Analytical Chemistry 

WL-ACP-7 I Molecular Spectroscopy and Thermal Analysis 

Dr. D. Wandschneider 

M. Shaukat 

tr +49-6151-72-561 0 dirk.wandschneider@merck.de 

tr +49-6151 -72-4561 manuela.shaukat@merck.de 

Analytical Report MS10_52 

UVNis spectroscopy of MAFS-092 

Client I Date of commission I Ob"ective: 

Dr. N. Fichtner, WL-ACP8 UVNis spectroscopy of MAFS-092 

09.08.2010 

s amp.es: 

Sample 

MAFS-092 Batch: FS-049-10-3 

Article- no.: -

SA -7: 2085313 

Summary: 

UVNis 

Raw date 

U21021 21 

The spectrum is plausible with the indicated structure. 

Report 

Date 

Page 

No additional absorption bands that may hint to an UVNis active impurity were observed. 

History of document 

I First version 113.08.10 I -

Distribution list: 

Dr. N. Fichtner WL-ACP 8 

M. Shaukat WL-ACP 7.0 

Reviewed: !flJ I Approved: 

I 

1

MERCK 

I 

MS10 52 

13.08.10 

1/3 

113! Zo.-zu !I'LJ 

~ .. fJ ~~!?~ ... 13 0 @; ... ... ......................... q1 ..... S. BrOninghoff 

WL-ACP-7.0 

S. Eichler 

WL-ACP-7.0 

Dr. D. Wandschneider 

WL-ACP-7 

Head of Laborato 
I 

Analytical Chemistry 

'dMERCK 

I 

WL-ACP-7 I Molecular Spectroscopy and Thermal Analysis Report MS10 52 

Dr. D. Wandschneider tl +49-6151-72-561 0 dirk.wandschneider@merck.de Date 13.08.10 

M. Shaukat if +49-6151-72-4561 manuela.shaukat@merck.de Page 2/3 

Results I Discussion: 
Analytical Chemistry 

I I 

,MERCK •, 

WL-ACP-7 I Molecular Spectroscopy and Thermal Analysis Report MS10 52 

Dr. D. Wandschneider tr +49-6151-72-561 0 dirk.wandschneider@merck.de Date 13.08.10 

M. Shaukat V +49-6151-72-4561 manuela.shaukat@merck.de Page 3/3 
0000000000 FS-049-10-3 

Auftrag : 0002085313 Teilauftrag fur Labor: AC7 

Auftrag: 0002085313 Kostenstelle: 

* kein Zertifikat * 

Artikel: oooooooooo Sparte: 

MAFS - 092 

09.08 . 10 

FF- Lab: AC80 

Charge: FS- 049-10-3 Menge: 0,5g Gefahrensymbol(e): 

Altern Chargen: 

Muster : 1 

f Eingegangen am 

0 9. Aug. 2010 

Methode: 9 UV-VIS - NIR- Spektrometrie CAS I AC7 

Pruftext: 

Auftragtext: 

Spektrum von 200 bis 700nm 

Spektrum bitte mit Interpretation 

mitliefern 

Restsubstanz zuruck an Dr.Fichtner 

und Bericht 

Termin: 13.08.10 

========= ======== 

------- --------------------- Ergebnis der Analyse --- --------------- ----------

)(s· jc __ s:--z 

r M. Shaukat tr 

1 6. Aug. 20t0 

WL-ACP 7 Tel. 4 61 

Datum Unterschrift 
13.08.2010 10:30:52 Page 1 of 1 

Scan Analysis Report 

Repor t Ti me : Fr 13 Aug 10:30 :43 AM 2010 

Ba tch: C:\Vari an\Cary WinUV\Datal\U2 l 0212l . BSW 

Software version: 02 . 00(25) 

Operator: 

Instrument Parameters 

I nstrument 

Instrument Version 

Start (nm) 

St op (nm) 

X Mode 

Y Mode 

UV-Vis Scan Rate (nm/minl 

UV-Vis Data Interval (nm) 

UV-Vis Ave . Time (sec) 

UV-Vis SBW (nm) 

Slit Height 

Beam Mode 

Signal-to-noise Mode 

uv Source 

Vis Source 

Third Source 

Source Changeover (nm) 

Detect or Changeover (nm) 

Baseline Correction 

Baseline Type 

Baseline Fil e Name 

Baseline St d Ref File Name 

Cycle Mode 

Comments 

Sample Name: U2102121 

Collecti on Time 

Wavelength (nm) Abs 

213,000 1,56682 

Cary soo 

8,01 

700 , 000 

200 , 000 

Nanometers 

Abs 

300,000 

0,500 

0 ,100 

2,000 

Full 

Double 

Off 

On 

On 

Off 

350,00 

BOO,OO 

On 

Basel ine correction 

C:\Vari an\Car y Wi nUV\Datal\U210212l.BSW 

Off 

MAFS- 092 

Charge : FS- 049 -10-3 FFL: AC80 

SA7 : 2085313 

Ref.: Wasser LiChroSol v 

d=lcm T=20°C C= 0,03280g/20mL 

: A11.?4Q IL 

11 .08 .2010 11 :34:20