### Name:

Title: Company: Sign Date: Name:
Title: Company: Sign Date: Permitted Facility Representative / Date Testing Company Representative / Date Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Wednesday, February 02, 2011 Page 1 of 31

### Facility Information:

OH_WH Zimmer Unit 1

1781 US Route 52

Moscow OH 45153
Contact: Jon Hays

Phone: 317-838-4445

Fax: 317-8382490

Email: jon.hays@duke.energy.com Testing Company:

AECOM 2 Technology Park Drive

Westford MA 01886
Contact: Patrick Ford

Phone: 978-589-3427

Fax: 978-589-3100

Email: pat.ford@aecom.com

Air Permit Number: Permitted Source ID/Name: No. 2 Fuel Oil/Coal-Fired Electric Utility Boilers Unit 1

Permitted Maximum Process Rate:
12656 Max. Normal Operation Process Rate:
12656 Target Process Test Rate
12656

Description of the source (including control equipment). Please see the attachments for source or process flow diagram:
This description should describe the process and associated controls to differentiate this facility from, or document similarity with others of same SCC. Industry/SCC/NAIS 221112

Sampling Location Information:

Test Parameter Information: AFS #: FRS #:

SCC / Description 10100202 External Combustion Boilers - Electric Generation - Bituminous/Subbituminous Coal - Pulverized Coal: Dry Bottom (Bituminous Coal)

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width

Stack Exit 512 8 2 4 0 12 0 0

Target Parameter Test Method Number of

Test Runs Test Run

Duration Sample

Points Comments Location

% H2O Method 1 - 4 3 60 0 Stack Exit Carbon Monoxide Method 10 4 120 0 Stack Exit Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Stack Exit

Hydrogen Fluoride Method 26A 3 60 0 Stack Exit Hydrogen Chloride Method 26A 3 60 0 Stack Exit
Arsenic Method 29 3 180 0 Stack Exit Manganese Method 29 3 180 0 Stack Exit



### Wednesday, February 02, 2011 Page 2 of 31

### The following describes any modifications and/or deviations to the applicable test

methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates.
EPA Method 26A was modified to include the provisions cited in Method CTM-033 to allow for the collection and analysis of HCN. Also, a higher strength NaOH was used in order to maintain the pH at a level that would ensure good HCN collection efficiency. This involved using 100 ml of 6N NaOH in the first impinger and 100 ml each of 2N NaOH in impingers 3 and 4. The sample time was also reduced to 1-hour as allowed by EPA (see FAQ's section on the ICR website) again to ensure that the pH of the absorbing solution remained high.

Lead Method 29 3 180 0 Stack Exit Antimony Method 29 3 180 0 Stack Exit Beryllium Method 29 3 180 0 Stack Exit Cobalt Method 29 3 180 0 Stack Exit Chromium Method 29 3 180 0 Stack Exit Selenium Method 29 3 180 0 Stack Exit Cadmium Method 29 3 180 0 Stack Exit Nickel Method 29 3 180 0 Stack Exit
O2 Method 3A O2 3 60 0 Stack Exit
Co2 Method 3A CO2 3 60 0 Stack Exit Total Particulate Method 5/OTM-28 3 180 0 Stack Exit Filterable Particulate Method 5/OTM-28 3 180 0 Stack Exit Organic Condensible

Particulate Method 5/OTM-28 3 180 0 Stack Exit

Inorganic (Aqueous)

Condensible Part. Method 5/OTM-28 3 180 0 Stack Exit

Sulfur Dioxide Method 6C 3 60 0 Stack Exit Nitrogen oxides (NOx) Method 7E 3 180 0 Stack Exit



### Wednesday, February 02, 2011 Page 3 of 31

### Sampling / Stack Data Results Summary



### Location Stack Exit - Method 10
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 10 3
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Wednesday, February 02, 2011 Page 4 of 31

