. . . . , 

# •
. .. CARGILL,.· INCORPORATED·

. 

# ·>SICUX 

# CITY,- IOWA

....

. ; j 

# EMI·SSI.ONSTEST

... 

# RESULTS ".

. '. .



# ... ' . FROM TESTING 

# CONDUCTiED: 

# •. . .... Dl.=CEMBER 

# '7-10, 14-16 1999

. ' ..



# .... Thompson Environmental 

# Consulting, I,nc.

'. .' 11' t ... a member of THE COMPLIANCE GROUP 

# •
Environmental Engineering, Permitting rutd Compliance $eroices

# •
.; EMISSION TEST REPORT 

### for the Cargill Incorporated Soybean Processing Plant located in 

### Sioux 

### City, Iowa on December**7~10** 

### and, 14-161999



### Conducted by Comprehensive Emission Services 1112 Maple Street. 

### West Des Moines, Iowa 50265 (515) 225-7372 

### Project No. 8899


# •

# '. TABLE OF CONTENTS

CONTENTS
Preface
....................................................................... : ................................................ 2 Introduction
............................................................................................................... . 3 Summary of Results
................................................................................................... 4 Salllpling and Analytical Procedures
......................................................................... 9 Particulate Emission Results
...................................................................................... 12 M5 Sampling Apparatus
............................................................................................ 10 M17 SaltI.pling Apparatus
....................................................... ; .................................. 11 Appendix A" Example Calculations Appendix B- Laboratory Data Forms Appendix 

### C - Field 

### Data Forms Appendix D

- Pretest Calibrations Appendix 

### E - Posttest Calibrations Appendix F - Process Data
. Appendix G**~** Opacity Observer Certification
TABLES Table 

### 1, Summary of Test Results 

### Bean Dust Bag Filter (EP #2)
......................... .. 4 Table 1, Summary of Test Results Grain Dryer (EP #21)
..................................... .. 4 Table I, Summary of Test Results Grain Dryer II (EP #22)
................................... . 4 Table 

### 2, Summary of Test Results Hull Grinding (EP #4)
....................................... 5 Table 3, Summary of Test Results Meal Dust Grinding (EP #6)
............................ . 5 Table 4, Summary of Test Results Bean Tank Conveying (EP #11)
........................ 6 Table 5, Summary of Test Results Flaker Aspiration II (EP #13A)
......................... 6 Table 6, Summary of Test Results Hull Transfer Storage (EP #15)
......................... 7 Table 7, Summary afTest Results Pellet Transfer (EP #20)
.................................... 7 Table 8, Summary of Test Results Bean Conditioner (EP #27)
............................... 8 Table 9, Stunmary of Test Results Pellet Cooler (EP #28)
............................... » ...... 8

FIGURES 

# .' Figure 1, M5 Saxnpling Apparatus
................................................................. · ........... 10 Figure 2, M17 Sampling Apparatus
......................................................................... . 11

# • PREFACE
This report slll!1.IIUU'izes the results of the data collected for compliance testing 

### performed at the 

### Cargill Incorporated plant in Sioux 

### City, Iowa To the 'best of 

### our knowledge, the 

### data in this report are accurate and complete. Any questions concerning this report should be directed to Mr. Tim Titus or 

### Mr. Jay Titus. They may be reached by phone at (515) 225-7372.

Jay Titus 

### Test Leader 

# h
• ',,­ 

# \

December 17, 1999



# •

2

# • INTRODUCTION
Emission testing was conducted by Comprehensive Emission Services on the following sources using the corresponding methods. Testing was conducted at the Cargill Incorporated plant, Sioux City: E.P. #2

- Bean Dust Bag Filter, Method 5 with 

### 202 backhalf, TSP and, Opacity. E.P. #4

- Hull Grinding, Method 5 with 202 backhaJf, TSP and, Opacity. E.P. #6

- 

### Meal Dust Grinding) Method 5 with 

### 202 backhalf, TSP and, Opacity. E.P. #11- 

### Bean Tank Conveying, Method 5 with 202 backhalf, TSP and, Opacity. E.P. #13A

- Flaker Aspiration II. Method 5 with 

### 202 backhalf, TSP and Opacity. B.P. #15 Hull Transfer Storage. Method 17 

### with 202 backhalf, TSP and Opacity. E.P. #20

- Pellet Transfer, Method 17 with 

### 202 backhalf, TSP and, Opacity. 

### E.P. #21

- Grain Dryer, Opacity. , E.P. #22

- Grain Dryer II. 

### Opacity. E.P. #27

- Bean**Conditioner~** 

### Method 5 with 202 backhalf, TSP**an~** 

### Opacity. E.P. #28

- Pellet Cooler, Method 5 with 202 backhalf, TSP and, Opacity. The test results for these sources appear in order by emission point number. The testing 

### was performed on December 7-10 and 14-16. 

### 1999. Coordinating the 

### field tests: Tim Titus

- Comprehensive Emission Services Lisa Schmidt

- Thompson Environmental Consulting Conducting the field tests: Jay Titus

- Comprehensive Emission 

### Services Chad Siems**~** 

### Comprehensive Emission Services Mike Ankerstjerne

- Comprehensive Emission Services Dan Deatsch

- Comprehensive Emission Services Brad Buckley

- Comprehensive Emission Services Doug Ostrander

- Comprehensive Emission Services Witnessing the field tests: 

### Aaron Wauters**~** 

### University ofIowa Hygienic Laboratory Matt Lyon

- University ofIowa Hygienic Laboratory The appendices to this report contain the following infonnation and data: Appenclix A: Example Calculations 

# • Appendix B: Laboratory Data Forms Appendix C: Field Data Fanns Appendix D: Pretest Calibrations Appendix E: Posttest Calibrations Appendix F: Process Data

,. J ' 

### Appendix G: Opacity Observer Certification

3

# I SUMMARY OF RESULTS 

## I­ ! In accordance with current IDNR protocol, when less than 10 mg of sample is collected, 

# .' I

10 rug of sample catch is used for calculations. Sources with sample collections less than 1 • 10 mg are shown with a 

### '<' symbol 

### in the following tables to indicate that actual samples were less than the assumed 10 mg catch. Both the actual and the assluned emission rates can found in Appendix C. 

# I , 

## I 1 

## I I**~** .

, !**~** 

### .

# -. Table 4 summarizes the test results for testing performed on the Bean T auk Conveying (EP # 11) at the Cargill Corporation facility in Sioux City, Iowa. EPA Method 5 with 202 backhalf, TSP and, Opacity 

### were used for testing. PMIO emissions will have to be assumed from the TSP samples for this sources. Testing 'Was performed on December 9 and 10, 1999. The teSting fulfills the requirements for testing in the IDNR Permit # 95­ A-324-S3_ The allowable limit for TSP is 0.006 gr/dscf and 1.40 Iblhr. The allowable limit for PMlO is 0.003 gr/dscf and 0.60 Iblhr. The allowable limit for Opacity is 0%
.

