NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 1 of 38

**Enclosure 1 Information Collection Request for**  **S econdary Aluminum**  **Production National Emission Standards for Hazardous Air Pollutants (NESHAP)**  **Part A. F**  **acility Information** 1. Name and address of legal OWNER of the facility :

________________________________ ________________________________ ______________

________________________________ ________________________________ ______________

________________________________ ________________________________ ______________ 2. Name and address of legal OPERATOR of the facility , if different from the legal OWNER

________________________________ ________________________________ ______________

________________________________ ________________________________ ______________

________________________________ ________________________________ ______________ 3. Complete street address of facility (phys ical location): a. Address:

________________________________ ____________________________ b. City :

________________________________ ________________________________ c. State:

________________________________ _______________________________ d. Zip:

________________________________ ________________________________ _ e. County :

________________________________ ______________________________ 4. Provide mailing address of the facility if diff erent from phy sical location: a. Address:

________________________________ _____________________________ b. City :

________________________________ ________________________________ c. State:

________________________________ _______________________________ d. Zip:

________________________________ ________________________________ _ 5. Facility contact able to answer technical questions about the completed survey a. Name (First Name, Last Name):

________________________________ __________ b. Title:

________________________________ ________________________________ c. Telephone number: _______________

___ _________ ext.

____________________ d. Fax number:

________________________________ __________________________ e. E - mail:

________________________________ ______________________________ f. **If the facility is permanently closed or is**  **not subject to 40 CFR part 63**  **, subpart RRR, please complete this page, sign below and send this page certified mail to**  **the non -**  **CBI address listed on the**  **instr uction sheet by XXX,**  I certify that this facility i s permanentl y closed or is not subject to the National Emission Standards for Hazardous Air Pollutants for Secondary Aluminum Production as defined in 40 CFR part 63 , subpart RRR
. (Print Name) (Title) (Signature of Responsible Official) (Date) A Responsible Official can be the president, vice
- president, secretary, or treasurer of the company that owns the facility, owner of the facility, plant manager, plant engineer or supervisor
.NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 2 of 38 6. What is the facility size classification for hazardous air pollutant (HAP) emissions ? ( C HECK one) EPA Major Source of Hazardous Air Pollutants (HAP) : **** EPA Area source (based on potential to emit) of HAP **** EPA Area source (Sy

nthetic Minor) of HAP **** 7. Facility NAICS codes Note : The primary NAICS code represents the line of business that generates the most income for the facility a. Primary

NAICS code

________________________________ ___________________ b. Other facility

NAI CS codes: ____________ __, ______________,

________________ 8. Company Size

– (CHECK one ) Note: Approximate average number of all employees (worldwide) of the business enterprise that owns this facility , including where applicabl e, the parent company and all subsidiaries, branches, and unrelated establishments owned by the parent company : If your company has a primary

NAICS code that does not begin with “ **331** --- ,” please also in clude your average annual sales receipt s $___________ (How to calculate average annual receipts and average emplo ym ent of a firm can be found in 13 C FR § 121.104 and 13 CFR § 121.1 0 6 , respectivel y).

___ ≤ 50 ___ 5 1 - 100 ___ 10 1 - 500 ___ 50 1 - 750 ___ 75 1 - 1000 ___ >1000 9. Facility Size

– (CHECK one) Note : Approximate average number of all employees at facility in location identified in question #3 above .
___ ≤ 50 ___ 5 1 - 100 ___ 10 1 - 500 ___ 50 1 - 750 ___ 75 1 - 1000 ___ >1000 10. Is the legal owner a small entity as defined b y the Regulatory Flexibility Act? ( CHECK one) ___ Yes___ No Note : For private businesses, small entity is defined for each NAI CS of the owning entity based on number of employees and/or company revenue. The NAICS codes used for Secondary Aluminum production are 331312, 331314, 331315, 331316, 331319, 331521, 331524 and various codes used for operations with Sweat Furnaces. The smallNESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 3 of 38 business size standards for NAICS subsectors are located at the following link: http://www.sba.gov/contractingopportunities/officials/size/table/index.html 11. Federal and State rule/permit coverage. ( CHECK all that app ly to this facility)
. ___ Subpart RRR (Secondary Aluminum) ____ Diecasting Operations ____ Foundry ____ Extruder ___ Subpart LL ( Primary Aluminum) _________________________________ Other (SPECIFY rule name and subpart) _________________________________ Other (SPECIFY rule name and subpart) New Source Performance Standards (NSPS)