### Location Stack Exit - Method 25A
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 26A
Average

Run Number 1 2 3

Test Date 4/20/2010 4/20/2010 4/20/2010

Run Start Time 9:28:00 AM 12:38:00 PM 3:15:00 PM

Run Finish Time 12:07:00 PM 2:51:00 PM 5:28:00 PM

Net Run Time, minutes 120 120 120 Dry Gas Meter Volume Sampled, dscf 98.410 97.142 96.138 97.230
Moisture Content of Stack Gas, % 14.16 14.83 14.94 14.643 Moisture Saturation at Stack Gas Temperature, % 15.14 15.14 15.14 15.140
Carbon Dioxide, % 12.51 12.51 12.48 12.500 Oxygen, % 6.81 6.78 6.77 6.787 Average Stack Gas Temperature, °F 129.00 129.00 129.00 129.000 Dry Volumetric Flow Rate, dry scfm 3,363,483.4 3,274,888. 2 3,263,034.7 3,300,468.76 7
Actual Wet Volumetric Flue Gas Flow Rate, acfm 4,500,356.6 4,416,285. 9 4,405,991.6 4,440,878.03 3 Percent Isokinetic of Sampling Rate, % 103.9 105.4 104.6 104.633
F-Factor, dscfm/MMBtu @ %O2 9780 9780 9780 9,780.000

Fw 10640 10640 10640 10,640.000

Fc 1800 1800 1800 1,800.000



### Wednesday, February 02, 2011 Page 5 of 31

### Location Stack Exit - Method 29
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Location Stack Exit - Method 3A CO2
Average
Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Wednesday, February 02, 2011 Page 6 of 31

### Location Stack Exit - Method 3A CO2 3
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 3A CO2 3 6
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Wednesday, February 02, 2011 Page 7 of 31

### Location Stack Exit - Method 3A O2
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 3A O2 3
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Wednesday, February 02, 2011 Page 8 of 31

### Location Stack Exit - Method 3A O2 3 6
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 5/OTM-28
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf
Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, %
Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm
Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, %
F-Factor, dscfm/MMBtu @ %O2

Fw

Fc



### Wednesday, February 02, 2011 Page 9 of 31

### Location Stack Exit - Method 6C
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Location Stack Exit - Method 7E
Average

Run Number

Test Date

Run Start Time

Run Finish Time
Carbon Dioxide, % Oxygen, % Dry Volumetric Flow Rate, dry scfm
F-Factor, dscfm/MMBtu @ %O2
Moisture, % Fuel Type

Fw

Fc



### Wednesday, February 02, 2011 Page 10 of 31

### Emissions Summary



### Location: Stack Exit - Method 10 Compound: Carbon Monoxide Average
Run M26A-1 M26A-2 M26A-3 Elb/hr 7.27E+01 2.07E+02 2.06E+02 161.900 lb/mmBtuO2 5.23E-03 1.52E-02 1.52E-02 0.012
ppm 4.96E+00 1.45E+01 1.45E+01 11.320 ppm@7%O2 4.89E+00 1.43E+01 1.43E+01 11.163



### Location: Stack Exit - Method 10 3 Compound: Carbon Monoxide Average
Run Organic-1 Organic-2 Organic-3 Elb/hr 1.05E+02 2.78E+02 2.61E+02 214.667 lb/mmBtuO2 7.79E-03 2.09E-02 1.94E-02 0.016
ppm 7.34E+00 1.96E+01 1.83E+01 15.080 ppm@7%O2 7.29E+00 1.95E+01 1.81E+01 14.963



### Location: Stack Exit - Method 25A Compound: Total organic compounds (TOC) as Average
Run 1 2 3 lb/mmBtuO2 1.04E-03 1.94E-04 5.00E-04 0.001
ppm 6.23E-01 1.16E-01 3.00E-01 0.346 ppm@7%O2 6.19E-01 1.15E-01 2.97E-01 0.344



### Location: Stack Exit - Method 26A Compound: Hydrogen Chloride Average RunNumber 1 2 3 Mass_mg 2.84 2.44 2.74 2.673 Elb/hr 1.28E+01 1.09E+01 1.23E+01 12.000 lb/mmBtuO2 9.23E-04 8.02E-04 9.09E-04 0.001 mg/dscm 1.02E+00 8.87E-01 1.01E+00 0.972 mg/dscm@7%O2 1.01E+00 8.73E-01 9.94E-01 0.959



### Compound: Hydrogen Fluoride Average RunNumber 1 2 3 Mass_mg 0.6 0.43 0.421 0.484 Elb/hr 2.71E+00 1.92E+00 1.89E+00 2.173 lb/mmBtuO2 1.95E-04 1.41E-04 1.40E-04 0.000 mg/dscm 2.15E-01 1.56E-01 1.55E-01 0.175 mg/dscm@7%O2 2.12E-01 1.54E-01 1.52E-01 0.173



