SW-846 Update VSTATUS TABLE - 1 Revision July 2014**STATUS TABLES FOR SW-846, THIRD EDITION** **FINAL UPDATES I, II, IIA, IIB, III, IIIA, IIIB, IV AND UPDATE V** **PLUS OTHER NEW AND REVISED SW-846 METHODS AT THE ORCR METHODS WEB SITE** **REVISED July 2014**SW-846 Update VSTATUS TABLE - 2 Revision July 2014HOW TO USE THIS DOCUMENT**This document provides historical information regar ding EPA-published SW-846 methods and chapters. I** **t contains two status tables, namely; the "SW-846 Method Status Table," which is** **a listing of SW-846 methods; and the "Status Table for SW-846 Chapter Text and Other** **Documents," which lists all other documents in SW-8 46 (e.g., chapters).** **Use the "SW-846 Method Status Table" as a reference guide to identify the historical and latest versio** **ns of SW-846 methods. Methods in this status table are listed sequentially by method numb** **er. The column showing "Other Methods" includes th ose new and revised validated methods** **which have not been incorporated into SW-846 method s compendium. Those methods appear at EPA's Office** **of Resource Conservation and Recovery Methods Team internet site,** **http://www.epa.gov/SW-846/ . An integrated version of the manual through Fina** **l Update IV is also available at the Methods Team internet site.** **Methods that have "deleted" as the latest status ar e those methods that have been removed from SW-846** **for various reasons, and you will not find that method at the Methods Team web site. See** **the associated update rulemakings or notices for a n explanation regarding why a method was** **deleted from SW-846. Use the "Status Table for SW-846 Chapter Text and O** **ther Documents" as a reference guide to identify th e historical and latest versions of** **chapters and other SW-846 documents (e.g., the Disc laimer).** **With the publication of the Final Methods Innovatio n Rule, SW-846 and most of the methods contained th** **erein are no longer required in general by any RCRA regulation. See 40 CFR 260.11(** **a) (11) for a listing of those SW-846 methods that may be still required by the RCRA** **regulations for the analysis of method-defined para meters.** **Do**not**use a status table as a guide for putting together a paper version of SW-846. Refer to the "Table of** **Contents" of the update for the order in which chapters and methods should appear i** **n SW-846.**SW-846 Update VSTATUS TABLE - 3 Revision July 2014SW-846 METHOD STATUS TABLEMETHOD NUMBERMETHOD TITLE(Date in parenthesis is found at bottom right-handcorner of method).THIRDED(9/86)FIN. UP.I(7/92)FIN. UP.II (9/94)IIA (8/93)IIB (1/95)FIN. UP.III (12/96)IIIA (4/98)IIIB (11/04)FIN. UP.IV(2/07)OTHERMETHODS(VARIOUSDATES)UPDATEV**0010 -- -- -- -- -- -- Modified Method 5 Sampling T rain** **-- -- -- 0011** **(Up. III) -- -- --** **Sampling for Selected Aldehyde and Ketone Emissions from** **Stationary Sources 0020 -- -- -- -- -- -- Source Assessment Sampling S** **ystem (SASS) -- -- --** **0023A (Up. III)** **-- -- -- Sampling Method for Polychlorinated Dibenzo-p-Dioxi** **ns and Polychlorinated Dibenzofuran Emissions from Station** **ary Sources (Note: This method is a revision of Method 23, 40** **CFR Part 60.) -- -- -- --** **25D Referral** **-- -- Determination of the Volatile Organic Concentration** **of Waste Samples** **-- -- -- -- 25E** **Referral -- --** **Determination of Vapor Phase Organic Concentration in