# Instructions The EPA secondary aluminum production test program requires emissions and other test data for several pollutants. EPA understands that you own one or more secondary aluminum production facilities. For at least one thermal chip dryer and at least one scrap dryer/delacquering kiln/decoating kiln that you own, you must perform a stack test for volatile and semi-volatile organic HAPs as specified in the letter and instructions accompanying this file. You should collect emissions samples for the identified pollutants downstream of the last relevant emissions control device (i.e., stack or other point representing the composition of the flue gases at the exit to the atmosphere), unless otherwise indicated. (Contact the EPA project lead for situations with multiple stacks or other complex emissions points for the unit.)
Sample and analyze the particulate matter collected in the hopper from at least one bag house used to control particulate matter from each type of affected source subject to 40 CFR 63, subpart RRR at your secondary aluminum production facilities. Choose bag houses that are used to control particulate matter from each of the six different types of affected sources (i.e.group 1 furnaces, scrap shredders, chip dryers, scrap dryers/delacquering kilns/decoating kilns, dross only furnaces, and rotary dross coolers) if you have these controlled affected sources at your facilities. Where more than one bag house discharges solids to a common hopper, a single sample will be adequate. In cases where solids from different compartments of a single bag house are collected in multiple hoppers or multiple collection sacks, a single composite sample will be adequate. If you have a total of three or fewer bag houses at all of your facilities, sample and analyze particulate matter from all of them, even if they are controlling the same type of affected source. It is not necessary to conduct a stack test for multi-metals analysis.
Sample and analyze the lime used for injection to any of the lime-injected bag houses from which particulate matter samples were collected. If lime of the same type, obtained from the same supplier, is used for more than one lime injected bag house, a single sample will be adequate to represent the lime used in these bag houses.

You must report the results of these tests and chemical analyses in this Microsoft® Excel Emission Test Template. The Excel templates are specific to each type of pollutant. You must report the results of each test on the appropriately labeled worksheet corresponding to the specific tests and analyses conducted at your facilities. If more than one source was tested, you must make a copy of the worksheet and update the source ID in order to distinguish between each separate test of a chip dryer or scrap dryer/ delacquering kiln/decoating kiln at each facility and each different source of particulate matter. After completing the worksheet, you must also submit an electronic copy of the emission test report and the chemical analyses. (PDF format preferred).
Please refer to the cover letter of this packet (CAA section 114 letter) for additional testing information. Please note that you do not have to submit a test plan to EPA for approval prior to testing; however, we recommend that you prepare a test plan for your own use to assist in the planning and to verify that you address all of the testing and reporting requirements. You must follow all of the procedures as specified in the test methods, including the quality assurance and quality control measures, and document the results in any test report provided to EPA.**Facility Name and A ddress**  **Unit Description Process Unit ID**  **Control Device ID** Golden Aluminum Delacquering Kiln S002 S002

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing **9/9/2010 9/9/2010**  **9/10/2010** Feed/Charge Rate 2.67 2.31 2.97 Mg/hr Afterburner Operating Temperature 1408 1409 1416 degree F

Type of Charge:_______________________________________________________________________ coated aluminum scrap

**Compound Volatile Organic HA** **P Emission Rate Sample 1** 

**(kg/hr) Volatile Organic HA** **P Emission Rate Sample 1**  **(kg/Mg of feed/charge) Volatile Organic HA** **P Emission Rate Sample**  **2 (kg/hr) Volatile Organic HA** **P**

