### Name:

Title: Company: Sign Date: Name: Title: Company: Sign Date: Permitted Facility Representative / Date Testing Company Representative / Date 

## Northport Unit 3 ICR Test Program

Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Monday, February 28, 2011 Page 1 of 52

### Northport Unit 3 ICR Test Program

Facility Information: Northport

301 Eatons Neck Road

Northport NY 11768
Contact: Paul Lynch

Phone: 516-545-2564

Fax: 516-545-2582

Email: paul.lynch@us.ngrid.com Testing Company:

AirNova Inc. 5845 Clayton Avenue

Pennsauken NJ 08109
Contact: Lenny D. Katerynczuk

Phone: 856-486-1500

Fax: 856-486-9896

Email: lenny@airnova.com

Air Permit Number:
1-4726-00130/00041 Permitted Source ID/Name:
Boiler 3 U-00003

Permitted Maximum Process Rate:
N/A Max. Normal Operation Process Rate:
N/A Target Process Test Rate
N/A

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: This source is a tangential fired external combustion boiler used for electric generation. Rated at 385 MW and can fire either #6 residual oil or natural gas. Exhaust gases from the boiler are split between two air heaters then travel through individual dual pass Buell electrostatic precipitators. From the ESP exhaust gas is passed through dual induced draft fans then enters the stack through dual breechings. Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: Enter ARS ID FRS #: Enter FRS ID

SCC / Description 10100404 External Combustion Boilers - Electric Generation - Residual Oil - Grade 6 Oil: Tangential Firing

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width

Duct near stack breaching 0 12 12 4 65.29 24 124 108

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location
% H2O Method 1 - 4 3 180 0 Duct near stack breaching Regulation Description Compound Limit Unit

0



### Monday, February 28, 2011 Page 2 of 52

### Northport Unit 3 ICR Test Program

Carbon Monoxide Method 10 3 120 0 Duct near stack breaching Formaldehyde Method 0011 3 120 0 Duct near stack breaching 2,3,7,8-TCDD Method 23 3 480 0 Duct near stack breaching 1,2,3,7,8-PeCDD Method 23 3 480 0 Duct near stack breaching OCDD Method 23 3 480 0 Duct near stack breaching 2,3,7,8-TCDF Method 23 3 480 0 Duct near stack breaching 1,2,3,7,8-PeCDF Method 23 3 480 0 Duct near stack breaching 2,3,4,7,8-PeCDF Method 23 3 480 0 Duct near stack breaching 1,2,3,4,6,7,8-HpCDF Method 23 3 480 0 Duct near stack breaching OCDF Method 23 3 480 0 Duct near stack breaching Other TCDD Method 23 3 480 0 Duct near stack breaching Other PeCDD Method 23 3 480 0 Duct near stack breaching Other HxCDD Method 23 3 480 0 Duct near stack breaching Other HpCDD Method 23 3 480 0 Duct near stack breaching Other TCDF Method 23 3 480 0 Duct near stack breaching Other PeCDF Method 23 3 480 0 Duct near stack breaching Other HxCDF Method 23 3 480 0 Duct near stack breaching Other HpCDF Method 23 3 480 0 Duct near stack breaching 3,3',4,4'-TCB (PCB77) Method 23 3 480 0 Duct near stack breaching



### Monday, February 28, 2011 Page 3 of 52

### Northport Unit 3 ICR Test Program

3,4,4',5-TCB (PCB81) Method 23 3 480 0 Duct near stack breaching 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 0 Duct near stack breaching 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 0 Duct near stack breaching 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 0 Duct near stack breaching 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 0 Duct near stack breaching 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 0 Duct near stack breaching 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 0 Duct near stack breaching 2,3',4,4',5,5'-HxCB (PCB167) Method 23 3 480 0 Duct near stack breaching 3,3',4,4',5,5'-HxCB (PCB169) Method 23 3 480 0 Duct near stack breaching 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 0 Duct near stack breaching Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Duct near stack breaching Hydrogen Fluoride Method 26A 3 180 0 Duct near stack breaching Hydrogen Chloride Method 26A 3 180 0 Duct near stack breaching Hydrogen Chloride Method 26 3 180 0 Duct near stack breaching Hydrogen Fluoride Method 26 3 180 0 Duct near stack breaching Filterable PM2.5 OTM - 27/28 3 364 0 Duct near stack breaching Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 364 0 Duct near stack breaching Organic Condensible

Particulate OTM - 27/28 3 364 0 Duct near stack breaching Total PM2.5 OTM - 27/28 3 364 0 Duct near stack breaching



### Monday, February 28, 2011 Page 4 of 52

### Northport Unit 3 ICR Test Program

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.

Filterable Particulate Method 29 3 240 0 Duct near stack breaching Antimony Method 29 3 240 0 Duct near stack breaching Manganese Method 29 3 240 0 Duct near stack breaching Cadmium Method 29 3 240 0 Duct near stack breaching Selenium Method 29 3 240 0 Duct near stack breaching Lead Method 29 3 240 0 Duct near stack breaching Chromium Method 29 3 240 0 Duct near stack breaching Arsenic Method 29 3 240 0 Duct near stack breaching Beryllium Method 29 3 240 0 Duct near stack breaching Nickel Method 29 3 240 0 Duct near stack breaching O2 Method 3A O2 3 480 0 Duct near stack breaching Co2 Method 3A CO2 3 480 0 Duct near stack breaching O2 Method 3A O2 3 120 0 Duct near stack breaching Co2 Method 3A CO2 3 120 0 Duct near stack breaching O2 Method 3A O2 3 240 0 Duct near stack breaching Co2 Method 3A CO2 3 240 0 Duct near stack breaching Filterable Particulate Method 5 3 240 0 Duct near stack breaching Sulfur Dioxide Method 6C 3 180 0 Duct near stack breaching Nitrogen oxides (NOx) Method 7E 3 180 0 Duct near stack breaching



### Monday, February 28, 2011 Page 5 of 52

### Northport Unit 3 ICR Test Program

The following describes any modifications and/or deviations to the applicable test methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.
Selection of sampling location is not in accordance with applicable methods. 3D traverses were conducted in accordance with a plan previously approved by Bill Maxwell to verify cyclonic conditions were not present in the sampling location utilized during testing.