Waste** **Samples 0030 -- -- -- -- -- -- Volatile Organic Sampling Tr** **ain -- -- --** **0031 (Up. III)** **-- -- -- Sampling Method for Volatile Organic Compo unds (SMVOC)** **-- -- -- 0040** **(Up. III) -- -- --** **Sampling of Principal Organic Hazardous Constituent s from** **Combustion Sources Using Tedlar® Bags -- -- --** **0050 (Up. III)** **-- -- -- Isokinetic HCl/Cl2 Emission Sampling Train -- -- --** **0051 (Up. III)** **-- -- -- Midget Impinger HCl/Cl2 Emission Sampling Train** SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 4 Revision July 2014**-- -- -- 0060** **(Up. III) -- -- -- Determination of Metals in Stack Emissions** **-- -- -- 0061** **(Up. III) -- -- --** **Determination of Hexavalent Chromium Emissions from Stationary** **Sources -- -- --** **0100 (Up. III)** **-- -- -- Sampling for Formaldehyde and Other Carbonyl Compou** **nds in Indoor Air** **-- -- -- -- 207** **Referral -- -- A Method for Measuring Isocyanates in Station** **ary Source Emissions 1010 -- --** **1010A (Up. IIIB)** **-- -- -- Test Methods for Flash Point by Pensky-Martens Clos** **ed Cup Tester (Method text is a referral to ASTM Standard D 93-79** **or Standard D 93-80)** **1020 1020A -- 1020B** **(Up. IIIB) -- -- --** **Standard Test Methods for Flash Point by Setaflash (Small Scale)** **Closed-cup Apparatus (Method text is a referral to ASTM Standard D** **3278-78) -- -- --** **1030 (Up. III)** **-- -- 1030** **(07/14) Ignitability of Solids** **-- -- -- -- 1040 -- -- Test Method for Oxidizing So lids** **-- -- -- -- 1050 -- -- Test Methods to Determine Substances Likely to Spon** **taneously Combust** **1110 -- -- 1110A** **(Up. IIIB) -- -- -- Corrosivity Toward Steel** **-- -- 1120** **(Up. III) -- -- -- Dermal Corrosion** **1310 1310A -- 1310B** **(Up. IIIB) -- -- --** **Extraction Procedure (EP) Toxicity Test Method and Structural** **Integrity Test -- 1311 -- -- -- -- -- Toxicity Characteristic Leac** **hing Procedure -- -- 1312 -- -- -- -- Synthetic Precipitation Leac** **hing Procedure 1320 -- -- -- -- -- -- Multiple Extraction Procedur** **e 1330 1330A -- -- -- -- -- Extraction Procedure for** **Oily Wastes 3005 3005A -- -- -- -- --** **Acid Digestion of Waters for Total Recoverable or D issolved Metals** **for Analysis by FLAA or ICP Spectroscopy**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 5 Revision July 2014**3010 3010A -- -- -- -- -- Acid Digestion of Aqueous Samples and Extracts for** **Total Metals for Analysis by FLAA or ICP Spectroscopy** **-- -- 3015** **(Up. II) -- 3015A -- -- Microwave Assisted Acid Digestion of** **Aqueous Samples and Extracts 3020 3020A -- -- -- -- --** **Acid Digestion of Aqueous Samples and Extracts for Total Metals for** **Analysis by GFAA Spectroscopy -- -- --** **3031 (Up. III)** **-- -- -- Acid Digestion of Oils for Metals Analysis by Atomi** **c Absorption or ICP Spectrometry** **3040 -- -- 3040A** **(Up. III) -- -- -- Dissolution Procedure for Oils, Greases, o** **r Waxes 3050 3050A --** **3050B (Up. III)** **-- -- -- Acid Digestion of Sediments, Sludges, and Soils** **-- -- 3051** **(Up.II) -- 3051A -- --** **Microwave Assisted Acid Digestion of Sediments, Slu dges, Soils, and** **Oils -- -- --** **3052 (Up. III)** **-- -- -- Microwave Assisted Acid Digestion of Siliceous and** **Organically Based Matrices** **-- -- -- 3060A** **(Up. III) -- -- -- Alkaline Digestion for Hexavalent Chromium** **-- -- -- -- -- 