**Emission Rate Sample 2 (kg/Mg of**  **feed/charge) Volatile Organic HA** **P**

**Emission Rate Sample 3**

**(kg/hr) Volatile Organic HA** **P**

**Emission Rate Sample 3 (kg/Mg of**  **feed/charge) Test Method**  **Used Detection Limit** 

**Information (BDL,DLL,A** **DL) Other Supporting**  **Information** Acrylonitrile 107-13-1 2.13E-04 8.00E-05 2.17E-04 9.39E-05 2.01E-04 6.75E-05 0031 DLL Benzene 71-43-2 5.04E-04 1.89E-04 4.98E-04 2.16E-04 3.44E-04 1.16E-04 0031 DLL Bromodichloromethane 75-27-4 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL Carbon disulfide 75-15-0 4.23E-05 1.59E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 DLL Carbon tetrachloride 56-23-5 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL Chlorodibromomethane 124-48-1 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL Chloroform 67-66-3 4.62E-05 1.73E-05 4.56E-05 1.97E-05 4.00E-05 1.35E-05 0031 DLL Chloroprene 126-99-8 0 0 0 0 0 0 0031 BDL Dibromomethane 74-95-3 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL 1,1-Dichloroethane 75-34-3 4.20E-05 1.57E-05 4.56E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL 1,2-Dichloroethane 107-06-2 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL 1,1-Dichloroethene 75-35-4 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL trans-1,2-Dichloroethene 156-60-5 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL 1,2-Dichloropropane 78-87-5 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL 1,3-Dichloropropene 542-75-6 4.74E-05 1.78E-05 4.86E-05 2.10E-05 4.52E-05 1.52E-05 0031 BDL Methylene chloride 75-09-2 1.79E-04 6.73E-05 6.29E-05 2.72E-05 4.47E-05 1.51E-05 0031 DLL Tetrachloroethene 127-18-4 2.10E-05 7.87E-06 2.14E-05 9.28E-06 2.00E-05 6.74E-06 0031 BDL Toluene 108-88-3 1.77E-03 6.63E-04 1.97E-04 8.51E-05 7.62E-04 2.56E-04 0031 DLL 1,1,1-Trichloroethane 71-55-6 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL 1,1,2-Trichloroethane 79-00-5 4.20E-05 1.57E-05 4.29E-05 1.86E-05 4.00E-05 1.35E-05 0031 BDL Trichloroethene 79-01-6 2.10E-05 7.87E-06 2.14E-05 9.28E-06 2.00E-05 6.74E-06 0031 BDL Trichlorofluoromethane 75-69-4 1.19E-04 4.48E-05 4.29E-05 1.86E-05 5.01E-05 1.69E-05 0031 DLL **Speciated Volatile Organic HA P Emission Data** **Facility Name and Address Unit Description**  **Process Unit ID Control Device ID** 

Golden Aluminum Delacquering Kiln S002 S002

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing **9/9/2010 9/9/2010**  **9/10/2010** Feed/Charge Rate 2.67 2.31 2.97 Mg/hr Afterburner Operating Temperature 1408 1409 1416degree F

Type of Charge:_______________________________________________________________________ coated aluminum scrap

