Projfd 10: 40942525 

ACEMOl/IQ 

7720 

·I """"., I p,....T .. tCEMS Run No. CyUnderVa ~.te CEMS n me Response Resoonst 

Runt 2.07 2.00 08:01 2.02 

11.00 1().85 08;03 10.85 

Run2 07 2.00 09:31 2.02 

11.00 10.85 09:33 10.87 

Runl ~01 2.00 10:21 2.02 

11.00 10.85 10:23 1.0.89 

Run4 = 2.00 10:57 2.01 

11.00 10.85 10;59 10.86 

RunS Ui1 2.00 11:34 2.01 

11.00 10.85 11:35 t0.86 

Run 6 01 2.00 12:;12 2.02 

11.00 10.85 l 2:J4 10.85 

Run7 ~-01 2.00 12:54 1.83 

11.00 10.85 12:58 10.70 

Run S UJ1 2.00 U:l:l 2.00 

11.00 10.85 J3:3S 10.81 

Run9 Ul7 2.00 .. ,,~ 2.00 

11.00 10.85 14:1• 10,78 

RunlO Ul7 2.00 14:52 1.82 

11.00 10.85 1•1:54 10.12. 

Veolla Sauget Unit 3 RATA 

Wet 0 1 Calibtation Da1a Summary 

Calibration Error Tnt Ruults 

CylindttiO etrtifitd vaw. nmt C£M RtJpons.t 

JefOJt!S CC121944 2 .07 07:SS 2 .00 

span cas CC18966S 22.50 0? ~1 2.2.48 

mid-raN!e CCJS7679 11.00 08:00 10.8S 

a MS Calibration 8 i3s and Drift Tests 

.... POSt·TestCEMS Bias "''k 

(."of Span} nmo (:.::.:::' (%of Sp•n} 

s ........ Response '·'"'''""' 

0.1$ 09,31 2.02. 0 .1" 0.0% 

0.0% 09:33JJ 10.87 0.1" 0.1% 

0.1% 10;21 2.o2 0.1,. 0.0% 

0.1% 10:13 10.89 0.1" 0.1% 

0.1$ 10:57 2.01 .0~ 0.0% 

0.1% 16!59 10.86 O.OS< -O.lSIIi 

0.0!( 11:34 2.01 c.o" 0.0% 

0.0'~ U :lS 10.86 0.0" O.OK 

o.cm 12.:-12 J 2.02 0.1% 0.0% 

"·"" 12!14 lO.SS 0.0!6 .().1?5 

0.1% rl2:5'4 . 1.83 •I ·0.8'14 -0.8'36 

0.0% .12!S8 .10.10 ·0.7" ·0.7% 

.0.8% 13:~1 2.00 0.0% 0.8% 

.0.7% u:as· .lD.81 ·0.2" O.S% 

0.0% "1 4:13 2.00 o.o" 0.0% 

.0.2% 14:14 .l0.78 

• 

·0.3%- -0.2!< 

0.0% 14:52 1.82. ·0.8% .0. ~ 

•O.l91. 4: ~ ::10.12 ·3.2"- -2.9" 

.0.8% lS:48 2.0< 0.211 '·"" ·3.2% l.S:SO ..U0.94 0.4" 3,6% 

B·2 

Absolute tal Error 

Diff«ence '"of ""'•' 

2 JJ% Umit 

0.07 0 .3% 

O.o2 0.1,. 

0.15 0.6~ 

~ ?E-S 

to• 2.017 

UC...·CQI 1.244 

C..= 2.0l7 

C..J(C..,.Co) 1.241 

Co• 2.015 

c...JIC.,..C(I) 1.'2.42 

c,~ 2.012 

<..1«.·<.1 1.243 

C.,o; 2.0 13 

c..I<C.-<.l '· 244 

Co· 1.924 

r:...,Jfc...-ccJ 1.24:?. 

Co= 1.918 

C'w/tc""Co) 1.244 

Co• 2.000 

C..JK .. ·C.J U .SO 

~· 1.906 

c...ttC..·CJ 1.'287 

C.= 1.927 

L -- C'~w-C'(.)l 27$ 

A-14{; 

VESO I2600 
Proie« ID: 40942SZS 

1440 

1ero1as 

~I'IJillf. 

mld loi~I(Q 

1 Cal Error nme IPr .. lestCEMS 

.... Run No. ('flindtr Vatue CtM$ {" of Spl!ln) 

........ Rts90M4 S.O"Limlt 

Runt 0.00 -<>.05 07:48 2 0.1" 

11.00 10-94 08:0! "10.9 3 0.0% 

R~o~n2 0.00 -o.os 09':27 0.03 M% 

n .oo 10.94 09:33 10.90 ..0.2W. 

Run3 0.00 ..0.05 tO:lS 0.04 Q.4% 

11.00 1094 10:23 10.90 -<),2)l< 

Run4 0.00 .o.os 10:$3 0 .04 0.4)6 

11.00 10.94 10:$9 10.89 -<) ~ 

A.uoS 0.00 ·O.OS 11:30 0 .04 0 .4\16 

11.00 10.94 11:35 J0.&9 -D.2" 

Run6 0.00 ·0.05 12:08 0.04 C.4" 

11..00 10.90 12:14 10.89 -<),291 

~~n 7 o.oo ·O.OS 12:51 0.04 4~ 

11.00 10,94 U:SS 10.91 -<).194 

Run8 0.00 ·O.OS 13:30 0.04 0.4" 

11.00 10.94 13:35 1Q.89 -o.2'l< 

..,4, I 

Aun9 o.oo ·0.05 14:0S O.D4 0.<1" 

11.00 10.94 14!1A 10.SS -<).3% 

Run tO 0.00 -<l.OS 14:48 OD3 0.306 

11.00 10.94 14!54 10.89 .0.2% 

Veolia Sauget Unit 3 RATA 

Dry 02 Calibration _ Data SUmmary 

CMibtatloon Error Test 1\Qsuh$ 

Cyinder 10 Certified Value Tim• 

52 40019ll57~1A 0.00 07:31 

CC18966S 22.50 07:113 

CC157679 11.00 0?:34 

C£MS Cilibriltion Bias. mel Drift Tests 

Post-Test CfMS .... Tlmo ("-of Span) R~l'l$tl S.O!<Umit 

09:27 0.03 0.3% 

09:33 10.90 -<).2% 

10:~ 0.04 (),4% 

1fY.23 10.90 ·0.2% 

0:~ 0.04 M" 10'.59 10.89 ~" 

=> 

ll:jl> 0 .04 0.4'!6 

tt:lS 10.89 ·0.2" 

12:08 

I 

0.04 0.4" 

JJ 10.89 ·0.2% 

J 0.04 0.4" 

1,2.:58 10.9 1 ·0.1% 

U :30 0.04 OAIJ( 

13:3S' 10.89 -<).1;% 

14:08 

=> 

I 0.0< 0.4% 

,14:14 10.88 .0.3:96 

14:48 l 0.0 3 I 0.3'1 

14:5:4 10.89 I .0.29(; 

15:45 - 0.04 Q.4% 

- 0 \ o.s6 .(),4_9$ 

B-3 

AMCMt C81Etr« 

CEM~.e Olff ~ '" ol Soan) 

1.0% Umlt 

-o.os o.os 0.2% 

22.68 0.18 0.8% 

10.94 0 .05 11.3% 

Dfif't 

of ~n) Eq, 7E-S 

3.0'K.UMit 

0.2% c.:- 0.006 

·0 .2% C....!!Ctr<'o! 1.008 

0 .0% <.:.· 0.034 I 

O.OK Yt~ .Ol2 

o.o" Ce- 0.040 I 

0.0% <fiJlC,·Col L013 

~ "'"0.039 

0.0% C.,JiC..<ol 1..014 

··"" ""0.037 o .... C.....AG..<oi 1.014 

0.0% c.;- 0.037 

0.1% C..~l Oll 

0.0% Ct• 0.038 

.0.1% {...,/((.~ 1.013 

0.0% G;•0.041 

0.0!< tw/((w~ l.OtS 

-o.t% ~~ 0.037 

0.00> C.wfjC..,.c,.)i.Ol4 

0. ~ ~" 0.034 

·0.1% ('..J'fC:.rCPI l.OlS 

A·147 

VES012601 
~il "U! t a ... w '!; >' ~dd 3!!:3 • N 6~ ~:: p ~ ~~ =:e H 5§ ~ ;:: s !! § :OS ::l o ~~ NO .. Q..i ci ..i .;.; o!l ~ 9.; 9 .; ~ ,q .1~ .l-3' H .l-~ 3-3' H ~~ .:t ~ .11 • 5 i ~ i ~ ~ 5 j ; ~ a~a J J J ! • 

"'"' <iS 

• < C' 

.<.:! 

a 4H ~H "'"' 

""' S2 ~~ ~~ "'" ,. "' ~~ Ui .... ;; -: 4d 6d ~~ ~ ~ 

" H o9 qq q<;> o, q ~ ..1..; 

:; 

w 

... " 

~ 

J:u " i JH ~ 0 

~~ '~'"' .... H .... "'" "'"' as .... e "'"' E s~ s ~ ~ ~ ~ ~ N"l ~ .. ~~ ~~ " ·-a~ .;a 00 d9 9-! o-: q~ .. ~ .. • j 1- .. ... ~ - - ~I .,. § > om~ 

a~ ., m "1 ~ ~ i*- ~; ""':::! ~a '"""'! 1l gi ~ ~ ~ O't/ d'9 q .. ~ 0 ... ':/ 

! ~ l~ l • I j l-- < 

~ I !l ~~01 ~ ~ . !=1~ == ~~. ~~ ~~ ~ :; ~ z ~ ~ 

~ ~ ll= ~ ~; 

{ §!lg 0: ~ ~ ~s: ~~ N N :::.-. m m 00 - ~ ~ ~ :.~ !I !I 

v .. .. 

-- -- C\ ~ 

Ui 'i' ,<,:! Hi • E b'; ~:§ "" ~a "~ ~~ .... • E ~~ u ~ ! ~ .,., d<? N -

o9 

d cj o q ~ 0~ d<:> qf ~ .. f-;;-

lE I 

tj i ~"! ~., ~ .. a~ N". 

~ ~- .. "! Nm "" li P: d~ 0~ 0~ q; 90: 9~ "'"' dri ~ ... . . i: 

r'-

:.; ~ '9~ [:;ill ~!!I ~~ ~;1 ~ 0 

- m ON <;?";"! '(!I(! .,., 1'1 ::1 ~Iii :l. S§ SIS !'ill ::: :: ~!::! :::~ :::: ::. ... -~ ~ ~ 

0~ 

<:- Iii" u _gj § 

i! t ~ ., ., ., ., H ~~ :; ; ; ~; ~~ H mo 

. .. .. 0! .. .... . ~I '? '9 ~ 

~::, ~.e:; <? ~ ~r~: .. i n:sj -i c ... -!t;l! r-r 

! f.P ~ !: o"! o"! q"! ::1 ~:d o"l om om om o"! i"_ .. i ci' .... o'9 0~ o'.# 0'4 d'# o '9 - e o . o . 