3200** **(7/05) 3200** **(07/14) Mercury Species Fractionation and Quantification by** **Microwave Assisted Extraction, Selective Solvent Extraction a** **nd/or Solid Phase Extraction** **3500 3500A -- 3500B** **(Up. III) 3500C -- -- Organic Extraction and Sample Preparati** **on 3510 3510A** **3510B (Up. II)** **3510C (Up. III)** **-- -- -- Separatory Funnel Liquid-Liquid Extraction -- -- -- -- --** **3511 (11/02)** **3511 (07/14)** **Organic Compounds in Water by Microextraction 3520 3520A** **3520B (Up. II)** **3520C (Up. III)** **-- -- -- Continuous Liquid-Liquid Extraction -- -- --** **3535 (Up. III)** **3535A -- -- Solid-Phase Extraction (SPE) 3540 3540A** **3540B (Up. III)** **3540C (Up. III)** **-- -- -- Soxhlet Extraction -- --** **3541 (Up. II)** **-- -- -- -- Automated Soxhlet Extraction**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 6 Revision July 2014**-- -- -- 3542** **(Up. III) --** **3542A (5/05)** **-- Extraction of Semivolatile Analytes Collected Using** **Method 0010 (Modified Method 5 Sampling Train)** **-- -- -- 3545** **(Up. III) 3545A -- -- Pressurized Fluid Extraction (PFE)** **-- -- -- -- 3546 -- -- Microwave Extraction -- --** **3550A (Up. II)** **3550B (Up. III)** **3550C -- Ultrasonic Extraction** **-- -- -- 3560** **(Up. III) -- -- --** **Supercritical Fluid Extraction of Total Recoverable Petroleum** **Hydrocarbons -- -- --** **3561 (Up. III)** **-- -- -- Supercritical Fluid Extraction of Polynucl ear Aromatic Hydrocarbons** **-- -- -- -- 3562 -- -- Supercritical Fluid Extraction of Polychlorinated B** **iphenyls (PCBs) and Organochlorine Pesticides** **-- -- -- -- -- 3572** **(7/07) 3572** **(07/14) Extraction of Wipe Samples for Chemical Agents** **3580 3580A -- -- -- -- -- Waste Dilution -- -- --** **3585 (Up. III)** **-- -- -- Waste Dilution for Volatile Organics 3600 3600A** **3600B (Up. II)** **3600C (Up. III)** **-- -- -- Cleanup 3610 3610A --** **3610B (Up. III)** **-- -- -- Alumina Cleanup 3611 3611A --** **3611B (Up. III)** **-- -- -- Alumina Column Cleanup and Separation of P etroleum Wastes** **3620 3620A -- 3620B** **(Up. III) 3620C --** **3620C (07/14)** **Florisil Cleanup 3630 3630A** **3630B (Up. II)** **3630B (Up. III)** **-- -- -- Silica Gel Cleanup 3640 --** **3640A (Up. II)** **-- -- -- -- Gel-Permeation Cleanup 3650 3650 --** **3650B (Up. III)** **-- -- -- Acid-Base Partition Cleanup 3660 3660A --** **3660B (Up. III)** **-- -- -- Sulfur Cleanup**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 7 Revision July 2014**-- -- 3665** **(Up. II) 3665A** **(Up. III) -- -- -- Sulfuric Acid/Permanganate Cleanup** **-- -- -- -- 3815 -- -- Screening Solid Samples for Volatile Organics** **3820 -- -- -- -- -- -- Hexadecane Extraction and Sc reening of Purgeable Organics** **-- -- -- 4000** **(Up. III) -- -- -- Immunoassay** **-- -- 4010** **(Up. IIA) 4010A** **(Up. III) -- -- -- Screening for Pentachlorophenol by Immunoa** **ssay -- -- --** **4015 (Up. III)** **-- -- -- Screening for 2,4-Dichlorophenoxyacetic Ac id by Immunoassay** **-- -- -- 4020** **(Up. III) -- -- -- Screening for Polychlorinated Biphenyls by** **Immunoassay -- -- -- -- --** **4025 (10/02)** **4025 (07/14)** **Screening for Polychlorinated Dibenzodioxins and Po lychlorinated** **Dibenzofurans (PCDD/Fs) by Immunoassay -- -- --** **4030 (Up. III)** **-- -- -- Soil Screening for Petroleum Hydrocarbons by Immunoassay** **-- -- -- 4035** **(Up. III) -- -- --** **Soil