Projf d 10: 40942525 ACEMOl /I Q 772

0



# · I """ "., I
p ,....T
..

tCEMS Run N o.**CyUnderVa ~.te**  CEMS 

### n me Response R

esoo n st Runt 2
. 0 7 2.00 08:01 2.02 11
. 00 1().85 08;03 10
. 85 Run2**07** 2.00 09:3 1 2 .0 2 11.00 10. 8 5 09 : 33 10
. 87 Runl**~01** 2.00 10:21 2.02 11.00 10. 85 10 : 23 1 .0. 89 Run4 

# = 2 .00 10 : 57 2.01 11
. 00 10
. 8 5 10;5 9 10
. 86 RunS Ui1 2 .00 11 : 34 2
. 01 11.00 10
. 8 5 11 : 35 t0
. 86 Run 6**01** 2
. 00 

### 12:;12 2.02 11
. 00 10.85 l 2 :J 4 1 0. 85 Run7**~-01** 2.00 12 : 54 1
. 83 11 .00 1 0. 85 12:5 8 10
. 70 Run S UJ1 2.00 

### U : l:l 2
. 00 11.00 10
. 85 J3 :3S 10.81 Run9 Ul7 

### 2
. 00 

# ..**,, ~**  2
. 00 11
. 00 1 0
. 85 14: 1 • 1 0 , 7 8 

### Ru n l O Ul7 2.00 1 4: 52 1
. 82 11
. 00 10
. 85 1• 1 :54 1 0
. 12
. 

### Veolla Sauget Unit 3 RATA Wet 0 1 Calibtation Da1a Summary

Calibration E rror Tnt R uu l ts Cyli n dttiO etrtifit d 

## vaw. nm t C£ M R tJ p ons.t
JefOJt!S CC121944 2 .07 07:SS 2 .00 

### s pa n c as CC 18 966S 22
. 50**0? ~1**  

### 2.2.48 mid - ra N! e CCJS7679 11.00 08:00 10
. 8S

a MS C al i bration 8 i 3s a nd Dr i ft Te sts 

# .... POSt·TestCEMS Bias 

# "' 'k (

. "o f S pan} 

## nmo 

# (:.::.:::' (%of Sp•n} 

## s .

... .... Response 

# ' · '"'''""' 0
. 1$ 09 , 31 2. 02. 0
. 1 " 0 .0% 0 .0% 09 : 33 JJ 10.8 7 

### 0
. 1 " 0
. 1% 0
. 1% 10 ;2 1 2.o2 0
. 1,. 0 .0% 0. 1% 10 : 13 10.89 

### 0 .1 " 0.1% 0
. 1 $ 10 :57 2.01**.0~** 0. 0% 0.1 % 1 6!5 9 1 0. 86 

### O. OS< -O
. lSIIi 0 .0!( 11:34 2
. 01 

# c.o" 0. 0%**0. 0'~**  U : lS 1 0.86 

### 0 .0 " O .OK 

## o .cm 12. :- 12 

# J 2.02 0.1% 0. 0% 

# " · "" 12 ! 1 4 l O. S S 0.0!6 .().1?5 0 .1% r l2:5'4 

# . 1.83 •I ·0
. 8'14 -0
. 8 '36 0. 0% .12 ! S 8 .10.10 · 0
. 7 " ·0 .7 % .0
. 8%**13:~1** 2
. 00 0. 0% 0 .8% .0

. 7% 

## u:as · .lD.81 · 0 .2 " O .S% 0.0% " 1 4 : 13 2
. 00 

## o. o " 0 .0% .0. 2% 1 4 : 1 4 .l0. 78 

# • ·0
. 3%- -0.2!< 0 .0% 14:52 1.82. · 0.8%**.0. ~**  • O.l91.**4: ~**  ::1 0.12 · 3
. 2 "-
- 2
. 9 " .0.8% lS:4 8 2.0< 

### 0
. 211 

# '·""

· 3
. 2% l.S : S O ..U 0.94 

### 0
. 4" 3,6%



### B · 2 Absolute ta l E rr or Diff«ence 

# '"o f

""' • ' 2 JJ% Um it 0
. 0 7 0
. 3% O .o2 

### 0. 1 ,. 0.1 5**0.6~ ~**  ?E-S


### to • 2
. 017 UC...·CQI 1.244 C..= 

### 2
. 0l7 C..J(C..,.Co) 1
. 241 

### Co• 2
. 0 15 

### c...JIC.,..C(I) 1 .'2.42**c,~** 2
. 012 <..1«. · <.1 1. 243 C.,o; 2

. 0 13 c..I<C.-<.l '· 244 

### Co· 1.92 4 

### r:...,Jfc ...- ccJ 1
. 24:?. Co= 1.918 C'w/tc""Co) 1
. 2 44 Co• 2
. 000 C..JK

.. ·C.J U .SO**~·** 1
. 906 

### c...ttC..·CJ 1.'287 C.= 1. 927 L

--**C'~w-C'(.)l 27$** 

A - 1 4{; 

# VESO I2 600Proie« ID: 40942S Z S 1440
1ero1as**~I'IJillf.**

### mld**loi~I(Q 1**  C a l Error 

# n me I Pr
.. lestCEMS 

# .... Ru n No. ('flin d t r Vatue Ct M$ {" o f Spl!ln ) 

# ........ Rts90M4 S.O" Limlt Runt 0
. 00 -<>. 05 07:48

# 2 0
. 1" 11
. 00 10-94 08:0 ! "1 0. 9 3 0.0%**R~o~n2** 0.00 

## -o.os 09':2 7 0.03 M% 

## n .oo 10
. 9 4 09:33 1 0
. 90 ..0

. 2 W. Run3 0.00 ..0
. 05 t O:lS 0
. 04 Q.4% 11. 00 

### 1094 10 : 23 1 0
. 90 -<),2)l< Run4 0. 00 

## . o . o s 10 : $3 0
. 04 0.4)6 11 .00 10
. 94 10 : $ 9 10
. 89**-<) ~**  A.uoS 0 .00 

### · O.OS 11:3 0 0
. 04 0 .4\16 11.00 10
. 9 4 11:35 J 0. &9 -D.2 " 

## Run6 0
. 00 · 0
. 05 12:08 0.04 C
. 4" 11..00 10
. 90 12 :1 4 10 .8 9 -<) , 291**~~n** 7 

## o.oo ·O .OS 12:5 1 0
. 0 4**4~** 11 .00 10 , 94 U:SS 1 0.9 1 -<)
. 194 Run8 0
. 00 

### · O.OS 13:30 0.04 0.4" 11.00 1 0.94 13:35 1Q.89 

### -o.2'l< ..,4, I Aun9 

## o . oo · 0.05 14:0S 

### O .D4 0. <1" 11.

00 

### 10.94 14 ! 1A 1 0.SS -<)
. 3% 

### Run tO 0. 00 

### -<l
. OS 14 : 48 OD3 0 .306 11.00 10
. 94 1 4!54 10. 89 .0.2% 

### Veolia Sauget Unit 3 RATA 

### Dry 0 2 

### Ca

_ libration Data SUmmary
CMibtatloon Er r o r Te st 1\Qsuh$ Cyinder 1 0 Certified Value Tim•**52 40019ll57~** **1A** 0
. 00 0 7 : 31 CC

1 8966S 

### 22
. 50 07 : 113 CC1 57679 1 1. 00 0?: 34 C£MS Cili br iltio n Bias. mel Drift Te sts P ost-Test CfMS 

# .... Tlmo ("-of Span)**R~ l'l** **$tl** S .O!<Umit 09 : 27 0.03 0.3% 09 : 33 1 0
. 90 -<).2%**10 :~**  0
. 04 (),4% 1 fY.23 10
. 90 · 0.2 %**0: ~**  0.04 

## M" 10'.59 

### 1 0
. 89**~"** 

## => ll : jl> 0
. 04 0
. 4'!6 tt:lS 1 0 .89 · 0 .2" 

### 12:08 I 0
. 0 4 0.4 " 

# JJ 10 .89 ·0
. 2% 

# J 0 .0 4 0. 4" 1,2.:58 10
. 9 1 

### · 0
. 1% U : 30 0 .0 4 OAIJ( 13:3S' 10.89 -<).1;% 1 4:08 

## => I 0.0< 0
. 4%



### , 1 4 : 14 10.88 

### .0.3:96 1 4:48 

# l 0
. 0 3 

# I 0.3'1 1 4 :5:4 1 0.89 

### I .0

. 29(; 1 5 : 45 

# - 0
. 04 Q.4%



### -**0** 

## \ o. s6 .(),4_9$



### B-3 AMC Mt C81Etr «**CEM~.e Ol** **ff ~**  '" ol Soan) 1.0% U ml t 

## -o.os o.os 0.2% 22
. 68 0.18 0.8% 1 0
. 94 0
. 05 11.3%

Df

i f't**of ~n)**  E q , 7E-S 3.0'K.UMit

0.2% 

## c.:- 0
. 006

· 0 .2% C....!!Ctr<'o! 1
. 008 0 .0 % 

### <.:. · 0
. 034 I 

### O. O

K**Yt~ .O** **l2** 

## o.o" Ce- 0.040 I 0
. 0 % <fi JlC,· Co l L013**~** "'"0
. 039 0
. 0% C.,JiC..<ol 1..01 4



# · ·

"" ""0
. 0 37 

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. 0 1 4 0 .0% 

### c.;- 0. 0 37 0 .1%**C..~l Oll**  0 .0% Ct • 0. 038 .0
. 1%**{...,/((.~** 1
. 0 13 0
. 0% G;•0 .04 1 0 .0!<**tw/((w~** l.OtS
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### 0 .037 0
. 00> C.wfjC..,.c,.)i.Ol4**0. ~** **~"** 0 .034

· 0.1 % ('..J'fC:.rCPI l.OlS



### A·147 

# VES012601

## ~il 

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# a ... w '!; >'

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# p**~**

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# APPENDIXC Unit 3 CEMS Relative Accuracy Data

A- 14 9 

# VES012603

### Time

. stamp 

## CO DryCorr 02Wet 02Dry H20 9/S/ 13 9 : 04AM 0.00 8.89 13.46 33.97 9/5/13 9:05AM 0
. 00 8.88 13.5 1 34.19 9/5/13 9:06AM 0.00 8.62 13.12 34.13 9/5/13 9 :07 AM 0.00 8
. 14 1 2.33 34.05 9/S/13 9:08AM 0.00 8.25 12 .73 3 4.95 9/S/13 9 : 09AM 0.00 8
. 62 13 .30 35.14 9/S/13 9:10AM 0.00 8
. 44 12.89 34.62 9/5/13 9:11AM 0.00 8.42 12 .98 35.11 9/5/13 9:12AM 0.00 8
. 72 13.47 35.29 9/5/13 9:13AM 0.00 8.48 12
. 98 34.67 9/5/13 9:14AM 0
. 00 8
. 35 12 .89 l5
. 16 9/S/13 9:15AM 0
. 00 8.74 13 .48 35.27 9/5/13 9:16AM 0
. 00 8.77 13
. 32 34
. 24 9/S/13 9:17AM 0,00 8
. 74 13
. 28 34.19 9/S/13 9:18AM 0,00 8
. 95 13.65 

## 34.42 9/S/13 9:19AM 0.00 8.69 13.18 34
. 04 9/5/13 9:20AM 0
.00 8.51 13
. 00 34
. 63 9/5/13 9:21AM 0.00 8.74 13 .50 35
. 19 9/5/13 9:22AM 0.00 8.62 13.13 34.33 9/5/13 9:23 AM 0.00 8 .4 1 12.85 34.57 9/5/13 9:2 4AM 0.00 8.69 13
. 46 35.36 Average 0
. 00 8.60 13.17 34.64 Unit3 

## Run 1 09/05/13

C- 1 

### A- 1 150 

# VES01260 4**Time~Stamp** 

# I CO OryCorr 02Wet 020ry H20 

## 9/5/13 9:53AM 0.00 8.40 12 .94 35
. 03 9/5/13 9:5-4A.M 0.00 8.58 13.13 34.72 9/5/13 9:55AM 0.00 8.65 13.19 34.44 9/5/13 9:56AM 0 .00 8.63 13
. 14 34.34 9/5/13 9:57A. M 0.00 8.26 1 2 .62 34.58 9/5/13 9:58 A.M 0.00 8.83 13
. 71 35.66 9/5/13 9:59 AM 0.00 8.47 12.95 34.61 9/5/13 10 :00 AM 0
. 00 8.67 13.46 35.27 9/S/13 10:01 AM 0.00 8 .89 13.64 34.82 9/5/13 10 :0 2 AM 0.00 8.76 13.29 34.05 9/5/13 10:03 AM 0.00 9.20 13.93 34.10 9/5/13 10:04 AM 0.00 9.07 13.56 33.12 9/5/13 10:05 AM 0
. 00 8.72 13 .12 33.53 9/5/13 · 10:06 AM 0
. 00 8.46 13.00 3 4 .84 9/5/13 10:07 AM 0.00 8
. 74 

## 13
. 54 35.4 8 9/5/13 10:08 AM 0.00 8
. 63 13 .11 34.29 9/5/ 1 3 10 : 09 AM 0.00 8
. 60 13.0 9 34.24 9/5/13 1 0:10 AM 0.00 8.52 13.03 34.57 9/5/13 10:11 AM 0.00 8.76 13.50 35.03 9/5/13 10 : 12 AM 0.00 8.60 13.10 3 4 .36 9/5/13 10 :13 AM 0.00 8.43 12.89 3 4 .61 Average 0.00 8.66 1 3.23 34.56 Unit 3 Run 2 

## 09/0S/13

C·2 A-151 

# VES012605

## Tlme

_ Stamp 

# I CO OryCorr 02 Wet 020ry H20 9 / 5/13 10:30 AM 0.00 8A6 12.94 34
. 63 9/5/13 10:31 AM 0
. 00 8
. 6 1 13.31 35
. 41 9

/ 5/13 10:32 AM 0
. 00 8.54 

## 13 .16 35
. 03 9/5/13 1 0:33 AM 0
. 00 8.46 13
. 00 34.99 9/5/13 1 0:34 AM 0
. 00 8.46 13.04 

## 35
. 11 9/S /13 10:35 AM 0.00 8.70 13.38 34.96 9/5/13 1 0:36 AM 0.00 8.89 1 3..53 34.23 9/5/13 1 0:37 AM 0
. 00 8.79 13.27 33.84 9/5/13 10 :38 AM 0.00 8.63 13.18 34.55 9/5/13 10:39 AM 0.00 8.72 13
. 50 35. 3 1 9/5/13 1 0 : 40 AM 0.00 8.78 13.50 34
. 95 9

