2079_Hawthorn_5A_OETM Part III notes.txt

This file contains additional information for the 2079_Hawthorn_5A_Other_Emission_Test_Methods_Part_I II.xls

General comment for all other emission test methods spreadsheet data: Since the ERT would not allow less than values entered in the res ults, the other emission test methods spreadsheet were enter in the same manner. For Data Flags DLL and BDL, the results should be considered less than values.

CO Emission Data: Method 10 entered in ERT.

Formaldehyde Emission Data: USEPA Method 316 enter ed.

CH4 Emission Data: USEPA Method 18 results entered . Run 1 bag leaked, an additional run 4 was added.

SO2 Emission Data: USEPA Method 6C entered in ERT.

Hg Emission Data 30B: USEPA Method 30B results ent ered. The measured value and the emission rate value in lb/mmBtu are an average of b oth tubes (A&B). On run 3, the tubes stuck in the probe and were broken while tryi ng to recover. No samples available for analysis on run 3 due to breakage.

Speciated Volatile Organic HAP: USEPA Method 31 re sults entered. The Rpt. Limit was substituted for Not Detected values. Compounds other than those listed in method 0031 se ction 1.1, may exhibit poor recovery from the Anasorb. In addition the laboratory method has not been validated for recovery of these additional compounds from Anasorb and the values are semi-quan titative in nature and reported as estimated. Each tube was spiked with Dibromofluoromethane, 1,2 -Dichloroethane-d4, Toluene-d8 and 4-Bromofluorobenzene prior to shipment to the fieldas an additional QC step. The recoveries of surrogates Dibromofluoromethane a nd 1,2-Dichloroethane-d4 in samples M0031-R1-TS4-C4-Anasorb, M0031-R2-TS1-C4-Anasorb, a nd M0031-R2-TS2-C4-Anasorb was outside control limits. It is not possible to re-ru n to confirm matrix or dilute for matrix using sorbent tube media. Data is reported as qualified. The recovery of surrogate Toluene-d8 in samples M00 31-R1-TS1-C4-Anasorb, M0031-R1-TS2-C4-Anasorb, M0031-R1-TS3-C4-Anasorb, M 0031-R1-TS4-C4-Anasorb, M0031-R2-TS1-C4-Anasorb, and M0031-R2-TS2-C4-Anasor b was outside control limits. It is not possible to re-run to confirm matrix or dilute for matrix using sorbent tube media. Data is reported as qualified. Each tube was spiked with Dibromofluoromethane, 1,2 -Dichloroethane-d4, Toluene-d8 and 4-Bromofluorobenzene prior to shipment to the fieldas an additional QC step. The recoveries of surrogates Dibromofluoromethane, 1,2-Dichloroethane-d4, and Toluene-d8 in samples M0031-R2-TS3-C4-Anasorb, M0031-R2-TS4-C4-An asorb, M0031-R3-TS1-C3-Anasorb, M0031-R3-TS2-C4-Anasorb, M0031-R3-TS3-C4-Anasorb an d M0031-R3-TS4-C4-Anasorb was outside control limits. It is not possible to re-ru n to confirm matrix or dilute for matrix using sorbent tube media. Data is reported as qualified. Each tube was spiked with Dibromofluoromethane, 1,2 -Dichloroethane-d4, Toluene-d8 and 4-Bromofluorobenzene prior to shipment to the fieldas an additional QC step. The recoveries of surrogates Dibromofluoromethane, 1,2-Dichloroethane-d4, and Toluene-d8 in samples M0031-BT-TS1-C4-Anasorb and M0031-Trip Blan k-TS1-C4-Anasorb was outside control

Page 12079_Hawthorn_5A_OETM Part III notes.txt

limits. It is not possible to re-run to confirm mat rix or dilute for matrix using sorbent tube media. Data is reported as qualified. Since the surrogates wer e high, there is a high uncertainty of the data and the results may be bias ed.

Speciated Semi-Volatile Organic HAP: USEPA Method 0010 results entered. For Data Flags DLL and BDL, the results should be consideredless than values.

HCN Emission Data: USEPA Conditional Test Method 0 33 results entered. Run 1 failed pH criteria, an additional run 4 was added. A high spike recovery may bias results, but all results were ND (non-detects).

HCl Emission Data: Method 26A entered in ERT.

HF Emission Data: Method 26A entered in ERT.

NOx Emission Data: Method 7E entered in ERT.

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