; !~ 0 ~ s 

I 

- N m .. .. ... ... ' ~ 0 

• • c J c c • i ~ 

j , , , i! i , i! c 

"' "' " "' , 

.. 
APPENDIXC 

Unit 3 CEMS Relative Accuracy Data 

A-149 

VES012603 
Time. stamp CO DryCorr 02Wet 02Dry H20 

9/S/13 9:04AM 0.00 8.89 13.46 33.97 

9/5/13 9:05AM 0.00 8.88 13.51 34.19 

9/5/13 9:06AM 0.00 8.62 13.12 34.13 

9/5/13 9:07 AM 0.00 8.14 12.33 34.05 

9/S/13 9:08AM 0.00 8.25 12.73 34.95 

9/S/13 9:09AM 0.00 8.62 13.30 35.14 

9/S/13 9:10AM 0.00 8.44 12.89 34.62 

9/5/13 9:11AM 0.00 8.42 12.98 35.11 

9/5/13 9:12AM 0.00 8.72 13.47 35.29 

9/5/13 9:13AM 0.00 8.48 12.98 34.67 

9/5/13 9:14AM 0.00 8.35 12.89 l5.16 

9/S/13 9:15AM 0.00 8.74 13.48 35.27 

9/5/13 9:16AM 0.00 8.77 13.32 34.24 

9/S/13 9:17AM 0,00 8.74 13.28 34.19 

9/S/13 9:18AM 0,00 8.95 13.65 34.42 

9/S/13 9:19AM 0.00 8.69 13.18 34.04 

9/5/13 9:20AM 0 .00 8.51 13.00 34.63 

9/5/13 9:21AM 0.00 8.74 13.50 35.19 

9/5/13 9:22AM 0.00 8.62 13.13 34.33 

9/5/13 9:23 AM 0.00 8.41 12.85 34.57 

9/5/13 9:24AM 0.00 8.69 13.46 35.36 

Average 0.00 8.60 13.17 34.64 

Unit3 Run 1 09/05/13 

C-1 A-1150 

VES012604 
Time~Stamp I CO OryCorr 02Wet 020ry H20 

9/5/13 9:53AM 0.00 8.40 12.94 35.03 

9/5/13 9:5-4A.M 0.00 8.58 13.13 34.72 

9/5/13 9:55AM 0.00 8.65 13.19 34.44 

9/5/13 9:56AM 0.00 8.63 13.14 34.34 

9/5/13 9:57A.M 0.00 8.26 12.62 34.58 

9/5/13 9:58 A.M 0.00 8.83 13.71 35.66 

9/5/13 9:59 AM 0.00 8.47 12.95 34.61 

9/5/13 10:00 AM 0.00 8.67 13.46 35.27 

9/S/13 10:01 AM 0.00 8.89 13.64 34.82 

9/5/13 10:02 AM 0.00 8.76 13.29 34.05 

9/5/13 10:03 AM 0.00 9.20 13.93 34.10 

9/5/13 10:04 AM 0.00 9.07 13.56 33.12 

9/5/13 10:05 AM 0.00 8.72 13.12 33.53 

9/5/13 ·10:06 AM 0.00 8.46 13.00 34.84 

9/5/13 10:07 AM 0.00 8.74 13.54 35.48 

9/5/13 10:08 AM 0.00 8.63 13.11 34.29 

9/5/13 10:09 AM 0.00 8.60 13.09 34.24 

9/5/13 10:10 AM 0.00 8.52 13.03 34.57 

9/5/13 10:11 AM 0.00 8.76 13.50 35.03 

9/5/13 10:12 AM 0.00 8.60 13.10 34.36 

9/5/13 10:13 AM 0.00 8.43 12.89 34.61 

Average 0.00 8.66 13.23 34.56 

Unit 3 Run 2 09/0S/13 

C·2 A-151 

VES012605 
Tlme_Stamp I CO OryCorr 02 Wet 020ry H20 

9/5/13 10:30 AM 0.00 8A6 12.94 34.63 

9/5/13 10:31 AM 0.00 8.61 13.31 35.41 

9/ 5/13 10:32 AM 0.00 8.54 13.16 35.03 

9/5/13 10:33 AM 0.00 8.46 13.00 34.99 

9/5/13 10:34 AM 0.00 8.46 13.04 35.11 

9/S/13 10:35 AM 0.00 8.70 13.38 34.96 

9/5/13 10:36 AM 0.00 8.89 13..53 34.23 

9/5/13 10:37 AM 0.00 8.79 13.27 33.84 

9/5/13 10:38 AM 0.00 8.63 13.18 34.55 

9/5/13 10:39 AM 0.00 8.72 13.50 35.31 

9/5/13 10 :40 AM 0.00 8.78 13.50 34.95 

9/ 5/13.10:41 AM 0.00 8.65 13.25 34.69 

9/5/13 10:42 AM 0.00 8.60 13.24 34.98 

9/ 5/13 10:43 AM 0.00 8.74 13.44 35.00 

9/ 5/13 10:44 AM 0.00 9.00 13.67 34.28 

9/5/13 10:45 AM 0.00 8.87 13.34 33.57 

9/5/13 10:46 AM 0.00 8.72 13.24 34.15 

9/5/13 10:47 AM 0.00 8.70 13.36 34.99 

9/5/13 10:48 AM 0.00 8.76 13.48 34.97 

9/5/13 10:49 AM 0.00 8.59 13.15 34.68 

9/5/13 10:50 AM 0.00 8.54 13.15 35.08 

Average 0.00 8.68 13.29 34.73 

Unit3 Run3 09/05/13 

C·3 A-151 

VES012606 
Tlme_Stamp CO DryCorr 02Wet 02Dry H20 

9/S/ 13 11:08 AM 0.00 8.71 13.41 35.16 

9/ S/ 13 11:09 AM 0.00 8.58 13.08 34.35 

9/ 5/13 11:10 AM 0.00 8.51 13.09 34.85 

9/5/13 11:11 AM 0.00 8.51 13.11 35.10 

9/S/13 11:12 AM 0.00 8.76 13.41 34.73 

9/5/13 11:13 AM 0.00 8.65 13.08 33.91 

9/5/13 11:14 AM 0.00 8.56 13.03 34.32 

9/5/13 11:15 AM 0.00 8.47 13.02 34.95 

9/S/13 11:16 AM 0.00 8.65 13.33 35.13 

9/S/13 11:17 AM 0.00 8.51 12.98 34.51 

9/ 5/13 11:18 AM 0.00 8.47 12.99 34.71 

9/5/13 11:19 AM 0.00 8.44 12.97 34.93 

9/5/13 11:20 AM 0.00 8.60 13.18 34.84 

9/5/13 11:21 AM 0.00 8.35 12.69 34.29 

9/ 5/13 11:22 AM 0.00 8.32 12-80 34.95 

9/S/ 13 11:23 AM 0.00 8.29 12.92 35.67 

9/5/13 11:24 AM 0.00 8.90 13.85 35.78 

9/5/13 11:25 AM 0.00 9.22 13.96 34.02 

9/5/13 11:26 AM 0.00 9.11 13.66 33.21 

9/5/13 11:27 AM 0.00 8.71 13.13 33.58 

9/5/13 11:28 AM 0.00 8.77 13.34 34.12 

Average 0.00 8.62 13.19 34.63 

Unlt3 Run4 09/0S/ 13 

A-153 

VES012607 
Ti,.,_Stamp CO OryCorr 02Wet 02Dry HZO 

9/5/13 11:46 AM 0.00 8.18 12.55 34.87 

9/5/13 11:47 AM 0.00 8.25 U .80 35.58 

9/5/13 11:48 AM 0.00 8.38 12.96 35.24 

9/5/13 11:49 AM 0.00 8.29 12.66 34.50 

9/5/13 11:50 AM 0.00 8.29 12.74 34.92 

9/5/13 11:5·1 AM 0.00 8.30 12.82 35.27 

9/5/13 11:52 AM 0.00 8.07 12.46 35.14 

9/5/13 11:53 AM 0.00 8.23 12.83 35.78 

9/5/13 11:54 AM 0.00 8.42 13.14 35.98 

9/5/13 11:55 AM 0.00 8.67 13.47 35.65 

9/5/13 11:56 AM 0.00 8.58 13.15 34,71 

9/5/13 11:57 AM 0.00 8.57 13.16 34.78 

9/5/13 11:58 AM 0.00 8.61 13.25 34.96 

9/5/13 11:59 AM 0.00 8.63 13.29 35.04 

9/5/13 U:OO PM 0.00 8.66 13.34 35.08 

9/S/13 12:01 PM 0.00 8.74 13.47 35.11 

9/5/13 12:02 PM 0.00 8.80 13.51 34.89 

9/5/13 12:03 PM 0.00 8.81 13.45 34.53 

9/5/13 12:04 PM 0.00 8.67 13.22 34.42 

9/5/13 12:05 PM 0.00 8.64 13.25 34.73 

9/5/13 12:06 PM o.oo 8.95 13.68 34.61 

Average 0.00 8.51 13.11 35.04 

Unit 3 RunS 09/05/13 

c-5 >.154 

VES012608 
Time_Stamp CO DryCorr 02Wet 02Dry H20 

9/S/13 12:26 PM 0.00 8.51 12.76 33.44 

9/5/13 12:27 PM 0.00 8.56 12 .. 99 34.02 

9/5/13 12:28 PM 0.00 8.57 12.94 33.85 

9/5/13 12:29 PM 0.00 8.67 13.09 33.70 

9/5/13 12:30 PM 0.00 8.72 13.23 34.12 

9/5/13 12:31 PM 0.00 9.02 13.71 34.28 

9/5/13 12:32 PM 0.00 8.88 13.37 33.57 

9/5/13 12:33 PM 0.00 8.81 13.29 33.72 

9/5/ 13 12:34 PM 0.00 8.95 13.56 34.02 

9/5/13 12:35 PM 0.00 8.98 13.50 33.54 

9/5/13 12:36 PM 0.00 8.85 13.19 32.92 

9/5/13 12:37 PM 0.00 8A7 12.70 33.34 

9/5/13 12:38 PM 0.00 8.31 12.65 34.31 

9/5/13 12:39 PM 0.00 8.11 12.42 34.76 

9/5/13 12:40 PM 0.00 7.93 12.25 35.22 

9/5/13 12:41 PM 0.00 7.95 12 .. 46 36.16 

9/5/13 12:42 PM 0.00 8.06 12.68 36.38 

9/5/13 12:43 PM 0.00 8.23 12.78 35.63 

9/5/13 12:44 PM 0.00 8.69 13.44 35.35 

9/5/13 12:45 PM 0.00 9.11 13.97 34.82 

9/5/13 12:46 PM o.oo 8.86 13.44 34.06 

Average 0.00 8.58 13.07 34.34 

Unit 3 Run 6 09/05/13 

C·6 A-155 

VESOl2609 
Time_Stamp CODryCorr 02Wet 020!1: H20 

9/5/13 1:08PM 0.00 8.28 12.63 34.53 

9/5/13 1:09 PM 0.00 8.38 12.86 34.73 

9/5/13 1:10PM 0.00 8.51 13.07 34.84 

9/5/13 1:11PM 0.00 8.69 13.32 34.82 

9/5/13 1:12PM 0.00 8.56 13.12 34.63 

9/5/13 1:13PM 0.00 8.50 13.14 35.31 

9/5/13 1:14PM 0.00 8.60 13.35 35.52 

9/5/13 1:15PM 0.00 8.89 13.64 34.80 

9/5/13 1:16PM 0.00 8.80 13.32 33.96 

9/5/13 1:17PM 0.00 8.73 13.27 34.24 

9/5/13 1:18PM 0.00 8.66 13.25 34.61 

9/5/13 1:19PM 0.00 8.59 13.19 34.85 

9/5/13 1:20 PM 0.00 8.00 12.23 34.59 

9/5/ 13 1:21 PM 0.00 8.03 12.39 35.22 

9/5/13 1:22 PM 0.00 8.24 12.78 35.43 

9/5/13 1:23PM 0.00 8.59 13.26 35.26 

9/5/13 1:24PM 0.00 8.61 13.13 34.49 

9/5/13 1:25 PM 0.00 8.76 13A2 34.63 

9/5/13 1:26 PM 0.00 8.79 13.45 34.61 

9/5/13 1:27 PM 0.00 8.98 13.68 34.39 

9/5/13 1:28 PM 0.00 8.55 12.84 33.44 

Average 0.00 8.56 13.11 34.71 

Unit3 Run7 09/05/13 

C·7 A-156 

VES012610 
Time Stamp CO DryCorr 02Wet 02 Dry H20 

9/5/13 1:46 PM 0.00 8.33 12.74 34.63 

9/5/13 1:47 PM 0.00 8.62 13.20 34.74 

9/5/13 1:48PM 0.00 8.71 13.34 34.63 

9/5/13 1:49 PM 0.00 9.06 13.86 34.62 

9/5/13 1:50PM 0.00 9.03 13.67 34.02 

9/5/13 1:51PM 0.00 8.84 13.42 34.14 

9/5/13 1:52 PM 0.00 8.67 13.27 34.67 

9/5/13 1:53 PM 0.00 8.77 13.43 34.71 

9/5/13 1:54 PM 0.00 8.94 13.55 33.98 

9/5/13 1:55 PM 0.00 8.74 13.13 33.49 

9/5/13 1:56PM 0.00 8.67 13.22 34.42 

9/5/13 1:57 PM 0.00 8.63 13.30 35.15 

9/5/ 13 1:58 PM 0.00 8.55 13.24 35.35 

9/5/ 13 1:59PM 0.00 8.56 13.17 35.01 

9/5/13 2:00 PM 0.00 8.58 13.12 34.71 

9/5/13 2:01PM 0.00 8.67 13.22 34.43 

9/5/13 2:02 PM 0.00 8.64 13.17 34.39 

9/5/13 2:03 PM 0.00 8.47 13.00 34.88 

9/5/13 2:04 PM 0.00 8.87 13.70 35.31 

9/5/13 2:05 PM 0.00 8.06 12.29 34.43 

9/5/13 2:06 PM 0.00 8.50 13.29 35.91 

Average 0.00 8.66 13.25 34.65 

Unit 3 Run S 09/05/13 

... 157 

VES012611 
nme.stamp COOryCorr OlWet 020ry H20 

9/5/13 2:25 PM 0.00 8.47 12.90 34.47 

9/5/13 2:26 PM 0.00 8.64 13.16 34..35 

9/5/13 2:27 PM 0.00 8.85 13.46 34.29 

9/5/13 2:28 PM 0.00 8.61 13.05 34.06 

9/5/13 2:29PM 0.00 8.55 13.04 34.35 

9/5/13 2:30PM 0.00 8.54 13.09 34.74 

9/5/13 2:31 PM 0.00 8.81 13.57 35.11 

9/5/13 2:32 PM 0.00 8.98 13.70 34.52 

9/5/13 2:33 PM 0.00 8.96 13.62 34.19 

9/5/13 2:34 PM 0.00 8.90 13.59 34.40 

9/5/13 2:35 PM 0.00 9.05 13.79 34.40 

9/5/13 2:36 PM 0.00 9.03 13.64 33.83 

9/5/13 2:37 PM 0.00 8.94 13.45 33.50 

9/5/13 2:38PM 0.00 8.93 13.49 33.85 

9/5/13 2:39 PM 0.00 9.04 13.78 34.23 

9/5/13 2:40 PM 0.00 9.03 13.66 34.00 

9/5/13 2:41PM 0.00 8.68 13.11 33.84 

9/S/13 2:42PM 0.00 8.60 13.12 34.42 

9/5/13 2:43 PM 0.00 8.76 13.43 34.73 

9/5/13 2:44 PM 0.00 8.79 13.38 34.30 

9/5/13 2:45 PM 0.00 8.70 13.15 33.92 

Average 0.00 8.80 13.39 34.26 

Unit 3 Run9 09/05/13 

C-9 A-158 

VES012612 
T1me Stamp I COO!:)!Corr 02Wet 0201)' H20 

9/ 5/ 13 3:21PM 0.00 8.96 13.65 34.30 

9/5/13 3:22 PM 0.00 8.45 12.73 33.57 

9/5/13 3:23PM 0 .00 8.30 12.58 33.98 

9/5/13 3:24 PM 0.00 8.50 12.97 34.47 

9/5/13 3:25 PM 0.00 8.59 13.08 34.37 

9/5/13 3:26 PM 0.00 8.33 12.69 3UO 

9/5/13 3:27PM 0.00 8.46 13.10 35.48 

9/5/13 3:28PM 0.00 8.58 13.23 35.19 

9/5/ 13 3:29 PM 0.00 8.52 13.00 34.50 

9/5/13 3:30 PM 0.00 8.74 13.35 34.58 

9/5/13 3:31 PM 0.00 8.44 12.79 33.91 

9/5/13 3:32 PM 0.00 8.55 13.02 34.33 

9/ 5/13 3:33 PM 0.00 8.52 12.98 34.35 

9/ 5/13 3:34 PM 0.00 8.37 12.76 34.42 

9/5/13 3:35 PM 0.00 8.57 13.19 35.07 

9/5/ 13 3:36PM 0.00 8.40 12.84 34.60 

9/5/13 3:37 PM 0.00 8.55 13.10 34.82 

9/5/13 3:38 PM 0.00 8.55 13.12 34.76 

9/5/13 3:39PM 0.00 8.44 12.90 34.49 

9/5/13 3:40PM 0.00 8.73 13.45 35.09 

9/5/ 13 3:41PM 0.00 8.59 13.16 34.73 

Average 0.00 8.53 13.03 34.54 

Unit3 Run 10 09/05/13 

0.10 A-159 

VESOJ2613 
APPENDIXD 

Unit 3 Waste Feed Characterization Data 

A-160 

VESOl2614 
Hourly Report ln<:,ioerator 3 

~ONYX Veolia Created 9/S/201310:00 AM 

Env®nmental Serviees Period Swt 9/S/20 13 9:00 AM 

Sauget tttinois Period End 9/S/2013 10:00 A.'lol 

Page I of I 

CALCULATIONS 

Thermodynamic BTU 12.8 mblu 

Chlorine 35.2 lbs 

LowVolalile 0.013 lbs Mercury 0.0001 lbs 

Semi Volatile 0.007 lbs Ash 145.5 lbs 

WEIGHTS 

Weight 1264 lbs 

Solids Weight 202 lbs Liquid Weight 1062 lbs 

Low BTU Weight 495 lbs Special Feed Weight 167 lbs 

High BTU Weight 399 lbs 

Tank 2 Weight 0 lbs Tank 6 Weight 495 ibs 

Tank 4 Weight o lbs Tank 8 Weight 0 ibs 

Direct Inject Weight 399 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 8084 cf 