/ 5/13. 1 0:41 AM 0
. 00 8
. 65 13.25 34
. 69 9 / 5/13 10:42 AM 0
. 00 8
. 60 13.24 34
. 98 9

/ 5/13 10:43 AM 0
. 00 8.74 13.44 35
. 00 9

/ 5/13 10:44 AM 0
. 00 9
. 00 13.67 34
. 28 9/5/13 10:45 AM 0
. 00 8.87 13.34 

## 33 .5 7 9/5/13 10:46 AM 0.00 8.72 13 .2 4 34. 1 5 9/5/13 10:47 AM 0.00 8.70 13.36 34.99 9/5/13 10:48 AM 0.00 8.76 13.48 34.97 9/5/13 10:49 AM 0.00 8.59 13.15 3 4 .68 9/5/13 10:50 AM 0.00 8.54 13.15 35.08 Average 0
. 00 8.68 13.29 34.73 Unit3 Run3 09/05/13

C·3 A-151 

# VES012606

## Tlme

_ Stamp CO DryCorr 02Wet 02Dry H20 

## 9 / S / 13 11:08 AM 0
. 00 8
. 71 13. 4 1 35.16 9 / S / 13 11:09 AM 0
. 00 8
. 58 13
. 08 34
. 35 9 / 5/13 11:10 AM 0.00 8.51 13.09 34
. 85 9/5/13 11:11 AM 0
. 00 8.51 13.11 35
. 10 9/S/13 11:12 AM 0.00 8.76 13.4 1 34.73 9/5/1 3 11:13 AM 0
. 00 8.65 13.08 33
. 91 9/5/13 11:1 4 AM 0.00 8.56 13 .03 34
. 32 9/5/13 11:15 AM 0.00 8.47 13.02 3 4
. 95 9/S/13 11:16 AM 0.00 8.65 13
. 33 35.13 9/S/13 11:17 AM 0.00 8.5 1 12 .98 3 4
. 5 1 9

/ 5/13 11:18 AM 0
. 00 8.47 12.99 34
. 7 1 9/5 /1 3 11:19 AM 0
. 00 8.44 12.97 34
. 93 9 / 5 / 13 11:20 AM 0
. 00 8.60 13.18 34.84 9 / 5 / 13 11:2 1 AM 0. 00 8
. 35 12.69 34
. 29 9 / 5 /1 3 11:22 AM 0
. 00 8
. 32 12-80 34
. 95 9/S / 13 11:23 AM 0.00 8
. 29 12
. 92 35.67 9/5 /1 3 11:24 AM 0.00 8.90 13
. 85 3 5.78 9/5/ 1 3 11 : 25 AM 0
. 00 9
. 22 13.96 34
. 02 9/5/1 3 11:26 AM 0
. 00 9.11 13 .66 33
. 21 9/5/13 11:27 AM 0.00 8.71 1 3
. 13 33.58 9/5/13 11:28 AM 0.00 8.77 13. 34 34.12
Ave r age 0
. 00 8.62 13 .1 9 34.63 Unlt3 Run4 09/0S / 13

A

- 153 

# VES012607

### Ti,.,_Stamp 

## CO OryCorr 02Wet 02Dry HZO 9/5/13 11 :46 AM 0.00 8.18 12. 55 34.87 9/5/13 11:47 AM 0
. 00 8.25 U .8 0 35
. 58 9/5/13 11 :48 A M 0.00 8.38 12.96 35
. 24 9/5/13 11 :49 AM 0 .00 8.29 12.66 34.50 9/5/13 11:50 AM 0.00 8.29 12 .74 34.92 9/5/13 11 : 5 · 1 AM 0
. 00 8.30 12
. 82 35.27 9/5/13 11:52 AM 0.00 8.07 12.46 35.14 9/5/13 11:53 AM 0.00 8.23 12.83 35.78 9/5/13 11:54 AM 0.00 8.42 13.14 35.98 9/5/13 11:55 AM 0.00 8.67 1 3.47 35
. 65 9/5/13 11:56 AM 0.00 8.58 13.15 34,71 9/5/13 11:57 AM 0.00 8.57 13. 16 34.78 9/5/13 11:58 AM 0.00 8.61 13.25 34.96 9/5/13 11:59 AM 0.00 8.63 13.29 

## 35
. 04 9/5/13 U:OO PM 0.00 8 .6 6 13.34 35
. 08 9/S/13 12: 01 PM 0.00 8.74 13.47 35.11 9/5/13 12:02 PM 0.00 8.80 13
. 51 34.89 9/5/13 12 :0 3 PM 0.00 8.81 13
. 45 34.53 9/5/13 12 :04 PM 0 .00 8.67 13.22 34.42 9/5/13 12:05 PM 0.00 8.64 13 .25 34.73 9/5/13 12:06 PM 

# o.oo 8.95 13.68 34.61 Average 

## 0.00 8.51 

## 13.11 35.04 Unit 

## 3 RunS 

## 09/05/13

c-5 >.154 

# VES012608

## Time_Stamp CO DryCorr 02Wet 02Dry H20 9/S/13 12 :26 PM 0.00 8.51 12.76 33. 44 9/5/13 12: 27 PM 0
. 00 8.56 12
. . 99 34.02 9/5/13 12:28 P M 0.00 8 .57 12 .94 33.85 9/5/13 12:29 PM 0 .00 8
. 67 13.09 33.70 9/5/ 13 12 : 30 PM 0.00 8.72 13
. 23 3 4
. 12 9/5/13 12:31 PM 0
. 00 9.02 

## 13
. 71 3 4
. 28 9/5/13 12 : 3 2 PM 0
. 00 8.88 13
. 37 33.57 9/5/13 12:33 P M 0.00 8.81 13
. 29 33.72 9/5 / 1 3 12:3 4 PM 0.00 8.95 1 3
. 56 34
. 02 9/5/13 12: 35 PM 0.00 8.98 13. 50 33.5 4 9/5/ 1 3 12 :36 PM 0 .00 8
. 85 13.19 32.92 9/5/13 12:37 PM 0.00 

## 8A7 12
. 70 33.34 9/5/13 12:38 PM 0.00 8.31 12.65 34.31 9/5/13 12:39 PM 0.00 8.11 12.42 34.76 9/5/13 12:40 PM 0.00 7.93 12.25 35.22 9/5/13 12:41 P M 0.00 7.95 12
. . 4 6 36.16 9/5/13 12:42 PM 0.00 8.06 12
. 68 36.38 9/5/ 13 12:43 P M 0.00 8.23 12.78 35
. 63 9/5 /13 12:44 P M 0
. 00 8.69 13.44 35.35 9/5/13 1 2 : 45 PM 0.00 9.11 13
. 97 34.82 9/5/ 13 1 2 : 46 P M 

# o.oo 8.86 13.44 34.06 

## Average 0.00 8.58 13
. 07 34.34 Unit 3 Run 6 09/05/13

C·6 A-155 

# VES O l2609

## Time

_ Stamp CODryCorr 

## 02Wet 020!1: H20 9/

5 /13 1:08PM 0.00 8.28 12
. 63 34.53 9/5/13 1:09 PM 0.00 8.38 12
. 86 34.73 9/5/13 1:10PM 0.00 8.51 13.07 34.84 9/5/13 1:11PM 0.00 8.69 13.32 34.82 9/5/13 1:12PM 0.00 8.56 13
. 12 34.63 9/5/13 1 : 13PM 0.00 8.50 13.14 35.31 9/5/13 1:14PM 0.00 8.60 13.35 35.52 9/5/13 1 : 15PM 0.00 8.89 13.64 34.80 9/5/13 1:16PM 0.00 8
. 80 13.32 33
. 96 9/5/ 1 3 1:17PM 0
. 00 8.73 13.27 3 4
. 24 9/5/13 1:18PM 0.00 8
. 66 13.25 34
. 61 9/5 /1 3 1 : 19PM 0
. 00 8
. 59 13
. 19 34.85 9/5/13 1 :20 PM 0.00 8.00 12.23 34.59 9/5 / 13 1:21 PM 0.00 8.03 12.39 35.22 9/5/13 1:22 PM 0
. 00 8.24 

## 12.78 35.43 9/5/13 1 : 23PM 0.00 8.59 13.26 35.26 9/5/13 1:24PM 0
. 00 8.61 13 .13 34
. 4 9 9/5/13 1:25 PM 0
. 00 8.76 13A2 34.63 9/5/13 1: 26 PM 0.00 8.79 13.45 34
. 61 9/5/13 1:27 PM 0.00 8.98 13.68 34
. 39 9/5/13 1:28 PM 0.00 8.55 12.84 33.44 Average 

## 0.00 8.56 13.11 34
. 71 Unit3 Run7 09/05/13

C·7 A-156 

# VES012610

### Time Stamp 

## CO DryCorr 02Wet 02 Dry H20 

## 9/5/13 1 : 46 PM 0.00 8 .33 12.74 3 4 .63 9/5/ 13 1 :4 7 PM 0.00 8
. 62 13.20 3 4 .74 9/5/13 1 : 48PM 0.00 8.71 13.34 3 4
. 63 9/5/13 1 : 49 PM 0
. 00 9.06 13.86 3 4
. 62 9/5/ 1 3 1 :50PM 0.00 9
. 03 13.67 34.02 9/5/13 1:51P M 0.00 8.84 13.42 34
. 1 4 9/5/13 1 : 52 PM 0
. 00 8.67 13.27 34.67 9/5/13 1:53 PM 0
. 00 8.77 13.43 34.71 9/5/13 1 : 54 PM 0.00 8.94 13.55 33.9 8 9/5/13 1 : 55 PM 0 .00 8.74 13.13 33.49 9/5/13 1:56PM 0 .00 8.67 13.22 3 4
. 4 2 9/5 /13 1 : 57 PM 0
. 00 8
. 63 13
. 30 35.15 9/5 / 13 1:58 P M 0.00 8.55 13.24 35.35 9/5 / 13 1:59PM 0 .00 8.56 13 .17 3 5.01 9/5/13 2:00 PM 0.00 8. 58 1 3
. 12 34 .7 1 9/5/ 13 2:01PM 0.00 8
. 67 13.22 34 .4 3 9/5/13 2:02 PM 0.00 8 .64 13
. 17 34.39 9/5/13 2:03 PM 0.00 8.47 13.00 34
. 88 9/5/13 2 : 04 PM 0.00 8. 8 7 13
. 70 35.31 9/5/ 1 3 2:05 PM 0
. 00 8.06 12 .29 3 4.43 9/5/13 2 : 06 PM 0.00 8.50 13
. 29 35.91 Average 

## 0
. 00 8
. 66 13
. 25 34.65 Un it 3 Ru n S 

## 09/05/13

... 15 7 

# VES012611

## nme.stamp COOryCo rr OlWet 020ry H20 

## 9/5/13 2:25 PM 0.00 8.47 12
. 90 34.47 9/5/13 2:26 PM 0.00 8.64 13. 16 34..35 9/5/13 2:27 PM 0.00 8.85 13. 46 34.29 9/5/13 2:28 PM 0.00 8.61 13 .05 34.06 9/5/ 13 2: 29P M 0.00 8.55 13.04 34.35 9/5/13 2:30PM 0 .00 8.54 1 3
. 09 34.7 4 9/5/13 2 : 31 PM 0. 00 8.81 13.5 7 35.11 9/5/13 2:32 PM 0.00 8.98 13
. 70 3 4. 5 2 9/5/13 2:33 PM 0. 00 8.96 13. 62 34.19 9/5/13 2:3 4 PM 0.00 8.90 13.59 34.40 9/5/13 2:35 PM 0
. 00 9.05 13.79 34. 4 0 9/5/13 2:36 PM 0.00 9 .03 13.64 33.83 9/5/13 2 : 37 P M 0.00 8 .94 13.45 

## 33.50 9/5/13 2:38PM 0.00 8.93 13
. 4 9 33
. 85 9/5/13 2:39 PM 0.00 9.04 13.78 34
. 23 9/5/13 2:40 PM 0.00 9.03 13.66 34.00 9/5/13 2:41PM 0.00 8.68 13
. 11 33.84 9/S/13 2:42P M 0.00 8.60 13.12 34
. 42 9/5/1 3 2:43 PM 0.00 8.76 13.43 34.73 9/5 / 13 2 : 44 PM 0.00 8
. 79 13 .38 34.30 9/5/13 2:45 PM 0
. 00 8.70 13 .15 33.92 Ave ra ge 

## 0
. 00 8
. 80 13 .39 34.26 Unit 3 Run9 09/05/13

C-9 

### A- 1 58 

# VES012612

### T1me Stamp 

# I COO!:)!Co rr 

### 02Wet 0201)' H20 

## 9

/ 5 / 13 3:2 1P M 0
. 00 8
. 96 13
. 65 34 .3 0 9/5 / 13 3:22 PM 0
. 00 8
. 4 5 

## 12.73 33.57 9/5/13 3:23PM 0
. 00 8
. 30 12
. 58 33.98 9/5/13 3:24 PM 0.00 8
. 50 12 .9 7 34.47 9

/5/ 13 3:25 PM 0.00 8
. 59 13 .08 3 4 .37 9/5/13 3 :26 PM 0. 00 8.33 12
. 69 3UO 9/5/13 3:27PM 0.00 8.46 13
. 10 35.48 9/5/13 3:28PM 0.00 8.58 13.23 35.19 9/5 / 13 3: 29 P M 0.00 8.52 13.00 3 4 .50 9/5/13 3:30 PM 0.00 8.74 13.35 3 4. 58 9/5/13 3:3 1 PM 0
. 00 8.44 12 .79 33.91 9/5/13 3:32 PM 0
.00 8.55 13
. 0 2 34
. 33 9

/ 5/13 3:33 PM 0.00 8.52 12 .98 34. 3 5 9

/ 5/13 3:34 PM 0
. 00 8.37 12.76 34.42 9 / 5 / 13 3:35 PM 0 .00 8
. 57 13
. 19 35.07 9/5 / 13 3:36PM 0.00 8.40 12
. 84 34
. 60 9/5/13 3:37 PM 0.00 8
. 55 13.10 34
. 82 9/5/13 3:38 PM 0
. 00 8.55 13
. 1 2 34.76 9/5/13 3:39PM 0
.0 0 8.44 12. 90 34.49 9/5/13 3:4 0PM 0 .00 8.73 13
. 45 35
. 09 9/5 / 13 3:41P M 0.00 8.59 13.16 3 4. 73
Ave r age 

