~AIR ~ POLL-UTION ~ TESTING, INC. 

DENVER, SALT LAKE CITY 

Report prepared for: 

Mr. Joe Eck 

Interstate Brick Company 

9780 South 5200 West 

West Jordan, Utah 84088 

Test Date: 

May 8, 2007 

APT Project: ISB7144 

Source Emissions Testing Report 

for Interstate Brick Company 

PM and Metals Testing 

Kiln No. 3 and 4 Scrubbers 

West Jordan, Utah 

Report prepared by: 

Karl Breuer 

Senior Technical Writer 

DE:t\v'"ER OFFICE 

5530 Marshall Street 

Arvada, CO 80002 

( 303) 420-5949 

FAX (303) 420-5920 

( 800) 268-6213 
Table of Contents 

1. Introduction I Process Description............................................... 1 

2. Test Results Summary............................................................... 2 

3. Methods....................................................................................... 5 

4. Test Program Summary.............................................................. 5 

5. Test Method Details.................................................................... 6 

Tables 

Table 1.1 : Contact Personnel.................................................... 1 

Table 2.1 :Emissions Testing Results, Scrubber #3.................. 3 

Table 2.2: Emissions Testing Results, Scrubber #4.................. 4 

Table 4.1 : Sampling and Analytical Methods Summary............. 6 

Appendices 

Testing Parameter............................................................. Appendix 1 

Field Data........................................................................ Appendix 2 

Laboratory Data................................................................ Appendix 3 

Calibration Data................................................................ Appendix 4 

Schematics..................................................................... Appendix 5 
APT Project ISB7144 

Test Report, Kiln No.3 and 4 Metals and PM Emissions 

1. Introduction I Process Description 

Air Pollution Testing, Inc. (APT) was contracted to perform source emission testing 

services at the Interstate Brick facility located in West Jordan, Utah. Testing was 

performed May 81

h, 2007 

The purpose of the testing program was to determine the concentrations and mass 

emission rates of multiple metals from the Kiln No. 3 scrubber stack and the Kiln No. 4 

scrubber stack. 

Exhaust gases (with temperatures of approximately 500° F) are removed from Kiln 3 by 

one (1) New York fan rated at 60,000 actual cubic feet per minute (acfm) and are routed 

directly to a wet scrubber. Exhaust gases (with temperatures of approximately 500° F) are 

removed from Kiln 4 by two (2) Robinson fans rated at 45,000 acfm each and routed 

directly to a wet scrubber. 

Personnel involved in the test program are listed in Table 1.1 below. 

Interstate Brick Company 

Emissions Testing Program Contact Personnel 

Name, Title Company, Affiliation Address Phone, FAX 

Mr. Joe Eck, Interstate Brick Company 801-280-5215, 

Process Engineer 9780 South 5200 West 801-280-5220 West Jordan, Utah 84088 

Mr. Harold Burge, Utah DAQ 801-536-4129, 1950 West North Temple Air Quality Engineer Salt Lake City, Utah 84114-4820 801-536-4099 

Mr. Robert Weidenfeld, Severn Trent Laboratories 916-374-4333, 880 Riverside Parkway Project Manager West Sacramento, California 95605 916-372-1059 

Mr. Nick Legare, Air Pollution Testing, Inc. 801-97 4-0481' 

Project Manager 1959 South 4130 West, Unit B 801-974-0483 Salt Lake City, Utah 84104 

Table 1.1: Emissions Testing Program Contact Personnel 

The emissions data collected during testing are being used for internal engineering 

purposes. 

page 1 
2. Test Results Summary 

APT Project ISB7144 

Test Report, Kiln No.3 and 4 Metals and PM Emissions 

The results of the testing are summarized in Tables 2.1 and 2.2. Any emission parameters 

not found in the tables may be found in Appendix 1. The following terms are used in the 

tables: 

• oF -temperature, degrees Fahrenheit 

• %vd -diluent concentration, dry volume percent 

• %vw - stack gas water vapor content, wet volume percent 

• dscfm- stack gas flow rate, dry standard (one atmosphere, 68°F) cubic feet per 

minute 

• gr/dscf- grains per dry standard (one atmosphere, 68°F) cubic foot 

• mg/dscm- milligrams per dry standard (one atmosphere, 68°F) cubic meter 

• lb/hr- pollutant mass emission rate, pounds per hour 

page 2 
APT Project 1887144 

Test Report, Kiln No.3 and 4 Metals and PM Emissions 

Interstate Brick Company, Scrubber 3 

Emissions Testing Summary- Multi-Metals, Ma' 8, 2007 

Run# 1 2 Average 

Start Time 11:46 14:55 

Stop Time 12:53 16:02 

Stack Temperature (°F) 114 115 115 

02 (%vd) 17.4 17.4 17.4 

C02 (%vd) 2.4 2.4 2.4 

H20 (%vw) 11.5 11.8 11.7 

Gas flow ( dscfm) 25,824 25,302 25,563 

Pollutant Data :- Metal$ .. 

Particulate emissions (gr/dscf) 0.0212 0.0214 0.0213 

Particulate emissions (mg/dscm) 48.6 49.0 48.8 

Particulate emissions (lb/hr) 4.70 4.65 4.67 

Sb emissions (mg/dscm) 0.0001 0.0001 0.0001 

Sb emissions (lb/hr) 7.28 E-06 6.91 E-06 7.10 E-06 

As emissions (mg/dscm) 0.0696 0.0564 0.0630 

As emissions (lb/hr) 6.73 E-03 5.34 E-03 6.04 E-03 

Ba emissions (mg/dscm) 0.0044 0.0044 0.0044 

Ba emissions (lb/hr) 4.23 E-04 4.19 E-04 4.21 E-04 

Be emissions (mg/dscm) 0.0000 0.0000 0.0000 

Be emissions (lb/hr) 0.00 E+OO 0.00 E+OO 0.00 E+OO 

Cd emissions (mg/dscm) 0.0027 0.0042 0.0035 

Cd emissions (lb/hr) 2.61 E-04 4.02 E-04 3.31 E-04 

Cr emissions (mg/dscm) 0.0056 0.0057 0.0057 

Cr emissions (lb/hr) 5.41 E-04 5.43 E-04 5.42 E-04 

Co emissions (mg/dscm) 0.0020 0.0020 0.0020 

Co emissions (lb/hr) 1.96 E-04 1.87 E-04 1.91 E-04 

Cu emissions (mg/dscm) 0.0042 0.0061 0.0051 

Cu emissions (lb/hr) 4.08 E-04 5.75 E-04 4.92 E-04 

Pb emissions (mg/dscm) 0.0020 0.0019 0.0019 

Pb emissions (lb/hr) 1.92 E-04 1.78 E-04 1.85 E-04 

Mn emissions (mg/dscm) 0.0045 0.0072 0.0059 

Mn emissions (lb/hr) 4.36 E-04 6.84 E-04 5.60 E-04 

Hg emissions (mg/dscm) 0.0047 0.0032 0.0039 

HQ emissions (lb/hr) 4.56 E-04 2.99 E-04 3.78 E-04 

Ni emissions (mg/dscm) 0.0017 0.0058 0.0038 

Ni emissions (lb/hr) 1.61 E-04 5.54 E-04 3.58 E-04 

P emissions (mg/dscm) 0.0506 0.0301 0.0404 

P emissions (lb/hr) 4.90 E-03 2.85 E-03 3.88 E-03 

Se emissions (mg/dscm) 0.0268 0.0232 0.0250 

Se emissions (lb/hr) 2.60 E-03 2.20 E-03 2.40 E-03 

Ag emissions (mg/dscm) 0.0001 0.0001 0.0001 

Ag emissions (lb/hr) 9.15 E-06 1.08 E-05 9.99 E-06 

Tl emissions (mg/dscm) 0.0013 0.0012 0.0013 

Tl emissions (lb/hr) 1.28 E-04 1.17 E-04 1.22 E-04 

Zn emissions (mg/dscm) 0.0186 0.0183 0.0184 

Zn emissions (lb/hr) 1.80 E-03 1.73 E-03 1.77 E-03 

Table 2.1: Emissions Testing Results, Scrubber #3 

page 3 
APT Project ISB7144 

Test Report, Kiln No.3 and 4 Metals and PM Emissions 

Interstate Brick Company, Scrubber 4 

Emissions Testing Summary- Multi-Metals, Ma~ 8, 2007 

Run# 1 2 Average 

Start Time 10:41 12:36 

Stop Time 11:53 13:43 

Stack Temperature (°F) 123 124 124 

02 (%vd) 17.1 17.1 17.1 

C02 (%vd) 2.4 2.4 2.4 

H20 (%vw) 8.7 15.1 11.9 

Gas flow (dscfm) 37,278 33,579 35,429 

Pollutant Data ;' ', 

Particulate emissions (gr/dscf) 0.0076 0.0053 0.0065 

Particulate emissions (mg/dscm) 17.4 12.1 14.8 

Particulate emissions (lb/hr) 2.43 1.52 1.98 

Sb emissions (mg/dscm) 0.0000 0.0000 0.0000 

Sb emissions (lb/hr) 6.10 E-06 4.72 E-06 5.41 E-06 

As emissions (mg/dscm) 0.0053 0.0055 0.0054 

As emissions (lb/hr) 7.45 E-04 6.93 E-04 7.19 E-04 

Ba emissions (mg/dscm) 0.0059 0.0043 0.0051 

Ba emissions _(lb/hr}_ 8.22 E-04 5.42 E-04 6.82 E-04 

Be emissions (mg/dscm) 0.0000 0.0000 0.0000 

Be emissions (lb/hr) 0.00 E+OO 0.00 E+OO 0.00 E+OO 

Cd emissions (mg/dscm) 0.2820 0.0145 0.1482 

Cd emissions (lb/hr) 3.94 E-02 1.83 E-03 2.06 E-02 

Cr emissions (mg/dscm) 0.0070 0.0045 0.0058 

Cr emissions (lb/hr) 9.72 E-04 5.72 E-04 7.72 E-04 

Co emissions (mg/dscm) 0.0031 0.0026 0.0028 

Co emissions(lb/hr} 4.27 E-04 3.23 E-04 3.75 E-04 

Cu emissions (mg/dscm) 0.0151 0.0066 0.0109 

Cu emissions (lb/hr) 2.11 E-03 8.32 E-04 1.47 E-03 

Pb emissions (mg/dscm) 0.0019 0.0020 0.0019 

Pb emissions (lb/hr) 2.65 E-04 2.46 E-04 2.56 E-04 

Mn emissions (mg/dscm) 0.0066 0.0101 0.0083 

Mn emissions (lb/hr) 9.19 E-04 1.27 E-03 1.10 E-03 

Hg emissions (mg/dscm) 0.0024 0.0063 0.0043 

Hg emissions _(lb/hr)_ 3.36 E-04 7.91 E-04 5.64 E-04 

Ni emissions (mg/dscm) 0.0264 0.0078 0.0171 

Ni emissions {lb/hr) 3.69 E-03 9.85 E-04 2.34 E-03 

P emissions (mg/dscm) 0.0326 0.0343 0.0334 

P emissions (lb/hr) 4.55 E-03 4.32 E-03 4.43 E-03 

Se emissions (mg/dscm) 0.0274 0.0350 0.0312 

Se emissions (lb/hr) 3.83 E-03 4.41 E-03 4.12 E-03 

Ag emissions (mg/dscm) 0.0002 0.0001 0.0001 

Ag_ emissions (lb/hr) 2.57 E-05 7.15 E-06 1.64 E-05 

Tl emissions (mg/dscm) 0.0003 0.0003 0.0003 

Tl emissions (lb/hr) 3.66 E-05 3.29 E-05 3.48 E-05 

Zn emissions (mg/dscm) 0.0211 0.0282 0.247 

Zn emissions (lb/hr) 2.95 E-03 3.55 E-03 3.25 E-03 

Table 2.2: Emissions Testing Results, Scrubber #4 

page 4 
3. Methods 

APT Project ISB7144 

Test Report, Kiln No.3 and 4 Metals and PM Emissions 

APT tested in accordance with the following U.S. Environmental Protection Agency 

(USEPA) source emission test methods referenced in 40 CFR Part 60. Appendix A. 

• Method 1 - Sample and Velocity Traverses for Stationary Sources 

• Method 2- Determination of Stack Gas Velocity and Volumetric Flow Rate 

• Method 3 - Gas Analysis for the Determination of Dry Molecular Weight 

• Method 5 - Determination of Particulate Emissions from Stationary Sources 

• Method 29 - Determination of Metals Emissions from Stationary Sources 

4. Test Program Summary 

The sampling program determined all emission parameters detailed in Table 4.1. Two test 

runs (60 minutes each in duration) were performed at each scrubber stack location. 