0·1 A-161 

VES0126LS 
Hourly Report lo~ncrator 3 

ONYX Veolia Cle•l<d 9iSI20 1311 :00 AM 

Environmental Servioes Period Start 9/S12Dill0:00 AM 

Sau&et lllinoi.s Period End 9/S/2013 II :00 AM 

P&&e lofl 

CALCULATIONS 

Thennodynamic BTU 12.9 mbtu 

Chlorine 39.2 lbs 

Low Volatile 0.013 lbs Mercury 0.0000 lbs 

Semi Volatile 0.009 lbs Ash 144.8 lbs 

WEIGHTS 

Weight 1237 lbs 

Solids Weight 202 lbs Liquid Weight 1035 lbs 

Low BTU Weight 499 lbs Special Feed Weight 183 lbs 

High BTU Weight 352 lbs 

Tank 2 Weight 0 lbs Tank 6 Weight 499ibs 

Tank 4 Weight 0 lbs Tank 8 Weight 0 lbs 

Direct Inject Weight 352 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 9155 cf 

1\·162 

VES012616 
Hourly Report Incinerator 3 

~ONYX Voolia <:=ted 915/2013 12:00 PM 

Environmenw Services Period Sta11 9/51201311:00 AM 

Sau'et Illinois Period End 9/512013 12:00 PM 

Page I of I 

CALCULATIONS 

Thermodynamic BTU 13.0 mbtu 

Chlorine 33.7 lbs 

Low Volatile 0.264 lbs Mercury 0.0001 lbs 

Semi Volatile 0.013 lbs Ash 126.1 lbs 

WEIGHTS 

Weight 1280 lbs 

Solids Weight 209 lbs Liquid Weight 1071 lbs 

Low BTU Weight 483 lbs Special Feed Weight 171 lbs 

High BTU Welghl 415 lbs 

Tank 2 Weight 0 lbs Tank 6 Weight 188 lbs 

Tank 4 Weight 0 lbs Tank 8 Weight 295 lbs 

Direct Inject Weight 415 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 8566 cf 

A-163 

VES012617 
Hourly Report lneinerator 3 

4'0NYX Vc:olia Created 915/2013 I :00 PM 

Environmental Service5 Period Sl3rt 9/5/2013 12:00 PM 

Sauaet Illinois Period End 915/2013 1:00 PM 

Page I of I 

CALCULATIONS 

Thermodynamic BTU 12.8 mbtu 

Chlorine 35.6 lbs 

Low Volatile 0.013 lbs Mercury 0.0001 lbs 

Semi Volatile 0.009 lbs Ash 124.9 lbs 

WEIGHTS 

Weight 1240 lbs 

Solids Weight 213 lbs Liquid Weight 1027 lbs 

Low BTU Weight 250 lbs Special Feed Weight 199 lbs 

High BTU Weight 577 lbs 

Tank 2 Weight 0 lbs Tank 6 Weight 0 lbs 

Tank 4 Weight 0 lbs Tank 8 Weight 250 lbs 

Direct Inject Weight 577 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 7501 cf 

VESOJ2618 
Hourly Report Incinerator 3 

40NYX Vcolla Cr<:ated 9/S/2013 2:00PM 

En._ironmtntal Services Period S141t 9/S/2013 1:00PM 

Saut~tliHnois Period Eod 9/S/2013 2:00PM 

Page I of I 

CALCULATIONS 

Thermodynamic BTU 13.0 mbtu 

Chlorine 30.3 lbs 

Low Volatile 0.695 lbs Mercury 0.0001 lbs 

Semi Volatile O.D18 lbs Ash 113.6 lbs 

WEIGHTS 

Weight 1264 lbs 

Solids Weight 213 lbs Liquid Weight 1051 lbs 

Low BTU Weight 501 lbs Special Feed Weight 178 lbs 

High BTU Weight 370 lbs 

Tank 2 Weight 0 lbs Tank 6 Weight 0 lbs 

Tank 4 Weight 0 lbs Tank 8 Weight 501 lbs 

Direct Inject Weight 370 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 7800 cf 

0 ·6 A-165 

VES012619 
Hourly Report 1ttcinera1or 3 

4 0NYX Veolia Cr<>led 91512013 3:00 PM 

En\l'ironmcntal Sen-ices Period Statt 9/S/2013 2:00PM 

Sauget Illinois Period End 9/SI2013 3:00PM 

1'3ge I of I 

CALCULATIONS 

Thermodynamic BTU 12.9 mbtu 

Chlorine 29.5 lbs 

Low Volatile 1.403 lbs Mercury 0.0001 lbs 

Semi Volatile 0.017 lbs Ash 112.0 lbs 

WEIGHTS 

Weight 1226 lbs 

Solids Weight 207 lbs Liquid Weight 1018 lbs 

Low BTU Weight 499 lbs Special Feed Weight 177 lbs 

High BTU Weight 342 lbs 

Tank 2 Weight o lbs Tank 6 Weight o lbs 

Tank 4 Weight 0 lbs Tank 8 Weight 499 lbs 

Direct Inject Weight 342 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 7997 cf 

0-6 A-166 

VES012620 
Hourly Report Incinerator 3 

~ONYX Vcolia Qeau:d 915n0 13 4:00PM 

l!nvironmema! Scovices Period Start 9/S/20 13 3:00PM 

Sau:etlllinois Period End 915n0 13 4:00 PM 

Page I ort 

CALCULATIONS 

Thermodynamic BTU 12.9 mbtu 

Chlorine 31 .6 lbs 

Low Volatile 1.165 lbs Mercury 0.0001 lbs 

Semi Volatile 0.020 lbs Ash 109.4 lbs 

WEIGHTS 

Weight 1225 lbs 

Solids Weight 202 lbs Liquid Weight 1022 lbs 

Low BTU Weight 480 lbs Special Feed Weight 187 lbs 

High BTU Weight 353 lbs 

Tank 2 Weight 0 lbs Tank 6 Weight 0 lbs 

Tank 4 Weight 0 lbs Tank 8 Weight 480 lbs 

Direct Inject Weight 353 lbs 

MISCELLANEOUS 

Waste Permit Time 0.99 hrs Natural Gas Flow 7990 cf 

0·7 A·167 

VES012621 
APPENDIXE 

Reference Method EPA Protocol Gas Certifications 

A-168 

VES012622 
Air Liquide America Specialty Gases LLC Page I of I 

g AIR LIOUIDE ,.S_ Scott 

r. 

tu:tr"ltMONTrt<WY lAP'OA.T!,TX775ill'h:n: 1100·2 .. ·lc<l1Fio. 2et"'n 041t 

RATA CLASS 

CERTIFICATE OF ACCURACY: Interference FreeTM Multi-Component EPA Protocol 

Gas 

MNy Ubcntoty - PGVPVendot n A320 11 

A,_LIQUG AIII(IIICAf!IPECio\LT'I'GA.SESUC 

IIC.rAINII)HT Pti\WV 

LAfiOitlf, TXTml 

C.tomet 

~ (;(lff'OMT'CN 

~,.VtQ.f.NaVO 

:ANALYTICAL INFORMATION Gas Typ;:coz,oz.aALN,._ _ _____ __ _ 

CyliiiMtr Number: CC119665 

Cyflndtt' Pm•urr·•: 1t.ro PSI~ 

COWOHENT 

CAA80t1 L\1 roc !DE: 

CERTIFIED COHCeNTRA110N (Mollt) 

1~.;! • 

OlNOtll tfi1~CIW 

a .s t. 

O~l.Atr-t 

, .. CO Mh.ll• wi'-!H,-,fncl• jlnK1111of11 8 tldltM 150 04ig 

•• ~cM•CIIIIt'ecl#" IN$1d an IN R:QIJ.._.,) «EPA PfiiiiiO:II ~ ,~lltf IH'l 

INSTRUMENTATION 

OAT! 

_,.,. L.AIT CAUMATED 

010ic2t11 

ACCURACY ... 1- lit 

H- l\ 

Ellp. OM! U l,.c:CI)1t 

Batch No: I.APOQS.OI 

TRACl!MtlfTY 

l>it&et 1118'1' and \1.!11. 

Oitect illST and V5L 

COMPONENT 

.,__,. 

-

(Z•Zeta Cot R•RofOtonot' Gat ,._Teet Go& r-Corrollr!lon Coelfdont) Se~ond fl'ltd Antlvt lt Calibrtllon Cwve 

QUALITY ASSURANCE 

APPROVED BY: SARAH HERBERT 

•M;ni1J.n on file) 

E-1 

CllfiC*'I' Cd.•O.o:.t•C,;-1 

~~7&1 

on~:A=O.COOIIot•O a:s.a!i981E-.1 Oo1.t13eQE-2: o-o..ooo;a£ o<~ t..o..ooooot .o 

C<irui'IWI;cn...IWI .. o(!d •Oil)• r,.. ...... ,_ c~~.,.., 

8~ a5715VH c= o- ~ 

hnp:/fl72.24. 128. 11falasglrxc.arp 17?0oC"''40 1904&Cyi=CCI &9665 &Usr=SHOP 

A-169 

1/1612013 

VES012623 
Air Liquide America Specialty Gases LLC Page I of 1 

AIR UQUIOE c S Scott 

,,_.~. FAA-.IONrPKW'f.lAPORJE. TX 71571 Pflcltle:!00-21!&-1421 I'M ftt.-4'1•· .. 10 

RATA CLASS 

Dunl mil)'i;ed Calibn~llnu StnndunJ 

CERTlFICATE OF ACCURACY: Interference FreeT"' Multi-Component E PA Protocol 

Gas 

A.IMy Labcw-'OfY · PGVP Vendor 10: AnGff 

AlltUOUCII"\E:AtCA Sl"lCW.1YGUUU.C ttQSf'AafltNOHT JII¥:Nf 

LA ~1'1. tx ln.l t 

Custold...lro.cYWII..I!SliK-"-"'WOA fi,.OC ... 11tl 

tVQ:J&aTEXDR ..........,."""""' 

~TX18el 

us 

~AL YnCAliNFORMATION Gas Ty~ : C02,0 2,8AlN ----- --- -

CylndtrNumber: CC157679 

CylinderPttUiit.......-: !&eOPSIG 

COMPONENT 

C'AA&Ot! OLOXlOE 

oxvca:tf 

Ml'!I'II.OCitN 

CERnFteD CCIHUNTI';ATION (Molts) 

~. 4'J t 

u .o t 

CI'.LJ..t.Ct 

FERENCE STANDARD 

CYUNDER NUMBER 

-·· ......... 

ACCURACY"' 

•1- h 

f/- u 

&p. O.c.; 14l)edil)tt 

B•tc:hH o:~ 

TRACEA8U.I'TY 

0Lrflr.L Nl$1 llAd VI I, 

Oiree l »IS1 ~~d VCL 

COMPOH911 

--

0.....,. 

~STRUMENTATION __ _.:::1 

HAL YZER READINGS 

QUALrrY ASSURANCE 

APPRO~O BY; SARAH HeRBERT 

('1"1111\'W"t on ~le) 

(,Z.Zero OAt R•Roforonot GM T•T•t Gas r=Corr$500 Coetfident) 

Second Trf.od Antlyslt C•libtation Cul'\'e 

E-2 

hup:ffl72.24.128.1 1/alasglrxcarpi7?D0¢'<040 1905&Cyi=CC 157679 &Usr=SHOJ> 

,A,170 

1/16/2013 

VES012624 
RATA CLASS 

Dual-Analyzed CalibraJion Sta11dard 

1290 CO RE STREET. TROY, MI4S083 Phone: 248-589·29150 FliX: 248·589·2134 

CERTIFICATE OF ACCURACY: EPA Protocol Gas 

Auay Laboretoa • PGVP Vendof 10: A22012 

AIR UOUIDE AMERICA SPECIALTY GASES UC 

1 290 COMB~MER-~ STREET 

TROV, Ml 4$083 

h!J cen atlon was per otmi eccor ing \0 

Proe-.clure G#l; September, UlD7. 

Cylinder Number: CC121944 

Cylinder Pressure•••: 2000 PSIG 

P.O. No.: 59933-71•615000 

~ntl 4753436~003 

Certiiicatlon Date: 

Cus1omer 

ClEAN AJR ENGINEEAJHG 

DON ALLEN 

500 wtST WOOD STREET 

PALATINE IL 60067 

us 

tandards; 

11Sep2012 Exp. Oato: 12Sep2020 

Botch No: TR00065750 

COMPONENT 

OxvGEk 

CARBON DIOXIDE 

NITROGEN 

CERTlFED CONCENTRATION !Moles) 

2.07 "' 

ACCURACY " 

+I· 1 '% 

TRACEABIUTY 

D•rect N1ST and VSL 

2.09 ,. +1- ,. Ditect NIST and VSL 

BALANCE 

• ' • Do 1'10'1 use when ey{Wttr Pfuat.~•• II Mlow t 50 psig.. 

•' Analytical o:~cc:uracv Is bn:ttd on d'l• ,..Mtf'.U ot EPA ProtccOI ProcaCIUnl 01. S.~tt.mber \$1$7. 

CYLINDER NUMSER 

1(024582 

J:.02S987 

CONCENTRATION 

23.20 " 

5.006 % 

OAU LAST CAUBRA TED 

Z8Aug2012 

1$e~20U 

CARlON DIOXIDE 

HDIA 

ANAL VZER READINGS 

CZ•ZeroGas. R• Riferenc:eGas l•lestGas r•COrrel8nonCOifliC:~enU 

OXYGEN 

O.tet 1151!$)20\2 A••p!)!\1• Unil: ,. 

Zl •0.00000 1\1•23.20000 T1•2.08000 

l\2oo2),'20CQ0 Z2•0.00000 T2•2.080QO 

u •0.00000 T3 = 2.08000 R.3. 23.20000 

Ayg C9t!C!Qua00n: 2.068 M 

n·••-70000 

IU•IOO.OOOO z2 .. 0.00000 T2 ~tl 10000 

Z.3•0.00000 T3•46.7()C)OC) ft3•100.0000 

A!!• Conc•:n.r<1rion: 2.091 ! 

S10«1d l r'ad Anilllvs:is 

E-3 

Page I of 1 

Calibration Corve 

Concllfttt• tlon• A +Bx + Dl.2 + Dx3 • h4 

f•0.9999'99 

Con1tW\ls: A.•·0.0 \310834 

•· t.ooo1o5107 c.o 

0•0 E=O 

Conoentlatioa = A+ Bx<t Cx2 +01C3+fl(<l 

r•O.HOSU$ 

Co,.-.Jtl:LS! A = Q.COCSII ,J 1 03 

8•0.041•30365 C• S.Sll!..OS 

O•:Z.701tel.07 E •O 

A·111 

VES012625 
Airuas 

CERTIFICATE OF ANALYSIS Airgas Specialty Gases 

11111 S.OU.O.AI.,...,_&r-. 

Grade of Produ ct: EPA Protoc J;:O~"':'mC:.=-:23)..,. ,. .. 

Pan Number. 

Cylinder Number. 

Laboratory: 

PGVP Number. 

E02N199E15A0406 

CC14436 

ASG - Los Angeles - CA 

832011 

-.elcgaa.t.OM 

Reference Number: 48-124294203-8 

Cylinder Volume: 144 Cu. Fl. 