## 0
. 00 8.5 3 13.03 34.5 4
Un i t3 Run 10 09/05/13

0. 1 0 

### A-159 

# VESOJ261 3

# APPENDIXD Unit 3 Waste Fee d C haracterization Data

A- 1 60 

# VESOl2614

## H o urly Report ln<: , ioerator 3

# ~ONYX Veoli a Creat

e d 9 / S/201310 : 00 AM 

## Env®nmental Serviees Period Swt 9 / S/20 1 3 9:00 A M Sauget tttin ois 

## Period End 9 / S/2013 1 0:00 A. 'lol 

## P ag e I o f I 

# C AL C U L ATI O N S Thermodynamic BTU 12

. 8 mblu
Chlorine 35.2 lbs
L owVolalile 0

. 013 lb s Mercury 0.0001 lbs Semi Volati le 0

. 007 lbs Ash 145

. 5 lbs 

# WEIGHT S Weigh t 1264 lbs
Solids Weight 202 l bs Liquid Weight 1062 lbs Low BTU Weight 495 l bs Special Feed Weight 167 lbs High B T U Weight 399 lbs
Tank 2 Weight 0 lbs Tank 6 Weight 4 95 ibs Tank 4 Weight 

# o l bs Tank 8 Weight 0 ibs
D i re c t I n ject We i ght 399 l bs 

# MI S CELLAN EOU S Was t e Permit Ti me 0

. 99 hrs Natural Gas Flow 8084 

## cf

0 · 1 A-161 

# VES0126LS

## H o u rl y R eport**lo~ncrator** 

## 3

# ONYX Veolia Cle• l<

d 

## 9iSI20 1311 :00 AM 

## Environmental Servioes Period Start 9/S12Dill0:00 AM 

## Sau& et lllinoi.s Peri od 

## End 9/S/2013 I I :00 A M P &&e lo fl 

# C AL C ULATIONS T hennodynam ic BTU 12.9 mbtu
Chlorine 39.2 lbs
L ow Volat il e 0

. 013 lbs Mercury 0

. 0000 lbs Se mi V olatile 0. 009 l bs Ash 1 44

. 8 lbs 

# WE IG H T S Weight 12 3 7 l b s
Solids Weight 202 lbs L iquid Weigh t 1035 lbs Low BTU Weight 49 9 lbs S pe cial Feed We i g ht 183 l bs H i gh BTU Weight 352 lb s
Tank 2 Weig h t 0 l bs Tank 6 Weight 499ibs Tank 4 Weigh t 0 l bs Tank 8 We i g h t 0 l bs

D i rect I n j ect Weight 3 52 lbs 

# MISCELLANEOUS Waste Pe rm it Ti me 0

. 99 hrs Nat ural Gas F l ow 9155 cf

1\·162 

# VES012616

## H o urly R eport Incinerator 

### 3

# ~ONYX Voolia 

## <:=ted 9 15/2 013 12:00 P M 

## Environmenw Services Period Sta11 

## 9 / 51201311 : 00 AM Sau'et Illinois 

### P eriod End 

## 9 /512 013 12:00 PM Pag e I o f I 

# CALCULAT I O N S Thermo dy namic BTU 13.0 mbtu
Ch l orine 33

. 7 l bs
Low Vo la tile 0

. 264 lbs Mercury 0

. 0001 lbs Sem i Volatile 0.013 l bs Ash 126

. 1 l bs 

# W E IGH TS We i ght 1280 l bs
Solids Weight 209 l bs Liquid Weight 107 1 lbs Lo w BTU Weight 483 lbs Special Feed Weight 171 l bs High BTU Welghl 415 lbs
Tank 2 We ig h t 0 lbs Tank 6 Weig ht 188 lbs Tank 4 Weight 0 lbs Tank 8 Weight 295 lbs

D i rect I n j ect Weight 41 5 l bs 

# MIS C ELLANEOUS Waste Permit T i me 0

. 99 hrs Natura l Gas Flow 8566 cf

A

- 1 63 

# VES012617

## Hourly Report lneine r a to r 

## 3 

# 4'0NYX Vc:o l ia Cr e ate d 915 / 2 0 13 I :00 PM Envir o nm e ntal Serv i ce5 

## Per i o d Sl3rt 9 / 5

/2 013 1 2:00 P M 

## S aua et Ill ino is Period En d 9 1 5/20 13 1:00 PM P

age I o f I 

# CALCULATIONS Thermodynamic BTU 12.8 mbtu
Chlorine 35

. 6 lbs
Low Volatile 0

. 0 1 3 lbs Mercury 0.0001 lbs Semi Vo l at i le 0

. 009 lbs Ash 124.9 lbs 

# WEIGHTS Weight 1240 lbs
Soli d s Weight 213 lbs Liquid Weight 1027 l bs Low B TU Weight 250 l bs Special F eed We i ght 199 l bs H igh BTU Weight 577 lbs
Ta n k 2 We i ght 0 lbs Tank 6 Weight 0 lbs Tank 4 Weight 0 lbs Tank 8 Weight 250 lbs
Direct Inject Weight 577 lbs 

# MISCELLANEOUS Waste Permit T i me 0

. 99 hrs Natural Gas Flow 7501 cf



# VESOJ26 1 8

## H ourly Report Incinerator 3 

# 40NYX Vcolla Cr<:ated 

### 9 /S/20 13 2:00PM 

## En._iro nmtnt al Services 

## Pe riod S141t 9 / S/2013 1:00PM**Saut~tliHnois** 

## Period Eod 9 / S/2013 2:00PM 

## Page I of I 

# CAL C ULATIONS Thermodynamic BTU 13

. 0 mbtu
Ch l o rine 30

. 3 l bs
Lo w Volatile 0.695 l bs Mercury 0 .000 1 lbs Semi Vol at ile O.D18 lbs Ash 113

. 6 l bs 

# WEIGHTS Weigh t 1264 lbs
Solids Weight 213 l bs L i quid Weig h t 105 1 lb s Low BTU Weight 50 1 lbs Spec ial F e ed Weigh t 178 lb s Hig h BTU Weight 370 l bs
Tank 2 Weight 0 lbs Tan k 6 We i ght 0 l bs Tank 4 Weight 0 l bs T ank 8 Weight 501 l b s
D i rect I n ject We i ght 3 7 0 lbs 

# MISCELLANEOUS Waste Perm i t Time 0

. 99 h rs Natura l G a s Flow 7800 

## cf

0 · 6 A- 1 65 

# VES012619

## H our l y R e port 1ttcinera1or 3 

# 4 0NYX Veoli a Cr<>led 91512013 3:00 PM 

## En\l'ironmcntal Sen-ices Period Statt 9/S/2013 2:00PM 

## Sauget Illinois Period End 9/SI2013 3:00PM 

### 1'3g e 

### I o f 

### I 

# C AL C ULATION S Thermodynamic B TU 12 .9 mbtu
Chlorine 29

. 5 l bs
Low Volatile 1

. 40 3 lbs Mercury 0

. 000 1 lbs Semi Vol atil e 0

. 017 lbs Ash 112 .0 lbs 

# WEIG H TS Weight 122 6 l bs
Solids Weight 207 lbs L iquid Weight 1018 lbs Low BTU Weight 499 lbs Spec ia l Feed Weight 177 lbs High BTU Weight 342 lbs
Tank 2 We i ght 

# o l bs Tank 6 Wei gh t 

# o lbs Tank 4 Weight 0 lb s Tank 8 Weight 499 lbs
Direc t Inject Weight 342 l bs 

# MIS C ELLANEOUS Waste Permit Time 0

. 99 hr s Natura l Gas Flow 7997 cf

0- 6 A-166 

# VES012620

## H o urly R eport Incinerator 3

# ~ONYX Vcolia Qeau:d 

### 915n0 

### 1 3 4:00P M 

## l!nviron mema! Scovices Period Start 9/S/20 13 3:00P M Sau:etlllinois Period 

## End 915n0 

### 13 4:00 PM Page I ort 

# CALCULATIONS Thermodynamic BTU 12.9 mbtu
Ch lori ne 31 .6 l bs
L ow Vo l atile 1

. 1 65 lb s Mercury 0.0001 l b s Se m i Vo l atile 0

. 020 lbs As h 109

. 4 lbs 

# WE IGH TS We i gh t 1225 lbs
Solids Weight 202 l bs Liquid Weight 1022 lbs L ow B TU Weight 480 l bs Spec i al Feed Weight 1 87 lbs High BTU We igh t 353 l bs
Tank 2 We i ght 0 lbs Tank 6 Weight 0 lbs Tank 4 Weight 0 lbs Tank 8 Weight 48 0 lbs
Direct Inject We i ght 353 lbs 

# MIS CEL LANEOUS Waste Permit Time 0

. 99 hrs Natural G a s Flow 7990 c f

0·7 A · 16 7 

# VES01262 1

# APPENDIXE Reference Method EPA Protocol Gas Certifications

A- 1 68 

# VES012622

# Air Liq u ide Am erica Speci alty Ga s e s LLC 

# Pa ge I of I 

# g AIR LIOUIDE 

# ,.S_ Scott

r.
tu:tr "ltMONTrt<WY lAP'OA.T! , TX775ill'h:n: 1100 · 2
.. · lc<l1Fio. 2et"'n 041t 

# RATA CLASS
CE RT I F I CA TE OF ACCURACY: Interference Free TM 

# Multi-Compon e nt EPA Prot oco l 

# Gas MNy Ubcntoty

- PGVPVendot n A320 11 A,_LIQUG AIII(IIICAf!IPECio\LT'I'GA.SESUC IIC.rAINII)HT Pti\WV LAfiOitlf , TXTml C.tomet**~** (;(lff'OMT'C N**~,.VtQ.f.NaVO**



### :ANALYTICAL INFORMATION Gas T yp;: coz , oz.aALN ,._ _ __ __ _ __ _
CyliiiMt r Numbe r: CC119665 Cyflndtt' Pm•urr·•: 1 t.ro**PSI~**
COWOHE N T CAA80 t1 L\1 

### roc !DE: CE RTIFIED COHCeNTRA110N ( M ollt )**1~.;!** • 

### OlNOt ll**tfi1~CIW** 

## a . s t.**O~l.Atr-t**

, .. CO Mh.ll• wi'-!H,-,fncl• jlnK1111of11 8 tldltM 150 04ig ••**~cM•CIIIIt'ecl#"** IN$1d an IN R:QIJ.._., ) «E PA PfiiiiiO:II**~ ,~lltf**  IH'l



### INSTRUMENTATION OAT! L.AIT CAUMATED 

# _,.,. 010ic2t11 

### ACCURACY
...**1-** lit H- l\ Ellp. OM ! U l ,.c:CI)1t Batch 

### No : I.APOQS.O I

T RACl!MtlfTY l>it&et 111 8 '1' and \1.!11. Oitect ill ST and V5L

COMPONENT 

# .,__,. 

# -

(Z • Zeta C o t R • RofOtonot' Gat ,._Tee t Go& r-Cor ro llr!lon Coelf dont)**Se~ond** fl'ltd Ant l v t lt C al ibrt ll on Cwve



### QUALITY ASSURANCE APPROVED BY: SARAH HERBERT 

### •M;ni1J.n on fi l e) 

### E-1**CllfiC*'I'****Cd.•O.o:.t•C,;-1 ~~7&1** **on~:A=O.COOIIot•O** a:s . a!i98 1 E -. 1 Oo1.t13eQE-2: 

### o-o..ooo;a£**o<~** 

### t..o..ooooot 

### .o C<irui'IWI;cn...IWI

.. o(!d •Oil)• 

### r,.. 

# ...... ,_**c~~.,.., 8~**  a5715VH 

### c= 

### o-**~**



# hnp:/fl72.24
. 128. 1 1 f alasglrxc.arp 17?0o C"'' 40 1904&Cyi=CC I &9665 &Usr=SHOP A-169 

# 1 / 16 12013 

# VES012623

# Air Liquid e America Speci alty Gases LL C Page I of 1**AIR** 

## UQU I OE c 

# S Scott**,, _.** **~.** F A A-.IO N rPK W 'f.lAPORJE. TX 71571 Pflcltle:!00-21!&- 1421 I'M ftt
. -4'1• · .. 10 

## RATA C L ASS**Dunl mil)'i;ed** **Calibn~llnu** 

### StnndunJ 

## CE RTlFICATE OF ACCURACY: I nterference FreeT"' Multi-Compon ent E P A Protocol 

# Gas A.IMy Labcw-'OfY · PGVP Vendor 10: AnGff AlltUOUCII"\E:AtCA Sl"lCW.1YGUUU.C ttQSf'AafltNOHT JII¥:Nf LA**~1'1.** tx ln.l t Custold...lro.cYWII..I!SliK-"-"'WOA fi,.OC

... 11tl tVQ:J&aTEXDR 

# ..........,."""""'**~TX18el** 

### us**~AL** 

### YnCAliNFORMATION 

### Gas**Ty~ :**  

### C02 , 0 2, 8AlN

-- -- - -- - -
Cylnd trNumber : CC157679 Cyli nderPttUiit.......- : !&eOPSIG
C OMPONENT C' AA&Ot! OLOXlOE 