Screening for Polynuclear Aromatic Hydrocarbon s by** **Immunoassay -- -- --** **4040 (Up. III)** **-- -- -- Soil Screening for Toxaphene by Immunoassa y** **-- -- -- 4041** **(Up. III) -- -- -- Soil Screening for Chlordane by Immunoassa** **y -- -- --** **4042 (Up. III)** **-- -- -- Soil Screening for DDT by Immunoassay -- -- --** **4050 (Up. III)** **-- -- -- TNT Explosives in Soil by Immunoassay -- -- --** **4051 (Up. III)** **-- -- -- Hexahydro-1,3,5-trinitro-1,3,5-triazine (R DX) in Soil by Immunoassay** **-- -- -- -- 4425 -- -- Screening Extracts of Environmental Samples for Pla** **nar Organic Compounds (PAHs, PCBs, PCDDs/PCDFs) by a Reporter G** **ene on a Human Cell Line** **-- -- -- -- -- 4430** **(12/07) 4430** **(07/14) Screening For Polychlorinated Dibenzo-p-Dioxins And** **Furans (PCDD/Fs) By Aryl Hydrocarbon-Receptor PCR Assay** SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 8 Revision July 2014**-- -- -- -- -- 4435** **(2/08) 4435** **(07/14) Method for Toxic Equivalents (TEQs) Determinations** **for Dioxin-like Chemical Activity with Calux® Bioassay** **-- -- -- -- 4670 -- -- Triazine Herbicides as Atrazine in Water by Quantit** **ative Immunoassay** **-- -- -- 5000** **(Up. III) -- -- -- Sample Preparation for Volatile Organic Co** **mpounds -- -- --** **5021 (Up. III)** **-- 5021A** **(6/03) 5021A** **(07/14) 5021: Volatile Organic Compounds in Soils and Othe** **r Solid Sample Matrices Using Equilibrium Headspace Analysis** **-- -- -- -- -- 5021A: Volatile Organic Compounds in Various Sampl** **e Matrices Using Equilibrium Headspace Analysis** **-- -- -- 5030B** **(Up. III) --** **5030C (5/03)** **-- Purge-and-Trap for Aqueous Samples -- -- --** **5031 (Up. III)** **-- -- -- Volatile, Nonpurgeable, Water-Soluble Compounds by** **Azeotropic Distillation** **-- -- -- 5032** **(Up. III) -- -- -- Volatile Organic Compounds by Vacuum Disti** **llation -- -- --** **5035 (Up. III)** **-- 5035A** **(7/02) --** **Closed-System Purge-and-Trap and Extraction for Vol atile Organics** **in Soil and Waste Samples -- --** **5041 (Up. II)** **5041A (Up. III)** **-- -- -- Analysis for Desorption of Sorbent Cartridges from** **Volatile Organic Sampling Train (VOST)** **-- -- 5050** **(Up. II) -- -- -- -- Bomb Preparation Method for Solid Waste** **6010 6010A -- 6010B** **(Up. III) 6010C --** **6010D (07/14)** **Inductively Coupled Plasma-Atomic Emission Spectrom etry** **-- -- 6020** **(Up. II) -- 6020A --** **6020B (07/14)** **Inductively Coupled Plasma-Mass Spectrometry -- -- -- -- 6200 -- --** **Field Portable X-Ray Fluorescence Spectrometry for the** **Determination of Elemental Concentrations in Soil a nd Sediment** **-- -- -- -- 6500 -- -- Dissolved Inorganic Anions in Aqueous Matrices by C** **apillary Ion Electrophoresis** **-- -- -- -- 6800 -- 6800** **(07/14) Elemental and Speciated Isotope Dilution Mass Spect** **rometry 7000 7000A -- -- 7000B -- -- Flame Atomic Absorptio** **n Spectrophotometry -- -- -- -- 7010 -- -- Graphite Furnace Atomic Abso** **rption Spectrophotometry**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 9 Revision July 2014**7061 7061A -- -- -- -- -- Arsenic (Atomic Absorptio n, Gaseous Hydride)** **-- -- 7062** **(Up. II) -- -- -- -- Antimony and Arsenic (Atomic Absorption** **, Borohydride Reduction) -- -- --** **7063 (Up III)** **-- -- -- Arsenic in Aqueous Samples and Extracts by Anodic S** **tripping