**Compound Semi-volatile Organic HAP**  **Emission Rate Sample 1**

**(kg/hr) Semi-volatile Organic HAP** 

**Emission Rate Sample 1 (kg/Mg of feed/charge)**  **Semi-volatile Organic HAP Emission Rate**  **Sample 2 (kg/hr) Semi-volatile Organic HAP**  **Emission Rate Sample 2 (kg/Mg of feed/charge)**  **Semi-volatile Organic HAP Emission Rate**  **Sample 3 (kg/hr) Semi-volatile Organic**  **HAP Emission Rate Sample 3 (kg/Mg of**  **feed/charge) Test Method Used**  **Detection Limit Information**  **(BDL,DLL,ADL) Other Supporting**  **Information** Acenaphthene 83-32-9 1.25E-04 4.69E-05 1.15E-04 4.99E-05 7.02E-05 2.36E-05 0010ADL Acenaphthylene 208-96-8 5.64E-04 2.12E-04 4.53E-04 1.96E-04 2.85E-04 9.58E-05 0010ADL Anthracene 120-12-7 8.06E-05 3.03E-05 5.76E-05 2.49E-05 5.07E-05 1.71E-05 0010ADL Benz[a]anthracene 56-55-3 1.57E-05 5.90E-06 4.12E-05 1.78E-05 3.90E-05 1.31E-05 0010DLL Benzo[a]pyrene 50-32-8 2.78E-05 1.04E-05 1.85E-05 8.02E-06 3.90E-05 1.31E-05 0010DDL Benzo[b]fluoranthene 205-99-2 4.03E-04 1.51E-04 4.12E-04 1.78E-04 3.90E-04 1.31E-04 0010BDL Benzo[g,h,i]perylene 191-24-2 3.55E-05 1.33E-05 3.05E-05 1.32E-05 3.51E-05 1.18E-05 0010ADL Benzo[k]fluoranthene 207-08-9 4.03E-04 1.51E-04 4.12E-04 1.78E-04 3.90E-04 1.31E-04 0010BDL Chrysene 218-01-9 3.35E-05 1.26E-05 5.76E-05 2.49E-05 3.90E-05 1.31E-05 0010DDL Dibenz[a,h]anthracene 53-70-3 4.03E-05 1.51E-05 4.12E-04 1.78E-05 3.90E-05 1.31E-05 0010BDL Fluoranthene 206-44-0 1.25E-04 4.69E-05 3.09E-04 1.34E-04 7.02E-05 2.36E-05 0010ADL Fluorene 86-73-7 1.61E-04 6.05E-05 1.77E-04 7.66E-05 5.85E-05 1.97E-05 0010ADL Indeno(1,2,3-cd)pyrene 193-39-5 2.94E-05 1.10E-05 2.80E-05 1.21E-05 3.90E-05 1.31E-05 0010DDL Naphthalene 91-20-3 2.82E-02 1.06E-02 2.59E-02 1.12E-02 1.36E-02 4.59E-03 0010ADL Phenanthrene 85-01-8 1.49E-03 5.60E-04 1.48E-03 6.41E-04 5.85E-04 1.97E-04 0010ADL Pyrene 129-00-0 2.42E-04 9.08E-05 2.76E-04 1.19E-04 2.34E-04 7.87E-05 0010DDL **Speciated Volatile Organic HAP Emission Data**

### Facility Name and A **ddress Unit ID**  **Unit Type (Chip dryer or scrap**

**dryer /delacq /decoating kiln)** 

## Golden Aluminum, 1405 East 14th Street, Fort Lupton, Colorado 80621 **Delacquering Kiln Delacquering Kiln** 

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information Date of Testing**  **9/9/2010 9/9/2010**  **9/10/2010** Feed/Charge Rate 

## 2.67 2.31 2.97 Mg/hr Afterburner residence time 

## >1 >1 >1 sec Afterburner Operating Temperature 1408 

## 1409 1416degree F



## 1 9/9/2010 8:47 9/9/2010 12:55 2 9/9/2010 13:55 9/9/2010 18:00 3 9/10/2010 7:45 9/10/2010 11:52

**Run Number THC Emission Rate (kg/hr)**  **THC Emission Rate (kg/Mg of feed/charge)**  **Data Flag (A DL, BDL, DDL)** *** **Detection Limit (ng/dscm)**  

## 1 0.027 0.010BDL 3846490 2 0.027 0.012BDL 3769074 3 0.021 0.007BDL 3792558 *** See Appendix A to Enclosure 1 **Test End Time**

**Run Number Test Start Date**  **Test Start Time Test End Date** 

### Facility Name and A**ddress Unit Description**  **Process Unit ID Control Device ID** 



## Golden Aluminum, 1405 East 14th Street, Fort Lupton, Colorado 80621 Delacquering Kiln S002 S002

**Parameter Sample 1**  **Sample 2 Sample 3**  **Unit of Measure Other Supporting**  **Information** Date of Testing **9/9/2010 9/9/2010**  **9/10/2010** Feed/Charge Rate 