. Table 4 S.uBllnary of Test Results Bean Tank Conveying (EP #11J units 

### Run 1 Run 2 Run 3 Particulate Net Weight g <0.0100 <0.0100 <0.0100 

### Particulate Emissions gr/dscf <O.QOll <0.0012 <0.01)11 Particulate Emission Rate lblhr <0.25 <0.26 <0.25 Opacity % 

### 0.0 0.0 

### 0.0

_ Flow Rate dscfin 26,877 25,941 26,033

Flow Rate acfm 27,093 25,784 25,763 Isokinetics % 99.0 95.7 98.5 Start Time HltMM 8:50 . 13:17 7:22 

# .­

, ---.:;

# • SAMPLING AND ANALYTICAL PROCEDURES Sampling Procedures 

### Particulate emissions were determined 

### by U.S. Environmental Protection Agency (EPA) Methods 1,2,3,4,5, 17 

### and 

### 202. These 

### Methods are titled; 

### Method 1 - "Sample and Velocity Traverse for Stationary Sources" Method 2 - "Determination of Stack Gas Velocity and Volumetric Flow Rate" Method 3 - 

### "Gas Analysis 

### for Carbon Dioxide, Oxygen, Excess Air and Dry Molecular Weight tl 

### Method 

### 4 - "Determination for Moisture Content in 

### Stack Gases" Method 5 - "Determination 

### of Particulate Emissions.from Stationary Sources" Method 17

- "Detennination 

### of Particulate Emissions from Stationary Sources, In-Stack Filtration 

### Method" Method 202

- 

### "Condensible Particulate Emissions" These methods appear in 

### detail in Title 40, Code of Federal Regulations (CFR), Part 60, Appendix A, 

### and Part 51, Appendix M. 

# • The Sampling Apparatus is shown in Figure 1 on Page 10. All equipment was calibrated at Comprehensive Emission Services' office prior to shipment to the test site,

. Sampling Locations 

### The stack 

### sampling point locations can be 

### found along with 

### the fieLd data sheets in Appendix C. Analytical Procedures 

### The particulate emission rate was detennined following procedures detailed in EPA Methods 5 and 202. Particulate samples collected on Whatman glass fiber filters were analyzed gravimetrically. The probe and nozzles were rinsed with 

### acetone. The rinse was transferred to tarred beakers and evaporated to 

### dryness. The 

### back-half water was collected and separated into organic and in-organic parts. The samples were then transferred to tarred beakers and evaporated to dryness. 

# •

9

# • • •

Probe Nozzle S Type Pitot Tube

Thermocouples Fine 

### AdJus.t Orifice

Meter 

# >, Leak Free Pump 

### Schematic of 

### Method 

## 5 Sampling Figure 

### 1 Heated Filter

# ~ Ice. Bath
Vacuum Gauge



### Train Exit Temp

Sample Line

# • • •

Stack In-stack: T hermocoup Ie Filter Sample Probe
Probe Nozzle S Type Pitot Tube

Thermocouples Orifice 

### Dry Gas Meter


### SC/lematic of Method 17. . Ice Bath Sample line Fine 

### Vacuum Adjust Gauge

Leak Free· Pump 

### Sampling Tra in

# • Particulate Emission Results Bean Tank Conveying (EP #11) 

### Parameters 

### Units Run 1 Run 2 Run 3 TSP Emissions Actual 

### gr/dscf <0.0011 <0.0012 <0.0011 

### Weight Collected g <0.0100 <0.0100 <0.0100



### Emission Rate Iblhr <0.25 <0.26 <0.25 

### Opacity % 0.0 0.0 0.0 

### Stack Flow Rates Velocity ftImin 3,440 3,274 I 3,271



### Actual acfm 27.093 25,7&4 25,763 

### Sta.ndard Conditions dscfin 26,877 25,941 26,033 

### Sampling Results Isokinetics % 99.0 95.7 98.9 

### Sample Volume dscf 143.716 134.137 139.028 

### Ave. Stack Temperature 

### OF 63 

### 56 56

Ave. Square Root AP inchesHzO 1.0195 0.9772 0.9772 

### Ave.AH inchesH:p 1.46 1.38 1.38 

### Ave. Meter Temperature 

### OF 88.3 89.9 89.9 

### Oxygen % 2l.00 21.00 21.00 

### Carbon Dioxide % 0.00 0.00 0.00 

### Moisture Collected m1 28.5 27.0 15.0 

### Moisture % H 2 0 0.9 0.9 0.5 

### Run Start Time HH:MM 8:50 13:17 7:22 

### Sampling Time minutes 240 240 240 

# .>



# •

15

# • AppendixA . Example Calculations

' 

# •

. '

# • S'lIDbol 

### acfm As Bws 

### C,**~.** DII 

### dscfm gr/dscfrn ID 

### Md Ms**~** Ph 

## P, SF 

# • Tm Ts Vi V, Vf;l VI1'IM Vs**W~** \VtE.=':' Y 

# e % 

### H 2 

### O % COl 

### % O 2 

### %1 liH liP 

# • NOMENCLATURE Descriptio.n 

### Actual cubic feet per minute Area of stack 

### Percent 

### water Pitot rube. 

### calibration coefficient
. Concentration 

### of particulate dry 

### basis, standard 

### conditions Diameter of nozzle Dry standard cubic feet per minute Gzains per dry 

### stancwd cubic feet per minute Inside diameter of stack Molecular weight, dry 

### stack gas 

### Molecular weight, stack 

### gas Stack flow rate, dry 

### standard conditions 

### Barometric pressure Stack pressure Static pressure 

### Average meter temperature Temperature of stack gas 

### Initial meter reading Final 

### meter reading 

### Volume meter, actual Volume meter, standard conclitions A 

### verage stack gas velocity Total moisture collected Total particulate 

### matter collecred Meter correction factor 

### Sampling- rime Percent moismre by 

### volume Percent carbon 

### dioxide by volume, 

### dry Percem oxygen by 

### volume, dry Percent isok:i.ietic 

### Pressure drop across orifice meter 

### Gas velocity pressw-ePARTICULATE CACULATION EQUATIONS 

### Run I 1. Volume of meter



### Vol 

## = (1036.655

- 842.400) x ].003 V,;, =:; 194.838 fl3
2. Volume of meter, standard conditions (68" 