Pollutant concentration data were reduced to mass emission rates using stack gas velocity 

and volumetric flow rate data collected concurrent with the concentration data. 

A sample recovery trailer was provided to minimize sample contamination during recovery. 

The metals samples were recovered, carefully packaged in an effort to minimize sample 

container breakage risk, and shipped via overnight express by APT personnel to Severn 

Trent Laboratories (STL) in West Sacramento, California for analysis following particulate 

analysis at Air Analytical in Arvada, Colorado. 

page 5 
Interstate Brick Company 

Sampling and Analytical Methods 

Gas Parameter Sampling Method 

APT Project ISB7144 

Test Report, Kiln No.3 and 4 Metals and PM Emissions 

Analytical Method Laboratory 

gas flow Methods 1 , 2 and 29 draft gauge, thermocouple, pitot tube 

APT, on-site 

H20 Method 29 gravimetric 

PM Method 5 gravimetric AA, off-site 

02, C02 Method 3 wet chemical - Orsat instrument 

Inductively Coupled Plasma - Mass 

metals Method 29 Spectroscopy (ICP-MS) STL, 

Cold Vapor Atomic Absorbtion Sacramento, CA 

Spectrophotometry (CVAAS; for Hg) 

Table 4.1: Sampling and Analytical Methods 

The Kiln #3 exhaust sampling location consisted of a vertical, round stack with an interior 

diameter of 59" and two sampling ports arranged 90° from one another in accordance with 

EPA Method 1. PM and metals sampling was performed along a grid of 20 points across 

the exhaust stack cross section. 

The Kiln #4 exhaust sampling location consisted of a vertical, round stack with an interior 

diameter of 72 inches and two sampling ports arranged 90° apart in accordance with EPA 

Method 1 . PM and metals sampling was performed along a grid of 24 points across the 

exhaust stack cross section. 

Appendix 5 provides schematics of the sampling locations including sampling points. 

5. Test Method Details 

PM and metals emissions were determined following EPA Methods 5 and 29 procedures. 

Each sampling period consisted of conducting a temperature and differential pressure 

traverse of the stack with a K-type thermocouple and an S-type pitot tube. Concurrently, a 

gas sample was extracted from the stack at an isokinetic flow rate for a 60-minute period. 

The gas passed through an in-stack glass nozzle, a heated Teflon probe, a heated quartz 

fiber filter, a series of six chilled glass impingers, and a calibrated dry gas meter. Diluent 

data was determined from Orsat analysis of dry, integrated Tedlar bag samples. 

Prior to sampling, the first two impingers contained 100 ml of 10% hydrogen peroxide/5% 

nitric acid. The third impinger was empty. The fourth and fifth impingers contained 100 ml 

of 4% potassium permanganate/10% sulfuric acid. The sixth impinger contained 250 

page 6 
APT Project ISB7144 

Test Report, Kiln No. 3 and 4 Metals and PM Emissions 

grams of dried silica gel. A sampling train schematic diagram can be found in Appendix 5 

- Schematics. 

Following each sampling period, the filter, a series of acetone and dilute nitric acid rinses of 

the probe and nozzle, and the contents of the impingers were recovered for subsequent 

Inductively Coupled Plasma - Mass Spectroscopy (ICP-MS) and Cold Vapor Atomic 

Absorbtion Spectrophotometry (CVAAS) analysis (performed by STL). Prior to metals 

analysis, the filter and acetone rinses were sent to Air Analytical for gravimetric analysis. 

The metals laboratory data were combined with field data to calculate the (on an elemental 

basis) concentrations in milligrams per dry standard cubic meter (mg/dscm) and mass 

emissions in lb/hr. The PM laboratory data were combined with field data to calculate the 

concentrations in grains per dry standard cubic foot (gr/dscf) and mg/dscm; additionally 

mass emissions were calculated in lb/hr. 

page 7 
AIR 

POLLUTION 

TESTING, INC. 

Appendix ()ne: Testing Paran1eters 

Interstate Brick 

West Jordan, Utah 

Scrubber 3 

May 8, 2007 

EPA Method 29 : Determination of Metals Emissions from Stationary Sources 

Field Data Run#1 Run#2 Average 

date 5/8/2007 5/8/2007 

start time 11:46 14:55 

stop time 12:53 16:02 

sam ole volume (ft3

) 43.099 42.759 42.929 

sampling duration (minutes) 60 60 60 

stack temperature (°F) 114 115 115 

meter temperature (°F) 83 84 84 

barometric pressure (mbar) 859 859 859 

barometric pressure (" Hg) 25.37 25.37 25.37 

stack pressure (" H20) -0.10 -0.10 -0.10 

moisture (grams) 96.2 126.3 111.3 

oxygen (o/ovd) 17.4 17.4 17.4 

carbon dioxide (o/ovd) 2.4 2.4 2.4 

orifice setting delta H (" H20) 1.3 1.3 1.3 

average (delta P)l<l C' HzO)l<l 0.513 0.505 0.509 

meter box Yd (unitless) 0.974 0.974 0.974 

pilot tube constant (unitless) 0.83 0.83 0.83 

nozzle diameter (inches) 0.280 0.280 0.280 

stack diameter (inches) 59.00 59.00 59.00 

Laboratorv Data 

mass particulate, FY. rinse (grams) 0.00160 0.00060 0.00110 

mass particulate, filter (grams) 0.04615 0.04715 0.04665 

mass Sb (micrograms) 0.07 0.07 0,07 

mass As (micrograms) 68.40 54.89 61.65 

mass Ba (micrograms) 4.30 4.30 4.30 

mass Be (micrograms) ND ND NO 

mass Cd (micrograms) 2.65 4.13 3.39 

mass Cr (micrograms) 5.50 5.58 5.54 

mass Co (micrograms) 1.99 1.92 1.96 

mass Cu (micrograms) 4.15 5.91 5.03 

mass Pb (micrograms) 1.95 1.82 1.89 

mass Mn (micrograms) 4.44 7.03 5.73 

mass Hg (micrograms) 4.63 3.07 3.85 

mass Ni (micrograms) 1.64 5.69 3.67 

mass P (micrograms) 49.80 29.30 39.55 

mass Se (micrograms) 26.40 22.63 24.52 

mass Ag (micrograms) 0.09 0.11 0.10 

mass Tl (micrograms) 1.30 1.20 1.25 

mass Zn (micrograms) 18.30 17.80 18.05 

Calculations 

sample volume (dscf) 34.723 34.381 34.552 

moisture volume (scf) 4.528 5.945 5.237 

moisture content (%/1 00) 0.115 0.147 0.131 

saturated moisture content (%/1 00) 0.115 0.118 0.117 

molecular weight (dry) 29.08 29.08 29.08 

molecular weight (actual) 27.80 27.77 27.79 

gas velocity (ft/sec) 32.9 32.4 32.6 

gas flow (acfm) 37,444 36,861 37,153 

gas flow (dscfm) 25,824 25,302 25,563 

% isokinetic 99.5 104.1 101.8 
Interstate Brick 

West Jordan, Utah 

Scrubber 3 

MayS, 2007 

EPA Method 29 : Determination of Metals Emissions from Stationary Sources 

Particulate Emissions 

Run#1 Run#2 Average 

particulate emissions (gr/dscf) 0.0212 0.0214 0.0213 

particulate emissions (mg/dscm) 48.6 49.0 48.8 

particulate emissions (lb/hr) 4.70 4.65 4.67 

Multi-Metals Emissions 

Sb emissions (mg/dscm) 0.0001 0.0001 0.0001 

Sb emissions (lb/hr) 7.28E-06 6.91E-06 7.10E-06 

As emissions (mg/dscm) 0.0696 0.0564 0.0630 

As emissions (lb/hr) 6.73E-03 5.34E-03 6.04E-03 

Ba emissions (mg/dscm) 0.0044 0.0044 0.0044 

Ba emissions (lb/hr) 4.23E-04 4.19E-04 4.21E-04 

Be emissions (mg/dscm) 0.0000 0.0000 0.0000 

Be emissions (lb/hr) O.OOE+OO O.OOE+OO O.OOE+OO 

Cd emissions (mg/dscm) 0.0027 0.0042 0.0035 

Cd emissions (lb/hr) 2.61E-04 4.02E-04 3.31E-04 

Cr emissions (mg/dscm) 0.0056 0.0057 0.0057 

Cr emissions (lb/hr) 5.41E-04 5.43E-04 5.42E-04 

Co emissions (mg/dscm) 0.0020 0.0020 0.0020 

Co emissions (lb/hr) 1.96E-04 1.87E-04 1.91E-04 

Cu emissions (mg/dscm) 0.0042 0.0061 0.0051 

Cu emissions (lb/hr) 4.08E-04 5.75E-04 4.92E-04 

Pb emissions (mg/dscm) 0.0020 0.0019 0.0019 

Pb emissions (lb/hr) 1.92E-04 1.78E-04 1.85E-04 

Mn emissions (mg/dscm) 0.0045 0.0072 0.0059 

Mn emissions (lb/hr) 4.36E-04 6.84E-04 5.60E-04 

Hg emissions (mg/dscm) 0.0047 0.0032 0.0039 

Hg emissions (lb/hr) 4.56E-04 2.99E-04 3.78E-04 

Ni emissions (mg/dscm) 0.0017 0.0058 0.0038 

Ni emissions (lb/hr) 1.61E-04 5.54E-04 3.58E-04 

P emissions (mg/dscm) 0.0506 0.0301 0.0404 

P emissions (lb/hr) 4.90E-03 2.85E-03 3.88E-03 

Se emissions (mg/dscm) 0.0268 0.0232 0.0250 

Se emissions (lb/hr) 2.60E-03 2.20E-03 2.40E-03 

Ag emissions (mg/dscm) 0.0001 0.0001 0.0001 

Ag emissions (lb/hr) 9.15E-06 1.08E-05 9.99E-06 

Tl emissions (mg/dscm) 0.0013 0.0012 0.0013 

Tl emissions (lb/hr) 1.28E-04 1.17E-04 1.22E-04 

Zn emissions (mg/dscm) 0.0186 0.0183 0.0184 

Zn emissions (lb/hr) 1.80E-03 1.73E-03 1.77E-03 

A laboratory result of NO was assummed to be zero; all detected fractions were added. 

