. . . . ,

• ... CARGILL,.· 

INCORPORATED· . 

·>SICUX CITY,- IOWA .... 

. ;j 

EMI·SSI.ONSTEST... 


RESULTS ". 


. '. . 

... ' .FROM TESTING CONDUCTiED: 

•. ..... Dl.=CEMBER '7-10, 14-16 1999 

. ' .. 

.... Thompson Environmental Consulting, I,nc. '. .' 11' t ... 

a member of THE COMPLIANCE GROUP 

• 


Environmental Engineering, Permitting rutd Compliance $eroices 
• 


.; 


EMISSION TEST REPORT 


for the 


Cargill Incorporated 


Soybean Processing Plant 


located in 


Sioux City, Iowa 


on 


December 7~10 and, 14-161999 


Conducted by 

Comprehensive Emission Services 


1112 Maple Street. 


West Des Moines, Iowa 50265 


(515) 225-7372 


Project No. 8899 

• 

'. TABLE OF CONTENTS 

CONTENTS 

Preface....................................................................... : ................................................ 2 


Introduction................................................................................................................3 


Summary ofResults ...................................................................................................4 


Salllpling and Analytical Procedures .........................................................................9 


Particulate Emission Results ......................................................................................12 


M5 Sampling Apparatus ............................................................................................10 


M17 SaltI.pling Apparatus ....................................................... ; .................................. 11 


Appendix A" Example Calculations 

Appendix B- Laboratory Data Forms 

Appendix C - Field Data Forms 

Appendix D - Pretest Calibrations 

Appendix E - Posttest Calibrations 

Appendix F - Process Data . 

Appendix G ~ Opacity Observer Certification 

TABLES 

Table 1, Summary ofTest Results Bean Dust Bag Filter (EP #2) ...........................4 


Table 1, Summary of Test Results Grain Dryer (EP #21) .......................................4 


Table I, Summary ofTest Results Grain Dryer II (EP #22) ....................................4 


Table 2, Summary of Test Results Hull Grinding (EP #4) .......................................5 


Table 3, Summary ofTest Results Meal Dust Grinding (EP #6) .............................5 


Table 4, Summary of Test Results Bean Tank Conveying (EP #11) ........................6 


Table 5, Summary ofTest Results Flaker Aspiration II (EP #13A) .........................6 


Table 6, Summary ofTest Results Hull Transfer Storage (EP #15).........................7 


Table 7, Summary afTest Results Pellet Transfer (EP #20) ....................................7 


Table 8, Summary ofTest Results Bean Conditioner (EP #27) ...............................8 


Table 9, Stunmary of Test Results Pellet Cooler (EP #28)............................... » ......8 


FIGURES 

.' 


Figure 1, M5 Saxnpling Apparatus ................................................................. · ........... 10 


Figure 2, M17 Sampling Apparatus ..........................................................................11 

• PREFACE 

This report slll!1.IIUU'izes the results of the data collected for compliance testing performed 

at the Cargill Incorporated plant in Sioux City, Iowa To the 'best of our knowledge, the 

data in this report are accurate and complete. Any questions concerning this report 

should be directed to Mr. Tim Titus or Mr. Jay Titus. They may be reached by phone at 

(515) 225-7372. 

Jay Titus 


h 

Test Leader 


• 

',,­

\ 

December 17, 1999 

• 


2 
• INTRODUCTION 

Emission testing was conducted by Comprehensive Emission Services on the following 

sources using the corresponding methods. Testing was conducted at the Cargill 

Incorporated plant, Sioux City: 

E.P. #2 - Bean Dust Bag Filter, Method 5 with 202 backhalf, TSP and, Opacity. 

E.P. #4 - Hull Grinding, Method 5 with 202 backhaJf, TSP and, Opacity. 

E.P. #6 - Meal Dust Grinding) Method 5 with 202 backhalf, TSP and, Opacity. 

E.P. #11- Bean Tank Conveying, Method 5 with 202 backhalf, TSP and, Opacity. 

E.P. #13A - Flaker Aspiration II. Method 5 with 202 backhalf, TSP and Opacity. 

B.P. #15 Hull Transfer Storage. Method 17 with 202 backhalf, TSP and Opacity. 

E.P. #20 - Pellet Transfer, Method 17 with 202 backhalf, TSP and, Opacity. 

E.P. #21 - Grain Dryer, Opacity. , E.P. #22 - Grain Dryer II. Opacity. 

E.P. #27 - Bean Conditioner~ Method 5 with 202 backhalf, TSP an~ Opacity. 

E.P. #28 - Pellet Cooler, Method 5 with 202 backhalf, TSP and, Opacity. 

The test results for these sources appear in order by emission point number. The testing 

was performed on December 7-10 and 14-16. 1999. 

Coordinating the field tests: 

Tim Titus - Comprehensive Emission Services 

Lisa Schmidt - Thompson Environmental Consulting 

Conducting the field tests: 

Jay Titus - Comprehensive Emission Services 

Chad Siems ~ Comprehensive Emission Services 

Mike Ankerstjerne - Comprehensive Emission Services 

Dan Deatsch - Comprehensive Emission Services 

Brad Buckley - Comprehensive Emission Services 

Doug Ostrander - Comprehensive Emission Services 

Witnessing the field tests: 

Aaron Wauters ~ University ofIowa Hygienic Laboratory 

Matt Lyon - University ofIowa Hygienic Laboratory 

The appendices to this report contain the following infonnation and data: 

Appenclix A: Example Calculations 

•

Appendix B: Laboratory Data Forms 

Appendix C: Field Data Fanns 

Appendix D: Pretest Calibrations 

Appendix E: Posttest Calibrations 

Appendix F: Process Data ,.

J ' Appendix G: Opacity Observer Certification 

3 
I 

SUMMARY OF RESULTS I­

! .' In accordance with current IDNR protocol, when less than 10 mg of sample is collected,

I 


10 rug ofsample catch is used for calculations. Sources with sample collections less than 1 • 

10 mg are shown with a '<' symbol in the following tables to indicate that actual samples 

were less than the assumed 10 mg catch. Both the actual and the assluned emission rates 

can found in Appendix C. 

I 

, 

I 

1 

I 

I 

~ . 

, 

! 

~ . 
-. Table 4 summarizes the test results for testing performed on the Bean T auk Conveying 

(EP # 11) at the Cargill Corporation facility in Sioux City, Iowa. EPA Method 5 with 202 

backhalf, TSP and, Opacity were used for testing. PMIO emissions will have to be 

assumed from the TSP samples for this sources. Testing 'Was performed on December 9 

and 10, 1999. The teSting fulfills the requirements for testing in the IDNR Permit # 95­

A-324-S3_ 

The allowable limit for TSP is 0.006 gr/dscf and 1.40 Iblhr. 

The allowable limit for PMlO is 0.003 gr/dscf and 0.60 Iblhr. 

The allowable limit for Opacity is 0% . 

. Table 4 


S.uBllnary of Test Results 


Bean Tank Conveying (EP #11J 


units Run 1 Run 2 Run 3 

Particulate Net Weight g <0.0100 <0.0100 <0.0100 

Particulate Emissions gr/dscf <O.QOll <0.0012 <0.01)11 

Particulate Emission Rate lblhr <0.25 <0.26 <0.25 

Opacity % 0.0 0.0 0.0 

_Flow Rate dscfin 26,877 25,941 26,033 

Flow Rate acfm 27,093 25,784 25,763 

Isokinetics % 99.0 95.7 98.5 

Start Time HltMM 8:50 . 13:17 7:22 .­ , ---.:; 
• SAMPLING AND ANALYTICAL PROCEDURES 

Sampling Procedures 

Particulate emissions were determined by U.S. Environmental Protection Agency (EPA) 

Methods 1,2,3,4,5, 17 and 202. These Methods are titled; 

Method 1 - "Sample and Velocity Traverse for Stationary Sources" 


Method 2 - "Determination of Stack Gas Velocity and Volumetric Flow Rate" 


Method 3 - "Gas Analysis for Carbon Dioxide, Oxygen, Excess Air and Dry 


Molecular Weighttl 

Method 4 - "Determination for Moisture Content in Stack Gases" 

Method 5 - "Determination of Particulate Emissions.from Stationary 

Sources" 

Method 17 - "Detennination of Particulate Emissions from Stationary 

Sources, In-Stack Filtration Method" 

Method 202 - "Condensible Particulate Emissions" 

These methods appear in detail in Title 40, Code of Federal Regulations (CFR), Part 60, 

Appendix A, and Part 51, Appendix M. 

• 

The Sampling Apparatus is shown in Figure 1 on Page 10. All equipment was calibrated 

at Comprehensive Emission Services' office prior to shipment to the test site, 

. Sampling Locations 

The stack sampling point locations can be found along with the fieLd data sheets in 

Appendix C. 

Analytical Procedures 

The particulate emission rate was detennined following procedures detailed in EPA 

Methods 5 and 202. Particulate samples collected on Whatman glass fiber filters were 

analyzed gravimetrically. The probe and nozzles were rinsed with acetone. The rinse 

was transferred to tarred beakers and evaporated to dryness. The back-half water was 

collected and separated into organic and in-organic parts. The samples were then 

transferred to tarred beakers and evaporated to dryness. 

• 

9 
• • • 

Probe 

Nozzle 

S Type Pitot Tube 

Thermocouples Fine 

AdJus.t 

Orifice 

Meter >, 

Leak Free 

Pump 

Schematic of Method 5 Sampling 

Figure 1 

Heated 

Filter 

~ Ice. Bath 

Vacuum 

Gauge 

Train 

Exit Temp 

Sample Line 
• • • 

Stack In-stack: ThermocoupIe Filter Sample Probe 

Probe 

Nozzle SType Pitot Tube 

Thermocouples 

Orifice 

Dry 

Gas 

Meter 

SC/lematic of Method 17. 

. Ice Bath 

Sample line 

Fine Vacuum Adjust Gauge 

Leak Free· 


Pump 


Sampling Tra in 
• Particulate Emission Results 

Bean Tank Conveying (EP #11) 

Parameters Units Run 1 Run 2 Run 3 

TSP Emissions 

Actual gr/dscf <0.0011 <0.0012 <0.0011 

Weight Collected g <0.0100 <0.0100 <0.0100 

Emission Rate Iblhr <0.25 <0.26 <0.25 

Opacity % 0.0 0.0 0.0 

Stack Flow Rates 

Velocity ftImin 3,440 3,274 I 3,271 

Actual acfm 27.093 25,7&4 25,763 

Sta.ndard Conditions dscfin 26,877 25,941 26,033 

Sampling Results 

Isokinetics % 99.0 95.7 98.9 

Sample Volume dscf 143.716 134.137 139.028 

Ave. Stack Temperature OF 63 56 56 

Ave. Square Root AP inchesHzO 1.0195 0.9772 0.9772 

Ave.AH inchesH:p 1.46 1.38 1.38 

Ave. Meter Temperature OF 88.3 89.9 89.9 

Oxygen % 2l.00 21.00 21.00 

Carbon Dioxide % 0.00 0.00 0.00 

Moisture Collected m1 28.5 27.0 15.0 

Moisture % H20 0.9 0.9 0.5 

Run Start Time HH:MM 8:50 13:17 7:22 

Sampling Time minutes 240 240 240 

.> 


• 


15 
• 


AppendixA . 

Example Calculations 

' •.' 
• S'lIDbol 

acfm 

As 

Bws 

C, 

~. 

DII 

dscfm 

gr/dscfrn 

ID 

Md 

Ms 

~ 

Ph 

P, 

SF 

• 

Tm 

Ts 

Vi 

V, 

Vf;l 

VI1'IM 

Vs 

W~ 

\VtE.=':' 

Y 

e %

H2O 

% COl %O2 

%1 

liH 

liP 

• 


NOMENCLATURE 

Descriptio.n 

Actual cubic feet per minute 


Area of stack 


Percent water 


Pitot rube. calibration coefficient . Concentration of particulate dry basis, standard conditions 

Diameter of nozzle 

Dry standard cubic feet per minute 

Gzains per dry stancwd cubic feet per minute 

Inside diameter of stack 


Molecular weight, dry stack gas 


Molecular weight, stack gas 


Stack flow rate, dry standard conditions 


Barometric pressure 


Stack pressure 


Static pressure 


Average meter temperature 


Temperature of stack gas 


Initial meter reading 


Final meter reading 


Volume meter, actual 


Volume meter, standard conclitions 
 Average stack gas velocity 


Total moisture collected 


Total particulate matter collecred 


Meter correction factor 


Sampling- rime 


Percent moismre by volume 


Percent carbon dioxide by volume, dry 


Percem oxygen by volume, dry 


Percent isok:i.ietic 


Pressure drop across orifice meter 


Gas velocity pressw-e 
PARTICULATE CACULATION EQUATIONS 

Run I 

1. Volume of meter 

Vol =(1036.655 - 842.400) x ].003 

V,;, =:; 194.838 fl3 

2. Volume of meter, standard conditions (68" ,29.92 in.Hg) 

. (.AH) 17.65x Vm x p" +­13.6 

T17I +460 

( . 192) 17.65x194,838x 29.96+-'­

V = 13.6 

lII(ml) 75.2 + 460 

3, Percent moisture by volume 

B = lOOx0.4707x We 

lIl< 0.04707 X We + V"'($/d) 

B :=:. 100x 0.4707 x47.0 

"'.. 0.04107 X 47.0+193.394 

4. Molecular weight, dry stack gas 

Mti =O.l6xO.OO+21.00+28.0 

Md =28.84 
5. Molecular weight, stack gas 

M:=. MdX(l- Bws)+18X(1~ B~) s 100 100 

M ",,' 28.84X(1-~)+18X(1-..!..:!.) s 100 100 

Ms = 28.72 

6. Stack Presure 

P == 29.96+ 0.05 
 s 13.6 


.1 1'.. = 29.96 inch. Hg 

1. 	 Velocity of stack gas 

T +460 (JKP) V. = 60x 85.349 xC x 	 S X An .. . p 	 P +M or ",'g S .Y • 

78+460 

Vs = 60x85.349xO.84x 	~ X 0.7260

29.96 + 28.72 

Vs =: 2,472 ftlmin 

8. 	 Percent isokinetic 

100 x (Ts +460) x Vm($/rl) %1 == ----......:....:..--~~::.:.::..<----:

17.65x8xV.xp X(l-:- B.... )X7rx(DII )2 •. • 100 	 24 

%1 = lOOx(178+460)x193.394 

17.65x 240x 2,472 x 29.96X(1 ~)x 7rX (.250)2 100 24 

%1 =: 98.0 
9. Area of stack 

A = 1t' X(ID)2 s 	 24 

A = 1t' X(30.00)2 s 24 

10. Stack volummetric flow rate actual conditions 

Qa =2,472 x 4.91 

Qa "" 12,136 actin 

11. Stack volununetric fiowrate, standard conditions (68" , 29.92 in .Hg) 

17.65x 2,472 x 4.91x 29.96 X (1- 1.:!.J 100 

QSIJ. == 78 + 460 

Q.flJ = 11~803 dscfm 

12. 	 Grains per dry standard cubic feet 

15,43 x Wt8,,;)1 

== ---=­

15.43xO.OllO = 

• 

Cs1d 193.394 

em! = 0.0009 gr/dscf 
13. Emission rate 

• 1b 60x Wtgaiu X QSld 

- = 

hr 453.5924 x V.,(~<f] 

Ib 60x O.Ol10x 11,803 - = hr 453.5924x 193.394 

Ib ;::: O.091blhr 

hr 

• 


• 

• 


AppendixB 


Laboratory Data Forms 


• 


• 

<:-c;. 1<1 

• 

Project 

Plant Name: 

Number: 

. Lqlji 

:---u~~ 'f --:!-,;,.-I

StUff 

---r-,;--­

r C;/ r'1 


Date: IJ. _/'VY r 


Analy.sis Type: _.....Jt:.......)~p_____ 


Run I £PI/ 

Type Identification Final Tare Net 

Number Weigbt Weight Weight 

Filter F S'Gj 11 0:rtr. .3.0:<77 0, ()OOD 

PIobe Rinse ( ml) trfd-.i- C/l. 9~J0 L C!-/, 7l-/~ r 0,0012 

Organic ( ml) C (\ 1. q iO'. Li"f5~ Iat.c-f 1- 0/ O,OO}() 

Inorganic D 1 <J G~I n1,95J7 i~ 1-. 1{,/~ 4 010053 . Total Net Weight O,OOY,SRun Z 

Type Identification Final Tate Net 

Number Weight Weight Weight 

Filter p Cf~} 510)~}:< JI O:J. J i 010003 

PIobe Rinse ( ml) .t}9-2~ 1f. 0I~'i t7-1 0/3r 0, Dory 

Organic ( ml) C 1\') 0 )0 ?,~10, JOJ/1/~f O. 00' t-f 

Inorganic 01,Ob) J5'. l-Jc,/1' IS" L../ lrIS3 O,OO~J 

Total Net Weight 0.0011 

Run 3' 

Type Identi fication Final Tate 

) 

Net 

Number Weight Weight Weight .~ 

Filter F ?; 1o 3,0(1,2 ).0/9) O.OOO{) 

PIobe Rinse ( mI) .e/:;2<? £t, 'b2~ I tt. C[J.:{"f _at 00 I~ 

Organic ( mI) C 1/ 'j ) )0 '6, 5~ 11 10'/, y}?? ()I OO( 3 

Inorganic o"Z'fJ G.6 l~t.~3i-' l~tl ~3~1 DIDO» 

Total Net Weight O. GO~2 Blanks 

Type Identification Final Tare Net 

Number Weigbt Weight Weight 

Water Blank ( ml) 

Acetone Blank ( mI) 

MeC~ Blank ( mI) 

O../l(}l), 

• 

• 

Identification 

F ~ 3 inch ruter P '" 47mm filter B - 150m] Be<lktr C c 250m) Beaker D" 400ml Beaker
FINAL WEIGHT 
 • • 

WEIGHING SHEET 


'•. 

Time ,b: ') Ii 

Date 

Analyst 

ID No. Run 

1 2 

5. oL( !f3 

).oV6{/ 

3('3 1. D"3 91 

3.DI tb J.OIU,g 

3. D 3S-.;2 ;z 

,.f;;? 1. 

'3JO) 1..j;;;Z I.:;;. o..z t/~ 

·3.DZ'ifC( 1:3·0290 

'3.0 z','1- !). 0:1 "3 ? 

'3 _;7 2 T;-3 /5.02 

;;.O'Ob 

Check WeiglJ! )J' C' <J '3 pO'S .:2_ 

Check Weight 

Check Weigh! 

Check Weight 

Wci!:hing (grams) 

J <I 5 

Average 

Fin:.' 

WCil:ltl 

=-c 

E 

S 

Tare 

Weight 

Net 

Weight 

COMPREHENSIVE 

EMISSION. 

SERVICES 
• 

FINAL WEIGHT • • 

WEIGHING SHEET 

Time I }t1:)O

Date 

Analyst 

In No, Run I I 1 

"1 /" 5-&-(;. ...... ' IT' -

Cbeck Weight 5,6'0 5') 

Check Weight 

Cbeck Weight 

Check Weight 

, I I 

Weighing (grams) 

2 J 4 

5.()o{ 2, 

5 

=-c­ -

- --­ --­ - -­ - E 

S~ 

COMPREHENSIVE 

EMISSION 

SERV[CES 
• 

FINAL WEIGHT 

• • 

WEIGHING SHEEr 

Time 1'= /5' ,a;I-H 

Date 

Analyst 

10 No. Run 

1 2 

j·G·.01;2 ~ 1+&,O~2 D 

66, 'z <-iI? !?b. <: I{ f dWeighing (grams) 

3 " 

Weight 

5 

1t. /J!3 ?6~ 1/ 0 

6;, f,01./ b-r;-"-bO~'-:;-!.-'-1-1--­ I " _. ~. ~ '. -1-----1---.:.----1 

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t'r 

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/ ~,'1 3 t.?), f:, 1?{/ ;J.. 

CheclcWejghl ~) ':}·jl-I :}S,0;2LI3 91,ol~((/ 75.0).Q2. ~ C 

Check Weight ~~n'1 S . bb, '3 '11 '3 66. ')::t-o C; ~,. 31- II COMPREHENSIVE E 

EMISSION 

Check Weight =1.0.r.i1 16 1-0. 0 71 S _ .S SERVICES 

Check Weight 

......,..........,,, ........ . 

• • 

---- -- --- -- ----

FINAL WEIGHT 


, WEIGHING SHEET 


_ --- E---- --­

- S~ 

• 

I 

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Dnte 

Analyst 

10 No. Run 

S r'?-3 I:. 

11- 31' 

/rJf: 

? 1I'2'? 

11"5 47 

II 3 I 

II '3 'Z 

j/J) 

~,.,':;-~I .dJI 

I} '3 

J/3b 

lr~ 1-

Check Weigbt 

Check Weigh! 

Check Weight 

Check Weight 

}6:/tfl lo;'(tl 

Weighing (grnnls) 

1 2 J 4 

b>- r:l.'1-;Z !6j'.IZt{r 

6"J .G5'';jt/ 

9'i~ '/30:2 

lo6,l(l-56 

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Ip 1. () 'fr{:t:t 

loq.ifl5'1 

/0),o6tfJ.... 

()D. ()t~+6 Ir00.0017 

5 

10J, So 

=-C 

Weigltt 

i

I 

! 

COMPREHENSIVE 

EMISSION 

SERVICES 
• • • 

FINAL WEIGHT 


WEIGHING SHEET 


i 

'Time 

Date 

Analyst VL-f ( """ ., . l -" Weighing (grams) 

ID No. RlIn ~-

..,­

G 

Check Weight /00, 

Check Weight 

Check Weight 

Check Weight 

3 4 

Final 

5 

=.c - ­.--­ -

~ --- --­ = -­ E=--­ -­-­ ---­ ==­ --­ S­- ---­ -

Weigbt Weight 

COMPREHENSIVE 

EMISSION 

SERVICES 
• • 

- --- - --- -- --- -- --

FINAL WEiGHT • 

WEIGHING SHEET 


Time I J6 :00 

Dale 

Analyst 

Wd~hing (grana) 

m No. RUn 

I 2 J_3 4 

J) ZD0 1/ tt'7~ 9536 

t.tO (15 )S{ l(t/CP/ 

?o?b lri~(;'")_~l? )16'1<659B 

2.0 I)t(, 02 03 

'20bfr 

ta6 

'2. 0 7-p 

7.0 '1-/ 

(.0::; 2. 

7...aJ 7" 3 

-C 0 l' "/ 

(:) -:; -;j 

Check Weight 

'Check Weigh! 

Check Weigh! 

Check Weisht 

5 

Weight 

:.- c---­ - --- COMPREHENSIVE 

--- E---- EMfSSION 

S SERVrCES 
• 

FINAL WEIGHT 


• •

WEIGHING SHEET 


Time 

D:llc 

Analyst 

ID N G. RUIl 

2 

"I O'i G. '1 () . ~ i1;- I II 7- o. 6 

I f 20 1-7-1 1/6. 1,.-jif'9B!/69,1¥'1 

Weighing (gram.';) 

J 4 

I J .". '. ' j,b'7. 7 )'fY 

{, f:r •{(f;1 r 

c..of) 0 

Zo"6-/ 

Check Weight (to_>i.131'llt9-o,o311 

Check Weight 

Check Weight 

all:ck Weight 

5 

~c 

E 

S 

COMPREHENSIVE 

EMISSION 

SERVICES 
FINAL WEIGHT 


• • 

WEIGHING SHEET 


(. 

Time 

Date 

Analyst 

I --, 

m Nu. Rml 

1 2 

Check Weight 51 00::;2 

Check Weight 

Check Weight 

aleck Weight 

7",·'°: (g.~..~) 4 5 

Final Weight Weight 

_. '" I' 'G/ ~ l • 

=-c­ =-

-- E-=-­ ==:. -= :==.. S -=: 

COMPREHENSIVE 

EMISSION 

SERVICES 
• 

FINAL WEIGHT 


• •

WEIGHING SHEET 


Time I ~:po 

Date II). -).{l-¥' 

Analyst ..... L J \I 

In No. Run 

1 

Check Weight 

Check Weight 

Check Weight 

aleck Weight 

1/5: 6"0 

I 

Weighing (gram",) 

2 3 4 5 

COMPREHENSIVE 

EMISSION· 

SERVICES 
• 

FINAL WEIGHT 

• • 

WEIGHING SHEET 

Time 

Date 

Analyst - L J \. I 

Wciglling (grams) 

lDNo. Run 

1 2 j 4 5 

Check Weight 

=­ C COMPREHENSIVE - - E EMISSION 

S~ SERVICES 

Check Weight 

Check Weight 

Check Weight 
• 

FINAL WEIGHT • • 

WEIGHING SHEET· 


Time 

Date 

Analyst ......­ It. , .. - - I , 

[DNa. Run 

1 2 

Check: Weight f.(Ic{i; rLf II f~039) 

Check Weight 

Check Weight 

Check Weight 

Weighing (gr:uns) Average 

Fimd 

l 4 S 

-C­---~ - --­ = 

-­

-­ E=--­ -­

-­

-­ --­ -­-­-­

==­ --­ --­ s-=--

Tare Net 

Weight Weight 

COMPREHENSIVE 

EMISSION 

SERVICES 

.. 
•••• 

\{:'~.':.:": t<". '" P:"· r.::-. 0,",' .;:..... "" 

TARE WEIGHT 


WEIGHING SHEET 


Time 

Dale 

Analyst 

ID No. 

Check Weight 

Weighing (grams) 

3 4 5 

Average 

COMPREHENSIVE 

EMISSrON 

SERVICES 

:.c ­ :::. E 

-- S-:::: ====- ':; 
- --- -- ---

•••• (::.;-;';.• "')' 


TARE WEIGHT 


WEIGHING SHEET 


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Dnte 

Analyst 

m No. 

F~66 

;:<f>b 7­

r B'615 

Oeck Weight I S. 

Weighing (gr:lltls) 

2 3 <I 5 

=c- - .--­ COMPREHENSIVE

--=- - E--­-- EMISSrON 

==.. --- S-­ :=:=:=.. -= --- - SERVICES 
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r.q ~ t:.l 

~ -r" l:vJ 

~ ,. 
0~· f':::•••• '.'., ::. :,:It


TARE WEIGHT 


WEIGHING SHEET 


Time 

DlIlc 

Analyst 

IDNo. 

Check Weight 

Weighing (grams) 

3 4 s 

COMPREHENSIVE 

EMISSfON 

SERVrCES 
•

:: .; 

• 


0 ~ ~ --­ M-. 0--. r).. 

~ ~ ~ f'i ; <I> ~ =:t- I:JJ D­ iY) e <J-.. ~ ~ 'X v~ ~ "­ I'( 

~ I~ 't: a: <I> \:l ... ()... \~ (J V:> "­ 'I' -< fr. \10 ~ 'C

~ l'( ~ \.r{ ~ ~ 

-~ ~ if ~ ~ ~~ 

1:::: \(; rr­ \Cl 'Q f),. li­ \\) '0 N-. 

V} 

'1:1' 

,-. , 

'" ::: 

~ .s 

ell ..., .f: 

~ .., 

~ 

rt.. N (YJ ()'-­ ~ M-. \I) r-{ 

~ ~ (J :::r­ \() ~ \r­ - 0--... ::::,. '\Y1 \'i 

-­ ~ 

~ Y\ ........ ~ ,I ~ (}-... 0­ t't\ ;::;... -.. \'( t'< ~ -­ M ('4 \'t'>

\: "­ \.(', <J- Vv (Jt-­ \:). \:p i IS ~ c:J 0 ~ 

" ~ ...t) "'c cr-: \.r) ~ t..: '-f) ~ ~ V\ '..l \,r~ tS f\-. ~ f1­ -J) '-C.J rf.. ---t !1-­ \..(} \.J:) {r.. t}. 

I~ Ii '-t; \f.. ~ <:J'-. \0 ~ ~ ~ - ('0 ::r-­

<:t- O­ --­ ~ ::r­ \i, '; I~

~ ~ '\f1 1:2 \:: .... ~ \}-.. g: ~ ~ '­ ~ N '.t -­ r.... 