### Monday, February 28, 2011 Page 6 of 52

### Northport Unit 3 ICR Test Program

Sampling / Stack Data Results Summary



### Location Duct near stack breaching - Method 0011 Average
Run Number NPT3 R1N NPT3 R1S NPT3 R2N

Test Date 6/12/2010 6/19/2010 6/19/2010

Run Start Time 6/19/2010 8:05:00 AM 6/19/2010

8:05:00 AM 6/19/2010 11:30:00 AM

Run Finish Time 6/19/2010 10:29:00 AM 6/19/2010

10:29:00 AM 6/19/2010 1:56:00 PM

Net Run Time, minutes 120 120 120 Dry Gas Meter Volume Sampled, dscf 90.181 100.238 88.754 93.058
Moisture Content of Stack Gas, % 7.72 8.24 7.84 7.933 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000
Carbon Dioxide, % 10.7 10.8 10 10.500 Oxygen, % 7.7 7.6 8.5 7.933 Average Stack Gas Temperature, °F 289.42 303.46 292.58 295.153 Dry Volumetric Flow Rate, dry scfm 344,252.5 392,502.9 350,318.1 362,357.833
Actual Wet Volumetric Flue Gas Flow Rate, acfm 525,803.4 614,804.4 538,023.6 559,543.800 Percent Isokinetic of Sampling Rate, % 95.9 93.5 92.8 94.067
F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000

Fw 10320 10320 10320 10,320.000

Fc 1420 1420 1420 1,420.000



### Monday, February 28, 2011 Page 7 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 0011 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Duct near stack breaching - Method 10 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, February 28, 2011 Page 8 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 10 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Duct near stack breaching - Method 23 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Monday, February 28, 2011 Page 9 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 23 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Duct near stack breaching - Method 25A Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, February 28, 2011 Page 10 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 25A 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Duct near stack breaching - Method 26A Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Monday, February 28, 2011 Page 11 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 26A 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Duct near stack breaching - Method 29 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Monday, February 28, 2011 Page 12 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 29 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Duct near stack breaching - Method 6C Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, February 28, 2011 Page 13 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 6C 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Duct near stack breaching - Method 7E Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Monday, February 28, 2011 Page 14 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 7E 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Duct near stack breaching - OTM - 27/28 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Monday, February 28, 2011 Page 15 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - OTM - 27/28 3 Average
Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Monday, February 28, 2011 Page 16 of 52

### Northport Unit 3 ICR Test Program

Emissions Summary



### Location: Duct near stack breaching - Method 0011 Compound: Formaldehyde Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0069 0.00645 0.00635 0.007 lb/mmBtuO2 2.45E-06 2.05E-06 2.44E-06 0.000
ppm 2.16E-03 1.82E-03 2.02E-03 0.002 ppm@7%O2 2.27E-03 1.90E-03 2.26E-03 0.002



### Location: Duct near stack breaching - Method 0011 3 Compound: Formaldehyde Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00635 0.00638 0.006 0.006 lb/mmBtuO2 2.14E-06 2.40E-06 2.17E-06 0.000
ppm 1.80E-03 1.97E-03 1.79E-03 0.002 ppm@7%O2 1.99E-03 2.23E-03 2.02E-03 0.002



### Location: Duct near stack breaching - Method 10 Compound: Carbon Monoxide Average
Run NPT3 R1N NPT3 R1S NPT3 R2N Elb/hr 2.01E+01 2.51E+01 1.15E+01 18.900 lb/mmBtuO2 1.53E-02 2.01E-02 8.64E-03 0.015 mg/dscm 1.54E+01 1.98E+01 8.72E+00 14.640



### Location: Duct near stack breaching - Method 10 3 Compound: Carbon Monoxide Average
Run NPT3 R2S NPT3 R3N NPT3 R3S Elb/hr 2.15E+01 1.56E+01 2.41E+01 20.400 lb/mmBtuO2 1.37E-02 1.08E-02 1.57E-02 0.013 mg/dscm 1.56E+01 1.21E+01 1.77E+01 15.133



### Location: Duct near stack breaching - Method 23 Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000001832 0.000000003765 0.000000012319 0.000 lb/mmBtuO2 2.05E-12 4.37E-13 1.32E-12 0.000 ng/dscm 2.06E-03 4.31E-04 1.33E-03 0.001 ng/dscm@7%O2 2.39E-03 5.08E-04 1.53E-03 0.001


### Compound: 1,2,3,7,8-PeCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000000214 0.00000000152 0.00000000132 0.000 lb/mmBtuO2 2.40E-13 1.77E-13 1.41E-13 0.000 ng/dscm 2.40E-04 1.74E-04 1.43E-04 0.000



### Monday, February 28, 2011 Page 17 of 52

### Northport Unit 3 ICR Test Program

ng/dscm@7%O2 2.78E-04 2.05E-04 1.64E-04 0.000


### Compound: 1,2,3,7,8-PeCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000000663 0.000000000795 0.00000000295 0.000 lb/mmBtuO2 7.44E-13 9.24E-14 3.16E-13 0.000 ng/dscm 7.44E-04 9.09E-05 3.18E-04 0.000 ng/dscm@7%O2 8.62E-04 1.07E-04 3.65E-04 0.000


### Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000279 0.00000000501 0.0000000147 0.000 lb/mmBtuO2 3.13E-12 5.82E-13 1.57E-12 0.000 ng/dscm 3.13E-03 5.73E-04 1.59E-03 0.002 ng/dscm@7%O2 3.63E-03 6.75E-04 1.83E-03 0.002


### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000065 0.0000001266 0.000000316 0.000 lb/mmBtuO2 7.29E-11 1.47E-11 3.38E-11 0.000 ng/dscm 7.30E-02 1.45E-02 3.41E-02 0.041 ng/dscm@7%O2 8.46E-02 1.71E-02 3.92E-02 0.047


### Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000209 0.000000489 0.00000119 0.000 lb/mmBtuO2 2.34E-10 5.68E-11 1.27E-10 0.000 ng/dscm 2.35E-01 5.59E-02 1.28E-01 0.140 ng/dscm@7%O2 2.72E-01 6.58E-02 1.47E-01 0.162


### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000212 0.0000000431 0.000000105 0.000 lb/mmBtuO2 2.38E-11 5.01E-12 1.12E-11 0.000 ng/dscm 2.38E-02 4.93E-03 1.13E-02 0.013 ng/dscm@7%O2 2.76E-02 5.81E-03 1.30E-02 0.015


### Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000164 0.000000036 0.0000000919 0.000 lb/mmBtuO2 1.84E-11 4.18E-12 9.83E-12 0.000 ng/dscm 1.84E-02 4.12E-03 9.92E-03 0.011 ng/dscm@7%O2 2.13E-02 4.85E-03 1.14E-02 0.013