Interstate Brick 

West Jordan, Utah 

Scrubber4 

May 8, 2007 

EPA Method 29 : Determination of Metals Emissions from Stationary Sources 

Field Data Run#1 Run#2 Average 

date 51812007 51812007 

start time 10:41 12:36 

stop time 11:53 13:43 

sample volume (tel 40.041 38.936 39.489 

sampling duration (minutes) 60 60 60 

stack temperature ("F) 123 124 124 

meter temperature (°F) 87 93 90 

barometric pressure (mbar) 859 859 859 

barometric pressure (" Hg) 25.37 25.37 25.37 

stack pressure (" H20) 0.22 0.22 0.22 

moisture (grams) 65.5 117.8 91.7 

oxygen (o/ovd) 17.1 17.1 17.1 

carbon dioxide (o/ovd) 2.4 2.4 2.4 

orifice setting delta H (" H20) 1.0 1.0 1.0 

average (delta P)10 (" H20)10 0.488 0.468 0.478 

meter box Yd (unitless) 0.983 0.983 0.983 

pitot tube constant (unitless) 0.83 0.83 0.83 

nozzle diameter (inches) 0.275 0.275 0.275 

stack diameter (inches) 72.00 72.00 72.00 

Laboratory Data 

mass particulate, FY:. rinse (grams) 0.00825 0.00260 0.00543 

mass particulate, filter (grams) 0.00770 0.00805 0.00788 

mass Sb (micrograms) 0.04 0.03 0.04 

mass As (micrograms) 4.88 4.84 4.86 

mass Ba (micrograms) 5.39 3.79 4.59 

mass Be (micrograms) ND ND ND 

mass Cd (micrograms) 258.08 12.76 135.42 

mass Cr (micrograms) 6.37 4.00 5.19 

mass Co (micrograms) 2.80 2.26 2.53 

mass Cu (micrograms) 13.81 5.82 9.81 

mass Pb (micrograms) 1.74 1.72 1.73 

mass Mn (micrograms) 6.02 8.90 7.46 

mass Hg (micrograms) 2.20 5.53 3.87 

mass Ni (micrograms) 24.18 6.89 15.53 

mass P (micrograms) 29.80 30.20 30.00 

mass Se (micrograms) 25.10 30.80 27.95 

mass Ag (micrograms) 0.17 0.05 0.11 

mass Tl (micrograms) 0.24 0.23 0.24 

mass Zn (micrograms) 19.32 24.84 22.08 

Calculations 

sample volume (dscf) 32.323 31.056 31.690 

moisture volume (scf) 3.083 5.545 4.314 

moisture content (%/1 00) 0.087 0.151 0.119 

molecular weight (dry) 29.07 29.07 29.07 

molecular weight (actual) 28.10 27.39 27.75 

gas velocity (ftlsec) 31.3 30.4 30.9 

gas flow (acfm) 53,149 51,599 52,374 

gas flow (dscfm) 37,278 33,579 35,429 

% isokinetic 99.1 105.7 102.4 
Interstate Brick 

West Jordan, Utah 

Scrubber4 

May 8, 2007 

EPA Method 29 : Determination of Metals Emissions from Stationary Sources 

Particulate Emissions 

Run #1 Run#2 Average 

particulate emissions (gr/dscf) 0.0076 0.0053 0.0065 

particulate emissions (mg/dscm) 17.4 12.1 14.8 

particulate emissions (lb/hr) 2.43 1.52 1.98 

Multi-Metals Emissions 

Sb emissions (mg/dscm) 0.0000 0.0000 0.0000 

Sb emissions (lb/hr) 6.10E-06 4.72E-06 5.41E-06 

As emissions (mg/dscm) 0.0053 0.0055 0.0054 

As emissions (lb/hr) 7.45E-04 6.93E-04 7.19E-04 

Ba emissions (mg/dscm) 0.0059 0.0043 0.0051 

Ba emissions (lb/hr) 8.22E-04 5.42E-04 6.82E-04 

Be emissions (mg/dscm) 0.0000 0.0000 0.0000 

Be emissions (lb/hr) O.OOE+OO O.OOE+OO O.OOE+OO 

Cd emissions (mg/dscm) 0.2820 0.0145 0.1482 

Cd emissions (lb/hr) 3.94E-02 1.83E-03 2.06E-02 

Cr emissions (mg/dscm) 0.0070 0.0045 0.0058 

Cr emissions (lb/hr) 9.72E-04 5.72E-04 7.72E-04 

Co emissions (mg/dscm) 0.0031 0.0026 0.0028 

Co emissions (lb/hr) 4.27E-04 3.23E-04 3.75E-04 

Cu emissions (mg/dscm) 0.0151 0.0066 0.0109 

Cu emissions (lb/hr) 2.11E-03 8.32E-04 1.47E-03 

Pb emissions (mg/dscm) 0.0019 0.0020 0.0019 

Pb emissions (lb/hr) 2.65E-04 2.46E-04 2.56E-04 

Mn emissions (mg/dscm) 0.0066 0.0101 0.0083 

Mn emissions (lb/hr) 9.19E-04 1.27E-03 1.10E-03 

Hg emissions (mg/dscm) 0.0024 0.0063 0.0043 

Hg emissions (lb/hr) 3.36E-04 7.91E-04 5.64E-04 

Ni emissions (mg/dscm) 0.0264 0.0078 0.0171 

Ni emissions (lb/hr) 3.69E-03 9.85E-04 2.34E-03 

P emissions (mg/dscm) 0.0326 0.0343 0.0334 

P emissions (lb/hr) 4.55E-03 4.32E-03 4.43E-03 

Se emissions (mg/dscm) 0.0274 0.0350 0.0312 

Se emissions (lb/hr) 3.83E-03 4.41E-03 4.12E-03 

Ag emissions (mg/dscm) 0.0002 0.0001 0.0001 

Ag emissions (lb/hr) 2.57E-05 7.15E-06 1.64E-05 

Tl emissions (mg/dscm) 0.0003 0.0003 0.0003 

Tl emissions (lb/hr) 3.66E-05 3.29E-05 3.48E-05 

Zn emissions (mg/dscm) 0.0211 0.0282 0.0247 

Zn emissions (lb/hr) 2.95E-03 3.55E-03 3.25E-03 

A laboratory result of NO was assummed to be zero: all detected fractions were added. 
AIR 

POLLUTION 

TESTING, INC. 

Appendix 'Tvvo: Field Data 

- .. :.... _: . : .. :.;:.._·_:. 

', 

Air Pollution Testing, Inc. : Laboratory lmpinger Weight Gain Datasheet 

APT Job#: IS I i I{ 71 'I lf Barometric Pressure : 

Facility: /.rfcrs:. k~c... l£r-:ck :>5'\1 Date: :51~/0'f 

Orsat 10: Op_erator: I}!). L Stack 10: Sc...ru.bl~c- 1 Lea!< Check: v 

Run#: ) Methoc: Sample Box ID: 

Impinge;# I lni~::.: Mass Final Mass 

I Gain I Loss Notes 

and Contents I (c-~ms) . (arams) (a rams) 

1 - I :!1~1?..~ 7--SB, <o ~-?_ Fi· (fee TP 2 I 73~ .3 I 7-SL~ \C:,.1 OoG ).Cf() 

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' I Total ! 

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Run#: i'Jet~od: Sample Box ID : 

lmping-s~ != 1:-~i:::.· :,i::.::s Fi:"'al Mass 

I Galn I Loss ~·))tGS 

and Con:en:s (C'2T:S) (qrams) (<:)rams) 

{ 97 _z_ I (flO.( I ,..-

·ro i I t' . 1 f .: I' 

2 : 73'-f,Z_ I 75r'o. ·'A I 6o b2 en 

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Total 

8 

I 

I 

L\)'iq t; '-(L(/5. ~ 

8 (tLL ~) 

Run#: i.iethod: '-... / SampleBox ID : 

Impinge;# l ~:ita~ L~c.ss Final Mass Gain I Loss Notes 

and Conte:-~ts (qr<:T:S) (a rams) (grams) 

1 I 

I 2 • 

3 I 

4 I 

5 I 

6 

7 

8 

Total 
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Air Pollution Testing, Inc. : Laboratory lmplnger Weight Gain Datasheet i 

APT Job# : L::i) 7/Y L{ Barometric Pressure : CJ.') ~ Date: .'JX!OiFacility:\ \(\\(t'S Yv; c \"x;:c,l_.,, Orsat ID: / Operator : 1 N. L-, 

Stack ID: k:i, L/ Leak Check:v 

/ 

Sample Box ID : I 

Run#: Method: 

lmpinger # lnital Mass Final Mass Gain I Loss Notes 

I 

and Contents (grams) (qrams) (grams} 

L /-;II er TO 

2 7/f~ .~ s-ot. 1 0062r;?? 

I 3 ~11 ,_J)-1 '"l,.ll ;;: 

/ 77 2.2 

I 4 ~ilS, b b lt. 4 

{ 5 ~ 737-. 7__ 731. I 

6 · r~e,~ 780.7 

7 lo~-t ?- 7Cft.l 

~ 8 f /"'-.\ I 

Total 41.130.7 Lj ~ qb. ) ( 6s. s.) 

\ Run#: Method: · SambteB~: 

lmpinger # lnital Mass Final Mass Gain I Loss Notes 

and Contents (grams) (grams) (gram~ 

1 -;'-jy l ~02,1 £-J-fev 1fJ 

2 77~~· {) 776.,_5 ;d--1 .... 

3 CfJL. s 6!1~ '7 1l ~~~~ 

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5 785.6 7~5,'2 

6 ~I l 7C)6,6 

7 

8 ....--""--....... 

Total L-l~~o.Y L)'St)K z ( l/7 8? 

Run#: Method: Sa~xiD: 

lmpinger # lnital Mass Final Mass Gain I Loss Notes 

and Contents (grams) (grams) (Qrams) 

1 

2 

3 

4 

5 

6 

7 

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AIR 

POLLUTION 

TESTING, INC. 

Appendix Three: Laboratory Data 
Air Pollution Testing, Inc. 

Gravimetric Laboratory Data Sheet 

Analytical Balance APX-1 00 

Project Code: IS87144 Stack ID: Scrub 3 

Run#: F.8. Test Date: 5/8/2007 

Description: Filter 

APT Sample ID: #6330 

Identification: Metals Filter 

Project Code: IS87144 Stack ID: Scrub 3 

Run#: 1 Test Date: 5/8/2007 

Description: Filter 

APT Sample ID: #6290 

Identification: Metals Filter 

Project Code: IS87144 Stack ID: Scrub 3 

Run#: 2 Test Date: 5/8/2007 

Description: Filter 

APT Sample ID: #6291 

Identification: Metals Filter 

Project Code: IS87144 Stack ID: Scrub 3 

Run#: 1 Test Date: 5/8/2007 

Description: Acetone 

APT Sample ID: 811524 

Identification: Cont. #2 

Project Code: IS87144 Stack ID: Scrub 3 

Run#: 2 Test Date: 5/8/2007 

Description: Acetone 

APT Sample ID: 811518 

Identification: Cont. #2 

Project Code: IS87144 Stack ID: Scrub 3 

Run#: T.8. Test Date: 5/8/2007 

Description: Acetone 

APT Sample ID: 811510 

Identification: Cont. #2 

Project Code: IS87144 Stack ID: Scrub 4 

Run#: F.8. Test Date: 5/8/2007 

Description: Filter 

APT Sample ID: #6327 

Identification: Metals Filter 

Project Code: IS87144 Stack ID: Scrub 4 

Run#: 1 Test Date: 5/8/2007 

Description: Filter 

APT Sample ID: #6283 

Identification: Metals Filter 

Project Code: IS87144 Stack ID: Scrub 4 

Run#: 2 Test Date: 5/8/2007 

Description: Filter 

APT Sample ID: #6287 

Identification: Metals Filter 

Project Code: IS87144 Stack ID: Scrub 4 

Run#: 1 Test Date: 5/8/2007 

Description: Acetone 

APT Sample ID: 811286 

Identification: Cont. #2 

Date Time Tare Date Time Final Net 

20-Nov-06 2:55PM 0.4186 18-May-07 7:22AM 0.4200 0.00130 

27-Nov-06 12:48 PM 0.4187 18-May-07 2:19PM 0.4199 

avg tare mass (gm): 0.41865 avg final mass(gm): 0.41995 

Date Time Tare Date Time Final Net 

8-0ct-06 9:55AM 0.3792 18-May-07 7:23AM 0.4257 0.04615 

18-0ct-06 4:00PM 0.3795 18-May-07 2:21PM 0.4253 

avg tare mass (gm): 0.37935 avg final mass(gm): 0.42550 

Date Time Tare Date Time Final Net 

25-Sep-06 7:57PM 0.3794 18-May-07 2:33PM 0.4268 0.04715 

3-0ct-06 11:04 AM 0.3796 21-May-07 8:10AM 0.4265 

avg tare mass (gm): 0.37950 avg final mass(gm): 0.42665 

Date Time Tare Date Time Final Net 

18-Apr-07 10:02 AM 6.1604 17-May-07 3:16PM 6.1622 0.00160 

19-Apr-07 10:21 AM 6.1607 18-May-07 7:36AM 6.1621 

avg tare mass (gm): 6.16055 avg final mass(gm): 6.16215 

Date Time Tare Date Time Final Net 

18-Apr-07 10:03AM 6.2373 17-May-07 3:12PM 6.2381 0.00060 

19-Apr-07 10:18 AM 6.2372 18-May-07 7:36AM 6.2376 

avg tare mass (gm): 6.23725 avg final mass(gm): 6.23785 

Date Time Tare Date Time Final Net 

18-Apr-07 3:47PM 6.2267 17-May-07 3:14PM 6.2267 0.00000 

19-Apr-07 10:07 AM 6.2264 18-May-07 7:37AM 6.2264 

avg tare mass (gm): 6.22655 avg final mass(gm): 6.22655 

Date Time Tare Date Time Final Net 

30-0ct-06 2:00PM 0.4311 18-May-07 7:25AM 0.4318 0.00100 

2-Nov-06 4:36PM 0.4309 18-May-07 2:20PM 0.4322 

avg tare mass (gm): 0.43100 avg final mass(gm): 0.43200 

Date Time Tare Date Time Final Net 

25-Sep-06 7:48PM 0.3780 18-May-07 7:21 0.3849 0.00770 

8-0ct-06 9:52AM 0.3768 18-May-07 2:24PM 0.3853 

avg tare mass (gm): 0.37740 avg final mass(gm): 0.38510 

Date Time Tare Date Time Final Net 

8-0ct-06 9:50AM 0.3784 18-May-07 7:21AM 0.3865 0.00805 

18-0ct-06 4:01PM 0.3789 18-May-07 2:20PM 0.3869 

avg tare mass (gm): 0.37865 avg final mass(gm): 0.38670 

Date Time Tare Date Time Final Net 

13-Feb-07 5:17PM 6.2015 17-May-07 3:17PM 6.2097 0.00825 

14-Feb-07 11:21 AM 6.2010 18-May-07 7:35AM 6.2093 

avg tare mass (gm): 6.20125 avg final mass(gm): 6.20950 
Project Code: ISB7144 Stack ID: Scrub 4 Date Time Tare Date Time Final Net 

