# * (1-Bws) Ts (R) 

## *29.92 316,684 * 528 

## * 28.92 

## * 0.9885 853.4 

## * 29.92 187,206 DSCFM

# Method 5D Velocity Calculation
Area ofmeasurement site Ao= Temp. at measurement site To= Ambienttemp. Tamb= Inlet temp. Ti = Inlet gas volume flow rate Qi=


### Eq. SD-3 Dilution AirFlow Rate Qd = Qi (Ti-To) To-Tamb Qd = 

### 5971.313 (DSCFS)



### Eq. SD-2 Volumetric Flow Rate Qo = Qi+Qd Qo = 

### 9091.413 (DSCFS)


### Eq. SD-1 Average Gas Velocity Qo v =----"-- 

### Ao

v= 1.377487 (FPS) . 6600}ft2 158! 

### (F) 618 ( R)

35}(F) 495 ( R) 393.4 (F) 853.4 ( R) 187,206 (DSCFM) 3120.1 (DSCFS)

## ISOKINETIC PRELIMINARY SETUP CALCULATIONS %Moisture Md C02 =

02 

# co N2 = MWd

MW AssumedRm

Assumed Tt Assumedcf = Velocity Calculation
Vs



### \IL\

L\



### Nozzle Diameter Dn = 

### 1.15 % Y= 1.0283 0.9885 L\ 

### p = 0.000494 "H20

0.01 % 

### \IL\ p = 0.022 "H20 20.80 % Pb 28.95 "Hg % Cp = 0.84 79.19 % Ts = 158 OF 618 28.834 Tm = 40 OF 500 28.709 (28.966) Psa = -0.400 "H20 28.92 0.650 (0.60-0.85) cfm

120 mm 78.0 (scfm * Tt)

85.49 • Cp • 

### \ld p •

# \I(MW•

# ~:.,) ( 

### 61.9550 *

### \IL\ p ) = 1.3775 fps p 0.02223 p 0.000494

Rm 

# *Ts 

# *Y \ 0.33 * Vs * Tm * Md

= 

### Desired 1.337 in Actual 1.500 in
MeterRate Rm= 0.33 * (Vs *

## \~) * Tm * Md * Dn 2 

### Ts* Y

= 0.795 cfm cf* Tt= 95.46 cf Correction factor = cfm 

### \IL\ p 35.778 @ 40

Rate Correction Multipliers Rm(new)= Tm(new) 

### +460 * Rm(old) Tm( old) 

### +460 35.778 *

### \IL\ p 

# ® 40 °FTm 36.493 *

### \IL\ p 

# ® 50 °FTm 37.209 *

### \IL\ p 

# ® 60 °FTm OR OR

"Hg

### 37.924

## *'I~ p 

## ® 70 

### °FTm 38.640 

# ***\1~** p @ 80 

### °FTm 39.355 

# ***\1~** p @ 90 

### °FTm
40.071 

# ***\1~** p @ 100 

### °FTm
40.786 

# ***\1~** p @ 110 

### °FTm

# TEST, Inc. I Comments: 

## Method 5D Setup Project# Meter Box # 2010 MST %C02 0.01 Imp. Initial Final Plant Meter Cal. (Y) 1.0283 %02 20.80 1 703.7 695 Unit/Stack Pitot Cal. (Cp) 0.84 %CO 2 711.3 723.5

Operator Nozzle# %N2 79.19 3 597.8 601.3 Run # BH2 Inlet Nozzle Dia. (in.) Assumed Moist % 1.15 4 896.3 908.3

Date 3/12/13 Stack Dia.(in.) 144 Final Moist. % 1.13 5 Sample Time 30 Static Press.("H20) -0.40 Final Isokinetic% #REF! 6 

### Min/pt 5 Bar. Press. ("Hg) 28.95 

### Initial Leak Rate 0.006 cfm@ 14 "Hg Filter# Leak Check Vol. Final Leak Rate 0.006 cfm@ 14 "Hg Dry Gas Pitot Orifice Vacuu Stack Probe Filter Imp. 

### Dry Gas Port/ Time Meter (CF) Velocity Press. Rate m Temp. Temp. Temp. Temp. 

### Temp. Point 163.555 ("H20) ("H20) (cfm) ("Hg.) (F) (F) (F) (F) 

### In 

### Out 236.550 0.50 1.20 0.628 2.0 406 30 30 0.48 408 0.47 407 0.44 411 0.44 412 0.43 412 0.42 412 0.40 410 0.33 404 0.24 392 0.20 380 0.21 398 0.50 405 0.47 402 0.44 402 0.42 408 0.40 407 0.40 410 0.40 412 0.38 411 0.35 409 0.26 406 0.23 389 0.24 372

## Example Calculations Run Number BH2 Inlet Pb 28.95 "Hg Barometric Pressure Cp 0.84 Pitot Cal Vw 19 Water weight gain Ds 144 in. Stack Diameter Pm 1.2 "H20 Meterpressure As 16,286.0 Sq in. Stack Area Avg**~** 

### P 0.377 "H20 Differential pressure On 0 m Nozzle Diameter Avg Sqrt**~** 

### P 0.609 "H20 Sqrt Diff. press. Tt 30 mm Sample Time %C02 0.01 Carbon Dioxide %CO 0.00 Carbon Monoxide %02 20.80 Oxygen

Vm 72.995 acf Ps -0.40 "H20 Tm 30.0 (F) Ts 403.5 (F)

Vmstd = 17.65 * Vm * [ Pb 

### +

# 1~] Tm(R)

Vwgas = 0.0471 *Vw = 0.0471 *

Bws= Vwgas Vmstd 

### + Vwgas

Ts (R) 

### Vs = 5129.4 * Cp * \ Ps * Mw

5129.4 * 0.84 75.061 (acf* Y) 28.92 "Hg 490 (R) 

### 863.5 (R)



### =17.65 * 75.061 %N2 79.19 Dry Gas Volume Stack Pressure Meter Temperature Stack Temperature 

# ·[ 1.20 28.95 

### + 13.6 490.0 

# }Nitrogen

78.511 sft j



### 1.309 scfm

19 0.8949 sft 3



### Bws*100 = 1.13 %Moist. Md = 28.834 ===== 

### 1-Bws = 0.9887 MW = 28.712 =====



### * sqrt**~** 

### P 863.5 28.92 * 28.712 * 0.609 

## = 2,675.9 fpm 44.60 =====


### ACFM= Vs *As 144 2,675.9 * 16286.0 144 302,637 ACFM fps

DSCFM = ACFM * 528 * Ps * 

### (1-Bws) Ts (R) * 29.92 302,637 * 528 * 28.92 * 0.9887 863.5 * 29.92 176,846 DSCFM

# Method 5D Velocity Calculation
Area ofmeasurement site Ao= Temp. at measurement site To= Ambienttemp. Tamb= Inlet temp. Ti = Inlet gas volume flow rate Qi=


### Eq. SD-3 Dilution AirFlow Rate Qd = Qi (Ti-To) To-Tamb Qd = 

### 5882.885 

### (DSCFS)



### Eq. SD-2 Volumetric Flow Rate Qo = Qi+Qd Qo = 

### 8830.319 

### (DSCFS)


### Eq. SD-1 Average Gas Velocity Qo**v=-~-** 

### Ao

v= 1.337927 

### (FPS) 6600)ft2 158J

### (F) 618 ( 

### R)

351 

### (F) 495 ( 

### R) 403.5 

### (F) 863.5 ( 

### R) 176,846 

### (DSCFM) 2947.433 

### (DSCFS)

## ISOKINETIC PRELIMINARY SETUP CALCULATIONS %Moisture Md C02

02 

# co N2 = MWd

MW AssumedRm

Assumed Tt Assumed cf = Velocity Calculation
Vs



### \1.1

.1

Nozzle Diameter Dn =



## = Meter Rate Rm 1.13 % Y= 1.0283 0.9887 

### .1 p = 0.000466 "H20

0.01 % 

### \1.1 p = 0.022 "H20 20.80 % Pb 28.95 "Hg % Cp 0.84 79.19 % Ts = 158 OF 618 28.834 Tm 30 OF 490 28.711 (28.966) Psa = -0.400 "H20 28.92 0.650 (0.60-0.85) cfm

240 mm 156.0 (scfm 

# *Tt)

85.49 • 

## cp • llt.r •

# \I(Mw•

# ~:,.l ( 61.9526 

# *\1.1 p ) = 1.3379 fps p = 0.02160 p = 0.000466

Rm

# *Ts

# *Y \ 0.33 

# *Vs

# *Tm

# *Md

Desired 1.370 in Actual 1.500 in

0.33 

# * (Vs 

# *\(A"i>") 

# *Tm

# *Md

# *Dn 2 

### Ts* Y 0.757 cfm cf

# *Tt= 181.76 cf Correction factor= cfm 

### \1.1 p 35.068 @ 30

Rate Correction Multipliers Rm(new)= Tm(new) 

### +460 Tm( old) 

### +460 35.068 

# *\1.1 p @

__ 3_0

-- 35.783 

# *\1.1 p @

__ 4_0

__ 36.499 

# *\1.1 p 

### @

__ 5_0

-- 

# * Rm(old)

°FTm °FTm °FTm OR OR

"Hg

### 37.215 

### *\lAp @ 60 

### °FTm 37.930 

### *\lAp @ 70 

### °FTm 38.646 

### *\lAp @ 80 

### °FTm
39.362 

### *\lAp @ 90 

### °FTm
40.077 

### *\lAp @ 100 

### °FTm

### APPENDIXC ANALYTICAL DATA



# 'I

### Run Number 1 2 3 

# ANALYTICAL RESULTS

Filter Number

1007 1006 1005 

## Particulate Matter FelmanProductions LLC Baghouse#2

Filter Acetone Rinse Final Weight Final Weight (grams) (grams) 0.0008 0.0043 0.0004 0.0038 0.0003 0.0045 Total Particulate

Matter (grams) 0.0051 0.0042 0.0048_·.·'\ 

### Lab Conditions

,, ) > .i ·1 

# . Filter Gravimetric Analysis Temperature: 18 

# oc Bar. Press.: 29.03 "Hg ProjectNumber: TI1550 Location: Baghouse #2 Company: FelmanProductions LLC EPA Method: 5 Analyst: JPS Initial Tray FilterTare Tray/Filter Weight Weight Weight Weight Results FilterNumber: 1007 Number Date Time 

### .(gl .(gl .(gl .(gl Notes: 1 4115/2013 800 0.9230 0.5558 1.4796 0.0008 2 4/15/2013 1200 0.9230 0.5558 1.4796 0.0008 3 4/15/2013 1600 0.9230 0.5558 1.4796 0.0008



## - FinalWeight: 0.0008 Initial Tray FilterTare Tray/Filter Weight Weight Weight Weight Results FilterNumber: 1006 Number Date Time 

### .(gl .(gl .(gl .(gl Notes: 1 4/15/2013 800 0.9230 0.5567 1.4801 0.0004 2 4/15/2013 1200 0.9230 0.5567 1.4802 0.0005 3 4115/2013 1600 0.9230 0.5567 1.4801 0.0004 

### Final Weight: 0.0004 Initial Tray FilterTare Tray/Filter Weight Weight Weight Weight Results FilterNumber: 1005 Number Date Time 

### .(gl .(gl .(gl .(gl Notes: 1 4115/2013 800 0.9230 0.5282 1.4515 0.0003 2 4115/2013 1200 0.9230 0.5282 1.4515 0.0003 3 4/15/2013 1600 0.9230 0.5282 1.4515 0.0003 

### Final Weight: 0.0003

### ~ 

# Inc,. 

# Rinse Gravimetric Analysis

Project Number: TI1550



## ---------------- Lab Conditions Company: Felman Productions LLC Temperature: 18 °C



### ------------ Location: Baghouse #2 Bar. Press.: 29.03 "Hg

Analyst: JPS



### ----------------

Initial Beaker Beaker/Sample Final Filter Beaker Weight Weight Weight Number Number Date Time {g} {g} {g}



### 1007 2-1 4/15/2013 800 102.9716 102.9759 0.0043 1006 2-2 4/15/2013 800 95.7555 95.7593 0.0038 1005 2-3 4115/2013 800 106.8597 106.8642 0.0045Your P.O.#: 10244

Your Project#: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Your C.O.C. #: NA Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/04/18 

### CERTIFICATE OF ANALYSIS MAXXAM JOB#: 8351189 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train #Samples Received: 8
Analyses Hydrogen Halides in H2S04 Imp. Volume of Sulfuric Acid lmpinger Quantity 8 8 Date Extracted 2013/04/12 N/A Date Analyzed Laboratory Method 2013/04/12 BRL SOP-00108 2013/04/12
* RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.

Ancy Sebastian

## vttb~..__ 18 Apr 201311:13:25-04:00 Encryption Key

# E

Please direct all qu stions regarding this Certificate of Analysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Taxies Email: ASebastian@maxxam.ca Phone# (905) 817-5831 

## ==================================================================== Method Reference EPA Method 26A

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate# CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of7

1\!1axxarn /\na!ytics International Corporation o/a Maxxam Analytics 6740 Campobello Road. Mtssissauga, Ontario, LSN 2L8 Tel: (905}**817~5700** Toll-free: BOD-563-6266 Fax: (905} 817-5777 v1vvw.maxxam.ca

# Ma-62am

Maxxam Job #: 8351189 Report Date: 2013/04/18

Maxxam ID**~ampling** Date 

### r.oc Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN RC1306 RC1307 RC1308 RC1309 2013/03/27 2013/03/27 2013/03/19 2013/03/19 00:01 00:01 00:01 00:01

NA NA NA NA Units**~LANK-H2S04-M26A** BLANK-H20·M26A RUN RUN RDL QC Batch 1·BAGH2·M26A 2·BAGH 2·M26A Sulfuric Acid Volume ml 325 354 360 409 1 3179578 Hydrochloric Acid ug <200 <200 3100 2500 200 3179677 RDL 

### =Reportable Detection Limit QC Batch 

### =Quality Control Batch

Maxxam ID RC1310 RC1311 RC1312 RC1313 Sampling Date 2013/03/19 2013/03/15 2013/03/15 2013/03/15 00:01 00:01 00:01 00:01 COC Number NA NA NA NA Units RUN RUN RUN RUN RDL QC Batch 3-BAGH 2·M26A 1·BAGH 5·M26A 2·BAGH 5·M26A 3·BAGH 5·M26A Sulfuric Acid Volume ml 379 390 357 406 1 3179578 Hydrochloric Acid ug 1900 230 <200 <200 200 3179677 RDL = Reportable Detection Limit QC Batch = Quality Control Batch

Page2 of7
l\ila,xam l•nalytics lrnernational COrporalion o/a Maxxam**Anal~'lics** 6740 Canpobello Road, M!SSissauga, omario, L5N 2LB Tel: (905) 817-5700 Toll-Free: 800-563·6266 Fax: (905) 817-5777 www.maxxam.ca

## MaO-am Keika Ventures Maxxam Job #: 8351189 Client Project #: Tl1550 Report Date: 2013/04/18 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Maxxam ID RC1306 Collected 2013/03/27 Sample ID BLANK-H2S04-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICISPEC 3179677 2013104/12 3179578 N/A
Maxxam ID RC1307 Collected 2013103127 Sample ID BLANK-H20-M26A Shipped Matrix Stack Sampling Train Received 2013/04106 Instrumentation Batch Extracted ICISPEC 3179677 2013104112 3179578 N/A
Maxxam ID RC1308 Collected 2013/03/19 Sample ID RUN 1-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A
Maxxam ID RC1308 Dup Collected 2013/03/19 Sample ID RUN 1-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st IC/SPEC 3179677 2013/04/12 2013/04112 Ann-Marie Stern
Maxxam ID RC1309 Collected 2013/03/19 Sample ID RUN 2-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st IC/SPEC 3179677 2013104/12 2013/04/12 Ann-Marie Stem 3179578 N/A 2013/04/12

Maxxam ID RC1310 Collected 2013/03/19 Sample ID RUN 3-BAGH 2-M26A Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A

Page 3 of?

Maxxam Analylics lrnernatlonal COrporation o/a Maxxam Analytics 6740 C<mpoDello Road, Mlsslssauga, Ontario, L5N 2L8 Tel: (905) 817-5700 TOll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## l\11 

# a({}la m

Maxxam Job #: 8351189 Report Date: 2013/04/18

Maxxam ID RC1311 Sample ID RUN 1-BAGH 5-M26A Matrix Stack Sampling Train

Maxxam ID RC1312 Sample ID RUN 2-BAGH 5-M26A Matrix Stack Sampling Train

Maxxam ID RC1313 Sample ID RUN 3-BAGH 5-M26A Matrix Stack Sampling Train Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Collected 2013/03/15 Shipped Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A
Collected 2013/03/15 Shipped Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A
Collected 2013/03/15 Shipped Received 2013/04/06 Instrumentation Batch Extracted IC/SPEC 3179677 2013/04/12 3179578 N/A

Page4 of?

Ma<Xam Analylics lrnernational COrporation ola Maxxam**Anal~"'ics** 6740 CampobeHo Road, Mlsslssauga, Ontario, L5N 2L8 Tel: (905) 817·5700 Toll-Free: 800·563-6266 Fax: (90s) 817·5777 www.maxxam.ca

# Ma"62-am
Maxxam Job #: 8351189 Report Date: 2013/04/18

Results relate onlvto the items tested. Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244

GENERAL COMMENTS

Page5of7

1\i!a"xam Analylics lrrternational COrporation o/a Maxxam Analytlcs 6740 C<mpobeno Road, Mlsslssauga, OntariO, L5N 2L8 Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777www.maxxam.caQA/QC Batch Num lnit QC Tvoe Parameter 3179677 A_S Matrix Spike (RC1308) Hydrochloric Acid Spiked Blank Hydrochloric Acid Method Blank Hydrochloric AcidRPDSample/Sample Duo Hydrochloric Acid Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.**~** FELMAN PRODUCTIONS

Quality Assurance Report Maxxam Job Number: GB351189 Date Analyzed vvvv/mm/dd 2013/04/12 2013/04/12 2013/04/12
2013/04/12 Value %Recoverv 100 102 <200

0.2 Units % % ug

% Matrix Spike: A sample to which a known amount ofthe analyte of interest has been added. Used to evaluate sample matrix interference. QC Limits
•' 80-120 90- 110

20 Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method !accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.

Page 6 of7

1\ilaxxam AnalyUcs lmernational COrporation o!a Maxxam Analyllcs 6740 campobello Road, Mlsslssauga, OntariO, L5N 2L8 Tel: (905) 817·5700 Toll-free: 800.563·6266 Fax: (905) 817·5777 www.maxxam.ca

# Ma?_{)2am

Validation Signature Page

Maxxam Job 

### #: 8351189

The analytical dataand all QC contained inthis report were reviewed and validated bythe following individual(s).

Frank Mo, B.Sc., Inorganic Lab. Manager

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.10.2 of ISO!IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page? of?

Ma:<xam Analytics International Corporation o/a Maxxam Anal}'lics 6740 Campobello Road, MlssiSsauga, Ontario, L5N 2L8 Tel: (905) 817·5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# M.r-3?{)2am

Attention: Lorri L White Keika Ventures Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Your P.O.#: 10244

Your Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS

Report Date: 2013/04/17 

### CERTIFICATE OF ANALYSIS MAXXAM JOB#: 8351214 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train # Samples Received: 7
Analyses Metals in Combined Train (6020) Date Date Method Quantity Extracted Analyzed Laboratory Method Reference 7 2013/04/10 2013/04/12 BRL SOP-00103/ BRL EPA 6020 I M29 SOP-00102

• RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.