### Compound: 2,3',4,4',5-PeCB (PCB118) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000543 0.00000143 0.0000031 0.000



### Monday, February 28, 2011 Page 18 of 52

### Northport Unit 3 ICR Test Program

lb/mmBtuO2 6.09E-10 1.66E-10 3.32E-10 0.000 ng/dscm 6.10E-01 1.64E-01 3.35E-01 0.370 ng/dscm@7%O2 7.07E-01 1.93E-01 3.85E-01 0.428


### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000237 0.0000000239 0.0000000697 0.000 lb/mmBtuO2 2.66E-11 2.78E-12 7.46E-12 0.000 ng/dscm 2.66E-02 2.73E-03 7.53E-03 0.012 ng/dscm@7%O2 3.08E-02 3.22E-03 8.65E-03 0.014


### Compound: 2,3,4,7,8-PeCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000000562 0.000000000828 0.00000000416 0.000 lb/mmBtuO2 6.30E-13 9.62E-14 4.45E-13 0.000 ng/dscm 6.31E-04 9.47E-05 4.49E-04 0.000 ng/dscm@7%O2 7.31E-04 1.12E-04 5.16E-04 0.000


### Compound: 2,3,7,8-TCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000000148 0.000000000917 0.00000000096 0.000 lb/mmBtuO2 1.66E-13 1.07E-13 1.03E-13 0.000 ng/dscm 1.66E-04 1.05E-04 1.04E-04 0.000 ng/dscm@7%O2 1.92E-04 1.24E-04 1.19E-04 0.000


### Compound: 2,3,7,8-TCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000000479 0.000000000831 0.00000000149 0.000 lb/mmBtuO2 5.37E-13 9.66E-14 1.59E-13 0.000 ng/dscm 5.38E-04 9.50E-05 1.61E-04 0.000 ng/dscm@7%O2 6.23E-04 1.12E-04 1.85E-04 0.000


### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00000000581 0.0000000026 0.00000000355 0.000 lb/mmBtuO2 6.52E-13 3.02E-13 3.80E-13 0.000 ng/dscm 6.52E-04 2.97E-04 3.83E-04 0.000 ng/dscm@7%O2 7.55E-04 3.50E-04 4.40E-04 0.001


### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000033 0.00000000468 0.0000000124 0.000 lb/mmBtuO2 3.70E-12 5.44E-13 1.33E-12 0.000 ng/dscm 3.70E-03 5.35E-04 1.34E-03 0.002 ng/dscm@7%O2 4.29E-03 6.30E-04 1.54E-03 0.002


### Compound: 3,3',4,4'-TCB (PCB77) Average



### Monday, February 28, 2011 Page 19 of 52

### Northport Unit 3 ICR Test Program

RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000515 0.0000000355 0.000000173 0.000 lb/mmBtuO2 5.78E-11 4.12E-12 1.85E-11 0.000 ng/dscm 5.78E-02 4.06E-03 1.87E-02 0.027 ng/dscm@7%O2 6.70E-02 4.78E-03 2.15E-02 0.031


### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000325 0.00000000755 0.0000000165 0.000 lb/mmBtuO2 3.65E-12 8.77E-13 1.77E-12 0.000 ng/dscm 3.65E-03 8.63E-04 1.78E-03 0.002 ng/dscm@7%O2 4.23E-03 1.02E-03 2.04E-03 0.002


### Compound: OCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000496 0.000000037 0.0000000336 0.000 lb/mmBtuO2 5.56E-12 4.30E-12 3.59E-12 0.000 ng/dscm 5.57E-03 4.23E-03 3.63E-03 0.004 ng/dscm@7%O2 6.45E-03 4.98E-03 4.17E-03 0.005


### Compound: OCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000227 0.00000000869 0.0000000121 0.000 lb/mmBtuO2 2.55E-12 1.01E-12 1.29E-12 0.000 ng/dscm 2.55E-03 9.94E-04 1.31E-03 0.002 ng/dscm@7%O2 2.95E-03 1.17E-03 1.50E-03 0.002


### Compound: Other HpCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000012 0.00000000376 0 0.000 lb/mmBtuO2 1.35E-12 4.37E-13 0.00E+00 0.000 ng/dscm 1.35E-03 4.30E-04 0.00E+00 0.001 ng/dscm@7%O2 1.56E-03 5.07E-04 0.00E+00 0.001


### Compound: Other HpCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0 0 0 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 0.00E+00 0.00E+00 0.00E+00 0.000


### Compound: Other HxCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000123 0 0 0.000 lb/mmBtuO2 1.38E-12 0.00E+00 0.00E+00 0.000 ng/dscm 1.38E-03 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 1.60E-03 0.00E+00 0.00E+00 0.001



### Monday, February 28, 2011 Page 20 of 52

### Northport Unit 3 ICR Test Program

Compound: Other HxCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000283 0.00000000111 0 0.000 lb/mmBtuO2 3.17E-12 1.29E-13 0.00E+00 0.000 ng/dscm 3.18E-03 1.27E-04 0.00E+00 0.001 ng/dscm@7%O2 3.68E-03 1.50E-04 0.00E+00 0.001


### Compound: Other PeCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000101 0 0 0.000 lb/mmBtuO2 1.13E-12 0.00E+00 0.00E+00 0.000 ng/dscm 1.13E-03 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 1.31E-03 0.00E+00 0.00E+00 0.000


### Compound: Other PeCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000603 0.00000000227 0 0.000 lb/mmBtuO2 6.76E-12 2.64E-13 0.00E+00 0.000 ng/dscm 6.77E-03 2.60E-04 0.00E+00 0.002 ng/dscm@7%O2 7.84E-03 3.06E-04 0.00E+00 0.003


### Compound: Other TCDD Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.0000000375 0.00000000822 0 0.000 lb/mmBtuO2 4.21E-12 9.55E-13 0.00E+00 0.000 ng/dscm 4.21E-03 9.40E-04 0.00E+00 0.002 ng/dscm@7%O2 4.88E-03 1.11E-03 0.00E+00 0.002


### Compound: Other TCDF Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000000156 0.00000000166 0 0.000 lb/mmBtuO2 1.75E-11 1.93E-13 0.00E+00 0.000 ng/dscm 1.75E-02 1.90E-04 0.00E+00 0.006 ng/dscm@7%O2 2.03E-02 2.24E-04 0.00E+00 0.007