Run#: 2 Test Date: 5/8/2007 18-Apr-07 9:59AM 6.0946 17-May-07 3:11PM 6.0971 0.00260 

Description: Acetone 19-Apr-07 10:13 AM 6.0944 18-May-07 7:37AM 6.0971 

APT Sample ID: 811516 

Identification: Cont. #2 avg tare mass (gm): 6.09450 avg final mass(gm): 6.09710 

Project Code: ISB7144 Stack ID: Scrub 4 Date Time Tare Date Time Final Net 

Run#: T.B. Test Date: 5/8/2007 18-Apr-07 3:45PM 6.2271 17-May-07 3:15PM 6.2267 -0.00010 

Description: Acetone 19-Apr-07 10:11 AM 6.2267 18-May-07 7:35AM 6.2269 

APT Sample ID: 811513 

Identification: Cont. #2 avg tare mass (gm): 6.22690 avg final mass(gm): 6.22680 

Project Code: ISB7144 Stack ID: Scrub 3/4 Date Time Tare Date Time Final Net 

Run#: F.B. Test Date: 5/8/2007 20-Nov-06 9:44AM 0.4224 18-May-07 7:22AM 0.4228 0.00040 

Description: Filter 27-Nov-06 1:01PM 0.4227 18-May-07 2:23PM 0.4231 

APT Sample ID: #6342 

Identification: Metals Filter Blank avg tare mass (gm): 0.42255 avg final mass(gm): 0.42295 

Project Code: ISB7144 Stack ID: Scrub 3/4 Date Time Tare Date Time Final Net 

Run#: R.B. Test Date: 5/8/2007 18-Apr-07 9:57AM 6.2139 17-May-07 3:12PM 6.2139 -0.00040 

Description: Acetone 19-Apr-07 10:25AM 6.2142 18-May-07 7:38AM 6.2134 

APT Sample ID: 811501 

Identification: Cont. #2 avg tare mass (gm): 6.21405 avg final mass(gm): 6.21365 
June 19, 2007 

STL SACRAMENTO PROJECT NUMBER: G7E230399 

PO/CONTRACT: ISB 7144 

Karl Breuer 

Air Pollution Testing 

5530 Marshall Street 

Arvada, CO 80002 

Dear Mr. Breuer, 

STL 

STL Sacramento 

880 Riverside Parkway 

West Sacramento, CA 95605 

Tel: 916 373 5600 

Fax: 916 372 1059 

www.stl-inc.com 

This report contains the analytical results for the samples received under chain of custody by 

STL Sacramento on May 15, 2007. These samples are associated with your ISB 7144 

project. 

The test results in this report meet all NELAC requirements for parameters that accreditation 

is required or available. Any exceptions to NELAC requirements are noted in the case 

narrative. The case narrative is an integral part of this report. 

Ifyou have any questions, please feel free to call me at (916) 374-4333. 

Sincerely, 

Robert W eidenfeld 

Project Manager 

@2007, Severn Trent Laboratories, Inc. All rights reserved. 

STL & Design• are registered service marks of Severn Trent Laboratories, Inc. 
TABLE OF CONTENTS 

STL SACRAMENTO PROJECT NUMBER G7E230399 

Case Narrative 

STL Sacramento Quality Assurance Program 

Sample Description Information 

Chain of Custody Documentation 

Metals - Various Methods 

Samples: 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11, 12, 13, 14, 15 

Sample Data Sheet 

Method Blank Reports 

Laboratory QC Reports 

Full Raw Data Package 
G7E230399 

CASE NARRATIVE 

STL SACRAMENTO PROJECT NUMBER G7E230399 

General Comment 

As requested, the desiccated acetone rinse was analyzed independently from the other front 

half fractions. Usually, the reconstituted acetone rinse is combined with the filter and front 

half rinse for a single analysis. 

AIR, ICPMS Metals-BH 

Sample(s): 3, 6, 9, 12, 15 

The method blank associated with the above sample fractions is positive for phosphorous at 

10.7 ug which is above the 10.0 reporting limit. 

There were no other anomalies associated with this project. 

STL Sacramento (916) 373 - 5600 1 of 678 
G7E230399 

STL Sacramento Certifications/Accreditations 

*NELAP accredited. A more detailed parameter Jist is available upon request. Update 1/27/05 

QC Parameter Definitions 

QC Batch: The QC batch consists of a set of up to 20 field samples that behave similarly (i.e., same matrix) 

and are processed using the same procedures, reagents, and standards at the same time. 

Method Blank: An analytical control consisting of all reagents, which may include internal standards and 

surrogates, and is carried through the entire analytical procedure. The method blank is used to define the level 

of laboratory background contamination. 

Laboratory Control Sample and Laboratory Control Sample Duplicate (LCSILCSD): 

An aliquot of blank matrix spiked with known amounts of representative target analytes. The LCS (and LCSD 

as required) is carried through the entire analytical process and is used to monitor the accuracy of the analytical 

process independent of potential matrix effects. If an LCSD is performed, it may also be used to evaluate the 

precision of the process. 

Duplicate Sample (DU): Different aliquots of the same sample are analyzed to evaluate the precision of 

an analysis. 

Surrogates: Organic compounds not expected to be detected in field samples, which behave similarly to 

target analytes. These are added to every sample within a batch at a known concentration to determine the 

efficiency of the sample preparation and analytical process. 

Matrix Spike and Matrix Spike Duplicate (MS/MSD): An MS is an aliquot of a matrix fortified 

with known quantities of specific compounds and subjected to an entire analytical procedure in order to 

indicate the appropriateness of the method for a particular matrix. The percent recovery for the respective 

compound(s) is then calculated. The MSD is a second aliquot of the same matrix as the matrix spike, also 

spiked, in order to determine the precision of the method. 

Isotope Dilution: For isotope dilution methods, isotopically labeled analogs (internal standards) of the 

native target analytes are spiked into the sample at time of extraction. These internal standards are used for 

quantitation, and monitor and correct for matrix effects. Since matrix effects on method performance can be 

judged by the recovery of these analogs, there is little added benefit of performing MS/MSD for these methods. 

MS/MSD are only performed for client or QAPP requirements. 

Control Limits: The reported control limits are either based on laboratory historical data, method 

requirements, or project data quality objectives. The control limits represent the estimated uncertainty of the 

test results. 

STL Sacramento {916) 373- 5600 2 of 678 
G7E230399 

WO# SamQle # 

JXKWV I 

JXKWO 2 

JXKW1 3 

JXKW3 4 

JXKW4 5 

JXKW5 6 

JXKW6 7 

JXKW7 8 

JXKW8 9 

JXKW9 10 

JXKXA 11 

JXKXC 12 

JXKXD 13 

JXKXE 14 

JXKXF 15 

Notes(s): 

Sample Summary 

G7E230399 

Client SamQle ID Sam12ling Date 

SCRUB 3-RUN 1-FH 5/8/2007 

SCRUB 3-RUN 1-FH/ACETONE 5/8/2007 

SCRUB 3-RUN 1-BH 5/8/2007 

SCRUB 3-RUN 2-FH 5/8/2007 

SCRUB 3-RUN 2-FHIACETONE 5/8/2007 

SCRUB 3-RUN 2-BH 5/8/2007 

SCRUB 3-TRAIN BLANK-PH 5/8/2007 

SCRUB 3-TRAIN BLNK-FHIACETONE 5/8/2007 

SCRUB 3-TRAINBLANK-BH 5/8/2007 

SCRUB 4-RUN 1-FH 5/8/2007 

SCRUB 4-RUN 1-FHIACETONE 5/8/2007 

SCRUB 4-RUN l-BH 5/8/2007 

SCRUB 4-RUN 2-FH 5/8/2007 

SCRUB 4-RUN 2-FHIACETONE 5/8/2007 

SCRUB 4-RUN 2-BH 5/8/2007 

The analytical results of the samples listed above are presented on the following pages. 

All calculations are perfonned before rounding to avoid round-off errors in calculated result.~. 

Results noted as "ND" were not detected at or above the stated limit. 

This report must not be reproduced, ex.cept in full, without the written approval of the laboratory. 

Received Date 

5115/2007 09: I 0 AM 

5115/2007 09: I 0 AM 

5115/2007 09: I 0 AM 

5/15/2007 09: 10 AM 

5115/2007 09: I 0 AM 

5/15/2007 09:10AM 

5115/2007 09:10AM 

5115/2007 09:10AM 

5/15/2007 09:10AM 

5115/2007 09: I 0 AM 

5115/2007 09: I 0 AM 

5/15/2007 09:10AM 

5/15/2007 09:10AM 

5/15/2007 09: I 0 AM 

5115/2007 09: I 0 AM 

Results for the following parameters are never reported on a dry weight basis: color, corrosivity, density. nashpoint. ignitability, 

layers, odor, paint filter test, pH, porosity, pressure, reactivity, redox. potential, specific gravity, spot tests, solids. solubility, 

temperature, viscosity, and weight 

STL Sacramento (916) 373 - 5600 3 of 678 
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Chain of Cu$tody I Sample Log T: (303) 420 5949 

F: (303) 420 5920 t-f Project Code Page_1,_ of_. Client 

Facility Name 

Project Manager 

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f.·~ nLL 6rx 342__ 

Rrt~r~kl 

Date/Time 

Collected 

'5;. 8· 67 

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. 
G7E230399 

Chain of Custody 

May 21, 2007 

To: Robert Weidenfeld 

STL West Sacramento 

880 Riverside Parkway 

West Sacramento, CA 95605 

From: Mike Cugnetti 

Air Pollution Testing, Inc. 

5530 Marshall St. 

Arvada, Colorado 80002 

RE: ISB7144 Method 29 analysis 

Dear Robert, 

This shipment includes seven filters and seven aluminium tins for Method 29 analysis 

and APT chain of custody documentation for these samples. The samples have been 

shipped one box. 

Please contact Paul Ottenstein regarding the details of this analysis before starting. 

We would ask for summary data to bee-mailed to Karl Breuer (kbreuer@airtest.net). As 

usual, we would also ask for the raw data to mailed at your convenience and may be 

directed to Karl Breuer. 

Please do not hesitate to call me if you should have any questions- and as always, 

thank you as always for your continued assistance! 

Relinquished by: Date/Time: Received by: Daterrime: 

STL Sacramento (916) 373- 5600 8 of678 
m 

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g_~
TL LOT RECEIPT CHECKLIST 

STL Sacramento 

CLIENT frfl PM~ LOG # 4:5 Lf7 {;:; 

LOT# (QUANTIMS 10) G'rtJ:;o :11 q QUOTE# 7 ~ r r LOCATION Y'f" -rc__ ~-"2-( --c"1 

DATE RECEIVED y£>" .-c '1 

qW 

TIME RECEIVED D( { (2 

DELIVERED BY -j1FEDEX 

0AIRBORNE 

D UPS 

0 CA OVERNIGHT 

0 GOLDENSTATE 

0 BAX GLOBAL 

~CLIENT 

ODHL 

0 GO-GETTERS 

0 STL COURIER 

OOTHER 

CUSTODY SEAL STATUS 0 INTACT 

0 COURIERS ON DEMAND 

0 BROKEN )1 N/A 

CUSTODY SEAL #(S) ·-------------==----------

SHIPPPING CONTAINER($) 0 STL ~ENT 0 N/A 

TEMPERTURE RECORD (IN °Cl IR 10 3D ~HER f{J( 

coc #($) 

TEMPERATURE BLANK Observed: corrected: __ _ 

SAMPLE TEMPERATURE 

Observed: tlth~£.-Average: corrected Average: __ _ 

COLLECTOR'S NAME: 0 Verified from COC ja1\fot on COC 

pH MEASURED DYES OANOMALY .clN/A 

LABELED BY ......................................................................................... . 

LABELS CHECKED BY .... · ..................................................................... .. 