Ancy Sebastian m£1>\.- 17Apr 201314:33:19 -{J•I:OO Encryption KeyE

Please direct all qu ""v"" '"Y"''u'"Y '"'"Certificate ofAnalysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Toxics Email: ASebastian@maxxam.ca Phone#(905)817-5831 

## ==================================================================== Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of8

1\ila,xam Analytics International COrporation o/a Maxxam**Anal~>tics** 6740 GampobeRo Road, Mlssissauga, OnlariO, L5N 21..8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## J\/1 

## a 

# ({)2a m

Maxxam Job #: 8351214 Report Date: 2013/04/17

Maxxam ID Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN) RC1448 RC1449 RC1450 RC1451 Sampling Date 2013/03/27 2013/03/13 2013/03/13 2013/03/13 00:01 00:01 00:01 00:01 Units BLANK-M29 RDL RUN RUN RUN RDL 1-BAGH 2-M29 2-BAGH 2-M29 3-BAGH 2-M29 Combined Train Arsenic (As) ug <0.40 0.40 <2.0 <2.0 <2.0 2.0 Combined Train Cadmium (Cd) ug <0.10 0.10 <0.50 <0.50 <0.50 0.50 Combined Train Chromium (Cr) ug 1.80 0.30 3.9 11.4 6.5 1.5 Combined Train Lead (Pb) ug 0.84 0.20 50.0 25.0 28.3 1.0 Combined Train Manganese (Mn) ug 8.25 0.75 3370 976 1280 3.8 Combined Train Nickel (Ni) ug 1.69 0.50 4.7 11.1 9.1 2.5 RDL = Reportable Detection Limit QC Batch = Quality Control Batch

Maxxam ID RC1452 RC1453 RC1454 Sampling Date 2013/03/13 2013/03/13 2013/03/13 00:01 00:01 00:01 Units RUN RUN RUN RDL QC Batch 1-BAGH 5-M29 2-BAGH 5-M29 3-BAGH 5-M29 Combined Train Arsenic (As) ug <2.0 <2.0 <2.0 2.0 3177251 Combined Train Cadmium (Cd) ug <0.50 <0.50 <0.50 0.50 3177251 Combined Train Chromium (Cr) ug 7.4 38.3 3.6 1.5 3177251 Combined Train Lead (Pb) ug 25.9 36.2 14.0 1.0 3177251 Combined Train Manganese (Mn) ug 607 547 400 3.8 3177251 Combined Train Nickel (Ni) ug 5.7 14.7 4.3 2.5 3177251 RDL = Reportable Detection Limit QC Batch = Quality Control Batch

Page 2 of8 

## pc Batch

3177251 3177251 3177251 3177251 3177251 3177251

Ma«amAnalyUcs lrnernational COrporation O!a Maxxam Analy·rics 6740 campobello Road, Mlssissauga, Ontario, L5N 2LB Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fa>:: (905) 817-5777 www.maxxam.r.a

## M 

# a 

# ({52am Keika Ventures Maxxam Job #: 8351214 Client Project #: Tl1550 Report Date: 2013/04/17 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244 Test Summary

Maxxam ID RC1448 Collected 2013/03/27 Sample ID BLANK-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10
Maxxam ID RC1449 Collected 2013/03/13 Sample ID RUN 1-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10
Maxxam ID RC1449 Dup Collected 2013/03/13 Sample ID RUN 1-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st ICP1/MS 3177251 2013/04/10 2013/04/12 Nan Ra kha
Maxxam ID RC1450 Collected 2013/03/13 Sample ID RUN 2-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st ICP1/MS 3177251 2013/04/10 2013/04/12 Nan Ra kha
Maxxam ID RC1451 Collected 2013/03/13 Sample ID RUN 3-BAGH 2-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10
Maxxam ID RC1452 Collected 2013/03/13 Sample ID RUN 1-BAGH 5-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10
Maxxam ID RC1453 Collected 2013/03/13 Sample ID RUN 2-BAGH 5-M29 Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted ICP1/MS 3177251 2013/04/10

Page 3 of8

Ma-.am P.nalylics lrrternational COrporation o/a Maxxam**Anal~'tics** 6740 CampobeUo Road, Mlsslssauga, omario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: BOQ-563-6266 Fax: (905) 817-5777 \YWW.maxxam.caMaxxam Job #: 8351214 Report Date: 2013/04/17

Maxxam ID RC1454 Sample ID RUN 3-BAGH 5-M29 Matrix Stack Sampling Train Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Collected 2013/03/13 Shipped Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st ICP1/MS 3177251 2013/04/10 2013/04/12 Nan Ra kha

Page4 of 8

f\ilaxxam AnalyHcs Jnternalional Corporation o/a Maxxam Analytics 6740 Campobello Road, Mlssissauga, Ontario, L5N 2l8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777W\VW.maxxam.ca

## f\/1 

## a 

# ?.{)2a m
Maxxam Job #: 8351214 Report Date: 2013/04/17 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244

ELEMENTS BY ICP/MS (STACK SAMPLING TRAIN) Metals in Combined Train (6020): Extra 5x dilution was required for all samples except RC1448, due to the matrix Post digestion duplicate and spike was done on sample RC1449.

Results relate onlvto the items tested.

Page5of8

MauamAnalyUcs lrnernatlonal COrporation o/a Maxxam Analytlcs 6740 C<mpobello Road, M!Sslssauga, omarlo, L5N 2L8 Tel: (905) 817•5700 Toll-Free: 800.563·6266 Fax: (905) 817·5777 www.maxxam.ca

# Ma{!52am

QA/QC Batch Num lnit QC Type 3177251 N_R Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSDRPD Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSD RPD Matrix Spike (RC1449) MS/MSD RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Method Blank RPD Method Blank RPD Method Blank RPD Method Blank RPD Method Blank RPD Method Blank RPDRPDSample/Sample Dup Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC. -FELMAN PRODUCTIONS

Quality Assurance Report Maxxam Job Number: GB351214 Date Analyzed Parameter yyyy/mm/dd Combined Train Arsenic (As) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12 Combined Train Nickel (Ni) 2013/04/12

Combined Train Arsenic (As) 2013/04/12 Combined Train Cadmium (Cd) 2013/04/12 Combined Train Chromium (Cr) 2013/04/12 Combined Train Lead (Pb) 2013/04/12 Combined Train Manganese (Mn) 2013/04/12 Combined Train Nickel (Nil 2013/04/12 Value %Recovery 98 7.4 103 6.0 104 5.9 109 7.6 126 13.6 105 6.9 98 6.1 99 7.2 98 5.4 102 5.9 101 5.4 101 6.6 <0.40

NC <0.10

NC <0.30

NC <0.20

NC <0.75

NC <0.50

NC

NC NC NC 2.3 1.4 NC Duplicate: Paired analysis of a separate portion ofthe same sample. Used to evaluate the variance in the measurement. Units % % % % % % % % % % % % % % % % % % % % % % % % ug % ug % ug % ug % ug % ug %

% % % % % %

Matrix Spike: A sample to which a known amount ofthe analyte of interest has been added. Used to evaluate sample matrix interference. QC Limits; 70

## -13~ 20 70-130 20 70-130 20 70-130 20 70- 130 20 70- 130 20 85- 115 20 85- 115 20 85-115 20 85-115 20 85-115 20 85- 115 20 20 20 20 20 20 20

20 20 20 20 20 20

Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.
Page 6 of8

Mauam AnalyUcs lrrternational COrporation o/a Maxxam Analytics 6740 GampobeHo Road, MISSiSsauga, Ontario, L5N as Tel: (905) 817·5700 Toll-Free: 81)()-563·6266 Fa>:: (905) 817-5777 www.maxxam.ca

# Ma?§f.am Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS QualityAssurance Report (Continued) Maxxam Job Number: GB351214
NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

Page 7 of8

Ma.xam Analytics !rtternauonal corporation Ola Maxxam Analytlcs 6740 campolleHo Rosa, Mtsslssauga, Ontarlo,l5N as Tel: (905) 817-5700 Ton-Free: 800-563-6266 Fax: (9Q5) 817-5777 www.maxxam.ca

## Ma[{)2am

Validation Signature Page
Maxxam Job #:8351214

The analytical dataand all QC contained in this report were reviewed and validatedbythe following individual(s).

FrankMo, B.Sc., Inorganic Lab. Manager

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation pleaserefer to the Validation Signature Page.

Page8of8

1\flaxxam Anatylics trnernattonal COrporation o/a Maxxam Analytlcs 6740 Campobello Road, MISsiSsauga, Ontario, LSN 2LB Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: (905) 817-5777 www.maxxam.ca-**~rFI'' ~~·**  ,:·.¥' 

### ............,.... ·**~' -JJ~<·6**  

# If:**<,~'fa '~**  .**~~:e,.l11~ ~ljlir** 

- .IV"l!m'**~ ...!lJI~,** **~·""** 

# rbent Trap Analysis Report

3nt Name 

## Keika Ventures, LLC act Name Lorri White
=tp 

### J.D. Plant/Source Date Analyzed Scientist 156035 Felman 

### 4/10/2013 John Perko 

### 150823 Felman 

### 4/10/2013 John Perko 

### 156060 Felman 

### 4/10/2013 John Perko 

### 156021 Felman 

### 4/10/2013 John Perko 

### 156066 Felman 

### 4/10/2013 John Perko 

### 156064 Felman 

### 4/10/2013 John Perko 

### 156014 Felman 

### 4/10/2013 John Perko 

### 150797 Felman 

### 4/10/2013 John Perko 

### 156042 Felman 

### 4/10/2013 John Perko 

### 156034 Felman 

### 4/10/2013 John Perko 

### 156058 Felman 

### 4/10/2013 John Perko 

### 156006 Felman 

### 4/10/2013 John Perko 

### 156057 Felman 

### 4/10/2013 John Perko 

### 156069 Felman 

### 4/10/2013 John Perko 

### 150824 Felman 

### 4/10/2013 John Perko

'-- -----·---------·-

s than 

### 0.027 ng is considered"< 

### LDL." Which is less than the lowest detection limit.**:~tion** Report Available

# -------~==--=1 iliti±10%J Massng Sect.1 0.86 21.06

0.67 0.65 0.51 0.73 0.65 21.20

0.61 19.31 17.28 28.22 26.06 22.55 45.09**-~~---·-··---** Ohio Lumex Co., Inc. 9263 Ravenna Rd., Unit A-3 Twinsburg, OH 44087 Phone: (330) 405-0837 Fax: (330) 405-0847 vvww.ohiolumexcom Turn -Around Time

### ~~~~:J Standard 

# D 48 hour rush Other

Project Number 2001307 

## 4/11/2013 Date

________ _ Phone 

## 919-933-9569 Mass ng Mass ng Spike BreakSect.2 Sect.3 Level (ng) through% Comme1 0.74 FiE 0.54 20 Trc: 0.54 Trc: 0.61 #5 Baghouse 0.52 #5 Baghouse 0.74 #5 Baghouse 0.55 #5 Baghouse 0.74 20 #5 Baghouse 0.47 #5 Baghouse 0.72 #2 Baghouse 0.72 #2 Baghouse 0.87 #2 Baghouse 0.72 #2 Baghouse 0.73 #2 Baghouse 0.57 20 #2 Baghouse**--------~------** -·------- ----**----~-------------** --

# Ma?§i.am

Your P.O.#: 10244

Your Project #: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Your C.O.C. #: N/A Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/04/29 

### CERTIFICATE OF ANALYSIS MAXXAM JOB#: 8351227 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train # Samples Received: 7
Analyses 2,3,7,8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A) Quantity 6 7 7 Date Extracted N/A 2013/04/16 2013/04/16 Date Analyzed Laboratory Method 2013/04/24 BRL SOP-00404 2013/04/25 BRL SOP-00404 2013/04/24 BRL SOP-00408, 409

• RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

Ancy Sebastian**~~rd.~** 29 Apr 2013 23:03:49 .04:00 Encryption

### Key~
Please direct all qu "'"v""' '"!ofo•u•"l:l .,,;:; Certificate ofAnalysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Toxics Email: ASebastian@maxxam.ca Phone# (905) 817-5831 

## ==================================================================== Method Reference EPA1613Bmod(M23/23A) EPA1613Bmod(M23/23A) EPA 1668A (0010) mod

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of29

1\<la.Xxam Analylics International COrporation o/a Maxxam Analytics 6740 Gampobello Road, Mtssissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: BOQ-563·6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1495**~ampling** Date 2013/03/15 00:01 

### roc Number N/A TOXIC EQUIVALENCY Units TRAIN EDL**~DL** TEF (2005 WHO) TEQ(DL) BLANK·M23/PCB 33'44'-TetraCB-(77) ng 1.4 0.037 0.30 0.00010 0.00014 344'5-TetraCB-(81) ng 0.081**~.038** 0.30 0.00030 0.000024 233'44'-PentaCB-(105) ng 1.4 0.032 0.30 0.000030 0.000042 2344'5-PentaCB-(114) ng 0.12 0.030 0.30 0.000030 0.0000036 23'44'5-PentaCB-(118) ng 3.9 0.032 0.30 0.000030 0.00012 23'44'5'-PentaCB-(123) ng 0.073 0.034 0.30 0.000030 0.0000022 33'44'5-PentaCB-(126) ng <0.031 0.031 0.30 0.10 0.0031 HexaCB-(156)+(157) ng 0.17**~.033** 0.60 0.000030 0.0000051 23'44'55'-HexaCB-(167) ng 0.069 0.035 0.30 0.000030 0.0000021 33'44'55'-HexaCB-(169) ng <0.037 0.037 0.30 0.030 0.0011 233'44'55'-HeptaCB-(189) ng <0.030**~.030** 0.30 0.000030 0.00000090 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.0045 Surrogate Recovery(%) C13-233'44'55'-HeptaCB-(189) % 96 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 107 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) o/o 107 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) o/o 117 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) o/o 104 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) o/o 114 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) o/o 113 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) o/o 113 N/A N/A N/A N/A**~13-33'44'55'-HexaCB-(169)** o/o 97 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) o/o 117 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) o/o 119 N/A N/A N/A N/A C13-344'5-TetraCB-(81 ) o/o 119 N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.**~c** Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization. Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 2 of29

Ma:<xam Ana!ylics !rnernational COrporation a/a Maxxam Analytics 6740 Campollello Road. Mlssissauga. Ontario. L5N 2'-8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 \YWW.maxxam.c.a

# rv1c:t"§am

Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1497 Sampling Date 2013/03/19 00:01 OC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) 1·BH2·M23/PCB 33'44'-TetraCB-(77) ng 4.3 0.036 0.30 0.00010 0.00043 344'5-TetraCB-(81) ng 0.26 0.037 0.30 0.00030 0.000078 233'44'-PentaCB-(105) ng 4.4 0.033 0.30 0.000030 0.00013 2344'5-PentaCB-(114) ng 0.36 0.031 0.30 0.000030 0.000011 23'44'5-PentaCB-(118) ng 12 0.033 0.30 0.000030 0.00036 23'44'5'-PentaCB-(123) ng 0.23 0.035 0.30 0.000030 0.0000069 33'44'5-PentaCB-(126) ng 0.081 0.032 0.30 0.10 0.0081 HexaCB-(156)+(157) ng 0.46 0.029 0.60 0.000030 0.000014**~3'44'55'-HexaCB-(167)** ng 0.18 0.031 0.30 0.000030 0.0000054 33'44'55'-HexaCB-(169) ng <0.033 0.033 0.30 0.030 0.00099 233'44'55'-HeptaCB-(189) ng <0.028 0.028 0.30 0.000030 0.00000084 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.010 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 95 N/A N/A N/A : N/A

--· ... C13-233'44'5-HexaC:B-{15Fl**~10** 10fl

. ',1·!'., N/A f\:''' N/A**;--------------------~----** -·- r----······ ----· ·-·--- C13-23:::"<;..+'5'-hex<,. '-·· ::,; J I % 1i

..... ·::: N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 114 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 107 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 118 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 116 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 115 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 106 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 117 N/A N/A N/A N/A C13-33'44'- TetraCB-(77) % 121 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 115 N/A N/A N/A N/A N/A

### =Not Applicable RDL 

### =Reportable Detection Limit EDL

## =Estimated Detection Limit QC Batch 

### = Quality Control Batch TEF 

### = Toxic Equivalency Factor, TEO

## = Toxic Equivalency Quotient, #of somers 

## pc Batch

N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A N/A ' 

### ' N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.**~H0(2005):** The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 3 of 29

Ma:<xam Analylics lrnemational Corporation o!a Maxxam**Anal~'lics** 6740 campobello Road, Mlssissauga, Ontario, L5111 2LB Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# rvra;:{)iam

Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1498**~ampling** Date 2013/03/19 00:01 

### toe Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL [TEF (2005 WHO) TEQ(DL) 2-BH2-M23/PCB 33'44'-TetraCB-(77) ng 2.6 0.036 0.30 0.00010 0.00026 344'5-TetraCB-(81) ng 0.15 0.036 0.30 0.00030 0.000045 233'44'-PentaCB-(105) ng 2.5 0.031 0.30 0.000030 0.000075 2344'5-PentaCB-(114) ng 0.20 0.029 0.30 0.000030 0.0000060 23'44'5-PentaCB-(118) ng 6.7 0.031 0.30 0.000030 0.00020 23'44'5'-PentaCB-(123) ng 0.11 0.033 0.30 0.000030 0.0000033 33'44'5-PentaCB-(126) ng 0.048 0.030 0.30 0.10 0.0048 HexaCB-(156)+(157) ng 0.25 0.034 0.60 0.000030 0.0000075 23'44'55'-HexaCB-(167) ng 0.11 0.036 0.30 0.000030 0.0000033 33'44'55'-HexaCB-(169) ng <0.037 0.037 0.30 0.030 0.0011 233'44'55'-HeptaCB-(189) ng <0.023 0.023 0.30 0.000030 O.OC000069 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.0065 Surrogate Recovery (%) C13-233"44'55'-HeptaCB-I1 &91**~-~,** 97 N/.A NIA N_,.,**~'-!',A.**

.. 

### -· --··.-·---· --- ·c**l3-233'44'!.)'Rr-:t·,~-!~i~-(_, ~-.,**  1 '1o 110 I. r• '•'<iA Ni"- :·,,A C13-233'44'-PentaCB-(105) % 113 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 106 N/A N/A N/A N/A 

# : C13-2344'5-PentaC5-\ ·: i..1 .·**~'c** ; I**~:** 13 ; N/A**~i/A** N/f- NIA

·-·-- --·--------·- C13-23'44'5-PentaCB-(118) % 113 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 111 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 106 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 117 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 115 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 115 N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF = Toxic Equivalency Factor, TEO = Toxic Equivalency Quotient, #of somers**~c** Batch

N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A N/A**~**..,::':::. .:... ?::50F**~** .. -...... ..:
.--·"'"":3Ct) N/A 3182506 N/A 3182506 ;**~-1/,.'!** I**2"!0:':'7~-f-':**

--- N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 4 of29

Ma:<xam Analytics rrnernational COrporation o/a Maxxam Analytics 6740 campobello Road. Mlssissauga. Ontario. L5N 2L8 Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## Ma({)2am
Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1499**~ampling** Date 2013/03/19 00:01 OC Number N/A TOXIC EQUIVALENCY Units RUN EDL fRDL rrEF (2005 WHO) TEQ(DL) 3-BH2-M23/PCB 33'44'-TetraCB-(77) ng 1.5 0.038 0.30 0.00010 0.00015 344'5-TetraCB-(81) ng 0.085 O.Q38 0.30 0.00030 0.000026 233'44'-PentaCB-(105) ng 1.4 0.032 0.30 0.000030 0.000042 2344'5-PentaCB-(114) ng 0.12 0.030 0.30 0.000030 0.0000036**~3'44'5-PentaCB-(118)** ng 3.9 0.032 0.30 0.000030 0.00012 23'44'5'-PentaCB-(123) ng 0.082 0.034 0.30 0.000030 0.0000025 33'44'5-PentaCB-(126) ng 0.033**~.031** 0.30 0.10 0.0033 HexaCB-(156)+(157) ng 0.17 0.035 0.60 0.000030 0.0000051 23'44'55'-HexaCB-(167) ng 0.068 0.038 0.30 0.000030 0.0000020 33'44'55'-HexaCB-(169) ng <0.039 0.039 0.30 0.030 0.0012 233'44'55'-HeptaCB-(189) ng <0.023 0.023 0.30 0.000030 0.00000069 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.0049 Surrogate Recovery(%) i
"' C13-233'44'55'-HeptaCB-(189) % 94 IN/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 102 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 102 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 109 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 100 N/A N/A N:A NiA C13-2344'5-PentaCB-(114) % 106 N'A N/A N'A N/A C13-23'44'5-PentaCB-(118) % 105 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 103 N/A N/A N/A N/A lc13-33'44'55'-HexaCB-(169) % 90 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 113 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 110 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 111 N/A N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL 

### =Estimated Detection Limit QC Batch =Quality Control Batch TEF =Toxic Equivalency Factor, TEQ =Toxic Equivalency Quotient, #of somers 

### pc Batch

N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A N/A

- NIA 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182:0•'3 N/A 318250·3 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506 N/A 3182506

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 5 of29 ! I

Ma'Xam Analy!iGs !mernational COrporation o!a Maxxam**Anal~'tics** 6740 Campobello Road, Mtssissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1500 Sampling Date 2013/03/15 00:01 OC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ{DL} 1-BH5-M23/PCB 33'44'-TetraCB-(77) ng 5.2 0.039 0.30 0.00010 0.00052 344'5-TetraCB-(81) ng 0.31 0.040 0.30 0.00030 0.000093 233'44'-PentaCB-(105) ng 5.4 0.031 0.30 0.000030 0.00016 2344'5-PentaCB-(114) ng 0.42 0.030 0.30 0.000030 0.000013 23'44'5-PentaCB-(118) ng 15 0.031 0.30 0.000030 0.00045 23'44'5'-PentaCB-(123) ng 0.31 0.033 0.30 0.000030 0.0000093 33'44'5-PentaCB-(126) ng 0.10 0.031 0.30 0.10 0.010 HexaCB-(156)+(157) ng 0.52 0.033 0.60 0.000030 0.000016 23'44'55'-HexaCB-(167) ng 0.22 0.036 0.30 0.000030 0.0000066 33'44'55'-HexaCB-(169) ng <0.037 0.037 0.30 0.030 0.0011**~33'44'55'-HeptaCB-(**189) ng <0.026 0.026 0.30 0.000030 0.00000078 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.012 Surrogate Recovery {%) C13-233'44'55'-HeptaCB-(189) % 94 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 110 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 110 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 112 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 107 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 115 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 115 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 114 N/A N/A N/A N/A C13-33'44'55'-HexaCB-{169) % 111 N/A N/A N/A N/A**~13-33'44'5-PentaCB-(126)** % 123 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 123 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 117 N/A N/A N/A N/A N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch**~EF** =Toxic Equivalency Factor, TEQ =Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum of Toxic Equivalent Quotients for the congeners tested.