### Location: Duct near stack breaching - Method 23 3 Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.000000008441 0.00000001788 0.0000000072 0.000 lb/mmBtuO2 7.85E-13 1.63E-12 6.88E-13 0.000 ng/dscm 8.90E-04 1.82E-03 7.74E-04 0.001 ng/dscm@7%O2 9.10E-04 1.89E-03 7.97E-04 0.001


### Compound: 1,2,3,7,8-PeCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000124 0.00000000166 0.00000000212 0.000



### Monday, February 28, 2011 Page 21 of 52

### Northport Unit 3 ICR Test Program

lb/mmBtuO2 1.15E-13 1.51E-13 2.02E-13 0.000 ng/dscm 1.31E-04 1.69E-04 2.28E-04 0.000 ng/dscm@7%O2 1.34E-04 1.75E-04 2.35E-04 0.000


### Compound: 1,2,3,7,8-PeCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000213 0.00000000432 0.00000000442 0.000 lb/mmBtuO2 1.98E-13 3.94E-13 4.22E-13 0.000 ng/dscm 2.25E-04 4.40E-04 4.75E-04 0.000 ng/dscm@7%O2 2.30E-04 4.56E-04 4.89E-04 0.000


### Compound: 2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000175 0.0000000159 0.0000000178 0.000 lb/mmBtuO2 1.63E-12 1.45E-12 1.70E-12 0.000 ng/dscm 1.85E-03 1.62E-03 1.91E-03 0.002 ng/dscm@7%O2 1.89E-03 1.68E-03 1.97E-03 0.002


### Compound: 2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000003756 0.0000003177 0.0000004034 0.000 lb/mmBtuO2 3.49E-11 2.90E-11 3.85E-11 0.000 ng/dscm 3.96E-02 3.24E-02 4.34E-02 0.038 ng/dscm@7%O2 4.05E-02 3.36E-02 4.47E-02 0.040


### Compound: 2,3,3',4,4'-PeCB (PCB105) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000129 0.00000141 0.00000141 0.000 lb/mmBtuO2 1.20E-10 1.29E-10 1.35E-10 0.000 ng/dscm 1.36E-01 1.44E-01 1.52E-01 0.144 ng/dscm@7%O2 1.39E-01 1.49E-01 1.57E-01 0.148


### Compound: 2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.000000126 0.000000107 0.000000131 0.000 lb/mmBtuO2 1.17E-11 9.76E-12 1.25E-11 0.000 ng/dscm 1.33E-02 1.09E-02 1.41E-02 0.013 ng/dscm@7%O2 1.36E-02 1.13E-02 1.45E-02 0.013


### Compound: 2,3,4,4',5-PeCB (PCB114) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000988 0.000000104 0.0000000948 0.000 lb/mmBtuO2 9.19E-12 9.48E-12 9.05E-12 0.000 ng/dscm 1.04E-02 1.06E-02 1.02E-02 0.010 ng/dscm@7%O2 1.06E-02 1.10E-02 1.05E-02 0.011


### Compound: 2,3',4,4',5-PeCB (PCB118) Average



### Monday, February 28, 2011 Page 22 of 52

### Northport Unit 3 ICR Test Program

RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000381 0.0000034 0.00000371 0.000 lb/mmBtuO2 3.54E-10 3.10E-10 3.54E-10 0.000 ng/dscm 4.02E-01 3.47E-01 3.99E-01 0.383 ng/dscm@7%O2 4.11E-01 3.60E-01 4.11E-01 0.394


### Compound: 2',3,4,4',5-PeCB (PCB123) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000666 0.000000101 0.000000117 0.000 lb/mmBtuO2 6.19E-12 9.21E-12 1.12E-11 0.000 ng/dscm 7.02E-03 1.03E-02 1.26E-02 0.010 ng/dscm@7%O2 7.17E-03 1.07E-02 1.30E-02 0.010


### Compound: 2,3,4,7,8-PeCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000131 0.00000000336 0.00000000182 0.000 lb/mmBtuO2 1.22E-13 3.06E-13 1.74E-13 0.000 ng/dscm 1.38E-04 3.43E-04 1.96E-04 0.000 ng/dscm@7%O2 1.41E-04 3.56E-04 2.02E-04 0.000


### Compound: 2,3,7,8-TCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000107 0.00000000118 0.00000000137 0.000 lb/mmBtuO2 9.95E-14 1.08E-13 1.31E-13 0.000 ng/dscm 1.13E-04 1.20E-04 1.47E-04 0.000 ng/dscm@7%O2 1.15E-04 1.24E-04 1.51E-04 0.000


### Compound: 2,3,7,8-TCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000106 0.00000000228 0.00000000281 0.000 lb/mmBtuO2 9.85E-14 2.08E-13 2.68E-13 0.000 ng/dscm 1.12E-04 2.32E-04 3.02E-04 0.000 ng/dscm@7%O2 1.14E-04 2.41E-04 3.11E-04 0.000


### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000304 0.00000000485 0.00000000523 0.000 lb/mmBtuO2 2.83E-13 4.42E-13 5.00E-13 0.000 ng/dscm 3.21E-04 4.94E-04 5.62E-04 0.000 ng/dscm@7%O2 3.28E-04 5.12E-04 5.79E-04 0.000


### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000682 0.0000000162 0.0000000229 0.000 lb/mmBtuO2 6.34E-13 1.48E-12 2.19E-12 0.000 ng/dscm 7.19E-04 1.65E-03 2.46E-03 0.002 ng/dscm@7%O2 7.35E-04 1.71E-03 2.53E-03 0.002



### Monday, February 28, 2011 Page 23 of 52

### Northport Unit 3 ICR Test Program

Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000708 0.000000262 0.000000351 0.000 lb/mmBtuO2 6.58E-12 2.39E-11 3.35E-11 0.000 ng/dscm 7.47E-03 2.67E-02 3.78E-02 0.024 ng/dscm@7%O2 7.63E-03 2.77E-02 3.89E-02 0.025


### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000113 0.0000000243 0.0000000191 0.000 lb/mmBtuO2 1.05E-12 2.22E-12 1.82E-12 0.000 ng/dscm 1.19E-03 2.48E-03 2.05E-03 0.002 ng/dscm@7%O2 1.22E-03 2.57E-03 2.11E-03 0.002


### Compound: OCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000459 0.0000000263 0.0000000506 0.000 lb/mmBtuO2 4.27E-12 2.40E-12 4.83E-12 0.000 ng/dscm 4.84E-03 2.68E-03 5.44E-03 0.004 ng/dscm@7%O2 4.95E-03 2.78E-03 5.60E-03 0.004