~ '"­ V> ~ \:t-­ \) , , \)::l :::r­ ~ '{, ~ \:4 ,r) ~ ~ ($. 't V\ ~ n­ ~ ~ "-1:>' vi -.".,'

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~ rv­ > 

lS 

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~ C> f0 '01 '" oJ ..s >. N N r1 r6 M {Yl E Z :l:: ~ 

c; Iii r\­ r\-­ rn Ii­ Cl s:; Cl f}. .I< \'1-­ \i--. '~ 0-­ ~ \t­ fi... u -< - I~ ....... fi­

-­

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--­ "­ "" -.. -.. -... "­ e

" -:2 
• 


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<i 

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<: 

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.2 

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,

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 - - - -. -

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6 - "­ -... '\j ..:"­

,­
• (:r>t. , , 1~' :'..:.~ ::'.\ 

TARE WEIGHT 

'WEiGHlNG SHEET 

Time 10: 1·0 

O:l(e ,,)0 1-/ tj'r:r 

Analyst -rr 

ION,,_ 

I 

;;//3 fr I o(}. 50"9- 3 

11;9 /1)t{.. l{o'ft.{ 

1/10 I oL{Jr :rJ. LJ 

1/'1/ Jol.{.o(06 

//t/2. /lO.:f/33 

IILI) lo3,fr1)' {, 

)jl/L/ to3, l1ffr9 

1191 IOO~ S1f}o 

//L/6 105. tj)'1iIjL/? 105. 0 6t'.Jt.( 

/)1,1<6­ Jot(. il'!16 

~ JJIjq J(J fC3 I ff'tr 

Check Weight L­/1(10;00 ?--fJ 

/ c;: lj 0 

I L.-/o "­

-r/ 

Weighing {gram£} 

2 3 

10;?, £O6&' 

lotf, l.{oc;rs 

I p r. fJ""1-Z ~ 

I (Jtl. 0101­

Jf(). "-7-/2. f( 

/01 {;-3;:;:J 

IflY. I.g-&<; 

It?c1.. .5-;!;1:3 

i 05.5) -:r3 

{oS, 0690 

/01(., 'lll!:Z 

! 0 6: 7 j 'f:r::;­

/t?G7. 0t7 :t1­

•

Average 

4 ' 5 I 

I 

/O;;? )0::;-/ 

lot(. '1095 I 

10,/, &- 1·;;2-6 I 

/.() 1/. 0 10 =t-­ j 

If0» :;-1'3 I I 

/03, '5-3::z5 l 

/03. /15-6-9 j 

1/<00. <5 '6-1(}. 

/175,5:,( '3 S I 

/o5.ot9;;( 

/0'1, 'ltllf 

JOf;-~ J1'f5-'6­

==- C COMPREHENSIVE 

- E EMISSION 

S~ SERVICES 

,"_." 
t::':':: ~, •

" t:,':':\. 

l",.,',' ,,:,,':'. " "," 

TARE WEIGHT 


WEIGHING SHEET 


Time I Js~'l2o I It'':' c? 0 

Dnlc ~11 if+? 1/~IIDlr1' 

Analyst 11 ' I 1/ 

Weighing (gnlllls) 

lnNo. 

t 2 3 

L.-lf5o ItJ'(·r, -; 1- V()f{,95l.fo 

}) ') / /C'b,Of991f06J'>'?O« 

I) 52. Ic.t'9'1?"1-II03; 7-9'3 J 

1J5 "3 }O(.$Obb llt>t.509-0 

J1sJ/ 10', l.-/ffS 6 1103, o/ff6/ 

1[5{ J[oS.VI17 110 5... '3'50:> 

Jjfj, 1(}6. fOJ,J::1­ !ltJb~ f; Z "3/ 

J/~7- I()(._'i~ " I;o!.t/5III 

1/5.:(; J!£e'-Ji-J-l £I 1/00. ~113 

Hif f06. 0.2!~ 1/06__ q_I~J 

1/6' loff. (r!, <ill 1(0'0.0"3 '7 -r 

)/ 1/6! /05, tftlJ<j 1105. If '[rtf I 

Check Weight !Joo.oC'·::rllfI10.oo1'1 

4 5 

Average 

)/01(, '75:5 <7 

10&_ o~o~ 

10J. 1-9 z 9 

110 /" 5' 0JG'5­

/07. 'f-tr>_ '1 

/05. ~5@j 

l!~6- if;{::<. '1 

/0(_ '15/3 

/.00, "fi-_t-I;{ 

lo6~ 0 '9~'i 3 

/o'ii. 03?6 

1/05_ o/'6-/fO 

COMPREHENSIVE 

EMISSION 

SERVlcns 
/?'!.• ': ~':' ..:" -.. ,~~'.. t··::· .-•.. \, ::,': ._. .... '

, 

TARE WEIGHT 


WEIGHING SHEET 


Time I j 0; I() /6 ;"1 p 

Date I rzJ!>.!JJj 112-/ G 1./ f[Cf 

Anlllyst ff -rr 

Weighing (grnms) 

ID No. 

1 2 :> 

D 1.. o 5l-( 'b~.of1cr If6'l,O-l5L{ 

(jJ 55 1/66, f9/fS 116(,,1110 

2-oS(. tb;(. fr:t13 1/6 :2, ~1-Z '1 

ZO 51'_ /53, -&-63B I If], '¥6 '3 3 

-Zo,<fr I&?-. 6b'1~L IJ6-7. £.6 ryO 

7..oS9 J63,tfSt{rtj !/63.t-f51rtO 

LobO I/GJ, Z)'d-;L r/6.7. z,-:ri­

'2-061 /l66"l{3l(O II6rG, l/'33b 

z.66:1 /16-1. 'l3 0 LJ 1/{:'1, ;;t;;1J[1. 

Zob3 1b6, zb 1. q 1/[.6, 1-G-C0 

_ILL 7..,.a 6 q 11:."-1.9'1 '8" ,[61-; 9 t{ (f~ 

W/-Z-O b5 I56Jll/55 I)56, iF-!, I 

Check Weight IlrO. 051' '3 !1'1 o. p 3'j'';Z 

Average 

4 5 

ii67. o Y'37 

/bb. /'7/3 

16d~ '[j]."5 ) 

J53~1-'6"36 

/L67.. 6&92. 

/163" t.15 '&-01­

116;(,;Z ~ ifV 

lit?, £/J3 8'" 

116~:;Z 30'::<' 

1M.., 2..G2~ 

167(> ]>L/ir6 

J.5b~ t-j 9 53 

C· COMPREHENSIVE 

. E EMfSSION 

S~ SERVICES 
--'''--­

e 

z 

a

-

• 


• 

• ~,:.'::. ':.~::. ": :. 


TARE WEIGHT 


WEIGHING SHEET 


TinlC 1~:'110 

Date n)()(; lfi 

Analyst -r'; 

lD No, 

.1 

1) -z. 0 1-7:r I['''i', ?)S:;" 

?Oi- q 16~, 7fttO 6 

7. 0 '90 11'0,9'197­

"l.of) J /(;.5,030/ 

7.0'&;'\ If/J ,0'1- '19 

20-6'3 trb,qf{ J5 

"?.. 0 'f:; Lf 11-L 11ft" S 

-Z o1f5 Jb?Sf05 

(.0 fj 6 /'5~, 'lr'b 0 5 

?.o~-:;.. fb'1,b7; tf'] 

Z.0-'&"';­ (}of, L{ 91f3 

lv -Z O 'iS"7 I bl{,6 ') 't' 0 

Check Weight J:ft1. tJ j 1') 

I"; 0'0 

Ilj?J?{ 

71' 

Weighing (grams) 

2 3 

lilt. 1555 

(611. f if'tll/ 

Ii0, 17'1(; 

/t5, 030"'3 

162,O1:~ll 

(j-b, f'ir/3 

Irl. 'Z,?60 

167·"1103 

1<; (). *-6OD 

169.6-<?1~ 

(l-/.'-/9 r '3 

16 t(, b'?-b 

i"7o.0·) '1L/ 

4 5 

: ,~' "~"'. "~.1! 

. ?

. 

" '.~~ . "~ 

,,' 

Average 

I 

1 169" T5~ b t 

/bfJ. Y"6-05 

/70. ~'7 'f 1­ 1 

165,o3o:J.. I 

16:<'_ Of; '17 i 

17-6. ? <0- / tj I 

Irl. 2'?6 3 

U;:1; 91D'{ 

!) '6: &--60] 

/69", 6.zr9 '} 

J7-/" L/'t1-t I 

1("-1.657-<6 

=.C COMPREHENSIVE 

E EMISSION 

S~ SERViCES 
t:.'·'· 

•,'" 

\::.~":.: .,:.•" 

," 

... 

TARE WEIGHT 


WEIGHING SHEET' 


Time r~Jo 

nate 1,//6(11 

Annlyst 77­

In No. 

1 

:P2 at 6 A· 166. £/3 if i­

'201'1-4 1:;'-:;.10'-/'] 

"20"0-'1:( A J09" ').31 9 

'7..(J~ i If 1'1';;.9 to 3 

7.040 ib1 bf/~8 

7~)"1 ) I w,~ 25 9& 

lC7'9'J... I &h,f '9t? 7­

1-0'73 1~3.rc-{.33 

(0'7 i/ 163,Lf5=!-9 

7.0"9 ~ /66. -z &;l3 

7.096 16;J~'?TJ& 

(' 7..cF!'1 167,,07/9 

Check Weight 1=70.01<1S -.~.. - ... --­ ...----­

15~')(1 

17.}lb 

-r} 

Weighing (grams) 

2 3 

Itd:-.tj1 t/3 

FJ 7. 'z 0'1'1 

IGi.?3/5 

nJ..1091 

16 r~ 66'73 

I(;..;!. t 51:z 

J66, /909 

J55, ~(,11' 

/£3. L(s£,tf 

/1,6.. Z(, Z+ 

/t.7.. '? r 21.. 

I b=;- 0 j·ztf 

1"90.o11i 

Average 

4 5 

16/., (13t./S i 

1?-1. 'Zt..1tf?· 

/67. z "3/77­

17::<. 'Tlo/ 

167'.6C<.i?­

/62 Z57r...j 

Ibt'f /9'tt.? K 

/53.. 'frt 35 

/;.:.3. ~-I5 'ir.2 

/6t:..26:?S· i 

16~ "8-9-~o i 

/6'7.0"7);('2. j 

j 

I 

C COMPREHENSIVE 

E EMISSION 

S~ SERVICES 
• 


AppendixC 

Field Data Forms 

• 

________________ __________11 . 
Run No. 


Location: Cargill ep11 


Date: 

Project # 

Isokinetic:;: 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate (cu Ftlmin)=· 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Oeg)= 


Barometric Pressure (in Hg) :;; 


Static Pressure (Inches H20)::: 


Stack Pressure (in Hg)= 


Percent Oxygen :: 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water:::: 


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp {F)"" 


:Jry Molecular Weight:: 


• Wet Molecular Weight= 

Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Diameter (Inches)= 


Stack Area (Square Feet) :;; 


Pitet Coefficient= 


Average Square Root of Delta P (inches H20)= 

Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= 


P~rticulate Loading ~ Front Half 

Particulate Weight Net (9)= 


Paticulate Loading. Dry Std. 68 Deg (gr/set): 


Emission Rate (Ib/hr)= 


Particulate Loading - Total Catch Including fmpingers 


Particulate Weight Net (9)­

; Partic~late Loading, Dry Std. 68 Deg (grlscf)= 


•	 . Emission Rate (rb/hr)= 

Percent Impinger Catch= 

1 Assumed 10mg 

Dec 9, 99 

8899 

99.0 

72.400 

223.524 

0.993 

0.004 

150.066 

143.716 

29.65 

0.60 

29.69 

21.00 

0.00 

28.5· 

0.9 

88.3 

1.46 

1.2621 

63 

28.84 

28.74 

240.0 

0.180 

38.00 

7.88 

0.84 

1.0195 

3,440 

27,093 

26,877 

0.0022 

0.0002 

0.05 

0.0100 

0.0011 

0.25 

78.00 
Run No. 


Location: Cargill ep11 


Date: 


Project #
 .0/0Isokinetic= 

Initial Meter Volume (Cubic reet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Oeg)= 


Barometric Pressure (in Hg) ;: 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent oxygen := 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water: 


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)::: 


Average Stack Temp (F)= 


Dry Mo[ecular Weight:: 


• Wet Molecular Weight::: 

Sampling Time (Minutes);;:.; 


Nozzle Diameter(lnches):: 


Stack Diameter (Inches)= 


Stack Area (Square Feet) == 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20}:;:: 


Stack Velocity (Actual, fUmin)= 


Flow Rate (Actual, Cubic ftlmin)'" 


Flow Rate (Std, Dry. Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (9)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (lb/hr)= 


Particulate Loading ~ Total Catch Including lmpingers 

Particulate Weight Net (9)= 


Particulate Loading, Dry Std. 68 Deg (gr/sct)"" 


Emission Rate (Ib/hr)::::
 • 

Percent Impinger Catch::: 

Dec 9,99 

8899 

99.0 

72.400 

223.524 

0.993 

0.004 

150.066 

143.716 

29.65 

0.60 

29.69 

21.00 

0.00 

28.5 

0.9 

88.3 

1.46 

1.2621 

63 

28.84 

28.74 

240.0 

0.180 

38.00 

7.88 

0.84 

1.0195 

3,440 

27,093 

26,877 

0.0022 

0.0002 

0.05 

0.0085 

0.0009 

0.21 

74.12 
Run No. 


Location: Cargill ep11 


Date: 


Project # 
 e% Isokinetic= 

Initial Meter Volume (Cubic Feet)=: 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin):: 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet 68 Oeg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water-


Average Meter Temperature (F):.: 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)= 


e Dry Molecular Weight::::; 

Wet Molecular Weight= 

Sampling Time (Minutes)::; 


Nozzle Diameter(lnches)= 


Stack Diameter {Inches)= 


Stack Area (Square Feet) ::; 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20)"" 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= 


Particulate Loading - Front Half 


Particulate Weight Net (9):::: 


Paticulate Loading. Dry Std. 68 Deg (grlscf)= 


Emission Rate (Ib/hr):::: 


Particulate Loading - Total Catch Including Impingers 


Particulate Weight Net (g)= 


Partic.ulate Loading, Dry Std. 68 Deg (grlscf)= e, Emission Rate (Ib/hr)= 

Percent Impinger Catch;:; 

2. Assumed 10mg 

Dec 9,99 

8899 

95.7 

223,900 

365.388 

0.993 

0.005 

140.498 

134.137 

29.65 

0.60 

29.69 

21,00 

0.00 

27.0 

0.9 

89.9 

1.38 

1.1613 . 56 

28.84 

28.74 

240.0 

0,180 

38.00 

7.88 

0.84 

0.9772 

3,274 

25.764 

25,941 

0.0022 

0.0003 

0.06 

0.0100 

0.0012 

0.26 

78.00 
Run No. 

Location: Cargill ep11 

Date: 

.roject# 

% Isokinetic== 

Initial Meter Volume (Cubic Feet)::: 


Final Meter Volume (Cubic Feet)= 


Meter Factor-


Final Leak Rate (cu Ftlmin)= 


Net meter Volume (Cubic Feet):.:: 


Gas Volume (Dry Std Cubic Feet 68 Deg}:::: 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20);;; 


Stack Pressure (in Hg)= 


Percent Oxyg~n ::: 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water-


Average Meter Temperature (F)= 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


Average Stack Temp (F)::: 


Dry Molecular Weight::::
 • Wet Molecular Weight: 


Sampling Time (Minutes)= 


Nozzle Diameter(lnches)= 


Stack Diameter (Inches};:: 


Stack Area (Square Feet) = 


Pitot Coefficient= 


Average Square Root of Delta P (inches H20):: 


Stack Velocity (Actual, ftlmin)= 


Flow Rate (Actual, Cubic fUmin)= 


Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= 


Particulate loading - Front Half 

Particulate Weight Net (g)= 


Peticulate Loading, Dry Std. 68 Deg (grlscf)= 


Emission Rate (lblhr)= 


Particulate Loading - Totar Catch Including Impingers 


" Particulate Weight Net (g)= 


Particulate Loading, Ory Std. 68 Deg (grlsc:f)= 


• 	 Emission Rate (lbfhr)= 

Percent Impinger Catch: 

2 

Dec 9,99 

8899 

95.7 

223.900 

365.388 

0.993 

0.005 

140.498 

134.137 

29.65 

0.60 

29.69 

21.00 

0.00 

27.0 

0.9 

89.9 

1.38 

1.1613 


56 


28.84 

28.74 

240.0 

0.180 

38.00 

7.88 

0.84 


0.9772 


3,274 


25,784 


25,941 
 : . 