## pc Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins snd Dioxin-like Compounds

Page 6 of29 i

1\ilaxxaon Analylics InternatiOnal COrporation ola Maxxam**Anal~'lics** 5740 C<mpobello Road, MISSiSsauga. OntariO, LSN 21..8 Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #:8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1505 Sampling Date 2013/03/15 00:01 OC Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ(DL) 2·BH5-M23/PCB 33'44'-TetraCB-(77) ng 8.4 0.037 0.30 0.00010 0.00084 344'5-TetraCB-(81) ng 0.48 O.Q38 0.30 0.00030 0.00014 233'44'-PentaCB-(105) ng 8.3**~.036** 0.30 0.000030 0.00025 2344'5-PentaCB-(114) ng 0.69 0.034 0.30 0.000030 0.000021 23'44'5-PentaCB-(118) ng 23 0.036 0.30 0.000030 0.00069 23'44'5'-PentaCB-(123) ng 0.32**~.038** 0.30 0.000030 0.0000096 33'44'5-PentaCB-(126) ng 0.16**~.035** 0.30 0.10 0.016 HexaCB-(156)+(157) ng 0.76**~.032** 0.60 0.000030 0.000023 23'44'55'-HexaCB-(167) ng 0.32 O.D35 0.30 0.000030 0.0000096 33'44'55'-HexaCB-(169) ng <0.036**~.036** 0.30 0.030 0.0011 233'44'55'-HeptaCB-(189) ng <0.029 0.029 0.30 0.000030 0.00000087 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.019 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 101 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 120 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 120 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 121 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 120 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 130 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 129 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 129 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 113 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 136 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 137 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 127 N/A N/A N/A N/A N/A =Not Applicable RDL 

### =Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch TEF 

### = Toxic Equivalency Factor, TEQ 

### = Toxic Equivalency Quotient, #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A
N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WvH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for**Dioxin~** and Dioxin-like Compounds

Page 7 of29 ·•

Maxxam Analytics lrnernational COrporation o/a Maxxam Analytics 6740 CampobeHo R<>att, Mlsslssauga. Onlario, L5N 2LB Tel: (905) 817·5700 Toll-Free: BOQ-563-6266 Fax: (905) 817·5777 www.maxxam.r.a

## Ma§am
Maxxam Job #: 8351227 Report Date: 2013/04/29 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1511**~ampling** Date 2013/03/15 00:01 

### toe Number N/A TOXIC EQUIVALENCY Units RUN EDL RDL TEF (2005 WHO) TEQ{DL) 3-BH5-M23/PCB 33'44'-TetraCB-(77) ng 6.6 0.054 0.30 0.00010 0.00066 344'5-TetraCB-(81) ng 0.42**~.055** 0.30 0.00030 0.00013 233'44'-PentaCB-(105) ng 6.2**~.037** 0.30 0.000030 0.00019 2344'5-PentaCB-(114) ng 0.51 0.035 0.30 0.000030 0.000015 23'44'5-PentaCB-(118) ng 17 0.038 0.30 0.000030 0.00051 23'44'5'-PentaCB-(123) ng 0.34 0.039 0.30 0.000030 0.000010 33'44'5-PentaCB-(126) ng 0.17 0.037 0.30 0.10 0.017 HexaCB-(156)+(157) ng 0.60 0.036 0.60 0.000030 0.000018 23'44'55'-HexaCB-(167) ng 0.23 0.038 0.30 0.000030 0.0000069 33'44'55'-HexaCB-(169) ng <0.040 0.040 0.30 0.030 0.0012 233'44'55'-HeptaCB-(189) ng <0.030 0.030 0.30 0.000030 0.00000090 TOTAL TOXIC EQUIVALENCY ng N/A N/A N/A N/A 0.020 Surrogate Recovery (%) C13-233'44'55'-HeptaCB-(189) % 95 N/A N/A N/A N/A C13-233'44'5-HexaCB-(156) % 114 N/A N/A N/A N/A C13-233'44'5'-HexaCB-(157) % 114 N/A N/A N/A N/A C13-233'44'-PentaCB-(105) % 113 N/A N/A N/A N/A C13-23'44'55'-HexaCB-(167) % 112 N/A N/A N/A N/A C13-2344'5-PentaCB-(114) % 118 N/A N/A N/A N/A C13-23'44'5-PentaCB-(118) % 119 N/A N/A N/A N/A C13-2'344'5-PentaCB-(123) % 114 N/A N/A N/A N/A C13-33'44'55'-HexaCB-(169) % 110 N/A N/A N/A N/A C13-33'44'5-PentaCB-(126) % 124 N/A N/A N/A N/A C13-33'44'-TetraCB-(77) % 121 N/A N/A N/A N/A C13-344'5-TetraCB-(81) % 112 N/A N/A N/A N/A N/A

## = Not Applicable RDL 

## = Reportable Detection Limit EDL

## =Estimated Detection Limit QC Batch 

## = Quality Control Batch #of somers

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A

N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A**~EF** 

## = Toxic Equivalency Factor, TEO

## = Toxic Equivalency Quotient,**~he** Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.QC Batch

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

N/A

3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506 3182506

WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dic>:'ns**E~c** Dioxin-like Compounds

Page8of29

1\!laxxam AnalyUcs lrnernational COrporatiOn o/a Maxxam Analytics 6740 C<mpObeHo Roao, MISSissauga, Ontario, L5N 2l.S Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777 W\V'N.maxxam.ca

# Ma?_(lam

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS {STACK SAMPLING TRAIN)
RC1495 2013/03/15

00:01 N/A TOXIC EQUIVALENCY #of Units TRAIN EDL RDL TEF (2005 WHO) fEQ(DL) somers BLANK-M23/PCB 2,3,7,8-Tetra COD* pg <3.7 3.7 30 1.00 3.70 N/A 1,2,3,7,8-Penta COD pg <7.7 7.7 30 1.00 7.70 N/A 1,2,3,4,7,8-Hexa COD pg <5.3 5.3 30 0.100 0.530 N/A 1,2,3,6,7,8-Hexa COD pg <5.2 5.2 30 0.100 0.520 N/A 1,2,3,7,8,9-Hexa COD pg <5.2 5.2 30 0.100 0.520 N/A 1,2,3,4,6,7,8-Hepta COD pg <6.4 6.4 30 0.0100 0.0640 N/A 1,2,3,4,6,7,8,9-0cta COD pg 8.2 (1) 5.2 300 0.000300 0.00246 N/A Total Tetra COD pg <3.7 3.7 30 N/A N/A N/A Total Penta COD pg <7.7 7.7 30 N/A N/A N/A Total Hexa COD pg <5.2 5.2 30 N/A N/A N/A Total Hepta COD pg <6.4 6.4 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <2.5 2.5 30 0.100 0.250 N/A 1,2,3,7,8-Penta CDF pg <7.6 7.6 30 0.0300 0.228 N/A 2,3,4,7,8-Penta CDF pg <7.2 7.2 30 0.300 2.16 N/A 1,2,3,4,7,8-Hexa CDF pg <3.9 3.9 30 0.100 0.390 N/A 1,2,3,6,7,8-Hexa CDF pg <3.8 3.8 30 0.100 0.380 N/A 2,3,4,6,7,8-Hexa CDF pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,7,8,9-Hexa CDF pg <5.3 5.3 30 0.100 0.530 N/A 1,2,3,4,6,7,8-Hepta CDF pg <2.9 2.9 30 0.0100 0.0290 N/A 1,2,3,4,7,8,9-Hepta CDF pg <4.0 4.0 30 0.0100 0.0400 N/A 1,2,3,4,6,7,8,9-0cta CDF pg <5.2 5.2 300 0.000300 0.00156 N/A Total Tetra CDF pg <2.5 2.5 30 N/A N/A N/A Total Penta CDF pg <7.4 7.4 30 N/A N/A N/A Total Hexa CDF pg <4.4 4.4 30 N/A N/A N/A Total Hepta CDF pg <3.4 3.4 30 N/A N/A N/A N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD =Chloro Dibenzo-p-Dioxin, •• CDF =Chloro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEO = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency F;;ctors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 9 of29

Ma:<xam Analytics lrnernational corporation o/a Maxxam Analytlcs 6740 CampoDeQo Road, MJsslssauga. Ontario, L5N as Tel: (905) 817-5700 Toll-Free: aoo-563·6266 Fax: (905) 817-5777 wwwmaxxam.ca

## M 

# azS}la m

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COG Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1495 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units TRAIN EDL RDL TEF (2005 WHO) rEQ(DL) somers BLANK·M23/PCB TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 17.5 N/A Surrogate Recovery (%) C13-1234678 HeptaCDD * % 125 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF ** % 130 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 93 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 101 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 85 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 76 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 73 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 44 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 49 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 73 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 99 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 60 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 88 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 120 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 129 N/A N/A N/A N/A N/A N/

A 

### =Not Applicable RDL 

### =Reportable Detection Limit EDL

### =Estimated Detection Limit QC Batch 

### = Quality Control Batch * COD 

### = Chiaro Dibenzo-p-Dioxin, ** CDF

### = Chiaro Dibenzo-p-Furan TEF 

### = Toxic Equivalency Factor, TEO

### = Toxic Equivalency Quotient, QC Batch

N/A

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 10 of29

Ma<Xam Analytics lrnernational COrporation o/a Maxxam**Anal~'tics** 6740 campobello Road. Mlssissauga. Ontario. L5N 2L8 Tel: (905) 817-5700 Toll-Free: SOD-563-6266 Fax: {905) 817-5777 www.maxxam.ca

# 1\/la&arn
Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID !Sampling Date COC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC. -FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1497 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)TEQ(DL) somers 1·BH2-M23/PCB 2,3,7,8-Tetra COD* pg <3.3 3.3 30 1.00 3.30 N/A 1,2,3,7,8-Penta COD pg <3.5 3.5 30 1.00 3.50 N/A 1,2,3,4,7,8-Hexa COD pg <4.9 4.9 30 0.100 0.490 N/A 1,2,3,6,7,8-Hexa COD pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,7,8,9-Hexa COD pg <4.8 4.8 30 0.100 0.480 N/A 1,2,3,4,6,7,8-Hepta COD pg 15.8 5.8 30 0.0100 0.158 N/A 1,2,3,4,6,7,8,9-0cta COD pg 30.4 5.3 300 0.000300 0.00912 N/A Total Tetra COD pg 123 3.3 30 N/A N/A N/A Total Penta COD pg 8.0 3.5 30 N/A N/A N/A Total Hexa COD pg 21.2 4.9 30 N/A N/A N/A Total Hepta COD pg 36.6 5.8 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <190 (1) 190 30 0.100 19.0 N/A 1,2,3,7,8-Penta CDF pg 21.2 4.6 30 0.0300 0.636 N/A 2,3,4,7,8-Penta CDF pg 23.4 (2) 4.4 30 0.300 7.02 N/A 1,2,3,4,7,8-Hexa CDF pg 33.3 3.2 30 0.100 3.33 N/A 1,2,3,6,7,8-Hexa CDF pg 15.1 3.1 30 0.100 1.51 N/A 2,3,4,6,7,8-Hexa CDF pg 12.2 3.9 30 0.100 1.22 N/A 1,2,3,7,8,9-Hexa CDF pg <4.4 4.4 30 0.100 0.440 N/A 1,2,3,4,6,7,8-Hepta CDF pg 25.7 3.4 30 0.0100 0.257 N/A 1,2,3,4,7,8,9-Hepta CDF pg <4.6 4.6 30 0.0100 0.0460 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 16.1 (2) 5.2 300 0.000300 0.00483 N/A Total Tetra CDF pg 1210 5.3 30 N/A N/A N/A Total Penta CDF pg 329 4.5 30 N/A N/A N/A Total Hexa CDF pg 124 3.6 30 N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, 

### pc Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. !wH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) RT > 3 seconds- PCDD/DF analysis- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 2) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 11 of29

Ma'xam Analylics lrnernalional COrporatiOn o/a Ma""am Analy1ics 6740 CampobeRo Road, MISSISsauga, Ontario, L51\1 21.8 Tel: (905) 817-5700 TOII·Free: 800.563·6266 Fax: (905) 817·5777 www.maxxam.ca

## Ma'§am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date

OC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244 DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN) RC1497 2013/03/19

00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) fEQ(DL) somers 1-BH2-M23/PCB Total Hepta CDF ** pg 34.9 3.9 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 39.8 3.2 30 0.100 3.98 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 26.9 N/A Surrogate Recovery (%} Confirmation C13-2378 TetraCDF % 78 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 112 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 115 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 93 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 103 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 91 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 80 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 79 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 77 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 86 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 77 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 97 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 66 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 90 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 112 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 127 N/A N/A N/A N/A N/A N/A

### =Not Applicable RDL 

### =Reportable Detection Limit EDL 

### =Estimated Detection Limit QC Batch 

### =Quality Control Batch • COD 

### = Chloro Dibenzo-p-Dioxin, ** CDF

### =Chloro Dibenzo-p-Furan TEF 

### = Toxic Equivalency Factor, TEQ

### = Toxic Equivalency Quotient, QC Batch

3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 12 of29

1\!la'Xam Analylocs lrnernational COrporation o/a Maxxarn**Anal~'lics** 6740 C<mpobello Road, MlssiSS8!JIIll, Ontario, L5N 2LB Tel: (905) 817-5700 TOll-Free: BOo-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## 1\./1 

## a 

# ({)2a m
Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date

OC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1498 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) fEQ(DL) somers 2-BH2-M23/PCB 2,3,7,8-Tetra CDD * pg <3.7 3.7 30 1.00 3.70 N/A 1,2,3,7,8-Penta CDD pg <3.6 3.6 30 1.00 3.60 N/A 1,2,3,4,7,8-Hexa CDD pg <3.6 3.6 30 0.100 0.360 N/A 1,2,3,6,7,8-Hexa CDD pg <3.4 3.4 30 0.100 0.340 N/A 1,2,3,7,8,9-Hexa CDD pg <3.5 3.5 30 0.100 0.350 N/A 1,2,3,4,6,7,8-Hepta CDD pg <3.5 3.5 30 0.0100 0.0350 N/A 1,2,3,4,6,7,8,9-0cta CDD pg 12.3 4.1 300 0.000300 0.00369 N/A Total Tetra CDD pg 16.1 3.7 30 N/A N/A N/A Total Penta CDD pg <4.0 (1) 4.0 30 N/A N/A N/A Total Hexa CDD pg <9.6 (1) 9.6 30 N/A N/A N/A Total Hepta CDD pg <3.5 3.5 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg**<53~** 53 30 0.100 5.30 N/A 1,2,3,7,8-Penta CDF pg 5.9 3.5 30 0.0300 0.177 N/A 2,3,4,7,8-Penta CDF pg 6.0 3.3 30 0.300 1.80 N/A 1,2,3,4,7,8-Hexa CDF pg 8.0 3.4 30 0.100 0.800 N/A 1,2,3,6,7,8-Hexa CDF pg <3.2 3.2 30 0.100 0.320 N/A 2,3,4,6,7,8-Hexa CDF pg <4.1 4.1 30 0.100 0.410 N/A 1,2,3,7,8,9-Hexa CDF pg <4.5 4.5 30 0.100 0.450 N/A 1,2,3,4,6,7,8-Hepta CDF pg 5.9@) 2.3 30 0.0100 0.0590 N/A 1,2,3,4,7,8,9-Hepta CDF pg <3.1 3.1 30 0.0100 0.0310 N/A 1,2,3,4,6,7,8,9-0cta CDF pg <5.3 5.3 300 0.000300 0.00159 N/A Total Tetra CDF pg 335 4.5 30 N/A N/A N/A Total Penta CDF pg 67.8 3.4 30 N/A N/A N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * CDD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organizaticr., Human and Mammalian Toxic Equiva!ency Factors for Dioxins &.:c Dioxin-like Compounds ( 1 ) EMPC I NDR
- Peak detected does net rr:eet ratio criteria and has resulted in an elevated detection limit. ( 2) RT > 3 seconds- PCDD/DF analysis- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 3) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 13 of29

Mauam Analylics Jrnernational Corporation o!a Maxxam Analytics 6740 campobello Road, MlssissaJga, Onlario, L5N 2LB Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?§2am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1498 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 2-BH2-M23/PCB Total Hexa CDF ** pg 18.3 3.7 30 N/A N/A N/A Total Hepta CDF pg 5.9 (1) 2.6 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 10.1 3.4 30 0.100 1.01 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 13.4 N/A Surrogate Recovery(%) Confirmation C13-2378 TetraCDF 'Yo 76 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * 'Yo 119 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF 'Yo 111 N/A N/A N/A N/A N/A C13-123478 HexaCDD 'Yo 106 N/A N/A N/A N/A N/A C13-123478 HexaCDF 'Yo 107 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF 'Yo 89 N/A N/A N/A N/A N/A C13-123678 HexaCDD 'Yo 73 N/A N/A N/A N/A N/A C13-123678 HexaCDF 'Yo 77 N/A N/A N/A N/A N/A C13-12378 PentaCDD o/o 88 N/A N/A N/A N/A N/A C13-12378 PentaCDF 'Yo 93 N/A N/A N/A N/A N/A C13-123789 HexaCDF 'Yo 75 N/A N/A N/A N/A N/A C13-23478 PentaCDF 'Yo 99 N/A N/A N/A N/A N/A C13-2378 TetraCDD 'Yo 65 N/A N/A N/A N/A N/A C13-2378 TetraCDF 'Yo 85 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin 'Yo 105 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD 'Yo 129 N/A N/A N/A N/A N/A N/A =NotApplicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chiaro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEQ =Toxic Equivalency Quotient, QC Batch

3190066 3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Marnm&:'an Toxic**Equiv&i~·** :•1 Factors for [.,cxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 14 of29 ' 

# I

1\ilaxxam Analytics International COrporation ola Maxxam AnalytiGs 6740 GampobeHo Road, Mlssissauga. Ontario, LSN 2L8 Tel: (905) 817-5700 Toll-Free: 800-563·6266 Fax: (905) 817·5777 wvvw.mal<xam.oa

## Ma({)2am
Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID**~ampling** Date COG Number Keika Ventures Client Project #: Tl1550 Site location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1499 2013103119 00:01 NIA TOXIC EQUIVALENCY #of Units RUN IEDL RDL TEF (2005 WHO) fEQ(DL) somers 3-BH2-M23/PCB 2,3,7,8-Tetra COD* pg <4.1 4.1 30 1.00 4.10 NIA 1,2,3,7,8-Penta COD pg <4.1 4.1 30 1.00 4.10 NIA 1,2,3,4,7,8-Hexa COD pg <3.9 3.9 30 0.100 0.390 NIA 1,2,3,6,7,8-Hexa COD pg <3.8 3.8 30 0.100 0.380 NIA 1,2,3,7,8,9-Hexa COD pg <3.8 3.8 30 0.100 0.380 NIA 1,2,3,4,6,7,8-Hepta COD pg <3.2 3.2 30 0.0100 0.0320 NIA 1,2,3,4,6,7,8,9-0cta COD pg 7.7 3.3 300 0.000300 0.00231 N/A Total Tetra COD pg 24.8 4.1 30 NIA N/A N/A Total Penta COD pg 4.9 4.1 30 NIA N/A N/A Total Hexa COD pg <9.8 (1) 9.8 30 N/A NIA N/A Total Hepta COD pg <3.2 3.2 30 NIA NIA N/A 2,3,7,8-Tetra CDF ** pg <78 (2) 78 30 0.100 7.80 N/A 1,2,3,7,8-Penta CDF pg 9.7 4.4 30 0.0300 0.291 N/A 2,3,4,7,8-Penta CDF pg 12.6 4.2 30 0.300 3.78 N/A 1,2,3,4,7,8-Hexa CDF pg <13@) 13 30 0.100 1.30 N/A 1,2,3,6,7,8-Hexa CDF pg <5.2@) 5.2 30 0.100 0.520 NIA 2,3,4,6,7,8-Hexa CDF pg <4.1 4.1 30 0.100 0.410 N/A 1,2,3,7,8,9-Hexa CDF pg <4.5 4.5 30 0.100 0.450 N/A 1,2,3,4,6,7,8-Hepta CDF pg 7.2 (4) 2.9 30 0.0100 0.0720 N/A 1,2,3,4,7,8,9-Hepta CDF pg <4.0 4.0 30 0.0100 0.0400 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 5.3 3.6 300 0.000300 0.00159 N/A Total Tetra CDF pg 455 2.9 30 N/A NIA N/A N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, 

## pc Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I NOR
- Peak detected does not meet ratio criteria and has resulted in an elevated detection limit. ( 2) RT > 3 seconds
- PCDD/DF analysis
- Peak detected exceeds expected retention time (from internal standard) by greater than 3 seconds. ( 3) EMPC I OPE
- Diphenylether interierence present caused dibenzofuran detected to become a "non-detect" with an elevated detection limit. ( 4) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 15of29

Ma'Xam Analytics lrnerna1i<lnal COrporation 0/a Maxxarn**Anal~'1ics** 6740 C;mpobello Roa<l, Mlsslssauga, Ontario, L5N 21..8 Tel: (905) 817-5700 Toii-Ftee: BOQ-563-6266 Fax: {905) 817-5777 www.maxxarn.ca