Cylinder Pressure: 2015 PSIG 

Valw 0\JIIet 350 

Analysis Date: Dec 16, 201 1 

Expiration Date: Dec 16, 2014 

CtrtfiQIIIbn PMO~mt>d In aooordanc& wtl\ •EPA rac;aa~ry P'rrAOOOI ($4ol. 19'37}' uti!'!) lie MMY pooeo.."e$1$ted, Anll'j\lcal ~ dG$1 not rtq.Jife con9CC!on fOI 

~ietl . This cylnder Nt ••*~ 8IW)1ieal tn::ectmcJ ae 5tattd below wr" a~ lt'f'OI ~ 95%. Thole ••• no $igt'lieant _..... -.'h!c:t\ atlect NUN 

"'.,._ <*118Skn modln. AI OOIICOJ6alio!iS ate on a~ bniS ""*" CllhtrMM ..,..,_ Do Not U..l .. ~billow 150 pete le. 1 Woog:a P** 

ANALYTICAL RESULTS 

Component Requ .. ted Actual Protocol Toll I Rol t!IVI 

Conconlrollon ConCM"ttration .Method Uncortalnty 

CAR80H MOHOXIOE 90.00Pft,l 89.80Pft,l Gt +J-1% NlSTT-o 

NllRO<lEN Balanc.e . CAIJBRATJON STANDARDS 

Type kot ID Cy11ncler No Concentration Expiration Date 

NlRM 090605 CC2Wa9 9U11PPM CARBON MOHOXIOE/NITROClEN Fo~OI,20 3 

ANALYTICAL EQUIPMENT 

lnslwmenUMakellllodel Anolytlcal Principle kosi Multipoint Colillralion 

Nieoi<M 0700 AHR08015S1 CO FTIR . 0EtC08, 201, 

Triad Dolo AY1111able Upon Roqu•sl 

Notes: 

r.~' 1/ 

Approved for Release 

E-4 

A-172 

VES012626 
Air Liquide America Specialty Gases LLC 

{S'' Scott ~~·· 

11oU6fAIR:fltOHT f'KWY,LA P~TE. TX77$11 f'h:ln9 800o248-14~7 e:oc: Ult-41<!-$419 

RATA CLASS 

Dunt.Amtly.,ed C.alibnulon Sumd«l'd 

CERTIFICATE OF ACCURACY: EPA Protocol Gas 

Assay t..a.boratory • PGVP Vendor ID; A32011 

AIRLIQUfPE N.U:!IU:';A SP£CII\1.TYGASES UC 11426fA!RtiONT A<.VN LAPORTE, TX77571 

P.o. No.: sr<X:K Ooc~fM!'it~ 4375 001 

Fdioii:IJRS012 

!ANALYTICAL INFORMATION Gas Type : NONE 

Cylilnder Number. CC215149 

Cylinder PtHture_.: 20XIPSIG 

C.-rtifl~tion Date: 18tfuV2.011 

CUstomer 

URS CORPORA.llQK 

9400 "*''BtRGlEN Bl VO 

A.V$Titf l X 7Bf29 

us 

Exp, D•·: 16N1!'1201!f 

Batch No: l.APOQ$2I.Sl 

TRACEASJUTY 

Page I of I 

COIIPON£NT 

CJ\1\l!ON muox"! of: 

CEfUI:f'IED CONCENTRAnoN (Mole&) 

3 1'ffi 

ACCt.mACY•• +1 - i\: Direct. JltS1' .:~ nd VSL 

N't1li.OGtW a.Jt...LA!4::r. 

\REFERENCE STANDARD 

TYPEISRM NO. NTRU 1678 EXPIRATION DATE 150ec®11 

CVUNOER NUMBER 

I<NJ.M).$11{1 

CONCEHTRATION 4MOPPIA 

COMPONENT CARSON. MONOXIO£ 

NSTRUMENTATlON 

INSTRUMENTIMODEUSEfUAU f:'tfRIXI()I)929(16() 

@.:!AL VZER READINGS 

DATE LAST CAUBAATEO 200U201l 

(Z.•ZeroGas R=Rererence Gas T=Test Gas r=CCttetalloo Coefficient) 

Second Triad An:~ly$1 $ Calibration Cu:rve Fint Triod Analy,1s 

CARBON MONOXJDE O&flel ~l1 R:eapt~~~'Cie 1Mt: PPI<1 

:1 ~~ 011763 Rl "' \24~719 11=4&.14483: 

RZ=-1Zoi6.806Z2• 0.06757 67'21 

t~M 46.MI08 IU'-124Ug2 

Avg, C0flQerollliiM: 4fi.25 PPM 

Ollie: 9~W2011 Rl::lflOI"I$1:1kiil:ffM Z1 :.0.01497 R 1-..:6,5e4$4 H=46. 16tll e R;2>r4f~S7 %2:0.()1493 T?-o4U846e 

Z3•0,11036 1l""'.33MrA 8.6S616 

AYQ. Cone~ltafg~: 4ij,;(!>PPIA 

Special Notn: l ll$ 61lpil'etklfl d~ # Ms. been ~~6 wli'IOIA 1'9-~)' p::r £PA OOOIR23-2'.Y5<12, 

o~r ... P<l)'tl40f OGA no 

(QUALITY ASSURAN= C,_,E:...._ __ _ 

APPROVED BY: SARAH HERBERT 

(~ al ro ¢I\ fie) 

E-5 

~~e;..~QI(l<64 

,::U9S96£•1 

Con A=\l l!llOXI£<0(1 

8-8.39797£ ·1 C=!o.tlll00£.4-

D=1.0COO!lE·6 E-<l.OOOOOEtO 

hup://172.24. 128.11/alasglrxcarp 17?Doc=040 1179&Cyi=CC215749 &Usr=SHOP 

A-173 

1/28/2013 

VES012627 
Performance Specification Test Results 

for the CO and Wet 0 2 CEMS 

for Rotary Kiln Incinerator Unit 4 

Prepared for: 

Veolla ES Technical Solutions, L.LC. 

7 Mobile Avenue 

Sauget, IL 62201 

Prepared by: 

URS Corporation 

9400 Amberglen Boulevard (78729) 

P. 0. Box 201088 

Austin, Texas 78720-1088 

September 2013 

J\.174 

VES012628 
Table of Contents 

Page 

1.0 lntroduction ...............................................•.......... -.. -.................................................... 1-1 

2.0 Summary ofResult$ ................................................... - .................................................. 2-1 

2.1 Relative Accuracy ................................................................................................ 2-2 

3.0 Test Protocol ................................................................................................................... J-1 

3.1 RelativeAccuracy ................................................................................................ 3-l 

4.0 Q uality Assurance ............................... -·····················-··-······-······-······························ 4-1 

APPENDIX A - Relative Accuracy Spreadsheet and Reference Method Dalll 

APPENDIX B - Reference Method Calibration ResultS 

APPENDIX C - Unit 4 CEMS Relative Accuracy Data 

APPENDIX D - Unit 4 Waste Feed Characterization Data 

APPENDIX E - Reference Method EPA Protocol Gas Certifications 

Unit 4CEMSRATA iii Veolio Sougcl 40942525 

A·175 

VES012629 
list of Tables 

Pa!Je 

1-1 General Facility and Testing lofonnation ........................................................................ 1-2 

1-2 CEMS Identification ........................................................................................................ 1-2 

2-1 PST Requirements and Acceptance Criteria .................................................................... 2-1 

2-2 CO CEMS Relative Accuracy Test Results ..................................................................... 2-3 

2-3 Wet 0 2 CEMS Relative Accuracy Test Results .............................................................. 2-4 

3-1 Oxygen Correction of Reference Method CO Concentration Results ............................. 3-4 

Unil4 CEMS RATA iv Veolio Sauget 40942525 

A-176 

VES012630 
1.0 Introduction 

Veolia ES Technical Solutions, L.L.C. (Veolia) operates three incinerators at its Sauget, 

Illinois facility. Two of the incinerators are fixed hearth units (Units 2 and 3), and the third 

incinerator is a rotary kiln unit (Unit 4). All of the incinerators treat certain wastes that nre 

c lassified as hazardous under staLe and/or federal regulations, and are subject to the National 

Emission Standards for Hazardous Air Pollutants (NESHAPs) for Hazardous Waste 

Combustors (Title 40 of the Code of Federal Regulations, Part 63 [40 CFR Part 63), Subpart 

EEE), (i.e., the HWC MACT). Unit 4 is equipped with a continuous emission monitoring 

syS1em (CEMS) that consists of an oxygen (02) monitor and a crubon monoxide (CO) monitor 

whicb are used to monitor tbe emissions from the stack. The CEMS underwent Relative 

Accuracy (RA) Testing. This report presents the RA test results for the Unit 4 CO and wet 02 

CEMS. The general information regarding the testing at this faciliry is summarized in Table 

1-1. The RA acceptance criteria are shown in Table 2-I. 

TheRA test of the Unit4 CEMS was completed in September of2013, as the initial step 

in the 2013 Comprehensive Perfonmmce Test of Unit 4. The CEMS were audited according to 

the RA procedures detailed in 40 CFR 60, Appendix B, Performance Specification 4B, 

"Specifications and Test Procedures for Carbon Monoxide and Oxygen Continuous Monitoring 

Systems in Stationa•y Sources" and 40 CFR 63 Subpart EEE, "National Emission Standards for 

Hazu•·dous Air Pollutants from Hazardous Waste Combustors." The CEMS met all the RA 

criteria outlined in the abov~ited references. Section 2.0 presents a detailed summary of these 

test results. Supporting documentation is located in the appendices. 

The analyzer identification numbers and serial numbers for the monitors are presented 

below in Table 1-2. Veolia opernrcs a CO analyzer, an 0 2 analyzer, and a moisture analyzer. 

The oxygen correction of the plant CO concentrations is performed using a dry basis oxygen, 

derived from the measured wet basis oxygen concentration and the measured percent moisture. 

The E''Ochem MC3 infrared CO analyzer is designed using a single sample cell equipped with an 

individual detector system for each o r two measurement ranges (0-200 ppmv and 0-3,000 ppmv). 

The 0 2 analyzer is a COSA electrochemical analyzer. Responses rrom each CEMS are recorded 

by the Control System (CS). Data printouts from these monitors documenting the CEMS 

performance are presented in Appendix C of this report. Characterization of waste fed during the 

RATA testing is included in Appendix D. 

Unit 4 CEMS RATA 1-1 Veolio Sou get 40942525 

A·177 

VESOl2631 
Table 1-1 . General Facility and Testing Information 

Unit 4 CEMS Performance Specification Testing 

facility Name Ve<>lia ES Te<:hnical Solutions, L.L.C. 

Contact Person David Klarich 

Telephone Number 61R-271 -2804, xl20 

Facility Address #7 Mobile Avenue 

Sauget, IL 62201 

Types of Process Sampled Rotary Kiln Incinerator Exhaust Gas 

Person Responsible for Conducting TeSI M iclmel Fuchs 

Telephone Number s 12-454-4797 

Company Name URS Corporation 

Addr<ss 9400 Ambctglen Boulevard 

Awtin. Texas 78729 

~n(s) Conducting Tests Jesse Rocha 

Mcggcn Delollis 

Megan Bowien 

Noah Prescott 

Test Methods Performed EPA Method3A aod EPA Method 10 

Date ofTe<ting September 4, 2013 

Table 1-2. CEMS Identification 

Unit 4 CEMS Performance Specification Testing 

Paramt:t.e.r J\la•uf1.eturer Range AnalyurTa; 

Carbon Monoxide EA:ochem MC3 0-200ppmv AT-556£ 

0-J.OOO ppm•• 

Oxygen (Wet) COSA Q-25% AT-560B 

Unit4 CEMS RATA l-2 

ADal)'t<r Sulal 

Number 

107 

A2H6S94T 

Vcolia Sou get 40942525 

A·118 

VES012632 
2.0 Summary of Results 

Detailed results are presented in this section. Section 2.1 details the results (rom the 

relative accuracy (RA) tests. 

AU test results were within the acceptance criteria as stated in the RA portion of 40 CFR 

60, Appendix B, Perfonnance Specification 48, "SpecijiCIJtions and Test Procedrll'esfor Carbon 

Monoxide and Oxygen Cominuous Monitoring Systems in Stationary Sources." These criteria 

are shown below in Table 2-1. 

AU calculations are done with unrounded values, and therefore, it may not be possible to 

reproduce a calculated value exactly from the data shown in a table. 

Table 2·1. PST Requirements and Acceptance Criteria 

Unit 4 CEMS Performance Specification Testing 

CO Monitor 

Parameters Low Ronee I Hie)J R•nge 

(~·200 p pm•·) (0-3,000 ppmv) 

10% ofrbe overage Reference Method (RM) value 

Relative Accuracy (RA) · orS% of the applicable standard 

(S ppmv CO correeled to 7% 0 2> 

o, Monitor 

Ronge (0-25%) 

1.0"/. o, 

Unit 4 CEMS RAT A 2-1 Veolia Sauget 40942525 

Ar179 

VES012633 
2.1 Relative Accuracy 

Relative accuracy (RA) testing was performed by URS pcrsotmel on September 4. 2013. 

The relative accuracy test results are presented in Tables 2-2 and 2-3. RA testing compares the 

plant CEMS measurement of CO (corrected to 7% oxygen) and Oz (on a wet basis) to the 

Reference Method (RM) measured using EPA Method 10 for CO and EPA Method 3A for 0 2. 

Relative accuracy for the CO CEMS is calculated by adding the confidence coelllcient to the 

absolute average difference between plant averages and the RM averages. Relative accuracy for 

the 02 CEMS is equivaleot to the absolute average difference between plant averages and the 

RM averages. The acceptance criterion is the greater of either I 0% of the average RM or 5% of 

the applicable standard (5 ppmv CO corrected to 7% oxygen for the CO CEMS and 1.0"/o 02 for 

the wet 02 CEMS). All CEMS met the prescribed performance criteria. 

Hard copies !Tom the RM monitoring sySTem along with hard copies of the relative 

accuracy calculation spreadsheet can be found in Appendix A. Hard copies oftbe Veolia Unit 4 

CEMS data are presented in Appendix C. 