0.0022 


0.0003 


0.06 

0.0079 


0.0009 


0.20 

72.15 
Run No. 

location: Cargill ep11 

Date: 

.roject# 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)'" 


Meter Factor::: 


Finsl Leak Rate (cu Ftlmin)== 


Net meter Volume (Cubic Feet):: 


Gas Volume (Dry Std Cubic Feet 68 Oeg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen ;;;; 


Percent Carbon Dioxide= 


Moisture Collected(ml)= 


Percent Water::: 


Average Meter Temperature (F);' 


Average Delta H ( in H20)= 


Average Delta P (inches H20)= 


~verage Stack Temp (F)= 

..~ry Molecular Weight= 

.. Wet Molecular Weight::! 

Sampling Time (Minutes)""­


NoZzle Diameter(lnches)=­


Stack Diameter (Inches): 


Stack Area (Square Feet) ::: 


Pitot Coefficient:::: 


Average Square Root of Delta P (inches H20)= 


Stack Velocity (Actual, fVmin)= 


Flow Rate (Actual, Cubic fVmin)== 


Flow Rate (Std, Dry, Cubic fVmin 68 Oeg)= 


Particulate Loading - Front Half 


Particulate Wejgh~ Net (g):: 


Paticulate Loading, Dry Std. 68 Oeg (grlscf)= 


EmiSSion Rate (Ib/hr)= 


Particulate Loading - Total Catch Including Impingers 


Partlculate Weight Net (g)= 


ParticulateLoading, Dry Std. 68 Deg (grlscf)= 


• 	 Emission Rate (lb/hr)= 

Percent Impinger Catch= 

3 Assumed 10mg 

Dec 10,99 

8899 

98.9 

365.700 

512.347 

0.993 

0.002 

145.620 

139.028 

29.65 

0.60 

29.69 

21.00 

0.00 

15.0 

0.5 

89.9 

1.38 

1.1613 

56 

28.84 

28.79 

240.0 

0.180 

38.00 

7.88 

0.84 

0.9772 

3,271 

25,763 

26,033 

0.0014 

0.0002 

0.03 

0.0100 

0.0011 

0.25 

86.00 
RUn No. 


location: CargHl ep11 


Date: 


• 	 roject# 

% Isokinetic= 

Initial Meter Volume (Cubic Feet)= 


Final Meter Volume (Cubic Feet)= 


Meter Factor= 


Final Leak Rate (cu FUmin);:: 


Net meter Volume (Cubic Feet)= 


Gas Volume (Dry Std Cubic Feet as Oeg)= 


Barometric Pressure (in Hg) = 


Static Pressure (Inches H20)= 


Stack Pressure (in Hg)= 


Percent Oxygen = 


Percent Carbon Dioxide= 


Moisture CoHected(ml)::: 


Percent Water: 


Average Meter Temperature (F)= 


Average Delta H (in H20): 


Average Delta P {inches H20)'" 


a'::,verage Stack Temp (F)=

w::ry Molecular Weight= 

Wet Molecular Weight: 

Sampling Time (Minutes):::: 


Nozzle Diameter(lnches)= 


Stack Diameter (Inches)= 


Stack Area (Square Feet) 


Pitot Coefficient'" 


Average Square Root of Delta P (inches H20)::: 


Stack Velocity (Actual, ftfmin)= 


Flow Rate (Actual, Cubic ftlmin)= 


Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= 


Particulate loading Front Half 

P~rticulate Weight Net (g)= 


Paticulate Loading, Dry Std. 68 Deg (grlscf}::: 


Emission Rate (Ib/hr)= 


Particulate Loading Total Catch Including Impingers 

. 	 Particulate Weight Net (9)= 


Particulate Loading, Dry Std. 68 Deg (grlscf)= 


• 	 Emission Rate (lb/hr)= . 

Percent Impinger Catch'"" 

3 

Dec 10, 99 

8899 

98.9 

365.700 

512.347 

0.993 

0.002 

145.620 

139.028 

29.65 

0.60 

29.69 

21.00 

0.00 

15.0 

0.5 

89.9 

1.38 

1.1613 

56 

28.84 

26.79 

240.0 

0.180 

38.00 

7.88 

0.84 

0.9772 

3,271 

25.763 

26.033 

0.0014 

0.0002 

0.03 

0.0062 

0.0007 

0.15 

77.42 
COMPREHENSIVE 

EMISSION 

SERVICES 

Project Number..--;g=g..:.q'_"1'--__ ..~_ Project Leader _-"!!.DOc=..______~_ 

Run Number__..:..)____________ Meter Operator --'-M--'-A"--_______ 

ubP~on _____________- ______ Date J')../1/f1 

Sample Type .tY15/p.02 Support Personnel --"'C""-S-'-______­

Plant &r;t I [ 


Lxation E' P II 


Assumed Moisture % .a Meter Number g-


Minutes Per Point (min.)..J.S;;L.. Oven Number ___ 


Sampling Time (min.) J.Ho Umbilical Number 100 hll«,. . 


Meter Factor Y e. 29. -3 Pilot Number ___ 


Meter ~H@ 1,:Hi~Jf- Probe Number ___ 


J J 3' Pitot Coefficient Cp o.3:r Probe Length --'''''-_ 

Stack Axis 1 (inch.) ,5t[ Nozzle Type _...:;:5...:;5,---_ Schematic of Testing Location 

Stack Axis 2 (inch.) Jg 

Barometric Pressure (in. Hg) •.21. f) 


Static Pressure (in. H20) ~_I_&_Q___ 


Nozzle Diameter (inch.) _..l.,1;..;J6::...Q~~_ 

Initial Meter Volume (fil) 7':<,'toQ 

! Final Meter Volume (fr) 223 L52.t1. 

Leak Rate Before 0.010 CFM@ ;;; 15 in. Hg 

Leak Rate After O,O(J<i CFM@ If in. Hg 

Pirot Leak Check \../"" Before ;..-­ After 

RECOVERY DATA 

Orsat lmpingers 

Trial %COz %C02+%Ol %02 

1 

2 /J I "~ f3 IQrf rFJIC n 

Avg 

Final Initial Difference 

hnpinger 1 5,5 100 -Y5 

Impinger 2 I ~G? 100 ?~ 

Impinger 3 10(., lao_ &, 

Impinger 4 7';).015 6t~O LJ lIS 

Conrunon/Color Total ~g'2

• Notes: Filter Number: _ ...... f-"&""'"-'I .......... · _____ 

---.. ----

RUn No._!.....-.-__-_~ 

Project No. ~$;::.:;g;....:9....J.'1_____ 

Location Co.<s HI £ P II 

Date ,ia/,1/11 

Operator ~1tY):.f...;f+,------_____ 

Start TIme --,!'Q.~ 9,'50____~ 

Stop TIme ...L.L;;:.:...;:::l;...::..;5'2~____ 

ei 

• Notes;

~~'¥~"" ........,.,,'. ·,v,,·., ft:'!'o,,,,., , ,. ~'~~; . iKr'" 'p",,,"M""'!i' .......- ...... ,' 'F"""": .. ","",V;"";fjl;1'~7i ' M'j"'" ','" VAC·'····,··'·:·· i'!',"'5j;;;e[?b' .", T' " . 

. ,.::::..3;(~i~::>;~;~li$:i;.i;..:'~i~~:~\: :': ~;.~::i·;!:;;·I,41~e~~,...>'(":: ;/;~,H~atl. ;~\!~l.·~~;;;imi:;' ,;~. !:j.'~:;~~:;; ~!f~: .. : 

T itiar::1-,Z, . ? .... HO" i--'.' 1;'/J~I~t;:: l..pT.IIlet. ", .>,~" .., r·,"'~':W';'~':)lS;\';, .N ......, ·n .;.:,.. '1f\.'1'-' ..... ,' ..,:,*.""":"";,.,,,, .•.. <.~., ..':,.;.... ~ :': .• " 

I .fa I ?5,Cjrp I ,35 I 58 I 0g I(#7' I 13~ 12 I .252\ 32. I 2tf5 

'2 20 I - r ,QSI 57 I '7t:. G:>A'I i;(g I L I ;2.5SI,.1L; J245 

I '3Q . I gZ.IZ I I 5il , (0"1 I , ;(~I 2 t lSu, 135 J

3 ! j 25 J gs 1.243 

'I I LfO !2C(,9S . ! ! (22 I ~o I $<7 I "1-01 ,2sl "< J ~5gl :!!.( !ZljS 

'5 I So iS$,Ol ! 1:z~1 (PO 1Cj 0 I "1- II 1271 2 1ZS'L31 3'1 124& 

(p /po .q/, £;2­ I ,33­ r ~I i 7'2 1 '2 1 ! t I ,.5-f I I Z 125"7 13S' 120/ J

f }Q q£,:lCo I i ,5 I (P r I 9S'1· 131 /.11 5 1;(551 34> 1:<¥Cp 

g 9.0 1/02, Cjl j ;2..1- I (oz 110£/ t-G:J I 3d (0 125&1 e.tl 12L!~' 

9­ I '10 I - ±t5,1 &5 tO$ 7,g1 l.( l I .8 1.25SI 4.A'1 ;24 ( 

10 I 100 1/3)., 3t'P . 7 I· Co 3 I(1g 11a'1 4,gl ·cr I .2S tl 50 I ~45 

If II 25 I ,3,5" 1(;; '{ II 1 0 " Xl I LJJl l,g I 25S1 52 12<1 { 

12 120 /'5'5,5f1/ I ~,1; 1&'11 If{ 12.31 4( t ..g I ')5s I 5 <-{. I 23'1 

{ io iIPv Iq J .53 I ~'-{ qqH~ IlhO 2 12S& .5·'{ 1.:2'13 

z ':<'0 I /!.,.J;.13 I ,&3 ~5 I i ec. 'I 1 13 2 I <257- 15 <f I 24''7 

"3 J:> I 17-0,/& 1.,67­ /" S lOw I gol ,71 z. 25"21 5( Izsr 

4 lfo I .- 1IrZ­ roC?> I /0 (pI ..&9 I I p,? 2. 1 7~ '71 S I 12s</ 

5 50 I /JOj 51 I , 101 (d5 I 1t?G:, d1? (.20 2­ ZS'7' 150 ZS~ 

&. w 11$5,31 J I~ 3 f ,,(;? 1 10&..1 86 ,j-l/ 2· 2(pQ £9125g 

f- to I/~o 35 I 6,,'2 i ::;> I GG>I 10t0 gol ,1-3! '2 ;;55' . SI .255 

.g 9,Q CJ5',;'I I tn I (pCp I/Ow .to I ,9/1 '2 I .;;(% 50 12$~~ 

'1 90 :;(0 /. 9~ I 175' C,t.:- Jjt?~ &2 I;, I I '7 , '­ 1..<>(.:;. 5'0 123.7

10 /O(? 'Mi. RLf 1/" 3' J {pC; 1106'1 B"O_' 1t'5 ,.. 1.255' SI / 251 

1/ //0 I '­ I /,? (.;,t.,. ) //0 d/l I, S' 3 25&\ 5'z... 12Sg' 

12­ 120 22?Aj'~Y I / 4 ILot; I /11 Rzl Ida t.f 255 5'1 255 

! I I I I I 
- -- - --

- -

'C­ -, - --­ - --- COMPREHENSIVE 

=- E=-­ - - EMISSION 

--====- s== -- -

- SERVICES ·' 

-- ­

,g qwt' Project Number__......;;::'~""'$"-'-(..f...L______ Project Leader _...;:f)C)::....:;,._________ 

RooNuwrer____~,~~~_____--~-- Meter Operator ....<..:M............ A _______ _

Lab Person ____________ Date _~/,)::!..0.L.9:....!9::...9~-----

Sample Tjpe /y/S!20'6 Support Personnel _.."C..::.:.:;S'---_______ 

Plant La r., u I 

~tion __~1=5~p~/~I____________ 

Assumed Moisture % _~::Z""'--_ Meter Number -:JjZ" 

Minutes Per Point (min.)....!.!l....... Oven Number -,--____ 

\ ( r) i

S~pling Time (min.) ;2.. 'i9 Umbilical Number 100 BIl4of:.. 


Meter Factor Y O. qCJ 3 Pitot Number ____ 


Meter AH@_-"_'..;;J._'..;.f__ ProbeNumber ___ 


.' Pitot Coefficient Cp 0, gL/ Probe Length ---....2 I 

Stack Axis 1 (inch.) _:$""",,,,8__ Nozzle Type 5'5 Schematic of Testing Location 

36 Stack Axis 2 (inch.) ____ 

Barometric Pressure (in. Hg) J 9, , f 


Static Pressure (in. HP) t/aQ 


Nozzle Diameter (inch.) I I gO


Initial Meter Volume (ff) 22..3/;00 

Final Meter Volume (f~) 3Lo5.3 :9.':.) 

Leak Rate Before (I.OOT- CFM@ ~ 15 in. Hg 

Leak Rate After 0.005 CFM@ in, Hg 

Pitot Leak Check Before /,./' ~ After 

RECOVERY DATA 

Orsat lmpingers 

• Notes: Filter Number: _ F 8b 5 

Trial %COl %C02+%02 %02 

1 /'\ 

2 fl f'1 ~"PY1 i 

3 ,/ VI' '/r I 

Avg 

Fioal Initial Difference 

Impinger 1 55 /0_0 -ys 

Impinger 2 i12. /00 22 

Impinger 3 /10 100 10 

Impinger 4 79-{,S 7/4,5 (.(0 

Condi tion/Color Total ).1 
Run No. :d 

• 

Project No. --'~"""""'-'_'-- :-"ntJ:1 _____ 

Location Cc.Yfj; If EPII 

Date 1119/19 I 

Operator ----.!:..A=ifA:..I.___---'-___ 

StartTIma ......;;;i3;.....:.;_r..:..-t_____ 

Stop TIme -l1-.J1:.,..:.:...!,;./J:=:..-.-_____ 

•" Noles: 

COMl'RE."tE....':SM 

'. EMiSSlO~ 

. SE)tVlCES 
--_.... - ... _. 