Voltammetry (ASV)** **7195 -- -- -- -- -- -- Chromium, Hexavalent (Coprec ipitation)** **7196 7196A -- -- -- -- -- Chromium, Hexavalent (Col orimetric)** **7197 -- -- -- -- -- -- Chromium, Hexavalent (Chelat ion/Extraction)** **7198 -- -- -- -- -- -- Chromium, Hexavalent (Differ ential Pulse Polarography)** **-- -- -- 7199** **(Up. III) -- -- --** **Determination of Hexavalent Chromium in Drinking Wa ter,** **Groundwater and Industrial Wastewater Effluents by Ion** **Chromatography 7470 -- 7470A -- -- -- --** **Mercury in Liquid Waste (Manual Cold-Vapor Techniqu e)** **7471 -- 7471A** **(Up II) -- 7471B -- --** **Mercury in Solid or Semisolid Waste (Manual Cold-Va por Technique)** **-- -- -- 7472** **(Up. III) -- -- --** **Mercury in Aqueous Samples and Extracts by Anodic S tripping** **Voltammetry (ASV) -- -- -- 7473 -- -- --** **Mercury in Solids and Solutions by Thermal Decompos ition,** **Amalgamation, and Atomic Absorption Spectrophotomet ry** **-- -- -- 7474 -- -- -- Mercury in Sediment and Tissue Samples by Atomic Fl** **uorescence Spectrometry** **-- -- 7580** **(Up. III) -- -- --** **White Phosphorus (P4) by Solvent Extraction and Gas Chromatography** **7741 -- 7741A** **(Up. II) -- -- -- --** **Selenium (Atomic Absorption, Gaseous Hydride) -- --** **7742 (Up. II)** **-- -- -- -- Selenium (Atomic Absorption, Borohydrid e Reduction)** **8000 8000A -- 8000B** **(Up III) --** **8000C (3/03)** **8000D (07/14)** **Determinative Chromatographic Separations -- 8011 -- -- -- -- --** **1,2-Dibromoethane and 1,2-Dibromo-3-chloropropane b y** **Microextraction and Gas Chromatography**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 10 Revision July 2014**8015 8015A -- 8015B 8015C -- -- 8015C: Nonhalogena ted Organics by Gas Chromatography** **-- -- -- -- -- 8015D** **(06/03) --** **8015D: Nonhalogenated Organics by Gas Chromatograp hy Using** **GC/FID -- 8021** **8021A (Up. II)** **8021B (Up. III)** **-- -- 8021B** **(07/14) Aromatic and Halogenated Volatiles by Gas Chromatog** **raphy Using Photoionization and/or Electrolytic Conductivity De** **tectors -- --** **8031 (Up. II)** **-- -- -- -- Acrylonitrile by Gas Chromatography -- --** **8032 (Up. II)** **8032A (Up. III)** **-- -- -- Acrylamide by Gas Chromatography -- -- --** **8033 (Up. III)** **-- -- -- Acetonitrile by Gas Chromatography with Nitrogen-Ph** **osphorus Detection** **-- -- -- 8041** **(Up. III) 8041A -- -- Phenols by Gas Chromatography** **-- -- 8061** **(Up. II) 8061A** **(Up. III) -- -- --** **Phthalate Esters by Gas Chromatography with Electro n Capture** **Detection (GC/ECD) -- 8070 --** **8070A (Up. III)** **-- -- -- Nitrosamines by Gas Chromatography -- --** **8081 (Up. II)** **8081A (Up. III)** **8081B -- -- Organochlorine Pesticides by Gas Chroma tography** **-- -- -- 8082** **(Up. III) 8082A -- -- Polychlorinated Biphenyls (PCBs) by Gas** **Chromatography -- -- -- -- 8085 -- --** **Compound-independent Elemental Quantitation of Pest icides by Gas** **Chromatography with Atomic Emission Detection (GC/A ED)** **-- -- -- 8091** **(Up. III) -- -- -- Nitroaromatics and Cyclic Ketones by Gas C** **hromatography -- -- -- -- 8095 -- -- Explosives by Gas Chromatogr** **aphy 8100 -- -- -- -- -- -- Polynuclear Aromatic Hydroca** **rbons -- -- --** **8111 (Up. III)** **-- -- 8111** **(07/14) Haloethers by Gas Chromatography** **-- -- 8121** **(Up. II) -- -- -- --** **Chlorinated Hydrocarbons by Gas