Unit 4 CEMS RATA 2-2 Veotin Sauget 40942525 

A-180 

VES012634 
R•n 

Number 

I 

2 

3 

4 

5 

6 

7 

8 

9 

10 

Unit4 GEMS RATA 

Table 2-2. CO CEMS Relative Accuracy Test Results 

Unit 4 CEMS Performance Specification Testing 

Reference 

Motbo<I(RM) Unit 4 CEMS 

D•te RunThm! CEMS (ppmv CO, 

(PPnt'' CO, corretted tn 

corrccttd to 7% 0,) 

7% 0,) 

9/412013 09:05.()9:26 0.95 0,07 

9/412013 09:54-10: IS 1.1 4 0.10 

9/41201 3 10:29-10:50 0.75 0.08 

914/2013 11:00-11:21 0.30 0.11 

9/4!2013 11:31-11:52 0.60 0.13 

9/4!2013 12:03-12:24 1.02 0,10 

9/412013 12:36-12:57 0.67 0.09 

9/412013 13:1>9-13:30 0.30 0.23 

91412013 13:43-14:04 0.3 1 0.07 

9/4/2013 14:17-14:38 0.60 0.34 

Absolute Avera&t Dll'fcreoce 

Stand>rd De•1ntlon 

Conficlence Coofficlcnl (CC) 

Relative Accuracy (ppm•• CO) 

Arlthonetlc 

Dlfforon« 

(IIIIIDV CO) 

.(),88 

-1.04 

-0.67 

419 

-0.47 

-0.92 

-0.58 

-0,07 

-0.24 

·0.26 

0.47 

0.31 

0.24 

0.7 

2-3 Veolin Sougcl 40942525 

A-181 

VES012635 
Run 

Number 

I 

2 

3 

4 

5 

6 

7 

8 

9 

10 

Table 2·3. Wet 0 2 CEMS Relative Accuracy Test Results 

Unit 4 CEMS Performance Specification Testing 

Referen<e 

Dote Run nme 

M<thod (RM) Unlt4 CEMS 

CEMS (•fo Q,, Wtl) 

(% 0 1, wet) 

9/4/2013 09:05..()9:26 8.88 8.58 

9/412013 09:54· 1 0: I 5 9.16 8.94 

914120ll 10:29-10:50 8.84 8.70 

9/412013 11:00·11:21 9.44 9.15 

91412013 11:31-11:52 927 9.03 

9/4f2013 12:03-12:24 929 9.04 

91412013 12:36-12:57 9.43 8.89 

9/412013 13:09-13:30 9.02 8.70 

9/412013 13:43-1 4:04 9.15 8.96 

9/412013 14:17-14:38 8.97 8.75 

Absolute Average Dlfferente 

Standard Deviation 

Ftehlfll'eAccuracy (0

/• 0:, Wft a~l,.) 

Arit.hmdit 

Dlrfeneace 

('lo 0 1, wet) 

·0.30 

.0.22 

-0. 14 

-0.29 

.().24 

.{1,25 

-0.54 

-0.32 

.0.19 

-0.22 

0.24 

0.06 

0.24 

Unil4 CEMS RAT A 2-4 Veolio Sougcr 40942525 

A-182 

VES012636 
3.0 Test Protocol 

The carbon monoxide and oxygen monitors located at the Veolia Unit 4 location were 

audited according to the Relative Accuracy procedures outlined in 40 CFR 60, Appendix B, 

Performance Specification 4B, "Specij)carlons and Test Procedures for Carbon Monoxide and 

Oxygen Continuous MoniWTing Systems in Stationary Sources" and 40 CPR 6.1 Subpart BEE, 

"National Emission Standards j'01· Hazardous Air Pollutants ji-om Hazard<Jus Waste 

Combustors. ·• 

3.1 Relative Accuracy 

URS monitored the emission gas CO and 0 2 concentrations from the Unit 4 E.'t.haust 

Stack location using mobile continuous emission monitors. A stainless-steel probe was inserted 

into the stack and used to collect sample gas. A heated TeOon sample line transported sample 

gas from the probe to the URS monitors located at ground level. The analyzers were kept at a 

constant temperature inside the mobile lnbomtory. 

For eacb run, sample gas was collected over 21-minute test periods. Tiuee traverse 

points across the Unit4 Exhaust Stack interior diameter were selected according to tbe procedure 

outlined in 40 CFR 60, Appendix B, Performance Specification 2, Section 8.1 .3.2, and sample 

gas was extracted at each of three paints for seven minutes during the test period. The sampling 

location met PS 2 criteria by being greater than 2 stack interior diameters downstream from the 

nearest disturbance and greater than 0.5 stack interior diame-ters upstream of the stack exhaust 

orifice. At the mobile laboratory, the stack gas is split between the wet and dry analyzers. The 

portion of the sample gas that is not sent directly to the wet 0 2 analyzer is routed to a condenser 

and then transported to the dry 0 2 and dry CO analyzers for analysis. CO analyses were 

performed in accordance with EPA Method 10. 0 2 analyses were perfonned in accordance with 

EPA Method 3A. 

URS used a Thenno Modei48C CO analyzer to measure the CO concentration according 

to EPA Method 10. This analyzer is a gas lilter correlation (GFC) analyzer. The analyzer 

measures CO by comparing infrared ab.~orption of a reference concentration to the absorption of 

the sample. The Thermo Modei48C CO measurements are not affected by carbon dioxide. For 

this reason, the C02 interference trap was not incorporated into the extraction system. The 

exclusion of the C02 interference trap eliminates the need to correct sample concentrntion, 

improving the accuracy ofthe analyses. URS bas demonstrated through in-house testing that 

C02 is not an interferant at typical combustion C02 concentration levels by introducing 20% 

col calibration standards to a calibrated Tllenno 48. The instrument's response to this gas was 

less than 2 ppmv (I% of scale). 

Unit 4 CEMS RATA 3-1 Veolia Stmgct 40942525 

A-183 

VES012637 
URS measured both dry and wet oxygen concentrations for the duration of the Unit 4 RA 

test. From these rwo measurements, URS was able to calculare the moisture percentage and then 

use the percent moisture to convert the RM wet oxygen concentrations from each nm to dry 

bas~s. The oxygen corrections of RM CO concentrations were calculated using this dry basis 

oxygen. Table 3-1 presents the concentration data for the steps of this calculation for all runs. 

Dry oxygen was measured using a Servomex Series 1440 02 analyzer. This analyzer 

measures 0 2 on the basis of its paramagnetic properties. Wet oxygen was measured using an 

Amctek RM CEM 0 2/IQ analyzer. This analyzer measures 0 2 on a wet basis using a zirconium 

oxide sensor. 

The analyzers' e.Jectronic output signals were converted to a digital format and stored by 

a computerized data acquisition system. The system translated tlris digital signal into the proper 

units of measurement (ppmv CO,% 0 2) and stored them on a bard disk. The system stored the 

data as ten-second averages. 

The analyzers were calibrated prior to initiating testing using appmpriatcly certified 

standards as specified by EPA Methods 10 and 3A. Both of these methods reference procedures 

specified in EPA Method 7E for calibration, standardization, calculation, and data m1aJysis. The 

UR.S system response was then checked. The total system, which included the probe, sample 

line, sample pump, and water trap, was incorporated into the system response. A system 

response time test was performed and documented for each instrument. The system drill was 

calculated using the pre- and post-test System responses. These checks ensured that the system 

remained within the tolerance level defined by the above EPA methods. A sampling system 

calibration bias correction was applied to all RM CO and 0 2 data measured during each test run 

by using equation EPA Method 7E-5: 

Wltere: 

Cg.., 

C,.-g 

c .. 

c_ 

c. 

= 

= 

= 

= 

= 

Effiueot gas concentration, dry basis, percent or ppmv; 

Average gas concentration indicated by analyzer, dry basis. percent or ppmv; 

Average of initial and final system calibration bias check responses for the 

upscale calibration gas, percent or ppmv; 

Actual concentration of the upscale calibration gas. percent orppmv: and 

Average of initial and final system calibration bias check responses for the zero 

calibration gas. percent or ppmv. 

Unil 4 CEMS RATA 3-2 Veolia Sauget 40942525 

A-184 

VES012638 
The data from each 21 -minute test period was averaged for each of the RA runs. This 

averaged data was tabulated as shown in Tables 2-2 and 2-3. The arithmetic differences between 

tbe URS reference method (RM) results for the analyte gas concentrations and the Unit 4 CEMS 

result' for the analyte gas concentratiOM are ulso tabulated there. Carbon monoxide results for 

both the RM and the Unit 4 CEMS were corrected to 7% oxygen before calculating arithmetic 

ditlerences. The absolute average difference. stw1dard de,~ation (Sd) and confidence coefficient 

(CC) of the arithmetic differences were calculated using the equations described in 40 CFR 60, 

Appendix B, PS 2, Section 12. At least nine runs must be used to detem1ioe relative accuracy. 

Ten runs were performed during the September 4, 2013 RA testing. TheRA procedures allow, 

at the tester's discretion, for up to three tests to be rejected from the calculations to determine 

average difference and standard deviation. After rejecting one unwanted run. the confidence 

coefficient (CC) was calculated according to the following equation: 

Where: 

cc . , •. ,,x s~ 

">/II 

tn.m = 97.5% Student- t variable (2.306 for nine runs); and 

11 = Number of tests used (must be<: 9). 

Relative accuracy for the Unit4 CO CEMS was calculated in ppmv CO according to 40 

CFR 60, Appendix B, PS 4A, Sec~ ion 13.2, by adding together the absolute value of the average 

difference between the RM and Unit 4 CEMS and the confidence coefficient applicable to nine 

te:,'l runs. Relative accuracy for the Unit 4 0 2 CEMS was calculated in% 02 according to 40 

CFR 60, Appendix B, PS 3, Section 12.0, and was equivalent to the absolute average difference 

between the RM and Unit4 CEMS for nine test runs. 

Unil4 CEMS RATA 3-3 Vcoliu Sauget 40942525 

A-185 

VES012639 
Table 3·1. Oxygen Correction of Reference Method CO Concentration Results 

Unit 4 CEMS Performance Specification Testing 

Run \\'rt: Ot Dry 0 1 

Numbe-r o ... Run Time (%, ·wei (%, d_ry 

basis) basb) 

I 9/412013 09:05.()9:26 8.88 13.21 

2 9/412013 09:54-10:15 9.16 13.70 

3 9/4/2013 10:29-10:50 8.84 13.33 

4 91412013 11 :00-11 :21 9.44 13.91 

5 91412013 11:31-11:52 9.27 13.S3 

6 9/412013 12:03-12:24 9.29 13.83 

7 9/412013 12:36-12:57 9.43 13.67 

8 91412013 13:09·13:30 9.02 13.4 I 

9 9/4/2013 13:43-14:04 9.15 13.74 

10 91412013 14:17-14:38 8.97 13.44 

Unit 4 CEMS RATA 3-4 

.1\toin:ure \VetO, 

(%) (%. dr)' 

basis) 

32.75 13.21 

33.15 13.70 

33.65 13.33 

32.12 13.91 

32.93 13,83 

32.83 13.83 

31.04 13.67 

32.73 13.41 

33.44 13.74 

33.30 13.44 

co co 

(ppm''• {ppmv, 

dry bosit) @7%0,) 

0.53 0.95 

0.59 1.14 

0.4 1 0.75 

0.15 0.30 

0.30 0.60 

0.52 1.02 

0.35 0.67 

0.16 OJO 

0.16 0.31 

0.32 0.60 

VcoUa Snuget40942525 

A-186 

VES012640 
4.0 Quality Assurance 

To ensure accurate and defensible results, strict quality assurance and control measures 

were followed. All testing was petformed following standard EPA protocol as outlined in 40 

CFR, Prut 60, Appendices A and B. All PST testing was perfonned while the plant was 

operating under oonnal conditions with at least 50% load from waste feeds and/or natural gas. 

Hard copies of incinerator waste feed rate datu are included in Appendix D. All test criteria were 

thoroughly documented and checked for completeness. EPA Protocol gas certification 

documentation for compressed gas cylinders used during the RA testing is included in Appendix 

E. 

The CO and 0 2 analyzers used by URS were operated and calibrated in accordance with 

the EPA Methods 10 and 3A except that the C02 interference trap was not used. The gas ftlter 

correlation analyzer nsed for CO measurement uses the characteristic absorption of infrared light 

by CO molecules to measure its relative concentration. This is a highly specific method for 

determining CO and is virtua lly free of interference from compounds such as wntcr or carbon 

dioxide. System bias checks were pcrfonned before and after each test run to ensure that the 

measutiug systems remained 'ViOlin their performance specifications. All method performance 

specifications were met. Calibration results are documented in Appendix B. 

Uoit4 CEMS RATA 4-1 Veoltn S•us•• 40942525 

A·l87 

VES012641 
APPENDIX A 

Relative Accuracy Spreadsheet 

and Reference Method Data 

1\-188 

VES012642 
Veola Saua:tt Unit 4 RATA 

RelotJve Acxurwt Resutu 

9(4(20U TIME 

Run 1 09:05-()9:26 

Run 2 09:54-10:15 

Run 3 10:2!HO:SO 

Run4 1.1 :00-11 :21 

RunS 11:31-1.1:52 

RunG U :03·12:24 

Run 7 12:36-12:57 

Run8 13:09-13:30 

Rvn9 13:43-14:04 

Run 10 14:17-14:'18 

Oz, Wet 

(%) 

8.88 

9.16 

8.84 

9.44 

9.27 

9.29 

9.43 

9.02 

9.15 

8.97 

REFERENCE METHOD 

O,Ory 

o,Oty Mob:ture '"· from 

('l6) (%) Wet) 

13.21 32.75 13.21 

13.70 33.15 13.70 

13.33 33.65 1333 

13.91 32.1l 13.91 

13.83 32.93 13.83 

13.83 32.83 13.83 

13.67 31.04 13.67 

l3.41 32.73 13.41 

13.74 33,44 13.74 

13.44 33.30 13.44 

STACK ANALYZERS ARITHMETIC DIFFERENCE 

co o, Use co Use 0,. Wet Use co u .. 

co (0, Corr) Wtt of (0, Con) ol ol (0, Con) "' (%) Aun1 Run' (ppm) (ppm) ('l6) Run1 (ppm) Run1 (ppm) 

0.53 0.95 8.58 0.o7 -0.30 -0.88 

0.59 1.14 8.94 0.10 X .0.22 -1.04 X 

0.41 0.75 8.70 0.08 .().14 .().67 

0 IS 030 9.15 0.11 .0.29 .0.19 

0.30 0.60 9.03 0.13 .0.24 -0.47 

0.52 1.02 9,04 0.10 -0.25 -0.92 

0.35 0.67 8.89 X 0.09 -0.54 ~ -0.58 

0.16 0.30 8.70 0.23 .0.32 .().Q7 

0.16 031 8.96 0.07 .0.19 .0.24 

0.32 0.60 8.75 034 .0.22 .0.26 

Number of Runs Used in CaJculatlon {rt 9 9 

Average Oiffetence Cd,.11G) ·0.24 .0.47 

Standard Deviation (S,) o.oo 0.31 

t-Valuo (lo.m) 2.306 2.306 

Confidena Coeff...,t (CC) 

- 0.04 

- 0.24 

Pern"Mt Um' - 100 

Average of Reft!rence Method tRM.\'6) 9.11 0.61 

Relotlvo Accura<Y (O, CO,) (ld,""l) 0.24 ~::-~:.:· Relotive Accuracy (CO, NO,. so,) Ud..voi• ICCI) ::::::~~=:;: 0.7 

ReJative Accuracy l" of Pe1mit Umit) (RA ....::::;'"-· ·-· 0.7 . An X in this column denotes a run which is not ust"d In c.akutation of fmttve i1CCUI'3Cy 

A-ltll 

.... 