## 2.67 2.31 2.97 Mg/hr Afterburner Operating Temperature 1408 

## 1409 1416degree F Flow Rate 

## 464 470 458actual M3

## /min Flow Rate 

## 277 285 276dry sM3

## /min

**Emission Test Results Constituent**  **Composition Sample 1**  **(%) Composition** 

**Sample 2 (%)**  **Composition**

**Sample 3 (%)**  **Test Method Used**

**(ex. U.S. EPA**

**Method 3B) Other Supporting Information**  O2 

## 18.1 18.4 18.5 3A CO2 

## 2.1 1.9 1.7 3A H2

### O 

## 4.8 2.8 3.4 4

## Facility Name and A**ddress Unit Description**  **Process Unit ID Control Dev** **ice ID***



## Golden Aluminum, 1405 East 14th Street, Fort Lupton, Colorado 80621 Delacquering Kiln & Melt Baghouse S002 & S006 S002 & S006
**Sample ID No._Virgin Lime Type of Sample (Lime or Particulate):_____________________________**  Lime
**Date Sampled Date(s) Analyzed**  9/9/20109/21-22/2010

**HA P Metal**  **mg/kg** Antimony 

## ND Beryllium 

## 0.14 Chromium 

## 5.9 Hexavalent chromium 

## 0.000654 Lead 

## 0.34 Mercury 

## ND Selenium 

## ND Arsenic 

## 2.5 Cadmium 

## 0.32 Cobalt 

## 0.57 Manganese 

## 95.4 Nickel 

## 3.3
*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**

## Facility Name and A**ddress Unit Description**  **Process Unit ID Control Dev** **ice ID***



## Golden Aluminum, 1405 East 14th Street, Fort Lupton, Colorado 80621 Delacquering Baghouse S002 S002
**Sample ID No. Delacque Baghouse Dust Type of Sample (Lime or Particulate):_____________________________**  Particulate + Lime (composite sample) Lime injected at 60 lbs./hr
**Date Sampled Date(s) Analyzed**  9/9/20109/21-22/2010

**HA P Metal**  **mg/kg** Antimony 

## 6.5 Beryllium 

## 0.16 Chromium 

## 16.1 Hexavalent chromium 

## 0.000043 Lead 

## 108 Mercury 

## 0.20 Selenium 

## ND Arsenic 

## 2.6 Cadmium 

## 0.94 Cobalt 

## 2.0 Manganese 

## 179 Nickel 

## 12.0
*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**

## Facility **Name and A**

**ddress Unit Description**  **Process Unit ID Control Device ID** * 

## Golden Aluminum, 1405 East 14th Street, Fort Lupton, Colorado 80621 Melt Baghouse S006 S006
**Sample ID No._Melt Baghouse Dust Ty** **pe of Sample (Lime or Particulate):_____________________________** Particulate + Lime (composite sample) Lime injected at 22.5 lbs./hr
**Date Sampled Date(s) Analyzed**  9/9/2010 9/21-22/2010

**HA P Metal**  **mg/kg** Antimony 

## 2.8 Beryllium 

## 0.74 Chromium 

## 18.2 Hexavalent chromium 

## 0.0000999 Lead 

## 15.6 Mercury 

## 0.072 Selenium 

## 2.5 Arsenic 

## 2.3 Cadmium 

## 4.4 Cobalt 

## 1.2 Manganese 

## 187 Nickel 

## 5.2

*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**

## Facility

**Name and A ddress**  **Unit Description Process Unit ID**  **Control Device ID*** 

## Golden Aluminum, 1405 East 14th Street, Fort Lupton, Colorado 80621 Shredder Baghouse S001 S001
**Sample ID No._Shredder Baghouse Dust Ty** **pe of Sample (Lime or Particulate):_____________________________** Particulate
**Date Sampled Date(s) Analyzed**  9/9/2010 9/21-22/2010

**HAP M etal**  **mg/kg** Antimony 

## 6.8 Beryllium 

## 0.86 Chromium 

## 235 Hexavalent chromium 

## 0.0000249 Lead 

## 261 Mercury 

## 1.2 Selenium 

## 3.9 Arsenic 

## 6.1 Cadmium 

## 4.7 Cobalt 

## 8.5 Manganese 

## 1390 Nickel 

## 37.9
*** Enter multiple control device ID Nos. if the lime results apply to mulitiple control devices.**