### ,29.92 in.Hg)



# . (.AH) 17.65x 

### Vm x 

### p" 

### +­ 13.6 T17I 

### +460 

# ( . 1 92) 17.65x194,838x 29.96+-'­ 

### V 

## = 13.6

lII(ml) 75.2 + 460

3, Percent moisture by volume
B = lOOx0.4707x We

lIl< 0.04707 X 

### We + V"'($/d) B :=:. 100x 0.4707 x47.0

"'.. 0.04107 X 47.0+193.394

4. Molecular weight, dry stack gas



### Mti =O.l6xO.OO+21.00+28.0 

### Md =28.845. Molecular weight, stack gas 

# M :=. 

# MdX(l-**Bws)+18X(1~ B~)**  s 100 100


### M ",,'

# 28.84X(1-~)+18X(1-..!..:!.) s 

### 100 100 

### Ms = 28.72
6. Stack Presure



### P == 29.96+ 0.05

s 

### 13.6 

# .1 1'.. = 29.96 inch. Hg
1. Velocity of stack gas T +460 

# (JKP) V. 

## = 60x 85.349 

### xC x S X An



### .. . p 

### P +M or ",'g S .Y • 78+460 Vs 

### = 60x85.349xO.84x X 0.7260

# ~ 29.96 

### + 28.72 

### Vs =: 2,472 

### ftlmin
8. Percent isokinetic
100 x 

## (Ts + 460) x Vm($/rl) %1 ==**----......:....:..--~~::.:.::..<----:** 

### 17.65x8xV.xp 

# X(l-:- B
.... 

# )X7rx(D II 

# )2 •. • 100 24
%1 = lOOx(178+460)x193.394 

### 17.65x 240x 2,472 

### x 29.96X(1

# ~)x 7rX 

### (.250)2 

### 100 24
%1 =: 98.09. Area 

### of stack 

### A 

### = 1t' 

# X(ID)2

s 24


### A 

## = 1t' 

# X(30.00)2

s 24



### 10. Stack volummetric flow rate 

### actual conditions



### Qa 

## = 2,472 x 4.91 Qa "" 

### 12,136 actin 

### 11. Stack volununetric fiowrate, 

### standard conditions (68" , 29.92 in 

### .Hg)

17.65x 2,472 x 4.91x 29.96 X 

### (1- 

# 1.:!.J 100 QSIJ. == 

### 78 

### + 460 Q.flJ =**11~803** 

### dscfm
12. Grains per dry standard cubic feet 15,43 x Wt 8,,;)1 == 

### ---=­
15.43xO.OllO = 

# • C s1d 193.394

em! 

## = 0.0009 gr/dscf13. Emission rate 

# • 1b 60x Wtgaiu X QSld - = 

### hr 453.5924 x**V.,(~<f]** 

### Ib 60x O .Ol10x 11,803 - = 

### hr 453.5924x 193.394
Ib ;::: O.091blhr hr


# •

•

# • AppendixB Laboratory Data Forms 

# •

•

# <:-c;. 

# 1<1 

# • Project Number:**:---u~~** -:!-,;,.-I ---r-,;--­ 

### Plant 

### Name:
. 

### Lqlji 

# 'f
- StUff 

## r C;/ 

# r'1 Date: 

## IJ. _/'VY 

## r Analy.sis Type:**_.....Jt:.......)~p** 

# ____ _ Run I 

## £PI/ Type Identification Final Tare Net Number Weigbt Weight Weight Filter 

# F S'Gj 1 1 

# 0:rtr. .3.0:<77 

# 0, ()OOD PIobe Rinse ( ml) 

# trfd-.i- 

# C/l.**9~J0** 

# L 

# C !-/,**7l-/~** 

# r 0,0012 Organic ( ml) 

### C (\ 

## 1. 

# q 

# iO'. Li"f**5~** 

# I 

# at.c-f 1- 

# 0/ O,OO}() Inorganic 

## D 1 <J

### G~I 

# n1,95J7**i~** 

## 1-.**1{,/~** 

# 4 010053
. Total Net Weight 

## O,OOY,SRun 

## Z Type Identification Final Tate Net Number Weight Weight Weight Filter 

# p**Cf~}**

### 510)~}:< 

# JI O:J. J 

# i 010003 PIobe Rinse ( ml)

### .t}9-2~ 

# 1f. 0 

# I**~'i** 

# t7- 1 

## 0/3r 

# 0, Dory Organic ( ml) 

### C 1\') 

### 0 

## )0**?,~10,**

## JOJ/1/~f 

# O. 00' t-f Inorganic 

### 01,Ob) J 

# 5'. l-Jc,/1' IS" L../ lr 

# IS3**O,OO~J** Total Net Weight 

# 0.0011 Run 

## 3' Type Identi fication Final Tate ) Net Number Weight Weight Weight**.~** Filter 

# F ?; 

# 1o 3,0(1,2 ).0/9) 

# O.OOO{) PIobe Rinse ( mI) 

## .e/:;2<? 

# £t,**'b2~** 

# I 

# t 

# t. C[ 

# J.:{"f 

# _at 00**I~** Organic ( mI) 

### C 

### 1/ 'j ) 

## )0 

# '6,**5~** 

# 11 

# 10'/, y}?? ()I 

## OO( 3 Inorganic 

# o "Z'fJ 

## G.6**l~t.~3i-' l~tl** **~3~1** 

# DIDO» Total Net Weight 

# O.**GO~2** Blanks Type Identification Final Tare Net Number Weigbt Weight Weight Water Blank ( ml) Acetone Blank ( mI)**MeC~** Blank ( mI) 

# O
.. /l(}l),


# •

•

Identification F**~** 3 inch ruter P '" 47mm filter B - 150m] Be<lktr C 250m) Beaker D" 400ml Beaker c

# • • FINAL WEIGHT WEIGHING SHEET 

# ' 

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### ,b: ') Ii Date Analyst
ID No. Run 1 2 

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## m No. RUn 

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________________ __________ 11

.Run No. Location: Cargill ep11 Date: Project # Isokinetic:;: Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu Ftlmin)=· Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Oeg)= Barometric Pressure (in Hg) :;; Static Pressure (Inches H20)::: Stack Pressure (in Hg)= Percent Oxygen :: Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water:::: Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp {F)"" 

### :Jry Molecular Weight:: • Wet Molecular Weight= Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Diameter (Inche s )= Stack Area (Square Feet) :;; Pitet Coefficient= Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)=**P~rticulate** Loading**~** Front Half Particulate Weight Net (9)= Paticulate Loading. Dry Std. 68 Deg (gr/set): Emission Rate (Ib/hr)= Particulate Loading
- Total Catch Including fmpingers Particulate Weight Net (9)­ ;**Partic~late** Loading, Dry Std. 68 Deg (grlscf)= •
. Emission Rate (rb/hr)= Percent Impinger Catch= 1 Assumed 10mg Dec 9, 99 