PEER REVIEW ~ 

SHORT HOLD TEST NOTIFICATION SAMPLE RECEIVING 

WETCHEM )Z( N/ A 

VOA-ENCORES J2(N/A 

0 METALS NOTIFIED OF FILTER/PRESERVE VIA VERBAL & EMAIL 

dcoMPLETE SHIPMENT RECEIVED IN GOOD CONDITION WITH f ~PPROPRIATE TEMPERATURES, CONTAINERS, PRESERVATIVES 

6N/A 

ON/A 

D Clouseau 

0WET ICE 

0 TEMPERATURE EXCEEDED (2 oc- 6 ocl·1 rzl N/A 

0 BLUE ICE 0 GEL PACK 0 NO COOLING AGENTS USED 

Initials 

0)-

~ 

I 

\\ v 

\J 0 PM NOTIFIED 

Notes: _________________________________ ___ 

*1 Acceptable temperature range for State of Wisconsin samples is~4°C. 

G?E M:fs~E NO SPACES BLANK. USE "N/A" IF NOT APPLI~S§.cr!iWil;kfh. (!#6) f3?3~5frkie "N/A" ENTRIES. QA-185 5/05 EM, Paget 3 of 678 
S.EVE=RN ~· .;;. - ~, ~ •• _ ...... '!: .. -

TL 1:50Uie LUl H IVt:::ll LUI y 

~t (j 7E?=~o:I0 1 

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 

VOA* / / / v / v v v / / / v v / / .L v k:' /_ 

VOAh* / / / v ~ L v v / / v v L / / v / / / 

AGB 

AGBs 

250AGB 

250AGBs 

250AGBn 

500AGB 

AGJ 

500AGJ :?) ·~ -~ ~ :; 3 "3 - 250AGJ 

125AGJ ., ~ J 1 \ \ J ( 

CGJ 

500CGJ 

250CGJ 

125CGJ 

pJ 

PJn 

500PJ 

500PJn - 500PJna 

500PJzn/na 

250PJ 

250PJn 

250PJna 

250PJzn/na 

Acetate Tube 

__ "CT 

Encore 

Folder/filter 

PUF 

Petri/Filter I l r r \ [ i 

XADTrap . " , 

Ziploc 

\' tt . \A. I I \ f I J I 

1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 

1 == hydrochloric acid s = sulfuric acid na = sodium hydroxide 

..Jumb~r of VOAs with air bubbles present I total number of VOA's 

n = nitric acid zn = zinc acetate 

G7E230399 

QA-185 3/05 EM 

Page2 

20 

v 

/ 

20 

STL Sacramento (916) 373 - 5600 14 of 678 
Metals - Various Methods 

G7E230399 STL Sacramento (916) 373 - 5600 15 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 1-FH 

Lot-Sample f ... : G7E230399-001 

Date Sampled ••• : 05/08/07 

TOTAL Metals 

Date Received •• : 05/15/07 

REPORTING 

Matrix ••••.•• : AIR 

PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS ~ME~T~H~O~D ___________ ANALYSIS DATE ORDER # 

Prep Batch 1 ... : 7152355 

Hg (FH) 0.018 B 0.030 ug SW846 7470A 06/01/07 JXKWVlAA 

Dilution Factor: 0.15 

Prep Batch .... : 7155426 

Sil.ver 0.056 B 0.15 ug SW846 6020 05/29-06/15/07 JXKWV1AC 

Dilution Factor: 1 

Arsenic 66.5 J 0.30 ug SW846 6020 05/29-06/15/07 JXKWV1AD 

Dilution Factor: 1 

Barium 3.2 0.15 ug SW846 6020 05/29-06/16/07 JXKWV1AE 

Dilution Factor: 1 

Beryllium ND 0.15 ug SWB46 6020 05/29-06/15/07 JXKWV1AF 

Dilution Factor: 1 

Cadmium 0.23 0.15 ug SW846 6020 05/29-06/15/07 JXKWV1AG 

Dilution Factor: 1 

Cobal.t 1.0 0.15 ug SW846 6020 05/29-06/15/07 JXKWV1AH 

Dilution Factor: 1 

Chromium 4.1 0.30 ug SW846 6020 05/29-06/15/07 JXKWV1AJ 

Dilution Factor: 1 

Copper 2.3 0.30 ug SW846 6020 05/29-06/15/07 JXKWV1AK 

Dilution Factor: 1 

Manganese 1.4 0.15 ug SW846 6020 05/29-06/15/07 JXKWVlAL 

Dilution Factor: 1 

Nickel 0.68 0.30 ug SW846 6020 05/29-06/15/07 JXKWVlAM 

Dilution Factor: 1 

Lead 1.6 0.15 ug SW846 6020 05/29-06/15/07 JXKWVlAN 

Dilution Factor: 1 

Phosphorus 7.8 7.5 ug SW846 6020 05/29-06/15/07 JXKWVlAP 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373- 5600 16 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 1-FH 

TOTAL Metals 

,Lot-Sample I ... : G7E230399-001 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Antimony 0.074 B 0.30 ug SW846 6020 

Dilution Factor: 1 

Selenium 18.7 0.30 ug SW846 6020 

Dilution Factor: 1 

Thallium 1.3 0.15 ug SW846 6020 

Dilution Factor: 1 

Zinc 12.2 0.75 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is less than RL. 

J Method blank contamination. The a'iSOciated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/29-06/15/07 JXKWV1AQ 

05/29-06/15/07 JXKWV1AR 

05/29-06/15/07 JXKWV1AT 

05/29-06/15/07 JXKWV1AU 

17 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 1-FH/ACETONE 

Lot-Sample 1 ••• : G7E230399-002 

Date Sampled ••• : 05/08/07 

TOTAL Metals 

Date Received •• : 05/15/07 

Matrix ••••••• : AIR 

REPORTING PREPARATION- WORK 

~P~A~RAM~=E=T=E~R~---- ~R~E~S=U~L~T _______ LIMIT ~UN~I~T~S _____ ~M~E~T~H~O~D ___________ ANALYSIS DATE ORDER # 

Prep Batch t ... : 7152355 

Hg (FH) 0.015 B 

Prep Batch t ... : 7155426 

Silver 0.0090 B 

Arsenic 0.20 B,J 

Barium ND 

Beryllium ND 

cadmium 0.12 B 

Cobalt 0.12 B 

Chromium ND 

Copper 0.048 B 

Manganese 0.035 B 

Nickel 0.038 B 

Lead 0.048 B 

Phosphorus ND 

G7E230399 

0.030 ug SW846 7470A 06/01/07 JXKW01AA 

Dilution Factor: 0.15 

0.15 ug SW846 6020 05/29-06/15/07 JXKW01AC 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKWOIAD 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/16/07 JXKW01AE 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW01AF 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW01AG 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW01AH 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKW01AJ 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKW01AK 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW01AL 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKWOlAM 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW01AN 

Dilution Factor: 1 

7.5 ug SW846 6020 05/29-06/15/07 JXKW01AP 

Dilution Factor: 1 

(Continued on next page) 

STL Sacramento (916) 373- 5600 18 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 1-FH/ACETONE 

TOTAL Metals 

Lot-Sample t ... : G7E230399-002 Matrix .•....... : AIR 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Antimony ND 0.30 ug SW846 6020 05/29-06/15/07 JXKW01AQ 

Dilution Factor: 1 

Selenium ND 0.30 ug SW846 6020 05/29-06/15/07 JXKW01AR 

Dilution Factor: 1 

Thallium ND 0.15 ug SW846 6020 05/29-06/15/07 JXKW01AT 

Dilution Factor: 1 

Zinc ND 0.75 ug SW846 6020 05/29-06/15/07 JXKW01AU 

Dilution Factor: 1 

NOTE S : 

B Estimated result. Result isles.< than RL. 

J Method blank contamination. The as.<ociated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 19 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 1-BH 

TOTAL Metals 

Lot-Sample f ••• : G7E230399-003 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

PARAMETER RESULT 

Prep Batch 1 ... : 7152356 

Hg (HN03/H202) 1.9 G 

Prep Batch t ... : 7152357 

Hg (KMn04) ND 

Prep Batch I ... : 7152358 

Hg (Empty) ND G 

Prep Batch .... : 7152359 

Hg (HCl) 2.7 

Prep Batch i ... : 7155429 

Silver 0.028 B 

Arsenic 1.7 J 

Barium 1.1 

Beryllium ND 

Cadmium 2.3 

Cobalt 0.87 

Chromium 1.4 

Copper 1.8 

G7E230399 

REPORTING 

LIMIT =U~N=I=T~S _____ ~M~E~T~H~O~D~---------

0.73 ug SW846 7470A 

Dilution Factor: 3.67 

0.10 ug SW846 7470A 

Dilution Factor: o.s 

0.20 ug SW846 7470A 

Dilution Factor: 1 

0.10 ug SW846 7470A 

Dilution Factor: 0.5 

0.21 ug SW846 6020 

Dilution Factor: 1 

0.41 ug SW846 6020 

Dilution Factor: 1 

0.21 ug SW846 6020 

Dilution Factor: 1 

0.21 ug SW846 6020 

Dilution Factor: 1 

0.21 ug SW846 6020 

Dilution Factor: 1 

0.21 ug SW846 6020 

Dilution Factor: 1 

0.41 ug SW846 6020 

Dilution Factor: l 

0.41 ug SW846 6020 

Dilution Factor: 1 

(Continued on next page) 

STL Sacramento (916) 373- 5600 

Matrix •••••.• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

06/01/07 JXKW11AA 

06/0 l/07 JXKW11AC 

06/01/07 JXKW11AD 

06/01/07 JXKWllAE 

05/31-06/15/07 JXKW11AF 

05/31-06/15/07 JXKWllAG 

05/31-06/15/07 JXKWllAH 

05/31-06/15/07 JXKW11AJ 

05/31-06/15/07 JXKWllAK 

05/31-06/15/07 JXKW11AL 

05/31-06/15/07 JXKW11AM 

05/31-06/15/07 JXKW11AN 

20 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 1-BH 

TOTAL Metals 

Lot-Sample f .•• : G7E230399-003 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Manganese 3.0 0.21 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.92 0.41 ug SW846 6020 

Dilution Factor: 1 

Lead 0.30 J 0.21 ug SW846 6020 

Dilution Factor: 1 

Phosphorus 42.0 J 10.3 ug SW846 6020 

Dilution Factor: 1 

Antimony ND 0.41 ug SW846 6020 

Dilution Factor: 1 

Selenium 7.7 0.41 ug SW846 6020 

Dilution Factor: 1 

Thallium ND 0.21 ug SW846 6020 

Dilution Factor: 1 

Zinc 6.1 1.0 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

G Elevated reporting limit. The reporting limit is elevated due to matrix interference. 

B E.<timated result. Result is less than RL. 

J Method blank contamination. The as.wciated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento {916) 373 • 5600 

Matrix ••••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/31-06/15/07 JXKW11AP 

05/31-06/15/07 JXKWllAQ 

05/31-06/15/07 JXKW11AR 

05/31-06/15/07 JXKW11AT 

05/31-06/15/07 JXKWllAU 

05/31-06/15/07 JXKW11AV 

05/31-06/15/07 JXKWllAW 

05/31-06/15/07 JXKW11AX 

21 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 2-FH 

TOTAL Metals 

Lot-Sample 1 ••• : G7E230399-004 Matrix ••••••• : AIR 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Prep Batch I ... : 7152355 

Hg (FH) 0.033 0.030 ug SW846 7470A 06/01/07 JXKW31AA 

Dilution Factor: 0.15 

Prep Batch .... : 7155426 

Silver 0.080 B 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AC 

Dilution Factor: 1 

Arsenic 54.0 J 0.30 ug SW846 6020 05/29-06/15/07 JXKW31AD 

Dilution Factor: 1 

Barium 3.1 0.15 ug SW846 6020 05/29-06/16/07 JXKW31AE 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AF 