VESOJ2643 
4-Sep-13 

R\ln l 

Run2 

Run 3 

Rurt4 

Run S 

Run 6 

Run7 

Run! 

Ruo9 

RmlO 

.. s.u 

""" 1 

Run 2 

Run 3 

Run • 

RunS 

Ftun 6 

Run 7 

RunS 

Run 9 

Run 10 

.. _13 

Runt 

""" 2 ..... Ron• 

...... Roo 6 

"""' R"" 8 

Run9 

Run 10 

4-Sep-13 

Run 1 

flun 2 

Run3 

Run4 

Run S 

Run G 

Run7 

Run S 

Ru\9 

Run l D 

2013 Unh 4 CEMS RATA 

Bl~u Correc'lld Concentrations 

0910412013 

Veolia Saucet Unit 4 RATA 

Uncorr.cted Conctntratiom 

Time o, Wt t a. Drt co 

(!I) (!I) (P9m) 

09:05•09:26 t.09 13:21 .0.2 

09:S4-10:1S 9 .. 17 13.69 0.0 

10;29-10 :50 9.01 13.32 .0.1 

11:00-11:2.1 t.s.o 1.1-90 ·0.:2 

11 31 11:S2 9~ L 0.0 

2,0).12 2.4 

~ lUO 0.0 

~3S:12 S7 !J,.44 U.6S .O.l B:09 1J )O 90fl IUO .0.1 

1~43 14.1»4 9.29 u.n '<>.3 

1.&:17-14:38 ..... UAl "<>.2 

Con-Ktcd Wet~ CCII<. 

"""' D,(!Q Co 

£4- 7£·5 Factors 

c..J(c..<ol 

09;05t-Q!kl6 909 138 1.2> 

09:-S4-10t15 9.17 1.92 1.26 

S.O:&l&.SO SI,Ol 1.94 1.25 

U ;D0-11;21 9S4 1.98 LIS 

Jl!3l·ll:S2 9.40 1.91 1.25 

12:03-12,24 9 42 1 .97 1.25 

12:.'36-12:57 9 • .1111 1.95 1.26 

U :e&.U:!O 9.08 J.96 1.27 

13;4)..14:04 29 2.00 1.26 

14:17·14:18 9.19 2 .0 1 L2S 

Corrected Drv 0t Cone. 

Tim• co, !!II Eq. 7f.S Factors 

c. C..J!c..<ol 

09:0>-09:26 U.ll o.os 1.00 

09;54-llklS UM 0 06 LOO 

10:.&-lO".SO 13.32 0,06 LOO 

U:B).lLll ll.tO OJ)7 L01 

tl;ll· U.:Sl 13 81 0.07 1.01 

12:01-12:24 IJ.BO 0.06 LOI 

11:35-11:57 U.65 0.00 LOl 

~ll:.lO 13.40 0.06 LOl 

U;4)-l<l.04 1).12 0.06 1.0·1 

l4:17·14.l8 n.u 0.06 1.01 

CorrHtecJ CO COnt. 

Tlme CO (ppm( Co 

EQ, 7£•' F1ClOtS 

c..Jcc •. c.t 

09:05·09:] 6 ·0.16 -0.67 1.02 

09:S4·10:1S 0,01 ..,_,., l.Ol 

10;29·10oSO ·0.10 .().50 1.01 

11:00-U:Zl .0.19 .0.'14 )..03 

11:.3l ·U:S2 0.01 .0.29 l.Ol 

121ll•ll;2-4 000 .0.50 L02 

l2..36-ll.n .0.10 .0.~ l.Ol 

13:09•1UO .009 .024 1.03 

ll:4l--1.:04 .(),27 .(),43 1.03 

~11-14~ .0.17 -0.49 LD3 

A·2 

~ 

""Con"tatd 

ConctftC:tl tkm 

Ul 

t.l6 

1.84 

.... 

9.27 

9 29 

9.43 

9.02 

9.15 

$,97 

1111.,-Corrected 

Conufrtrttk>ft 

13.21 

13711 

13.33 

l'J.-91 

1U3 

IUJ 

U.C? 

11.41 

11.74 

t3.44 

8111 Corttcttd 

Concentrttlol'l 

0.5 

0.6 

••• 

0.1 

OJ 

OS 

0.) 

0.2 

o.2 

O.l 

A-190 

VESOI2644 
Project Name 2013 CPT RAT As Pas• I of A ,. .. 'fl 

> Project Number 40942S)B't,.or, Operator IJ.-\.DD 

!" 

"' 

m < '~ en 

0 

-

N 

~ 

"" 

FacQity veorta Sauget Condition(s) IU<-T.A 

SOUrce UO'I ;+ 4 ~~ Run(s) ~~S l-j 0 

Date '1 l..<t lt "> 

Calibration Gases 

Componentts) 1 Suppltar" concontratlon(s) Cylinder lO 

~·1.. A& pvv~ 1- '"l-..,...:-= . , -

~le o~ s 2. .<R"f. o,./z.<n1. a: (.{.\1.11~ 

I .A:L.. t.z . .-,ofnfr "\ .1 *1. CC.IS"'IPV"' 

l AL.. 1\.1·1. I "'.-:t4"1. AAI..IMOt. 

c.o A& 8'1. eo o<>""' CC ~t~ 

.L )rl, 4\t ~ oPIAA CC2.\? "t-4'1 

' lndiute multkclm.ponent stoandards appropri3ttfy 

'Coda: AG·A1rc-.s; AL·Air Uqulde; s-scott; p.:,taxarr 

Instrument Identification 

Anafyte MOW'IUIK· Modo! Serial N'umbct lnstn.l.ment NI!I'M t\lrar J Numbe:r 

OL~ !> I 144o I~PI /Jit-ts, o, \N ....... , 

o .. ~ ~~\< IAl0!-~1 Ol.J~~~-2 2o"l"l20 

U> T 4eC.. . AIIC..-~5,1,-~M -r~~ 

- '7i' 2000 61 14-\1~ K.AA+ ,_ 

~ 

J Code: T-Thttmo; W-Wtsttrn.; C-Ca.Jlfoml•; s-~rvomtx; O.()rntp 

~~ 

~ 

~ 

Method Performance Checks 

Activity Method Criterion Initials 

3A. «;. '" Emissiofu: bdwun ~ Md 10(),;. of a i brltion spu ll) tuJI!) l.pM Sdec:don 

$pan 1..5•2.5 ~mes tt.e tm ulon Rmit; If no tmtuSon Bmit:, 2SA spon 1.s-:z.s time$ expec.ted kvtl - 3A. «;. 7E, Protocol pt;; Clllbfa:tion ~n. 40·60" of aibralion sptn, 

Clllbr.ltion GI \)..q)1) S 10 and ~of ealibui.Jeft U~oJ,n {ot 1tro aut 

Seloclloo 2SA """""'PJ' 2S-lSl< • ..S.SS11 and 81).- cl """ ..,.. C1'11d9~ir -- Span sas YAthln !-2.0" of calbratlon span 'IM-121)_ 3.4,6C.Jt. Mid~n~ I" wtlhin .!2..'"' oi alib"Uon fl)tn ll) ll.U>D 

Olbation (IT"CK 

2.tto p5 ~ :l.2.0:5 of allbnoWn Sptn •.. 1M®. Low-flnee a;u within 5" or ct.rtifled v•lu:e - 2SA Mid-n"ge GM wkhin S" of certlfte:d value - ~n ps wtthln 5" of cettifttd vaftre 

Co!WelteT Chtct 7! ~ conYffttf tffk:ieney - 1 

System Bias k 3A. GC, 7(. Gas throu.eft JVS't*m agrtej with e.libr~ 'lon errOf' vatuc fat 

ll) that gas wltlllll t5.0!4 ol calil>noon >9>0 I.UW 

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lO. lSA MD 

3A. 6C. 7£, 

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Stlitded cas rt3<fing within :tl.O% of ~tlr.atbn $~n of 

3A. GC, 7~, pre-iest re.ldltlfl; VvlllP : 

Post-Test tO Zero ps wtthan tl.m( of callbrttlott .span or cwe-ust 

c.r...-.-- rudin& !MOO 

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--- FDS-018 <EMS Opuorro. 

Pv E'M SOP.C/6, SCN'-OZT. S0N)28, SONJZ9. SOP-037 

Revl:1lon Otlte: Aprl'/ Z0/3 
I 

CEMS Operation Log 

Project Name 2013 CPT RATAs 

Project Number 09425~2-'> 

Facility Veolia Sauget 

Source V11 it- 4 ')~c.~ 

Time Ac;tj~ty 

Turn on Analvtfrs 1 

OHS CA.! En~.-- /IJ ; ~» o 

OM~ 2-2 ~'1· o.Jt1.? 'l.rr.. ~ .. 

01-Al.t 11.1 .. 1. o •. h.::t-4-.'1. to IMic:t 

0 1-i<,\ ~ .1'.0 ""~ CD "!. ....... "'" 

Ol?'t 4V, '> iiPAA c0 ~;.,l. 

c?l~ CGU. Si<A-<, 1\r.l. ?:<Yb 

0801 -41. . .; ;,., W\ C'.O 1M ,;,A 

~~ tu'!.o: h .'M"1.CO.. IAA•(f ~ .. ..... 

~ ~7. o.J z...O'\ '1. tOt. "t>t~o" 

OOl l ZZ.'J*Io 0.. 1'1.2.~~ CIJ, Sao,.,. 

~,., l\.1 '7o O, I "1.14,. ro, w;.J. 

OJ!IC:. Z.l>'l•f. o 1.01 •f. (.o, "t:a-o" 

~--~·"~- ~ II.I•J.o.l'f.14,.CO. ll.li 

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<»,!1,1; J: • ..l 12...1 

<Y'I!h <::. U I.A. fZ..\l11t. I 

0'\"ll.t P. wJ.. fZ..X1' .A. 2.."" l 

O'I?.JI. eM p,;.., .. N• ?~vo 

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(OV:. -4\,.~ m ........ C'IJ tAMd. 

IOZ.."' $~+ . ~1".). ~"' :1, 

l oi;O ~Y\d. ru.·u . eu"' 3 l Comments 

' "T\Ifi'IOI\ ll m" iS odowm~N sufflcrt'(lt \.,.iiMH4'1 time. 

!f ap¢ltlob1t. "ye~tetd~y" k III'I &Oteptable crrtrv. 

. 

o._ "'t+ 

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Conditlon(s) ~lA 

Run(s) 

Date 

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(1 . 22. 

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0 .0':1-

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Ct> .. .,1."'1 co """' Flow Rate 

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FDS·OI,< CE/ofS {)pur>IIM 

Per EM S0/'.()16, 501'·027. SOP-028, $Glllo<l42 SOP-IE7 

bvisi()n~ts: Apt'11'POJ3 

VES012646 
CEMS Operation Log 

Project Name 2013CPTRATAs 

~' Project Number 40942S)(1V.. 

F>eility Veolia Sauget 

Source Urt•'t- -4 Sto-Lt. 

Time 

o.oo 

II'ZM 4u ~ ... o.u.. c.o llli..l. -

111..1' 1 o"'t'•J. o.ll.Cf\"1 .. en. 1~ \."15 

12PI II. I •1o o, l'l."f'4.7,.. co. ~o<i 1a.'\ll 

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li?l, I (> ' R t iB 1.. ~ 'HYt":l o.oo 

l C~monu 

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U JCII)IIctbl•, "Y~ntiN)" i.S ;;~t XJto:pta~e t'l'ltf"1. 

Pore .3 

Operotor IU-1>!) 

Conditlon(s) !it-~T .A 

Run(s) 12.vw; J1- -

Date "1/""tll :>, 

~ · o.oe -o. "12.. 

1-. 12.. 

1\. Of> 

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M-. 12. 

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of -4 

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.L 

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4~. 

I 

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lA U>...-

l' 

FOS·OJ.A C6115 Opuat!M 

f><r fM SCNJ/6, 501'.()27. 501'.()28, S{ll!-£!i9. 5~7 

Rct~t:SWI'f>}}li: Apn12013 

A·5 

VES012647 
CEMS Operation Log 

Project Namo 2013 CPT RAT As Paae 4- of 4 

Project Number 409425~ t.'J Operator lAM)[) 

Facility veolla Sauset Condltlon(s) !U-TA 

So~rce \)V' i-t- 4 c;~q:_ Run(s) ~II\'> " ~ I'D 

Date " 1411?. 

Time Actlvfty 

Analyzer AelpOM6 Sample 

o ... ~ (h~ c.o .. """o.t (.OclY\., Flow R>lt 

Twn on A.Miyters 1 .. - - - - .. 

,~;~ r .oJ l'.>o..~ •. J. ?.I .Yo o.oc 0 ,0\1 ' o .os ...:o .t z. 4LDM 

(1,~ Alo.~ <>n••"' C' 0 UAI,.,l -- - - 44. "fZ. 

\ 

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1404 ~Y\ol. ~n. e. .... -.,- J. 

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1410 -'\v.; .,.....,._ c.o 1M icl - - - 41- ~ .1 

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A·6 

VESOI2648 
Response Time Determination - EPA Method 7E 

Applicable to Performance of EPA Methods 3A, 6C, 7E and 10 

Project Name: 2013 CPT RAT As 

Project Number: 40942S)a'V, 

location: Veolla Sauget 

Parameter .t ~ Oz. 

AMiyzor Make and A>"< ~t-~ Jt« Model IZ."I'A caus o,~, Q 

AnalyJtr Name A'S!><-t t 2o'l"t'Z.O 

Arnoly1er Ran1e o- Zb"/. 

From Zero Upscale 

To Upscale Zero 

Stort Time (hh:mml or,, lir :tz.:~o 

15 sec 2.00 ~2 44 

30$0< t:Z.. 11:> 2 ,01!. 

4S sec z.z.?l 0~ 

60sec ~V7u 2 .oz. 

75 sec 2.1.#0 

90sec 21 .63 

10S se< 

120sec 

t35 sec 

lSOsec 

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180 sec 

195 sec 

b:sponst nme 1 <?O src. ?Osee 

AMiyaer 1\tsj>onst Time • .;o sec.. 

1 Time io Jee»Dd.ftO ttatb 9S~o( dn.al N.ble \'IIUt. 

'Cruter of upscale aM~ rupom-etimt 

Source: l_Mo't- 4 Spo..c); 

Date: "11411 ? 

Time ()8 : U - 08: '!>0 

DY'1 0 1. 'Dv'-1 (O 

SQ-vo'I'Y\~ 144o "J"»ul\l\0 48C. 

W"'·i+s ::r: "\ "1. "1 

o- 2.5"'Jo o .: loo R>W\ 

Zero Upscale zero Upscale 

Upscale zero Upscale Zero 

~ ot>'ZS ~ ·. ~Z. io 

O .C)'f· ~Z-42 -o.zo ')o.<;1-

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1-Z .4 z. 0 . 11 <M."f:J. z.z.s 

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'08 ~1-

$ ."\'1 

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-:t? s~ c.. "Ostc.. 