### 8899 99.0 72.400 223.524 0.993 0.004 150.066 143.716 29.65

0.60 29.69 21.00

0.00 28.5·

0.9 88.3 1.46 1.2621 63 28.84 28.74 240.0 0.180 38.00

7.88 0.84 1.0195

3,440 27,093 26,877

0.0022 0.0002 0.05

0.0100 0.0011 0.25 78.00Run No. Location: Cargill ep11 Date: Project # 

# .0/ 0

Isokinetic= Initial Meter Volume (Cubic reet)= Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Oeg)= Barometric Pressure (in Hg) ;: Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent oxygen := Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water: Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)::: Average Stack Temp (F)= Dry Mo[ecular Weight:: • Wet Molecular Weight::: Sampling Time (Minutes);;:.; Nozzle Diameter(lnches):: Stack Diameter (Inches)= Stack Area (Square Feet) == Pitot Coefficient= Average Square Root of Delta P (inches H20}:;:: Stack Velocity (Actual, fUmin)= Flow Rate (Actual, Cubic ftlmin)'" Flow Rate (Std, Dry. Cubic ftlmin 68 Deg)= Particulate Loading
- Front Half Particulate Weight Net (9)= Paticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lb/hr)= Particulate Loading**~** Total Catch Including lmpingers Particulate Weight Net (9)= Particulate Loading, Dry Std. 68 Deg (gr/sct)"" Emission Rate (Ib/hr):::: • Percent Impinger Catch::: Dec 9,99 

### 8899 99.0 72.400 223.524 0.993 0.004 150.066 143.716 29.65

0.60 29.69 21.00

0.00 28.5

0.9 88.3 1.46 1.2621 63 28.84 28.74 240.0 0.180 38.00

7.88 0.84 1.0195

3,440 27,093 26,877

0.0022 0.0002 0.05

0.0085 0.0009 0.21 74.12Run No. Location: Cargill ep11 Date: Project # 

# e% Isokinetic= Initial Meter Volume (Cubic Feet)=: Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin):: Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet 68 Oeg)= Barometric Pressure (in Hg) = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen = Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water- Average Meter Temperature (F):.: Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)= 

# e Dry Molecular Weight::::; Wet Molecular Weight= Sampling Time (Minutes)::; Nozzle Diameter(lnches)= Stack Diameter {Inches)= Stack Area (Square Feet) ::; Pitot Coefficient= Average Square Root of Delta P (inches H20)"" Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= Particulate Loading
- Front Half Particulate Weight Net (9):::: Paticulate Loading. Dry Std. 68 Deg (grlscf)= Emission Rate (Ib/hr):::: Particulate Loading
- Total Catch Including Impingers Particulate Weight Net (g)= Partic.ulate Loading, Dry Std. 68 Deg (grlscf)= 

# e

, Emission Rate (Ib/hr)= Percent Impinger Catch;:; 2. Assumed 10mg Dec 9,99 

### 8899 95.7 223,900 365.388 0.993 0.005 140.498 134.137

29.65

0.60 29.69 21,00

0.00 27.0

0.9 89.9 1.38 1.1613

. 56 28.84 28.74 240.0 0,180 38.00

7.88 0.84 0.9772

3,274 25.764 25,941

0.0022 0.0003 0.06

0.0100 0.0012 0.26 78.00Run No. Location: Cargill ep11 Date: .roject# % Isokinetic== Initial Meter Volume (Cubic Feet)::: Final Meter Volume (Cubic Feet)= Meter Factor- Final Leak Rate (cu Ftlmin)= Net meter Volume (Cubic Feet):.:: Gas Volume (Dry Std Cubic Feet 68 Deg}:::: Barometric Pressure (in Hg) 

### = Static Pressure (Inches H20);;; Stack Pressure (in Hg)= Percent**Oxyg~n** ::: Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water- Average Meter Temperature (F)= Average Delta H ( in H20)= Average Delta P (inches H20)= Average Stack Temp (F)::: Dry Molecular Weight:::: • Wet Molecular Weight: Sampling Time (Minutes)= Nozzle Diameter(lnches)= Stack Diameter (Inches};:: Stack Area (Square Feet) 

## = Pitot Coefficient= Average Square Root of Delta P (inches H20):: Stack Velocity (Actual, ftlmin)= Flow Rate (Actual, Cubic fUmin)= Flow Rate (Std, Dry, Cubic ftlmin 68 Deg)= Particulate loading

- Front Half Particulate Weight Net (g)= Peticulate Loading, Dry Std. 68 Deg (grlscf)= Emission Rate (lblhr)= Particulate Loading
- Totar Catch Including Impingers " Particulate Weight Net (g)=

Particulate Loading, 

### Ory Std. 68 Deg (grlsc:f)= • Emission Rate (lbfhr)= Percent Impinger Catch: 2 Dec 9,99 8899 95.7 223.900 365.388 0.993 0.005 140.498 134.137 29.65

0.60 29.69 21.00

0.00 27.0



### 0.9 89.9 1.38 1.1613 56 28.84 28.74 240.0 0.180 38.00

7.88 0.84 0.9772

3,274 25,784 25,941 : .

0.0022 0.0003 0.06

0.0079 0.0009 0.20 72.15Run No. location: Cargill ep11 Date: .roject# % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)'" Meter Factor::: Finsl Leak Rate (cu Ftlmin)== Net meter Volume (Cubic Feet):: Gas Volume (Dry Std Cubic Feet 68 Oeg)= Barometric Pressure (in Hg) 

# = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen ;;;; Percent Carbon Dioxide= Moisture Collected(ml)= Percent Water::: Average Meter Temperature (F);' Average Delta H ( in H20)= Average Delta P (inches H20)=**~verage** Stack Temp (F)=

..**~ry** Molecular Weight=

.. Wet Molecular Weight::! Sampling Time (Minutes)""­ NoZzle Diameter(lnches)=­ Stack Diameter (Inches): Stack Area (Square Feet) ::: Pitot Coefficient:::: Average Square Root of Delta P (inches H20)= Stack Velocity (Actual, fVmin)= Flow Rate (Actual, Cubic fVmin)== Flow Rate (Std, Dry, Cubic fVmin 68 Oeg)= Particulate Loading
- Front Half Particulate**Wejgh~** Net (g):: Paticulate Loading, Dry Std. 68 Oeg (grlscf)= EmiSSion Rate (Ib/hr)= Particulate Loading
- Total Catch Including Impingers Partlculate Weight Net (g)= Particulate Loading, Dry Std. 68 Deg (grlscf)= • Emission Rate (lb/hr)= Percent Impinger Catch= 3 Assumed 10mg Dec 10,99 

### 8899 98.9 365.700 512.347 0.993 0.002 145.620 139.028

29.65

0.60 29.69 21.00

0.00 15.0

0.5 89.9 1.38 1.1613 

### 56 28.84 28.79 240.0 0.180 38.00

7.88 0.84 0.9772

3,271 25,763 26,033

0.0014 0.0002 0.03

0.0100 0.0011 0.25 86.00RUn No. location: CargHl ep11 Date: • roject# % Isokinetic= Initial Meter Volume (Cubic Feet)= Final Meter Volume (Cubic Feet)= Meter Factor= Final Leak Rate (cu FUmin);:: Net meter Volume (Cubic Feet)= Gas Volume (Dry Std Cubic Feet as Oeg)= Barometric Pressure (in Hg) 

# = Static Pressure (Inches H20)= Stack Pressure (in Hg)= Percent Oxygen 

# = Percent Carbon Dioxide= Moisture CoHected(ml)::: Percent Water: Average Meter Temperature (F)= Average Delta H (in H20): Average Delta P {inches H20)'" a'::,verage Stack Temp (F)= 