## J\/ie:l"§am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1499 2013/03/19 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) ITEQ(DL) somers 3-BH2-M23/PCB Total Penta CDF ** pg 126 4.3 30 N/A N/A N/A Total Hexa CDF pg 15.6 3.7 30 N/A N/A N/A Total Hepta CDF pg 7.2 (1) 3.4 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 15.0 3.0 30 0.100 1.50 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 17.7 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 71 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 97 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 101 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 99 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 96 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 93 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 73 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 81 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 84 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 83 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 76 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 105 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 57 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 77 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 98 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 124 N/A N/A N/A N/A N/A N/A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chiaro Dibenzo-p-Dioxin, ** CDF = Chiaro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEO = Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

lfhe Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 16 of29

1\/ia<Xam Analytlcs ltnernatlonal COrporatiOn o/a Maxxam Analytlcs 6740 C<mpobeiiO Aoa!l, MIS&ISsauga. Ontario, L5N :21.6 Tel: (905) 817·6700 Toll.f'ree: SfJ0-563-6266 fax: (905) 817-5777www.ma.xam.caMaxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam 10 Sampling Date 

### r.oc Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1500 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 1·BH5-M23/PCB 2,3,7,8-Tetra COD* pg 6.7 (1} 3.5 30 1.00 6.70 N/A 1,2,3,7,8-Penta COD pg 3.5 2.8 30 1.00 3.50 N/A 1,2,3,4,7,8-Hexa COD pg <3.2 3.2 30 0.100 0.320 N/A 1,2,3,6,7,8-Hexa COD pg <3.1 3.1 30 0.100 0.310 N/A 1,2,3,7,8,9-Hexa COD pg <3.2 3.2 30 0.100 0.320 N/A 1,2,3,4,6,7,8-Hepta COD pg 5.2 (1} 3.4 30 0.0100 0.0520 N/A 1,2,3,4,6,7,8,9-0cta COD pg 11.9 (1} 3.1 300 0.000300 0.00357 N/A !Total Tetra COD pg 121 3.5 30 N/A N/A N/A Total Penta COD pg 31.8 2.8 30 N/A N/A N/A Total Hexa COD pg 11.8 3.2 30 N/A N/A N/A Total Hepta COD pg 10.8 3.4 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg 220 3.1 30 0.100 22.0 N/A 1,2,3,7,8-Penta CDF pg 23.7 3.6 30 0.0300 0.711 N/A 2,3,4,7,8-Penta CDF pg 20.6 3.5 30 0.300 6.18 N/A 1,2,3,4,7,8-Hexa CDF pg 13.0 2.8 30 0.100 1.30 N/A 1,2,3,6,7,8-Hexa CDF pg 5.5 2.7 30 0.100 0.550 N/A 2,3,4,6,7,8-Hexa CDF pg <3.4 3.4 30 0.100 0.340 N/A 1,2,3,7,8,9-Hexa CDF pg <3.8 3.8 30 0.100 0.380 N/A 1,2,3,4,6,7,8-Hepta CDF pg 4.6 (1} 2.6 30 0.0100 0.0460 N/A 1,2,3,4,7,8,9-Hepta CDF pg <3.5 3.5 30 0.0100 0.0350 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 4.5 (1} 3.5 300 0.000300 0.00135 N/A jTotal Tetra CDF pg 1560 3.1 30 N/A N/A N/A Total Penta CDF pg 396 3.6 30 N/A N/A N/A Total Hexa CDF pg 46.1 3.1 30 N/A N/A N/A Total Hepta CDF pg 4.6 (1} 3.0 30 N/A N/A N/A N/A

## =Not Applicable RDL 

## =Reportable Detection Limit EDL

## =Estimated Detection Limit QC Batch 

## = Quality Control Batch * COD 

## = Chloro Dibenzo-p-Dioxin, ** CDF

## = Chloro Dibenzo-p-Furan TEF

## = Toxic Equivalency Factor, TEO

## = Toxic Equivalency Quotient,**~c** Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO} value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical

Page 17 of29

1\/laxxam Analytics International COrporation o/a Maxxam Analytios 6740 C<impobaRo Road, Mlsslssauga, Ontario, L5N 21..8 Tel: (905) 817·5700 Toll-free: SOD-563·6266 Fax: (905) 817·5777 www.maxxam.caMaxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam 10**~ampling** Date**~oc** Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1500 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF {2005 WHO) ITEQ{DL) somers 1-BH5-M23/PCB Confirmation 2,3,7,8-Tetra CDF •• pg 54.4 3.2 30 0.100 5.44 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 26.2 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 65 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD • % 96 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 107 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 106 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 104 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 89 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 91 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 89 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 88 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 84 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 80 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 114 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 58 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 71 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 108 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 127 N/A N/A N/A N/A N/A N/A = NotApplicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch • COD =Chiaro Dibenzo-p-Dioxin,

.. CDF =Chiaro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, QC Batch

3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

!The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 18 of29

Ma<Xam Analylics lrnernatiOnal COrporatiOn o/a Maxxam**Anal~'lics** 6740 campobello Road, Mlsslssauga, OntariO, L5N 21..8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date

OC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS {STACK SAMPLING TRAIN) RC1505 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 2·BH5·M23/PCB 2,3,7,8-Tetra COD* pg 11.9 (1) 4.1 30 1.00 11.9 N/A 1,2,3,7,8-Penta COD pg 7.8 (1) 3.6 30 1.00 7.80 N/A 1,2,3,4,7,8-Hexa COD pg 4.5 3.2 30 0.100 0.450 N/A 1,2,3,6,7,8-Hexa COD pg 5.6 3.1 30 0.100 0.560 N/A 1,2,3,7,8,9-Hexa COD pg 6.0 3.2 30 0.100 0.600 N/A 1,2,3,4,6,7,8-Hepta COD pg 13.7 2.6 30 0.0100 0.137 N/A 1,2,3,4,6,7,8,9-0cta COD pg 37.8 5.4 300 0.000300 0.0113 N/A Total Tetra COD pg 194 4.1 30 N/A N/A N/A Total Penta COD pg 79.7 3.6 30 N/A N/A N/A Total Hexa COD pg 27.4 3.2 30 N/A N/A N/A Total Hepta COD pg 25.1 2.6 30 N/A N/A N/A 2,3,7,8-Tetra CDF ** pg <260 (2) 260 30 0.100 26.0 NIA 1,2,3,7,8-Penta CDF pg 32.9 4.9 30 0.0300 0.987 N/A 2,3,4,7,8-Penta CDF pg 28.7 4.6 30 0.300 8.61 N/A 1,2,3,4,7,8-Hexa CDF pg 20.2 (3) 3.6 30 0.100 2.02 NIA 1,2,3,6,7,8-Hexa CDF pg 11.3 (1) 3.4 30 0.100 1.13 NIA 2,3,4,6,7,8-Hexa CDF pg 8.4 4.3 30 0.100 0.840 NIA 1,2,3,7,8,9-Hexa CDF pg <4.8 4.8 30 0.100 0.480 NIA 1,2,3,4,6,7,8-Hepta CDF pg 10.9 (1) 2.6 30 0.0100 0.109 N/A 1,2,3,4,7,8,9-Hepta CDF pg <3.6 3.6 30 0.0100 0.0360 N/A 1,2,3,4,6,7,8,9-0cta CDF pg 17.5 3.5 300 0.000300 0.00525 N/A Total Tetra CDF pg 1830 3.5 30 N/A N/A N/A Total Penta CDF pg 465 4.8 30 N/A N/A N/A Nl

A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch • COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEO= Toxic Equivalency Quotient, QC Batch

3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical ( 2) RT > 3 seconds- PCDDIDF analysis- Peak detected exceeds expected retention time (from internal standara) 'Jy greater than 3 seconds. ( 3) EMPC I Merged Peak

Page 19 of29 

# i

1\!la'Xam Analytics lrrternational corporation o/a Maxxam**Anal~"tics** 6740 canpoballo Road, Mlsslssauga, Onlario, L5N 2L8 Tel: (905) 817·5700 Toii·Free: 800.563·6266 Fax: (905) 817·5777 www.maxxam.ca

# Ma1))i.arn

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam 10 Sampling Date 

### toe Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN) RC1505 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN fi=DL RDL TEF (2005 WHO) rreQ{DL) somers 2-BH5-M23/PCB Total Hexa CDF •• pg 77.5 4.0 30 N/A N/A N/A Total Hepta CDF pg 10.9 (1) 3.0 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 68.7 6.5 30 0.100 6.87 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 42.5 N/A Surrogate Recovery(%) Confirmation C13-2378 TetraCDF % 53 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 99 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 100 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 104 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 105 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 88 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 79 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 77 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 75 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 66 N/A N/A N/A N/A N/A C13-123789 HexaCDF % 73 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 134 (2) N/A N/A N/A N/A N/A C13-2378 TetraCDD % 49 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 53 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 98 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 165 (2) N/A N/A N/A N/A N/A N/

A = Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch * COD = Chiaro Dibenzo-p-Dioxin, ** CDF = Chiaro Dibenzo-p-Furan TEF =Toxic Equivalency Factor, TEO= Toxic Equivalency Quotient,**~c** Batch

3190066 3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEO) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical ( 2) Field spike exceeds upper control limit (70-130%)

Page20of29

Ma:<xam AnalyliGs lrnernationat COrporation o/a Maxxam Anal}"tics 6740 C<mpobello Road, Mlssissauga, Onlario,l5N 2LB Tel: (905) 817-5700 Toll-free: BD0-563-6266 Fax: (905) 817-5777wwwmaxxam.ca

# Ma~am Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam 10 Sampling Date

OC Number Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1511 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO) rrEQ(DL) somers QC Batch 3-BH5-M23/PCB 2,3,7,8-Tetra COD* pg 9.5 (1) 3.5 30 1.00 9.50 N/A 3190066 1,2,3,7,8-Penta COD pg 6.6 3.4 30 1.00 6.60 N/A 3190066 1,2,3,4,7,8-Hexa COD pg <3.3 3.3 30 0.100 0.330 N/A 3190066 1,2,3,6,7,8-Hexa COD pg <3.2 3.2 30 0.100 0.320 N/A 3190066 1,2,3,7,8,9-Hexa COD pg 4.6 3.2 30 0.100 0.460 N/A 3190066 1,2,3,4,6,7,8-Hepta COD pg 5.9 (1) 3.1 30 0.0100 0.0590 N/A 3190066 1,2,3,4,6,7,8,9-0cta COD pg 26.5 (1) 4.7 300 0.000300 0.00795 N/A 3190066 Total Tetra COD pg 326 3.5 30 N/A N/A N/A 3190066 Total Penta COD pg 105 3.4 30 N/A N/A N/A 3190066 Total Hexa COD pg 4.6 3.3 30 N/A N/A N/A 3190066 Total Hepta COD pg 5.9 (1) 3.1 30 N/A N/A N/A 3190066 2,3,7,8-Tetra CDF •• pg <460 (2) 460 30 0.100 46.0 N/A 3190066 1,2,3,7,8-Penta CDF pg 46.3 3.8 30 0.0300 1.39 N/A 3190066 2,3,4,7,8-Penta CDF pg 38.1 3.6 30 0.300 11.4 N/A 3190066 1,2,3,4,7,8-Hexa CDF pg 26.8 2.5 30 0.100 2.68 N/A 3190066 1,2,3,6,7,8-Hexa CDF pg 13.4 2.3 30 0.100 1.34 N/A 3190066 2,3,4,6,7,8-Hexa CDF pg 5.1 3.0 30 0.100 0.510 N/A 3190066 1,2,3,7,8,9-Hexa CDF pg <3.3 3.3 30 0.100 0.330 N/A 3190066 1,2,3,4,6,7,8-Hepta CDF pg 10.1 (1) 3.7 30 0.0100 0.101 N/A 3190066 1,2,3,4,7,8,9-Hepta CDF pg <5.0 5.0 30 0.0100 0.0500 N/A 3190066 1,2,3,4,6,7,8,9-0cta CDF pg 33.6 5.2 300 0.000300 0.0101 N/A 3190066 Total Tetra CDF pg 3230 4.0 30 N/A N/A N/A 3190066 Total Penta CDF pg 757 3.7 30 N/A N/A N/A 3190066 Total Hexa CDF pg 118 2.7 30 N/A N/A N/A 3190066 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch • COD = Chloro Dibenzo-p-Dioxin, ** CDF = Chloro Dibenzo-p-Furan TEF = Toxic Equivalency Factor, TEQ = Toxic Equivalency Quotient, The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested. WH0(2005): The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds ( 1 ) EMPC I Ratio
- Isotopic ratio adjusted to meet theoretical ( 2) RT > 3 seconds
- PCDD/DF analysis
- Peak detected exceed:; expected retention time (from ir.tu'lal s:.:c ;<;ard) by greater than 3 seconds.

Page 21 of29 

### I 

# I

1\ilaxxam Analy!ics ltnernational Corporation o!a Maxxam Analytics 6740 Canpobello Road, Mlssissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma-62am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID Sampling Date COC Number Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
DIOXINS AND FURANS BY HRMS (STACK SAMPLING TRAIN)
RC1511 2013/03/15 00:01 N/A TOXIC EQUIVALENCY #of Units RUN EDL RDL TEF (2005 WHO)**~EQ(DL)** somers 3-BH5-M23/PCB Total Hepta CDF •• pg 16.3 4.2 30 N/A N/A N/A Confirmation 2,3,7,8-Tetra CDF pg 96.0 3.4 30 0.100 9.60 N/A TOTAL TOXIC EQUIVALENCY pg N/A N/A N/A N/A 44.7 N/A Surrogate Recovery (%) Confirmation C13-2378 TetraCDF % 71 N/A N/A N/A N/A N/A C13-1234678 HeptaCDD * % 104 N/A N/A N/A N/A N/A C13-1234678 HeptaCDF % 118 N/A N/A N/A N/A N/A C13-123478 HexaCDD % 109 N/A N/A N/A N/A N/A C13-123478 HexaCDF % 104 N/A N/A N/A N/A N/A C13-1234789 HeptaCDF % 85 N/A N/A N/A N/A N/A C13-123678 HexaCDD % 79 N/A N/A N/A N/A N/A C13-123678 HexaCDF % 85 N/A N/A N/A N/A N/A C13-12378 PentaCDD % 81 N/A N/A N/A N/A N/A C13-12378 PentaCDF % 86 NIA N/A N/A N/A N/A C13-123789 HexaCDF % 82 N/A N/A N/A N/A N/A C13-23478 PentaCDF % 98 N/A N/A N/A N/A N/A C13-2378 TetraCDD % 59 N/A N/A N/A N/A N/A C13-2378 TetraCDF % 76 N/A N/A N/A N/A N/A C13-0ctachlorodibenzo-p-Dioxin % 95 N/A N/A N/A N/A N/A Cl37-2378 TetraCDD % 125 N/A N/A N/A N/A N/A N/A

### =Not Applicable RDL 

### =Reportable Detection Limit EDL

### =Estimated Detection Limit QC Batch 

### = Quality Control Batch * COD 

### = Chloro Dibenzo-p-Dioxin, ** CDF

### = Chloro Dibenzo-p-Furan TEF 

### = Toxic Equivalency Factor, TEQ

### = Toxic Equivalency Quotient, 

### pc Batch

3190066 3191218

N/A

3191218 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066 3190066

The Total Toxic Equivalency (TEQ) value reported is the sum ofToxic Equivalent Quotients for the congeners tested.**~H0(2005):** The 2005 World Health Organization, Human and Mammalian Toxic Equivalency Factors for Dioxins and Dioxin-like Compounds

Page 22 of29

Ma.<xam Analy!ics lrnernational COrporation o/a Maxxam Analytics 6740 Gampobello Road, MlssiSsauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma({)2.am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID RC1495 Sample ID TRAIN BLANK-M23/PCB Matrix Stack Sampling Train

Maxxam ID RC1497 Sample ID RUN 1-BH2-M23/PCB Matrix Stack Sampling Train Test Description 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air(1668A)

Test Maxxam ID RC1498 Sample ID RUN 2-BH2-M23/PCB Matrix Stack Sampling Train Descr1pt1on 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A)

Maxxam ID RC1499 Sample ID RUN 3-BH2-M23/PCB Matrix Stack Sampling Train Test Description 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A)
Maxxam ID RC1500 Sample ID RUN 1-BH5-M23/PCB Matrix Stack Sampling Train Test Description 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Congeners in Air (1668A) Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Instrumentation Batch Extracted HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Instrumentation Batch Extracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

I t t 

### r ns rumen a 1on B t h ac E tract d X e HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Instrumentation B h ate E xtracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Instrumentation Batch Extracted HRMS/MS 3191218 N/A HRMS/MS 3190066 2013/04/16 HRMS/MSEC 3182506 2013/04/16

Page23 of29 Analyzed 2013/04/24 2013/04/25 2013/04/24

A I d

na1yze 2013/04/24 2013/04/25 2013/04/24

A I d

na1yze 2013/04/24 2013/04/25 2013/04/24 Collected 2013/03/15 Shipped Received 2013/04/06

Collected 2013/03/19

Shipped Received 2013/04/06 Analyst Vica Cioranic OwenCosbv Cathv Xu
Collected 2013/03/19

Shipped Received 2013/04/06

A I t

na1ys Vica Cioranic Owen Cosby Cathy Xu
Collected 2013/03/19

Shipped Received 2013/04/06 A I

na1yst Vica Cioranic Owen Cosby Cathy Xu
Collected 2013/03/15

Shipped Received 2013/04/06 na1vze nalyst A I d A I 2013/04/24 Vica Cioranic 2013/04/25 OwenCosbv 2013/04/24 Cathv Xu

Ma<xam Analytics lrtternational COrporation o/a Maxxam Analytics 6740 campobello Roall, MISSiSSauga, Ontario, L5N 2L8 Tel: (905i 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777 www.maxxam.ca

### 1\/f 

# a 

# (!52.am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Maxxam ID RC1505 Sample ID RUN 2-BH5-M23/PCB Matrix Stack Sampling Train Test Description 2 3 7 8-TCDF Confirmation (M23) Dioxins/Furans in Air (Method 23) PCB Conqeners in Air (1668A)

Maxxam ID RC1511 Sample ID RUN 3-BH5-M23/PCB Matrix Stack Sampling Train Test DescriPtion 12 3 7 8-TCDF Confirmation (M23) IDioxins/Furans in Air (Method 23) (PCB Conaeners in Air (1668A) Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Collected 2013/03/15 Shipped Received 2013/04/06 Instrumentation Batch Extracted Analyzed Analyst HRMS/MS 3191218 N/A 2013/04/24 Vica Cioranic HRMS/MS 3190066 2013/04/16 2013/04/25 Owen Cosby HRMS/MSEC 3182506 2013/04/16 2013/04/24 Cathy Xu
Collected 2013/03/15

Shipped Received 2013/04/06 Instrumentation Batch Extracted Analvzed Analyst HRMS/MS 3191218 N/A 2013/04/24 Vica Cioranic HRMS/MS 3190066 2013/04/16 2013/04/25 Owen Cosby HRMS/MSEC 3182506 2013/04/16 2013/04/24 CathvXu

Page24 of29 I 

### I I

Ma><xam Analyllcs lnternauonal corporatiOn ota l\llaxxam**AnalytiC~~** 6740 C;mpoDBDo Roall, M!$Siisauga, Ontario, L5N as Tel: (905) 817·5700 Tofi·Free: 80()-563·6266 Fax: (905) 817·5777 www.maxxam.oa

## Ma§am

Maxxam Job #: 8351227 Report Date: 2013/04/29

Results relate onlyto the items tested. Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244

GENERAL COMMENTS

Page25of29

Ma'xam Analylics International COr!JGration o/a Maxxam Analytlcs 5740 campobello Roaa, MlssiSSa!J;Ia, Ontarlo,L5N 21.8 Tel: (905) 817·5700 Toll-Free: 800.563-6266 fax: (905) 817-5777 www.maxxam.ca