Dilution Factor: 1 

Cadmium 1.1 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AG 

Dilution Factor: 1 

Cobalt 0.63 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AH 

Dilution Factor: 1 

Chromium 5.0 0.30 ug SW846 6020 05/29-06/15/07 JXKW31AJ 

Dilution Factor: 1 

Copper 3.5 0.30 ug SW846 6020 05/29-06/15/07 JXKW31AK 

Dilution Factor: 1 

Manganese 5.3 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AL 

Dilution Factor: 1 

Nickel 5.1 0.30 ug SW846 6020 05/29-06/15/07 JXKW31AM 

Dilution Factor: 1 

Lead 1.6 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AN 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 05/29-06/15/07 JXKW31AP 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 22 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 2-FH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-004 Matrix •.••••••• : AIR 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD 

~~~----------- ANALYSIS DATE ORDER # 

Antimony 0.071 B 0.30 ug SW846 6020 05/29-06/15/07 JXKW31AQ 

Dilution Factor: 1 

Selenium 18.6 0.30 ug SW846 6020 05/29-06/15/07 JXKW31AR 

Dilution Factor: 1 

Thallium 1.2 0.15 ug SW846 6020 05/29-06/15/07 JXKW31AT 

Dilution Factor: 1 

Zinc 13.6 0.75 ug SW846 6020 05/29-06/15/07 JXKW31AU 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is less than RL. 

J Method blank contamination. The associated method blank contains the target analytc at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 23 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 2~FH/ACETONE 

Lot-Sample 1 ..• : G7E230399-005 

Date Sampled ••• : 05/08/07 

TOTAL Metals 

Date Received •• : 05/15/07 

Matrix ••••••• : AIR 

REPORTING PREPARATION- WORK 

PARAMETER RESULT 

Prep Batch t ... : 7152355 

Hg (FH) ND 

Prep Batch 1 ... : 7155426 

Silver 0.0083 B 

Arsenic 0.18 B,J 

Barium ND 

Beryllium ND 

Cadmium 0.028 B 

Cobalt 0.29 

Chromium ND 

Copper 0.11 B 

Manganese 0.026 B 

Nickel 0.084 B 

Lead 0.064 B 

Phosphorus ND 

G7E230399 

LIMIT ~U~N~I~T~S _____ ~M~E~T~H~O~D~--------- ANALYSIS DATE ORDER # 

0.030 ug SW846 7470A 06/01/07 JXKW41AA 

Dilution Factor: 0.15 

0.15 ug SW846 6020 05/29-06/15/07 JXKW41AC 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKW41AD 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/16/07 JXKW41AE 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW41AF 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW41AG 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW41AH 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKW41AJ 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/07 JXKW41AK 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW41AL 

Dilution Factor: 1 

0.30 ug SW846 6020 05/29-06/15/01 JXKW41AM 

Dilution Factor: 1 

0.15 ug SW846 6020 05/29-06/15/07 JXKW41AN 

Dilution Factor: 1 

7.5 ug SW846 6020 05/29-06/15/07 JXKW41AP 

Dilution Factor: 1 

(Continued on next page} 

STL Sacramento (916) 373 - 5600 24of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 2-FH/ACETONE 

TOTAL Metals 

Lot-Sample t ... : G7E230399-005 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Antimony NO 0.30 ug SW846 6020 

Dilution Factor: 1 

Selenium 0.33 0.30 ug SWB46 6020 

Dilution Factor: 1 

Thallium NO 0.15 ug SW846 6020 

Dilution Factor: 1 

Zinc NO 0.75 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is les.< than RL. 

J Method blank contamination. The as.<ociated method blank contains the target analytc at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••... : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/29-06/15/07 JXKW41AQ 

05/29-06/15/07 JXKW41AR 

05/29-06/15/07 JXKW41AT 

05/29-06/15/07 JXKW41AU 

25 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 2-BH 

Lot-Sample f ..• : G7E230399-006 

Date Sampled ••• : 05/08/07 

TOTAL Metals 

Date Received •• : 05/15/07 

REPORTING 

Matrix ••••••• : AIR 

PREPARATION- WORK 

PARAMETER RESULT LIMIT ~~=----- UNITS ~M=E~T~H~O~D~---------- ANALYSIS DATE ORDER # 

Prep Batch .... : 7152356 

Hg (HN03/H202) 0.34 B,G 0.73 ug SW846 7470A 06/01/07 JXKW51AA 

Dilution Factor: 3.65 

Prep Batch t ... : 7152357 

Hg (KMn04) ND 0.10 ug SW846 7470A 06/01/07 JXKW51AC 

Dilution Factor: 0.5 

Prep Batch ft ••• : 7152358 

Hg (Empty) ND G 0.19 ug SW846 7470A 06/01/07 JXKW51AD 

Dilution Factor: 0.97 

Prep Batch f .•• : 7152359 

Hg (HC1) 2.7 0.10 ug SW846 7470A 06/01/07 JXKW51AE 

Dilution Factor: 0.5 

Prep Batch f ... : 7155429 

Silver 0.023 B 0.21 ug SW846 6020 05/31-06/15/07 JXKW51AF 

Dilution Factor: l 

Arsenic 0.71 J 0.41 ug SW846 6020 05/31-06/15/07 JXKW51AG 

Dilution Factor: 1 

Barium 1.2 0.21 ug SW846 6020 05/31-06/15/07 JXKW51AH 

Dilution Factor: l 

Beryllium ND 0.21 ug SW846 6020 05/31-06/15/07 JXKW51AJ 

Dilution Factor: l 

Cadmium 3.0 0.21 ug SW846 6020 05/31-06/15/01 JXKW51AK 

Dilution Factor: l 

Cobalt 1.0 0.21 ug SW846 6020 05/31-06/15/07 JXKW51AL 

Dilution Factor: 1 

Chromium 0.58 0.41 ug SW846 6020 05/31-06/15/07 JXKW51AM 

Dilution Factor: 1 

Copper 2.3 0.41 ug SW846 6020 05/31-06/15/07 JXKW51AN 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 26 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-RUN 2-BH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-006 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Manganese 1.7 0.21 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.51 0.41 ug SW846 6020 

Dilution Factor: 1 

Lead 0.16 B,J 0.21 ug SWB46 6020 

Dilution Factor: 1 

Phosphorus 29.3 J 10.4 ug SW846 6020 

Dilution Factor: 1 

Antimony ND 0.41 ug SW846 6020 

Dilution Factor: 1 

Selenium 3.7 0.41 ug SW846 6020 

Dilution Factor: 1 

Thallium ND 0.21 ug SW846 6020 

Dilution Factor: 1 

Zinc 4.2 1.0 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is less than RL. 

G Elevated reporting limit. The reporting limit L• elevated due to matrix interference. 

J Method blank contamination. The associated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373- 5600 

Matrix ••••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/31-06/15/07 JXKW51AP 

05/31-06/15/07 JXKW51AQ 

05/31-06/15/07 JXKW51AR 

05/31-06/15/07 JXKW51AT 

05/31-06/15/07 JXKW51AU 

05/31-06/15/07 JXKW51AV 

05/31-06/15/07 JXKW51AW 

05/31-06/15/07 JXKW51AX 

27 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-TRAIN BLANK-FH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-007 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING 

PARAMETER RESULT LIMIT ~U~N~I~T~S~--- ~M~E~T~H~O~D __________ _ 

Prep Batch I ... : 7152355 

Hg (FH) ND 0.030 ug SW846 7470A 

Dilution Factor: 0. 15 

Prep Batch f: ••• : 7155426 

Silver 0.0076 B 0.15 ug SW846 6020 

Dilution Factor: 1 

Arsenic ND 1.5 ug SW846 6020 

Dilution Factor: 5 

Barium 6.2 0.15 ug SW846 6020 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Cadmium 0.015 B 0.15 ug SW846 6020 

Dilution Factor: 1 

Cobalt 0.17 0.15 ug SW846 6020 

Dilution Factor: 1 

Chromium 0.72 0.30 ug SW846 6020 

Dilution Factor: 1 

Copper 0.51 0.30 ug SW846 6020 

Dilution Factor: l 

Manganese 0.44 0.15 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.61 0.30 ug SW846 6020 

Dilution Factor: l 

Lead 0.14 B 0.15 ug SW846 6020 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

06/01/07 JXKW61AA 

05/29-06/16/07 JXKW61AC 

05/29-06/17/07 JXKW61AD 

05/29-06/16/07 JXKW61AE 

05/29-06/16/07 JXKW61AF 

05/29-06/16/07 JXKW61AG 

05/29-06/16/07 JXKW61AH 

05/29-06/16/07 JXKW61AJ 

05/29-06/16/07 JXKW61AK 

05/29-06/16/07 JXKW61AL 

05/29-06/16/0l JXKW61AM 

05/29-06/16/07 JXKW61AN 

05/29-06/16/07 JXKW61AP 

28 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-TRAIN BLANK-FH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-007 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Antimony ND 0.30 ug SW846 6020 

Dilution Factor: 1 

Selenium 2.5 1.5 ug SW846 6020 

Dilution Factor: 5 

Thallium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Zinc 15.2 0.75 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is less than RL. 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/29-06/16/07 JXKW61AQ 

05/29-06/17/07 JXKW61AR 

05/29-06/16/07 JXKW61AT 

05/29-06/16/07 JXKW61AU 

29 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-TRAIN BLANK-FH/ACETONE 

TOTAL Metals 

Lot-Sample i ... : G7E230399-008 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Prep Batch 1 ... : 7152355 

Hg (FH) ND 0.030 ug SW846 7470A 

Dilution Factor: 0.15 

Prep Batch i ... : 7155426 

Silver ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Arsenic 0.098 B,J 0.30 ug SW846 6020 

Dilution Factor: 1 

Barium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Cadmium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Cobalt 0.26 0.15 ug SWB46 6020 

Dilution Factor: 1 

Chromium ND 0.30 ug SW846 6020 

Dilution Factor: 1 

Copper 0.047 B 0.30 ug SWB46 6020 

Dilution Factor: 1 

Manganese 0.024 B 0.15 ug SWB46 6020 

Dilution Factor: l 

Nickel ND 0.30 ug SW846 6020 

Dilution Factor: 1 

Lead 0.014 B 0.15 ug SW846 6020 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

06/01/07 JXKW71AA 

05/29-06/16/07 JXKW71AC 

05/29-06/16/07 JXKW71AD 

05/29-06/16/07 JXKW71AE 

05/29-06/16/07 JXKW71AF 

05/29-06/16/07 JXKW71AG 

05/29-06/16/07 JXKW71AH 

05/29-06/16/07 JXKW71AJ 

05/29-06/16/07 JXKW71AK 

05/29-06/16/07 JXKW71AL 

05/29-06/16/07 JXKW71AM 

05/29-06/16/07 JXKW71AN 

05/29-06/16/07 JXKW71AP 

30 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-TRAIN BLANK-FH/ACETONE 

TOTAL Metals 

Lot-Sample f ••. : G7E230399-008 Matrix ••••••••• : AIR 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Antimony ND 0.30 ug SW846 6020 05/29-06/16/07 JXKW71AQ 

Dilution Factor: 1 

Selenium ND 0.30 ug SW846 6020 05/29-06/16/07 JXKW71AR 

Dilution Factor: 1 

Thallium ND 0.15 ug SW846 6020 05/29-06/16/07 JXKW71AT 

Dilution Factor: 1 

Zinc ND 0.75 ug SW846 6020 05/29-06/16/07 JXKW71AU 

Dilution Factor: 1 

NOTE S : 

ll Estimated result. Resul! is less than RL. 