# w::ry Molecular Weight= Wet Molecular Weight: Sampling Time (Minutes):::: Nozzle Diameter(lnches)= Stack Diameter (Inches)= Stack Area (Square Feet) Pitot Coefficient'" Average Square Root of Delta P (inches H20)::: Stack Velocity (Actual, ftfmin)= Flow Rate (Actual, Cubic ftlmin)= Flow Rate (Std. Dry, Cubic ftlmin 68 Deg)= Particulate loading Front Half**P~rticulate** Weight Net (g)= Paticulate Loading, Dry Std. 68 Deg (grlscf}::: Emission Rate (Ib/hr)= Particulate Loading Total Catch Including Impingers

. Particulate Weight Net (9)= Particulate Loading, Dry Std. 68 Deg (grlscf)= • Emission Rate (lb/hr)=

. Percent Impinger Catch'"" 3 Dec 10, 99 

### 8899 98.9 365.700 512.347 0.993 0.002 145.620 139.028 29.65

0.60 29.69 21.00

0.00 15.0



### 0.5 89.9 1.38 1.1613 56 28.84 26.79 240.0 0.180 38.00

7.88 0.84 0.9772

3,271 25.763 26.033

0.0014 0.0002 0.03

0.0062 0.0007 0.15 77.42COMPREHENSIVE 

### EMISSION SERVICES

Project Number..--;g=g..:.q'_"1'--

__ ..

### ~_ Project Leader 

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___________ _ Meter Operator 

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### J.Ho Umbilical Number 100 

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# e. 29. -3 Pilot Number

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### 7':<,'toQ ! Final Meter Volume (fr) 223 L52.t1.

Leak Rate Before 

### 0.010 CFM@ ;;; 15 in. Hg Leak Rate After 

### O,O(J<i CFM@ 

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### RECOVERY DATA Orsat lmpingers

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### ....<..:M
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___________ _ Date

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## La 

# r., u 

## I**~tion** __**~1=5~p~/~I** 

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### _~::Z""'--_ Meter Number 

### -:JjZ" Minutes Per Point (min.)....!.!l....... Oven Number -,--

__ __ \ ( r) i**S~pling** Time (min.) ;2.. 

### 'i9 Umbilical Number 100 BIl4of:.. Meter Factor Y O. 

### qCJ 3 Pitot Number

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# .' Pitot Coefficient Cp 0, 

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### _:$""",,,,8

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### 5'5 Schematic of Testing Location 

### 36 Stack Axis 2 (inch.)

___ _ Barometric Pressure (in. Hg) 

### J 9, , 

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### 0.005 in, Hg Pitot Leak Check Before /,./'**~** After RECOVERY DATA Orsat lmpingers 

# • Notes: Filter Number:

_ 

## F 8b 5 Trial %CO l %C0 2 +%02 %0 2 1 /'\ 2 

# fl f'1

## ~"PY1 i 3 ,/ VI' '/r I Avg Fioal Initial Difference Impinger 1 

# 55 /0_0 

# -ys Impinger 2 

### i12. /00 

## 22 Impinger 3 

### /10 100 

### 10 Impinger 4 

### 79-{,S 

### 7/4,5 (.(0 Condi tion/Co lor Total 

# ).1Run No. 

## :d 

# • :-"ntJ:1 Project No.**--'~"""""'-'_'--** ____ _ Location Cc.Yfj; 

## If EPII Date 

## 1119/19 I Operator ----.!:..A=ifA:..I.

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____ _



# • " Noles: COMl'RE."tE.
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## _.

. COMPREHENSIVE



### . EMISSION SERVICES

Project

### NUIIlber_~'gioi.l8.c....'1~1..L.- ____ _ Project Leader**_:.::.D_Oc...-_~** 

### _____ _ Run Number

__ 

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### ______ _ Date 1:;)00 

## /91 Lab Person _-

___ --

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### 0/ 

## '7'22 Pitot Number

__ _ Meter tlH@

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__ _ 

## 3 1 Pitot Coefficient Cp 

### (},g'-l Probe Length**_~_** Stack Axis 1 (iDch.) 

# 3..8 Nozzle Type _-,-S
__ Schematic of Testing Location Stack Axis 2 (inch.) 

### '3 

## g BaromelIic Pressure (in. Hg) Static Pressure (in. HzO)**_...:.(..:::.(p~O:!........** __ Nozzle Diameter (iDeh.) _,_1..;;;:£-.,0

__ _ Initial Mete! Volume 

## efr)**~(o5'1-00**
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# or) 512, Y/7C

Leak Rate Before 0.OQ7 CFM@**~** 15 in.Hg Leak Rate After 0, 0 (? 2 CFM@ 

# J in. Hg Pitot Leak Check V" Before t.,./ After 

### RECOVERY DATA Orsat Impingers 

# • Notes: Filter Number: 

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## 133.c '9'b Q 

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CO:MPREHENSIVE EMISSION SERVICES

### COMPREHENSIVE EMISSION 

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# • AppendixD Pretest Calibrations· 

# •

•METER CALIBRATION 0.3033 K Factor DO 

### 1 Operator Meter Number Dec3, 1999 1.004 Orifice Number

# '.~iOUS Y Factor 5

...... ,



### Meter Volume Final Initial

Net Meter Temperature Inlet Initial Final Outlet Initial Final Avg. Meter Temp Time _eter Delta H arornetric Pressure '. Room Temperature InItial Final Avg.Room Temperature Pump Vacuum Vcr (std) Vm (std) Y Factor Delta H@ Average Y Average Delta H@ +/" 2% Criteria Percent of A vg Y

• +/- 5% Criteria Percent of Final Y CubIc Feet Cubic Feet Cubic Feet
Oeg. F Oeg. F oeg.F Deg.F Oeg. F

sec inches H2O

inches Hg

Oeg. F Deg.F Deg.F inches Hg dscf dscf RUN 1 211.466 206.000 5.466

65.0 67.0 63.0 65.0 65.0 840.0

0.41 29.27

71.0 71.0 71.0 

### 23 5.394 5.381 1.002 1.564 1.003 1.556

0.04 PASS
0.13 PASS RUN2 217.185 211.700 5.485

68.0 69.0 65.0 67.0 67.3 840.0

0.41 29.27

71.0 71.0 71.0



### 23 5.394 5.377 1.003 1.547

## CON5CLE WORK SHE I



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# -ORIFICE BRACKETING BRACKET ORIFICES: 5 Orifice No. 1 0.3033 K Factor 

### 2 Orifice No.2 0.6426 K Factor ORIFICE #2 ORIFICE #1 223.012 229.990 217.500 224.100 5.512 5.890

69.0 71.0 70.0 71.0 67.0 69.0 69.0 69.0 

### 68.8 70.0 840.0 420.0

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### 71.0 72.0 11.0 72.0 

### 71.0 72.0

21 19 5.394 

### 5.708 5.388 5.768 1.001 0.990

0.20 1.34 PASS PASS 

### operator 

# e te Meter Number Meter Y Factor
Meter Volume

Meter Temperature Inlet
Outlet Avg. Meter Temp Time**~eter** Delta H .Barometric Pressure "Room Temperature InitIal Final Avg.Room Temperature pump Vacuum Vcr (std) Vm (std) Y Factor (brackets) +/- 2% Criteria Percent ofY 