. COMPREHENSIVE 

. EMISSION 

SERVICES 

Project NUIIlber_~'gioi.l8.c....'1~1..L.-_____ Project Leader _:.::.D_Oc...-_~______ 

Run Number__S'--________ Meter Operator --,-t1~AL-_______ 

Date 1:;)00 /91 Lab Person _-___--_____ 

Sampl6 Type . fY)S/2Q 2- Support Personnel --"C=:..'.... '5________ 

Plant Cg 1'$;/I 

Location liP /1 

JSi Assumed Moisture % _ .....2::0-.._ Meter Number ___ 


Minutes Per Point (min.) Oven Number __ 


Sampling Time (min.) Lf0 Umbilical NWllber ICO I:rllt~ 

Meter Factor Y 0/ '7'22 Pitot Number ___ 


Meter tlH@ _ .....l;,...!·c...::g::..:l..Ll~_ Probe Number ___ 


3 1 

Pitot Coefficient Cp (},g'-l Probe Length _~_ 

Stack Axis 1 (iDch.) 3..8 Nozzle Type _-,-S__ Schematic of Testing Location 

Stack Axis 2 (inch.) '3 g 

BaromelIic Pressure (in. Hg) 


Static Pressure (in. HzO) _...:.(..:::.(p~O:!........ __ 


Nozzle Diameter (iDeh.) _,_1..;;;:£-.,0___ 


Initial Mete! Volume efr) ~(o5'1-00 

, Fmal Meter Volume or) 512, Y/7C 

Leak Rate Before 0.OQ7 CFM@ ~ 15 in.Hg 

Leak Rate After 0, 0 (? 2 CFM@ J in. Hg 

Pitot Leak Check V" Before t.,./ After 

RECOVERY DATA 


Orsat Impingers 


• Notes: Filter Number: _-'E_-.....3"--7-0___~_ 

Trial %COz %C02+%O~ %02 

1 

2 /l J. ~ ,j 

3 zyrJ'/1'J If:' j/L !J 

Avg' 

Final Initial Difference 

Impinger 1 3 l 100 -u,o( 

Impinger 2 130 100 30 

ConditiOn/Color 

Impinger 

Impinger 4 

3 11'1­

133.c o '9'b 

/00 

Tota! 

f Q 31-­

l1­

lS 
_ RUn No.~_-....:..3___~~_ 

ProjectNo, _,1='2,-,-7-4.,.'1-:.,'_~__ 


Location -"e::;..:.p...;.,...:-r_____ 


Date @O/t{<j 


Operator --r..::.Jt!1::...l.!4_~~ ___ 


Start lima ____1=_:Z=2_____ 

Stop TIma --.-:!'-!....I:.....t:i...2:!.i_~___ 

f:Bfmi·~1~~~·I;::~~lr:~·!i:~:*11~1~~{~lt~ I 10 ,I ~.8. 7-S 1 .25 I 5"3_ I &1 I (;'£ I 12::1 2­ I 252 I 23 I 25"S" 

2 20 137-(, t7e:, i ,zS I ~c I ;v~1 (q9 I ;.:<'11 2 1254 I 23 255 

I ")741 Cf I i 52 I 90 I 7-( I Zl£, I I 2S:;J 25 3 30 ;22 I 2 I , 250

l[ I 40 I_~f.g ;O{ 

i ;27.. I :;;3 I I , g ( j :;;'L(l .2~1 2 12{oO I 3'1 I 25'(0 • 

I . , I ss I '12 I -:tt.( ! 5 So 13g J. Is I 1-27 1 I :31 I z I 2ggi.?1 I 2.sy 

to I 00 i1iz;, '14 I 

c 3/ I ss-i Cfb I 1V I 3 1 i I I (P I e. I 2S'1l VI 125(

7­ I 10 1370. !fa, r i,2 I 5'-( 1 7$ 1-5 I ) . <( I z ! 259'1 'It./- I Z5Z 

R RO 400.30 I 2\31 s j 110'7 I 7-7- I 2-11_ I '-I I 2S;G! S'o I 253 

9 I 7Q 1411 <:.Jet I J,L{I SO /)'3 ~I 4. I I s I zs:7l 5'1 I 252 

t() 10C? I t.tJ~, '17­ I .3(5 I' 5 I ! 04 22 '-lIZ 5 I 2S~ £ t.( I Z5L 

II t{C? 41:.5,32 I 3,31 51 ffil 'g'vl 4"IQI 5 I 2sx-1 sg 1249 

Il 12P ,'fLI(,r;,/ .5'( I 51 I I 51 .zq I 3,'11 5 , .25'71 5<7 1257­

( I() - I 15'3 1S~ 32 I,loS' I 2 I 2511 &'0 'Izsl{ 

2 20 I - I. t;::f­ (p( Iq9! 1.2- i ,(cCo I 2. I 251 J 42 !2S'Cc, 

'3 I so. I L}f::;O, lflt> ! ,110& 1 ~Q <1. <=-1 I F( , -T7 2 I 25'11 G'3 I Z5S 

i.[ l{o I - I I (P I 57 k;C;; gO I , }) I 2­ I 2Sj. &'2 I 25 ! 

~ <;(J 1 4?O, '-10 I ,~r; 57 I 107­,J91 ,. 7-0.1 2 1257-1 thZ I 

I 2SS

(, '=-0 r"l7-ff.. Itv I I 5 Co 57 j 1071 J"f I ,(PCa < 25f CPt I?SA' 

) 70 I if ,ct. '13 I ISO , Sf I/of go I /i7 L '251 ISJ' zS7 

JI flo 4$1. c/o I lGSI &0 I { (1 g go I t 1& I L I 52 1254> 

7 70 ii'lL. ri­1/,0 (po Jo"7T:?OI/,'Z. I 2 25th 5/ 127)8 

Iq I{XJ I.ftt 7- Cflo I }.2­ (,.,0 I 110 Rf j It'-! 2 2~Q 52 I 25« 

1/ 110 15"05 I () I I; '3 I {Pi iOo.; £2 I I,S z.. 25..f1 53 I 25-:;-

Ie 120 !,;J/,P 3<17- I I, '3 I (pI /[.>& , 82.1 ll5 z ;?e.fS ';-5 I 25<-/ 

I I I I I

•

NOles: 
Preliminary Velocity 


• 


e' 


e 


Plant Project No._d'-"ffi .........:1...L..-____ 


Date IZ/g/qq 

Location •CaG~ 1 ( 

Stack I.D.---IE;""",--P-,-i.:...t______ 

Pitot Cp Q. at{ 


Static Pressure in HaO'--::..tJ.l:4rO!lQ~___ 


Barometer Pressure in. 


Start Time __________ 


Stop Tjma_~~------

Operators_..;.J1_J1.;...A-....-______ 

t5 

Final Pitat Le.ak Check at 2:3" HP P I F 

SCHEMATIC OFTRAVERSEPOINT LAYOUT 

Traverse Velocity Stack Cyclonic Flow 

Point Heed Temp. Determination 

Number 6.P OF 

in. H2O [;P at O' Angle Which 

Reference Yields 

a NullllP 

( ,&'1 51 

:2' ,7) S1­

3 1&>'3 r;7 

Lf ,-.Be; 5if 

$ 1.32 '5~ 

{p t~S 5'1­

1­ t Co 0 Sit .&.$ 5$ ., 

"! 1"1!5 sg 

1(J 1,0 58 

I I I, ( Is.J 

It ,25 5'1 

Notes: 

Traverse 

Point 

Number 

( 

<­

J 

4 

'5 

<..t;; 

7 

J? 

7 

(a 

i i( 

'2 

Velocity 

He;!!d 

llP 

in. Hp 

,.35 

,:J..g 

,25 

22 

,25 

37 

Ido 

2-..5 

.3',·3 

3.8 

3.8 

3.2 

Stack 

Temp

OF 

£::t 

5CJ. 

51­

58 

158 

'51 

5,8 

58 

58 

58 

58 

58 

Cyclonic Row 

Determination 

llP at 0" Angle Which 

Reference Yields 

a Null LIP 

CO:MPREHENSIVE 

EMISSION 

SERVICES 
COMPREHENSIVE 

EMISSION 

• SERVICES 

1112 Maple 

West Des Moines, Iowa 50265 

~-'--r---'--'--'--~-'--'-I 

o 15 30 45 XX 0 15 30 45 

11 

8 

9 

STACK 

OBS 

.~ 

29 0 0 
.' 

COMPREHENSIVE 

EMISSION 

SER\'1CES 

1112 Maple 


West Des Moines, Iowa 50265 


--~--~---~-'--~'--r--~--.-~ 

o 15 30 45 XX, 0 15 30 4S 

o 

00 33 

o () 34 

7 

8 

9 

STACK 
-- --- - - -- -- --

='C --

-­ COMPREHENSIVE - E-· -- - EMISSION 

• 
 S -: SERVICES 


1112 Maple 


West Des Moines, IOwa 50265 


0 15 30 45 XX 0 15 30 45 

0 0 30 

Pl-ANT l<AM£ 31 

AIlDli:ESS 32· .5:0",'1< C.} 3 0 33 0 Dh1l! (/ ~ 34 6 

0 3S D 

36 a 0 

$OUllCE !Dlli"lll'lCAnON 7 

£,p,; 


RffiI.'l.'I1ION(S) N 


ruEl. 9\'~"ED 

OBS£I\\I,HlON l'QI>."T/poSlno.'f 0<5\,.,. STACK 

OlIS 43 

~. 44 

45 c::::.:> 

DISTA>;<;;E !'ROM DlI<ECJlo." F:t~~5 0 

STACK HlilGHT 0 

Sh')' <:O~""mo): 

18. 

\\'£\1> SPf£!) 

19 

~PliJlATVlU! .2:i 20 D 

ODOltS II 2J 51 

CQ.\{.\i&'1T.$ ! 52 " 

53 
• 


AppendixD 

Pretest Calibrations· 

• 


• 

METER CALIBRATION 

0.3033 K Factor 

Operator 	 DO 	 1 Meter Number Dec3, 1999 

1.004 Orifice Number '.~iOUS YFactor 	

5 

......, 

Meter Volume 

Final 

Initial 

Net 

Meter Temperature 

Inlet 

Initial 

Final 

Outlet 

Initial 

Final 

Avg. Meter Temp 

Time 


_eter Delta H 


arornetric Pressure 


'. Room Temperature 

InItial 

Final 

Avg.Room Temperature 

Pump Vacuum 

Vcr (std) 


Vm (std) 


Y Factor 


Delta H@ 


Average Y 

Average Delta H@ 

+/" 2% Criteria 

Percent of Avg Y 

• 	 +/- 5% Criteria 


Percent of Final Y 


CubIc Feet 

Cubic Feet 

Cubic Feet 

Oeg. F 

Oeg. F 

oeg.F 

Deg.F 

Oeg. F 

sec 


inches H2O 


inches Hg 


Oeg. F 

Deg.F 

Deg.F 

inches Hg 

dscf 

dscf 

RUN 1 

211.466 

206.000 

5.466 

65.0 

67.0 

63.0 

65.0 

65.0 

840.0 

0.41 

29.27 

71.0 

71.0 

71.0 

23 

5.394 

5.381 

1.002 

1.564 

1.003 

1.556 

0.04 

PASS 

0.13 

PASS 

RUN2 

217.185 

211.700 

5.485 

68.0 

69.0 

65.0 

67.0 

67.3 

840.0 

0.41 

29.27 

71.0 

71.0 

71.0 

23 

5.394 

5.377 

1.003 

1.547 
CON5CLE WORK SHE I 

. -.­

Ct=eracr: _-;:J)"D~'____ 

Met:r 1.0. __---_l=--_____ Da:te: 12/3jq:r I I 1" 

Frcvicus Y Pec:cr: /, Oo':i C,;;;ca Neffice;:_...... 'L_____ 

2t:n f'l~7.:et 

I: ME: ~~ ·j~L:..ME L:•....:ts ~. ·1 2­

.... i"::'".Sl .1 ., I ! I­ ~--~----~----~--~~~~~--~--~! . 

I 

: 

,.: 

J 

~;,,;:!:ti ., I 

j Metar ;.;;;nFe~~<! 

INt..:'T 

;r.~t:a.( :-:: 0~ t'i ·1 ~-,c.i 'f' r (p7 c.~ i 


Ctfil..::: I :.-J~zi ::;: I I <oS I cS- i 

;::'.::aJ. 'F I I «(,,5' I

- '7' I 

TIr=:a ~= I I <6l.fo I 1.'1D i Me!!:r~~ ~~ ;;'0 1 I , ~/ I ji.(/ I 

Ruc:metriC" .=:O'.......~"<i. ~- -...:~ .. 1& "'::! I I .2 '1.:::2"7 I .::2 q-. J.7 I 

. r r.ccm rcrn;:~:-~d 

:n:w.. <;:: 7f I I 7j .. ...: :=.::<.1 'F 71 I I 7/ 

rt..z.r::::: '/ar:...·!:..-:1 ~';_ r.; I ! .;l '3 .2.3 

:':"c­ ~ - - - C'c.~J:FRE- -,\:jS;:..(:.

- - E - l-'M!SSON ·S ~- ~ SS.V!G5 • 

.~----

-

ORIFICE BRACKETING 


BRACKET ORIFICES: 

Orifice No. 5 1 

K Factor 0.3033

Orifice No.2 2

K Factor 0.6426

ORIFICE #1 ORIFICE #2

223.012 229.990 

217.500 224.100 

5.512 5.890 

69.0 71.0 

70.0 71.0 

67.0 69.0 

69.0 69.0 

68.8 70.0 

840.0 420.0 

0.41 2.10 

29.27 29.27 

71.0 72.0 

11.0 72.0 

71.0 72.0 

21 19 

5.394 5.708 

5.388 5.768 

1.001 0.990 

0.20 1.34 

PASS PASS 

operator 

e te 

Meter Number 

Meter Y Factor 

Meter Volume 

Meter Temperature 

Inlet 

Outlet 

Avg. Meter Temp 

Time 

~eter Delta H 

.Barometric Pressure 

"Room Temperature InitIal 

Final 

Avg.Room Temperature 

pump Vacuum 

Vcr (std) 

Vm (std) 

Y Factor (brackets) 

+/- 2% Criteria 


Percent ofY 


• 

DD 

Dec. 3,1999 

Final 

Initial 

Net 

Initial 

Final 

Initial 

Final 

1 

1.003 

Cubic Feet 

Cubic Feet 

CubiC Feet 

Oeg. F 

Oeg.F 

Oeg.F 

Oe9. F 

Deg. F 

sec 


inches H2O 


Inches Hg 


Deg. F 

Oeg. F 

Oeg.F 

Inches Hg 

dscf 

dscf 
- - - -

8R;\CC<tJ lNG WORK SHEE I .'. Meter I.D.. _ ::r=. .