### Location: Stack Exit - Method 29 Compound: Antimony Average RunNumber 1 2 3



### Wednesday, February 02, 2011 Page 11 of 31Mass_mg 0.00028 0.0005 0.00059 0.000 Elb/hr 8.42E-04 1.47E-03 1.75E-03 0.001 lb/mmBtuO2 6.11E-08 1.07E-07 1.28E-07 0.000 ug/dscm 6.67E-02 1.18E-01 1.40E-01 0.108 ug/dscm@7%O2 6.65E-02 1.17E-01 1.39E-01 0.108



### Compound: Arsenic Average RunNumber 1 2 3 Mass_mg 0.0083 0.0122 0.0147 0.012 Elb/hr 2.50E-02 3.59E-02 4.36E-02 0.035 lb/mmBtuO2 1.81E-06 2.62E-06 3.18E-06 0.000 ug/dscm 1.98E+00 2.87E+00 3.48E+00 2.777 ug/dscm@7%O2 1.97E+00 2.86E+00 3.47E+00 2.767



### Compound: Beryllium Average RunNumber 1 2 3 Mass_mg 0.00007 0.00013 0.00012 0.000 Elb/hr 2.11E-04 3.83E-04 3.56E-04 0.000 lb/mmBtuO2 1.53E-08 2.79E-08 2.60E-08 0.000 ug/dscm 1.67E-02 3.06E-02 2.84E-02 0.025 ug/dscm@7%O2 1.67E-02 3.04E-02 2.83E-02 0.025



### Compound: Cadmium Average RunNumber 1 2 3 Mass_mg 0.00122 0.00236 0.0093 0.004 Elb/hr 3.67E-03 6.95E-03 2.76E-02 0.013 lb/mmBtuO2 2.66E-07 5.07E-07 2.01E-06 0.000 ug/dscm 2.91E-01 5.56E-01 2.20E+00 1.016 ug/dscm@7%O2 2.90E-01 5.53E-01 2.19E+00 1.011



### Compound: Chromium Average RunNumber 1 2 3 Mass_mg 0.0527 0.0854 0.0503 0.063 Elb/hr 1.59E-01 2.52E-01 1.49E-01 0.187 lb/mmBtuO2 1.15E-05 1.84E-05 1.09E-05 0.000 ug/dscm 1.26E+01 2.01E+01 1.19E+01 14.867 ug/dscm@7%O2 1.26E+01 2.00E+01 1.18E+01 14.800



### Compound: Cobalt Average RunNumber 1 2 3 Mass_mg 0.0011 0.0043 0.0012 0.002 Elb/hr 3.31E-03 1.27E-02 3.56E-03 0.007 lb/mmBtuO2 2.40E-07 9.24E-07 2.60E-07 0.000 ug/dscm 2.62E-01 1.01E+00 2.84E-01 0.519 ug/dscm@7%O2 2.61E-01 1.00E+00 2.83E-01 0.515



### Compound: Lead Average
RunNumber 1 2 3



### Wednesday, February 02, 2011 Page 12 of 31Mass_mg 0.00427 0.00357 0.00667 0.005 Elb/hr 1.28E-02 1.05E-02 1.98E-02 0.014 lb/mmBtuO2 9.31E-07 7.67E-07 1.44E-06 0.000 ug/dscm 1.02E+00 8.40E-01 1.58E+00 1.147 ug/dscm@7%O2 1.02E+00 8.36E-01 1.57E+00 1.142



### Compound: Manganese Average RunNumber 1 2 3 Mass_mg 0.0139 0.0172 0.0159 0.016 Elb/hr 4.18E-02 5.07E-02 4.71E-02 0.047 lb/mmBtuO2 3.03E-06 3.70E-06 3.44E-06 0.000 ug/dscm 3.31E+00 4.05E+00 3.76E+00 3.707 ug/dscm@7%O2 3.30E+00 4.03E+00 3.74E+00 3.690



### Compound: Nickel Average RunNumber 1 2 3 Mass_mg 0.0338 0.0694 0.0418 0.048 Elb/hr 1.02E-01 2.04E-01 1.24E-01 0.143 lb/mmBtuO2 7.37E-06 1.49E-05 9.04E-06 0.000 ug/dscm 8.06E+00 1.63E+01 9.89E+00 11.417 ug/dscm@7%O2 8.04E+00 1.62E+01 9.85E+00 11.363