# Maf9am

QA/QC Batch Num lnit QC Tvoe 3182506 

### cxu Spiked Blank

RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Method Blank Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS Quality Assurance Report Maxxam Job Number: GB351227 Date Analyzed Parameter ww/mm/dd C13-233'44'55'-HeptaCB-(189) 2013/04/24 C13-233'44'5-HexaCB-(156) 2013/04/24 C13-233'44'5'-HexaCB-(157) 2013/04/24 C13-233'44'-PentaCB-(105) 2013/04/24 C13-23'44'55'-HexaCB-(167) 2013/04/24 C13-2344'5-PentaCB-(114) 2013/04/24 C13-23'44'5-PentaCB-(118) 2013/04/24 C13-2'344'5-PentaCB-(123) 2013/04/24 C13-33'44'55'-HexaCB-(169) 2013/04/24 C13-33'44'5-PentaCB-(126) 2013/04/24 C13-33'44'-TetraCB-(77) 2013/04/24 C13-344'5-TetraCB-(81) 2013/04/24 33'44'-TetraCB-(77) 2013/04/24 33'44'-TetraCB-(77) 2013/04/24 344'5-TetraCB-(81) 2013/04/24 344'5-TetraCB-(81) 2013/04/24 233'44'-PentaCB-(105) 2013/04/24 233'44'-PentaCB-(105) 2013/04/24 2344'5-PentaCB-(114) 2013/04/24 2344'5-PentaCB-(114) 2013/04/24 23'44'5-PentaCB-(118) 2013/04/24 23'44'5-PentaCB-(118) 2013/04/24 23'44'5'-PentaCB-(123) 2013/04/24 23'44'5'-PentaCB-(123) 2013/04/24 33'44'5-PentaCB-(126) 2013/04/24 33'44'5-PentaCB-(126) 2013/04/24 HexaCB-(156)+(157) 2013/04/24 HexaCB-(156)+(157) 2013/04/24 23'44'55'-HexaCB-(167) 2013/04/24 23'44'55'-HexaCB-(167) 2013/04/24 33'44'55'-HexaCB-(169) 2013/04/24 33'44'55'-HexaCB-(169) 2013/04/24 233'44'55'-HeptaCB-(189) 2013/04124 233'44'55'-HeptaCB-(189) 2013/04/24 C13-233'44'55'-HeptaCB-(189) 2013/04124 C13-233'44'5-HexaCB-(156) 2013/04124 C13-233'44'5'-HexaCB-(157) 2013/04/24 C13-233'44'-PentaCB-(105) 2013/04/24 C13-23'44'55'-HexaCB-(167) 2013/04/24 C13-2344'5-PentaCB-(114) 2013/04/24 C13-23'44'5-PentaCB-(118) 2013/04/24 C13-2'344'5-PentaCB-(123) 2013/04/24 C13-33'44'55'-HexaCB-(169) 2013/04/24 C13-33'44'5-PentaCB-(126) 2013/04/24 C13-33'44'-TetraCB-(77) 2013/04/24 C13-344'5-TetraCB-(81) 2013/04/24 33'44'-TetraCB-(77) 2013/04/24 344'5-TetraCB-(81) 2013/04/24 233'44'-PentaCB-(105) 2013/04/24 2344'5-PentaCB-(114) 2013/04/24 23'44'5-PentaCB-(118) 2013/04/24 23'44'5'-PentaCB-(123) 2013/04/24 33'44'5-PentaCB-(126) 2013/04/24 HexaCB-(156)+(157) 2013/04/24 23'44'55'-HexaCB-(167) 2013/04/24

Page 26 of29 Value %Recoverv 98 108 108 111 107 108 108 107 104 120 112 107 98 0 99 0 99 1.0 96 1.0 98 3.0 99 1.0 93 4.2 100 1.0 100

0 102 0 93 2.1 102 115 115 115 111 115 113 113 106 123 116 113 <0.037, EDL=0.037 <0.037, EDL=0.037 <0.030, EDL=0.030 <0.028, EDL=0.028 <0.030, EDL=0.030 <0.031, EDL=0.031 <0.029, EDL=0.029 <0.036, EDL=0.036 <0.039, EDL=0.039 Units QC Limits % 20-150 % 20-150 % 20-150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20-150 % 20-150 % 20-150 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % 20 % N/A % N/A % 20-150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20- 150 % 20-150 % 20-150 % 20-150 % 20- 150 % 20-150 ng ng ng ng ng ng ng ng ng

Maxxam Analytics lrnernatlonal Corporation o/a Maxxam AnalyticS 6740 campobePo Road, Mlsslssauga, Ontario, L5N 21..8 Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## Ma-§am

QAIQC Batch Num lnit QC Tvoe 3182506 

### cxu Method Blank 3190066 OBC Spiked Blank

RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Method Blank Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS Quality Assurance Report (Continued) Maxxam Job Number: GB351227 Date Analyzed Parameter vvvv/mm/dd 33'44'55'-HexaCB-(169) 2013/04/24 233'44'55'-HeptaCB-(189) 2013/04/24 C13-1234678 HeptaCDD 2013/04/25 C13-1234678 HeptaCDF 2013/04/25 C13-123678 HexaCDD 2013/04/25 C13-123678 HexaCDF 2013/04/25 C13-12378 PentaCDD 2013/04/25 C13-12378 PentaCDF 2013/04/25 C13-123789 HexaCDF 2013/04/25 C13-2378 TetraCDD 2013/04/25 C13-2378 TetraCDF 2013/04/25 C13-0ctachlorodibenzo-p-Dioxin 2013/04/25 2,3,7,8-Tetra COD 2013/04/25 2,3,7,8-Tetra COD 2013/04/25 1,2,3,7,8-Penta COD 2013/04/25 1,2,3,7,8-Penta COD 2013/04/25 1,2,3,4,7,8-Hexa COD 2013/04/25 1,2,3,4,7,8-Hexa COD 2013/04/25 1,2,3,6,7,8-Hexa COD 2013/04/25 1,2,3,6,7,8-Hexa COD 2013/04/25 1,2,3,7,8,9-Hexa COD 2013/04/25 1,2,3,7,8,9-Hexa COD 2013/04/25 1,2,3,4,6,7,8-Hepta COD 2013/04/25 1,2,3,4,6,7,8-Hepta COD 2013/04/25 1,2,3,4,6,7,8,9-0cta CDD 2013/04/25 1,2,3,4,6,7,8,9-0cta COD 2013/04/25 2,3,7,8-Tetra CDF 2013/04/25 2,3,7,8-Tetra CDF 2013/04/25 1,2,3,7,8-Penta CDF 2013/04/25 1,2,3,7,8-Penta CDF 2013/04/25 2,3,4,7,8-Penta CDF 2013/04/25 2,3,4,7,8-Penta CDF 2013/04/25 1,2,3,4,7,8-Hexa CDF 2013/04/25 1,2,3,4,7,8-Hexa CDF 2013/04/25 1,2,3,6,7,8-Hexa CDF 2013/04/25 1,2,3,6,7,8-Hexa CDF 2013/04/25 2,3,4,6,7,8-Hexa CDF 2013/04/25 2,3,4,6,7,8-Hexa CDF 2013/04/25 1,2,3,7,8,9-Hexa CDF 2013104/25 1,2,3,7,8,9-Hexa CDF 2013/04/25 1,2,3,4,6,7,8-Hepta CDF 2013104/25 1,2,3,4,6,7,8-Hepta CDF 2013104/25 1,2,3,4,7,8,9-Hepta CDF 2013104/25 1,2,3,4,7,8,9-Hepta CDF 2013/04/25 1,2,3,4,6,7,8,9-0cta CDF 2013/04/25 1,2,3,4,6,7,8,9-0cta CDF 2013/04/25 C13-1234678 HeptaCDD 2013/04/25 C13-1234678 HeptaCDF 2013/04/25 C13-123678 HexaCDD 2013/04/25 C13-123678 HexaCDF 2013/04/25 C13-12378 PentaCDD 2013/04/25 C13-12378 PentaCDF 2013/04/25 C13-123789 HexaCDF 2013/04/25 C13-2378 TetraCDD 2013/04/25 C13-2378 TetraCDF 2013/04/25

Page 27 of29 Value %Recoverv <0.040, EDL=0.040 <0.014, EDL=0.014 115 115 77 70 70 68 73 41 57 100 113 NC 118 NC 98 NC 109 NC 131 NC 98 NC 95 NC 99 NC 104 NC 114 NC 103 NC 115 NC 122 NC 127 NC 90 NC 87 NC 99 NC 119 114 72 71 67 69 75 45 66 Units QC Limits ng ng % 25- 130 % 25- 130 % 40- 130 % 40- 130 % 40- 130 % 40-130 % 40-130 % 40- 130 % 40-130 % 25- 130 % 80-140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80-140 % 20 % 80-140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80-140 % 20 % 80- 140 % 20 % 80-140 % 20 % 80-140 % 20 % 80-140 % 20 % 80- 140 % 20 % 25- 130 % 25- 130 % 40- 130 % 40- 130 % 40-130 % 40- 130 % 40- 130 % 40- 130 % 40- 130

Maxxam Analyucs Jrnernational COrporation ala Maxxam Anal}'lics 6740 campobello Roaa, MISslssauga, Ontario, L5N 21..8 Tel: (905) 817-5700 Toll-Free: aoo-563-6266 Fax: (905) 817-5777 www.maxxam.ca

# rv1a(52am

QNQC Batch Num lnit QC Type 3190066 OBC Method Blank

3191218 VCI Method Blank Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS Quality Assurance Report (Continued) Maxxam Job Number: GB351227 Date Analyzed Parameter yyyy/mm/dd C13-0ctachlorodibenzo-p-Dioxin 2013/04/25 2,3,7,8-Tetra COD 2013/04/25 1,2,3,7,8-Penta COD 2013/04/25 1,2,3,4,7,8-Hexa COD 2013/04/25 1,2,3,6,7,8-Hexa COD 2013/04/25 1,2,3,7,8,9-Hexa COD 2013/04/25 1,2,3,4,6,7,8-Hepta COD 2013/04/25 1,2,3,4,6,7,8,9-0cta COD 2013/04/25 Total Tetra COD 2013/04/25 Total Penta COD 2013/04/25 Total Hexa COD 2013/04/25 Total Hepta COD 2013/04/25 2,3,7,8-Tetra CDF 2013/04/25 1,2,3,7,8-Penta CDF 2013/04/25 2,3,4,7,8-Penta CDF 2013/04/25 1,2,3,4,7,8-Hexa CDF 2013/04/25 1,2,3,6,7,8-Hexa CDF 2013/04/25 2,3,4,6,7,8-Hexa CDF 2013/04/25 1,2,3,7,8,9-Hexa CDF 2013/04/25 1,2,3,4,6,7,8-Hepta CDF 2013/04/25 1,2,3,4,7,8,9-Hepta CDF 2013/04/25 1,2,3,4,6,7,8,9-0cta CDF 2013/04/25 Total Tetra CDF 2013/04/25 Total Penta CDF 2013/04/25 Total Hexa CDF 2013/04/25 Total Hepta CDF 2013/04/25 Confirmation C13-2378 TetraCDF 2013/04/24 Confirmation 2 3 7 8-Tetra CDF 2013/04/24 Value %Recoverv 119 <6.7, EDL=6.7 <7.4, EDL=7.4 <6.5, EDL=6.5 <6.3, EDL=6.3 <6.4, EDL=6.4 <7.4, EDL=7.4 <6.4, EDL=6.4 <6.7, EDL=6.7 <7.4, EDL=7.4 <6.4, EDL=6.4 <7.4, EDL=7.4 <2.9, EDL=2.9 <7.0, EDL=7.0 <6.6, EDL=6.6 <3.0, EDL=3.0 <2.9, EDL=2.9 <3.6, EDL=3.6 <4.0, EDL=4.0 <3.6, EDL=3.6 <4.9. EDL=4.9 <7.1, EDL=7.1 <2.9, EDL=2.9 <6.8, EDL=6.8 <3.3, EDL=3.3 <4.1, EDL=4.1 61 <3.2 EDL=3.2 Duplicate: Paired analysis of a separate portion ofthe same sample. Used to evaluate the variance in the measurement. Units QC Limits % 25- 130 pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg pg % 40- 135 pq Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency. NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

Page 28 of29

!Vlaxxam Ana!ylics lrrternalional COrporation o!a Maxxam Analytics 6740 Canpobello Road, MlSsissauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: {905) 817-5777 wwvv.maxxam.ca

### Validation Signature Page

Maxxam Job 

### #: 8351227

The analytical data and all QC contained inthisreportwere reviewed andvalidatedbythe following individual(s).

Branko Vrzic, A.SC.T., SeniorAnalyst, HRMS Services



# /(u .)lhLUU Kaysr::&C. Chern, Scientific Specialist, HRMS Sen<lc.,;

Maxxam has procedures in place to guard against improperuse ofthe electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page29 of29

1\ilaxxam Analylics International COrporation o/a Maxxam Analytlcs 6740 C;mpot>ello Road, MISSiSsauga, On!arlo, L5N 2L8 Tel: (905) 817-5700 Toll-Free: 80Q-563-6266 Fax: (905) 817-5777 www.maxxam.caYour P.O.#: 10244
Your Project#: Tl1550 Attention: Lorri L White Keika Ventures Site Location: TEST INC.
- FELMAN PRODUCTIONS Your C.O.C. #: N/A Chapel Hill 101 Strangford Lane Durham, NC USA 27713 Report Date: 2013/05/02 

### CERTIFICATE OF ANALYSIS MAXXAM JOB#: 8351259 Received: 2013/04/06, 13:00 Sample Matrix: Stack Sampling Train #Samples Received: 7
Analyses PAH's in Air (CARB429) Date Date Quantity Extracted Analyzed Laboratory Method 7 2013/04/16 2013/05/01 BRL SOP-00418

* RPDs calculated using raw data. The rounding offinal results may result in the apparent difference.
Encryption

### Key~ 1 Ancy Sebastian 

### L$_,l;Pdw- 02 May 2013 16:52:06 -04:00 Please direct all qut:::suv11::s 

### '"'tl"''u'"tl '"'"Certificate of Analysis to your Project Manager. Ancy Sebastian, C.Tech., Senior Project Manager, Air Taxies Email: ASebastian@maxxam.ca Phone# (905) 817-5831 

## ==================================================================== Method Reference GARB 429mod(CARB429)

Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section 5.1 0.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page. Maxxam Analytics Inc. is a NELAC accredited laboratory. Certificate # CANA001. Use ofthe NELAC logo however does not insure that Maxxam is accredited for all ofthe methods indicated. This certificate shall not be reproduced except in full, without the written approval of Maxxam Analytics Inc. Maxxam has procedures in place to guard against improper use ofthe electronic signature and have the required "signatories", as per section.

Total cover pages: 1
Page 1 of 12

Ma-.::xarn 1\na!ytlcs lmernational Corporation o/a Maxxam Analy"tics 67<10 Campobello Road, Mlssissauga, ontario, L5N 2L8 Tel: (905i 817-5700 Toll-Free: 800-563-6266 Fax: (905,)**817-5777\,.VWW.m~xanu.:a**Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1605 RC1606 RC1607 Sampling Date 2013/03/14 2013/03/18 2013/03/18 00:01 00:01 00:01 COC Number N/A N/A N/A Units TRAIN FDL RDL RUN 1-BH2-PAH EDL RDL RUN 2-BH2·PAH BLANK-PAH Naphthalene ng 761 24 10 27400 (1) 1400 500 48800 (1) 2-Methylnaphthalene ng 329 18 10 21700 490 500 42900 (1) 2-Chloronaphthalene ng <1.8 1.8 10 46.6 1.2 10 94.2 Acenaphthylene ng <35 35 10 2600 140 500 3060 Acenaphthene ng <62 62 10 1730 940 500 2230 Fluorene ng 166 20 10 2230 300 500 3290 Phenanthrene ng 435 23 10 13400 480 500 25100 (1) Anthracene ng <27 27 10 1040 570 500 1180 Fluoranthene ng 19.6 6.8 10 11100 590 500 73500 (1) Pyrene ng 10.9 6.3 10 5200 550 500 42700 (1) Benzo(a)anthracene ng <5.9 5.9 10 618 150 500 3260 Chrysene ng <6.1 6.1 10 3660 140 500 29000 (1) Benzo(b)fluoranthene ng <2.0 2.0 10 503 60 500 3320 Benzo(k)fluoranthene ng <3.3 3.3 10 172 35 10 1310 Benzo(e)pyrene ng <4.8 4.8 10 364 30 10 1950 Benzo(a)pyrene ng <6.1 6.1 10 <37 37 10 <60 Perylene ng <3.5 3.5 10 <33 33 10 <55 lndeno(1 ,2,3-cd)pyrene ng <5.2 5.2 10 27.7 6.8 10 71.3 Dibenz(a,h)anthracene ng <3.9 3.9 10 <4.7 4.7 10 9.6 Benzo(g,h,i)perylene ng <4.7 4.7 10 36.4 6.7 10 81.5 Coronene ng <10 10 10 12.6 2.9 10 23.6 Surrogate Recovery (%) 2-Methylnaphthalene-2H10 % 66 NtA N/A 55 N/A N/A 43 (2) Acenaphthylene-2H8 % 64 NtA N/A 78 N/A N/A 67 Anthracene-2H10 % 42 (2) NtA N/A 95 N/A N/A 72 Benz(a)anthracene-2H12 % 98 NtA N/A 74 N/A N/A 142 Benzo(a)pyrene-2H12 % 48 (2) NtA N/A 93 N/A N/A 90 Benzo(b)fluoranthene-2H 12 % 76 NtA N/A 109 N/A N/A 91 Benzo(g,h,i)perylene-2H12 % 54 NtA N/A 97 N/A N/A 96 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch= Quality Control Batch ( 1 ) EMCL
- PAH analysis
- Exceeds Maximum Calibration Limit EDL RDL QC Batch

700 500 3182508 300 500 3182508 1.2 10 3182508 66 500 3182508 550 500 3182508 190 500 3182508 390 500 3182508 450 500 3182508 550 500 3182508 510 500 3182508 130 500 3182508 180 500 3182508 45 500 3182508 87 500 3182508 58 500 3182508 60 10 3182508 55 10 3182508 9.0 10 3182508 4.5 10 3182508 9.5 10 3182508 4.3 10 3182508
N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 2 of 12

Maxxam Analyucs lrnernational COrporation ola Maxxam Analytics 6740 CampobeHo Road, MlssiSsauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817·5777 www.maxxam.caMaxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1605 RC1606 RC1607 !Sampling Date 2013/03/14 2013/03/18 2013/03/18 00:01 00:01 00:01 COG Number N/A N/A N/A Units TRAIN DL RDL RUN 1-BH2-PAH EDL RDL RUN 2-BH2-PAH BLANK-PAH Benzo(k}fluoranthene-2H12 % 75 N/A N/A 98 N/A N/A 65 Chrysene-2H 12 % 80 N/A N/A 59 N/A N/A 91 Dibenzo(a,h)anthracene-2H14 % 53 N/A N/A 115 N/A N/A 120 Fluoranthene-2H10 % 79 N/A N/A 88 N/A N/A 88 Fluorene-2H10 % 123 N/A N/A 70 N/A N/A 68 lndeno(1,2,3-c,d}pyrene-2H12 % 51 N/A N/A 98 N/A N/A 103 Naphthalene-2H8 % 71 N/A N/A 46 (1} N/A N/A 35 (1} Perylene-2H12 % 54 N/A N/A 83 N/A N/A 75 Phenanthrene-2H10 % 44 (1} N/A N/A 110 N/A N/A 105 Terphenyi-2H14 % 108 N/A N/A 137 N/A N/A 153 (1} N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch EDL RDL 

## pc Batch

N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 3 of 12

Maxxam Analytics lmernational COrporation o!a Max.xam Analytlcs 6740 Campobello Road, Mtsslssauga, On!arlo, L5N 21..8 Tel: (905) 817·5700 TOll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1608 RC1609 RC1610 Sampling Date 2013/03/18 2013/03/14 2013/03/14 00:01 00:01 00:01 OC Number N/A N/A N/A Units RUN 3-BH2-PAH EDL RUN 1-BH5-PAH EDL RDL RUN 2-BH5-PAH Naphthalene ng 43800 (1) 480 45100 (1) 330 500 28600 (1) 2-Methylnaphthalene ng 29700 (1) 310 19200 120 500 15900 2-Chloronaphthalene ng 92.6 0.84 81.0 0.40 10 72.8 Acenaphthylene ng 4570 67 9040 89 500 4780 Acenaphthene ng 2520 490 4030 330 500 2680 Fluorene ng 3480 170 5080 220 500 2950 Phenanthrene ng 22400 230 67100 (1) 430 500 53400 (1) Anthracene ng 1630 270 2170 500 500 2650 Fluoranthene ng 15100 440 45700 (1) 310 500 43000 (1) Pyrene ng 7790 410 23000 290 500 26600 Benzo(a)anthracene ng 672 69 1210 110 500 1300 Chrysene ng 3830 80 6850 120 500 4500 Benzo(b)fluoranthene ng 902 30 956 120 500 466 Benzo(k)fluoranthene ng 246 15 344 16 10 135 Benzo(e)pyrene ng 519 33 1150 230 500 477 Benzo(a)pyrene ng 21 16 <27 27 10 <16 Perylene ng <15 15 <18 18 10 <11 lndeno(1 ,2,3-cd)pyrene ng 52.4 7.0 50.6 6.6 10 16.6 Dibenz(a,h)anthracene ng 9.6 3.5 8.5 3.8 10 <2.8 Benzo(g,h,i)perylene ng 64.5 7.0 58.9 6.9 10 25.2 Coronene ng 44.7 4.3 32.2 4.2 10 12.8 Surrogate Recovery(%) 2-Methylnaphthalene-2H10 % 47 (2) N/A 47 (2) N/A N/A 49 (2) Acenaphthylene-2H8 % 62 N/A 52 N/A N/A 57 Anthracene-2H10 % 69 N/A 55 N/A N/A 53 Benz(a)anthracene-2H12 % 127 N/A 95 N/A N/A 107 Benzo(a)pyrene-2H12 % 107 N/A 65 N/A N/A 54 Benzo(b)fluoranthene-2H12 % 111 N/A 111 N/A N/A 115 Benzo(g,h,i)perylene-2H12 % 103 N/A 98 N/A N/A 92 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ( 1 ) EMCL
- PAH analysis
- Exceeds Maximum Calibration Limit EDL RDL QC Batch 320 500 3182508 130 500 3182508 1.2 10 3182508 49 500 3182508 320 500 3182508 150 500 3182508 330 500 3182508 390 500 3182508 320 500 3182508 300 500 3182508 72 500 3182508 94 500 3182508 5.4 10 3182508 9.1 10 3182508 13 10 3182508 16 10 3182508 11 10 3182508 3.6 10 3182508 2.8 10 3182508 3.7 10 3182508 2.6 10 3182508
N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 4 of 12

lllla•xam Analylics lrrternalional COrporation o:a Maxxam Analylics 6740 C<mpobello Road, Mfsslssauga, Ontario, L5N 21..8 Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1608 RC1609 RC1610 Sampling Date 2013/03/18 2013/03/14 2013/03/14 00:01 00:01 00:01 COC Number N/A N/A N/A Units RUN 3-BH2-PAH EDL RUN 1-BH5-PAH EDL RDL RUN 2-BH5-PAH Benzo(k)fluoranthene-2H12 % 101 N/A 86 N/A N/A 88 Chrysene-2H12 % 85 N/A 70 N/A N/A 87 Dibenzo(a,h)anthracene-2H14 % 137 N/A 130 N/A N/A 126 Fluoranthene-2H10 % 88 N/A 99 N/A N/A 99 Fluorene-2H10 % 66 N/A 70 N/A N/A 72 lndeno(1,2,3-c,d)pyrene-2H12 % 114 N/A 110 N/A N/A 105 Naphthalene-2H8 % 34 (1) N/A 33 (1) N/A N/A 42 (1) Perylene-2H12 % 80 N/A 61 N/A N/A 57 Phenanthrene-2H10 % 92 N/A 97 N/A N/A 112 Terphenyi-2H14 % 151 (1) N/A 159 (1) N/A N/A 168 (1) N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch I=DL RDL QC Batch N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508 N/A N/A 3182508

( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 5 of 12

l\iianam Analytics lrnernational Corporation o/a Ma""am Analy!lcs 6740 Campobello ROO!I, Mlsslssauga, Ontario, L5N 2L8 Tel: (905) 817·5700 Toll-Free: SOD-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project #: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1611 Sampling Date 2013/03/14 00:01 COC Number N/A Units RUN 3-BH5·PAH EDL RDL CJC Batch Naphthalene ng 31100 (1) 330 500 3182508 2-Methylnaphthalene ng 19100 130 500 3182508 2-Chloronaphthalene ng 52.5 0.27 10 3182508 Acenaphthylene ng 3760 51 500 3182508 Acenaphthene ng 2370 270 500 3182508 Fluorene ng 2280 200 500 3182508 Phenanthrene ng 36900 (1) 120 500 3182508 Anthracene ng 1360 140 500 3182508 Fluoranthene ng 18200 130 500 3182508 Pyrene ng 9510 120 500 3182508 Benzo(a)anthracene ng 494 5.6 10 3182508 Chrysene ng 1620 68 500 3182508 Benzo(b)fluoranthene ng 266 3.0 10 3182508 Benzo(k)fluoranthene ng 92.7 5.4 10 3182508 Benzo(e)pyrene ng 273 8.1 10 3182508 Benzo(a)pyrene ng <10 10 10 3182508 Perylene ng <7.2 7.2 10 3182508 lndeno(1 ,2,3-cd)pyrene ng 8.0 2.4 10 3182508 Dibenz(a,h)anthracene ng <2.0 2.0 10 3182508 Benzo(g,h,i)perylene ng 10.9 2.5 10 3182508 Coronene ng 6.1 2.2 10 3182508 Surrogate Recovery (%) 2-Methylnaphthalene-2H10 % 42 (2) N/A N/A 3182508 Acenaphthylene-2H8 % 61 N/A N/A 3182508 Anthracene-2H10 % 51 N/A N/A 3182508 Benz(a)anthracene-2H12 % 174 (2) N/A N/A 3182508 Benzo(a)pyrene-2H12 % 54 N/A N/A 3182508 Benzo(b)fluoranthene-2H12 % 128 N/A N/A 3182508 Benzo(g,h,i)perylene-2H12 % 100 N/A N/A 3182508 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ( 1 ) EMCL
- PAH analysis
- Exceeds Maximum Calibration Limit ( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 6 of 12

:Vlauam Analylics lrnemational COrporation ola Maxxam Analytics 6740 Campobello Road. Mlsslssauga. Ontario. L5N 2L8 Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.caMaxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC. -FELMAN PRODUCTIONS Your P.O.#: 10244
RESULTS OF ANALYSES OF STACK SAMPLING TRAIN
Maxxam ID RC1611**~ampling** Date 2013/03/14 00:01 COC Number N/A Units RUN 3-BH5-PAH EDL RDL DC Batch Benzo(k)fluoranthene-2H12 % 94 N/A N/A 3182508 Chrysene-2H12 % 112 N/A N/A 3182508 Dibenzo(a,h)anthracene-2H14 % 132 N/A N/A 3182508 Fluoranthene-2H10 % 88 N/A N/A 3182508 Fluorene-2H10 % 79 N/A N/A 3182508 lndeno(1,2,3-c,d)pyrene-2H12 % 112 N/A N/A 3182508 Naphthalene-2H8 % 35 (1) N/A N/A 3182508 Perylene-2H12 % 56 N/A N/A 3182508 Phenanthrene-2H10 % 104 N/A N/A 3182508 Terphenyi-2H14 % 153 (1) N/A N/A 3182508 N/A =Not Applicable RDL = Reportable Detection Limit EDL = Estimated Detection Limit QC Batch = Quality Control Batch ( 1 ) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 7 of 12
l';laxxam Analylics lmernalional COrporation o/a Maxxam**Anal~>tics** 6740 GampobeHo Roao, Mlsslssauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-Free: BOQ-563-6266 Fa>:: (905) 811-5777 www.mro:xam.ca

### f\/1

# e:~**~a** rn Keika Ventures Maxxam Job #: 8351259 Client Project #: Tl1550 Report Date: 2013/05/02 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244
Test Summary

Maxxam ID RC1605 Collected 2013/03/14 Sample ID TRAIN BLANK-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1606 Collected 2013/03/18 Sample ID RUN 1-BH2-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1607 Collected 2013/03/18 Sample ID RUN 2-BH2-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1608 Collected 2013/03/18 Sample ID RUN 3-BH2-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1609 Collected 2013/03/14 Sample ID RUN 1-BH5-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil
Maxxam ID RC1610 Collected 2013/03/14 Sample ID RUN 2-BH5-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted Anal zed Anal st HRMS/MS 3182508 2013/04/16 2013/05/01 Edmond Mcneil

Maxxam ID RC1611 Collected 2013/03/14 Sample ID RUN 3-BH5-PAH Shipped Matrix Stack Sampling Train Received 2013/04/06 Instrumentation Batch Extracted HRMS/MS 3182508 2013/04/16

Page 8 of 12

Maxxam Analyties !rnernational COrporatiOn o/a Maxxam Analytlcs 6740 CampobeHo Road, Mlsslssauga, OntariO, L5N 2L8 Tel: (905) 817-5700 Toll-Free: SOQ-563-6266 Fax: (905) 817-5777 www.maxxam.<"'

## Ma§am
Maxxam Job #: 8351259 Report Date: 2013/05/02 Keika Ventures Client Project#: Tl1550 Site Location: TEST INC.
- FELMAN PRODUCTIONS Your P.O.#: 10244

GENERAL COMMENTS PAH Analysis: Some ofthe recoveries are outside of standard limits 50% -150-% due to matrix suppression.
Results relate onlvtothe items tested.

Page 9 of 12

Maxxam Ana!y!ics International Corporation o!a Maxxam Analy!ics 6740carnpobeno Road, Mlsslssauga, Ontario, L5N 2L8 Tel: (905) 817-5700 Toll-free: 800.563-6266 Fax: (905) 817-5777www.maxxam.caQA/QC Batch Num lnit QCTvoe 3182508 EM Spiked Blank

RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank RPD Spiked Blank Keika Ventures Attention: Lorri L White Client Project#: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS

QualityAssurance Report Maxxam Job Number: GB351259 Date Analyzed Parameter ww/mm/dd 2-Methylnaphthalene-2H10 2013/04/30 Acenaphthylene-2H8 2013/04/30 Benz(a)anthracene-2H12 2013/04/30 Benzo(a)pyrene-2H12 2013/04/30 Benzo(b)fluoranthene-2H12 2013/04/30 Benzo(g,h,i)perylene-2H12 2013/04/30 Benzo(k)fluoranthene-2H12 2013/04/30 Chrysene-2H12 2013/04/30 Dibenzo(a,h)anthracene-2H14 2013/04/30 Fluoranthene-2H10 2013/04/30 lndeno(1 ,2,3-c,d)pyrene-2H12 2013/04/30 Naphthalene-2H8 2013/04/30 Perylene-2H12 2013/04/30 Phenanthrene-2H10 2013/04/30 Naphthalene 2013/04/30 Naphthalene 2013/04/30 2-Methylnaphthalene 2013/04/30 2-Methylnaphthalene 2013/04/30 2-Chloronaphthalene 2013/04/30 2-Chloronaphthalene 2013/04/30 Acenaphthylene 2013/04/30 Acenaphthylene 2013/04/30 Acenaphthene 2013/04/30 Acenaphthene 2013/04/30 Fluorene 2013/04/30 Fluorene 2013/04/30 Phenanthrene 2013/04/30 Phenanthrene 2013/04/30 Anthracene 2013/04/30 Anthracene 2013/04/30 Fluoranthene 2013/04/30 Fluoranthene 2013/04/30 Pyrene 2013/04/30 Pyrene 2013/04/30 Benzo(a)anthracene 2013/04/30 Benzo(a)anthracene 2013/04/30 Chrysene 2013/04/30 Chrysene 2013/04/30 Benzo(b)fluoranthene 2013/04/30 Benzo(b)fluoranthene 2013/04/30 Benzo(k)fluoranthene 2013/04/30 Benzo(k)fluoranthene 2013/04/30 Benzo(e)pyrene 2013/04/30 Benzo(e)pyrene 2013/04/30 Benzo(a)pyrene 2013/04/30 Benzo(a)pyrene 2013/04/30 Perylene 2013/04/30 Perylene 2013/04/30 lndeno(1 ,2,3-cd)pyrene 2013/04/30 lndeno(1 ,2,3-cd)pyrene 2013/04/30 Dibenz(a,h)anthracene 2013/04/30 Dibenz(a,h)anthracene 2013/04/30 Benzo(g,h,i)perylene 2013/04/30 Benzo(g,h,i)perylene 2013/04/30 Coronene 2013/04/30

Page 10 of 12 Value %Recoverv 84 73 91 81 86 64 93 77 64 86 67 99 77 53 283 (1) 7.3 (1) 111 0.9 85 4.8 110 2.7 110 1.8 169 (1) 17.4 (1) 111

1.8 98 11.5 109 10.6 103 5.0 106

0 132 5.2 107 1.9 98 16.6 115 5.4 79 3.7 110 1.8 131 12.1 124 2.4 134 0.7 126 Units QC Limits % 50- 150; % 50 -150; % 50-150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50-150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 60-140 % 50 % 60- 140 % 50 % N/A % 50 % 60- 140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60-140 % 50 % 60-140 % 50 % 60-140 % 50 % 60-140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60-140 % 50 % 60- 140 % 50 % 60- 140 % 50 % 60- 140 % 50 % N/A

Ma'xam ''nalylics lmernati<mal corporation ala Maxxam**Anal~'lics** 6740 campobello Road, MlssiSsauga, Ontario, L5N 2LB Tel: (905) 817-5700 Toll-Free: 800-563-6266 Fax: (905) 817-5777 www.maxxam.ca

## lV1a§am

QNQC Batch Num lnit QC Tvoe 3182508 EM RPD Method Blank Keika Ventures Attention: Lorri L White Client Project #: Tl1550 P.O.#: 10244 Site Location: TEST INC.
- FELMAN PRODUCTIONS QualityAssurance Report (Continued) Maxxam Job Number: GB351259 Date Analyzed Parameter vvvv/mm/dd Coronene 2013/04/30 2-Methylnaphthalene-2H10 2013/04/30 Acenaphthylene-2H8 2013/04/30 Benz(a)anthracene-2H12 2013/04/30 Benzo(a)pyrene-2H12 2013/04/30 Benzo(b)fluoranthene-2H12 2013/04/30 Benzo(g,h,i)perylene-2H12 2013/04/30 Benzo(k)fluoranthene-2H12 2013/04/30 Chrysene-2H12 2013/04/30 Dibenzo(a,h)anthracene-2H14 2013/04/30 Fluoranthene-2H10 2013/04/30 lndeno(1,2,3-c,d)pyrene-2H12 2013/04/30 Naphthalene-2H8 2013/04/30 Perylene-2H12 2013/04/30 Phenanthrene-2H10 2013/04/30 Naphthalene 2013/04/30 2-Methylnaphthalene 2013/04/30 2-Chloronaphthalene 2013/04/30 Acenaphthylene 2013/04/30 Acenaphthene 2013/04/30 Fluorene 2013/04/30 Phenanthrene 2013/04/30 Anthracene 2013/04/30 Fluoranthene 2013/04/30 Pyrene 2013/04/30 Benzo(a)anthracene 2013/04/30 Chrysene 2013/04/30 Benzo(b)fluoranthene 2013/04/30 Benzo(k)fluoranthene 2013104/30 Benzo(e)pyrene 2013/04/30 Benzo(a)pyrene 2013/04/30 Perylene 2013104/30 lndeno(1 ,2,3-cd)pyrene 2013/04/30 Dibenz(a,h)anthracene 2013/04/30 Benzo(g,h,i)perylene 2013/04/30 Coronene 2013/04/30 Value %Recovery 3.9 82 74 83 78 90 59 82 74 57 82 59 112 71 47 (2) 105, EDL=0.81 3.11, EDL=0.56 <0.60, EDL=0.60

<2.1, EDL=2.1 <4.6, EDL=4.6 0.76, EDL=0.40 1.23, EDL=0.34 <0.40, EDL=0.40 <0.53, EDL=0.53 <0.49, EDL=0.49 <0.70, EDL=O.?O <0.76, EDL=0.76 <0.46, EDL=0.46 <0.76, EDL=0.76 <0.53, EDL=0.53 <0.76, EDL=0.76 <0.67, EDL=0.67 <0.38, EDL=0.38 <0.68, EDL=0.68 <0.39, EDL=0.39

<3.2, EDL=3.2 Duplicate: Paired analysis of a separate portion ofthe same sample. Used to evaluate the variance in the measurement. Units QC Limits % 5Q' % 50-150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50- 150 % 50-150 % 50-150 % 50- 150 % 50- 150 % 50- 150 % 50-150 % 50- 150 % 50-150 ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng ng Spiked Blank: A blank matrix sample to which a known amount ofthe analyte, usually from a second source, has been added. Used to evaluate method accuracy. Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination. Surrogate: A pure or isotopically labeled compound whose behavior mirrors the analytes of interest. Used to evaluate extraction efficiency. ( 1 ) Recovery Exceeds method acceptance criteria 50%- 150% due to matrix background ( 2) Recovery or RPD for this parameter is outside control limits. The overall quality control for this analysis meets acceptability criteria.

Page 11 of12

Ma•xam Analylics International COrporatiOn ola Max.xam Analytles f>740 C<rnpobei!O Roatl, M!SsiSSauga, Ontarlo,l5N 21..8 Tel: (905) 817·5700 Toll-Free: SOQ-563·6266 Fax: (905) 817-5777 www.maxxam.ca

# Ma?§2-am

Validation Signature Page

Maxxam Job 

### #: 6351259

The analytical dataand all QC contained inthis report were reviewed and validatedbythe following individual(s).

Owen Cosby, BSc.C. em, Supervisor, HRMS Services

Maxxam has procedures in place to guard against improper nse ofthe electronic signature and have the required "signatories", as per section 5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Page 12 of 12

Maxxam AnalyUcs lrnernatlonal corporation ora Mal<Xam Analytlas 6740 Campobello Road, Mlsslssauga, Ontario, L5N 21.8 Tel: (905) 817·5700 Toii·Free: SOIJ-563·6266 Fax: (905) 817·5777 www.maxxam.ca

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## 0 High Flow 

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### ---------------- Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 

### 9263 Ravenna Road Unit A-3, Twinsburg, OH 

## 44g87 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

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Plant/Source:

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------ 

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## -------------------- 0 High Flow 

## D COIL 

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___**.....;;3_0~6;;;...._**

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Date:

------------- Received by:.

____________________________________________ _ Date:



### ------------ Relinquished by:.

_______________________________________ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon

- Refer to MSDS Deactivated glass and glass wool

# Sorbent Trap Chain ofCustody T t 

## L t. r;
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___ _ Spike Time:

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________ _ 

## Estimated Hg in Section 1 :

______**---=n=g~** 

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Date Time

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## __________ _ Date: 

### _!._i_·_l

### _-·-'---::.._~--- Received by:.

__________________________ _ Date:

_______ _ Relinquished by:.

________________________ _ Date:

_______ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented atall costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A"'3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

# WIEX Sorbent Trap Chain ofCustody T L . ,.· \""-.}"#I



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Flow Rate (cc/min)
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Relinquished by Tech.:_--'l.._-

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________________________________________________ _ Date:

_____________ _ Relinquished by:

_____________________________________________ _ Date:

_____________ _ Received for Laboratory by: Date: Make-sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss

### in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

# Sorbent Trap Chain ofCustody
Plant/Source:**~-e..** 

## \**,.~Y-.** <=-. 

# P. 1{**~~~~~~~--~~~-------** 

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# 5 

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# IZJ Unspiked 

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________ _ 

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______**_____,n~g:>-** 

## D High Flow 

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## D AGS I8J.I85 mm 0240mm 0300mm 0450mm 

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# s,**~;.f!:.!~ ~o**  \;::-do Total Volume Pulled



### Chain ofCustody

Date: 

## "1
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## (J
Received by:.

____________________________________________________ _ Date:

______________ _ Relinquished by:.

_______________________________________________ _ Date:

______________ _ Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Roaq Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon- Refer to MSDS Deactivated glass and glass wool

# Sorbent Trap Chain ofCustody
Test Location:**.~** 

## ___:-:: 

## vlJ,_ .;;**\}_jc~** 

## Boiler ID:

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## QA/QC Signature

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________ _ 

## D High Flow 

## D COIL 

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## SampledBy: 

## C.---

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___

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## 6- L'S. -1)



## Date/Time : L0

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## 3 Date/Time 

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### Sorbent Flow Rate Dry Gas Meter Dry Gas Meter Total Volume toC)

### ~/Jemp

## ~) Liters Initial Liters Final Pulled '"--/ 

### oc)**~-** lotS 

### fb·'-o**'--;J<1)e:~** f-tCO O,CbG

### ~**-;;t~2** 

# -/c't**f~.~s-** II 0**,:',\~£.:?** ·'-fCr?**~** '·:;**~** 2_**~,u** .:c<:;- '•. "' 

# 3/L?) 

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## i**''-~** 

### 5 ':; ,. <..:: i**;;~-:::o** !.loJ**~** {**~..,** 

## "

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### > 1.7 J 

## ((c::r, i 

### 1 i

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## "·';o '-LVD ,) • f. 

### I '::;**tX..~** f

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### .lo I

### "5 I 

### '5 \- c 

## a-5o &tDO 

## -s- d _Oj_ 

### 7 \ 

### '· ) 

# ITotal/ Average 

## Chain ofCustody
Relinquished by Tech.: 

# C

# j,~ 5i>

# ~Ldf Date: 

## lt
- i

- l 

# 3
Received by:.

__________________________ _ Date:

_______ _ Relinquished by:.

________________________ _ Date:


## ·--------- Received for Laboratory by: Date: Make sure all ofyour sampling conditions prevent moisture condensation in the trap media. Moisture condensation is a major cause ofbreakthrough and spike loss in sorbent traps and should be prevented at all costs. 

### For Analysis contact us: Ohio Lumex Co., Inc. 9263 Ravenna Road Unit A-3, Twinsburg, OH 44087 USA Phone 330-405-0837 Fax 330-405-0847 US Toll Free: 888-876-2611 Impregnated Activated Carbon

- Refer to MSDS Deactivated glass and glass wool

### APPENDIXE CALIBRATION DATA

## Dry Gas MeterBox Calibration MeterNo. 2010 Barometer 29.4 Date 04/02/13 PreTest Y 1.0203 Calibrator csm Po Vac Vw Tw Vd Td y 

### "H20 "Hg 

### ft3 

### op ft3 

### op 

## 1:::u::::

# ::::::::m 0.000 60 720.339 60.5

# ~· 0.5 10.000 

## 61 730.16 62.5 

## 1.0189 l;:r ::ill::' I 

# , ..**·~** 

### ;::.r:lf:**~·** 

### · !l!U!!: :iii; 

### 'I I 

### ·I I T



### 1.50 30.000 61 749.72 63 1.0242

2.00 40.000 61 759.505 64 1.0218

Average Y = 

### 1.0188

## Dry Gas MeterBox Calibration MeterNo. 2010 Barometer 29.4 Date 04/02/ PreTest Y 1.0203 Calibrator csm Po Vac Vw Tw Vd Td 

### y fP 

### op ft3 

### op 0.000 60 720.339 60.5 10.000 61 730.16 62.5

:...: : :

... 