Chromatography: Ca pillary** **Column Technique -- -- --** **8131 (Up. III)** **-- -- -- Aniline and Selected Derivatives by Gas Ch romatography** SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 11 Revision July 2014**8140 -- -- Deleted** **(Up. III) -- -- -- Organophosphorus Pesticides** **-- 8141 8141** **(Up. II) -- 8141B -- -- Organophosphorus Compounds by Gas Ch** **romatography -- --** **8151 (Up. II)** **8151A (Up. III)** **-- -- -- Chlorinated Herbicides by GC Using Methylation or** **Pentafluorobenzylation Derivatization -- -- --** **8260B (12/96)** **-- -- -- Volatile Organic Compounds by Gas Chromatography/ M** **ass Spectrometry (GC/MS)** **-- -- -- -- 8261 8261A** **(10/06) --** **Volatile Organic Compounds by Vacuum Distillation i n Combination** **with Gas Chromatography/Mass Spectrometry (VD/GC/MS )** **8270 8270A 8270B** **(Up. II) 8270C** **(Up. III) 8270D --** **8270D (07/14)** **Semivolatile Organic Compounds by Gas Chromatograph y/Mass** **Spectrometry (GC/MS) -- --** **8275 (Up. II)** **8275A (Up. III)** **-- -- -- Semivolatile Organic Compounds (PAHs and PCBs) in S** **oils/Sludges and Solid Wastes Using Thermal Extraction/Gas** **Chromatography/Mass Spectrometry (TE/GC/MS) -- -- -- -- -- --** **8276 (07/14)** **Toxaphene and Toxaphene Congeners by Gas Chromatography/Negative Ion Chemical Ionization Mas** **s Spectrometry (GC-NICI/MS)** **8280 -- -- 8280A** **(Up. III) 8280B -- --** **Polychlorinated Dibenzo-p-Dioxins (PCDDs) and Polyc hlorinated** **Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HR** **GC/LRMS) -- --** **8290 (Up. II)** **-- 8290A -- -- Polychlorinated Dibenzo-p-dioxins (PCDDs) and Polyc** **hlorinated Dibenzofurans (PCDFs) by High-Resolution Gas** **Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS)** **8310 -- -- -- -- -- -- Polynuclear Aromatic Hydroca rbons** **-- -- 8315** **(Up. II) 8315A** **(Up. III) -- -- --** **Determination of Carbonyl Compounds by High Perform ance Liquid** **Chromatography (HPLC) -- --** **8316 (Up. II)** **-- -- -- -- Acrylamide, Acrylonitrile and Acrolein by High Perf** **ormance Liquid Chromatography (HPLC)** **-- -- 8318** **(Up. II) -- 8318A -- --** **N-Methylcarbamates by High Performance Liquid Chrom atography** **(HPLC) -- --** **8321 (Up. II)** **8321A (Up. III)** **8321B -- -- Solvent-Extractable Nonvolatile Compounds by High-P** **erformance Liquid Chromatography/Thermospray/Mass Spectrometry** **(HPLC/TS/MS) or Ultraviolet (UV) Detection**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 12 Revision July 2014**-- -- -- 8325A** **(Up. III) -- -- --** **Solvent Extractable Nonvolatile Compounds by High P erformance** **Liquid Chromatography/Particle Beam/Mass Spectromet ry** **(HPLC/PB/MS) -- --** **8330 (Up. II)** **-- 8330A 8330B -- Nitroaromatics and Nitramines by High Performance L** **iquid Chromatography (HPLC)** **-- -- 8331** **(Up. II) -- -- -- --** **Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC)** **-- -- -- 8332** **(Up. III) -- -- -- Nitroglycerine by High Performance Liquid** **Chromatography -- --** **8410 (Up. II)** **-- -- -- 8410** **(07/14) Gas Chromatography/Fourier Transform Infrared (GC/F** **T-IR) Spectrometry for Semivolatile Organics: Capillary** **Column -- -- --** **8430 (Up. III)** **-- -- 8430** **(07/14) Analysis of Bis(2-chloroethyl) Ether and Hydrolysis** **Products by Direct Aqueous Injection GC/FT-IR** **-- -- -- 