### o xvca:tf Ml'!I'II.OCitN CERnFteD CCIHUNTI'; ATION ( M olts)**~. 4'J**  t 

## u . o t CI'

. LJ..t.Ct



### FERENCE STANDARD CYUNDER NUMBER 

# -·· ......... ACCURACY"' • 1- h f/- 

### u &p. O.c.; 14l)edil)tt**B•tc:hH o:~**  TRACEA8U

. I'TY 0Lrflr.L Nl$1 llAd V I I, Oire e l »IS1**~~d** V CL

COMPOH911 

# -- 0.....,.**~ST RUMENTATION**  

# __ _.:::1**HAL** 

### YZER READINGS

QUALrrY ASSURANCE**APPRO~O** BY ; SARAH HeRBERT ('1"1111\'W"t 

### on**~le)** (,Z.Zero OAt R• Roforon ot GM 

### T•T•t Gas r= C or r$500 Coetfident) Second Trf.od A nt l ys l t C•libtation C u l'\'e

E-2 

# hup: ffl72. 24
. 128.1 1 /a lasg l rxcarpi7?D 0¢'< 040 1 905 & C y i=CC 157679 &Us r=SHO J> ,A,170 

# 1 / 1 6/2 013 

# VES012624

# RATA C LA SS D ual- A nalyzed CalibraJion Sta 11d ard
12 90**CO RE**  

### S T R EET

. TROY , M I4S083 

### Phone: 248-589 · 29150 FliX : 

### 248 · 589 · 2134 

# C ERTIFICATE O F A CC URACY: EPA P r ot oco l G as Auay Laboretoa • PGVP Vendof 10: A22012 

### A

I R UOUIDE A MERICA SPECIALTY GASES UC 1 290**COMB~ MER-~**  STREET 

### TROV, Ml 4$083

h!J 

### cen a t lon w a s pe r ot m i ecco r ing \0 

### P r oe-.clure G #l ; Se pte m be r, UlD7
. 

### Cylinder N um b er: CC12194 4 

### Cy l inder Pres s u re••• : 2000 PSIG P.O. No .: 

### 59933-71•615000**~ntl 4753436~003** 



### C

e r tiiicatlo n Date: Cus1omer ClEAN AJR 

### ENGINEEAJHG 

### DON ALLEN 500 wtS T WOOD STREET 

### PALA T INE I L 

### 60067 

## u s tandards; 

### 11S e p2012 E x p. Oat o : 12Sep2020 Botch No: TR00065750 

### COMPONE NT 

## OxvGEk CARBON 

### DIOXIDE NITROGEN C E RTlFED CONCENTRATION ! M oles) 

## 2.07 "' ACCURACY " 

## +I

· 1 '% TRACEABIUTY 

### D•rect N 1 ST and VSL Ditect NIST and VS L 

### 2.09 ,. 

### + 1

- ,. BALANCE

• ' • Do 1'10'1 use when ey{Wttr**Pfuat.~••** II Mlow t 50 psig.. •' Analytical**o:~cc:uracv** Is bn:ttd on d'l• ,. .Mtf'
. U 

### ot EPA Pro tccOI ProcaCIUnl 01.**S.~tt.mber** \$1$7.

CY LINDER NUMSER 1(024582 

### J:.02S987 

### CO N CE NT RATIO N 23
. 20 " 5.00 6 % 

### OAU LAST CAUBRA TED Z8Aug2012**1$e~20U** CA RlO N DIOX IDE

HDIA 

## ANAL VZE R READI N GS CZ•ZeroGas. R • Riferenc:eGa s l•lestGas**r•COrrel8nonCOifliC:~enU**
OXYGEN O.tet 

### 1 1 51!$)20\2 

# A••p!)!\1 • Unil: ,. 

### Z

l •0.00000 1\ 1•23.20000 T 1 •2.08000 l\2oo2),'20CQ0 Z2 •0.000 00 T2•2.0 80QO 

## u •0.00000 T3 

### = 2.08000 R.3. 23.20000 Ayg C9t!C!Qua00n : 2.068 

## M 

# n·••-70000 IU•IOO .OOOO z2
.. 0.00000**T2 ~tl** **10000** Z.3•0.00000 T3•46.7()C)OC) ft3•100.0000 A!! • Conc•:n.r<1rion: 2
. 091 ! S10«1d l r 'ad Anilllvs:is



### E -3 

### Page I of 1 Calibration Corve
Concllfttt • tlon • A +Bx 

### + Dl.2 

### + D x3 • h4 f •0. 9999'99 Con1 t W\ l s: A. •·0. 0 \31083 4 

### •· t.ooo 1o5107 

## c.o 0•0 E=O
Conoentlatioa = A+ Bx<t Cx2 +01C3+fl(<l r•O.HOSU$ Co,.-.Jtl:LS ! A 

### = Q.COCSII ,J 1 03 

### 8•0
. 041•3036 5 C • S
. Sll!..OS O•:Z.701 te l.0 7 E •O



### A

· 111 

# VES012625

# Airuas CE R T I F I CATE OF ANAL Y S I S Airgas Specialty Gases 11111 S.OU.O.AI.,...,_&r-. 

# G rad e of P rod u ct : EPA**Prot oc** **J; :O~"':'mC:.=-:23)..,.** **,.** 

# .. Pan Number. Cylinder N umber. 

## Labora tory : PGVP Number. E02N 1 99E 1 5A0406 CC 1 4436 ASG
- Los Angeles - CA 832011 -.elcgaa
. t.OM 

### Reference Number: 48-124294203-8 Cyli nder Volume: 14 4 C u. F l. Cy lin der Pressure : 2015 PS I G Valw 0\JIIe t 350 Analysi s Date: 

## Dec 16 , 201 1 Expiration Date : Dec 16, 2014 CtrtfiQIIIbn**PMO~mt>d** In aooo rdanc& wtl\ •EPA**rac;aa ~ry**  P'rrAOOOI 

### ($4ol

. 1 9'37 }' 

### uti!'!) lie MMY pooeo.."e$1$ted, Anl l' j\lca l**~** dG$1 

### not rtq.Jif e con 9CC!on fOI**~ietl .**  Thi s cylnder Nt**••*~** 8IW)1ieal 

### tn::ectmcJ ae 5tattd belo w 

# wr "**a~** lt'f'OI**~** 95 %. Thole ••• no $igt'lieant _..... -.'h!c:t\ atlect NUN "'.,._ <*118Skn modln. AI OOIICOJ6a lio! iS ate on**a~** bniS 

# ""*" CllhtrMM ..,..,_ Do Not U..l
..**~billow** 150 pete 

### le. 1 Woog:a 

### P** 

## ANALYTICAL RESULTS Compone n t Requ

.. ted Ac t ual Proto co l Toll I Ro l t!IV I Conconlrollon ConCM"ttr ation


### . Method Uncortalnty CAR80H 

### MOHOXIOE 

### 90
. 00Pft,l 89.80Pft,l Gt + J-1 % NlS TT -o 

### NllRO<l E N 

### Balanc.e 

# . CAIJBRATJON STANDARDS T

y pe ko t I D Cy11ncler 

### No Concent r atio n Expiration Date 

### NlRM 

### 090605 CC2Wa9 

### 9U11P PM CARBON MOHOXIOE/NITROClEN**Fo~OI ,20** **3** 

## ANALYTICAL E QUIPMENT lns lwmenU M a kellllodel A nolytlcal Principle 

### kosi M u lt ipoint Colillralion N i eoi<M 0700 AHR080 1 5S1 CO 

### FTIR 

# . 0EtC08, 

### 201, 

### Tr

i ad D olo AY1111able 

### Upon Roqu•sl Not es :

## r.~' 1/ 

### App roved for Re l eas e

E-4 A-172 

# VES012626

# Air Liq u ide America Sp ecia l ty Gases LL C 

# {S'' Scott**~~··**

1 1oU6fAI R : fl t

OH T**f'KWY ,LA** **P~TE.** TX77$11**f'h:ln9 800o248-14~7** **e:oc:** Ul t -41<!-$419 

# RATA C LASS Dunt.Amtly .,e

d 

### C.a libnulon Sumd« l'd 

# CERTIFICATE OF ACCURACY: EPA Prot oco l Gas Assay t..a.bo ra to ry • PGVP V endo r I D ; A32011 AIR L IQUfPE N. U :!IU:';A SP£CII\1.TYGAS E S U C 11426fA!Rt iONT A<.VN LAPO R TE, TX7757 1 

## P
. o. No. : sr<X:K**Ooc~fM!'it~ 4375** **00 1**  Fdioii : IJRS012



### !AN ALYTICAL INFORMATION Gas Type : NONE

Cy lil n de r Numbe r. CC215149 Cylinde r Pt Ht u re_. : 20XIPSIG**C.-rtifl~tion** Date : 1 8tfuV2.011 CUstomer URS CO RP ORA.llQK 9400 "*''BtRGlEN Bl VO A.V$T i tf l X 7Bf29 

## us

Exp , D• · : 16N1!'1201!f Ba tch No: l.APOQ$2I.Sl
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## Page I of I

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### +1 - i\: Direct. Jlt S 1'**.:~ nd**  VSL N 't 1 li.O GtW a.Jt...LA!4::r.



### \ REFERENCE STANDARD TYPEI SRM NO
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### CVUNOER N U M BER I<NJ.M).$ 1 1{1 

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### @.:! AL VZER READINGS DATE LAST CAUBAATEO 2 00U20 1 l

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### T=Test Gas 

### r =CCttetalloo Coeffic i e n t) Second 

### Tria d**An:~ly$1 $**  

### Calibration Cu:rve Fin t T riod Ana ly, 1s CARBON MONOXJDE**O&flel ~l1** **R:eapt~~~'Cie** 1Mt: PPI<1**:1 ~~** **011763 Rl** **"' \24~719** **11 =4&.14483:**  RZ=-1Zoi6.806Z2 • 0.06757**67'21 t~M** **46.MI08** IU'- 1 24Ug2 Avg , C0flQerol l liiM : 4fi.25 PP M Ollie:**9~W2011** Rl::lflO I "I$1:1kiil:ffM Z1 :.0.0149 7 R 1 -..:6 , 5e4$4 H=46
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# h

up:/ / 172.2 4. 128
. 1 1 / al asgl rxcarp 1 7 ?Doc= 040 1179&Cy i= CC21 574 9 &Usr=SHOP A-1 73 

# 1/28/20 1 3 

# VES012627

# Performance Sp ec if i c a tion Test Result s for th e CO a nd W e t 

# 0 2 CEMS for Rot a ry Kiln In c inerator Unit 4

Prepared for: Veo ll a ES Te c hnical So l utio n s, L

. LC

. 7 M ob il e Avenue Sa u get, IL 6 2 2 0 1

P r epare d by : URS Corpo r ation 9400 Amberg l en Bouleva rd (78729) P

. 

# 0. Box 20 1 088 A us t i n , Texas 7872 0 - 10 88

Septe m ber 2013

J\.1 74 

# VES012628

# T ab l e o f Co nt e n ts Page 1.0 l ntrod u ction
....... . .. . ... . ..... . ......... . ........... . ... .• .. . ....... - .. - .................................. ..... ....... ...... 1

- 1 

# 2.0 Su mmary 

## o fR es ul t$

..... . . .. .. .. . . ... . ..................... . .. . ..... .. - .................. . ........ ......... . . .. . ..... .. .. 

# 2-1 2.1 Relativ e Accuracy
. . ........ . ......... ........................ .... .... . ... .. ...... . .. . ... ............... .. ........ 

# 2-2 3
. 0 T est Pro tocol
........ . ..... .. . ..... ... ....... ........... ... .. . ... . ........... ... ..... . ............ ... ... ... ......... .. .......... J

- 1 3.1 RelativeAccurac y .. ................ ........ .... .. .. .... . . ... .. .. . ....... . ..................................... .. . 

## 3

- l 4.0 

## Q u ality 

## Assurance
..... .. .. ..... . .. . ... .......... -···· ·················-·· -· ·· ···-·· ····-······· · ···· ···· ··· ·· ········ · 4- 1 

## APPENDIX A - R elati ve Accuracy Spreadsheet and Reference Method Dalll APPENDIX B

- Re fere n ce Method Calibration ResultS AP P ENDIX C

- Uni t 4 CE M S Relative Accuracy Data AP P EN DI X D

- U n it 4 Waste Feed Characterizatio n Data A PP END IX E

- Reference M ethod EPA P ro t oco l Gas Certifica t io n s

Un it 4CE MSRATA 

# iii Veo l io Sougc l 409 4 2525 A· 175 

# VES012629

# li s t o f Tables Pa !Je 1 -1 Gene ral Facility and Testing lofonnation
.. .......... . .. . . . . ...... .... . .. . ................................... .. .. 1

- 2 1 -2 

# CEM S I dentifica t ion
...... . ... . ...... ...... ..... ..... ........ . ........... .... ........ . ...................................... 1

- 2 2- 1 P ST Requirements and Acceptance Cri teria
........................................... .... .. ...... ... ..... .... . 2

- 1 2-2 CO CEMS Rel ative Accuracy Test Resu l ts .. .. . ............................. . . .. .. ............................. 2

- 3 2-3 Wet 0 2 

# CEMS Relative Accuracy Test Results
.... .. .......... . ............................. ....... .. ....... 2-4 3- 1 Oxygen Correction of Referen ce M et hod C O Concentration Results
......................... . ... 3-4

Unil4 CE MS RATA 

## iv Veolio Sauge t 40942525 A - 176 

# VES012630

# 1 . 0 I ntroduct io n Veolia ES Technical Solut io n s, L
. L .C. (Veo lia ) operates three incinerato rs a t its Sauget , Illinois facility. Two of the in c iner ators are fixed hearth uni ts (U n its 2 and 3), a n d th e th ird incinera to r is a rotary k iln unit (Unit 

## 4)
. All of the incinera to rs tr eat certa i n waste s t h a t nre c l

assified as hazardous u nder staLe 

## a n d/o r federal regu l ations, and are subject t o the Na t io n a l Emissio n Standards for Hazardous Air Pollut ants (NES HAP s) for Hazardo us Waste Com bustors (Tit l e 40 of the 

## Code of Feder a l Regulat i o ns , Part 63 [40 CF R Part 63 ) , Subpa rt 

# EEE), (i.e., th e 

# HWC MA CT). Unit 

# 4 is equipped with a co nt inuous e mi ssio n monitoring 

## syS1e m (CEMS) that consists of an oxygen 

## (0 

## 2 ) m oni tor and 

## a crubon mo noxid e (CO) monitor whicb are used to monitor tbe emis sions from the stack. The CEMS underwent Relative Accuracy 

## (RA) Testing. Th is repo rt presents the RA test results for the Unit 

## 4 CO and wet 

## 02 CEMS. 

## The gene ra l informatio n rega r ding 

## the testing at this faciliry i s summarized in Tab l e 

## 1-1. The RA acceptance crit e ri a 

# are s h own in Table 

## 2 - I. TheRA test of the Unit4 CE M S was comp l e t ed 

# in Sep t em ber of20 1 3, a s the i nit ia l step i n t h e 2013 Comprehen s ive Perfonmmc e Tes t 

# of U nit 

## 4. The CEMS were audited ac co rding to th e RA pr ocedures detailed in 40 CFR 60, Appendix B, Perfo rmance Spec i ficat i on 4B, 