### Compound: OCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0000000108 0.00000000796 0.0000000115 0.000 lb/mmBtuO2 1.00E-12 7.26E-13 1.10E-12 0.000 ng/dscm 1.14E-03 8.11E-04 1.24E-03 0.001 ng/dscm@7%O2 1.17E-03 8.41E-04 1.28E-03 0.001


### Compound: Other HpCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000531 0.00000000802 0.00000000832 0.000 lb/mmBtuO2 4.94E-13 7.31E-13 7.95E-13 0.000 ng/dscm 5.60E-04 8.18E-04 8.95E-04 0.001 ng/dscm@7%O2 5.72E-04 8.49E-04 9.22E-04 0.001


### Compound: Other HpCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000523 0 0 0.000 lb/mmBtuO2 4.86E-13 0.00E+00 0.00E+00 0.000 ng/dscm 5.52E-04 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 5.64E-04 0.00E+00 0.00E+00 0.000


### Compound: Other HxCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0 0.00000000636 0.00000000718 0.000 lb/mmBtuO2 0.00E+00 5.80E-13 6.86E-13 0.000



### Monday, February 28, 2011 Page 24 of 52

### Northport Unit 3 ICR Test Program

ng/dscm 0.00E+00 6.48E-04 7.72E-04 0.000 ng/dscm@7%O2 0.00E+00 6.72E-04 7.95E-04 0.000


### Compound: Other HxCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000962 0.0000000214 0.00000000996 0.000 lb/mmBtuO2 8.94E-13 1.95E-12 9.51E-13 0.000 ng/dscm 1.01E-03 2.18E-03 1.07E-03 0.001 ng/dscm@7%O2 1.03E-03 2.26E-03 1.10E-03 0.001


### Compound: Other PeCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0 0.0000000032 0.0000000064 0.000 lb/mmBtuO2 0.00E+00 2.92E-13 6.11E-13 0.000 ng/dscm 0.00E+00 3.26E-04 6.88E-04 0.000 ng/dscm@7%O2 0.00E+00 3.38E-04 7.08E-04 0.000


### Compound: Other PeCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.000000013 0.0000000492 0.0000000233 0.000 lb/mmBtuO2 1.21E-12 4.49E-12 2.23E-12 0.000 ng/dscm 1.37E-03 5.02E-03 2.51E-03 0.003 ng/dscm@7%O2 1.40E-03 5.21E-03 2.58E-03 0.003


### Compound: Other TCDD Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000809 0.0000000149 0.0000000175 0.000 lb/mmBtuO2 7.52E-13 1.36E-12 1.67E-12 0.000 ng/dscm 8.53E-04 1.52E-03 1.88E-03 0.001 ng/dscm@7%O2 8.72E-04 1.58E-03 1.94E-03 0.001


### Compound: Other TCDF Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.00000000986 0.0000000656 0.0000000508 0.000 lb/mmBtuO2 9.17E-13 5.98E-12 4.85E-12 0.000 ng/dscm 1.04E-03 6.69E-03 5.46E-03 0.004 ng/dscm@7%O2 1.06E-03 6.94E-03 5.62E-03 0.005



### Location: Duct near stack breaching - Method 25A Compound: Total organic compounds (TOC) as Average
Run NPT3 R1N NPT3 R1S NPT3 R2N Elb/hr 4.73E-01 8.08E-01 4.81E-01 0.587 gr/dscf 1.60E-04 2.40E-04 1.60E-04 0.000 lb/mmBtuO2 3.33E-04 4.96E-04 3.55E-04 0.000 mg/dscm 3.67E-01 5.50E-01 3.67E-01 0.428
ppm 2.00E-01 3.00E-01 2.00E-01 0.233 ppm@7%O2 2.11E-01 3.14E-01 2.24E-01 0.250



### Monday, February 28, 2011 Page 25 of 52

### Northport Unit 3 ICR Test Program

Location: Duct near stack breaching - Method 25A 3 

### Compound: Total organic compounds (TOC) as Average
Run NPT3 R2S NPT3 R3N NPT3 R3S Elb/hr 7.94E-01 1.71E+00 4.03E+00 2.178 gr/dscf 2.40E-04 5.61E-04 1.28E-03 0.001 lb/mmBtuO2 5.23E-04 1.25E-03 2.86E-03 0.002 mg/dscm 5.50E-01 1.28E+00 2.93E+00 1.587
ppm 3.00E-01 7.00E-01 1.60E+00 0.867 ppm@7%O2 3.31E-01 7.91E-01 1.81E+00 0.977



### Location: Duct near stack breaching - Method 26A Compound: Hydrogen Chloride Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.8 0.69 1 0.830 Elb/hr 2.55E-01 2.55E-01 3.31E-01 0.280 lb/mmBtuO2 1.86E-04 2.02E-04 2.22E-04 0.000 mg/dscm 2.03E-01 2.30E-01 2.48E-01 0.227 mg/dscm@7%O2 2.15E-01 2.33E-01 2.57E-01 0.235


### Compound: Hydrogen Fluoride Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.63 0.44 0.52 0.530 Elb/hr 2.01E-01 1.62E-01 1.72E-01 0.178 lb/mmBtuO2 1.47E-04 1.29E-04 1.16E-04 0.000 mg/dscm 1.60E-01 1.47E-01 1.29E-01 0.145 mg/dscm@7%O2 1.70E-01 1.49E-01 1.34E-01 0.151



### Location: Duct near stack breaching - Method 26A 3 Compound: Hydrogen Chloride Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.84 1.14 0.79 0.923 Elb/hr 3.16E-01 3.73E-01 2.98E-01 0.329 lb/mmBtuO2 2.25E-04 2.62E-04 1.99E-04 0.000 mg/dscm 2.53E-01 2.98E-01 2.22E-01 0.258 mg/dscm@7%O2 2.60E-01 3.05E-01 2.30E-01 0.265


### Compound: Hydrogen Fluoride Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.47 0.61 0.53 0.537 Elb/hr 1.77E-01 1.99E-01 2.00E-01 0.192 lb/mmBtuO2 1.26E-04 1.40E-04 1.33E-04 0.000 mg/dscm 1.41E-01 1.59E-01 1.49E-01 0.150 mg/dscm@7%O2 1.45E-01 1.63E-01 1.55E-01 0.154