# • DD Dec. 3,1999

Final Initial

Net

Initial Final Initial Final 

### 1 1.003

Cubic Feet Cubic Feet 

### CubiC Feet
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sec inches H2O

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# - 

# -
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# - 8R;\CC<tJ lNG WORK SHEE I
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### Nov. 24, 1999 Meter Number

ate • 

### 1.015 Orifice Number revious 

### Y Factor

RUN 1 Meter Volume Final Initial

Net Cubic Feet Cubic Feet Cubic Feet 

### 446.707 441.700 5.007 Meter Temperature Inlet 

### 64.0 Initial De9. F Final Oeg.F 

### 67.0 Outlet 

### 61.0 Initial Deg. F Final 

### Oeg. F 

### 64.0 64.0 Avg. Meter Temp Oe9. F
sec 

### 780.0 Time inches 

### H2O 0.46 .ater Delta H .3arometric Pressure inches Hg 

### 29.87

' ...**~**



### - Room Temperature Initial Oeg. F 

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### 24 dscf 

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### 1.016 Y Factor 

### 1.757 Delta H@ 

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### 1.748 Average Delta H@ +/- 

### 2% Criteria 

### 0.12 Percent of Avg Y PASS

• +/- 

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### 0.21 Percent of Final Y :'::, : PASS 0.3033' 2 

### 5

RUN2 452.526 447.500 5.026

68.0 69.0 66.0 68.0 

### 67.8 780.0

0.46 29.87

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### DO Operator 

# e Nov. 24, 1999 ate BRACKET ORIFICES: Orifice No. 1 5 K Factor 0.3033 Orifice No.2 2 

### K Factor 0.6426 ORIFICE #1 ORIFiCE #2 457.938 464.295 452.900 458.500 5.038 5.795

70.0 71.0 71.0 71.0 69.0 70.0 70.0 70.0 .70.0 70.5 780.0 420.0

0.46 2.2Q 29.87 29.87

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Meter Volume Final Initial

Net Meter Temperature

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... 

### ,,,**~** --:;,; Room Temperature Initial Final Avg. Room Temperature pump Vacuum Vcr (std) Vm (std) Y Factor (brackets) +/- 2% Criteria Percent ofY 2 1.017

Cubic Feet Cubic Feet Cubic Feet
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### Deg.F



### sec inches H2O inches Hg

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Meter Volume

Meter Temperature Inlet
Outlet RUN2 572.771 

### 566.900 5.871

69.0 73.0 67.0 68.0 69.3 420.0

2.20 29.22

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### 70.5

21 

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### 0.6426 

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• +/- 5% Criteria Percent of Final Y K Factor 

## BB Meter Number Dec 3, 1999 0.988 Orifice Number

Final Initial

Net

Initial Final Initial Final Cubic Feet Cubic Feet Cubic Feet
Deg.F Deg. F Deg. F Deg.F Oeg. F

sec inches H2O

inches Hg

Oeg. F Deg. F Oeg. F inches Hg dscf dscf RUN 1 

### 566.842 561.000 5.842



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2.20 29.22



### 71.0 70.0 

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21 5.707 

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### 0.03 PASS
0.49 PASS

## CON.sOLEWORKSHF I



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## BB operator Dec 3, 

### 1999 

# .te

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Meter Volume Final Initial

Net Meter Temperature Inlet Initial Final Outlet Initial Final Avg. MeterTemp Time**~eter** Delta H**,~arometriC** Pressure

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# • 4 0.993

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Oeg.F 

### oeg.F Deg. F De9. F Deg. 

## F

sec inches H2O

inches Hg

09g. 

### F 

### Oeg.F Oeg. F inches Hg dscf dscf BRACKET ORIFICES: Orifice No. 1 K Factor Orifice No. 2 K Factor ORIFICE 

### #1 578.713 572.800 5.913

70.0 75.0 70.0 70.0 71.3 420.0

2.20 29.22

72.0 71.0 71.5 21 5.701 5.769 0.988

0.47 PASS 

### 2 0.6426· 9 0.7964 ORIFICE 

### #2 595.230 590.100 5.130



### 74.0 75.0 72.0 73.0 73.5 300.0

3.30 29.22

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1.61 PASS

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## •

# Appendix E Posttest CalibrationsMETER CAUBRA TION· operator

ate • • revious Y Factor**M~ter** Volume

...

Meter Temperature Inlet
Outlet Avg. Meter Temp Time Meter Delta H eiBarometric Pressure Room Temperature !nitial Final Avg.Room Temperature Pump Vacuum Vcr (std) 

### Vm (sid) Y Factor Delta H@ Average Y Average Delta H@ +/- 2% Criteria Percent of Avg 

### Y

• +/- 5% Criteria Percent of Final Y BS K Factor 

### Dec. 

### 17. 1999 

### Meter Number 1.003 

### Orifice Number

Final Initial

Net

Initial Final Initial Final Cubic Feet Cubic Feet Cubic Feet
Oeg. F Oeg. F Oeg. F Oe9. F Oeg. F



### sec inches H2O

inches Hg

.

Oeg. F Deg. F Deg. F inches Hg dscf dscf RUN 1 899.174 894.100 5.074

62.0 65.0· 62.0 64.0 63.3 .780.0

0.43 29.69



### 70.0 68.0 69.0

25 5.090 5.084 1.001 1.612 1.002 1.602



### 0.05 PASS
0.14 PASS 

### RUN 2 904.293 899.200 5.093

65.0 68.0 64.0 66.0 

### 65.8 780.0

0.43 29.69

69.0 69.0 

### 69.0

25 5.090 5.079 1.002 1.592 0.3033 

### 1 

### 5

# ----

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# I

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## . .----­ORIFICE BRACKETING ,erator te Meter Number 

### Meter Y Factor
Meter Volume

Meter Temperature Inlet
Outlet Avg. Meler Temp Time .etar Delta H**~arometric** Pressure Room Temperature Initial Final Avg.Room Temperature Pump Vacuum Vcr (std) Vm (std) Y Factor (brackets) +/- 2% Criteria Percent of Y 

# • BB Dec 171999

Final Initial

Net

Initial Final Initial Final 1 1.002

Cubic Feet Cubic Feet Cubic. Feet
Oeg.F Oag. F Oeg. F Oeg. F Oeg. F

sec inches H2O

inches Hg

Oeg.F Oeg. F 

### Oeg.F inches Hg dscf dscf BRACKET ORIFICES: Orifice No. 1 K Factor Orifice No.2 K Factor ORIFICE #1 909.424 904.300 5.124

68.0 69.0 67.0 68.0 68.0 

### 5 0.3033 2 0.6426 ORIFICE #2 915.390 909.500 5.890

69.0 69.0 68.0 69.0 

### 68.8 780.0 420.0

0.43 2.10 29.69 29.69.