_________________________________ (SPECIFY rule name and subpart)

_________________________________ (SPECI FY rule name and subpart) Title V ______________________ (SPECIFY the basis for your Title V permit ) State Air Toxics:

_________________________________ (SPECIFY rule name and subpart)

_________________________________ (SPECIFY rule name and subpart ) Other MACT ( e.g. , Metal Coil Surface Coatings MACT) : ___________________________ Other MACT :

___________________________ (SPECIFY emission unit and rule)

_ ________________________________________ ________________________________ 12. Normal Facili ty

Production Hours: Hours/day :

___________________ Shifts/day : ___________________ Day s/week: _

____ _ ____________ Weeks/year: __________________ 13. Total amount of aluminum produced in 2009. If 2009 is not representative of normal operation s , please provide information for a representative year ( 2004 or later) and specify the ye ar.

_______________ Y ear

_______________ T ons of aluminum produced 14. Amount of total charge to the facility used to produce the amount of aluminum reported in question #13:

_______________ T ons of charge 15. Ap proximately

what percent age of the facility ’s total charge (in #14 above) is considered clean charge?

_______________ Percent (%)NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 4 of 38 16. Please provide a cop y of a schematic of the plant layout for equipment subject to subpart RRR , control devices , and discharge stacks associated with these units
. Label the schematic with the unit IDs , control device IDs, and stack IDs , which should also match the unit IDs , control device IDs, and stack IDs used to respond to later questions. Please properl y identify units that are permanently “out of service” or not yet installed. 17. Please provide all of the pertinent information listed below. Please provide electronic copies , if available , and indicate items provided below
. (CHECK all that apply

): □ Title V permit □ State Air Operating permit □ Pending air permit applications (except for state and Title V renewal applications) □ Performance t est reports **( submit most recent test reports**  **for each subpart RRR**  **related process**

**)** . This includes any

tes t data on air emission sources , e.g. HF testing, bag house dust anal ys es , etc., not previousl y submitted to our office under a section 114 request. □ Emission inventory

reports **( reporting year** 

**s should be the same as**  **the years selected for this survey** 

**)** □ Most recent Consent decree or ord er for air related issues □ Notice(s) of air operating permit violations for the past 3 years □ S tartup, shutdown, and malfunction (SSM) p lan □ O perating , maintenance , and monitoring plan (OM&M)NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 5 of 38 **P art B.**  **Facility Equipment Regulated under Subpart RRR ( Secondary Aluminum NESHAP)**  1 Please provide the information below for all equipment at your facility: 18. Regulated Equipment List
**Unit Identification**  **Numbers (Unit ID No.)**  **Unit ID No.**

**as D**  **esignated in Title V or**  **State Operating**  **Permit*** **Subpart RRR**

**Equi pment**  **Do Y**  **ou**

**H ave**  **T his**  **E quipment**  **at the**  **Facility? (Y or N)**  **Add -**  **on**

**Controls (Y or N)**  **Operating in**

**2009? (Y or N)**  **If “No ,**  **” list last year of**  **operation** Aluminum Scrap Shredder Thermal Chip Dryer Scrap D ryer/D elacquering/ D ecoating Kiln Group 1 Furnace Clean charge onl y** Group 1 Furnace Handling other than clean charge** Group 2 Furnace** In - line Fluxer Dross - only

Furnace Rotary Dross Cooler Sweat Furnace * Please complete this column if ID numbers used in this form are different from those in the permit
. ** Please indicate which of the Group 1 or Group 2 furnaces listed above that have side well s or scrap wells
.