J Method blank contamination. The associated method blank contains the target analytc at a reportable level. 

G7E230399 STL Sacramento {916) 373 - 5600 31 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-TRAIN BLANK-BH 

Lot-Sample 1 ••• : G7E230399-009 

Date Sampled ••• : 05/08/07 

TOTAL Metals 

Date Received •• : 05/15/07 

REPORTING 

Matrix ••••••• : AIR 

PREPARATION- WORK 

~P~A~RAM~~E~T~E~R~----- ~R=E~S~U=L~T _______ =L=I~M=I~T ____ ~U~N=I~T=S _____ ~M~E~T~H~O~D~---------- ANALYSIS DATE ORDER # 

Prep Batch 1 ..• : 7152356 

Hg (HN03/H202) ND G 

Prep Batch .... : 7152357 

Hg (KMn04) ND 

Prep Batch t ... : 7152358 

Hg (Empty) ND G 

Prep Batch t ... : 7152359 

Hg (HCl) 0.030 B 

Prep Batch I ... : 7155429 

Silver ND 

Arsenic 0.46 J 

Barium ND 

Beryllium ND 

Cadmium 0.038 B 

Cobalt 0.73 

Chromium 0.86 

Copper 1.3 

G7E230399 

0.59 ug SW846 7470A 06/01/07 JXKW81AA 

Dilution Factor: 2.95 

0.10 ug SW846 7470A 06/01/07 JXKW81AC 

Dilution Factor: 0.5 

0.19 ug SW846 7470A 06/01/07 JXKW81AD 

Dilution Factor: 0.97 

0.10 ug SW846 7470A 06/01/07 JXKW81AE 

Dilution Factor: 0.5 

0.23 ug SW846 6020 05/31-06/15/07 JXKW81AF 

Dilution Factor: 1 

0.45 ug SW846 6020 05/31-06/15/07 JXKW81AG 

Dilution Factor: 1 

0.23 ug SW846 6020 05/31-06/15/07 JXKW81AH 

Dilution Factor: 1 

0.23 ug SW846 6020 05/31-06/15/07 JXKW81AJ 

Dilution Factor: 1 

0.23 ug SW846 6020 05/31-06/15/07 JXKW81AK 

Dilution Factor: 1 

0.23 ug SW846 6020 05/31-06/15/07 JXKW81AL 

Dilution Factor: 1 

0.45 ug SW846 6020 05/31-06/15/07 JXKW81AM 

Dilution Factor: 1 

0.45 ug SW846 6020 05/31-06/15/07 JXKW81AN 

Dilution Factor: 1 

(Continued on next page) 

STL Sacramento (916) 373 - 5600 32 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 3-TRAIN BLANK-BH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-009 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Manganese 0.28 0.23 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.39 B 0.45 ug SW846 6020 

Dilution Factor: l 

Lead 0.10 B,J 0.23 ug SW846 6020 

Dilution Factor: 1 

Phosphorus 36.6 J 11.4 ug SWB46 6020 

Dilution Factor: 1 

Antimony ND 0.45 ug SW846 6020 

Dilution Factor: 1 

Selenium ND 0.45 ug SW846 6020 

Dilution Factor: 1 

Thallium ND 0.23 ug SW846 6020 

Dilution Factor: 1 

Zinc 0.38 B 1.1 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

G Elevated reporting limil. The reporting limit is elevated due to matrix interference. 

B F_c;timated result. Result is less than RJ .. 

J Method blank contamination. The as.'<Ociated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/31-06/15/07 JXKW81AP 

05/31-06/15/07 JXKW81AQ 

05/31-06/15/07 JXKWBlAR 

05/31-06/15/07 JXKW81AT 

05/31-06/15/07 JXKW81AU 

05/31-06/15/07 JXKW81AV 

05/31-06/15/07 JXKW81AW 

05/31-06/15/07 JXKW81AX 

33 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 1-FH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-010 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Prep Batch ' ... : 7152355 

Hg (FH) 0.018 B 0.030 ug SW846 7470A 

Dilution Factor: 0.15 

Prep Batch t ... : 7155426 

Silver 0.16 0.15 ug SW846 6020 

Dilution Factor: 1 

Arsenic 4.0 J 0.30 ug SW846 6020 

Dilution Factor: 1 

Barium 4.2 0.15 ug SW846 6020 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Cadmium 242 0.15 ug SW846 6020 

Dilution Factor: 1 

Cobalt 1.9 0.15 ug SW846 6020 

Dilution Factor: 1 

Chromium 4.6 0.30 ~g SW846 6020 

Dilution Factor: 1 

Copper 11.6 0.30 ug SW846 6020 

Dilution Factor: 1 

Manganese 3.1 0.15 ug SW846 6020 

Dilution Factor: 1 

Nickel 22.2 0.30 ug SW846 6020 

Dilution Factor: 1 

Lead 1.4 0.15 ug SW846 6020 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

06/01/07 JXKW91AA 

05/29-06/16/07 JXKW91AC 

05/29-06/16/07 JXKW91AD 

05/29-06/16/07 JXKW91AE 

05/29-06/16/07 JXKW91AF 

05/29-06/16/07 JXKW91AG 

05/29-06/16/07 JXKW91AH 

05/29-06/16/07 JXKW91AJ 

05/29-06/16/07 JXKW91AK 

05/29-06/16/07 JXKW91AL 

05/29-06/16/07 JXKW91AM 

05/29-06/16/07 JXKW91AN 

05/29-06/16/07 JXKW91AP 

34 of678 
Air Pollution Testing 

Client Sample ID: SCRrlB 4-RUN 1-FH 

TOTAL Metals 

Lot-Sample f ... : G7E230399-010 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Antimony 0.040 B 0.30 ug SW846 6020 

Dilution Factor: 1 

Selenium 6.8 0.30 ug SW846 6020 

Dilution Factor: 1 

Thallium 0.24 0.15 ug SW846 6020 

Dilution Factor: 1 

Zinc 14.0 0.75 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is less than RL. 

J Method blank contamination. The associated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373 • 5600 

Matrix ••••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/29-06/16/07 JXKW91AQ 

05/29-06/16/07 JXKW91AR 

05/29-06/16/07 JXKW91AT 

05/29-06/16/07 JXKW91AU 

35 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 1-FH/ACETONE 

Lot-Sample 1 ••• : G7E230399-011 

Date Sampled ••• : 05/08/07 

TOTAL Metals 

Date Received •• : 05/15/07 

Matrix ••••••• : AIR 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT ~U~N~I~T=S _____ ~M=E~T~H~O=D ___________ ANALYSIS DATE ORDER # 

Prep Batch 1 ... : 7152355 

Hg (FH} ND 0.030 ug SW846 7470A 06/01/07 JXKXAlAA 

Dilution Factor: 0.15 

Prep Batch t ... : 7155426 

Silver ND 0.15 ug SW846 6020 05/29-06/16/07 JXKXAlAC 

Dilution Factor: 1 

Arsenic 0.14 B,J 0.30 ug SWB46 6020 05/29-06/16/07 JXKXA1AD 

Dilution Factor: 1 

Barium 0.23 0.15 ug SWB46 6020 05/29-06/16/07 JXKXA1AE 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 05/29-06/16/07 JXKXA1AF 

Dilution Factor: 1 

Cadmium 0.082 B 0.15 ug SW846 6020 05/29-06/16/07 JXKXA1AG 

Dilution Factor: 1 

Cobalt 0.14 B 0.15 ug SW846 6020 05/29-06/16/07 JXKXA1AH 

Dilution Factor: 1 

Chromium 0.47 0.30 ug SW846 6020 05/29-06/16/07 JXKXA1AJ 

Dilution Factor: 1 

Copper 0.31 0.30 ug SW846 6020 05/29-06/16/07 JXKXA1AK 

Dilution Factor: 1 

Manganese 0.32 0.15 ug SW846 6020 05/29-06/16/01 JXKXAlAL 

Dilution Factor: 1 

Nickel 1.5 0.30 ug SW846 6020 05/29-06/16/01 JXKXAlAM 

Dilution Factor: 1 

Lead 0.11 B 0.15 ug SW846 6020 05/29-06/16/01 JXKXAlAN 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 05/29-06/16/07 JXKXA1AP 

Dilution Factor: 1 

(Continued on next page} 

G7E230399 STL Sacramento (916} 373 • 5600 36 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 1-FH/ACETONE 

TOTAL Metals 

Lot-Sample 1 ... : G7E230399-011 Matrix .......•. : AIR 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Antimony ND 0.30 ug SW846 6020 05/29-06/16/07 JXKXA1AQ 

Dilution Factor: 1 

Selenium ND 0.30 ug SW846 6020 05/29-06/16/07 JXKXA1AR 

Dilution Factor: 1 

Thallium ND 0.15 ug SW846 6020 05/29-06/16/07 JXKXA1AT 

Dilution Factor: 1 

Zinc 0. 72 B 0.75 ug SW846 6020 05/29-06/16/07 JXKXAlAU 

Dilution Factor: 1 

NOTE S : 

B r,~timated result. Result is les.~ than Rl.. 

J Method blank contamination. The as.~ociated method blank contains the target analytc at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 37 of678 
Air Po~~ution Testing 

Client Sample ID: SCRUB 4-RUN 1-BH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-012 Matrix ••••••• : AIR 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Prep Batch i ... : 7152356 

Hg (HN03/H202} 0.19 B,G 0.78 ug SW846 7470A 06/01/07 JXKXC1AA 

Dilution Factor: 3. 9 

Prep Batch i ... : 7152357 

Hg (KMn04) ND 0.10 ug SW846 7470A 06/01/07 JXKXC1AC 

Dilut.ion Factor: 0.5 

Prep Batch :fl: ••• : 7152358 

Hg (Empty) 0.094 B,G 0.21 ug SW846 7470A 06/01/07 JXKXC1AD 

Dilution Factor: l. 03 

Prep Batch t ... : 7152359 

Hg (HCl) 1.9 0.10 ug SW846 7470A 06/01/07 JXKXC1AE 

Dilution Factor: 0.5 

Prep Batch i ... : 7155429 

Silver 0.0083 B 0.20 ug SW846 6020 05/31-06/15/07 JXKXC1AF 

Dilution Factor: 1 

Arsenic 0.74 J 0.40 ug SW846 6020 05/31-06/15/07 JXKXC1AG 

Dilution Factor: 1 

Barium 0.96 0.20 ug SW846 6020 05/31-06/15/07 JXKXC1AH 

Dilution Factor: 1 

Beryllium ND 0.20 ug SW846 6020 05/31-06/15/07 JXKXC1AJ 

Dilution Factor: l 

Cadmium 16.0 0.20 ug SW846 6020 05/31-06/15/07 JXKXC1AK 

Dilution Factor: 1 

Cobalt 0.76 0.20 ug SW846 6020 05/31-06/15/07 JXKXC1AL 

Dilution Factor: 1 

Chromium 1.3 0.40 ug SW846 6020 05/31-06/15/07 JXKXC1AM 

Dilution Factor: 1 

Copper 1.9 0.40 ug SW846 6020 05/31-06/15/07 JXKXC1AN 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 38 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 1-BH 

TOTAL Metals 

Lot-Sample i ... : G7E230399-012 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Manganese 2.6 0.20 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.48 0.40 ug SW846 6020 

Dilution Factor: 1 

Lead 0.23 J 0.20 ug SW846 6020 

Dilution Factor: 1 

Phosphorus 29.8 J 10.1 ug SW846 6020 

Dilution Factor: 1 

Antimony ND 0.40 ug SW846 6020 

Dilution Factor: 1 

Selenium 18.3 0.40 ug SW846 6020 

Dilution Factor: 1 

Thallium ND 0.20 ug SW846 6020 

Dilution Factor: 1 

Zinc 4.6 1.0 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B !JI;timaled resull. Resull is less than RL. 

G Elcva1ed reponing limil. The reponing limil is elcvaled due to matrix interference. 

J Method blank contamination. The associated method blank contains the target analytc al a reportable level. 

G7E230399 STL Sacramento (916) 373 • 5600 

Matrix •••••••.• : AIR 

PREPARATIONANALYSIS DATE 

05/31-06/15/07 

WORK 

ORDER # 

JXKXC1AP 

05/31-06/15/07 JXKXClAQ 

05/31-06/15/07 JXKXC1AR 

05/31-06/15/07 JXKXC1AT 

05/31-06/15/07 JXKXC1AU 

05/31-06/15/07 JXKXC1AV 

05/31-06/15/07 JXKXC1AW 

05/31-06/15/07 JXKXC1AX 

39 of 678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 2-FH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-013 Matrix ••••••• : AIR 

Date Sampled ••• : 05/08/07 Date Received •. : 05/15/07 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Prep Batch t ... : 7152355 

Hg {FH) 0.010 B 0.030 ug SW846 7470A 06/01/07 JXKXDlAA 

Dilution Factor: 0.15 

Prep Batch t ... : 7155426 

Silver 0.050 B 0.15 ug SW846 6020 05/29-06/16/07 JXKXD1AC 

Dilution Factor: 1 

Arsenic 4.0 J 0.30 ug SW846 6020 05/29-06/16/07 JXKXD1AD 

Dilution Factor: 1 