### Compound: Selenium Average RunNumber 1 2 3 Mass_mg 0.2012 0.2347 0.3127 0.250 Elb/hr 6.05E-01 6.91E-01 9.27E-01 0.741 lb/mmBtuO2 4.39E-05 5.05E-05 6.76E-05 0.000 ug/dscm 4.80E+01 5.52E+01 7.40E+01 59.067 ug/dscm@7%O2 4.79E+01 5.49E+01 7.37E+01 58.833



### Location: Stack Exit - Method 5/OTM-28 Compound: Filterable Particulate Average RunNumber 1 2 3 Mass_mg 38.2 50.1 39.8 42.700 Elb/hr 1.15E+02 1.52E+02 1.21E+02 129.333 gr/dscf 4.01E-03 5.28E-03 4.18E-03 0.004 gr/dscf@7%O2 4.00E-03 5.25E-03 4.16E-03 0.004 lb/mmBtuO2 8.40E-03 1.10E-02 8.75E-03 0.009



### Compound: Inorganic (Aqueous) Condensible Pa Average RunNumber 1 2 3 Mass_mg 128 210 182 173.333 Elb/hr 3.84E+02 6.37E+02 5.55E+02 525.333 gr/dscf 1.34E-02 2.21E-02 1.91E-02 0.018 gr/dscf@7%O2 1.34E-02 2.20E-02 1.90E-02 0.018 lb/mmBtuO2 2.82E-02 4.63E-02 4.00E-02 0.038



### Wednesday, February 02, 2011 Page 13 of 31

### Process Run Data

Compound: Organic Condensible Particulate Average RunNumber 1 2 3 Mass_mg 25 5.9 6.7 12.533 Elb/hr 7.50E+01 1.79E+01 2.04E+01 37.767 gr/dscf 2.63E-03 6.22E-04 7.04E-04 0.001 gr/dscf@7%O2 2.62E-03 6.19E-04 7.01E-04 0.001 lb/mmBtuO2 5.50E-03 1.30E-03 1.47E-03 0.003



### Compound: Total Particulate Average RunNumber 1 2 3 Mass_mg 191.2 266 228.5 228.567 Elb/hr 5.74E+02 8.07E+02 6.97E+02 692.667 gr/dscf 2.01E-02 2.80E-02 2.40E-02 0.024 gr/dscf@7%O2 2.00E-02 2.79E-02 2.39E-02 0.024 lb/mmBtuO2 4.21E-02 5.86E-02 5.02E-02 0.050



### Location: Stack Exit - Method 6C Compound: Sulfur Dioxide Average
Run 1 2 3 Elb/hr 6.46E+03 4.89E+03 5.29E+03 5,546.667 lb/mmBtuO2 4.64E-01 3.60E-01 3.90E-01 0.405
ppm 1.92E+02 1.50E+02 1.62E+02 168.000 ppm@7%O2 1.89E+02 1.48E+02 1.59E+02 165.333



### Location: Stack Exit - Method 7E Compound: Nitrogen oxides (NOx) Average
Run 1 2 3 Elb/hr 1.42E+03 1.44E+03 1.57E+03 1,476.667 lb/mmBtuO2 1.02E-01 1.06E-01 1.16E-01 0.108
ppm 5.91E+01 6.16E+01 6.72E+01 62.633 ppm@7%O2 5.83E+01 6.06E+01 6.61E+01 61.667