Cylinder Number Actual Value 

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Upscale c.<:-14'"1- ~(.p 

UpSCale 

Zero l)t-4(le)n">l•n - lA 

c.c 2\~ 

A·7 

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... 227 

A-39 

VES012681 
APPENDIXB 

Reference Method Calibration Results 

A-228 

VES012682 
Project Trtle Veolra S.uaet Oriit4 RATA 

t.oation Sa set. ll 

Project 10 4094~5-ls 

D.lte 9/ 4/13 

Technician mdd 

O.cvcr.n. Wet 

lnsuument Ma.ke/ Model: Ametok ~M C£M 02/lQ 

ID Numbe.r/Nilme: 

Calibration Sp.an Value: 

Anllyttr Rance: 

tMits.:. 

Alsot1207720 

zzs 

25 

" ...'::1 

Ox en. Wet 

,. Value 

u 

0J(ygen, Dry 

So~l440 

Walts 

22.5 

.-25 

% 

=1 

, Gases Used 

Oxysen, Dry 

ty!inder W I Value 

I 

carbon MonoJCkSe 

Th:ermo48C 

IIIII' 

89.8 

100 ' 

ppm 

tarbon I 

Vah.ae 

Zero CC1219441 Span ccta966s , 22.5 

Mid,.range MU8906 11..1 JK 

0.0 

CC189665 :1 22.5 

AAU8906 Ill 

•• 

157-IA 

CC14436 

CC215749 

0:0 

89,8 

46.3 _, Low-Rare~ 

Nn. rh.ua. ....... Gas 

Zero 

Mid-Ranee 

lOw Aance 

Span 

Zerv 

Mld·R• nc• 

~Ranc~ 

Span 

Ze<o 

Span 

Mid rance 

Low-range 

>4 

Umlts for Calibration Gas Selcttion 

Oxygen, Wet Oxygen, Dry carbon Monoxide 

Lowtr I Upper Lowe r I Upper lower I Upper 

o.oo 1 •.so 

9.00 13.50 

a.oo I 4.50 

9.00 13SO 

o.oo I 17.96 

l5.92 53.88 ;:J 

I< 

Does the Calibration GS$ Meet the Sek!ctlon Criteria? 

oxv1en. wet 

Qlllbration 1 Is it GoocH 

G.n v.tu. 

2.07 

~ 11.10 

TRUE 

TRUE 

Oxygen, Drv I Carbon Monoxide 

Cllibratton Gas ~ Is ft Goodl 

Value 

0.00 

11.10 

TRUE 

T~UE 

c31ibriltlon Gas 

Va:lue 

0.0 

46.3 

Is it Good7 

TRUE 

TRUEd 

Umlts for Direct CaJibtationn (At the Instrument) 

Oxnen. wet 

Lowtr 

1.62 

22.05 

-- 10.65 

Uppt_r 

2.52 

22.95 

11.55 

Oxyf,en .. Dry I Carbon Mono)IJde 

Lower I Upper I Lowtr I Uppe.r 

.0.45 I 0.45 I ·1.8 I 1.8 

zz.os 22.95 88.0 91.6 

10.65 11.55 44.5 48.1 - l 

B·1 

A-229 

VES012683 
Profect:IO: 40942525 

._., CEM OZftCl 

7720 

te<eps 

........ 

mlcle I QJ,I liri'W 

Run No. Cytll\det Va~ CEMS 'flmt I Pre--Test aiMS I" of "" 31>1n) .... ..,.. ......... Run 1 2.07 2_00 01;16 2.00 0.0" 

LL10 10 ... 0818 ID.97 ..... llun2 21J7 2.(10 09.32 1.95 •lUll 

ll.lO 10-'8 09:J.C W.1S •1/J!< 

Run ~ 2.07 2.00 10:18 1.88 .•. s .. 11.10 10.98 10:22 10.68 •1.)% 

~ ... 2.01 2.00 10:56 2.00 0.0!1 

11.10 10.98 10:58 1Cl.97 ..... OunS 2JJ7 2.00 U :ll us .o.z,. 

11.10 10.98 IUO 10.17 .0""' 

ltun6 2.07 2.(10 11:S9 1.99 0.0!1 

LLtO 10.98 llill 10.96 .j),l,. 

Runi' 2 .07 t OO 12:31 L9S •0,2% 

11.1.0 10 ~ 12,35 10.80 .•.• ,. Rt.~nl 2.()1 2.00 ll:04 ,_,. .., .. ,. 

Jl.JO 10 ... 13:06 l0.74 · LilO 

Aunt 2.07 2.(10 13:58 1.97 ·CUS 

11..10 

··~ l):.CO l0.1Q •I 2S 

RunJO t07 2.00 14:13 2.03 0.1~ 

11.10 10.08 14: 14 10.99 0. 1" 

Veolla sau1et Unit 4 AATA 

Wet Oa Callbtatlon Oatil SUmmary 

calibration Error Test Result~ 

cylinde-r ID CIPrtified Valuot ,..,. CEMRtiPOnst 

CCU1944 2.07 08 ... I 2.(10 

CC13966S 22.50 08U 11.54 

AA!lm6 11..10 01•14 IO.SO 

ClMS tafibratiOfl llu Md Drift Tests 

Post·Ttst C£MS ... , Dflft 

Time C"o' Span) . ........ i" of"""' ...... ,., ... 

09:32 LOS .0.211 ..Q.Jt(. 

OUt l O.JS IIJ!< 1/J!< 

10:18 1.88 .o.s .. OliO 

ID:22 10.68 · l.l"'C ·0.)!0 

10 :S6 2.00 0.01< o.s .. 10:58 10.91 o.ox. 1.3" 

11:28. 1.05 ·0.2K -0.2ti 

11:!10 10.77 .,,,. .... ~ 

11!59 l I$ OIJ!< 0.1" 

U:Ol 1,0..96 .0 '" .. ,. 

lful 1,95 .0.2l0 ...... 12;;l.5 r -10.80 .0.8l; ...... H:04 t.94 ~.3" ·0.1% 

3~ - 7~ ·l.l 'M .5~ 

- 13:38 ... , .O.l" 02l; 

lUO 10.70 ·Uti .0"' - JJ;:U 2.03 O.J" .. ,. 14'14 10.99 0.1J'i l.ll< 

14:47 1.99 o.o• .4),2,. 

14:SO 10.82 .o .... ..0.8" 

B-2 

Cai Enw 

Absolute otfferenct i"ol~) ...,. ..... OIJ7 0.3% 

0.04 .. ,. 

o.u ... ,. 

Cq. 7E·S 

c.,.un 

c--1C..c.ll..lA9 

c.- 1.917 

~ll62 

Co• 1.941 

c_l(c,..<ot 1.2SO 

... 1.976 

C.../(~1.249 

Cr 1.971 

~l.l'l 

<.- 19n 

c...Jic.r-Col 1.211 6 

C." 1.945 

c...JIC..·Col 1.ua 

Cr l.D~7 

~1167 

..... 2.(102 

C.A~ 1 ZS.5 

eo,.l.OU 

c~c~ 1.248 

""2JO 

VES012684 
Projed IDl 094~SU 

·- ....... 

,,_.sas 

mlckt:nn 

'l tal'""' Tl ]P..-T ... CXMS .... R~mNo. [VI ~er Value CEMS "of S~taft.• 

.......... m~ h$pon5(l .... <H . 

..... 0.00 0.00 .,,, "o.os Om< 

U.JO IUl ..... 11.11 ...... .... , o.oo 0.06 09:16 0.06 0001 

11.10 11.22 09:34 u.u ·O..S" 

• ..,a 0.00 0.06 10:20 0.06 0.0 .. 

11.10 11,22 10:22 1lll ..... ..... 0.00 0.06 1051 0.06 ..... IUD 11..22 1058 1Lll 

0 '" 

..... 0.00 o.06 U23 Q.06 Cl.lll 

11.10 1Ll2 U.lO u.u -O.SlC 

Run' 0.00 0.06 1l:S6 0.07 0.1" 

U.lO u.:n: U<ll 11.10 ·0.6" 

.... , 0.00 006 ~:27 0.06 O.Ol< 

lLID u.u 11:55 11.09 .0601 

. """. 0.00 0.06 u.oo o.06 o.OOI 

U.lO 11..22 UOi 11.10 4 .5 .. 

I .... 9 0.00 0.06 1~.3 0.05 ..... LLIO ll.ll UA<> 1L10 .0.601 

Roft10 0.00 0.06 14:07 0.06 0.0% 

UJ.O 11.2l 14:14 JL09 .().6)i 

VtoHa Sau1et Unit' RATA 

Dry 0 2 Calibration Data Summaty 

C•ll,r.tk)n t:ffot Ten~ 

Cyti'ldw I) Gi!rtlfiedY,.Yf: r.,.. 

Sl-4001Ul57·lA 0.00 07cll 

CCl~l 22.50 07;43 

AAU&90' 11.10 07:.46 

CEMSCaflbttt III.IIS t l'ld Drift Tests 

Poft•TcJt CfMS .. .. TliM ("of Span) ........ s.o .. '"""" 

09:!1 O.ll6 

0034 1lll ...... """ 

1()'70 0.06 0,0% 

W:22 U .ll -O..S"' 

- 10:55 0.06 0.0 .. 

10:58 lLll -O.S .. 

11:.U ,..o.oe 0.1" 

U :)O 11.11 ..... , 

U"54_, - 0.07 .. ,,. I U~l - 11.10 ' 

.0.6 .. 

1'2 27 O,IW" 0,0,. 

12 1~ 11.09 ·0.6% 

- u-oo 0 .06 O.O'K. 

ll:06 - 11.10 .0.6" 

ll!lJ - o.os 

13.40 11.10 ...... ·~ 

14:07 -- 0.06 o.OOI 

l4;U 1L09 .0.6916 

14:4 1 ~ o.cm \4~ 11.10 .0.5" 

B-3 

Abseil~• Cll Error 

ClM ""'1101'1• Oiffere'KI! l""'""ol l.O.Umit 

0.00 0Jl6 CUOI 

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o.n, 

O.DII <...nc..<.IIM4 .... - ..... c.. o.o6l 

0.001 c../IC.,<,J LOOS 

..... C'o· 0.062 

O.oK c..,NC,.<.g,) t.oos 

0.101 ~· 0.071 

0001 c..nc..<oii.DOG 

..... ... 0.01S 

·O.l'C <.JIC..C,I 1.007 

o.o" "'0.003 

0.091 <-A<.<ot 1.006 

0.091 Cr O.OS7 

0.091 <.Jt<,. <.i 1.006 

..... "'o.os6 .... '-"'-"o'1.00S 

0.091 C.· O.OS8 

O.O'll ~1.006 I 

o.ow. "" 0.058 

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A·23 1 

VES012685 
·i"' 