1 See “Definitions” in Attachment 1 at the end of this survey for explanation of these terms. For the purposes of this survey, scrap wells and wells of similar function as the side well shall be considered a sidewell.NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 6 of 38 **Part C. Charge Rates and Controls Used for Major**  **Sources Subpart RRR MACT** Please p rovide the information below for all regulated equipment at your facility; Use information for this section from whichever year (2004 or later) is representative of the highest emissions per ton of production
.
_________ (please specify year ) For purposes of this section, “Maximum Capacity” of a unit is defined as the unit ’ s potential to process charge or produce aluminum at its maximum rate on mass/time basis. If your permit limits the throughput or output of the unit, then that permitted amount may be us ed to calculate the maximum capacity
. 19. For Each Scrap Shredder

**Unit ID No.**  **Am ount of** 

**Charge (tons/y**  **r) Maximum** 

**Capacity of Unit**  **(tons /yr)**  **Charge R**  **ate**

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device**

**Type Device** 

**ID No.**

20. For Each Thermal Chip Dryer
**Unit ID No.**  **A mount of** 

**Chips Charged**  **(tons/y r)**  **Maximum**

**Capacity of Unit**  **(tons chips**  **/yr) Charge**  **R ate** 

**During Most Recent**  **Performance Test (lbs/hr)** * **Control Device**

**Type Device** 

**ID No.**

* If more than one performance test was conducted to demonstrate operation with different types of charge, please enter the maximum charge rate. If a test on a representative unit was conducted to demonstrate compliance for similar u nits, please enter the charge rate during the test used to demonstrate compliance for untested units.NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 7 of 38 21. For Each Scrap Dryer/Delacquering Kiln/Decoating Kiln

**Unit ID No.**  **Am ount of** 

**Charge (tons/y**  **r) Maximum** 

**Capacity of Unit**  **(tons /yr)**  **Charge R**  **ate**

**D ur**  **ing M**  **ost R** **ecent P**  **erformance T**  **est (lbs/hr)** * **Control Device** ******

**Type Device** 

**ID No.**

* *I f the kiln is equipped with an afterburner operated at a minimum of 760°C (1400 ° F) , with a design residence time of 1 second minimum, enter the control device ID Nos. here:

_______________ 22. For Each Dross Onl y Furnace

**Unit ID No.**  **Am ount of** 

**Dross Charged**  **(tons/y r)**  **Maximum**

**Capacity of Unit**  **(tons dross**  **/yr) Charge**  **R ate** 

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device**

**Type De** **vice**

**ID No.**

23. For Each Rotary

Dross Cooler

**Unit ID No.**  **Am ount of** 

**Dross Charged**  **(tons/y r)**  **Maximum**

**Capacity of Unit**  **(tons dross**  **/yr) Charge**  **R ate** 

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device**

**Type Device** 

**ID No.** 

* If more than one performance test was conducted to demonstrate operation with different types of charge, please enter the maximum charge rate. If a test on a representative unit was conducted to demonstrate compliance for similar units, please enter the charge rate during the test used to demonstrate compliance for untested units.NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 8 of 38 24 . For Each Group 1 Furnace

**Unit ID No.**  **Am ount of** 

**Charge (tons/yr)**  **Only Clean** 

**Charge (yes/no)**  **Maximum**

**Capacity of Unit**  **(tons/yr) Charge**  **R ate** 

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device**

**Type Device** 

**ID No.** 

25 . For Each Group 2 Furnace
**Unit ID No.**  **Am ount of** 

**Charge (tons/yr)**  **Maximum**

**Capacity of Unit**  **(tons /y**  **r) Charge**  **R ate**  **D uring** 

**M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device**

**Type Device ID** 

**No.**

26 . For Each In - line Fluxer

**Unit ID No.**  **Am ount**  **of Charge**  **(tons/yr) Maximum** 

**Capacity of Unit**  **(tons/yr) Maximum** 

**Number of T**  **imes the U**  **nit C**  **a n**  **R un in a**  **24 -**  **hr P**  **eriod Charge**  **R ate** 

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est (lbs/hr)** * **Control Device**