72.0 71.0 69.0 69.0 70.5 70.0



### 25 21 5.083 5.801 5.088 5.864 0.999 0.989

0.31 

### 1.28 PASS PASS

## BRACKETING 

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# •METER CALIBRATION DO K Factor Operator Dec. 17.1999 Meter Number 

### ADele 1.017 OrificeNumber "Previous 

### Y Factor

RUN 1 Meter Volume Final Cubic Feet 563.467 Initial Cubic Feet 558.300

Net Cubic Feet 5.167 Meter Temperature Inlet Initial Deg.F 65.0 Final Oeg. F 68.0 Outlet Initial Deg. F 

### 64.0 Final Oeg. F 67.0 Avg. Meter Temp Oeg.F 66.0 Time Meter Delta H. '

.. sec inches H2O 960.0 0.30 • Barometric Pressure inches Hg 29.69 Room Temperature Initial 

### Deg. F 69.0 Final 

### D6g. F 71.0 Avg.Room Temperature 

### De9· F 70.0 Pump Vacuum inches Hg 24 dscf 5.227 Vcr (std) dscf 5.149 Vm (std) 1.015 Y Factor 

### 1.640 Delta H@ 1.016 Average Y 1.628 Average Delta H@ -t/- 2% Criteria 0.04 Percent of Avg Y PASS 

# •**+/~** 5% Criteria 0.14 Percent of Final Y PASS RUN2 569.187 564.000 5.187

68.0 69.0 67.0 68.0 68.0 960.0



### 0.30 29.69

69.0 69.0 

### 69.0

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### 2 4

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«ORIFICE BRACKETING Operator Dec 171999 

# eta DD

Meter Number Meter Y Factor
Meter Volume Final Initial

Net Meter Temperature Inlet Initial Final Outlet Initial Final Avg. Meter Temp Time _ster Delta H arometric Pressure Room Temperature Initial Final Avg.Room Temperature Pump Vacuum Vcr (std) Vm (std) Y Factor (brackets) +/- 2% Criteria Percent ofY 

# • 2 1.016

Cubic Feet Cubic Feet Cubic Feet
Deg. F Deg. F Deg.F Deg.F Oeg.F

sec inches H2O

inches Hg

Oeg. F Oeg.F Oeg.F 

### inches Hg

. dscf

dscf BRACKET ORIFICES: Orifice No. 1 

### K Factor Orifice No.2 K Factor ORIFICE #1 575.305 570.100 5.205

69.0 70.0 69.0 69.0 69.3 960.0

0.30 29.69

71.0 69.0 70.0

24 5.227 5.155 1.014

0.20 PASS 

### 4 0.2533 

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### 587.270 582.000 5.270

69.0 69.0 70.0 70.0 69.5 480.0

1.30 29.69

72.0 71.0 71.5

20 5.208 5.229 0.996

1.98 PASS

## BRACKETiNG 

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# • .­ORIFICE BRACKETING 

### B8 Operator Dec 171999 

# e te 4 Meter Number 1.014 Meter Y Factor
Meter Volume Final Cubic Feet Initial Cubic Feet

Net Cubic Feet Meter Temperature Inlet Initial Oeg. F Final Oeg. F outlet Initial Deg.F 

### FinaI Oeg. F Oeg.F Avg. Meter Temp seC Time inches H2O _eter Delta H inches Hg arometric Pressure Room Temperature Initial Oeg.F Final 

### Oeg. F Oeg. F Avg.Room Temperature inches Hg Pump Vacuum dscf Vcr (std) dscf Vm (std) Y Factor (brackets) +/- 2% Criteria Percent ofY 

# • BRACKET ORIFICES: Orifice No. 1 . K Factor Orifice No.2 K Factor ORIFICE#1 528.895 523.500 5.395

67.0 69.0 68.0 69.0 68.3 780.0

0.52 29.69

72.0 72.0 72.0



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### 5.170

69.0 

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### METER CALIBRATION 

### BB K Factor operator Deo.17,1999 

### Meter Number te 

### 0.993 Orifice Number • evious Y Factor

RUN 1 Meter Volume Final Cubic Feet 

### 518.005 Initial Cubic Feet 

### 512.600

Net Cubic Feet 5.405 Meter Temperature

. Inlet Initial Oeg. F 

### 60.0 Final Deg. F 

### 63.0 Outlet 

### 61.0 Initial D9g. F Final Oeg. F 

### 64.0 Avg. Meter Temp Deg. F 

### 62.0
sec 

### 780.0 Time 0.52 

### inches H2O _eter Delta H inches Hg 

### 29.69 arometrlc Pressure Room Temperature Initial Oeg. F 

### 70.0 Final Oeg.F 

### 70.0 Avg.Room Temperature Oeg. F 

### 70.0 inches Hg 

### 24 Pump Vacuum dscf 

### 5.484 Vcr (std) dscf 

### 5.430 Vm (std) 

### 1.010 Y Factor 1.728 Delta H@ 

### 1.014 Average Y 

### 1.730 Average Delta H@ +/- 

### 2% Criteria 

## DAD Percent of Avg Y 

## PASS

• +/- 

### 5% Criteria 

### 2.07 Percent of Final Y 

## PASS 0.3271 4 

### 3

RUN 

### 2

523.490 518.100 5.390

63.0 67.0 64.0 66.0 65.0 780.0

0;52 29.69

70.0 71.0 70.5 24 5.481 5.384 1.018 1.731**~----.** 

## _.



# AppendixF 

# Process Data 

# •

--------- ......... --------, I !

# •

•

• Compliance Emission Test Operating Data
Owner: Cargill,Inc. Date: December 9 & 10, 1999 Source: EP# 11

- Bean Tallk. Conveying Permit #: 96-A-332-S3

Maximum Continuous Process Rate {Manufacturer's**Rating},.:;2..;.;43;...t;::o:;;nsIhr=-=so.::,y~b:.;:;ean=s** _______ _ Historical Average Process Rate..;..N.;..,;/A

________________ ____ _ Historical Maximum Process Rate

.**.:;.N;:.:/A~** ____________________ _ Types and Sources ( if any) of Fuels normally 8umed,_N_/A

_________ __ __ Type of Fuel Burned During this 

### test . .:;,N;:..::/A;.::-

________ --------

__ _ If Fuel is us-ad ApprOXimate Quantities of each listed above burned Annually

________ _ Recycling Capability Recycling In Progress Pr:c08S$ Data Ot.! 'Jng**BlJn~**

Process Rate (gal/hr, Iblhr, tons/hr. etc ... ) Process Rate Wet Percent Moisture (%) Process Rate Dry How Process Rate was Determined Yes