# "Sp ec ifi ca tions and Test Proc edu r es

for Carbo n M o n ox id e and Ox yge n Continu o u s M o

nitoring Syste m s in Stati o na•y Sour ces" a nd 40 CF R 63 Subpart EEE , 

# "National E mi ssion S tand ards for Hazu•·dous Air Pollutants from Hazardous Waste Comb u stors . " The CE M S 

# m e t all th e 

# RA cri t eria out l ined in the**abo v~** **ite d**  

## references. Section 2.0 presents 

## a det a il ed s umma ry of 

## these test resu lt s. Supporting documentati on is located in 

## the appendices. The analyzer identification numbers and serial numbers for the monitors are presented below in Table 1- 2
. Veo l ia opernr cs a CO ana l yzer , an 0 2 

## analyzer , and a moisture analyzer. The oxygen correction of th e p l ant CO co n ce ntration s i s performed using a dry basis oxygen, derived from the m easured wet bas i s oxyge n concentratio n and th e measured p ercen t m o i s tur e . Th e E''Ochem MC3 i nfrared CO an a ly ze r i s designed u si ng a single sample ce ll equipped with an individua l detector syste m for eac h o r two measureme nt ranges (0-200 p pmv a n d 0

- 3,000 ppmv). The 0 2 

## a n alyzer is a COSA e l ec t r oc h e mical ana l yzer. Responses rrom each CE M S are recorded by t he Co ntrol System (CS). Data prin to u ts from these m o nit ors do cume n ti n g the CE MS performance are presented in Appendix C of this report. Characterization of was t e f ed d uri ng the RA TA testing i s included 

## in Appendix D
.

Un i t 4 CE MS RATA 

## 1-1 Veo l io So u 

## get 4094 252 5 A ·1 77 

# VESOl2631

## Table 1-1

. General F acili ty and Testing Informat ion Unit 4 CEMS Perform ance Specification Testing faci l it y Name Ve<>lia ES Te<:hnical So luti ons, L. L
. C
. Con t ac t Person 

## Dav i d Kl ar ich Telepho n e N u

m

b e r 6 1 R

- 271 -2 8 0 4 , xl20 

## Facility Ad d ress #7 Mobi le Avenue Sauget, IL 

## 6220 1 Types of P rocess S ampl e d R o t

ary Ki l n Inc inerator Exhau st 

## Ga s Person R esponsib le for Conduct i ng Te SI M iclmel Fuchs Telephone Number 

# s 12-454-4797 Company Name U RS Corporation Addr<ss 9 4 00 Ambctglen Boulevard Awt in. Texas 7 8729**~n(s)** 

## Con d ucting T ests Jesse Rocha Mcggc n D elollis M

egan Bowien Noah Pre scott 

## T

es t Met h

od s Performed E PA Method3A a od EPA Me t hod 1 0 Date ofTe<ti n g Sep t e m

ber 4, 

## 2013


## Table 1-2

. CEMS I dentificat ion Unit 4 CEMS Performance Spec i fication Testing
Paramt:t . e. r 

## J\la•uf1 . e t

urer 

## Ran ge AnalyurTa; Carbon Monoxide 

## EA:ochem MC 3 0-200ppmv A T-5 56£ 0-J.OOO ppm• • Oxygen (Wet) COSA Q-25% 

## AT

- 560B

Uni t4 CE MS 

## RATA 

# l -2 ADal) ' t<r Sulal N umber 

## 10

7 A2H6S94 T

Vcolia So u get 

## 4094 2525 A · 118 

# VES012632

# 2 . 0 S u mmary o f R esu lt s Detailed results are presented in this section. Sec t ion 2 .1 detail s the resu l ts 

## (rom the relative accuracy (RA) tests . 

## AU t est resu l ts were w it hin t h e acceptance criteria 

# as stated in the 

## RA portion of 

## 4 0 CFR 

## 60, Appendix 

## B, Perfonnance Specification 

## 48, 

# "SpecijiCIJtions and Test Procedrll'esfor Ca rbon Monoxide and Oxygen Cominuous Monitoring Systems in 

# Stationary Sources." These c riteria are shown below 

## in Table 2- 1
. 

## AU calculations are done with unrounded values, and therefore, it may not 

# be possible to reproduce a calculated value exactly from the data shown in a table. T able 2·1

. PST Requ ire ments and A cceptance Criteria Unit 

## 4 CE M S P erformance Specification Testing CO Monitor 

## P

aram e ters Low Ronee 

# I Hie)J R•n ge**(~·200** 

### p pm• · ) 

## ( 0-3 , 000 p pm v) 

## 1 0 % ofrbe overage Reference Method (RM) val ue Relative Accuracy (RA) · or 

## S

% of 

## the applicab l e standard 

## ( S ppmv 

## CO correeled to 

## 7% 0 2> 

# o, Monitor Ronge (0

- 25%)



## 1.0" /. 

# o,

U ni t 4 CEMS RAT A 

## 2-1 Veol i a Sauget 4094 2525 Ar179 

# VES012633

## 2 .1 Re l a tive Ac cu r acy 

# Relative accuracy (RA) testing was performed by URS pcrsotmel on September 4. 2013. The relative accuracy test results are presented in Tables 2-2 and 2-3. RA te sting co mpare s the plant CEMS measurement of CO (corrected to 7% oxyge n) and 

# O z (o n a wet basis) to th e Reference Method (R M ) measured u sing EP A Method 1 0 for CO and EPA Method 3A for 

# 0 2. Re la tive accuracy for t he CO CEMS is calculated by adding the confidence coelllcient to the abso lute average d iffer ence between plant averages and the RM averages . Relativ e accuracy for the 

# 02 CEMS is equivaleot to the a bsolu t e average difference between plant averages and the RM averages. The acceptance criterion is the greater of either I 0% of the average RM or 5% of t he applicable stand ard (5 ppmv CO corrected to 7% oxygen for the CO CEMS and 1.0"/o 

# 02 for the wet 

# 02 CEMS). All CEMS met the prescribed performance criteria. Hard copies !Tom the RM monitoring sySTem along with hard 

# copies of the relative accuracy calculation spreadsheet can be found in Appendix A. 

# Hard copies oftbe Veolia Unit 4 CEMS data are p r esented i n Appendix C
.

Un it 4 CE MS RATA 

# 2-2 Veotin Sauget 40942525 A-180 

# VES012634

### R•n N umb er


### I 

## 2 3 4 

## 5 6 7 8 9 1 0

Un it4 GE MS RAT A 

## Table 2-2. CO CEMS Relative Accuracy Test Resu l ts Unit 

## 4 CEMS Performance Specification Test ing Reference Motbo<I(RM) U nit 4 CEMS D•t e R unThm ! 

### CEMS 

### (ppmv CO , 

## (PPnt' ' CO , corretted tn 

### co rr ccttd to 

## 7 % 0,)

7 % 0,) 9

/ 4 1 20 1 3 09 : 05.()9: 2 6 0.95 0,07 9/

4120 1 3 09:5 4

- 1 0: I S 

## 1.1 4 0
. 1 0 9

/ 4 1201 3 10 :29

- 10 : 5 0 0
. 75 0
. 08 914/2 013 1 1 : 00- 1 1 : 21 0 .3 0 0
. 11 9

/ 4!2013 11 : 3 1

- 1 1 : 52 0.60 0. 13 9 / 4!2 01 3 12:03- 1 2:2 4 1. 02 0 , 10 9

/ 412013 12:36-12 : 57 0. 6 7 0
. 09 9

/ 4 1

2013 1 3:1>9-13 : 30 0.30 0
. 23 9 1

4 1

2013 1 3: 4 3

- 1 4 :

04 0 .3 1 0.07 9

/ 4

/2 0 1 3 1 4 : 17

- 1 4 :38 0.60 0
. 34 Abso l ute Avera&t D ll'fcreoce S ta n d>rd D e• 1 n t lon Co nfi clence Coofficlcnl (C C) Relative Accuracy (ppm• • C O ) Arlt ho ne tlc Dlfforon« 

### ( I

I III DV C O )



## .() ,88



## - 1.04 -0.67 419 -0
.

4 7 -0.92 -0
. 5 8 -0,07 -0
. 2 4

· 0 .2 6 0
. 4 7 0
. 3 1 0
. 2 4 0 .7



## 2 -3 Veolin S o ugcl 

## 4 094252 5 A- 181 

# VES012635

### Run 

### Number
I 

## 2 3 4 5 

## 6 7 

## 8 9 1 0 

## Tab le 2·3. W et 

## 0 2 

## CEMS Relative Accuracy Test Results Un i t 4 CE M S Performance Specification Testing Referen<e Do t e Run 

## nm e M<thod (RM) 

## Unl t4 CE M S CEMS (•fo Q,, 

### Wt l ) 

### (% 

## 0 1 , 

### wet) 

## 9 / 4/20 1 3 09 :05 ..()9 :26 8.88 

## 8. 5 8 9 / 412013 0 9:5 4 · 1 0: I 5 9.16 8
. 94 9 1

4 1

20ll 1 0 :29- 10 :5 0 8.84 8
. 70 9

/41 201 3 11:00·11:2 1 

## 9
. 44 9
. 1 5 9 1

4 120 13 1 1 :3 1

- 11:52 

## 927 9 .0 3 9/4f2013 12 : 03- 1 2 : 2 4 

## 929 9
. 04 914120 1 3 12:36-12 : 57 9. 43 8. 8 9 9/412013 13 : 09- 1 3 : 30 9.0 2 8.70 

## 9/

4 12 013 13: 4 3-1 4 : 04 9. 1 5 

## 8
. 9 6 9

/ 4 12013 1 4 :17- 1 4 :38 8
. 97 8 .7 5 Absolute Average Dlffer ente Standard Deviation F tehlfll'eAcc ura cy ( 0 /• 

### 0:, Wft**a~l,.)** 

### Arit.hmdit 

## Dlrf eneace ('

lo 

## 0 1 , 

### wet )



## · 0.30 

## .0.22 -0
. 14

- 0 .29 .().2 4 .{1 , 25 

## -0.54 -0.32 .0.19 

## -0.22 0 .2 4 0.06 0 .2 4

U

ni l4 CEMS RAT A 

## 2 -4 Ve o l io S ougc r 40942525 A-182 

# VES012636

# 3.0 T est Protocol The carbon monoxide and oxygen moni t ors located at the Veolia U ni t 4 l ocation were aud i t ed according to the 

## Relative Accuracy procedures outlined in 

# 40 CFR 60, Append i x 

# B, Performance Specification 

# 4B , "Specij)carlons and Test Procedures for Carbon Monoxid e and Oxygen Conti nuous MoniWTing Sy s tem s in Stationary Sources" and 

# 40 CPR 6.1 Subpart 

# BEE, "National Emission Standards j'01· 

# Hazard ous Air Pollutants ji-om Hazard<Jus Waste Co mbustors. · • 3.1 Re lative Accuracy URS monitored the emission gas CO and 0 2 

## concentrations from the Unit 4 E.'t.haust Stac k location using mobile continuou s emissio n monitors. A stainl ess-steel probe was inserted in to the stack and used to collect sample gas. A heated TeOon sample line transported sample gas from the probe to the 

## URS monito rs l ocated at ground level. The analyzers were k ep t at a constant temperatu re inside the mobile l nbomtory
. For eacb run, sample gas was collected over 21-min ute t est periods. Tiuee traverse points across the Uni t4 Exhaust Stack int erior diameter were selected accord in g to tbe procedure outlined in 40 CFR 60, Appendix B, P erformance Specification 2 , Section 8
. 1 .3.2, and s ample gas was extracted at each of three paints for seven minu tes d uri ng the test period. The samp ling l ocation met PS 2 cri teria by being greater than 2 stack interior diamet ers down stream from the nearest disturbance and greater than 0.5 stac k interior diame-ters upstream of the stac k exhaust orifice. At the mobile laboratory , the stac k gas i s split between the wet and dry analyzers. The portion of the sample gas that is 

## not sent directly to the wet 

# 0 2 

## analyzer is routed to a condenser and then transported 

## to the 

## dry 0 2 

## and dry CO analyzers for analysis
. CO analyses were performed in accordance with EPA Met hod 

# 1 0. 0 2 

## analyses were perfonned in accordance with EPA Me th o d 3A. URS used a Thenno Modei48C CO analyzer t o measure the CO concentrat io n according t o EPA Method 

# 10
. Thi s analyzer is a gas lilter correlation (GFC) analyzer. The analyze r measures CO by compar ing i nf ra r ed**ab.~orption** 

## of a reference concentration to the absorption of the samp l e. The Thermo Mode i4 8 C CO measurements are not affected by carbon dioxide. For this reason , the C0 2 

## in terference trap was not incorporated into the extraction syste m. The exclus ion of the C0 2 

## interference trap eliminates th e need to correct sample concentrnt i on, improving the accuracy ofthe analyses
. URS bas demonstrated through in-house te sting that C0 2 

## i s not an interferant at typical combustion C0 2 

## concentration levels by introducing 20% 

# col calibratio n standards to a calibrated Tllenno 48. The instrument's response to this gas was l ess than 2 ppmv (I% 

## of scale)
.

Un i t 4 CEMS RATA 

## 3-1 Veo l ia Stmgct 40942525 A-183 

# VES012637

## URS measured both dry 

## and wet oxygen concentrations for the duration of the Unit 4 RA test. From these rwo measurements , URS was 

## able to calculare the moistu re percentage and then use the percent moisture t o convert the RM wet oxygen concentrations from each 

# nm to dry**bas~s .**  

## The oxyge n corrections of RM CO concentratio ns were calcula t ed using this dry basis oxygen. Tab l e 

# 3-1 prese n t s the concentrat i on data for the steps of th i s calculat i on for 

# a ll runs. Dry oxygen was measured using 

# a Servomex Series 

# 1440 02 analyzer. This analyzer measures 

# 0 2 

## on the basis of its paramagnetic properties
. We t oxygen was measured u sing an Amctek RM CEM 0 2 

## / IQ 

## analyzer. Thi s analyzer measures 0 2 

## on a we t basis using 

# a zirconium oxide sensor. The analyzers ' 

## e.Jectroni c output s ignals were converted to a digital format a nd stored by 

# a computerized data acquisition system. The system translated tlris 

## digital signal into the proper units of measurement (ppmv CO,% 0 2) 

## and stored them on a 

## bard disk. The system stored the data 

# as ten-seco n d averages. The analyzers were calibrated prior to initiating testing using appmpriatcly certified s tandards a s 