**Type Device** 

**ID No.** 

* If more than one performance test was conducted to demonstrate operation with diff erent types of charge, please enter the maximum charge rate. If a test on a representative unit was conducted to demonstrate compliance for similar units, please enter the charge rate during the test used to demonstrate compliance for untested units.NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 9 of 38 2 7 . For Each Sweat Furnac e
**Unit ID No.**  **Am ount of** 

**Charge (tons/yr)**  **Maximum**

**Capacity of Unit**  **(tons/y r)**  **Charge R**  **ate**

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device** ******

**Type Device ID** 

**No.**

* If more than one performance test was conducted to demonstrate operation with different types of charge, please enter the maximum charge rate. If a test on a representative unit was conducted to demonstrate compliance for similar units, please enter the charge rate during the test used to demonstrate compliance for untested units. * * If the sweat furnace is equipped with an afterburner operated at a minimum of 1600°F, with a design residence time of 0.8 second minimum, enter the control device ID here: ____________

_ 2 8 . For E ach Secondary Aluminum Processing Unit (SAPU) Using Emissions Averaging (as per section 63.1505(k) )
a. Complete this table if your facility chose to measure compliance using the **weight of the feed/charge**  .

**SAPU Unit**  **ID No. Unit Nos. from** 

**Qu estions #24**  **and #26 making up the**  **SAPU(s) SAPU Type?** 

**N=New E=Existing**  **Am ount of** 

**Feed/Charge (tons/year)**  **Percent Clean**

**Charge (approximate)** 
b. Complete this table if your facility chose to measure compliance using the **weight of the aluminum p**  **roduced**.

**SAPU Unit**  **ID No. Unit Nos. from** 

**Questions #24 and #26**  **making up the SAPU(s)**  **SAPU Type?**

**N=New E=Existing**  **Am ount of** 

**Aluminum Produced**  **(tons /year** **) Percent Clean** 

**Charge (approximate)** DRAFT 7/13/2010 Page 10 of 38

**Part D**  **. Charge Rates and Controls**  **Used for**  **Area Sou**  **rces Subpart RRR MACT** Please provide the information below for all regulated equipment at your facility; Use information for this section from 2004 or later, whichever year is representative of the highest emissions per ton of production
.
_________ (pleas e specify year ) For purposes of this section, “Maximum Capacity” of a unit is defined as the unit ’ s potential to process charge or produce aluminum at its maximum rate on mass/time basis. If your permit limits the throughput or output of the unit, then that permitted amount may be used to calculate the maximum capacity. 2 9 . For Each Thermal Chip Dryer **Unit ID No.**  **Am ount of Chips** 

**Charged (tons**  **/yr )**  **Maximum**

**Capacity of Unit (tons**  **/yr) Charge**  **R ate**  **D uring**  **M ost** 

**R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device Type**  **Device ID No.** 

* If more than one performance test was conducted to demonstrate operation with different types of charge, please enter the m aximum charge rate. If a test on a representative unit was co nducted to demonstrate compliance for similar units, please enter the charge rate during the test used to demonstrate compliance for untested units.DRAFT 7/13/2010 Page 11 of 38

30 . For Each Scrap Dryer/Delacquering Kiln/Decoating Kiln **Unit ID**  **No. Am**  **ount of Charge** 

**(tons/y r)**  **Maxi mu**  **m**

**Capacity of Unit (tons/yr)**  **Charge R**  **ate D**  **uring M**  **ost**

**R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device** ****** **Type Device**  **ID No.**

* *If the kiln is equipped with an afterburner operated at a minimum of 760°C (140 0° F) , with a design residence time of 1 second minimum, enter the control device ID Nos. here: ________________ 31. For E ach Group 1 Furnace
**Unit ID No.**  **Am ount of** 