__ _ No 

## X No 

### X

Run 1 Run 2­ Run 3 204 tonslhr 240 tonslhr 204 tonslhr**~nk** levels 81ld throughput

Person Responsible for**Data,~B::::o=b::::_S.;..un-dIi.;..'-e--~--~:__-------------** Signature

# 3e~**5Vv~\t~** ntJelPOSltion Facility Superintendent

.... etease indicate in the same unilti. as your historical informatjon

### AIR :POLLUTION CONTROL EQUIPMENT OPERATING DATA 

# • Plant Cargill.lnc._ Location Sioux City, IA SO"QIQI**t~** ..e;;part1;:.;;;;;·c;.;::ul;;;;at;;;;e

______ _ Rated Production 243 tonsihr soYbeans Date 1219&1011999 TIme

____ _ Actual Production' 204,240,204 tons!hr soybeans AirFlaw Data**_~~** ______ _ Run No. 1,2,3**~~------~~--------** Mechanical Collector. TIlbe Dis. in., Numbet of Tubes Design Ap

____ in,. BiO Gas Temp

__**~** Observed t.\p in**H~** Design Cfinltube @ Observed .6p
__ @ "F FaD 

### Rated liP. Operating Volts Operating Amp!

____ _ E1 'c_Pn:cinitaIOr FicldN'Q, Se::ondary Prlmaxy SCf:Onduy Spark Rate 

# jPrimaIy Voltage (KV)

Voltage (volts) ClUl'ent (amps) CUlTent (ma) <l'lermin) 

# • Sgybber: Type
. Ap{actoss scrubber)**inH~O.** FanRatedHP Opcnuing Volcs Openuing Amps Liquid Cin.-u.lation Rate gal/min. % MaJre-up Slowdown gpm Scrubbing Water Change Interval Settling Tank Cle:ming Interval Eaghousc:**P~ositive** Negative No. Compartments Type Cle:uring Clean Cycle • min Avg. Baghouse t.\p LO inH:zO L\pRango Fan: RatedKP. Ope:ating Volts Operating Amps Cyclone: Type top inH.p Diameter Fan R4lai EP Operating**V?I~** , Operating Amps
Person Responsible for Data .;;;: B..:;.ob ;;...;;;.;Sun=dl_ie

_______ __**~_** Sig:narure

__________________ _ Tide/Position Facility S!¥,rintendent 

# •
10

# • Appendix G Opacity**C~rtification** 

# •

•

m7 ";] ," :DEPARTMENT OF NATURAL RESOURCES J. VILSACK. GOVERNOR PAUL W. JOHNSON, DIRECTOR SALLY J. PEDERSON, .IT. GOVERNOR 

### November 10,1999


### Mr. Jay Titus Comprehensive 

### Emission Services 1112 Maple Street West Des Moines, IA 50265 Dear Mr. Titus: We wish to acknowledge your attendance at the Fall 1999 session of the visible emissions recertification program conducted by 

### the Unh'ersity of Iowa Hygiemc Laboratory on October 19

­ 

### 20,1999.
. The records show that you have successfully met the criteria for making visual detenmnation of**th~** 

### opacity of emissions, as specified in subrule 567--29.1 of the Iowa Administrative Code. 

# • Transmitted 'with 

### this letter is a certificate indicating that you are qualified to make visible emissions evaluations pursuant to Chapter 567--29 of the Iowa Administrative Code. Notice of the Spring 2000 session 

### v"ill be issued around the end of March 2000 and you 

### ''''ill be infonned of the exact date and location of the next session. Sincerely, 

# /7) ;/ /) 

# /?J
. j7/

# ~z.t:/::lPJ;i{Mf AIR QUALITY BUREAU IOWA DEPARTMENT OF !'<ATURAl RESOl'RCES VISIBLE EMISS10:\S EVALUATION CERTIACATE THIS IS TO CERTIFY THAT 

### Enclosure Jay Titus ; ..**(I~l:iti('d** tt'**trul~<** ,·; .. lNc: Cllli",
...**im~"** of ;I1il pb!h.l'Iitd"l. pur"l,I:Jnl1r.**Ch.'1r'd'·:'<-~~!·}** oi tb.! l(t\\;, 

### cc: Pamela Kastle, D.H.L.**.~OJtlin~~U:'l;\'C** ("(\dr. promulYifl!!rl**\ltl~1 :.w'Mril~**  ,,), ('h,,!XtT**iI~** . .!;I;'**('~** ,.,Il"'a. 

# •

7900 HICKMAN ROAD. SUITE 1 f URBANDALE.IOWAS0322/515-242·5100 I FAX 515-242·5094 

### es'" 1'.R d.......... 

# - .. ".- .. 

# _. ­

## ~**STAT~OF**

### I~V\T~ DEPARTMENT OF NATURAL RESOURCES AS J. VII.SACK, GOVERNOR' PAUl. W, JOHNSON. DIRECTOR SALLY J. PEDERSON, LI. GOVERNOR 

### November 16, 1999


### Dan Deatsch Comprehensive Emissions 

### Servo 1112 Maple St 

### West Des Moines IA 50265 Dear Mr. 

### Deatsch: We 

### wish to acknowledge your attendance at the Fall 1999 session of the visible etnlSS10nS 

### recertification program conducted by 

### the University of Iowa Hygienic Laboratory on October 19

­ 20,1999. The records show that you ha,'e successfully met the criteria for making visual detenninatiol1 of the opacity of emissions; as specified 

### in subrule**567-~29.1** 

### of the Iowa Administrative Code. 

# • Transmitted with this Jetter is a certificate indicating that you are 

### qualified to make 

### visible emissions evaluations pursuant to Chapter 567--29 of the Iowa Administrative Code. Notice of the Spring 2000 session 

# ,,,ill be issued around the end of March 2000 and you will 

### be 

### infol111ed of the exact date and location ofthe 

### next session. Sincerely, 

### '/7 /:('. 

# (? 

# ._£P**~",,/(pr;.** 

## Lf 

# f..:..-;7k DOUGEAS A. 

### CAt'JPBELL AIR QUALITY BUREAU IOWA DEPARThlENT OF**~ATURAL** RESOl:RCES VISIBLE Ei\'IlSSIO"'S EVALUATION CERTIFICATE 

### Enclosure THIS IS TO CERTl FY THAT 

### cc: Pamela Kastle, U.RL. Dan Deatsch ! j""**Iltt:d.;n~rt** to n\:)Le vi
... ibk
... mi
..**~~'I1I"** ,'If ait j')(Jlhlt'(Ul. pur"U:lIIt tn**("h~vl('r** jr.;_.!';**l\lJb~ ~",..**  

### .. 1\4I'llini..,,..,,,llyt**Ccxi,~ promu~;nrd** **vnrt~r** :.Iulher.t) (If**("jrJPI\"r"~!iU.** ("(11ft' (Of**Jl'~\:;'** 

# •

7900 HICKMAN ReF,O. SUITE 1 I URBANDALE, IOWA 50322/515-242-5100 I FAX 515,242:5004


## •