## spec i fied by EPA Met h ods 10 

## and 3A. 

## Both of thes e me t hods reference procedures specified in EPA Method 7 E for calibration, standa rdizat i on, calc u lation, and data m1aJ ysis
. The 

# UR.S sys tem response was then checked. The total sys t em, wh i ch inc l uded the probe , sa mp l e line, sample pump, and water tra p, was incorporated into the sys te m resp onse. A 

## system response time t est was performed and documented for each instrument. Th e system drill was calculated using the pre- and post-test Syste m responses. These checks ensured that the system remained within the tolerance level defined by the above EPA methods
. A 

## sampling system calibration bias correction was applied to all RM CO 

## and 0 2 

## data measured during each test run 

## by using equation EPA Method 7E-5:

Wltere : Cg.., 

# C,.-g 

# c

.. c_ c. =
= 

## =

=
= 

## Effiueot gas co nc entra tion , dry basis, percent or ppmv; Average gas concentration indicated 

# by analyzer, dr y basis
. percent o r ppmv; Average of initial and final system calibration b ias check responses for the upscale calibration gas, percent or ppmv; Actual concentration of the upscale calibration 

# gas. percent orppmv: and Average of initial and final sys tem calibration bias chec k respon ses for the 

## zero calibration gas. percent or ppmv.

U

nil 4 CEMS RATA 

# 3-2 Veolia Sauget 40942525 A-184 

# VES012638

## The data from each 21

- minute test period was averaged for each of the RA runs. Thi s averaged data was tabulated as shown in Tables 2

- 2 and 2-3. The arithme t ic differences between tbe URS reference method (RM) result s fo r the analyte gas concentrations 

# and the Unit 

# 4 CEMS result' fo r the analyte gas co n centratiOM are u l so tabulated the r e. Carbon monoxide results for both the RM an d t he Unit 4 CEMS were corrected to 7% oxygen be fore calculat i ng ar i thmetic ditlerences
. The absolute average d iffe renc e . stw1dard**de,~atio n**  

## (Sd) and confidence coefficient (CC) of the arithm et ic differences were ca l cu l ated using the equations described in 40 CFR 60, Appendix B , PS 2 , Section 12
. At l east nine 

# runs must 

# be used to detem1ioe relative accuracy. Ten runs were performed durin g the September 4 , 2013 RA testing. TheRA p roced ure s al l ow, at the tester's discretion, for up 

## to three t ests to 

# be rejected from the calculations to determine average difference and standard d evia ti on . After rejecting one unwanted run. the confidence coefficie nt (CC) was calculated according t o the following equation:

Where: 

# cc . , • . 

# ,,x**s~** ">/II



## tn.m 

## = 

## 97
. 5% S t uden t- t variable (2.306 for nine runs); and 11 

## = 

## Number 

# of tests 

# u se d (mus t 

# be<: 9). Relati ve accuracy for the Unit4 

# CO CEMS 

# was calculated in ppm v 

# CO according t o 40 CFR 60, Appendix B, PS 4A,**Sec~** 

## ion 13.2, by adding together the absolute value of the average difference 

# between the RM 

## and Unit 4 

## CEMS and the confidence coefficient applicable to nine te :,'l 

# runs. Re l ative accurac y for th e Unit 4 

# 0 2 

## CEMS 

# was calculated 

# in% 02 according to 40 C FR 

# 60, Appendix 

# B, PS 

# 3, Section 1 2
.

0, and was 

## eq u iva len t to the absol u te average difference between the RM 

## and Unit4 CEMS for nine test runs.

Unil4 CEMS RATA 

## 3-3 Vcoliu 

## Sa u

ge t 40942525 A-185 

# VES0126 3 9

## Table 3 · 1

. Oxygen Correction of Reference Method CO Concentration Resu lts Unit 4 CEMS Performance Spec ifi cation Testing
Run \\ ' rt: 

## O t Dr y 0 1 

### N umbe-r 

# o ... Run Time (%, · we i 

### (% , d

_ r y basis ) 

## basb) I 

## 9/ 4 12013 09:05.()9:26 8.88 

## 1 3.2 1 2 9 / 4 120 1 3 09:54-10 : 1 5 9. 1 6 13
. 70 3 9/4/20 1 3 10:29- 10:5 0 8.84 1 3.33 4 9 1412 0 13 11 : 00

- 11 :2 1 9.44 1 3.91 5 

## 9 1 4 12013 1 1:31- 11: 52 9.2 7 1 3. S3 6 9 / 4 120 13 12 :03- 1 2 :2 4 9.29 13.83 7 9 / 4120 1 3 12:3 6 -12: 57 9 .4 3 1 3
. 67 8 9 1 412013 1 3:09·13:30 9.02 13
. 4 I 

## 9 9 / 4/2013 13:43-14:04 9. 15 1 3.7 4 10 91 4 120 1 3 14 : 1 7

- 1 4 :38 8. 97 

## 13. 44

Uni t 4 CEMS RATA 

## 3-4 .1\toin:ure \VetO , 

## (%) (%. dr)' 

### basis ) 

## 32.75 13.2 1 33 .15 13 .70 33.6 5 13
. 33 32
. 1 2 1 3 .9 1 32.93 13,83 32.83 13
. 83 3 1.04 13
. 67 32
. 73 13.4 1 33.44 13
. 74 33
. 30 1 3.44 

# c o co ( ppm' ' • {ppmv, 

## dr y bosi t) @ 7%0 ,) 0 .53 0
. 95 0.59 

## 1. 14 0
.

4 1 0
. 75 0. 15 0.30 0. 3 0 0
. 60 0.52 1. 02 0
. 35 0
. 6 7 0.16 

## OJO 0
. 16 0.31 0.32 0.60

Vco U a 

## Snuget409425 25 A-186 

# VES01 26 40

# 4 . 0 Quality Assurance To ensure accura te and defensible results, strict quality assurance and control measures were followed. All testing was petf ormed following sta ndard EPA 

## protocol as outlined in 40 

# CFR, Prut 60, Appendices A and 

# B. All 

# PST testing was perfonned while t h e plant was operating u n

der oonnal conditions with at 

## least 50% load from waste feeds and/or natural gas. 

## H ard copies of incinerator waste feed rate datu are included in Appendix D. All test cri t eria were thoroughly documented and checked for comp l eteness. EPA Protocol gas certification documentation fo r compressed gas 

## cylinders used during the RA 

## testi ng is included in Appendix 

# E. The CO and 

# 0 2 

## analyzers used by URS were operated and calibrated in accordance with the EPA Methods 10 and 3A excep t t hat the 

# C0 2 

## interference trap was not used
. The gas ftlter corre l ation analyzer nsed for CO mea sureme n t uses the characterist i c absorption of infrared l ight by CO mo lecu les to measure its relative concentra tion. This is a highly s p ecific method for determining CO and is v irtua lly fr ee of interference from 

## compou n ds suc h as wntcr or carbon dioxide
. System b i as checks were pcrfonned before and 

# after each t est r u n to 

# ensure that 

# the measutiug systems remained 'ViOlin their performance spec ification s. All me t hod performance s p

eci ficat ions were m et. Ca libra tion re su l ts are documented in 

## Appendix B.



## U

o

i t4 C E

MS RATA 

## 4-1 Veoltn S•us•• 40942525 A·l87 

# VES012641

# APPENDIX A Relative Accuracy Spreadsheet and Reference Method Data

1\-1 88 

# VES012642

### V eola Saua:tt Unit 4 RATA RelotJve Acxurwt Resutu



### 9(4(20U 

### T I ME Run 1 

### 09:05-()9: 26 

### Run 2 09 : 54

- 10 :15 

### Run 3 10 : 2!HO : SO Run4 

### 1
. 1 :00-11 : 21 RunS 

### 11:31-1.1 : 52 R

unG 

### U :03·12:2 4 R

un 7 

### 12: 36

- 1 2:57 Ru n8 

### 13:09-1 3 : 30 R vn9 

### 13 : 43

- 14:04 Run 10 

### 14 : 17

- 14 : '18 Oz, Wet 

### (%) 

### 8.88 9 .16 8
. 84 9.44 9
. 27 9.29 9.43 9
. 0 2 9.15 

### 8.97 

### R EF E R

E

NC E METHOD 

### O,Ory 

# o,Oty Mo b:ture '"· from

( 'l6) 

### ( %) Wet) 

### 13.2 1 32
. 7 5 13.21 13.70 33.15 13 .7 0 13.33 33.65 13 33 13.91 32
. 1l 13.91 13

. 83 32
. 93 13
. 83 1 3.83 32
. 8 3 13.83 13.67 31.0 4 1 3.67 l3.41 

### 32.73 13 .41 13.74 33 , 44 

### 13.74 13.44 33
. 30 13.44 

### S TACK ANA LYZERS ARIT HMETIC D I FF E R

E

N

CE 

# co 

# o, Use 

# co Use 0,. Wet Use 

# co u .. 

# co (0, Corr) Wtt of 

### (0, Con) ol ol 

### (0, Con) 

# "' (%) Aun 1 R u n' 

### (ppm) (ppm) 

### ('l6) Ru n 1 

### (ppm) Run 1 

### ( ppm) 

### 0.53 0
. 95 8.58 0.o7

- 0
. 30 -0
. 88 0 .59 

### 1.14 8.94 0
. 10 X .0
. 22 -1. 04 X 0
. 41 0
. 75 8.70 0
. 08 .().14 .().67 0 IS 030 

### 9.15 0
. 11 .0.29 .0.19 0.30 0 .60 

### 9
. 03 0
. 13 .0
. 24

- 0
. 47 0.52 1
. 02 9 , 04 0
. 10

- 0. 25

- 0 .92 0.35 0.67 8.89 X 

### 0.09 -0
. 54**~** 

### -0
. 58 0.16 0
. 30 8
. 70 0.23 .0
. 32 .().Q7 

### 0.16 

### 031 8
. 96 0
. 07 .0
. 19 .0
. 24 0.32 0
. 60 8
. 75 

### 034 .0
. 22 .0.26 

### Number of 

### Runs Used in Ca Jculatlon {rt 

### 9 9 Aver age O i f

fetence Cd,. 11 G) 

### · 0.2 4 .0. 4 7 

### Sta nd ar d Deviation (S,) 

# o.oo 0 .3 1 

### t- Va l uo (lo.m) 

### 2
. 306 2
. 306 

### Confidena Coeff...,t ( CC) 

# - 0
. 04


# - 0
. 24 Pern"Mt U m' 

# - 100 Ave rage of Reft!rence Met h od 

### t RM. \'6) 9.11 0.61 

### Re l otlvo A c cura<Y (O , CO ,) (ld,""l) 0.2 4

## ~::-**~:.: ·**  Re l ot i ve Accuracy (CO , NO,. 

# so ,) U d.. vo i • I CCI)

## ::::::~~=:;: 0
. 7 

### Re

Ja

t i

ve Accuracy l" of Pe 1m i t Umit) ( RA ....::::;'"-· 

# ·- · 0.7 

# . An 

### X in this 

### column denotes a run which is 

### not ust"d In c.akutation of 

## fmttve i1CCUI'3Cy

A- l tll



# .... VESOJ26434-Sep-13 R

\l n l R un2 R u n 3 R u rt 4 

### Ru n S R un 6 R u n7 R u n! Ruo9 R mlO



# ..

s.u """ 1 Ru n 2 

### Ru n 3 R

un • 

### R

u nS Ft u n 6 R un 7 R u nS R u n 9 R u n 1 0



# .. _13

Runt

""" 2 

# . ... . Ron• 

# . .... . Roo 6 

# """' R

"" 8 R u n9 Run 1 0
4-Sep-13

R u n 1 fl u n 

### 2 R u n3 Ru n 4 

### Ru n S R un G R un7 Run S Ru\9 R un l D 

### 2013 Unh 4 CE MS RATA**Bl~u** 

### Correc'lld Concentrations 

### 0910412013 Veolia 

### Saucet Unit 4 RATA Uncorr.cted Conctntratiom Time 

## o, W t t 

## a . Drt 

## co ( !I) (!I) (P9m) 

### 09:05•09 : 26 

### t.09 13:2 1 

### .0
. 2 09 : S4 -1 0:1S 9
.. 1 7 

### 13.69 0
. 0 1 0;29-1 0 :50 

### 9.0 1 13.32 

### .0
. 1 11 :00-11:2 .1 

## t . s.o 1
. 1-90 · 0 .:2**11 31** **11:S2 9~** **L** 0.0**2,0).12 2.4** 

# ~ lU O 0
. 0**~3S:12 S7**  !J ,. 44 U.6S 

## .O. l**B:09 1J** **)O** 

### 90fl IUO 

### .0. 1**1~43 14.1»4**  

### 9
. 29 

## u . n '<>. 3 1.&:1 7

- 14 : 38 

# . . ... UAl 

### "<> .2 Con-Ktcd**Wet~** CCII<. 

# """' D,(!Q 

### Co £4- 7£ · 5 Factors 

### c..J(c..<ol 09;05t-Q!kl6 

### 909 138 1
. 2> 09:-S4-10t15 

### 9.17 1.92 1. 26 S.O:&l&.SO SI , Ol 1.94 1.2 5 U ; D0-11;2 1 

### 9S4 1.98 

### LI S 

### J l! 3l · ll : S2 9
. 40 1 .91 

### 1. 2 5 12:0 3-1 2 , 2 4 9 4 2 1
. 97 1 .25 

### 12:
.

'36-12 :5 7 9 • .11 11 

### 1.95 1
. 26 U :e&.U :! O 

### 9
. 08 J .96 

### 1. 27 13 ; 4 )..1 4 : 04**29** 2
. 00 1 .26 14 :17 ·14 : 18 

### 9
. 19 2
. 0 1 L2S 

### Corrected 

### Drv 

### 0t Cone. Tim• 

## co, !!II E q. 7f.S Factors 

# c. C..J!c..<ol 09:0>-09:26 

### U.ll 

## o.os 1.00 09;54-llklS UM 0 06 LOO 

### 1 0:.&-lO".SO 13.32 0,06 LOO U:B).lLll ll.tO OJ)7 L01 tl;ll · U.:Sl 

### 13 81 0.07 1. 01 

### 12:01-12:2 4 

### IJ.BO 0. 06 LOI 11:35-11:57 

### U
. 65 0.00 

### LOl**~ll:.lO** 

### 13

. 40 0.06 LO l U ; 4)- l<l. 04 1)
. 12 0. 06 

### 1. 0 · 1 l4:1 7·1 4
. l8 

## n . u 0 .0 6 1. 01 CorrHtecJ CO COnt. Tlme 

### CO (ppm( Co EQ, 

### 7£ • ' F1ClOtS 

### c..Jcc •.

c.t 09 : 05 · 09 : ] 6 · 0 .16 

### -0. 6 7 1 .0 2 09: S4·1 0:1S 0, 01 

# .., _,., l. Ol 1 0 ; 29 ·10o SO ·0.10 .() .50 

### 1
. 0 1 11:00-U:Zl .0.19 .0. '14 )..03 11 :.3 l · U:S2 0 .01 .0.2 9 l. Ol 1 21ll•ll;2- 4 000 .0. 50 L02 

### l2 ..36- ll.n .0.10**.0.~** l.O l 13 :09•1UO 

### .009 .024 1.0 3 ll:4l-- 1 .:04 .(),27 .(),43 1.0 3**~11-14~** .0.17 -0.49 

### LD3



### A

· 2

# ~

"" Con" ta td ConctftC:tl tkm 

### Ul t.l6 

### 1.84 

# .. .. 9.27 

### 9 29 9 .4 3 

### 9.02 9.15 

### $ , 97
1111.,- Corrected Conufrtrttk>ft 13.21 

### 13711 13.33 l'J.-91 1U3 IUJ 

### U.C? 11.41 1 1.7 4 t3. 44

8111 Corttcttd 

### Conce ntr ttlol'l 0.5 0.6 

# • • • 0.1 OJ 

### OS 0
. ) 0.2 

### o.2 

### O.l

A-190 

# VESOI2644

### Project Name 2013 CPT RAT 

### As Pas• 

# I o f 

# A**,.**



## .. 'fl > Proj ect Number 

## 40942S)B' t,.or, Operator 

# IJ.-\.DD

!" 