### Location: Duct near stack breaching - Method 29



### Monday, February 28, 2011 Page 26 of 52

### Northport Unit 3 ICR Test Program

Compound: Antimony Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.12776 0.14392 0.1488 0.140 Elb/hr 2.43E-02 2.67E-02 2.88E-02 0.027 lb/mmBtuO2 1.98E-05 2.18E-05 2.47E-05 0.000 mg/dscm 1.98E-02 2.15E-02 2.33E-02 0.022 mg/dscm@7%O2 2.29E-02 2.53E-02 2.87E-02 0.026


### Compound: Arsenic Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00443 0.00424 0.00441 0.004 Elb/hr 8.42E-04 7.85E-04 8.53E-04 0.001 lb/mmBtuO2 6.85E-07 6.43E-07 7.31E-07 0.000 mg/dscm 6.86E-04 6.33E-04 6.89E-04 0.001 mg/dscm@7%O2 7.95E-04 7.46E-04 8.48E-04 0.001


### Compound: Beryllium Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000275 0.000289 0.000315 0.000 Elb/hr 5.23E-05 5.35E-05 6.09E-05 0.000 lb/mmBtuO2 4.25E-08 4.38E-08 5.22E-08 0.000 mg/dscm 4.26E-05 4.32E-05 4.92E-05 0.000 mg/dscm@7%O2 4.93E-05 5.09E-05 6.05E-05 0.000


### Compound: Cadmium Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.000622 0.000484 0.000408 0.001 Elb/hr 1.18E-04 8.96E-05 7.89E-05 0.000 lb/mmBtuO2 9.62E-08 7.34E-08 6.77E-08 0.000 mg/dscm 9.63E-05 7.23E-05 6.38E-05 0.000 mg/dscm@7%O2 1.12E-04 8.52E-05 7.85E-05 0.000


### Compound: Chromium Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00757 0.01454 0.01379 0.012 Elb/hr 1.44E-03 2.69E-03 2.67E-03 0.002 lb/mmBtuO2 1.17E-06 2.21E-06 2.29E-06 0.000 mg/dscm 1.17E-03 2.17E-03 2.16E-03 0.002 mg/dscm@7%O2 1.36E-03 2.56E-03 2.66E-03 0.002


### Compound: Filterable Particulate Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 50.7 138.9 46.7 78.767 Elb/hr 9.64E+00 2.57E+01 9.03E+00 14.790 lb/mmBtuO2 7.84E-03 2.11E-02 7.74E-03 0.012 mg/dscm 7.85E+00 2.07E+01 7.30E+00 11.950 mg/dscm@7%O2 9.09E+00 2.44E+01 8.98E+00 14.157



### Monday, February 28, 2011 Page 27 of 52

### Northport Unit 3 ICR Test Program

Compound: Lead Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.01119 0.010952 0.00934 0.010 Elb/hr 2.13E-03 2.03E-03 1.81E-03 0.002 lb/mmBtuO2 1.73E-06 1.66E-06 1.55E-06 0.000 mg/dscm 1.73E-03 1.64E-03 1.46E-03 0.002 mg/dscm@7%O2 2.00E-03 1.93E-03 1.80E-03 0.002


### Compound: Manganese Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.56245 0.73546 0.6902 0.663 Elb/hr 1.07E-01 1.36E-01 1.33E-01 0.125 lb/mmBtuO2 8.70E-05 1.12E-04 1.14E-04 0.000 mg/dscm 8.71E-02 1.10E-01 1.08E-01 0.102 mg/dscm@7%O2 1.01E-01 1.30E-01 1.33E-01 0.121


### Compound: Nickel Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.76901 0.8566 0.969 0.865 Elb/hr 1.46E-01 1.59E-01 1.87E-01 0.164 lb/mmBtuO2 1.19E-04 1.30E-04 1.61E-04 0.000 mg/dscm 1.19E-01 1.28E-01 1.51E-01 0.133 mg/dscm@7%O2 1.38E-01 1.51E-01 1.86E-01 0.158


### Compound: Selenium Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 0.00658 0.00755 0.006577 0.007 Elb/hr 1.25E-03 1.40E-03 1.27E-03 0.001 lb/mmBtuO2 1.02E-06 1.15E-06 1.09E-06 0.000 mg/dscm 1.02E-03 1.13E-03 1.03E-03 0.001 mg/dscm@7%O2 1.18E-03 1.33E-03 1.27E-03 0.001



### Location: Duct near stack breaching - Method 29 3 Compound: Antimony Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.2988 0.12767 0.491784 0.306 Elb/hr 5.39E-02 2.40E-02 8.83E-02 0.055 lb/mmBtuO2 3.43E-05 1.83E-05 5.48E-05 0.000 mg/dscm 3.92E-02 1.97E-02 6.22E-02 0.040 mg/dscm@7%O2 3.98E-02 2.12E-02 6.36E-02 0.042


### Compound: Arsenic Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0083 0.00463 0.01206 0.008 Elb/hr 1.50E-03 8.72E-04 2.16E-03 0.002 lb/mmBtuO2 9.54E-07 6.63E-07 1.34E-06 0.000 mg/dscm 1.09E-03 7.13E-04 1.52E-03 0.001



### Monday, February 28, 2011 Page 28 of 52

### Northport Unit 3 ICR Test Program

mg/dscm@7%O2 1.11E-03 7.68E-04 1.55E-03 0.001


### Compound: Beryllium Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.000769 0.000311 0.00128 0.001 Elb/hr 1.39E-04 5.85E-05 2.30E-04 0.000 lb/mmBtuO2 8.84E-08 4.45E-08 1.43E-07 0.000 mg/dscm 1.01E-04 4.79E-05 1.62E-04 0.000 mg/dscm@7%O2 1.02E-04 5.16E-05 1.66E-04 0.000


### Compound: Cadmium Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.000657 0.000608 0.001095 0.001 Elb/hr 1.18E-04 1.14E-04 1.97E-04 0.000 lb/mmBtuO2 7.55E-08 8.71E-08 1.22E-07 0.000 mg/dscm 8.63E-05 9.37E-05 1.38E-04 0.000 mg/dscm@7%O2 8.76E-05 1.01E-04 1.41E-04 0.000


### Compound: Chromium Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0238 0.01028 0.015152 0.016 Elb/hr 4.29E-03 1.94E-03 2.72E-03 0.003 lb/mmBtuO2 2.74E-06 1.47E-06 1.69E-06 0.000 mg/dscm 3.13E-03 1.58E-03 1.92E-03 0.002 mg/dscm@7%O2 3.18E-03 1.70E-03 1.96E-03 0.002