8440** **(Up. III) -- -- --** **Total Recoverable Petroleum Hydrocarbons by Infrare d** **Spectrophotometry -- -- -- -- 8510 -- -- Colorimetric Screening Proce** **dure for RDX and HMX in Soil -- -- --** **8515 (Up. III)** **-- -- -- Colorimetric Screening Method for Trinitro toluene (TNT) in Soil** **-- -- -- 8520** **(Up. III) -- -- -- Continuous Measurement of Formaldehyde in** **Ambient Air -- -- -- -- 8535 -- -- Screening Procedure for Tota** **l Volatile Organic Halides in Water -- -- -- -- 8540 -- -- Pentachlorophenol by UV-indu** **ced Colorimetry -- -- -- -- 9000 -- -- Determination of Water in Wa** **ste Materials by Karl Fischer Titration -- -- -- -- 9001 -- --** **Determination of Water in Waste Materials by Quanti tative Calcium** **Hydride Reaction 9010 9010A --** **9010B (Up. III)** **-- -- -- Total and Amenable Cyanide: Distillation** **-- -- -- 9010C** **(Up. IIIB) -- -- --** **9012 -- -- 9012A** **(Up. III) -- -- --** **Total and Amenable Cyanide (Automated Colorimetric, with Off-line** **Distillation) -- -- --** **9012B (Up. III)** **-- -- --**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 13 Revision July 2014**-- 9013 -- -- -- 9013A** **(11/04) 9013A** **(07/14) Cyanide Extraction Procedure for Solids and Oils** **-- -- -- 9014** **(Up. III) -- --** **9014 (07/14)** **Titrimetric and Manual Spectrophotometric Determina tive Methods** **for Cyanide -- -- -- -- --** **9015 (11/04)** **9015 (07/14)** **Metal Cyanide Complexes by Anion Exchange Chromatog raphy and** **UV Detection 9020 9020A** **9020B (Up. II)** **-- -- -- -- Total Organic Halides (TOX) -- 9021 -- -- -- -- -- Purgeable Organic Halides (P** **OX) 9022 -- -- -- -- -- -- Total Organic Halides (TOX)** **by Neutron Activation Analysis -- -- --** **9023 (Up. III)** **-- -- -- Extractable Organic Halides (EOX) in Solid s** **9030 9030A -- 9030B** **(Up. III) -- -- -- Acid-Soluble and Acid Insoluble Sulfides:** **Distillation -- 9031 -- -- -- -- -- Extractable Sulfides** **-- -- -- 9034** **(Up. III) -- -- -- Titrimetric Procedure for Acid-Soluble and** **Acid-Insoluble Sulfides 9035 -- -- -- -- -- -- Sulfate (Colormetric, Automa** **ted, Chloranilate) 9036 -- -- -- -- -- -- Sulfate (Colormetric, Automa** **ted, Methylthymol Blue, AAII) 9038 -- -- -- -- -- -- Sulfate (Turbidimetric)** **9040 -- 9040A** **(Up. II) 9040C** **(Up. IIIB) -- -- --** **pH Electrometric Measurement -- --** **9040B (Up. II)** **-- -- -- -- 9041 9041A -- -- -- -- -- pH Paper Method** **9045 9045A 9045B** **(Up. II) 9045D** **(Up. IIIB) -- -- --** **Soil and Waste pH -- --** **9045C (Up. II)** **-- -- -- --**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 14 Revision July 2014**9050 -- -- 9050A** **(Up. III) -- -- -- Specific Conductance** **-- -- 9056** **(Up. II) -- 9056A -- -- Determination of Inorganic Anions by** **Ion Chromatography -- -- --** **9057A (Up. III)** **-- -- -- Determonation of Chloride from HCl/CL2 Emission Sam** **pling Train (Methods 0050 and 0051) by Anion Chromatography** **-- -- -- 9060A** **(Up. IIIB) -- -- -- Total Organic Carbon** **9065 -- -- -- -- -- -- Phenolics (Spectrophotometri c, Manual 4-AAP with Distillation)** **9066 -- -- -- -- -- -- Phenolics (Colorimetric, Man ual 4-AAP with Distillation)** **9067 Phenolics (Spectrophotometric. MBTH with Distillation)** **9070 -- -- -- -- -- -- n-Hexane Extractable Materia l (HEM) for Aqueous Samples** **-- -- -- 9070A** **(Up. IIIB) -- -- --** **Note: Method text is a referral to Method 1664: n -Hexane** **Extractable Material (HEM; Oil and Grease) and Sili cia Gel Treated** **n-Hexane Extractable Material (SGT_HEM; Non-polar M aterial) by** **Extraction and Gravimetry) 9071 --** **9071A (Up. II)** **9071B (Up. IIIA)** **-- -- -- n-Hexane Extractable Material (HEM) for Sludge, Sed** **iment, and Solid Samples** **-- -- -- -- 9074 -- -- Turbidimetric Screening Method for Total Recoverabl** **e Petroleum Hydrocarbons in Soil** **-- -- 9075** **(Up. II) -- -- -- --** **Test Method for Total Chlorine in New and Used Petr oleum Products** **by X-Ray Fluorescence Spectrometry (XRF) -- --** **9076 (Up. II)** **-- -- -- -- Test Method for Total Chlorine in New and Used Petr** **oleum Products by Oxidative Combustion and Microcoulometry** **-- -- 9077** **(Up. II) -- -- -- --** **Test Method for Total Chlorine in New and Used Petr oleum Products** **(Field Test Kit Methods) -- -- --** **9078 (Up. III)** **-- -- -- Screening Test Method for Polychlorinated Biphenyls in Soil** **-- -- -- 9079** **(Up. III) -- -- --** **Screening Test Method for Polychlorinated Biphenyls in Transformer** **Oil 9080 -- -- -- -- -- -- Cation-Exchange Capacity of** **Soils (Ammonium Acetate)**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 15 Revision July 2014**9081 -- -- -- -- -- -- Cation-Exchange Capacity of Soils (Sodium Acetate)** **9090 9090A -- -- -- -- -- Compatibility Test for Wa stes and Membrane Liners** **9095 -- -- 9095A** **(Up. III) -- -- --** **Paint Filter Liquids Test -- -- --** **9095B (Up. IIIB)** **-- -- -- -- --** **9096 (Up. II)** **-- -- -- -- Liquid Release Test (LRT) Procedure 9100 -- -- -- -- -- --** **Saturated Hydraulic Conductivity, Saturated Leachat e Conductivity,** **and Intrinsic Permeability 9131 -- -- -- -- -- -- Total Coliform: Multiple Tu** **be Fermentation Technique 9132 -- -- -- -- -- -- Total Coliform: Membrane-Fi** **lter Technique -- -- --** **9210 (Up. III)** **9210A -- -- Potentiometric Determination of Nitrate in Aqueous** **Samples with an Ion-Selective Electrode** **-- -- -- 9211** **(Up. III) -- -- --** **Potentiometric Determination of Bromide in Aqueous Samples with** **Ion-Selective Electrode -- -- --** **9212 (Up. III)** **-- -- -- Potentiometric Determination of Chloride in Aqueous** **Samples with Ion-Selective Electrode** **-- -- -- 9213** **(Up. III) -- -- --** **Potentiometric Determination of Cyanide in Aqueous Samples and** **Distillates with Ion-Selective Electrode -- -- --** **9214 (Up. III)** **-- -- -- Potentiometric Determination of Fluoride in Aqueous** **Samples and Distillates with Ion-Selective Electrode** **-- -- -- 9215** **(Up. III) -- -- --** **Potentiometric Determination of Sulfide in Aqueous Samples and** **Distillates with Ion-Selective Electrode -- -- -- -- 9216 -- --** **Potentiometric Determination of Nitrite in Aqueous Samples and** **Distillates with Ion-Selective Electrode 9250 -- -- -- -- -- -- Chloride (Colorimetric, Auto** **mated Ferricyanide AAI) 9251 -- -- -- -- -- -- Chloride (Colorimetric, Auto** **mated Ferricyanide AAII) -- --** **9253 (Up. II)** **-- -- -- -- Chloride (Titrimetric, Silver Nitrate)**SW-846 METHOD STATUS TABLE (Cont.)SW-846 Update VSTATUS TABLE - 16 Revision July 2014**9310 -- -- -- -- -- -- Gross Alpha and Gross Beta 9315 -- -- -- -- -- -- Alpha-Emitting Radium Isotop** **es 9320 -- -- -- -- --** **9320 (07/14)** **Radium-228**