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APPENDIXC 

Unit 4 CEMS Relative Accuracy Data 

A·233 

VES012687 
Tlme_5tamp I COOryCorr 02 Wet 020ry H20 

9/4/ 13 9:06AM 0.12 8.28 12.58 34.16 

9/4/13 9:07 AM 0.19 8.16 12.40 34.24 

9/4/13 9:08 AM 0.11 7.95 12.19 34.73 

9/4/13 9:09AM 0.00 7.84 12.10 35.20 

9/4/13 9:10AM 0.11 7.82 12.10 35.38 

9/4/13 9:11AM 0.00 8.59 13.36 35.69 

9/4/13 9:12AM 0.00 8.92 13.77 35.25 

9/4/13 9:13AM 0.11 8.05 12.38 34.95 

9/4/13 9:14AM 0.04 8.28 12.92 35.91 

9/4/13 9:15AM 0.00 8.98 13.88 35.32 

9/4/13 9:16AM 0.09 9.31 14.12 34.10 

9/4/13 9:17 AM 0.15 9.40 14.20 33.83 

9/4/13 9:18AM 0.00 9.16 13.82 33.69 

9/4/13 9:19 AM 0.19 9.27 14.04 33.96 

9/4/13 9:20AM 0.13 8.98 13.62 34.10 

9/4/13 9:21AM 0.04 8.79 13.39 34.36 

9/4/13 9:22 AM 0.04 8.58 13.11 34.55 

9/4/13 9:23AM 0.04 8.44 12.95 34.79 

9/4/13 9:24AM 0.00 8.49 12.98 34.57 

9/4/13 9:25AM 0.04 8.45 12.89 34.46 

9/4/13 9:26AM 0.12 8.40 12.92 34.99 

Average O.o7 8.58 13.13 34.68 

Unit 4 Run 1 09/04/13 

C.1 A·234 

VESOl2688 
Tlme Stamp CODryCorr 02Wet 02Dry H20 

9/4/13 9:55AM 0.24 9.26 14.07 34.19 

9/4/13 9:56AM 0.10 9.40 14.26 34.07 

9/4/13 9:57AM 0.00 9.23 13.99 33.99 

9/4/13 9:58AM 0.04 8.84 13.40 34.04 

9/4/13 9:59AM 0.08 8.63 13.14 34.34 

9/4/13 10:00 AM 0.08 8.25 12.63 34.71 

9/4/13 10:01 AM 0.04 8.53 13.15 35.11 

9/4/13 10:02 AM 0.16 8.34 12.84 35.01 

9/4/13 10:03 AM 0.13 8.69 13.41 35.21 

9/4/13 10:04 AM 0.05 8.85 13.64 35.10 

9/4/13 10:05 AM 0.13 8.76 13.50 35.08 

9/4/13 10:06 AM 0.09 8.82 13.57 35.00 

9/4/13 10:07 AM 0.18 8.94 13.70 34.76 

9/4/13 10:08 AM 0.24 9.37 14.26 34.29 

9/4/13 10:09 AM 0.10 9.48 14.34 33.92 

9/4/13 10:10 AM 0.05 9.11 13.94 34.24 

9/4/13 10:11 AM 0.09 9.03 13.72 34.18 

9/4/13 10:12 AM 0.00 8.93 13.60 34.29 

9/4/13 10:13 AM 0.00 9.12 13.87 34.23 

9/4/13 10:14 AM 0.13 9.06 13.77 34.19 

9/4/13 10:15 AM 0.14 9.11 13.85 34.20 

Ave,...ge 0.10 8.94 13.65 34.48 

Unit 4 Run2 09/04/13 

C-2 A-235 

VES012689 
Time Stamp I CO DryCorr 02Wet 02Dry H2.0 

9/4/13 10:30 AM 0.08 8.71 13.25 34.23 

9/4/13 10:31 AM 0.13 8.79 13.39 34.40 

9/4/13 10:32 AM 0.04 8.81 13.44 34.40 

9/4/13 10:33 AM 0.17 8.71 13.26 34.28 

9/4/13 10:34 AM 0.17 8.69 13.25 34.44 

9/4/13 10:35 AM 0.13 8.65 13.25 34.73 

9/4/13 10:36 AM 0.17 8.70 13.39 35.03 

9/4/13 10:37 AM 0.04 8.63 13.21 34.65 

9/4/13 10:38 AM 0.09 8.91 13.47 33.83 

9/4/13 10:39 AM 0.04 8.95 13.46 33.50 

9/4/13 10:40 AM 0.04 8.78 13.25 33.71 

9/4/13 10:41 AM 0.13 8.77 13.37 34.41 

9/4/13 10:42 AM 0.05 8.82 13.58 35.09 

9/4/13 10:43 AM 0.00 8.53 13.09 34.85 

9/4/13 10:44 AM 0.08 8.31 12.82 35.22 

9/4/13 10:45 AM 0.00 8.32 12.90 35.52 

9/4/13 10:46 AM 0.04 8.22 12.72 35.39 

9/4/13 10:47 AM 0.00 8.53 13.17 35.25 

. ~/4/13 10:48 AM 0.12 8.31 12.76 34.84 

9/4/13 10:49 AM 0.10 8.95 13.74 34.88 

9/4/13 10:50 AM 0.05 9.52 14.47 34.22 

Average 0.08 8.70 13.30 34.61 

Unit4 Run 3 09/04/13 

C-3 M!36 

VES012690 
Time Stamp COOJ'V(orr 02 Wet 02Dry H20 

9/4/13 11:01 AM 0.18 8.77 13.48 35.00 

9/4/13 11:02 AM 0.13 8.91 13.61 34.53 

9/4/13 11:03 AM 0.18 9.00 13.71 34.37 

9/4/13 11:04 AM 0.05 9.04 13.76 34.31 

9/4/13 11:05 AM 0.10 9.34 14.22 34.35 

9/4/13 11:06 AM 0.19 9.45 14.26 33.75 

9/4/13 11:07 AM 0.14 9.41 14.11 33.28 

9/4/13 11:08 AM 0.05 9.45 14.24 33.66 

9/4/13 11:09 AM 0.09 9.31 14.09 33.90 

9/4/13 11:10 AM 0.09 8.95 13.63 34.32 

9/4/13 11:11 AM 0.00 8.68 13.29 34.69 

9/4/13 11:12 AM 0.00 9.06 13.89 34.73 

9/4/13 11:13 AM 0.09 9.05 13.65 33.71 

9/4/13 11:14 AM 0.04 8.92 13.49 33.83 

9/4/13 11:15 AM 0.14 9.22 13.99 34.07 

9/4/13 11:16 AM 0.09 9.34 14.12 33.84 

9/4/13 11:17 AM 0 .09 9.40 14.23 33.94 

9/4/13 11:18 AM 0 .19 9.43 14.31 34.13 

9/4/13 11:19 AM 0.19 9.39 14.23 33.98 

9/4/13 11:20 AM 0.13 9.08 13.77 34.10 

9/4/13 11:21 AM 0.13 9.00 13.71 34.35 

Average 0.11 9.15 13.89 34.13 

Unlt4 Run 4 09/04/13 

C·4 A-237 

VES01269l 
TlmecStamp I COD~Corr 02Wet 02Dry K20 

9/4/13 11:32 AM 0.15 9.66 14.62 33.90 

9/4/ 13 11:33 AM 0.05 9.52 14.48 34.25 

9/4/13 11:34 AM 0.15 9.38 14.30 34.46 

9/4/13 11:35 AM 0.00 8.89 13.62 34.70 

9/4/13 11:36 AM 0.09 8.75 13.58 35.53 

9/4/13 11:37 AM 0.05 8.86 13.81 35.86 

9/4/13 11:38 AM 0.05 8.90 13.86 35.82 

9/4/13 11:39 AM 0.67 9.13 14.15 35.48 

9/4/13 11:40 AM 0.72 8.97 13.66 34.35 

9/4/13 11:41 AM 0.04 8.89 13.52 34.23 

9/4/13 11:42 AM 0.04 8.92 13.56 34.18 

9/4/13 11:43 AM 0.04 8.90 13.50 34.08 

9/4/13 11:44 AM 0.13 9.17 13.92 34.11 

9/4/13 11:45 AM 0.19 9.33 14.14 33.97 

9/ 4/13 11:46 AM 0.00 9.2.5 14.01 33.97 

9/4/13 11:47 AM 0.09 9.11 13.86 34.27 

9/ 4/13 11:48 AM 0.04 8.71 13.35 34.74 

9/4/13 11:49 AM 0.04 8.23 12.71 35.22 

9/4/13 11:50 AM 0.04 8.96 13.87 35.44 

9/4/13 11:51 AM 0.18 8.99 13.79 34.82 

9/4/13 11:52 AM 0.05 9.13 14.00 34.79 

Average 0.13 9.03 13.82 34.67 

Unit4 Run 5 09/04/13 

C·5 A-238 

VES012692 
Time Stamp CODryCorr 02Wet 02Dry H20 

9/4/13 12:04 PM 0.00 8.82 13.51 34.69 

9/4/13 12:05 PM 0.05 8.72 13.42 34.97 

9/4/13 12:06 PM 0.14 9.11 13.96 34.73 

9/4/13 12:07 PM 0.05 9.08 13.78 34.10 

9/4/13 12:08 PM 0.05 9.19 13.97 34.23 

9/4/13 12:09 PM 0.10 9.38 14.26 34.24 

9/4/13 12:10 PM 0.10 9.44 14.32 34.05 

9/4/13 12:11 PM 0.00 9.34 14.19 34.15 

9/4/13 12:12 PM 0.05 9.15 13.94 34.37 

9/4/13 12:13 PM 0.00 9.30 14.19 34.48 

9/4/13 12:14 PM 0.24 9.33 14.20 34.29 

9/4/13 12:15 PM 0.05 9.34 14.19 34.17 

9/4/13 12:16 PM 0.14 9.14 13.93 34.35 

9/4/13 12:17 PM 0.19 9.18 14.04 34.61 

9/4/13 12:18 PM 0.09 8.88 13.58 34.64 

9/4/13 12:19 PM 0.22 8.76 13.44 34.85 

9/4/13 12:20 PM 0.09 8.83 13.52 34.69 

9/4/13 12:.21 PM 0.1.3 8.75 13.35 34.50 

9/4/13 12:22 PM 0.17 8.72 13.39 34.82 

9/4/13 12:23 PM 0.13 8.80 13.53 34.99 

9/4/13 12:24 PM 0.09 8.59 13.22 35.05 

Average 0.10 9.04 13.81 34.52 

Unit 4 Run 6 09/04/13 

A·239 

VES012693 
Tlme=Stamp CO OryCorr 02Wet 020,Y H20 

9/4/13 12:37 PM 0.04 8.45 13.03 35.16 

9/4/13 12:38 PM 0.13 8.72 13.45 35.14 

9/4/13 12:39 PM 0.09 8.95 13.71 34.72 

9/4/13.12:40 PM 0.28 9.21 13.99 34.15 

9/4/13 12:41 PM 0.13 8.81 13.39 34.21 

9/4/13 12:42 PM 0.09 8.97 13.82 35.11 

9/4/13 12:43 PM 0.09 8.87 13.71 35.33 

9/4/13 12:44 PM 0.05 9.01 14.00 35.64 

9/4/13 12:45 PM 0.00 9.15 14.10 35.14 

9/4/13 12:46 PM 0.09 8.93 13.68 34-72 

9/4/13 12:47 PM 0.05 9.08 13.93 34.82 

9/4/13 12:48 PM 0.09 9.04 13.91 34.98 

9/4/13 12:49 PM 0.00 8.72 13.43 35.05 

9/4/13 12:50 PM 0.09 8.59 13.30 35.48 

9/4/13 12:51 PM 0.09 8.67 13.51 35.84 

9/4/13 12:52 PM 0.05 9.02 14.00 35.56 

9/4/13 12:53 PM 0.14 9.00 13.84 34.97 

9/4/13 12:54 PM 0.00 8.82 13.56 35.01 

9/4/13 12:55 PM 0.05 8.84 13.63 35.13 

9/4/13 12:56 PM 0.09 8.98 13.81 34.99 

9/4/13 12:57 PM 0.18 8.97 13.76 34.80 

Average 0.09 8.89 13.69 35.05 

Unlt4 Run7 09/04/13 

C-7 .A-240 

VES012694 
Time Stamp CO Dry(orr 02Wet 02 Dry H20 

9/ 4/ 13 1:10PM o.oo 8.93 13.81 35.35 

9/4/ 13 1:11 PM 0.05 9.09 14.04 35.25 

9/4/13 1:12 PM 0.09 9.12 14.01 34.90 

9/4/13 1:13PM 0.05 9.10 13.96 34.80 

9/4/ 13 1:14 PM 0.05 9.18 13.98 34.33 

9/ 4/ 13 1:15PM 0.00 8.81 13.34 34.01 

9/4/13 1:16 PM 0.04 8.31 12..73 34.73 

9/4/13 1:17 PM 0.00 8.56 13.23 35.27 

9/4/13 1:18PM 0.00 8.86 13.63 35.02 

9/4/13 1:19PM 0.05 8.90 13.64 34.77 

9/4/13 1:20PM 0.04 8.57 13.10 34.58 

9/ 4/ 13 1:21PM 0.22 8.68 13.44 35.42 

9/ 4/ 13 1:22 PM 0.09 8.89 13.71 35.17 

9/ 4/ 13 1:23 PM 0.08 8.56 13.16 34.91 

9/4/13 1:24 PM 1.04 8.54 13.15 35.06 

9/4/13 1:25 PM 2.50 8.52 13.09 34.93 

9/4/ 13 1:26PM 0.12 8.33 12.86 35.19 

9/4/13 1:27 PM 0.04 8.22 12.77 35.63 

9/4/13 1:28PM 0.17 8.55 13.29 35.66 

9/4/13 1:29PM 0.04 8.39 13.00 35.41 

9/4/13 1:30PM 0.09 8.49 13.21 35.73 

Average 0.23 8.70 13.39 35.05 

Unit 4 Runs 09/04/13 

C-1! A-241 

VES012695 
Time_Stamp CO OryCorr 02Wet 020ry H20 

9/4/13 1:44 PM 0.00 9.01 13.74 34.40 

9/4/13 1:45PM 0.00 9.03 13.8.7 34.89 

9/4/13 1:46 PM 0.04 8.83 13.59 35.04 

9/4/13 1:47PM 0.13 8.58 13.26 35.32 

9/4/13 1:48PM 0.00 8.70 13.48 35.50 

9/4/13 1:49PM 0.18 8.90 13.70 35.02 

9/4/13 1:50PM 0.08 8.52 13.12 35.08 

9/4/13 1:51 PM 0.00 8.46 13.11 35.42 

9/4/13 1:52PM 0.04 8.62 13.36 35.44 

9/4/13 1:53PM 0.00 8.90 13.76 35.29 

9/4/13 1:54 PM 0 .09 9.14 14.04 34.95 

9/4/13 1:55 PM 0.15 9.55 14.50 34.10 

9/4/13 1:56 PM 0.14 9.60 14.41 33.37 

9/ 4/ 13 1:57 PM 0.05 9.33 14.06 33.63 

9/ 4/13 1:58 PM 0.05 9.26 14.04 34.04 

9/4/13 1:59 PM 0.04 9.15 13.89 34.12 

9/4/13 2:00PM 0.00 9.04 13.n 34.33 

9/4/13 2:01 PM 0.04 8.n 13.41 34.59 

9/4/13 2:02 PM 0.18 8.88 13.62 34.78 

9/4/13 2:03PM 0.13 8.89 13.63 34.74 

9/4/13 2:04 PM 0.14 9.03 13.83 34.74 

Average 0.07 8.96 13.72 34.70 

Unit 4 Run9 09/04/13 

C·9 A-242 

VES012696 
Time_Stamp :.: · I ;· CO DryCorr,· l :·.: 02 Wet:".. ·I ··02Dry ... · ,·· H20 ,,,,,I 

9/4/13 2:18 PM 0.00 8.18 12.73 35.77 

9/4/13 2:19 PM 0.19 8.96 13.84 35.27 

9/4/13 2:20 PM 0.10 9.11 13.89 34.39 

9/4/13 2:21PM 0.44 9.03 13.73 34.24 

9/4/13 2:22 PM 3.13 9.04 13.68 33.89 

9/4/13 2:23PM 1.03 8.37 12.78 34.48 

9/4/13 2:24PM 0.09 9.03 13.91 35.09 

9/4/13 2:25PM 0.09 9.08 13.92 34.80 

9/4/13 2:26 PM 0.09 9.04 13.84 34.69 

9/4/13 2:27PM 0.09 8.93 13.63 34.53 

9/4/13 2:28 PM 0.18 8.93 13.64 34.53 

9/4/13 2:29 PM 0.08 8.43 12.89 34.61 

9/4/13 2:30PM 0.04 8.22 12.70 35.30 

9/4/13 2:31PM 0.12 8.25 12.80 35.58 

9/4/13 2:32 PM 0.11 7.73 12.04 35.82 

9/4/13 2:33 PM 0.29 9.62 15.04 36.08 

9/4/13 2:34PM 0.13 8.95 13.60 34.19 

9/4/13 2:35PM 0.53 8.98 13.67 34.35 

9/4/13 2:36PM 0.09 8.86 13.51 34.46 

9/4/13 2:37PM 0.13 8.60 13.17 34.72 

9/4/13 2:38 PM 0.12 8.34 12.87 35.19 

Average 0.34 8.75 13.42 34.86 

Unit 4 Run 10 09/04/13 

C·IO 

VES012697 
APPENDIXD 

Unit 4 Waste Feed Characterization Data 

VESOl2698 
Hourly Report lnci,......tc< 4 

ONYX Veoli& Created 9141201310:01 AM 

Envlroament>l Services Period Start 9/412013 9:00AM 

Suget Illinois Period End 9/41201310:00 AM 

Pa&e I of I 

CALCULATIONS 

BTU 29.05 mbtu 

PCC BTU 22.33 mbtu Main Line BTU 0.000000 mbtu 

sec BTU 6.71 mbtu Aux Feed BTU 6.761200 mbtu 

Chlorine 93.2 lbs 

Low Volatile 0.147 lbs Mercury 0.0002 lbs 

Semi Volatne 0.942 lbs Ash 663.0 lbs 

WEIGHTS 

Weight 3146 lbs 

Solids Weight 1847 lbs PCC Liquid Weight 1299 tbs 

Shredded Weight 1325 lbs X10 Weight 399 lbs 

Containerized Weight 522 lbs X11 Weight 899 lbs 

Main Line Weight 0 lbs X12 Weight 0 lbs 

Aux Feed Weight 522 lbs X22Weight 782 lbs 

Pit 1 Weight 0 lbs Tank 300 Weight 899 lbs 

Pit2 Weight 1325 lbs Tank 302 Weig.ht o lbs 

Pit 3 Weight 0 lbs Tank 304 Weight 0 lbs 

Pit 4 Weight 0 lbs Tank 306 Weight 0 lbs 

Tank 308 Weight o lbs 

Direct Inject Weight 399 lbs Tank 310 Weight 782 lbs 

Special Feeds Weight 0 lbs Tank 312 Weight o lbs 

Tank 31 4 Weight 0 lbs 

MISCELLANEOUS 

Waste Penni! Time 0.99 hrs Natural Gas Flow 10420 cf 

O.t A-245 

VESOJ2699