### Compound: Filterable Particulate Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 212.3 85.5 333.8 210.533 Elb/hr 3.83E+01 1.61E+01 5.99E+01 38.100 lb/mmBtuO2 2.44E-02 1.22E-02 3.72E-02 0.025 mg/dscm 2.79E+01 1.32E+01 4.22E+01 27.767 mg/dscm@7%O2 2.83E+01 1.42E+01 4.31E+01 28.533


### Compound: Lead Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.0214 0.007814 0.029297 0.020 Elb/hr 3.86E-03 1.47E-03 5.26E-03 0.004 lb/mmBtuO2 2.46E-06 1.12E-06 3.26E-06 0.000 mg/dscm 2.81E-03 1.20E-03 3.70E-03 0.003 mg/dscm@7%O2 2.85E-03 1.29E-03 3.78E-03 0.003


### Compound: Manganese Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 1.5744 0.6726 2.93001 1.726 Elb/hr 2.84E-01 1.27E-01 5.26E-01 0.312 lb/mmBtuO2 1.81E-04 9.63E-05 3.27E-04 0.000 mg/dscm 2.07E-01 1.04E-01 3.70E-01 0.227



### Monday, February 28, 2011 Page 29 of 52

### Northport Unit 3 ICR Test Program

mg/dscm@7%O2 2.10E-01 1.12E-01 3.78E-01 0.233


### Compound: Nickel Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 2.022 0.8518 3.64078 2.172 Elb/hr 3.65E-01 1.60E-01 6.54E-01 0.393 lb/mmBtuO2 2.32E-04 1.22E-04 4.06E-04 0.000 mg/dscm 2.66E-01 1.31E-01 4.60E-01 0.286 mg/dscm@7%O2 2.70E-01 1.41E-01 4.70E-01 0.294


### Compound: Selenium Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 0.01003 0.00419 0.00915 0.008 Elb/hr 1.81E-03 7.89E-04 1.64E-03 0.001 lb/mmBtuO2 1.15E-06 6.00E-07 1.02E-06 0.000 mg/dscm 1.32E-03 6.46E-04 1.16E-03 0.001 mg/dscm@7%O2 1.34E-03 6.96E-04 1.19E-03 0.001



### Location: Duct near stack breaching - Method 6C Compound: Sulfur Dioxide Average
Run NPT3 R1N NPT3 R1S NPT3 R2N Elb/hr 7.82E+02 7.81E+02 9.36E+02 833.000 lb/mmBtuO2 5.71E-01 6.19E-01 6.29E-01 0.606 mg/dscm 6.24E+02 7.07E+02 7.03E+02 678.000 mg/dscm@7%O2 6.62E+02 7.17E+02 7.29E+02 702.667
ppm 2.34E+02 2.65E+02 2.64E+02 254.333 ppm@7%O2 2.48E+02 2.69E+02 2.74E+02 263.667



### Location: Duct near stack breaching - Method 6C 3 Compound: Sulfur Dioxide Average
Run NPT3 R2S NPT3 R3N NPT3 R3S Elb/hr 9.15E+02 9.09E+02 9.69E+03 3,838.000 lb/mmBtuO2 6.49E-01 6.40E-01 6.45E-01 0.645 mg/dscm 7.31E+02 7.26E+02 7.21E+02 726.000 mg/dscm@7%O2 7.53E+02 7.42E+02 7.48E+02 747.667
ppm 2.75E+02 2.73E+02 2.71E+02 273.000 ppm@7%O2 2.83E+02 2.79E+02 2.81E+02 281.000



### Location: Duct near stack breaching - Method 7E Compound: Nitrogen oxides (NOx) Average
Run NPT3 R1N NPT3 R1S NPT3 R2N Elb/hr 2.87E+02 2.16E+02 3.41E+02 281.333 lb/mmBtuO2 2.09E-01 1.71E-01 2.29E-01 0.203 mg/dscm 2.29E+02 1.95E+02 2.56E+02 226.667 mg/dscm@7%O2 2.43E+02 1.98E+02 2.66E+02 235.667
ppm 1.20E+02 1.02E+02 1.34E+02 118.667 ppm@7%O2 1.27E+02 1.03E+02 1.39E+02 123.000



### Monday, February 28, 2011 Page 30 of 52

### Northport Unit 3 ICR Test Program

Location: Duct near stack breaching - Method 7E 3 

### Compound: Nitrogen oxides (NOx) Average
Run NPT3 R2S NPT3 R3N NPT3 R3S Elb/hr 2.75E+02 2.32E+02 2.68E+02 258.333 lb/mmBtuO2 1.95E-01 1.64E-01 1.78E-01 0.179 mg/dscm 2.19E+02 1.86E+02 1.99E+02 201.333 mg/dscm@7%O2 2.25E+02 1.90E+02 2.06E+02 207.000
ppm 1.15E+02 9.71E+01 1.04E+02 105.367 ppm@7%O2 1.18E+02 9.92E+01 1.08E+02 108.400



### Location: Duct near stack breaching - OTM - 27/28 Compound: Filterable PM2.5 Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 11.9 8.6 9.4 9.967 lb/mmBtuO2 2.78E-03 1.85E-03 2.28E-03 0.002


### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 87.5 54.7 4.1 48.767 lb/mmBtuO2 2.05E-02 1.18E-02 9.93E-04 0.011


### Compound: Organic Condensible Particulate Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 5.1 5.1 93.1 34.433 lb/mmBtuO2 1.19E-03 1.10E-03 2.26E-02 0.008


### Compound: Total PM2.5 Average RunNumber NPT3 R1N NPT3 R1S NPT3 R2N Mass_mg 104.5 68.4 106.6 93.167 lb/mmBtuO2 2.44E-02 1.47E-02 2.58E-02 0.022



### Location: Duct near stack breaching - OTM - 27/28 3 Compound: Filterable PM2.5 Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 11.3 10.8 28.1 16.733 lb/mmBtuO2 2.05E-03 2.28E-03 5.32E-03 0.003


### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 43.6 53.5 63.5 53.533 lb/mmBtuO2 7.92E-03 1.13E-02 1.20E-02 0.010


### Compound: Organic Condensible Particulate Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S



### Monday, February 28, 2011 Page 31 of 52

### Northport Unit 3 ICR Test Program

Process Run Data Mass_mg 5.5 1.9 9.2 5.533 lb/mmBtuO2 9.99E-04 4.00E-04 1.74E-03 0.001