Date; 1';1 /31 '11 	 K F£c:cr No. 1 .?o3"3 (£) 1/ l.o()3 

Fr6'Jict!s Y F~c::r f' Ii K F~c:cr Nc. 2 ~ C.Lf 2." (R) 

'.. 

j ~;I,E!S~ JCU:~.iE L';:~!S 2 I I 	 I ,I

F:;:d ..... I ., I 	 I ~~3'.olA. I I I ..... 	 I ;n:t'a1 ., I I 2/2.5'"D"t;:. I ~2':1..l()l) I

I~/'cter T~mFHai\,:."a J 

INt..:: I 	 1 ~h}Oc1 'f 	 7t j I 	 /. ~~ I 

i 

r:.r.El :p 	 I 70 L 7£ I 

.' ":""-t I CUI t..::; 	 ) •...,... I :;:it'aJ _. 	 .~ 

~.{:i I 	 I r G.7 I ,~ I - l-;r~E.! ';= I ~ : [ ~ I ~'i : I G7 ~ .. 1 

TI~~ SeC ., I 	 I I : I. "'if~o I i fl.eter!!..~ ;;1.. H:O I 	 I I I~/ I .2... l 

~~(> 

J

I Eucmetrfc ?;o.s.s:.:rs :::.. Eg I / ;<~ .;(7 I ,,;) "I -2Z 1 "

I F.CCi.\ T~7.~~!i~= j 

.<::, ~r;i~~ . I 	 I I 71 7;., I 

r i"::'.a.1 'f I I ;; 	 ... 7;1... I . P'..;mp V.s.C''':L":;"t 	 . 1 "'. : .... 1.= ~.r"'I I = ..:13 I 

I 

I.:!J I 

'C-~ 

• 	 -

-

--

-

.-

--- C~MP~~~STV;; 

-

= 

~ E-=-

~ EMISSlON 

-

=- S-=---. 4":>'!',f''iC-:::' - l,.;.:-' ___ 

--	 , S .... \ .~~...... i 

'<-;­
METER CALIBRATION 

Operator DO K Factor 

Nov. 24, 1999 Meter Number ate 

• 1.015 Orifice Number revious Y Factor 

RUN 1 

Meter Volume 

Final 

Initial 

Net 

Cubic Feet 

Cubic Feet 

Cubic Feet 

446.707 

441.700 

5.007 

Meter Temperature 

Inlet 

64.0 Initial De9. F 

Final Oeg.F 67.0 

Outlet 

61.0 Initial Deg. F 

Final Oeg. F 64.0 

Avg. Meter 64.0 Temp Oe9. F 

sec 780.0 Time 

inches H2O 0.46 .ater Delta H 

.3arometric Pressure inches Hg 29.87 

' ... ~ 

- Room Temperature 

Initial Oeg. F 68.0 

Final 09g. F 70.0 

Avg.Room Temperature Deg.F 69.0 

Pump Vacuum inches Hg 24 

dscf 5.121 Vcr (std) dscf 5.040 Vm (std) 

Y 1.016 Factor 

Delta H@ 1.757

Average Y 1.017

Average Delta H@ 1.748

+/- 2% Criteria 

Percent 0.12 of Avg Y 

PASS 

• +/- 5% Criteria 

Percent 0.21 of Final Y 

:'::, : PASS 

0.3033' 

2 

5 

RUN2 

452.526 

447.500 

5.026 

68.0 

69.0 

66.0 

68.0 

67.8 

780.0 

0.46 

29.87 

70.0 

70.0 

70.0 

23 

5.116 

5.024 

1.018 

1.738 
- - - -

CON!:OLEWORKSHEI 

e\ CFera.rcr: --.;.J2",-12~~__- K F!c::;:r. .30 33 

Date: uhtf/Q1 MetErLD. _ 1L...I .......
 _~_____ 

. I I 

F;e'liCUS Y Faa:: Ii Olb 

I R~ ~~::ar 

I 
ME: =.-. '/CL:..:l.:E L::::ts , 


.=:,::j ..J., I '-7'1(. .707 . 41D ~~.l)"~ • 

I w t !:::!.!i a 'i'17.o:i'cro I

I11. eter T.!m!= eraD.:.·a ~.7~ ~! INL:T I I 


I :r.Hia/ If G.<-( e.g ,I 

•~.::\ ...... 

~ : -: : 

I 

I 

1: 

CLiil.=: 

Time 

r:.al 

;.-j~iti 

F.::ai 

I 

I 

I 

'P 

.=l 

~;.: 

s.a-::­

I 

:I 

I 

G7 

fQl 

(,,0/ 

71J:) 

I 

[ 

I 

Gf 

C:,~ 

&q 

iW 

:~ 

I 

i 

I 

I 

I 

MereJ!l.-: 

Es.tc:r.~c ;::e~;:-a 

I 

J 

u-~ :~o 

:­ \.,'­ • •,f.. I,,=, 

I 

I 

, Co 

27.~7 

I "<ie", 

I 2'1.137 

I 

! 

r.ccm ~.:: e;-,.:.:." '1 I :r,~ 'F I Co~ 7D I " .=::aI .r;

. I . /0 ~70 ~ ) 

P'.!r.'.p VaC'.:":::1 !... ;$'* t,:::! t".:,.. I 9~ 2~ I 

~ 

• -

-

-

'C--

- Co!TJ"J;~_ 

;r.:n..:-- -:'N~/;:: -- ­

=- =E=.::::::::. ­ EMISSLON 

=.. ~ S=-= -

-- --. Snvrc

. ". ~ 

:.;;;~~~) 

..- ..... _­

----------~~------~IiI. 

r 
ORIFICE BRACKETING 


Operator DO

e	 Nov. 24, 1999 ate 

BRACKET ORIFICES: 


Orifice No. 1 5 

K Factor 0.3033 

Orifice No.2 2 

KFactor 0.6426 

ORIFICE #1 ORIFiCE #2 

457.938 464.295 

452.900 458.500 

5.038 5.795 

70.0 71.0 

71.0 71.0 

69.0 70.0 

70.0 70.0 

.70.0 70.5 

780.0 420.0 

0.46 2.2Q 

29.87 29.87 

71.0 70.0 

71.0 70.0 

71.0 70.0 

25 19 

5.111 5.836 

5.014 5.787 

1.019 1.009 

0.22 0.83 

PASS PASS 

Meter Number 


Meter Y Factor 


Meter Volume 

Final 

Initial 

Net 

Meter Temperature 

. Inlet 

Initial 

Final 

Outlet 

Initial 

Final 

Avg. Meter Temp 

Time 

• 	 Meter Delta H 

.~arometric Pressure ...,,, ~ --:;,; 

Room Temperature 

Initial 

Final 

Avg. Room Temperature 

pump Vacuum 

Vcr (std) 


Vm (std) 


Y Factor (brackets) 


+/- 2% Criteria 


Percent ofY 


2 

1.017 

Cubic Feet 

Cubic Feet 

Cubic Feet 

Oeg. F 


Deg. F 


oeg.F 

Oeg.F 

Deg.F 

sec 

inches H2O 

inches Hg 

Oeg. F 

Oeg. F 

Oeg.F 

inches Hg 

dscf 

dscf 

•. -.: 
- -

- -

SAP-,eKE liNG WORK SHEF= I 

..-.-.-­ Meter I.D. --""".;;I.b::=-_____~ CI=Eratcr: --1m~,,----

Date: /1/2'-1&1 K Factr:'r No.1 ,3Q3"3 (1;)
 I I 

Prs'Iicl!s Y Fac::cr {.b/7. :<Fs.c:crNo.2 .{,41C:. (:2) 

L"r.i!s 2 .I 

w., 45;'. ~oO I '16'11.'700 I ~·-'-'-·r--I--~---~"·-"·-·~--~------~--~------~~~----·II _rlcL::' ~:nl&!""C.c.!...-_

I INl.:-r _J
 I i,.itiaJ I ~:= I 70 I 7 I i 1r------F-.~aJ~I---·p--~I--~-I----~1.--7-1----~! 

r CUTi..::: i 

I ~dtiaJ I Of I (, ~ I 70 I 

[ '-J1~,' = Of ~ I i~ I 70 I ~-----li~-.a----~~~~~c--~1--7~S-D------~'~'~o/2-D--~~j /

I" Meter ..4 I in. P.p I. I ;Z. ?.. I 

.-:r.a/ I 

[ f'.!mp V.\1.C-~;'-:'l • I 

I 71 

--I 

I 7b I 

:"'c -- ~ -- Cc".r.l~ .::t.Lt~_.~_ t::-:.. - ,-.;"';=­

• -

~ 

-

~ 

=. r:= -

-D­- EMlSSiON 

-

--

==- S-=--- . ) t::~~V':'C-':::' . l...:'" .... _ .... 

J ~ 

-, .. r' 
METER CALl8RA TION 

Operator 

ate •' ..: revious Y Factor 

Meter Volume 

Meter Temperature 

Inlet 

Outlet 

RUN2 

572.771 

566.900 

5.871 

69.0 

73.0 

67.0 

68.0 

69.3 

420.0 

2.20 

29.22 

70.0 

71.0 

70.5 

21 

5.707 

5.749 

0.993 

1.804 

0.6426 

4 

2 

.. 

Avg. MeterTemp 

Time 

~eter Delta H 

'. arometnc Pressure 

Room Temperature 

Initial 

Final 

Avg.Room Temperature 

pump Vacuum 

Vcr (std) 


Vm (std) 


Y Factor 


Delta H@ 


Average Y 

Average Delta H@ 

+/- 2% Criteria 

Percent of A vg Y 

• 	 +/- 5% Criteria 

Percent of Final Y 

BB K Factor 

Dec Meter Number 3, 1999 

0.988 Orifice Number 

Final 

Initial 

Net 

Initial 

Final 

Initial 

Final 

Cubic Feet 

Cubic Feet 

Cubic Feet 

Deg.F 

Deg. F 

Deg. F 

Deg.F 

Oeg. F 

sec 


inches H2O 


inches Hg 


Oeg. F 

Deg. F 

Oeg. F 

inches Hg 

dscf 

dscf 

RUN 	1 

566.842 

561.000 

5.842 

66.0 

69.0 

66.0 

67.0 

67.0 

420.0 

2.20 

29.22 

71.0 

70.0 

70.5 

21 

5.707 

5.745 

0.993 

1.830 

0.993 

1.817 

0.03 

PASS 

0.49 

PASS 
CON.sOLEWORKSHF I 


..

::•. C!=eratcr. .....;:~""'~.=-____ ;( P::.e:::r. . ....!o. (,,",-~..'"-!?~b=--____ . :.-.: 

Cae: \<;1. -- :; -9 q 
 MetE" 1.0. ___~':i...i....-_____

Previews Y r=ac:r.:r: . '1 ~%" Crffic~ Nt:mter. _~'--___ 


~,AE; =.--: 'ICLME 2. 

.,

~ 

!~:t.ai .1 !S&I.CbQ 

! INL:'i: 

I . Jiitisl 

I. ~r.ru I ('9 73 I 

.1. Cut"cET 

;;;it;aj ::F bk> _hI 

r-.r.aL J Of! 

Time I s.<C 

Meter-!L~ I ,,-~ ,-.•.0 

CatCIT:SC' p~~.ta. I :­·Ih • ~'-'!f 

I hi 

! t.f20 

I ~.'1 . l;q ;;}? 

I ifI 6r;5 

, LJQo 

I ~.~ 

I /). q. 'l 

I 

I 

j 

I 

I 

I 

I 

I 

;~~. ! +;: 

1 7) 1 70 . F.r:c.l I .c:;

, I 70 I 71 f'..!m~ Va!;"':!:::l I ~~. !-:;; I a\ I ~f 

CCMJ?RE..~'tS:V:: 

EM!SS"rON 

SSV1c:5 

. ~, ..---"_--. 
ORIFICE BRACKETING 

operator BB

Dec 3, 1999 .te.. 


Meter Number 


Meter Y Factor 


Meter Volume 

Final 

Initial 

Net 

Meter Temperature 

Inlet 

Initial 

Final 

Outlet 

Initial 

Final 

Avg. MeterTemp 

Time 

~eter Delta H ,~arometriC Pressure , ~...::. .," 

Room Temperature 

Initial 

Final 

Avg.Room Temperature 

Pump Vacuum 

Vcr (std) 

Vm (std) 

Y Factor (brackets) 

+/~ 2% Criteria 


Percent ofY 


• 

4 

0.993 

Cubic Feet 

Cubic Feet 

Cubic Feet 

Oeg.F 

oeg.F 

Deg. F 

De9. F 

Deg. F 

sec 


inches H2O 


inches Hg 


09g. F 

Oeg.F 

Oeg. F 

inches Hg 

dscf 

dscf 

BRACKET ORIFICES: 

Orifice No. 1 

K Factor 

Orifice No. 2 

K Factor 

ORIFICE #1 

578.713 

572.800 

5.913 

70.0 

75.0 

70.0 

70.0 

71.3 

420.0 

2.20 

29.22 

72.0 

71.0 

71.5 

21 

5.701 

5.769 

0.988 

0.47 

PASS 

2 

0.6426· 

9 

0.7964 

ORIFICE #2 

595.230 

590.100 

5.130 

74.0 

75.0 

72.0 

73.0 

73.5 

300.0 

3.30 

29.22 

73.0 

72.0 

72.5 

19 

5.042 

4.998 

1.009 

1.61 

PASS 
- - - -

BR.A.CKETiNG WORK SHEE I 

.' 

.•.r ~l ,. 

~. J' .:> CperEtcr. ~3..t.,;;\3=::-... ___ MetEr 1.0. ~ 

.Date: \?- 3 -1'1 K FE.Ccr No. 1 . 6L.\g,(, (~~ 

K rEc:cr No. 2 _ ·7'1' ':1 Ci) 

I 2 .1 

I inif2.1 I I s90.. l00 I 

I !Nr....:;:; 	 j .,m,,~ -".- I. 70 17Lj 

7cJ" 

-..,.......\. , . 
 I 	 CUTtEr I •.•.• o'. 