Barium 3.0 0.15 ug SW846 6020 05/29-06/16/07 JXKXD1AE 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 05/29-06/16/07 JXKXDlAF 

Dilution Factor: l 

Cadmium 9.2 0.15 ug SW846 6020 05/29-06/16/07 JXKXD1AG 

Dilution Factor: 1 

Cobalt 1.6 0.15 ug SW846 6020 05/29-06/16/07 JXKXDlAH 

Dilution Factor: 1 

Chromium 2.7 0.30 ug SW846 6020 05/29-06/16/07 JXKXD1AJ 

Dilution Factor: 1 

Copper 3.1 0.30 ug SW846 6020 05/29-06/16/07 JXKXD1AK 

Dilution Factor: 1 

Manganese 1.2 0.15 ug SW846 6020 05/29-06/16/07 JXKXD1AL 

Dilution Factor: 1 

Nickel 6.4 0.30 ug SW846 6020 05/29-06/16/07 JXKXD1AM 

Dilution Factor: l 

Lead 1.1 0.15 ug SW846 6020 05/29-06/16/07 JXKXD1AN 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 05/29-06/16/07 JXKXDlAP 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 40 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 2-FH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-013 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Antimony 0.033 B 0.30 ug SW846 6020 

Dilution Factor: 1 

Selenium 11.0 0.30 ug SW846 6020 

Dilution Factor: l 

Thallium 0.23 0.15 ug SW846 6020 

Dilution Factor: l 

Zinc 22.8 0.75 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B E.~timated result. Result is less than RL. 

J Method blank contamination. The as.wciated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••••.•• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/29-06/16/07 JXKXDlAQ 

05/29-06/16/07 JXKXDlAR 

05/29-06/16/07 JXKXDlAT 

05/29-06/16/07 JXKXD1AU 

41 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 2-FH/ACETONE 

TOTAL Metals 

Lot-Sample t ... : G7E230399-014 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING 

~P~A~RAM~=E~T=E~R~----- ~R=E~S~U=L~T_______ LIMIT UNITS METHOD 

Prep Batch t ... : 7152355 

Hg (FH} ND 0.030 ug SW846 7470A 

Dilution Factor: 0.15 

Prep Batch 1 ... : 7155426 

Silver ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Arsenic 0.094 B,J 0.30 ug SWB46 6020 

Dilution Factor: 1 

Barium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Beryllium ND 0.15 ug SW846 6020 

Dilution Factor: 1 

Cadmium 0.56 0.15 ug SW846 6020 

Dilution Factor: 1 

Cobalt 0.13 B 0.15 ug SW846 6020 

Dilution Factor: 1 

Chromium ND 0.30 ug SW846 6020 

Dilution Factor: 1 

Copper 0.017 B 0.30 ug SWB46 6020 

Dilution Factor: 1 

Manganese 1.1 0.15 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.058 B 0.30 ug SW846 6020 

Dilution Factor: 1 

Lead 0.44 0.15 ug SW846 6020 

Dilution Factor: 1 

Phosphorus ND 7.5 ug SW846 6020 

Dilution Factor: 1 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373- 5600 

Matrix ••••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

06/01/07 JXKXE1AA 

05/29-06/16/07 JXKXE1AC 

05/29-06/16/07 JXKXE1AD 

05/29-06/16/07 JXKXE1AE 

05/29-06/16/07 JXKXE1AF 

05/29-06/16/07 JXKXElAG 

05/29-06/16/07 JXKXE1AH 

05/29-06/16/07 JXKXE1AJ 

05/29-06/16/07 JXKXE1AK 

05/29-06/16/07 JXKXElAL 

05/29-06/16/07 JXKXElAM 

05/29-06/16/07 JXKXElAN 

05/29-06/16/07 JXKXE1AP 

42 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 2-FH/ACETONE 

TOTAL Metals 

Lot-Sample i ... : G7E230399-014 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Antimony ND 0.30 ug SW846 6020 

Dilution Factor: l 

Selenium ND 0.30 ug SW846 6020 

Dilution Factor: 1 

Thallium ND 0.15 ug SW846 6020 

Dilution Factor: l 

Zinc 0.24 B 0.75 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

B Estimated result. Result is less than RL. 

J Method blank contamination. The associated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento {916) 373 - 5600 

Matrix ••.•••••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/29-06/16/07 JXKXElAQ 

05/29-06/16/07 JXKXE1AR 

05/29-06/16/07 JXKXE1AT 

05/29-06/16/07 JXKXElAU 

43 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 2-BH 

TOTAL Metals 

Lot-Sample t ... : G7E230399-015 Matrix ••••••• : AIR 

Date Sampled ••• : 05/08/07 Date Received •• : 05/15/07 

REPORTING PREPARATION- WORK 

PARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER # 

Prep Batch t ... : 7152356 

Hg (HN03/H202) 2.8 G 0.79 ug SW846 7470A 06/01/07 JXKXFlAA 

Dilution Factor: 3.93 

Prep Batch i ... : 7152357 

Hg (KMn04) NO 0.10 ug SW846 7470A 06/01/07 JXKXF1AC 

Dilution Factor: 0.5 

Prep Batch i ... : 7152358 

Hg (Empty) 0.12 B,G 0.20 ug SW846 7470A 06/01/07 JXKXF1AD 

Dilution Factor: l. 02 

Prep Batch i ... : 7152359 

Hg (HCl) 2.6 0.10 ug SW846 7470A 06/01/07 JXKXF1AE 

Dilution Factor: 0.5 

Prep Batch I ... : 7155429 

Silver ND 0.20 ug SW846 6020 05/31-06/15/07 JXKXF1AF 

Dilution Factor: 1 

Arsenic 0.75 J 0.40 ug SW846 6020 05/31-06/15/07 JXKXF1AG 

Dilution Factor: 1 

Barium 0.79 0.20 ug SW846 6020 05/31-06/15/07 JXKXF1AH 

Dilution Factor: 1 

Beryllium ND 0.20 ug SW846 6020 05/31-06/15/07 JXKXF1AJ 

Dilution Factor: 1 

Cadmium 3.0 0.20 ug SW846 6020 05/31-06/15/07 JXKXF1AK 

Dilution Factor: 1 

Cobalt 0.53 0.20 ug SW846 6020 05/31-06/15/07 JXKXF1AL 

Dilution Factor: 1 

Chromium 1.3 0.40 ug SW846 6020 05/31-06/15/07 JXKXF1AM 

Dilution Factor: l 

Copper 2.7 0.40 ug SW846 6020 05/31-06/15/07 JXKXFlAN 

Dilution Factor: l 

(Continued on next page) 

G7E230399 STL Sacramento (916) 373 - 5600 44 of678 
Air Pollution Testing 

Client Sample ID: SCRUB 4-RUN 2-BH 

TOTAL Metals 

Lot-Sample i ... : G7E230399-015 

REPORTING 

PARAMETER RESULT LIMIT UNITS METHOD 

Manganese 6.6 0.20 ug SW846 6020 

Dilution Factor: 1 

Nickel 0.43 0.40 ug SW846 6020 

Dilution Factor: 1 

Lead 0.18 B,J 0.20 ug SW846 6020 

Dilution Factor: 1 

Phosphorus 30.2 J 10.0 ug SW846 6020 

Dilution Factor: 1 

Antimony ND 0.40 ug SW846 6020 

Dilution Factor: 1 

Selenium 19.8 0.40 ug SW846 6020 

Dilution Factor: 1 

Thallium NO 0.20 ug SW846 6020 

Dilution Factor: 1 

Zinc 1.8 1.0 ug SW846 6020 

Dilution Factor: 1 

NOTE s : 

G Elevated reporting limit. The reporting limit i'l) elevated due to matrix interference. 

B Estimated resul!. Resul! is less than Rl.. 

J Method blank contamination. The as.,ociated method blank contains the target analyte at a reportable level. 

G7E230399 STL Sacramento (916) 373 - 5600 

Matrix ••••.•••• : AIR 

PREPARATION- WORK 

ANALYSIS DATE ORDER # 

05/31-06/15/07 JXKXF1AP 

05/31-06/15/07 JXKXF1AQ 

05/31-06/15/07 JXKXFlAR 

05/31-06/15/07 JXKXFlAT 

05/31-06/15/07 JXKXFlAU 

05/31-06/15/07 JXKXF1AV 

05/31-06/15/07 JXKXFlAW 

05/31-06/15/07 JXKXF1AX 

45 of678 
AIR 

POLLUTION 

TESTING, INC. 

Appendix Four: Calibration Data 
AIR POLLUTION TESTING, INC. 

THERMOCOUPLE AND DRY GAS METER CALIBRATION DATA 

GAS METER ID : 

DATE: 

BARO. PRESS. 

Run #1 Run #2 

Yref 0.9990 0.9990 

Yd 0.988 0.987 

DH@ 1.73 1.69 

THERMOCOUPLE CALIBRATION 

Calibration Pyrometer 

Temperature Reading Reading 

PITOT LEAK CHECK 

Run #3 

0.9990 

0.949 

1.62 

ABS (Relative Difference) 

%R 

Average 

0.999 

0.974 

1.68 
AIR POLLUTION TESTING, INC. 

THERMOCOUPLE AND DRY GAS METER CALIBRATION DATA 

GAS METER ID: 

DATE: 

BARO. PRESS. 

Run #1 Run#2 Run #3 Average 

Yref 0.9990 0.9990 0.9990 0.999 

Yd 0.985 0.980 0.983 0.983 

DH@ 1.55 1.64 1.66 1.62 

THERMOCOUPLE CALIBRATION 

Calibration Pyrometer ABS (Relative Difference) 

Temperature Reading Reading (F) % R 

PITOT LEAK CHECK SLC Reference Meter - March 2006 

-

Technician:-
Quality Source Sampling Systems & Accessories 

Wind Tunnel Pitot Calibration 

Customer: Air Pollution Testing 

S-type Pitot ID: P-416 Date: 10-lun-04 

Standard Pitot ID: 001 Personnel: DH 

Cp(std): 0.99 Cp(actual): 1,...--~o--=.8~3---, 

Part Number: pps12-y-7 .s P(bar): 29.62 

Test Velocity (fps): 50 T(°F): 78.00 

UJ 

0 

1--4 

(f) 

I 

<( 

UJ 

0 

1--4 

(f) 

I 

c:o 

L1P<stct) ["H20] 

0.535 

0.533 

0.536 

0.535 

L1P(stct) ["H20] 

0.533 

0.535 

0.537 

0.538 

L1P(s) ["H20] Cp(s) Deviation* 

0.744 0.840 0.001 

0.745 0.837 -0.001 

0.745 0.839 0.001 

0.745 0.839 0.000 

AVERAGE 0.839 0.001 

Std deviation 0.001 

L1P(s) ["H20] CP(s) Deviation* 

0.757 0.831 0.001 

0.764 0.828 -0.002 

0.766 0.829 -0.001 

0.762 0.832 0.002 

AVERAGE 0.830 0.001 

Std deviation 0.002 

Cp(A) - Cp(B) =I 0.009 

{must be <0.010} 

*Deviation= I{Cp(s)- AVGCp(s)}l 

{must be <0.010} 

Standard deviation of the deviations must be less than 0.02 for both sides. 

Pitot tube S/N P-416 was calibrated in accordance with 

e of Federal Regulations, Title 40, Part 60, Appendix A, Method 2, Section 10 

Signature 

2142 E. Geer Street, Durham, North Carolina 27704 800-STACKS-5 (782-2575) 919-956-9688 FAX: 919-682-0333 
Quality Source Sampling Systems & Accessories 

Wind Tunnel Pitot Calibration 

Customer: Air Pollution Testing 

S-type Pi tot ID: P-444 Date: 17-Jan-05 

Standard Pitot ID: 001 Personnel: DH 

Cp(std): 0.99 Cp(actual): .--1 -....,....0......,..8....,.3----. 

Part Number: pps12-y-7 .s P(bar): 30.10 

Test Velocity (fps): 50 T(°F): 35.00 

w 

0 

~ 

(/) 

I 

<( 

w 

0 

~ 

(/) 

I 

en 

~Pcstd) ["H20] 

0.591 

0.590 

0.586 

0.580 

~Pcstd) ["H20] 

0.591 

0.590 

0.587 

0.592 

~Pes) ["H20] CPcs) Deviation* 

0.840 0.830 0.003 

0.841 0.829 0.002 

0.834 0.829 0.002 

0.842 0.822 -0.006 

AVERAGE 0.828 0.003 

Std deviation 0.004 

~Pes) ["H20] CPcs) Deviation* 

0.839 0.831 0.000 

0.836 0.832 0.001 

0.838 0.829 -0.002 

0.837 0.832 0.001 

AVERAGE 0.831 0.001 

Std deviation 0.002 

Cp(A) - Cp(B) = 1....___0_.0_0_3 ______, 

{must be <0.010} 

*Deviation= I{Cp(s)- AVGCp(s)}l 

{must be <0.010} 

Standard deviation of the deviations must be less than 0.02 for both sides. 

Pitot tube S/N P-444 was calibrated in accordance with 

of Federal Regulations, Title 40, Part 60, Appendix A, Method 2, Section 10 

j-IJ-Of) 

Signature Date 

2142 E. Geer Street, Durham, North Carolina 27704 800-STACKS-5 (782-2575) 919-956-9688 FAX: 919-682-0333 
AIR 

POLLUTION 

TESTING, INC. 

Appendix Five: Schen1atics 
heated filter box HNO/H202 

solution 

~ tc= thermocouple ~ 

EPA Method 29 

sampling train schematic 

chilled impinger ) 

train ,