Instructions for filling Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 7. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### EIA

Facility Code Facility Name Boiler ID Test Date

1564 Vienna 8 2/23/2010 1564 Vienna 8 2/24/2010

### Fuel Type 1 Fuel Type 2

No.6 Fuel Oil (residual or bunker C) No.6 Fuel Oil (residual or bunker C)

### Fuel Type 3 Other Fuel Description

### EIA

Facility Code Facility Name Boiler ID Basis An alyte

1564 Vienna 8 As Received Higher Heating Value 1564 Vienna 8 As Received % Moisture 1564 Vienna 8 As Received % Ash 1564 Vienna 8 As Received % Sulfur 1564 Vienna 8 Dry basis Higher Heating Value 1564 Vienna 8 Dry basis % Moisture 1564 Vienna 8 Dry basis % Ash 1564 Vienna 8 Dry basis % Sulfur 1564 Vienna 8 Dry basis Antim ony 1564 Vienna 8 Dry basis Arsenic 1564 Vienna 8 Dry basis Beryllium 1564 Vienna 8 Dry basis Cadmium 1564 Vienna 8 Dry basis Chlorine 1564 Vienna 8 Dry basis Chromium 1564 Vienna 8 Dry basis Cobalt 1564 Vienna 8 Dry basis Fluorine 1564 Vienna 8 Dry basis Lead 1564 Vienna 8 Dry basis Manganese 1564 Vienna 8 Dry basis Mercury 1564 Vienna 8 Dry basis Nickel 1564 Vienna 8 Dry basis Selenium

### An alysis M ethod for each Analyte

(example: ASTM D5865-04)

D240

D482 D1552 SW 6010B SW 6010B SW 6010B SW 6010B E776/9253 SW 6010B SW 6010B D3761 SW 6010B SW 6010B D3684/SW 7471 SW 6010B SW 6010BEIA Facility Code Facility Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6 260B) 1564 Vienna 8 30B, 29, 5, OTM-027, OTM-028, 23 NOTE: NRG Vienna received alternate fuel sampling approval for collecting only three total samples. All of the fuel samples came from the same tank and the same batch of fuel.

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### FG1075-01R \ SAMPLES #1 2/23/2010 FG1076-01R \ SAMPLES #2 2/23/2010 Fuel Testing Results

### 30B, 29, 5, OTM-027, OTM-028, 23 NOTE: NRG Vienna received alternate fuel sampling approval for collecting only three total samples. All of the fuel samples came from the same tank and the same batch of fuel.

% Moisture (as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 

### 18310 Btu/lb 0.15 18240 Btu/lb 0.08% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units 

### 1.35 0.02 % <0.100 mg /Kg <2.00 mg /Kg <1.00 mg /Kg 1.4 0.03 % <0.100 mg /Kg <2.00 mg /Kg <1.00 mg /KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 

### <1.00 mg /Kg <1.00 mg /Kg <1.00 mg /Kg 1.58 mg /Kg 1.84 <1.00 mg /Kg 1.14 mg /Kg 1.39 mg /Kg 1.52 mg /Kg 2.9Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### mg /Kg <2.00 mg /Kg 13 mg /Kg <0.100 mg /Kg mg /Kg <2.00 mg /Kg 17 mg /Kg <0.100 mg /KgEIA Facility Code Facility Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6 260B) 1564 Vienna 8 26A, CTM-033, 7E, 6C, SW 0031, 18, SW 0010, SW 0011, 25A, 10, 23

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 

### FG1077-01R \ SAMPLES #3 2/24/2010 Fuel Testing Results

### 26A, CTM-033, 7E, 6C, SW 0031, 18, SW 0010, SW 0011, 25A, 10, 23

% Moisture (as received) % A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) 

### 18330 Btu/lb 0.08% Sulfur

(Dry Basis) Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units 

### 1.46 0.02 % <0.100 mg /Kg <2.00 mg /Kg <1.00 mg /KgCadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) 

### <1.00 mg /Kg <1.00 mg /Kg <1.00 mg /Kg 1.41 mg /Kg 2.89Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### mg /Kg <2.00 mg /Kg 15 mg /Kg <0.100 mg /KgEIA Facility Code Facility

Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6 260B) 1564 Vienna 8

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 

### Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt UnitsEIA Facility Code Facility

Name Boiler ID 

### Emissions test method(s) conducted at time of fuel sample collection (e.g., M3 0B, M26A, M0031 with SW-846 M6 260B) 1564 Vienna 8

Sample Number (minimum of 3 composite samples) Sample Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units % Moisture (as received) 

### Fuel Testing Results% A sh (as received) % Sulfur (as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % Moisture (Dry Basis) % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units Arsenic (Dry

Basis) Arsenic Units Beryllium (Dry Basis) Beryllium

Units Cadmium

(Dry Basis)Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units Nickel (Dry

Basis) Nickel UnitsSelenium

(Dry Basis) Selenium

Units Fluoride

(Dry Basis) Fluoride

Units Cobalt (Dry

Basis) Cobalt Units

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /Kg

### Units of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm mg /Kg