# "'



# <

# '~ m 

# en 0 

# - N

# ~ 

# "" FacQity veorta Sauget 

### Condition(s) 

# IU<-T .A SOUrce 

# U O'I ;+ 

# 4**~~** Run(s)

### ~~S l-j 

# 0 Date 

# '1 

# l ..<t lt "> 

# C

alibrati on G ases Componen t ts) 1 

### S up p ltar " concontrat lon( s) Cylind er lO**~· 1..**  

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# "t -4 '1

' l

ndiute multkclm.ponent stoandards appropri3ttfy 

### 'Cod a : A G

· A1 rc-.s; AL· Air Uqulde; s-scott ; p.:,t axar r 

# I nstr u me nt I den tifi ca ti o n Anafyte 

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# M e t h od P e rform a n ce Ch ec k s Acti v ity 

## M ethod Criterion Initials 3A. 

## «;. '" Emissiofu: 

### bdwun**~** Md 10(),;. of a i brltion spu 

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### expe c.ted kvtl 

# - 3A. 

## «;. 7E, P rotocol 

### pt;; Cll lbfa: t ion**~n.** 

### 40 · 60" of aibra li on sptn, 

## \)..q)1) Clllbr.ltion GI S 

### 10 and**~of** 

### ealibui.Jeft**U~oJ,n** {ot 1tro 

## aut Seloclloo 

### 2SA 

### """""'PJ' 2S-lSl< • ..S.SS11 and 

### 81).- cl """ ..,..**C1'11d9~ir** 

# -- S p a n sas YA t h l n !-2. 0 " of calbratl on span 

## 'IM-121)
_ 3.4,6C.Jt.**Mid~n~** I" wtlh in .!2..'"' oi alib"Uon fl)tn 

# ll.U>D ll) Olbation (IT"CK 

### 2.tto p5**~** :l.2.0:5 of allbnoWn Spt n 

# • .. 1M®

. Low-flnee a;u within 5" or ct.rtifle d v• lu:e 

# - 2SA Mi d -n"ge GM wkhin 

### S" of certlfte:d value 

# -**~n** 

### ps wtth ln 

### 5 " of cettifttd 

### va ftr e Co!Welt eT Chtct 

### 7!**~** conYffttf tffk:ieney 

# - 1 Sys t e m Bi as**k** 3A. GC, 7(. Gas 

### throu.eft JVS't* m a grte j 

### with**e.lib r~** **'lon** errOf' vatuc fat 

# I.UW ll) 

### that gas wltlllll t5.0!4 

### ol calil>noon >9>0 

# ..._nmo 31..«:.71:. No**c:ritl'ria~** enlu:ated to fttwtniae duradoft M. 

### AmPk 

# MD lO

. lSA 

# - 3A. 6C. 7£, SUb!e**~mpllt** flow 

### me wk h l.n 1(M( of 

### Row rate embllsllod '**S~ Pk**  

### Flo w 

### Rate 10 duri n & sy . \l t m r es p onse U.ne the<k: a i'MI blb 

### c t 1 t:dc

### · JPoinr 

### 31..«:.71:. t 5" 

## ot mun**~t** 

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# I.U6> D ! Chedt" ll)
,. ::.10' 

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# u points Stlitde d cas rt3<fi ng wi thi n :tl
. O% of**~tlr.atbn $~n**  of 

# VvlllP : 3A. GC,**7~,** pre-iest re.ldltlfl; 

### Post-Test 

### tO 

### Zero ps wtthan 

### tl.m( of callbrttlott .span or 

### cwe-ust 

# !MOO 

# c.r...-.-- rudin& Chedt 

### Seleaed ps mdl n&**\~~!than** 1

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# CEMS Ope r a ti o n Log Proj ect Name 2013 C PT RA T As Project Number**09425 ~2-'>**  

### Facility Veolia Sauget 

## Source 

# V 11 it- 

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A-228 

# VES012682

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## o.cm**\4~** 11.10 .0.5"



### B-3**Abseil~•** Cll Error ClM 

# " "'1101'1• 

# l""'""ol Oiffere'KI! l.O.Umit 

### 0.00 0Jl6 CUOI 

### 2:2

. 6S O .l S 

# .. ,.,. 11.22 0,12 

# ..... """ l" ofSp1n) 

### E q. 1E·S 

### $,0011!""'



## o

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# .... 

# - O.DII <...nc..<.IIM4



# ..... c.. o.o6l 0
. 001 c../IC.,<,J 

### LOOS



# ..... C'o· 0.062 

### O

.oK 

## c ..,NC,.<.g,) t.oos 0.101**~·** 0.071 0001 

### c..nc..<oii.DOG



# ..... ... 0.01S

· O.l'C <.JIC..C, I 1.007 

## o.o" "'0.003 0
. 091 

### <-A<.<ot 1.006 0.091 

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. 091 <.Jt<,. 

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. 091 C. · O.OS8 I O

. O'll**~1.006** 

## o.ow. "" 0.058 

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A · 23 1 

# VES0126 85

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# J J J J J .;.l!**oo~** 

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# s 

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# ~ 

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# • 

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# APPENDIXC Unit 4 CEMS Relative Accuracy Data

A · 233 

# VES012687

## Tlme

_ 5tamp 

# I COOryC orr 

## 02 Wet 020ry H20 

## 9/

4 / 13 9:06AM 0.12 8.28 12.5 8 34.16 9/4/13 9:07 AM 0
. 19 8
. 16 12.40 34
. 24 9/4/13 9:08 AM 0.11 7 .9 5 12. 1 9 3 4 .73 9/4/13 9 : 09AM 0.00 7 .84 12.10 35.20 9/4/13 9:10AM 0.11 7
. 82 12.10 35.38 9/

4/ 13 9 : 11AM 0
.00 8.59 13
. 36 35.69 9

/4/1 3 9 : 12AM 0.00 8.92 13
. 77 35
. 25 9/

4/13 9:13AM 0 .11 8.05 12
. 38 3 4 .95 9/

4/13 9 : 14AM 0
. 04 8 .2 8 12 .9 2 35 .91 9/4/13 9:15AM 0 .00 8 .98 13 .88 35.32 9/

4 /13 9: 16AM 0 .0 9 9.31 14. 12 34.10 9/

4

/13 9:17 AM 0.15 9.40 14.20 33.83 9/

4 /13 9 : 18AM 0.00 9.16 13.82 33.69 9/4/13 9 : 19 AM 0.19 9.27 1 4
.04 33.96 9/4/13 9 : 20AM 0.13 8.98 13
. 62 34. 1 0 9/

4 /1 3 9 : 21AM 0.04 8. 79 13.39 34.36 9/4/13 9:22 AM 0
. 04 8
. 58 13.11 34.55 9/4/13 9:23AM 0
. 04 8.44 12.9 5 34.79 9/4/13 9:24AM 0.00 8. 49 12.98 34
. 57 9/4/ 1 3 9:25AM 0.04 8.45 12.89 3 4.46 9/ 4/13 9 : 26AM 0.12 8.40 12.92 34.99 Average O.o7 

## 8.58 

## 13.13 34.68
U

nit 4 R un 1 09/04/13

C. 1 A·234 

# VESOl2688

### Tlme Stamp CODryCorr 02Wet 02Dry H20 

## 9/4/13 9:55AM 0.2 4 9.26 14
. 07 34.19 9/4/13 9:56AM 0
. 10 9. 40 14.26 34.07 9/4/13 9:57AM 0
. 00 

## 9
. 23 13.99 33.99 9/4/13 9:58AM 0.04 8.84 13.40 34.04 9/4/13 9:59AM 0.08 8.63 13.14 34.34 9/4/13 10:00 AM 0.08 8 .25 12.63 34.71 9/4/13 10:01 AM 0.04 8.53 1 3.15 35.11 9/4/13 10:02 AM 0.16 8.34 

## 12.84 35.01 9/

4/ 13 10:03 AM 0.13 8 .69 13.41 35.21 9/4/13 10:04 AM 0.05 8.85 13.64 35
. 10 9/4/13 10:05 AM 0.13 8.76 13.50 35.08 9/4/13 10:06 AM 0.09 8.82 13.57 35.00 9/4/13 10:07 AM 0.18 8
. 94 13.70 34.76 9/4/13 10:08 AM 0.24 9.37 14.26 34.29 9/4/13 10:09 AM 0.10 9.48 14.34 33.92 9/4/13 10:10 AM 0.05 9.11 13 .94 34.24 9/

4/1 3 10:11 AM 0.09 9.03 13.72 

## 34.18 9/4/13 10:12 AM 0.00 8
. 93 13
. 60 34 .2 9 9/4/13 10:13 AM 0.00 9.12 13.87 34.23 9/4/13 10:14 AM 0.13 9.06 13.77 34.19 9/4/13 10:15 AM 0.14 9.11 13.85 34.20 Ave,...ge 0.10 8
. 94 13.65 34.48 Unit 4 Run2 

## 09/04/13

C-2 A-235 

# VES012689

### Time Stamp 

# I CO DryCorr 02Wet 02Dry H2.0 

## 9/4/13 10:30 AM 0
. 08 8.71 13 .25 34 .23 9/4/13 10:31 AM 0.13 8.79 13.39 34
. 40 9/4/13 10:32 AM 0.04 8.81 13 .44 

## 34.40 9/

4/13 10:33 AM 0
. 17 8.71 13.26 34.28 9/4/13 10:34 AM 0.17 8.69 13.25 34.44 9/4/13 10:35 AM 0.13 8.65 13
. 25 34.73 9/4/13 10:36 AM 0.17 8.70 13.39 35.03 9/4/ 1 3 10:37 AM 0.04 8.63 13
. 21 34.65 9/4/13 10:38 AM 0.09 8.91 13.47 33.83 9/4/13 1 0 :39 AM 0.04 8.95 13. 46 33.50 9/4/13 10 :40 AM 0.04 8.78 13.25 33.71 9/

4 /13 1 0:41 AM 0.13 8 .77 13.37 34.41 9/4/13 10 : 42 AM 0.05 8.82 13.58 35.09 9

/ 4/13 10:43 AM 0
. 00 8
. 53 13.09 34.85 9/4/13 10:44 AM 0.08 8.31 12.82 35
. 22 9/4/13 1 0:45 AM 0.00 8.32 12
. 90 35.52 9/4/13 10:46 AM 0.04 8.22 12
. 72 35.39 9/4/13 10:47 A M 0.00 8.53 13
. 17 35.25

.**~/4/ 13**  

## 10:48 AM 0.12 8.31 12
. 76 34.84

9/4/13 10: 49 AM 0
. 10 8.95 13. 74 34.88 9/4/13 10:50 AM 0.05 9.52 14.47 34.22 Average 0
. 08 8.70 13.30 34.61 Unit4 Run 3 09/0 4 /13

C-3 

### M!36 

# VES012690

### T ime Stamp COOJ'V(orr 

## 02 W e t 02Dry H20 9/4/13 11:01 AM 0.18 8.77 13.48 35.00 9/4/13 11:02 AM 0.13 8.91 13.61 34
. 53 9/4/13 11:03 AM 0.18 9.00 13
. 71 34
. 37 9/4/13 11:04 AM 0
. 05 9.04 13.76 34
. 31 9/4/13 11:05 AM 0.10 9.34 14.22 34.35 9/4/ 13 11:06 AM 0.19 9.45 14.26 33.75 9/4/13 11:07 AM 0.14 9.41 14.11 33.28 9/4/13 11 :08 AM 0.05 9
. 45 14
. 24 33.66 9/4/13 11:09 AM 0.09 9.31 14.09 33 .9 0 9/

4

/13 11:10 AM 0 .09 8.95 13.63 

## 34.32 9/4/13 11:11 AM 0 .00 8 .6 8 13.29 34.69 9/4/13 11:12 AM 0.00 9.06 13
. 89 

## 34
. 73 9/4/13 11:13 AM 0.09 9.05 13.65 33
. 71 9/4/13 11:14 AM 0.04 8 .92 13
. 49 33.83 9/4/13 11:15 AM 0
. 14 9.22 13.99 34.07 9/4/13 11:16 AM 0 .09 9 .3 4 14. 1 2 33
. 84 9/4/13 11 :17 AM 0
. 09 9.40 14
. 23 33
. 94 9/4/13 11: 18 AM 0
. 19 9.43 14
. 31 3 4
. 13 9/4/13 11 : 19 AM 0.19 9.39 14 .23 33.98 9/