### Wednesday, February 02, 2011 Page 14 of 31

### Process Run Data



### Run Name Value UOM Comments Target Value
1 Heat Input 0 Million Btus/million BTU using O2 0



### 2 Heat Input 0 Million Btus/million BTU using O2 0

3 Heat Input 0 Million Btus/million BTU using O2 0

4 Heat Input 0 Million Btus/million BTU using O2 0



### 1 Average Heat Input 0 MMBtu/hr 0

2 Average Heat Input 0 MMBtu/hr 0

3 Average Heat Input 0 MMBtu/hr 0



### 4 Average Heat Input 0 MMBtu/hr 0

1 Steam Output 0 1000 lb steam/hr 0

2 Steam Output 0 1000 lb steam/hr 0



### 3 Steam Output 0 1000 lb steam/hr 0

4 Steam Output 0 1000 lb steam/hr 0

1 Synfuel Firing Rate 0 1000 Tons/hr 0



### 2 Synfuel Firing Rate 0 1000 Tons/hr 0

3 Synfuel Firing Rate 0 1000 Tons/hr 0

4 Synfuel Firing Rate 0 1000 Tons/hr 0



### 1 Petroleum Coke Firing Rate 0 1000 Tons/hr 0

2 Petroleum Coke Firing Rate 0 1000 Tons/hr 0

3 Petroleum Coke Firing Rate 0 1000 Tons/hr 0



### 4 Petroleum Coke Firing Rate 0 1000 Tons/hr 0

1 Coal Gas Firing Rate 0 Ft^3/min 0

2 Coal Gas Firing Rate 0 Ft^3/min 0



### 3 Coal Gas Firing Rate 0 Ft^3/min 0

4 Coal Gas Firing Rate 0 Ft^3/min 0



### 1 Fuel Oil Firing Rate 0 gal/hr 0

2 Fuel Oil Firing Rate 0 gal/hr 0

3 Fuel Oil Firing Rate 0 gal/hr 0



### 4 Fuel Oil Firing Rate 0 gal/hr 0

1 Flue Gas Flow Rate 0 0

4 Flue Gas Flow Rate 0 0



### 1 Pressure Drop Across FGD (if applicable) 0 in H20 0

4 Pressure Drop Across FGD (if applicable) 0 in H20 0

1 FGD Scrubber Liquor pH 0 pH 0



### Wednesday, February 02, 2011 Page 15 of 31

### APCD Run Data

Process Lab Run Data 4 FGD Scrubber Liquor pH 0 pH 0



### 1 FGD Scrubber Liquor Flow Rate 0 gal/min 0

4 FGD Scrubber Liquor Flow Rate 0 gal/min 0

1 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0



### 4 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0

1 Flue Gas Oxygen Content 0 % 0



### 4 Flue Gas Oxygen Content 0 % 0

1 Flue Gas Carbon Dioxide Content 0 % 0

4 Flue Gas Carbon Dioxide Content 0 % 0



### 1 Flue Gas Moisture Content 0 % 0

4 Flue Gas Moisture Content 0 % 0

1 Flue Gas Sampling Point Temperature 0 Deg F 0



### 4 Flue Gas Sampling Point Temperature 0 Deg F 0

1 Flue Gas Pressure 0 atm 0



### 4 Flue Gas Pressure 0 atm 0

1 Standard Pressure 0 atm 0

4 Standard Pressure 0 atm 0



### 1 Standard Temperature 0 Deg F 0

4 Standard Temperature 0 Deg F 0

1 Unit Gross Electrical Output 0 Mwe 0



### 4 Unit Gross Electrical Output 0 Mwe 0

1 Unit Net Electric Generation 0 MWh 0

4 Unit Net Electric Generation 0 MWh 0

Run Name Value UOM Comments Target Value


### 1 List all emissions control devices in order of process flow. Choose from 0 0

1 drop down lists. If not on list add description and provide detailed 0 0



### 1 desription in section 5a. 0 0

Run Name Value UOM Comments
1 Fuel Higher Heating Value 0 Btu/lb
1 Fuel Moisture 0 %