, >~ ~~~,~) _. I '-J'- I :: I -;0 I ~~ I I= .~~ai I ' '7 D : I 13 I 1~__-_I;~_.e___ I~_s_~c__+I_~~~~o~__~,_._3_0_0__~.1

I Meter ;l.~ I i:1. H~O I ~- t;;{ I -'3 I 

j esrcmEttic ~j;.ss:.::r; I ;;1, ;':g I ?l,'J..? I ~5· ? ~ J 

I Rccm Te..-r:?~!a:t::a .. I 

I' F:::aJ I 'f I I J I 7 J. I J'---_F_~r.:_.P_vs~c--_·!::-_ .• ~.I:.--_:r'_ .. 1~ ... :g__2-I_~.;....;.f ___-.:.-_\-...:C;~~._i

'. 	

'C­ --- ---.­ - - CCM?.RE..~\isr..=: 

~Dr: - - E?..asS:CN 

-l 

I -

--

-

= s-=---. S;:;-:>Tr:c,,:,<:: t-':'" v .... __ 

• 

Appendix E 


Posttest Calibrations 

METER CAUBRA TION· 

operator 

ate 

• • revious Y Factor 

M~ter Volume 

... 

Meter Temperature 

Inlet 

Outlet 

Avg. Meter Temp 

Time 

Meter Delta H 

eiBarometric Pressure 

Room Temperature 

!nitial 

Final 

Avg.Room Temperature 

Pump Vacuum 

Vcr (std) 


Vm (sid) 


Y Factor 


Delta H@ 


Average Y 

Average Delta H@ 

+/- 2% Criteria 

Percent of Avg Y 

• 	 +/- 5% Criteria 

Percent of Final Y 

BS K Factor 

Dec. 17. 1999 Meter Number 

1.003 Orifice Number 

Final 

Initial 

Net 

Initial 

Final 

Initial 

Final 

Cubic Feet 

Cubic Feet 

Cubic Feet 

Oeg. F 


Oeg. F 


Oeg. F 

Oe9. F 

Oeg. F 

sec 

inches H2O 

inches Hg . 

Oeg. F 

Deg. F 

Deg. F 

inches Hg 

dscf 

dscf 

RUN 1 

899.174 

894.100 

5.074 

62.0 

65.0· 

62.0 

64.0 

63.3 

.780.0 

0.43 

29.69 

70.0 

68.0 

69.0 

25 

5.090 

5.084 

1.001 

1.612 

1.002 

1.602 

0.05 

PASS 

0.14 

PASS 

RUN 2 

904.293 

899.200 

5.093 

65.0 

68.0 

64.0 

66.0 

65.8 

780.0 

0.43 

29.69 

69.0 

69.0 

69.0 

25 

5.090 

5.079 

1.002 

1.592 

0.3033 

1 

5 
----.... 

CON::OLE WORK SHEEr 

! KP~r. ______________ .3033 _ O!=eratcr. _p~B~___ 

Cate: Metsr 1.0. _:....-..______ . i2--I1·Y1 

Crffics Nemes:. _____ ,J" _ FreviClJS Y i=ac::cr. 1,06 3 

~:':~'1 ;-..J~:a 

ME: =---: ,'/CL.:..M:! L:;"~!:s .2. 

?.;,Gj .:.:l 

.\ :ri1·1 '71 19o~.~9~

:::;+..:U - ~"llf. ;00 i '1l:). lE> " Iil.et&( i3l7tFe(~a 

~;= &1­ "s­

'F' &.5 b~ 

·1 

- i el.m.£: ' 

I .e; 

1 I c,'J. , 6!f I 

I - "~ I c,tf I b& I 

I ~ , 7f10 I 7'rfj I 

! ~~;~o I .i.(? I .C./3 I 

I :_ L:.­ I ;}.9. b'{ 1 oj·b'f j of'. ,.~ 

- I 

INL.::.; 

• .... 

..' "­

• 

. ":.', . " 

.: : • ',I 

,«J 

I :r.ifat 

r::-.aJ 

;;-;~:a 

r:.::cl 

I.r.-:e 

Me!e.r.l!.."': 

esr~7:E"17.c:- "?:c~ ·I~ 

./ ?:ccm i.'am;:e,~"'a

I ~~-------------------------------------' 

Ii------:.-....~~~ :;:~ ';0: 70 .. ~ .=::t;.l 'F b't ~ ?'..!.li:;:: Va~4!;::l ~ii .. r:; 9., 

:..c­ - - -

-­ -- :::::::'E=:;::

=. - .-= - --~ S-=- - - - -.. 

. 

bCJ 

t7 

if.5' 

Cc~ 

r.::~ C-:.... _ _ ~"7",:-= __ _ 

£MlSSON 

SER'<,iIC"ES 

J. 

j 

I 

.... ..----­
ORIFICE BRACKETING 

,erator 

te 

Meter Number 

Meter Y Factor 

Meter Volume 

Meter Temperature 

Inlet 

Outlet 

Avg. Meler Temp 

Time 

.etar Delta H ~arometric Pressure 

Room Temperature 

Initial 

Final 

Avg.Room Temperature 

Pump Vacuum 

Vcr (std) 

Vm (std) 

Y Factor (brackets) 

+/- 2% Criteria 


Percent of Y 


• 

BB 

Dec 171999 

Final 

Initial 

Net 

Initial 

Final 

Initial 

Final 

1 

1.002 

Cubic Feet 

Cubic Feet 

Cubic. Feet 

Oeg.F 


Oag. F 


Oeg. F 

Oeg. F 

Oeg. F 

sec 


inches H2O 


inches Hg 


Oeg.F 


Oeg. F 


Oeg.F 

inches Hg 

dscf 

dscf 

BRACKET ORIFICES: 

Orifice No. 1 

K Factor 

Orifice No.2 

K Factor 

ORIFICE #1 

909.424 

904.300 

5.124 

68.0 

69.0 

67.0 

68.0 

68.0 

5 

0.3033 

2 

0.6426 

ORIFICE #2 

915.390 

909.500 

5.890 

69.0 

69.0 

68.0 

69.0 

68.8 

780.0 420.0 

0.43 2.10 

29.69 29.69. 

72.0 71.0 

69.0 69.0 

70.5 70.0 

25 21 

5.083 5.801 

5.088 5.864 

0.999 0.989 

0.31 1.28 

PASS PASS 
BRACKETING WORK SHEF I 

CFe!'E.tCr. _6_3~___ Meter LD. ____ ___ 

Date: .:5033 (s-) 1').-1/,9 'I K Fac:cr No.1 ...........-___-::.._ 

Fr6Vicl.'s '( F-sc:cr '.ex:>!).. K Fsc:cr No. 2 _,_<':,...:.tl_~_f..:, __(Q_)_ 

MET:'~ '/CU:ME L·r.i~s i 

I z l 

.1 

r:;,iti 

initiaJ 

IMat:r Tsmpsran.::e 

,.:; 

" 

.:.-'

., 1d-1 :3./:>0 

! 9/s- 390 

I 9t11. S-C' CJ 

I 

I

-1 

••~:~{) 

~" ..' .. ,1... " . 

I 

I' 

r 

. :./ 

I 

I 

~ 

iNt..=:: 

. CLiTl.::: 

I~ma 

Meter ;!.~ 

ir.lic1 

f:j,af 

~n:t!cl 

~r:aJ 

I 

I 

, 

I 

'F 

.~

. 

.c: 

.c:

. 

.!E:C 

- ,- ('l in. r-:.;;...i 

-

&~ 

b.Of 

I {,7 

I &~ 

I 73"0 

I ·Lf3 

I b7 

I. b7 

I b~ 

I 67 

I q:20 

I Q. I 

j 

I 

I 

I 

I 

I 

I , . EP.ICmetiic ~:::ss:..!:a :::. ~g I g.9·b~ ! ~1.b . I . I 

F:CC!7l Te..r;::; Q!a.h.:ie I -J 

;r.i;;c../ I I . 'F I 7~ I 7/ I 

;::;::l1.1 'F ~~ I I 69 I b9 ~ j

~ r4.!lT.p 'la~-,t.::;'l ./ :tl. F; I [;lS- I ~I I 

• 
METER CALIBRATION 

DO K Factor Operator 

ADele Dec. 17.1999 Meter Number 

1.017 OrificeNumber "Previous Y Factor 

RUN 1 

Meter Volume 

Final Cubic Feet 563.467 


Initial Cubic Feet 558.300 


Net Cubic Feet 5.167 


Meter Temperature 

Inlet 

Initial Deg.F 65.0 

Final Oeg. F 68.0 

Outlet 

Initial Deg. F 64.0 

Final Oeg. F 67.0 

Avg. Meter Temp Oeg.F 66.0 

Time 

Meter Delta H. ' .. 

sec 

inches H2O 

960.0 

0.30 

• Barometric Pressure inches Hg 29.69 

Room Temperature 

Initial Deg. F 69.0 

Final D6g. F 71.0 

Avg.Room Temperature De9· F 70.0 

Pump Vacuum inches Hg 24 

dscf 5.227 Vcr (std) 

dscf 5.149 Vm (std) 1.015 Y Factor 

1.640 Delta H@ 

1.016 Average Y 

1.628 Average Delta H@ 

-t/- 2% Criteria 

0.04 Percent of Avg Y 

PASS 

•

+/~ 5% Criteria 

0.14 Percent of Final Y 

PASS 

RUN2 

569.187 

564.000 

5.187 

68.0 

69.0 

67.0 

68.0 

68.0 

960.0 

0.30 

29.69 

69.0 

69.0 

69.0 

24 

5.232 

5.149 

1.016 

1.615 

0.2533 

2 

4 

, 

i 
- -

----~'" 

CON:50LE WORK SHE! 


Cp:rc.tcr. -'P.!2 ......--,I ___~_ :-< Fac:r: .d5'33


..:J['" Date:· /2)1=jJ..; 1- MetEr r.a. ~~----__ 

Frevicl.!S Y raccr: • /, Cit 7 

I ~~c., .'Jl!Ji':=;r 

- ME: =-~ '/CL:..ME \.::::3 2- . j I ,>.l ;:r,at ., I SC,9.1B7 I_ .....: I :r.f..::i " 5(,,'1,000 i IM~i..r iar.:F&t2n::1! J 

INLE: I I :i:!~ti . I c,,£ (e<J ,I 

r;:a.f ';:­ I ~-<t (;1 I 

( Cl.fi1.Er ....... 
 i

;rJ:a :;F r I I G7 I • :t') -p ...~,. 1=.::21 I I it :I :c~ ~ J I iirr:e s<-:: q~o I q(;,o I I 

Me,ar:!..:.o: :-~ ~!J I .30 I .30 I ~crr.at;ic" ;;:e("':""'~ - ~', .. 1.. I.~ I I '1. c; '1 .I ~~. c,'-1 I 

r.ccm Tam;::arc.:.;.--a '/ I 

I ~~~ J .:= 

1 ~q I c;<; I .; I . ~::aj I tF I '71 I 9't. 1

r',..!.I7:p VC!C""'::':::"l =........­ .. :.. I,:: I I I J,Lf I r2~ I 

~c~ 

-

--

----

-

.-

---

- CC."""''D):;'';:! !YU_~_ --:N~i'"Z ~ __

=. E-= - - EMISS:ON 

-

~ S-=­ -- -- SS"/IC".:..s e. -- ­

.. '-:'; 'J' . "­

'- . ~-- .. -­ - « 
ORIFICE BRACKETING 


Operator 
 Dec 171999 eta DD 

Meter Number 


Meter Y Factor 


Meter Volume 

Final 

Initial 

Net 

Meter Temperature 

Inlet 

Initial 

Final 

Outlet 

Initial 

Final 

Avg. Meter Temp 

Time 

_ster Delta H 

arometric Pressure 

Room Temperature 

Initial 

Final 

Avg.Room Temperature 

Pump Vacuum 

Vcr (std) 

Vm (std) 

Y Factor (brackets) 

+/- 2% Criteria 


Percent ofY 


• 

2 

1.016 

Cubic Feet 

Cubic Feet 

Cubic Feet 

Deg. F 

Deg. F 

Deg.F 

Deg.F 

Oeg.F 

sec 


inches H2O 


inches Hg 


Oeg. F 

Oeg.F 

Oeg.F 

inches Hg 

. dscf 

dscf 

BRACKET ORIFICES: 

Orifice No. 1 

KFactor 

Orifice No.2 

K Factor 

ORIFICE #1 

575.305 

570.100 

5.205 

69.0 

70.0 

69.0 

69.0 

69.3 

960.0 

0.30 

29.69 

71.0 

69.0 

70.0 

24 

5.227 

5.155 

1.014 

0.20 

PASS 

4 

0.2533 

1 

0.5055 

ORIFICE #2 

587.270 

582.000 

5.270 

69.0 

69.0 

70.0 

70.0 

69.5 

480.0 

1.30 

29.69 

72.0 

71.0 

71.5 

20 

5.208 

5.229 

0.996 

1.98 

PASS 
BRACKETiNG WORK SHEE f 
 r ~! 

e· ...-, Cperc.tcr: J2'D Meter 1.0. _--"""'.2..-,_~___ 

Date: !~h7/1f K Fac:cr No.1 '2£33 (tt) . 

. Previews Y Fac:cr I C?/Cz .K Fac.cr No. 2 • Son: (0 

~t~ErS \/CLL'.',AE l:;;r.s <: [ I 

~.j ..:.J i=::;ai .. I 576. ~5"" ! 5.-aZciil ZO I ~i1ital ., I ""' 5'70. /00 1511;<.000 1

IMatsr T~mr:=ia\U:'; I 

INt.::: I I 

;rJtiti 'f I I 

I Gq I I F:~cj .;:

. '9 I I 7t> I. G<:f 1 o' j CtJil..::: .".' ~-.\ I 

Jr.itia.i Of ~. ~~.'{:;) _. I I I Gq I zo 1 

:-:riai eF I I I c.,q I 70 i I Time I sec I ;fk'Q I ?f<?o j 

Meter::l.~ tn. ~O I I I ,'32 I /. '3 I 

I earcmetr.c ;::~"""..::a i::. ;-:g i I ~~,G~ I dC(." q I 

I Rccm Tem;:erc1l...""a 1 . ~ :rj1:al ·e. I I I 1/ I 7::< I 

[ :--:r:aJ 'F I J I (£1 I 71 I • '0 P!Jmp Vac-..:u.'7l :n.. r:g I .1 I ;2'1. I 20 i 

=.c = -- -- COMPRE........l:..:.'\lSL'v:s 

= -- E=­ EMISSION . ·S ­ -

~ -- S-":>vrC'::1:: Co:\. ___

- - ~ 

.

