## Analytical Chemistry WL-ACP-7 

### I Molecular Spectroscopy and Thermal Analysis Dr . D . Wandschneide r M. Shaukat 

### tr +49-6151-72-561 0 d i rk.w andsch ne ider @ merck . d e 

### tr +49-6151 - 72 -4561 manuela . sha u kat@me r ck . de 

## Analytical Report MS10_52 UVNis spectroscopy of MAFS-092 Client 

### I Date of commission 

### I Ob " ective: Dr . N . F i chtner , WL-ACP8 UVNis spect roscopy of MAFS- 092 09 . 08 . 2010 

# s amp . es: Sample MAFS-092 Bat ch : FS-049-10-3 Artic l e- no .: - SA -7: 2085313 Summary: UVN is Raw date U21021 21

The spectrum is plausible w ith the ind i cated structure . Report Date Page

No add itional absorption bands that may hint t o an U VN is act ive impurity we re observed . History of document 

# I First version 1 13.08 . 10 

# I -

Distribution list: Dr. N . Fichtner WL-ACP 8 

### M . Shaukat WL-ACP 7 . 0

Rev i ewed : 

# !flJ I Approved: I 1 MERCK I MS10 52 13 . 08.10 1 /3



# 113! Zo.-zu 

# !I'LJ

**~** ..



# fJ **~~ !?~** 

# ... 13 0 

# @;

... ... .. ... .. .. . ...... ... ...... q1... .. S . BrOninghoff WL-ACP-7 . 0 S . Eichler WL -ACP-7. 0 Dr . D. Wandschne i der W L-ACP - 7 Head of LaboratoI 

### Analytical Chemistry ' d MERCK I WL-ACP - 7 

### I Molecular Spectroscopy and Therma l Ana l ys i s Report MS10 52 Dr . D . Wandschneider 

### tl +49 - 6151-72-561 0 d i rk.wa ndschne ider@merck.de Date 13.08 . 10 M . Shaukat 

### if +49-6151-72-4561 manue l a . shaukat@merck .de Page 2/3

Results 

### I Discussion:

## Analytical Chemistry I I , M

ERCK 

### • , WL-ACP-7 

### I Molecular Spectroscopy and Thermal Analysis Report MS10 52 Dr. D. Wandschneider 

### tr +49-6151-72-561 0 dirk.wandschneider@me r ck.de Date 13 .08 . 10 M. Shaukat 

### V +49-6151-72-4561 manuela . shaukat@merck .de Page 

### 3/3

### 0000000000 FS-049-10-3

Auftrag : 0002085313 Teilauftrag fur Labor: AC7 Auftrag: 0002085313 Kostenstelle: 

## * kein Zertifikat 

## * Artikel: 

## oooooooooo Sparte: MAFS - 092 09.08 . 10

FF - Lab: AC80 Charge: FS - 049-10-3 Menge: 0,5g Gefahrensymbol(e): Altern Chargen: Muster : 1 

# f Eingegangen am 

## 09 . Aug. 2010 Methode: 9 UV-VIS - NIR - Spektrometrie CAS 

### I AC7 

### Pruftext: Auftragtext: Spektrum von 200 bis 700nm Spektrum bitte mit Interpretation mitliefern Restsubstanz zuruck an Dr.Fichtner und Bericht

Termin: 13.08.10 

## =

=

=== = === = ====== =

---- -- - -- ------------------- Ergebnis der Analyse -- - -------------- - -------- -- 

# )(s· 

# jc __ 

# s:--z 

# r M. Shaukat

# tr 16. 

# Aug. 20t0 WL-ACP 7 

## Tel. 4 

## 61

Datum Unterschrift13 .08.2010 10 :30 : 52 Page 1 of 1



## Scan Analysis Report Repo r t T i me : Fr 1 3 Aug 1 0:30 :4 3 AM 20 1 0 B

a tch : C:\Vari an\Cary WinUV\Datal\U2 l 0 21 2l . BSW Software version : 02 . 00(25) Operator: 

### Instrument Pa r ameters I nst rument Instrument Version Start (nm) S t op (nm) X Mode Y Mode UV-Vis Scan Rate (nm/minl UV -V is Data I nte r val (nm) UV-Vis Ave . Time (sec) UV-Vis SBW (nm) Slit Height Beam Mode Signal-to-noise Mode 

### uv Source Vis Source Third Source Source Changeover (nm) Detec t or Changeov e r (nm) Baseline Correc ti on Base li ne Type B

as eline Fi l e Name Base li ne S t d Re f Fil e Name Cycle Mode Comments Sample Name: U2102121 Collect i on Ti m e Wavelength (nm) Abs 213,000 1 ,56682 Cary soo 8,01 700 , 000 200 , 000 Nanometer s Abs 300,000 0,500 0 ,100 2,000 Ful l Double Off On On Off 350,00 BOO,OO On Base l ine correction C:\Vari an\Car y W i nUV\Datal\U2102 12l.BSW Off MAFS - 092 C

harge : FS - 0 4 9 - 10- 3 FFL: AC80 SA7 : 2 0 85313 Ref.: Wasser LiChroSo l v d =lcm T=20°C C= 0,03280g/20mL 

### : A 1 

### 1.?4Q IL 11 .0 8 .2 0 1 0 11 :34:20