### 61 1.00

Average Y = 

### 1.0188

### Barometer 

### 29.4 PreTest Y 

### 1.0468 Po Vac 

### "H20 "Hg

0.5

1.00 

## Dry Gas Meter Box Calibration Meter No. 

### 2010 Date Calibrator Vw Tw Vd Td 

### ft3 

### op ft3 

### op 0.000 57 174.528 61.5 10.000 58 184.295 61.5 10.000 57.5 9.767 61.5 10.000 58 184.295 61.5 20.000 58 194.105 61.5 10.000 58 9.81 61.5 

## ::::=::::O:U.LU 2o.ooo 58 194.Ios 61.5 1.50 30.000 58 203.89 61 02/20113 csm

y



### 1.0305

1.0237

1.0245



# ..**!1N#~~~~1i\~~;** 

### 1o.ooo 58 9.785 

### 61.25

# :::::i~:::::::::u:S24-------+--3 __ o..o __ oo-+
___ 5_8

__-r
__ 

### 2_o3_.8_9

__ r-__ 6_1

__

# -F~~~

# 4 2.00 40.000 58 213.625 60.5 1.0275 

# "; ,:,so 1

# 1---------+--~-**:-·:~- --+---~-;:---+--;:-f-:~-~~-~** **--+-- 60** 

# ~-·?----r~1"""".o"""'o5.:..;.1~ ''' •F======*===

# 10

# o=.:~=~ci===P==~!===*====2;:::::::~·~==5**6=:5====9== 6=··;=** **=H+&:+++-+.+.BSI** 3.00 60.000 58 233.433 61 1.0117
Average Y = 

### 1.0205

### Barometer 29.3 PreTest Y 1.0342 Po Vac 

## Dry 

## Gas Meter Box Calibration Meter No. 2010 MST

Vw Tw

10.000 

## 74 Date Calibrator Vd



### 9.818 10/05112 csm Td y



### 86 Average Y 

### = 1.0302

### Barometer 29.35 PreTest Y 1.0302 

## Dry Gas MeterBox Calibration MeterNo. 2010 MST Date Calibrator Vd 

### Po Vac Vw Td Tw 

### "H20 "Hg :ft3 0 f 

### :ft3 

### op 04/02/13 csm



### y

0.5 1 10.000 63 334.735 71 1.0160

1.00 2 10.000 63 344.685 71 1.0178

1.50 3 10.000 63 354.6 72 1.0211

2.00 4 10.000 62 3ll4**~?~** 

### 73 1.0217

Average Y = 

### 1.0205CHEROKEE INSTRUMENTS INC 30B HgDual Console Meter Box Post Calibration

Cherokee#: 3620 Meter# Ml-Dual Hg Date: 03/05/13 Operator: J McK Serial#: DB 30B-1110-2017 Barometric Pressure: 29.73 in. Hg Vacuum: 0 in. Hg HgSide 1 DRY GAS METERVOLUME CALIBRATION DEVICE VOLUME
Flow Time Initial Final Total Temperature (°F) Initial Final Total Temperature ("F) Qmn) (minutes) (Liters) (Liters) (Liters) Initial Final (Liters) (Liters) (Liters) Initial Final
0.25 40.0 0.00 10.19 10.19 84 85 17883.00 17893.00 10.00 78 78
0.50 42.0 0.00 21.72 21.72 82 83 I7859AO 17881.50 22.10 77 78
0.75 31.0 0.00 23.24 23.24 80 81 I7831.20 17854.70 23.50 78 78

DRY GAS METERVOLUME CALIBRATION DEVICE VOLUME
Flow Time Initial Final Total Temperature (°F) Initial Final Total Temperature ("F) DR!!!.l (minutes) (Liters) (Liters) (Liters) Initial Final (Liters) (Liters) (Liters) Initial Final
0.25 40.0 0.00 12.22 11.52 78 82 17731.80 17742.60 10.80 76 78
0.50 35.0 0.00 18.07 18.07 80 82 17745.70 17762.80 17.10 76 77
0.75 35.0 0.00 27.17 27.17 82 84 17770.20 17796.30 26.10 77 77

Meter 1 Deviation Meter2 Deviation Calibration Gamma (Y)* 

## =I 1.0092 

## I 1.002 -0.018 0.951 -0.013 1.035 O.oi5 0.962 -0.002 1.023 0.003 0.979 0.015 

# I 

# A '""'e

# Grunma--=-- 1.02,;-

----**-~--=~~amma** =

## --~~-~

308 Console-3620 (Dual)

### APPENDIXF CHAIN OF CUSTODY

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, West Virginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304} 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

LU 1- SAMPLE DESCRIPTION 

### 0 0 Vi 

### z 0 (INCLUDE MATRIX) 

### z c..**~** LU LU**~** co 

### z 

## !d:**~** <( LU :::1 0 c::: 1- c::: Q i= u l!:} 

### 1 1 3/15/2013 Baghouse #5 Run 1Back-halfRinse H2S04 2 2 3/15/2013 Baghouse #5 Run 2 Back-halfRinse H2S04 3 3 3115/2013 Baghouse #5 Run 3 Back-halfRinse H2S04 4 1 3/19/2013 Baghouse #2 Run 1Back-halfRinse H2S04 5 2 3/19/2013 Baghouse #2 Run 2 Back-halfRinse H2S04 6 

### 3 3/19/2013 Baghouse #2 Run 3 Back-halfRinse H2S04 7 3/27/2013 Blank De-ionized Water 8 3/27/2013 Blank O.lN H2S04 9 10 1.1) c::: LU u.. 

### z 

## u 0<( :I: =1:1: 1- <( 

### z 1.0 0 N u**~** 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: 

### Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: 

### REQUESTED ANALYSIS COMMENTS I

I



### HCI1 of 1

BH#5 BH#5 BH#5 BH#2 BH#2 BH#2

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- 

### SAMPLE DESCRIPTION 

### ci v; 

### z ci 0 

### (INCLUDE MATRIX) 

### z c.. co 

### ::lE w w 

### ::lE 

### z !;;( ::lE <( w 

### => 0 ex: 1- ex: Cl i= 

### u l!) 

### 1 1 3/13/2013 Baghouse #5 Run 1Filter 1012 2 1 3/13/2013 Baghouse #5 Run 1Front-halfRinse HN03 3 1 3/13/2013 Baghouse #5 Run 1Back-halfRinse HN03 4 

### 2 3/13/2013 Baghouse #5 Run 2 Filter 1011 5 2 3/13/2013 Baghouse #5 Run 2 Front-halfRinse HN03 6 

### 2 3113/2013 Baghouse #5 Run 2 Back-halfRinse HN03 

### 7 3 3/13/2013 Baghouse #5 Run 3 Filter 1010 8 3 3/13/2013 Baghouse #5 Run 3 Front-halfRinse HN03 9 

### 3 3/13/2013 Baghouse #5 Run 3 Back-halfRinse HN03 10**~** ro 

# .. Q)**~** V') Q) ex: 

## c. w ·.;; Ll- 

### z 0 

### <C :::J :1:1: 1-**~** 

### z 

# "' 0 N 

### u**~** 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X


### RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Metals 1 of 3 arsenic, cadmium, chromium, manganese, nickle, lead



### BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#5
DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304} 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### d Vi 

### d 0 (INCLUDE MATRIX) 2 2 c.. co 

### ::!: w w 

### ::!: 2

### ~ ::!: <( w ::> 0 0:: 1- 0:: Cl i= u l!) 1 1 3/13/2013 Baghouse #2 Run 1Filter 1007 2 1 3/13/2013 Baghouse #2 Run 1Front-halfRinse HN03 3 1 3/13/2013 Baghouse #2 Run 1 Back-halfRinse HN03 4 2 3/13/2013 Baghouse #2 Run 2 Filter 1006 5 2 3113/2013 Baghouse #2 Run 2 Front-halfRinse HN03 6 2 3/13/2013 Baghouse #2 Run 2 Back-halfRinse HN03 7 3 3/13/2013 Baghouse#2 Run 3 Filter 1005 8 3 3/13/2013 Baghouse #2 Run 3 Front-halfRinse HN03 9 3 3113/2013 Baghouse#2 Run 3 Back-halfRinse HN03 10 ...!!! ro**~** Q)**~** 1./) Q) 0:: 0.. w :;; u. 2 :::::s 0<(**~** =1:1: 1- 2 0'1 0 N u**~** 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X
RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS I

I Metals 2 of 3 arsenic, cadmium, chromium, manganese, nickle, lead

BH#2 BH#2 BH#2 BH#2 BH#2 BH#2 BH#2 BH#2 BH#2
DATE: TIME:

# ~~· 

# • TEST, Inc. Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 

# Chain of Custody

EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- 

### SAMPLE DESCRIPTION 

### d v; 

### d 0 

### (INCLUDE MATRIX) 

### z z 0.. C'J 

### ::E w w 

### ::E 

### z**~** ::E <( w 

### => 0 0::: 1- 0::: 0 i= u (,!) 1 1 3/27/2013 BlankFilter 2 1 3/27/2013 Blank 5%HN03110% H202 3 1 3/27/2013 Blank O.lN HN03 4 5 6 7 8 9 10 ..!:!! rtl**~** CIJ**~** VI CIJ 0::: 0.. w ·,p u..Z :::::s 0<(**~** #I- 

### z O'l 0 N u**~** 1 X 1 X 1 X



### RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Metals 3 of 3 arsenic, cadmium, chromium, manganese, nickle, lead

I

I



### DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.corn


### PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN @TESTINCORP.COM

LU 1- SAMPLE DESCRIPTION 

### c:i c:i Vi 

### z 0 (INCLUDE MATRIX) 

### z c.. 

### ::lE LU LU 

### ::lE a::l 

### z**~** ::lE <( LU 

### => 0 c::: 1- c::: 

### c i= u**~** 

### 1 1 3115/2013 M23/PCB XAD Trap #7, Baghouse#5 Run 1 2 1 3115/2013 M23/PCB Filter, Baghouse #5 Run 1 3 2 3/15/2013 M23/PCB Trap #1, Baghouse#5 Run 2 4 

### 2 3115/2013 M23/PCB Filter, Baghouse #5 Run 2 5 3 3115/2013 M23/PCB Trap #6, Baghouse#5 Run 3 6 3 3/15/2013 M23/PCB Filter, Baghouse #5 Run 3 7 1 3119/2013 M23/PCB Trap #8, Baghouse#2 Run 1 8 1 3/19/2013 M23/PCB Filter, Baghouse #2 Run 1 9 2 3/19/2013 M23/PCB Trap #9, Baghouse#2 Run 2 10 2 3/19/2013 M23/PCB Filter, Baghouse #2 Run 2 u c..

......... Vl c: rtl !..... :::l 1.1-

......... Vl c: 

## ·x 0 

### i5 00 V') N c::: ..::t LU r::c LL Z c:::: 0<( 

## () =1:1: 1- 

### z m 0 N u**~** 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: 

### Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: 

### REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furansl 

## I PCB 1 of 2

BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

LU 1- SAMPLE DESCRIPTION 

### 0 0 Vi 

### z 0 (INCLUDE MATRIX) 

### z LU c.. l:C 

### :2: LU 

### :2: 

### z !;:( :2: <( LU :::> 0 0:: 1- 0:: Cl i= 

### u I.!J 1 3 3119/2013 M23/PCB Trap #3, Baghouse#2 Run 3 2 3 3119/2013 M23/PCB Filter, Baghouse #2 Run 3 3 3115/2013 M23/PCB Trap #2, Train Blank 4 3115/2013 M23/PCB Filter, Blank 5 M23/PCB Trap #4, NotUsed 6 M23/PCB Trap #5, Not used 

### 7 8 9 10 

### u c..

........ Vl c: ro I..**~** u.

........ Vl c: 

## ·x 0 

### i5 co V'l N 0:: o::t LU 

### c:c u.. 

### z 0::: 0 

### <C 

# 6 =1:1: 1- 

### z m 0 N 

### u**~** 1 X 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 2 of 2

BH#2 BH#2 Blank Blank No analysis No analysis

DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304} 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w I- SAMPLE DESCRIPTION 

### c:i c:i Vi 

### z 0 (INCLUDE MATRIX) 

### z Q. 1:0**~** w w**~** 

### z**~ ~**  <( w ::> 0 c::: I- c::: Cl i= u ID 1 1 3/15/2013 Baghouse #5 DIFIPCB Run 1 Front-halfRinse 2 1 3/15/2013 Baghouse #5 DIF /PCB Run 1Back-halfRinse 3 2 3/15/2013 Baghouse #5 DIFIPCB Run 2 Front-halfRinse 4 2 3/15/2013 Baghouse#5 DIFIPCB Run 2 Back-halfRinse 5 3 3/15/2013 Baghouse#5 DIFIPCB Run 3 Front-halfRinse 6 3 3115/2013 Baghouse#5 DIF /PCB Run 3 Back-halfRinse 

### 7 1 3119/2013 Baghouse #2 D/F/PCB Run 1 Front-halfRinse 8 1 3/19/2013 Baghouse #2 DIFIPCB Run 1Back-halfRinse 9 2 3119/2013 Baghouse #2 DIFIPCB Run 2 Front-halfRinse 10 2 3119/2013 Baghouse#2 DIFIPCB Run 2 Back-halfRinse u c..



### ....... Vl c:: ro**~** ;:, Ll-



### ....... Vl c:: 

## ·x 0 

### i5 co Vl N c::: 

## """ w co 1.1- 

### z c::: 0 <( <( =1:1: I- u 

### z m 0 N u**~** 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X 1 X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 1 of 2

BH#5 BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

LU I- SAMPLE DESCRIPTION 

### d d v; 

### z 0 (INCLUDE MATRIX) 

### z c.. co**~** LU LU**~** 

### z**~ ~**  <( LU ::> 0 a: I- a: 0 i= 

### u 1.!) 

### 1 3 3/19/2013 Baghouse #2 D/F/PCB Run 3 Front-halfRinse 2 3 3/19/2013 Baghouse #2 D/F/PCB Run 3 Back-halfRinse 3 3/15/2013 Train Blank D/F/PCB Front and back halfRinse 4 

### 5 6 

### 7 8 

### 9 10 

### :c Ill <( a: c.. LU ........ LL Z 

### en 0<( N :1:1: I- q

### z co 0 0:: 

### u <( 

### u 1 X 

### 1 X 

### 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 312712013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

Dioxins 

## I Furans 

## I PCB 2 of 2



### BH#2 BH#2 Blank

!

DATE: TIME:

I I

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### d d Vi 

### z 0 (INCLUDE MATRIX) 

### z c.. co**~** w w**~** 

### z**~ ~**  <( w :::> 0 0::: 1- 0::: Cl i= u**~** 

### 1 1 3114/2013 PAH XAD Trap #5, Baghouse#5 Run 1 2 1 3/14/2013 PAHFilter, Baghouse #5 Run 1 3 2 3/14/2013 PAH XAD Trap #8, Baghouse#5 Run 2 4 2 3/14/2013 PAH Filter, Baghouse #5 Run 2 5 3 3/14/2013 PAH XAD Trap #1, Baghouse#5 Run 3 6 3 3114/2013 PAH Filter, Baghouse #5 Run 3 7 1 3/18/2013 PAH XAD Trap #7, Baghouse#2 Run 1 8 1 3/18/2013 PAH Filter, Baghouse #2 Run 1 9 

### 2 3/18/2013 PAH XAD Trap #6, Baghouse#2 Run 2 10 2 3/18/2013 PAHFilter, Baghouse #2 Run 2 :I: (,/') <( 0::: 0.. w ""- u.. 

### z CTI 0<( N =1:1: 1- o:::t 

### z t:C 0 0::: u 

# 6 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X 

### 1 X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY:

----------- ---- - ·- REQUESTED ANALYSIS COMMENTS

PAH 1 of 2



### BH#5
' 

### BH#5 BH#5 BH#5 BH#5 BH#5 BH#2 BH#2 BH#2 BH#2 DATE: TIME:

# ~~· 

# • TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-'1 099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### 0 0 Vi 2 0 (INCLUDE MATRIX) 2 0. l:C**~** w w**~** 2 

### !;;(**~** <( w ::> 0 0::: 1- 0::: 

### c i= u <.!) 1 3 3/18/2013 PAHXAD Trap #9, Baghouse#2 Run 3 2 3 3/18/2013 PAHFilter, Baghouse #2 Run 3 3 3/14/2013 PAH XAD Trap #2, Train Blank 4 3/14/2013 PAHFilter, Train Blank 5 PAH XAD Trap#3, NotUsed 6 PAHXAD Trap#4, Not used 

### 7 8 9 10 

### :c Vl <( 0::: 0.. w 

### ....... u.. 2 CT'l 0<( N :tl: 1- o::t 2 c:l 0::: 0 u 

## ('; 1 X 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

PAH 2 of 2

BH#2 BH#2 Blank Blank No analysis No analysis

DATE: TIME:

## TEST, Inc

.. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 www.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN @TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### 0 0 Vi 0 (INCLUDE MATRIX) 

### z z CL 

### :E w w 

### :E co 

### z**~** :E <( w 

### => 0 c:: 1- c:: 0 i= 

### u l? 

### 1 1 3/14/2013 Baghouse #5 PAH Run 1Front-halfRinse 2 1 3/14/2013 Baghouse #5 PAH Run 1Back-halfRinse 3 2 3/14/2013 Baghouse #5 PAH Run 2 Front-halfRinse 4 2 3/14/2013 Baghouse #5 PAH Run 2 Back-halfRinse 5 3 3114/2013 Baghouse #5 PAH Run 3 Front-halfRinse 6 

### 3 3/14/2013 Baghouse #5 PAH Run 3 Back-halfRinse 7 

### 1 3/18/2013 Baghouse #2 PAH Run 1Front-halfRinse 8 1 3/18/2013 Baghouse #2 PAH Run 1Back-halfRinse 9 

### 2 3/18/2013 Baghouse #2 PAH Run 2 Front-halfRinse 10 2 3/18/2013 Baghouse #2 PAH Run 2 Back-halfRinse :c 1./) <( c:: a.. w ........ u.. 

### z en 0 

### <i: N 'O:j" ::1:1: 1- 

### r::c 

### z 0 

### c::: 

### u <( u 

### 1 

### X 1 

### X 1 

### X 1 

### X 1 

### X 1 

### X 1 

### X 1 

### X 1 

### X 1 

### X RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

PAH 1 of 2



### BH#5
I 

### BH#5 BH#5 I 

### BH#5 BH#5 BH#5 I 

### BH#2 BH#2 BH#2 BH#2 DATE: TIME:

## TEST, Inc. 

# Chain of Custody Route 2, Box 33 Poca, WestVirginia 25159 (304) 755-1077, Fx (304) 755-1099 vvww.testincorp.com
PROJECT NUMBER: Tl1550 COMPANY NAME: Felman Productions PROJECT MANAGER: Paul Chinuntdet PHONE NUMBER: (304) 755-1077 EMAIL ADDRESS: PCHIN@TESTINCORP.COM

w 1- SAMPLE DESCRIPTION 

### 0 0 Vi 0 

### z z c.. (INCLUDE MATRIX) 

### :2: w w 

### :2: co 

### z**~** :2: <:!: w :::> 0 0::: 1- 0::: 0 i= 

### u 1.9 1 3 3/18/2013 Baghouse #2 PAH Run 3 Front-halfRinse 2 3 3/18/2013 Baghouse #2 PAH Run 3 Back-halfRinse 3 3/14/2013 Train Blank PAH Front and back halfRinse 4 

### 5 6 7 8 9 10 :c Vl <( 0::: c.. w "'- u.. 

### z (j) 0 

### <i: N -.::!" :tl: 1- 

### co 

### z 0 0::: 

### u <( u 1 X 1 X 1 X

RELINQUISHED BY: DATE: TIME: RECEIVED AT LABORATORY BY: Paul Chinuntdet 3/27/2013 RECEIVED BY: DATE: TIME: NAME OF LABORATORY: REQUESTED ANALYSIS COMMENTS

PAH 2 of 2

BH#2 BH#2 Blank

DATE: TIME:

# ---.......

# ~ 

# ·-**_.,,.,_,,~ U~E.-**  rbent Trap Analysis Report

9nt Name 

## Keika Ventures, LLC 

## act Name Lorri White

9D 

### J.D. Plant/Source Date Analyzed Scientist 156035 Felman 4/10/2013 John Perko 150823 Felman 4/10/2013 John Perko 156060 Felman 4/10/2013 John Perko 156021 Felman 4/10/2013 John Perko 156066 Felman 4/10/2013 John Perko 156064 Felman 4/10/2013 John Perko 156014 Felman 4/10/2013 John Perko 150797 Felman 4/10/2013 John Perko 156042 Felman 4/10/2013 John Perko 156034 Felman 4/10/2013 John Perko 156058 Felman 4/10/2013 John Perko 156006 Felman 4/10/2013 John Perko 156057 Felman 4/10/2013 John Perko 156069 Felman 4/10/2013 John Perko 150824 Felman 4/10/2013 John Perko

s than 0.027 ng Is corisiaered 

### "< LDL."Which-Is lesstnalfthelowest detection limit. :atlon Report Available 

### mty ±1o% 

## I Massng Sect1 0.86 21.06

0.67 0.65 0.51 0.73 0.65 21.20

0.61 19.31 17.28 28.22 26.06 22.55 45.09 VJIIV 1-UIJJC.I\ \JU. 1 IJI\.1. 9263 Ravenna Rd., Unit A-3 Twinsburg, OH 44087 Phone: (330) 405-0837 Fax: (330) 405-0847 www.ohiolumex.com