**Charge (tons/yr)**  **Only Clean** 

**Charge (yes/no)**  **Maximum**

**Capacity of Unit (tons**  **/y r)**  **Charge R**  **ate D**  **uring**

**M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device Type**  **Device ID No.** 

* If more than one performance test was conducted to demonstrate operation with different types of charge, please enter the maximum charge rate. If a test on a representative unit was conducted to demonstrate compliance for similar units, please enter the charge rate during the test used to demonstrate compliance for untested units.DRAFT 7/13/2010 Page 12 of 38

32 . For Each Sweat Furnace **Unit ID No.**  **Am ount of Charge** 

**(tons/yr) Maximum Capacity of**  **Unit (tons**  **/y r)**  **Charge R**  **ate D**  **uring M**  **ost**

**R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device** ****** **Type Device ID** 

* * If the sweat furnace is equipped with an afterburner operated at a minimum of 1600°F, with a design residence time of 0.8 second minimum, enter the control device ID here: _____________ 33 . For Each In - line Fluxer

**Unit ID N**  **o. Am**  **ount of**

**Charge (tons/yr)**  **Maximum**

**Capacity of Unit (tons/yr)**  **Maximum N**  **um ber** 

**of T**  **imes the**  **U nit**  **C an**  **R un in a 24**  **- hr**  **P eriod**  **Charge R**  **ate**

**D uring**  **M ost**  **R ecent**  **P erformance**  **T est**  **(lbs/hr)*** **Control Device**

**Type Device ID**  **No.**

* If more than one performance test was conducted to demonstrate operation with different types of charge, please enter the maximum charge rate. If a test on a representative unit was conducted to demonstrate compliance for similar units, please enter the charge rate during the test used to demonstrate compliance for untested units.DRAFT 7/13/2010 Page 13 of 38

3 4 . E ach Secondary

Aluminum Processing Unit (SAPU) Using Emissions Averaging (as per section 63.1505(k)) a. Complete this table if your facility chose to measure compliance using the **weight of the feed/charge** .

**SAPU Unit**  **ID No. Unit**  **ID Nos.** 

**from Questions #31 a**  **nd #33 making up the**  **SAPU(s) SAPU Type?** 

**N=New E=Existing**  **Am ount of** 

**Feed/ Charge**  **(tons/year) Percent Clean** 

**Charge (approximate)** 
b. Complete this table if your facility chose to measure compliance using the **weight of the aluminum produced**.

**SAP U**  **Unit ID No.**  **Unit ID**  **Nos.**

**from Questions #31 and #33**  **making up the SAPU(s)**  **SAPU Type?**

**N=New E=Existing**  **Am ount of** 

**Aluminum Produced**  **(tons /year** **) Percent Clean** 

**Charge (approximate)** DRAFT 7/13/2010 Page 14 of 38

3 5 . Please complete this table for any **s crap shredder, group**  **2 furnace, in -** **line fluxer, dross -**  **only furnace, or rotary dross coole** **r** present at your facility .
**Unit ID No.**  **Type of**

**Equipment Maximum** 

**Capacity** ***** **(tons/year) What**  **T ype of** 

**C ontrol**  **D evice**  **, if A**  **ny is**  **U sed**  **? Height of** 

**S tack or**  **D ischarge**  **(ft) Discharge**  **Exit Gas Temperature**  **(degrees F) Latitude** ** **Longitude  ** Flow Rate (SCFM)** **Diam eter**  **(ft) Area**  **(sq. ft.) Maximum**  **Minim um** 

* For purposes of this section, “Maximum Capacity” of a unit is defined as the unit ’ s potential to process charge or produce aluminum at its maximum rate on mass/time basis. If your permit limits the throughput or output of the unit, then that permitted amount may be used to calculate the maximum capacity. ** Longitude and Latitude should be specified out to 6 decimal places. If coordinates are not known, please provide a scaled site diagram, with a latitude/longitude reference point, indicating stack locations.DRAFT 7/13/2010 Page 15 of 38

**Part E**  **. Em**  **issions and Limits for Subpart RRR Sources**  **and Non -**  **Subpart RRR Sources** Please provide the information below for all equipment at your facility; Use information for this section from 2004 or later, whichever year is representative of the highest emissions per ton of production
.
_________ (please specify year) For purposes of this section, “Maximum Capacity or Maximum Allowable” of a unit is defined as the unit ’ s potential to process charge or produce aluminum at its maximum rate on mass/time basis. If your permit limits the throughput or output of the unit, then that permitted amount may be used to calculate the maximum capacity. 3 6 . a . Please list all regulated pollutant emissions from equipment subject to 40 CFR 63, subpart RRR
.