### Wednesday, February 02, 2011 Page 16 of 31

### 1 Ultimate/Proximate Analysis 0



### 1 Fuel Chlorine Content 0 mg/kg
1 Fuel Fluorine Content 0 mg/kg
1 Metals Content 0 mg/kg



### Wednesday, February 02, 2011 Page 17 of 31

### Sampling / Stack Data Results Detail



### Location Stack Exit - Method 10 Average
Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 18 of 31

### Location Stack Exit - Method 10 3 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 19 of 31

### Location Stack Exit - Method 25A Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 20 of 31

### Location Stack Exit - Method 26A Average

Run Number 1 2 3
Test Date 4/20/2010 4/20/2010 4/20/2010
Run Start Time 9:28:00 AM 12:38:00 PM 3:15:00 PM Run Finish Time 12:07:00 PM 2:51:00 PM 5:28:00 PM Net Traversing Points 24 24 24 Net Run Time, minutes 120 120 120 Nozzle Diameter, inches 0.248 0.248 0.248 0.248 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.025 1.025 1.025 1.025 Barometric Pressure, inches of Mercury 29.1 29.1 29.1 29.100 Average Orifice Meter Differential, inches H2O 2.26 2.25 2.23 2.247 Dry Gas Meter Volume Sampled, cubic feet 97.682 98.025 98.453 98.053 Average Dry Gas Meter Temperature, °F 65.46 74.17 82.08 73.903 Dry Gas Meter Volume Sampled, dscf 98.410 97.142 96.138 97.230 Total Moisture Liquid collected, g 344.8 359.3 358.7 354.267 Volume of Water Vapor, standard cubic feet 16.23 16.91 16.88 16.673 Moisture Content of Stack Gas, % 14.16 14.83 14.94 14.643 Moisture Saturation at Stack Gas Temperature, % 15.14 15.14 15.14 15.140 Dry Mole Fraction 0.8584 0.8517 0.8506 0.854 Carbon Dioxide, % 12.51 12.51 12.48 12.500 Oxygen, % 6.81 6.78 6.77 6.787 Carbon Monoxide & Nitrogen, % 80.68 80.71 80.75 80.713 Fuel Factor 1.13 1.13 1.13 Dry Molecular Weight, lb/lb-Mole 30.27 30.27 30.27 30.270 Wet Molecular weight, lb/lb-Mole 28.53 28.45 28.44 28.473 Flue Gas Static Pressure, inches of H2O -0.51 -0.48 -0.51 -0.500 Absolute Flue Gas Pressure, inches of Mercury 29.06 29.06 29.06 29.060 Average Stack Gas Temperature, °F 129.00 129.00 129.00 129.000 Average Velocity Head, inches of H2O 0.7512696196 08125 0.721259583

317396 0.717879788

010599 0.730

Average Stack Gas Velocity, feet/second 52.46 51.48 51.36 51.767 Stack Cross-Sectional Area, square feet 1,429.774 1,429.774 1,429.774 1,429.774 Dry Volumetric Flow Rate, dry scfm 3,363,483.4 3,274,888.2 3,263,034.7 3,300,468.7 67 Actual Wet Volumetric Flue Gas Flow Rate, acfm 4,500,356.6 4,416,285.9 4,405,991.6 4,440,878.0 33 Percent Isokinetic of Sampling Rate, % 103.9 105.4 104.6 104.633 Percent Excess Air, % 47.0 46.7 46.5 46.733 F-Factor, dscfm/MMBtu @ %O2 9780 9780 9780 9,780.000 Round Duct Diameter, inches 512 512 512 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0
Fw 10640 10640 10640 10,640.000
Fc 1800 1800 1800 1,800.000



### Wednesday, February 02, 2011 Page 21 of 31

### Location Stack Exit - Method 29 Average

Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Wednesday, February 02, 2011 Page 22 of 31

### Location Stack Exit - Method 3A CO2 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 23 of 31

### Location Stack Exit - Method 3A CO2 3 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 24 of 31

### Location Stack Exit - Method 3A CO2 3 6 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 25 of 31

### Location Stack Exit - Method 3A O2 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 26 of 31

### Location Stack Exit - Method 3A O2 3 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 27 of 31

### Location Stack Exit - Method 3A O2 3 6 Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 28 of 31

### Location Stack Exit - Method 5/OTM-28 Average

Run Number
Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches
Fw
Fc



### Wednesday, February 02, 2011 Page 29 of 31

### Location Stack Exit - Method 6C Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 30 of 31

### Location Stack Exit - Method 7E Average

Run Number
Test Date Run Start Time Run Finish Time Carbon Dioxide, % Oxygen, % Fuel Factor Dry Volumetric Flow Rate, dry scfm F-Factor, dscfm/MMBtu @ %O2 Moisture, % Analyzer Make Analyzer Model Analyzer Serial Number Operating Range Operating Units No. Readings/Avg. Calibration Set Calibration Pre Zero Cylinder ID Calibration Pre Zero Cylinder Instrument Response Calibration Pre Zero Cylinder Bias Calibration Pre Zero Cylinder Drift Calibration Pre High Cylinder ID Calibration Pre High Cylinder Instrument Response Calibration Pre High Cylinder Bias Calibration Pre High Cylinder Drift Calibration Post Zero Cylinder ID Calibration Post Zero Cylinder Instrument Response Calibration Post Zero Cylinder Bias Calibration Post Zero Cylinder Drift Calibration Post High Cylinder ID Calibration Post High Cylinder Instrument Response Calibration Post High Cylinder Bias Calibration Post High Cylinder Drift Cavg Cavg Units Cgas Cgas Units Fuel Type
Fw
Fc Cgasw Cgasw Units



### Wednesday, February 02, 2011 Page 31 of 31