Project Number2001307 

# D D Other I UJ II • I"'\I VUIJU I JJJIV Standard 48 hour rush



### Date 

## 4/11/2013 Phone 

## 919-933-9569 Massng Massng Spike BreakSect.2 Sect.3 Level (ng) through% 

### Comme. 0.74 Fie 0.54 20 

### Tn: 0.54 

### Tn: 0.61 

### #5 Baahouse 0.52 #5 Baghouse 0.74 #5 Baghouse 0.55 

### #5 Baghouse 0.74 20 #5 Baghouse 0.47 #5 Baghouse 0.72 #2 Baghouse 0.72 #2 Baghouse 0.87 #2 Baghouse 0.72 #2 Baghouse 0.73 #2 Baghouse 0.57 20 

### #2 Baghouse

### APPENDIXG PLANT OPERATIONAL DATA

### 3/18/2013

FCE#2 Time Opened Time Plugged Tap Number Tap Weight Fines Usage Liquid Metal 8:25 8:55 468 10:25 10:55 469 12:25 12:55 470

2:25 2:55 471 4:25 5:00 472 6:25 7:00 473 8:35 9:00 474 10:30 11:00 475 12:35 1:00 476

2:35 3:00 477 4:35 5:00 478 6:25 7:00 479

Total LBS Total NT 

## Note: Production and Raw Material data submitted separately as Confidential Business Information Raw materials consumption



# Redacted With Fines

### 3/19/2013

FCE#2 Time Opened Time Plugged Tap Number Tap Weight Fines Usage Liquid Metal 8:30 8:55 480 10:30 11:00 481 12:30 1:00 482

2:30 2:55 483 4:30 5:05 484 6:25 6:45 485 8:25 9:00 486 10:35 11:00 487 12:35 1:10 488

2:35 3:00 489 4:35 5:00 490 6:25 6:45 491

Total LBS Total NT 

## Note: Production and Raw Material data submitted separately as Confidential Business Information 

# Redacted Raw materials consumption
With Fines

### 3/20/2013

FCE#2 Time Opened Time Plugged Tap Number Tap Weight Fines Usage Liquid Metal 8:45 9:10 492 10:45 11:25 493

1:05 1:45 494 3:20 4:00 495 5:35 6:00 496 7:30 8:00 497 9:40 10:00 498 11:35 10:05 499

1:40 2:10 500 3:30 4:10 501 5:35 6:05 502

Total LBS Total NT 

## Note: Production and Raw Material data submitted separately as Confidential Business Information 

# Redacted Raw materials consumption
With Fines

### SnDo --------------· 

### Name: :JEfF K\OC:>wtj"i

_____ (F) 

### IFlldB, (1/2) 

### Yz Fun? (E) lEmpt; 

### Date:**---~e,** 

### JJ) 

### 13

___________ FUME DUST 

### TRANSlFlERRED TO ll

## ~ :§ftL 

### lfime:**-~55 -~.:i!l_** ____________ Tempering Air Temp: illlllet Temperature: !Baglhlouse BRower

## __1~~---- J?§H**Tm~rnsfeJr** BRower: PSH

---------- StackTemperatllllre: Air PJressruure: 

### [DO
MAGNEHELIC GAUGES On Line Cleaning On Line No 

### 1 Hopper Pressure 

### ___!_l,_InHzO

- ..

## 5" InH2

### 0 No 

### 7 !Hopper Pressure 

### ___t__b__haH!20 No 

### 2 Hopper Pressure 

### _j:__b__IoH2

### 0 _-_l_hBH 2

### 0 No 8JH!opper Pressure**~hnlhO** No 

### 3 Hopper Pressure __:!:__h_HnH2

### 0 --=l__lnH2

### 0 No 

### 9 Hopper Pressure

## _il,o

_ _InH20 No 

### 4 Hopper Pressure ___i_b_InH2

### 0

### ~HnH**0** No 10 Hopper

### Pressure~lnfhO No 5 Hopper Pressure

### ~lnH**0** - 

## .S' InH20 No 11 Hopper Pressure__i_5_hJIHzO No 6 Hopper Pressure __±_f,_InHzO _:_L1uH20
Screw Rotary Bags PSK CDeall1ling 

## -=-l

__[Jlli.!H! 20**~lll1l.!H!z0** 

### -=l_

__l!nHzO _:_i_!nfhO -=-!_Ill1lH20

On/Off Conve:yor Lock Chute Missing No 

### 1 Hopper 

## ON 

## l/ 

# i J_ 0 No 2 Hopper OtJ 

## J 

## / ../ 

## 0 No3 Hopper 01\J ,/ 

### "/ ../ 

### __j_ No 4 Hopper OtJ 

### ./ 

# / ./ 0 No 5 Hopper 

### 0/J 

## / 

## / / 

## 0 No6Hopper 

## oN 

## / / 

### / 

## 0 • No 7 Hopper 

## ON ./ ./ 

# . ./ 

## 0 No 8 Hopper 

## ON / ../ 

### / I No 9 Hopper 

## OM 

## / ,/ 

### ._/ 

### 0 No 

### 10 Hopper 

### otJ ./ 

### / 

## ../ D No 11 Hopper 

### Of\)

### ~ 

# / v' 0

EQUIPMENT PROBLEMS

_______________________ _

MECHANICALWORKPERFORMED

________________ _



### COMMENTS:**B:~G!H!OlJSE,** 

## NUMJBHE!R 4!



# .. d.-
Sino----·----'-"-·-·-··--



### .... Name: ·

# J\:.FF. Ru>Gv.Jf!L_. Date;**_---.;)3~·....1..1 g...__~** **_.,;1.1">.-0,._.,.e;3~.----_** 

### (F)**!FuD~,** 

### 0 /2) 

## Yz Funn, (JE) 

### lEmrtty 

### FUME DUST TRANSFJERRJED TO

### ~~ :!)H.r\!.• Time: ·10:55 

## ft.W\. Tempering Air Temp: Baghollllse Blower Tnnnsffer BRower: 

## _1.5

____PSH !P'SI 

### IDlliet Temperature:
·-----·· 

### StackTemperature: Air Press1llre: 

### _lQ_Q__lP'SH
MAGNEHELIC 

### GAUGES On Line Cleaning On Line No 1 HopperPressure _±_]_inH2

### 0 

# -,.5 lnH2

### 0 No 7 Hopper Pressure _t_linHzO No 2 

### HopperPress1llre __±_]_lnH2

### 0 _:_l_lnH2

### 0 No 8 Hoppew Pwessure**~lnHzO** No 3 HopperPressure _±_}_InH2

### 0 -=-l_InllhO No 9 Hoppew Pressure 

## +7 lnH20 No 4 HopperPressure+ 

## b 5 InH20 _:_!__InH2

### 0 No 10 

### Hoppew PressMre__:t1_l!nHzO No 5 Hopper

### Pressure.\.~InH2

### 0

- ..

## S InH2

### 0 No tl 

### Hopper Pressure 

# A lnH20 No 6 Hopper Pressure _!_]_lnH2

### 0 -=l_lnH2

### 0
Screw Rotary Bags CBeannng =-l_KnH20 

## .-f HnH[zO 

### ::.J_huHzO -=l_RnlH.20 _:.:_/_hnHzO

On/Off ConveJ::or Lock Chute Missing No 1 Hopper 

## ()tJ**~I** 

# ./ 

# -7- 0 No 2 

### Hopper 

### OrJ 

# .J / 0 No3 Hopper 

# ON ./ 

# ./ J I No 4 Hopper. 

### OA.l 

# ./ 

# .L / 

## 0 No 5 Hopper 

### otJ 

# ./ J 

# v 0 No6Hopper 

# otJ**~L** 

## / _/ 

# 0 No 7 Hopper

### o~l 

### J 

# / v' 

# 0 No SHopper 

## ()tJ / 

## / 

# .; I No 9Hopper 

## OtJ**~I ~I**  

## / Q No 

### 10 Hopper 

### ON 

## ./**~** 

## / 0 No 11 Hopper 

# o,J 

# / ../ 

# v 0

EQUIPMENT**PROBLEMS._~---------------------**

---------------------------------- ···---


### MECHANICAL WORKPERFORMED



### COMMENTS:

## Snno

·----·-·------- Name:

## -~~E'"'-f~f___.R~\D...,b..._uJ~f)~i__ Date: 

### 3**_-I~-** J,.O 13 

### (F)**FaA~~.** 

### (l/2) 

### y; !FUABI, (E) Emplt) FlUME DUST TRANSFERRED TO 

### Fl

# J. :<ml •: '· 

### Time: 

### 11:55 A ,(Vl. 

### Tempering AirTemp: Inlet Temperature: 

### ___ oF 

## ow lBagllno!U!se Blower T!rams1fer BDower: 

## _L_$"

__PSH PSH



### --- -----·- 

### StackTemperature: 

## ow Anlr**P~ressttme:** 

### j.Qn__lP'Si
MAGNEHELIC GAUGES On Line Cleaning On Line No 1HopperPressure __±__fo__InH2

### 0**~InH 0**  

### No 7 Hopper Pressure i..k_..,S_InHzO No 2 HopperPressure**~InH 0**  

### -=-l_InH2

### 0 No 8 Hopper Pressmre**~InHzO** 

### No.3 HopperPressure

### +b 

## S InH2

### 0 _:_l_hoH2

### 0 No 9 Hopper Pressure**~inHzO** 

### No 4 HopperPressure __±_k_InH2

### 0 

### -=-l_InHzO No JO 

### Hopper

### Pressure~inHzO No 5 HopperPressure+'

### .S InH2

### 0

### ~InH**0** No tt 

### Hoppe1r Pressure ;- 

### SInH2

### 0 No 6 HopperPressure -=tk_InHzO 

### _::_l_tnHzO
Screw Rotary Bags Cleamil:llg _::__l__BnH20**~lnHizO** 

### _:l_

__linH 20 

### _::j_nnflhO 

### _:::_1__hniH!zO



### On/Off Convexor Lock

# ~ Missing No 1 Hopper 

## otJ

# ~ .I 0 No2 Hopper 

### ON 

## ./ 0 No3 Hopper 

# ON / 

# v / l No 4Hopper 

## otJ 

## ./ ./ 

## ./ () 

### No SHopper 

### orJ 

# / / ,/ 

### 0 No 6 Hopper 

### f)j\) 

### ,/ 

## ./ / 0 No 7 Hopper 

## otJ ./ ,/ ,/ ()



# .. No SHopper 

### ON 

# L ./

..L I No 9 Hopper ({)N 

### t/ 

# vi 1/ 0 No 10 Hopper Q{\) 

## ./**~** 

## / 0 No 11 Hopper 

# orJ ,L_· 

## J 

# ../ 0

EQUIPMENT PROBLEMS

_______________________ _

MECHANICALWORKPERFORMED



### COMMENTS:



### --

.. ...;

### BAG!H(HJSF' NUMBER: 

## -tl 

## d.-.

Name: 

## 1-t.t=F-__

## RJ-DG\.J~i Date:

__**3_l~_:_¢Q_**

## L3**Time:~** 

## 55 P

..**~«<--=.......-**___ _ 

### Tempering AirTemp: Inlet Temperature: StackTemperahure: 

## Snno

-------·- ----· .--- 

### (JF} Fo.nnn. (1/2) 

### Yz !FudD, (IE) 

### Emp1ty FUME DUST TRANSFEJRJRJED TO

__ 1:1

### ~ :'W1_ ·':·
JBagiJ:nOII.USe 

### JBDower Tmnsfer BDower: Air Press\Ulre: 

### _L_S

___ 

## Pm IP'SH

··--------- _\_Ql)__IP'SB


### MAGNEHELIC 

### GAUGES On Line Cleaning 

### On Line Cleaning -=.._{ _B'1111H20 

# =-1_hul!-i!J,O -=j__B1111H 20 

### =-l_I nll-izO**~j__**

### __ID1lH20 

### No 1 

### Hopper Pressll.llre -:!:..k.5:._In.H20

- •

## .5" InH20 

### No 7 

### Hopper Pressllllre

## tfo_!

..:S.JnH20 No 2 

### Hopper**Pressure~** 

### b.S lnH20 

### =-J_InH20 

### No 8 

### Hopper Pressure

### -1-b ,5InH20 

### No 3 

### HopperPressure**~InH 0**  

### _:_l_lnH20 

### No 9 

### Hopper Pressure**~inHzO** 

### No 4 

### Hopper Pressure _.::!:__k_InH20 

### _::_LinH20 

### No to 

### Hopper Pressure-+.-G:,,S inH2

### 0 No 

### 5 Hopper

### Pressure+~ 

### ,S InH2

### 0 ..,.. •

## 0 InH2

### 0 No 11 

### Hopper Pressure_!___§_bnHzO No 6 Hopper Pressure -1-- 

## b.S In.HzO 

### -=-L_InH20



### No 1 Hopper No 

### 2 Hopper No3 Hopper No 4 Hopper No 5 Hopper No 6Hopper No 7 Hopper No SHopper No 9 Hopper No 10 

### Hopper No 11 Hopper On/Off 

### o#J 

## ON ON 

## ON otJ ()t.J 

# ON OtJ 

## OrJ ON 

# ON Screw Conveyor 

### j 

# I ./ / / Rotary Lock



## / 

# / 

# / ./ / 

# / / 

## ./ / ./ /**~·** ... /



## ... Bags Missing () 

### 0



## I 

## 0 0 0 C)



### I 

### 0 () Q


### EQUIPMENT PROBLEMS.

_________________________ ..________

MECHANICAL WORKPERFORMED

_____________________ _



### COMMENTS:Sillo**·-~--- -~·-··**  .... ···--· 

### (JF) lFIIllfii, (J!/2) 

### Yi Fullll, (IE)**~t<:mpt;** 

### FUME DUST TRANSfi'!ERRED TO
Tempering Air Temp: lnBet Temperature: ___ "F "F 

### Baghm.11se BRower Translfer BRower: _l_l_S__PSH lP'SH



### --- -------- 

### Stack 'femperatmre: "F



### --- Air Pressure: 

## j_Ql.)_lP'SU


### MAGNEHELIC GAUGES On Line Cleallling Olll Lnne No l HopperPressure .i._k_InH2

### 0 :_tz..S:.JnHzO No 7 Hopper Pressuure 

### _±j,_InfhO No 2 HopperPressure _±.]_1nH2

### 0 -=J_InH2

### 0 No 8 Hoppell" Pressull"e

### ~lnHzO No 3 HopperPressure _±_llnH2

### 0 ...:::_LinH2

### 0 No 9 HopperPnessul!lf'e _-t_l_InHzO No 4 HopperPressure 

## -+ {a inH2

### 0 -=:l_!nH2

### 0 No 10 

### Hoppell"

### Pressure"!-~ 

## .5' lnH20 No 5 HopperPressure 

# +! InH2

### 0 =+-InH2

### 0 No 11 

### Hopper

### IPressure~lnHzO No 6 HopperPressure _k_d_InH2

### 0 _::l_lnHzO
Screw Rotary Bags Cleaning



# ..::J

____ll.lli1H20 

# --=-'-KnlHI 20 -=--LHnH 20 .=_!_lnH 20 

# -=i

__Hlrn!HbO



### On/Off Conveyor Lock Chute Missing 

# I No 1 Hopper 

### ON 

# J 

# / 0 No 2 Hopper 

## ON 

# J ./ 

# I () 

### No3 Hopper ON 

# / ,/ 

# J \ No 4 Hopper 

### orJ 

# .J / 

# / 0 No 5 Hopper Ql\) 

## ·L ..1 

# J 0 No 6 Hopper 

## o&0 ,_/... 

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### 01\J ,/ 

## D No 11 Hopper I() 

### 1\) 

# ./ / I ()

EQUIPMENT PROBLEMS.

______________________ _

MECHANICALWORKPERFORMED

__________________________ _



### COMMENTS:

## Snno**--~---------------** (F)**F~Hi,** (1/2)**~** FudH, (E) 

### !Emptr·; 

### FUME InJST TRANSFJE.RRED TO

__

# #_J,_ SH

...

/ 

### Tempering Air Temp: !Baglhtol!llse**BB~we_r** 

### Transfer.BRower: 

# _L,.S

_____)P'S

### n Inlet Temperature: StackTemperatmre: Air Piressume:
MAGNEHELIC GAUGES On Line Cleaning


### . On Line

...... . 

### No I Hopper**Pressure~I.nH 0**  

### -**.~** 

### InHiO No 7 Hopper Pressure _±1_InH! 2

### 0 No 2 HopperPressure·_±_]_inH2

### 0 --=l_InH20 No 8 Hoppen:: ·Pressure +C..S InHzO No 3 Hopper

## Pressure~_lnJ-1**0** -=-l__InHzO No 9

## Hoppe~**Pres~re** .!.b_,S)nlHzO No 4 HopperPressure**~lnH 0**  -=-l_InH2

### 0 No !0 

### Hopper Pressure...:tJ:u2inH2

### 0 No 5 Hopper

## Pr.essur~**~inH 0**  -

## ~S lnH2

### 0

## N~ H

## .Hopp~r**PtessUJure~hnlhO** No 6.Hopper Pressure 

### + 

## b 5 lnH20 

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Screw Rotary. Bags lP'SH

CDeaning 

### -I ln.H. 20 _-_l_lnll·llzO 

### -=:__l

____huthO -=L_nnlHzO 

## -=-1-**InlH~.o**



### On/Off Conve::ror Lock Chute Missing No 1 Hopper 

### otJ 

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# / 0 No2 Hopper 

# ON / 

# .I / 0 No 3 Hopper 

## OrJ 

# / 

# / ,/ No 4 Hopper f OtJ 

# ,/ 

# / I 0 v 

# . No 5 Hopper ·**o~J** 

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# J • No 6 Hopper 

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# / / 0 No 7 Hopper 

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### otJ

## ~ 0 No 10 Hopper 

## ot-> 

# -/;_ / /J 0 No 11 Hopper 

### OJ\j 

# I / 

# / ()

... 

### EQUIPMENT PROBLEMS

______________________ _

MECHANICAL WORKPERFORMED ·--------......,----------- -------.



### COMMENTS:



## ----------------------------------------N21me:

### ---~E...rr__R~~~\~~----­ DSJte; 

## _'J**:J-1{~--Q.--------------** 

### __ Tum.e·

_ _ __**_3_:~-~Q**

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Sta<ek Tempewatmre: ___ "F "JF Anw PwessiUlrrre: 

## \00 PSH
MAGNEHEUC GAUGES On Une Cleaning On Liil!lle No 

### »Hoppew PresslU!rne j:___:]_htH20

- ..

## .$" hnH 20 No 7 Hojpper JP'wessilllrre 1:-- 

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### 5 Hopper Pressure 

### -+ 

# l InEbO 

### -.!:; InllhO No 11 Hopper Pressu.nre

## _tk_llllllHI20 No 6 Hopjper Pressure 

# -\-·l InHzO -=l_lllllH[zO
Scwew Rotary Bags CHealllling 

# ---=J

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On/Off Conveyor Lock Chute Missing 

# T No 1 Hopper Ob.J 

## I I 

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### otJ 

# J 

# J / 0 No 3 Hoppew**6~** 

# J 

# J ./ I No 4 Hopper 

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# J J ', 

## 0 No 5 Hopper 

### O!V 

## vi 0 No 6 Hoppew 

## otJ ./ ./ / 

## 0 No 7Hoppew 

## otJ J 

# ,_/ ./ 

## 0 No 8 Hopper 

## O/'J 

# ../ ._/ ,/ I No 9 Hopper 

### orJ 

### .,/ 

## ,/ / 

## 0 No 10 Hopper 

### otJ 

## J ,/_ 

### ,/ 

# 0 No 11 Hopper 

# oJ J / 

# I 0

EQUIPMENT PROBLEMS.

_____________________________**~--**

MECHANICAL WORK PERFORMED



### COMMENTS:**~l-~** "t, .1':.'1. R .· R 'k 'Ill J;l J::L.: "", , M ""'-· !.t .:**.~** I' J.' Ill II! •·.**~** !/**.~** I;{ !/ R" 

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## 3 -• 0 • ' 0 

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## TO--~-~_ SHL(;, 

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## ______ Tempering AirTemp: !niet Temperat111re: StackTemperature: 

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--- Baglnouse lBDower Transfer Blower: Anr PressMil"e: 

# d

. '() JP'SR PSH

---- -10 

### 0 PSH


### MAGNEHEUCGAUGES On LiMe 

### Cleaning On Lnne CYeaning

### -=~_{_lnH**0** .No 1 Hopper Pressure 

# + / in:U20 ._.

## 5 InH20 No 7 Hopper Pressmre __:!_LinHzO No 2 Hopper Pressure _:tllnH20 --=-l_InH20 No 8 Hopper Pressure

### ~inHzO No 3 Hopper Pressure _t]JnH 20 -=i-huH 20 No 9 Hoppel!" Pressure _8hnHzO No 4 Hopper Pressure**~inH 0**  _::_LinH20 No 10 Hopper Pressunre_j:_]_InHzO No 5 Hopper Pressure 

# + flnH20 ..:::..__,_£inH20 No II Hopper Pressure ____±_hlnHzO 

### --=--L._HnlHI20 -=-l_huH20**~inl-hO** 

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