• 

.­
ORIFICE BRACKETING 


Operator 
 B8

Dec 171999
 ete 

4 Meter Number 

1.014 Meter Y Factor 

Meter Volume 

Final Cubic Feet 

Initial Cubic Feet 

Net Cubic Feet 

Meter Temperature 

Inlet 

Initial Oeg. F 

Final Oeg. F 

outlet 

Initial Deg.F 

FinaI Oeg. F 

Avg. Meter Temp Oeg.F

seC Time 

inches H2O _eter Delta H 

arometric Pressure inches Hg

Room Temperature 

Initial Oeg.F 

Final Oeg. F 

Avg.Room Temperature Oeg. F

Pump Vacuum inches Hg

Vcr dscf (std) 

Vm dscf (std) 


Y Factor (brackets) 


+/- 2% Criteria 


Percent ofY 


• 

BRACKET ORIFICES: 

Orifice No. 1 

. K Factor 

Orifice No.2 

K Factor 

ORIFICE#1 

528.895 

523.500 

5.395 

67.0 

69.0 

68.0 

69.0 

68.3 

780.0 

0.52 

29.69 

72.0 

72.0 

72.0 

24 

5.474 

5.356 

1.022 

0.79 

PASS 

3 

0.3271 

9 

0.7964 

ORWICE#2 

534.170 

529.000 

5.170 

69.0 

70.0 

70.0 

70.0 

6~.8 

300.0 

3.40 

29.69 

73.0 

71.0 

72.0 

18 

5.126 

5.154. 

0.994 

1.93 

PASS 
- -

8RP.CKETlNG WORK SHEt= i" 


Cl=ere.tcr. J.)33......______ 

Data: _\:;{ ~ n·'1: '1. 

Fre'licl.;s Y Fac:cr 1.01'-1 

Meter tD. ---""4'f--~----

K . .3all (::s) F~c:cr No, 1 _____..::.--,.... 

K ., 7'lbt./ C'1:) F~c:cr No.2 __...:...-..____ 

MEr::"~ ~Clt:ME L~::f!s 2­ I ~ I I - I :: J .,..:: )::":t:ai I I I j •• J s1.~. ~7S- i),YI" ttD I . ...:; f 1dt:t1 ,I ., IS";13.S00 I £<'9.000 I IMcMr r;;;~alf:!m,,::~ I­ I 

I Nt..::: 

~t;" I initial I . b7 I 

\ 

- 69 j 

i=:r.aI :.::: I - .""I bj I. 70 J 

! ~-'\ .' 1_- cun...::: .:. 

1 

- ~ 

- - ' 1 . ;". !r:iiiE1 t.;:

. I I I b~ I 70 -.;'-:.~ ~. - ',r'iI 

~::SJ 'f I I I bq I 70 

I Tirr:a I sac 

Meter ;;l.~ I ;n. ;--:0 

Sarcmetrlc P{~L.·:a I !r:. Hg 

r - - Rcc:":1 Ter.:F£tat.:l'a 

~ : lni;;~ j . 

-I:• 

I 7 if0 

I . :l 

I ~(ibq 

I 7~ 

I 

I 3:x:> ", I 3. t./ , 

I a1~b9 I 

I .. I 

P, I ?3 :=] 1- " .. 1 ,::; 

- I 7/ I Rr;2J 7:;{ 

P~mp '1tf..~":t.:t'7i , j :M. r.; 1 I Q4 I (~ .. ­

'C-~ 

- - COMl'E-"":..C.:.'!S'i'V=: =- r::::::::: -c-- [.MISsrON -- s-=-- l-...' ___ . ;::""v-:c--::::~ --;. .

• -

-

- -

­

' .. ~. 

-

- -

CONSOLE WORK SHE! 
 "

• 

.­ C~e~tc.r: ...;:::6--.6_"_____ K~r. __·~3a_/~I_________ ... : .. 

Date: L-I • I~ - 0- 'l~ Met=rlD. _----__~ 

Frnvicus Y Fac=r: ·99 :3 Ciffics Numcer. 3"---____ 

I ME; =.-: 'Ie L:.M~ t::::is 	 Z. j I i=.r;i!l ~ ,:nco. DOS- I S-~3. <'{'to I_ 
 Ir-----~--~-~~---~--~--S-I-~.~'~oo~--~i-s-18-.-ID-b--~i 

lINt.=: I 

I :r.::aJ ':=: I· t:o "3 .j 

:rj::~ =e 

I

I I 	G>t I bLj I 1:;:': I i=r.al I 164 	 ,& J 

Tirr:e 	 I I 	780 I 71'0 I . Me!e.r~~ ::t.. Foo:O 1 I 	.5"R I . S?-. I 

CStC:l.S!;iu- ;";:; ~ ~-r. ~; - . - I I ()'9·b'1 1~7'"b'r . I . I I ~ 

r:ccm i."""';:l;,'7.!.:.-a 

, 

CIJTt..::.: j 

~~ Of I I 70 i 71:> 


..' : I i=.:::;J I~ 'F I 7~ j 71 


j PI"::;:;:: '/aC"w~:;::J ~,,. r:~ . I 	 I ().Lj . I. 	 2~ 

-'C- -- -- CG;,y.u; ~ r..,o...~_~.... .... ;.. - Nr:;;-'v-:: _ 

=.

- E-==­ FM!SSiOli

• 	 ~ ·S .. ~ Sa"',11G5 

. - .. ~- .. --­
METER CALIBRATION 

BB KFactor operator Deo.17,1999 Meter Number te 0.993 Orifice Number

• evious Y Factor 

RUN 1 

Meter Volume 

Final Cubic Feet 518.005 

Initial Cubic Feet 512.600 

Net Cubic Feet 5.405 

Meter Temperature 

. Inlet 

Initial Oeg. F 60.0 

Final Deg. F 63.0 

Outlet 61.0 Initial D9g. F 

Final Oeg. F 64.0 

Avg. Meter Temp Deg. F 62.0 

sec 780.0 Time 

inches H2O 0.52 _eter Delta H inches Hg 29.69 arometrlc Pressure 

Room Temperature 

Initial Oeg. F 70.0 

Final Oeg.F 70.0 

Avg.Room Temperature Oeg. F 70.0 

inches Hg 24 Pump Vacuum 

dscf 5.484 Vcr (std) dscf 5.430 Vm (std) 1.010 Y Factor 1.728 Delta H@ 

1.014 Average Y 1.730 Average Delta H@ 

+/- 2% Criteria DAD Percent of Avg Y PASS 

• +/- 5% Criteria 2.07 Percent of Final Y PASS 

0.3271 

4 

3 

RUN 2 

523.490 

518.100 

5.390 

63.0 

67.0 

64.0 

66.0 

65.0 

780.0 

0;52 

29.69 

70.0 

71.0 

70.5 

24 

5.481 

5.384 

1.018 

1.731 
~----. _. 

AppendixF 


Process Data 


• 

---------.........--------, I! 

• 


• 


• 


Compliance Emission Test 


Operating Data 


Owner:Cargill,Inc. Date: December 9 & 10, 1999 

Source:EP# 11 -Bean Tallk. Conveying Permit #: 96-A-332-S3 

Maximum Continuous Process Rate {Manufacturer's Rating},.:;2..;.;43;...t;::o:;;nsIhr=-=so.::,y~b:.;:;ean=s________ 


Historical Average Process Rate..;..N.;..,;/A________________ _____ 


Historical Maximum Process Rate..:;.N;:.:/A~_____________________ 


Types and Sources ( if any) of Fuels normally 8umed,_N_/A_________ __ __ 


Type of Fuel Burned During this test..:;,N;:..::/A;.::-________--------___ 


If Fuel is us-ad ApprOXimate Quantities of each listed above burned Annually_________ 


Recycling Capability 

Recycling In Progress 

Pr:c08S$ Data Ot.! 'Jng BlJn~ 

Process Rate 


(gal/hr, Iblhr, tons/hr. etc ... ) 


Process Rate Wet 

Percent Moisture (%) 

Process Rate Dry 

How Process Rate was 

Determined 

Yes___ No X 

No X 

Run 1 Run 2­ Run 3 

204 tonslhr 240 tonslhr 204 tonslhr 

~nk levels 81ld throughput 

Person Responsible for Data,~B::::o=b::::_S.;..un-dIi.;..'-e--~--~:__-------------

Signature 3e~ 5Vv~\t~ 

ntJelPOSltionFacility Superintendent 

.... etease indicate in the same unilti. as your historical informatjon 
AIR :POLLUTION CONTROL EQUIPMENT OPERATING DATA 

• Plant Cargill.lnc._ Location Sioux City, IA 

SO"QIQI t~ ..e;;part1;:.;;;;;·c;.;::ul;;;;at;;;;e_______ Rated Production 243 tonsihr soYbeans 

Date 1219&1011999 TIme _____ Actual Production' 204,240,204 tons!hr soybeans 

AirFlaw Data _~~_______ Run No. 1,2,3 

~~------~~--------

Mechanical Collector. 

TIlbe Dis. in., Numbet ofTubes Design Ap ____in,. BiO Gas Temp __~ 

Observed t.\p in H~ Design Cfinltube @ Observed .6p __ @ "F 

FaD Rated liP. Operating Volts Operating Amp! _____ 

E1 'c_Pn:cinitaIOr 

FicldN'Q, Prlmaxy Se::ondary SCf:Onduy Spark Rate jPrimaIy 

Voltage (volts) ClUl'ent (amps) Voltage (KV) CUlTent (ma) <l'lermin) 

• Sgybber: 

Type . Ap{actoss scrubber) inH~O. 

FanRatedHP Opcnuing Volcs Openuing Amps 

Liquid Cin.-u.lation Rate gal/min. % MaJre-up Slowdown gpm 

Scrubbing Water Change Interval 

Settling Tank Cle:ming Interval 

Eaghousc: 

P~ositive Negative No. Compartments 

Type Cle:uring Clean Cycle • min 

Avg. Baghouse t.\p LO inH:zO L\pRango 

Fan: RatedKP. Ope:ating Volts Operating Amps 

Cyclone: 

Type top inH.p Diameter 

Fan R4lai EP Operating V?I~ , Operating Amps 

Person Responsible for Data .;;;:B..:;.ob;;...;;;.;Sun=dl_ie_______ __~_ 

Sig:narure ___________________ 

Tide/Position Facility S!¥,rintendent 

• 10 
• 


Appendix G 


Opacity C~rtification 

• 


• 


m7 ";] ," : 
DEPARTMENT OF NATURAL RESOURCES 

J. VILSACK. GOVERNOR PAUL W. JOHNSON, DIRECTOR 

SALLY J. PEDERSON, .IT. GOVERNOR 

November 10,1999 

Mr. Jay Titus 

Comprehensive Emission Services 

1112 Maple Street 

West Des Moines, IA 50265 

Dear Mr. Titus: 

We wish to acknowledge your attendance at the Fall 1999 session of the visible emissions 

recertification program conducted by the Unh'ersity of Iowa Hygiemc Laboratory on October 19 ­

20,1999. . 

The records show that you have successfully met the criteria for making visual detenmnation of th~ 

opacity ofemissions, as specified in subrule 567--29.1 ofthe Iowa Administrative Code. 

• Transmitted 'with this letter is a certificate indicating that you are qualified to make visible 

emissions evaluations pursuant to Chapter 567--29 of the Iowa Administrative Code. 

Notice of the Spring 2000 session v"ill be issued around the end of March 2000 and you ''''ill be 

infonned of the exact date and location ofthe next session. 

Sincerely, 

/7) ;/ /) /?J . j7/ 

~z.t:/::lPJ;i{Mf AIR QUALITY BUREAU IOWA DEPARTMENT OF !'<ATURAl RESOl'RCES 

VISIBLE EMISS10:\S EVALUATION CERTIACATE 

THIS IS TO CERTIFY THAT 

Enclosure Jay Titus ;.. (I~l:iti('d tt' trul~< ,·;..lNc: Cllli",...im~" of ;I1il pb!h.l'Iitd"l. pur"l,I:Jnl1r. Ch.'1r'd'·:'<-~~!·} oi tb.! l(t\\;, 

cc: Pamela Kastle, D.H.L. .~OJtlin~~U:'l;\'C ("(\dr. promulYifl!!rl \ltl~1 :.w'Mril~ ,,), ('h,,!XtT iI~..!;I;' ('~ ,.,Il"'a. 

• 


7900 HICKMAN ROAD. SUITE 1 f URBANDALE.IOWAS0322/515-242·5100 I FAX 515-242·5094 

es'" 1'.R d 
.......... -..".-.. _. ­

~ 

STAT~OF 

I~V\T~ DEPARTMENT OF NATURAL RESOURCES 

AS J. VII.SACK, GOVERNOR' PAUl. W, JOHNSON. DIRECTOR 

SALLY J. PEDERSON, LI. GOVERNOR 

November 16, 1999 

Dan Deatsch 


Comprehensive Emissions Servo 


1112 Maple St 


West Des Moines IA 50265 


Dear Mr. Deatsch: 

We wish to acknowledge your attendance at the Fall 1999 session of the visible etnlSS10nS 

recertification program conducted by the University of Iowa Hygienic Laboratory on October 19 ­

20,1999. 

The records show that you ha,'e successfully met the criteria for making visual detenninatiol1 ofthe 

opacity of emissions; as specified in subrule 567-~29.1 of the Iowa Administrative Code. 

• 

Transmitted with this Jetter is a certificate indicating that you are qualified to make visible 


emissions evaluations pursuant to Chapter 567--29 of the Iowa Administrative Code. 


Notice of the Spring 2000 session ,,,ill be issued around the end of March 2000 and you will be 

infol111ed ofthe exact date and location ofthe next session. 

Sincerely, 


'/7 /:('. (? ._£P
 ~",,/(pr;. Lf f..:..-;7k 

DOUGEAS A. CAt'JPBELL 

AIR QUALITY BUREAU 

IOWA DEPARThlENT OF ~ATURAL RESOl:RCES 

VISIBLE Ei\'IlSSIO"'S EVALUATION CERTIFICATE Enclosure THIS IS TO CERTl FY THAT 

cc: Pamela Kastle, U.RL. Dan Deatsch ! j"" Iltt:d.;n~rt to n\:)Le vi...ibk ... mi..~~'I1I" ,'If ait j')(Jlhlt'(Ul. pur"U:lIIt tn ("h~vl('r jr.;_.!'; l\lJb~ ~",.. .. 1\4I'llini..,,..,,,llyt Ccxi,~ promu~;nrd vnrt~r :.Iulher.t) (If ("jrJPI\"r"~!iU. ("(11ft' (Of Jl'~\:;' 

• 

7900 HICKMAN ReF,O. SUITE 1 I URBANDALE, IOWA 50322/515-242-5100 I FAX 515,242:5004 

•