### Compound: Total PM2.5 Average RunNumber NPT3 R2S NPT3 R3N NPT3 R3S Mass_mg 60.4 66.2 100.8 75.800 lb/mmBtuO2 1.10E-02 1.40E-02 1.91E-02 0.015



### Monday, February 28, 2011 Page 32 of 52

### Northport Unit 3 ICR Test Program

Process Run Data



### Run Name Value UOM Comments Target Value
1 Heat Input 0 Million Btus 0



### 2 Heat Input 0 Million Btus 0

3 Heat Input 0 Million Btus 0

1 Average Heat Input 0 MMBtu/hr 0



### 2 Average Heat Input 0 MMBtu/hr 0

3 Average Heat Input 0 MMBtu/hr 0

1 Steam Output 0 1000 lb steam/hr 0



### 2 Steam Output 0 1000 lb steam/hr 0

3 Steam Output 0 1000 lb steam/hr 0

1 Synfuel Firing Rate 0 0



### 2 Synfuel Firing Rate 0 0

3 Synfuel Firing Rate 0 0

1 Petroleum Coke Firing Rate 0 0



### 2 Petroleum Coke Firing Rate 0 0

3 Petroleum Coke Firing Rate 0 0

1 Coal Gas Firing Rate 0 0



### 2 Coal Gas Firing Rate 0 0

3 Coal Gas Firing Rate 0 0

1 Fuel Oil Firing Rate 0 gpm 0



### 2 Fuel Oil Firing Rate 0 gpm 0

3 Fuel Oil Firing Rate 0 gpm 0

1 Flue Gas Flow Rate 0 dscfm 0



### 1 Pressure Drop Across FGD (if applicable) 0 in H20 0

1 FGD Scrubber Liquor pH 0 pH 0



### 1 FGD Scrubber Liquor Flow Rate 0 gal/min 0

1 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0

1 Flue Gas Oxygen Content 0 % 0



### 1 Flue Gas Carbon Dioxide Content 0 % 0

1 Flue Gas Moisture Content 0 % 0

1 Flue Gas Sampling Point Temperature 0 Deg F 0



### 1 Flue Gas Pressure 0 atm 0

1 Standard Pressure 0 atm 0

1 Standard Temperature 0 Deg F 0



### Monday, February 28, 2011 Page 33 of 52

### Northport Unit 3 ICR Test Program

APCD Run Data

Process Lab Run Data 1 Unit Gross Electrical Output 0 MW 0



### 1 Unit Net Electric Generation 0 MWh 0

Run Name Value UOM Comments Target Value
1 ELECTROSTATIC PRECIPITATOR 0 0

1 0 0



### 1 0 0

Run Name Value UOM Comments
1 See 4b Comments. 0



### Monday, February 28, 2011 Page 34 of 52

### Northport Unit 3 ICR Test Program

Sampling / Stack Data Results Detail



### Location Duct near stack breaching - Method 0011 Average Run Number NPT3 R1N NPT3 R1S NPT3 R2N
Test Date 6/12/2010 6/19/2010 6/19/2010 Run Start Time 6/19/2010 8:05:00 AM 6/19/2010

8:05:00 AM 6/19/2010

11:30:00 AM Run Finish Time 6/19/2010 10:29:00 AM 6/19/2010

10:29:00 AM 6/19/2010

1:56:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 120 120 120 Nozzle Diameter, inches 0.197 0.197 0.197 0.197 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.03 0.99 1.03 1.017 Barometric Pressure, inches of Mercury 30.02 30.02 30.02 30.020 Average Orifice Meter Differential, inches H2O 1.80 2.51 1.89 2.067 Dry Gas Meter Volume Sampled, cubic feet 89.410 101.911 89.764 93.695 Average Dry Gas Meter Temperature, °F 83.38 76.50 94.42 84.767 Dry Gas Meter Volume Sampled, dscf 90.181 100.238 88.754 93.058 Total Moisture Liquid collected, g 160.1 191.2 160.3 170.533 Volume of Water Vapor, standard cubic feet 7.54 9.00 7.55 8.030 Moisture Content of Stack Gas, % 7.72 8.24 7.84 7.933 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.9228 0.9176 0.9216 0.921 Carbon Dioxide, % 10.7 10.8 10 10.500 Oxygen, % 7.7 7.6 8.5 7.933 Carbon Monoxide & Nitrogen, % 81.6 81.6 81.5 81.567 Fuel Factor 1.23 1.23 1.24 Dry Molecular Weight, lb/lb-Mole 30.02 30.03 29.94 29.997 Wet Molecular weight, lb/lb-Mole 29.09 29.04 29.00 29.043 Flue Gas Static Pressure, inches of H2O 1.5 1.1 1.5 1.367 Absolute Flue Gas Pressure, inches of Mercury 30.13 30.10 30.13 30.120 Average Stack Gas Temperature, °F 289.42 303.46 292.58 295.153 Average Velocity Head, inches of H2O 2.0135453473 0279 2.695247460

96668 2.093062065

3772 2.267

Average Stack Gas Velocity, feet/second 94.23 110.18 96.42 100.277 Stack Cross-Sectional Area, square feet 93.000 93.000 93.000 93.000 Dry Volumetric Flow Rate, dry scfm 344,252.5 392,502.9 350,318.1 362,357.833 Actual Wet Volumetric Flue Gas Flow Rate, acfm 525,803.4 614,804.4 538,023.6 559,543.800 Percent Isokinetic of Sampling Rate, % 95.9 93.5 92.8 94.067 Percent Excess Air, % 55.6 54.5 65.3 58.467 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Round Duct Diameter, inches 0 0 0 Rectangular Duct Width, inches 124 124 124 Rectangular Duct Length, inches 108 108 108
Fw 10320 10320 10320 10,320.000
Fc 1420 1420 1420 1,420.000



### Monday, February 28, 2011 Page 35 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 0011 3 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 36 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 10 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 37 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 10 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 38 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 23 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 39 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 23 3 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 40 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 25A Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 41 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 25A 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 42 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 26A Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 43 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 26A 3 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 44 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 29 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 45 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 29 3 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
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### Monday, February 28, 2011 Page 46 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 6C Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 47 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 6C 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 48 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 7E Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 49 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - Method 7E 3 Average Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Monday, February 28, 2011 Page 50 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - OTM - 27/28 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 51 of 52

### Northport Unit 3 ICR Test Program

Location Duct near stack breaching - OTM - 27/28 3 Average Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Monday, February 28, 2011 Page 52 of 52