4/ 13 11 :20 AM 0.13 9.08 13.77 34.10 9/4/13 11:21 AM 0.13 9
. 00 13.71 34.35 Average 0.11 9
. 15 13.89 34 .13 Unlt4 Run 4 09/04/13

C·4 A-237 

# VES01269l

### Tl me c Stamp 

# I**COD~Corr** 

## 02Wet 02Dry K20 

## 9/4/13 11:32 AM 0
. 15 

## 9
. 66 14.62 33
. 90 9/

4 / 13 11:33 AM 0
. 05 9
. 52 14 .48 34
. 25 9/4/13 11 : 34 AM 0
. 15 9
. 38 14.30 34.46 9/4/13 11:35 AM 0
. 00 8.8 9 13.62 34.70 9/

4/13 11 :36 AM 0.09 8.75 13 .58 35.53 9/4/13 11 : 37 AM 0
. 05 8.86 13
. 81 35
. 86 9/4/13 11: 38 AM 0
. 05 8.90 1 3.86 35
. 82 9/4/ 13 11 :39 AM 0.67 9
. 13 14.15 35.48 9/

4/13 11:40 AM 0.72 8.97 13
. 66 34
. 35 9/4/ 13 11:41 AM 0
. 04 8.89 13.52 34
. 23 9/4/13 11: 42 AM 0.04 8.92 13.56 34.18 9/4/13 11:43 AM 0.04 8
. 90 13 .50 34
. 08 9/4/13 11:44 AM 0.13 9.17 13.92 34
. 11 9/4/13 11 : 45 AM 0
. 19 9.33 14
. 14 33.97 9 / 4/13 11 : 46 AM 0
. 00 9.2
. 5 14.01 33
. 97 9/4/13 11 : 47 AM 0
. 09 9.11 13.86 34.27 9 / 4/13 11:48 AM 0.04 8 .7 1 13.35 34
. 74 9/4/13 11:49 AM 0
. 04 8.23 12.71 3 5.22 9/4/13 11:50 AM 0
. 04 8.96 13.87 35.44 9/4/13 11:51 AM 0.18 8.99 13.79 

## 34
. 82 9/4/ 1 3 11 : 52 AM 0
. 05 9.13 14.00 3 4.79 Average 0
. 13 9.03 13.82 34.67
Unit4 Run 5 09/ 04/13

C·5 A-238 

# VES012692

### Time Stamp CODryCorr 02Wet 02Dry H20 

## 9/4/13 12:04 PM 0.00 8.82 13.51 34
. 69 9/4/13 12:05 PM 0
. 05 8 .72 13.42 34.97 9/4/13 12:06 PM 0
. 14 

## 9.11 13.96 34.73 9/4/13 12:07 PM 0.05 9.08 13.78 34
. 10 9/4/13 12:08 PM 0.05 9.19 13.97 34.23 9/4/13 12:09 PM 0.10 9.38 14
. 26 34.24 9/4/13 12:10 PM 0.10 9.44 1 4 .32 34.05 9/4/13 12:11 PM 0.00 9.34 1 4 .19 34.15 9/

4/13 12:12 PM 0.05 9.15 13.94 34.37 9/4/13 12:13 PM 0
. 00 9
. 30 1 4
. 19 34.48 9/4/13 12 : 14 PM 0
. 24 9.33 1 4.20 34
. 29 9/4/13 12 :15 PM 0.05 9.34 14. 19 34.17 9/

4/ 1 3 12 : 16 PM 0.1 4 9.14 13
. 93 34
. 35 9/4/13 12:17 PM 0.19 9 .1 8 14.04 34.61 9/

4

/13 12:18 PM 0.09 8.88 13.58 34.64 9/4/13 12:19 PM 0.22 8.76 13 .44 34.85 9/4/13 12:20 PM 0.09 8.83 13.52 34.69 9/4/13 12:
. 21 PM 0.1
. 3 8.75 13
. 35 34
. 50 9/4/13 1 2:22 PM 0.17 8.72 13.39 34.82 9/

4/13 12:23 PM 0.13 8.80 13.53 34.99 9/4/13 1 2:2 4 P M 0.09 8.59 13.22 35
. 05 

# Average 0.10 9
. 04 13.8 1 34
. 52
Unit 4 Run 6 09/04/13

A · 239 

# VES012693

### Tlme = Stamp 

### CO OryCorr 

## 02Wet 020,Y H20 

## 9/4/13 12:37 PM 0.04 8.45 13.03 35.16 9/4/13 12:38 PM 0.13 8 .72 13.45 35.14 9/4/13 12 : 39 PM 0
. 09 8
. 95 13.71 

## 34.72 9/4/13.12:40 PM 0
. 28 9.21 13.99 3 4
. 15 9/4/13 12 :4 1 PM 0
. 13 8.81 13.39 34.21 9/4/13 12:42 P M 0.09 8.97 13.82 35.11 9/4/13 12 :43 PM 0.09 8.87 13.71 35 .3 3 9/4/13 12:44 PM 0.05 9
. 01 14.00 35 .6 4 9/4/13 12:45 PM 0
. 00 9.15 14.10 35.14 9/4/13 12:46 PM 0 .09 8.93 13.68 34-72 9/4/ 13 12:47 PM 0.05 9.08 13
. 93 34
. 82 9/4/13 12: 48 P M 0.09 9.04 13 .91 34.98 9/4/13 12:49 PM 0.00 8
. 72 13
. 43 35.05 9/4/13 12:50 PM 0
. 09 8.59 13.30 35
. 48 9/4/13 12:51 PM 0.09 8
. 67 13 .51 35
. 84 9/4/13 12:52 PM 0.05 9.02 14.00 35.56 9/4/13 12:53 PM 0.14 9
. 00 13.84 34.97 9/4/ 13 12:54 PM 0.00 8.82 13.56 35.01 9/4/13 12:55 PM 0.05 8
. 84 13.63 35.13 9/

4/1 3 12:56 PM 0
. 09 8.98 13.81 34.99 9/4/13 12:57 PM 0.18 8.97 13.76 34.80 Average 

## 0.09 8.89 13.69 35.05 Unlt4 Run7 09/04/13

C

-7 

### .A -2 40 

# VES012694

## T i m e S ta mp CO D ry(o rr 

## 02We t 02 Dry H20

9

/ 4

/ 13 1 : 1 0P M 

# o . oo 8
. 9 3 13.8 1 35
. 35 9 / 4 / 13 1: 11 PM 0
. 05 9.09 14. 04 35
. 25 9/4/13 1 : 12 PM 0
. 09 9
. 12 14.0 1 34
. 90 9/ 4 /13 1 : 13PM 0.05 9.10 13 .96 34.80 9/

4

/ 1 3 1: 1 4 PM 0.05 9 .18 13
. 98 3 4
. 33 9 / 4 / 1 3 1:15P M 0.00 8.81 13.3 4 3 4. 01 9/4/13 1 : 16 P M 0.04 8
. 31 

## 12..73 3 4 .73 9 /4/1 3 1 : 17 P M 0.00 8
. 56 13
. 2 3 35
. 27 9/

4

/13 1 : 18PM 0. 00 8. 86 1 3
. 63 35
. 02 9/4/ 1 3 1 : 19P M 0
. 05 8.90 13
. 64 

## 3 4
. 77 9/4/13 1 : 20P M 0
. 04 8.57 13 .1 0 34.58 9 / 4 / 13 1 : 21P M 0
. 22 8
. 68 1 3.44 3 5 .42 9 / 4 / 13 1 : 22 P M 0
. 09 8
. 89 1 3.7 1 3 5. 17 9

/ 4

/ 13 1 : 23 P M 0
. 08 8
. 5 6 13.16 34
. 9 1 9 / 4 /1 3 1 : 2 4 PM 1
. 04 8
. 54 13. 1 5 35
. 06 9 / 4 /13 1 : 25 PM 2
. 50 8
. 52 1 3
. 09 34
. 93 9/

4

/ 1 3 1:26PM 0
. 1 2 8
. 33 12.86 35 .1 9 9/4/ 1 3 1:27 PM 0.04 8.2 2 1 2
. 77 35
. 63 9/4/ 1 3 1 : 28PM 0
. 1 7 8
. 55 1 3.29 35
. 66 9/

4 /13 1 : 29PM 0 .0 4 8. 3 9 13.00 35. 4 1 9 /4/ 13 1:3 0PM 0
. 09 8.49 13
. 2 1 35.73 A

v erage 0
. 23 8.70 13
. 39 35
. 05 Unit 4 Runs 09/04/ 1 3

C-1! A- 24 1 

# VES012695

### Tim e

_ Stamp 

## CO OryCorr 02Wet 020ry H20 9/4/13 1: 44 PM 0.00 9.01 13
. 74 34
. 40 9/4/13 1 : 45PM 0
. 00 9.03 13.8.7 34
. 89 9/4/13 1:46 PM 0.04 8.83 13
. 59 35.0 4 9/4/13 1 :4 7P M 0.13 8.58 13.26 35.32 9/4/13 1 :48PM 0.00 8.70 13. 48 35
. 50 9/4/13 1: 49PM 0.18 8
. 90 13.70 35.02 9/4/13 1:50PM 0
. 08 8 .5 2 13.12 35.0 8 9/4/13 1 :5 1 P M 0
. 00 8.46 13.11 35 .4 2 9/

4/13 1 :5 2PM 0.04 8.62 13
. 36 35.44 9/

4 /13 1:53PM 0.00 8.90 13
. 76 35.29 9/

4 /13 1:54 PM 0
. 09 9
. 14 14
. 04 34.95 9/4/13 1 :55 PM 0
. 15 9
. 55 14.50 34
. 10 9/4/13 1:56 PM 0. 14 9
. 60 14.41 33 .3 7 9

/ 4

/ 13 1 :57 PM 0.05 9
. 33 14 .06 33
. 6 3 9

/ 4/13 1 :5 8 PM 0.05 9.26 14. 04 3 4
. 04 9/4/13 1 : 59 PM 0.04 9.15 13.89 34.12 9/4/13 2:00PM 0.00 9.04 13
. n 34
. 33 9/4/13 2:01 PM 0.04 

# 8.n 13
. 41 34.59 9/4/13 2 :02 PM 0.18 8.88 13.62 3 4
. 78 9/4/13 2:03PM 0.13 8.89 13.63 34.74 9/4/13 2 :04 PM 0.14 9.03 13.83 34.74 Average 0.07 8 .96 13.72 34.70 U nit 4 R u n9 

## 09/04/13

C · 9 

### A-242 

# VES012696

## Time

_ Stamp :.: 

# · I ;· CO DryCorr ,· l :·.: 

## 02 

# Wet :".. 

# · I

·· 02Dry
... · ,·· H 20 

# ,,,,, I 9/4/13 2:18 PM 0.00 8.18 12.73 35.77 9/4/13 2:19 PM 0.19 8.96 13.84 35.27 9/4/13 2 :20 P M 0 .10 9.11 13.89 34.39 9/4/ 1 3 2 :2 1PM 0
. 44 9.03 13.73 34.24 9/4/ 1 3 2:22 PM 3.13 9
. 04 13
. 68 33.89 9/

4 /13 2 : 23PM 1.03 8
. 37 12.78 34
. 48 9/4/13 2 : 24PM 0.09 9.03 13.91 35.09 9/4/ 1 3 2: 2 5PM 0.09 9.08 13
. 92 34
. 80 9/4/13 2:26 PM 0.09 9.04 13.84 34.69 9/4/13 2:27PM 0.09 8
. 93 13.63 34.53 9/4/13 2:28 PM 0.18 8
. 93 13.64 34
. 53 9/4/13 2:2 9 PM 0
. 08 8 .4 3 12
. 89 34
. 61 9/4/13 2:30PM 0.04 8
. 22 12
. 70 35.30 9/

4 /13 2 : 31PM 0.12 8.25 12.80 35.58 9/4/13 2:32 PM 0
. 11 7.73 12.04 35.82 9/4/13 2:33 PM 0
. 29 9
. 62 1 5.04 36.08 9/4/ 13 2 : 34PM 0.13 8
. 95 13.60 34
. 19 9/4/ 13 2:35PM 0
. 53 8.98 13.67 34
. 35 9/4/13 2:36PM 0.09 8
. 86 1 3
. 5 1 3 4
. 46 9/4/13 2:37PM 0.13 8.60 13
. 1 7 34.72 9/4/13 2:38 PM 0
. 12 8.34 12.87 35.19 Average 

## 0.34 8
. 75 1 3.42 34.86 Uni t 4 

## Run 10 09/04/13

C· IO 

# VES012697

# APPENDIXD Unit 4 Waste Feed Characterization Data

VESOl2698

## H ou r l y Report lnci,......tc< 4

# ONYX Veo li& Created 

### 9141201310:0 1 AM 

## Envlroament>l Services Period Start 9 / 412013 9:00AM Suget Illinois 

## Period End 9/41201310:00 AM 

## Pa&e I of I 

# CALCULAT I ONS B

T U 29

. 05 mbtu PCC BTU 22.33 mbtu M ain Line BTU 0

. 000000 mbtu 

# sec BTU 6.7 1 mbtu Aux Feed BTU 6.761 2 00 mbtu
Chlorine 93

. 2 lbs
Low Volatile 0

. 147 lbs Mercury 0

. 0002 l bs Semi Vol a tne 0

. 942 lbs Ash 663.0 lb s 

# WEIGHTS Weight 3146 lbs
Solids We i gh t 1847 l bs PCC Liqu i d Weight 1299 tbs Shredded We i ght 1325 l bs X10 Weight 399 l bs Containerized Weigh t 522 lbs X 1 1 We ig ht 899 lb s Main Line We i ght 0 lbs X 1 2 W ei ght 0 lbs Aux Feed Weight 522 lbs X22Weight 782 lbs
Pi t 1 Weight 0 lbs Tank 300 Weight 899 lbs Pit2 Weight 1325 l bs Tank 302 Weig

. ht 

# o lbs Pit 3 Weight 0 l bs Tank 30 4 Weight 0 l b s Pi t 4 Weight 0 lbs T ank 306 We i ght 0 l bs Tank 308 Weigh t 

# o lbs Direct Inject We i ght 399 lbs Tan k 310 Wei g ht 782 l b s Special Feeds We i ght 0 l bs Tank 31 2 Wei g ht 

# o lbs Ta n k 31 4 Weight 0 lbs 

# MISCELLANEOUS Waste Penn i ! Time 0

. 99 hrs Natural Gas Flow 10 420 

## cf

O. t A-245 

# VESOJ2699