**Unit ID No.**  **Emission s** 

**Unit Name**  **Emissions of**  **Regulated RRR Pollutants Based on**  **Perform ance Tests**  **Control Device (from** **Part C or D**  **above) List**  **Dates of the Applicable**  **Compliance Test**  **s PM**  **(lb s.**  **/ton) D/F**  ******

**( g**  **r ain** **/ton )**  **HCl**

**(lb s.**  **/ton) Total Hydrocarbons** 

**(THC) (lb**  **s. /ton)**  **Device Type**  ***** **Unit ID No**  **.**

* If you comply with subpart RRR requirements for sweat furnaces by controlling your afterburner residen ce time, enter “AB/RT” in the table
. * * Please include dioxin/

furan co ngeners . Use additional lines to break these out, if necessary.DRAFT 7/13/2010 Page 16 of 38

b
. Please list all other HAP emissions from equipment subject to 40 C FR 63, subpart RRR
. (Please include fugitive emissions
. ) **Equipment/Process Description**  **Unit ID**

**No. List**  **Each Individual**  **HAP CAS#**  **Emission Rate**  **( lbs.**  **/yr) Maximum** 

**Allowable (lb**  **s. /yr)**  **Maximum**

**Allowable (lbs.**  **/hr) Emission Factor** 

**Type** ******

c . Please list estimated HAP emissions from collocated sources that are n ot regulated under 40 C FR 63, subpart RRR
. (Please include fugitive emissions
. ) Do not include Primary Aluminum Sources. Gas f ired equipment (such as preheater boxes and annealing furnaces , etc.) not regulated under 40 CFR 63, subpart RRR may be combined into a single entry
. **Equipment/Process Description**  **Unit ID**

**N o.**  **List Each**  **Individual HAP**  ***** **CAS# Emission**  **Rate** ***** **( lbs.**  **/yr) Maximum** 

**Allowable (lb**  **s. /yr)**  **Maximum**

**Allowable (lbs.**  **/hr) Emission** 

**Factor Type 

** *** **Co pies of t**  **est data reports**  **for your HAP emissions from non**  **- subpart RRR**  **sources are not required. HAP emissions**  **data previously**  **submitted for Primary Aluminum, is not required. Please include all others HAP emissions.**  **** Emission Factor Type :**  **1** = Emissions calculated based on source test or other emissions measurements. **2** = Emissions calculated based on material balance using engineering knowledge of the process. **3** = Emissions calculated based on AP
- 42 or EPA 450/2
- 90 - 011 or other EPA emission factor. **4** = Emis sions calculated by engineering judgement. (Approved b y the State agency) **5** = Emissions calculated based on a state or local agency emission factor.DRAFT 7/13/2010 Page 17 of 38

**Part F. Detailed Control**  **D evice and Emission Release Information**  **for Subpart RRR MACT Sources and Other C**  **ollocated Sources**  **Emitting Hazardous Air Pollutants**  **(HAP)** Use information for this section from 2004 or later, whichever year is representative of the highest emissions per ton of production
.

_________ (please specify year ) 37 a . A dd
- on air pollution c ontrol device s (use multiple lines if the same control device is used to control more than one pollutant)
. Please provide the information below for subpart RRR MACT sources
. **Control Devices Units**  **Controlled**
**Device Type*** **Device**

**ID No. Pollutant** 

**Controlled Capture** 

**Efficiency (if known)**  **(percent) Control** 

**Device Efficiency**  **(if k** **nown) (percent)**  **Overall**

**Efficiency (**  **if known**  **) (percent)**  **Me thods Used for** 

**Determ ining Capture**  **& Control Efficienc**  **ies**  (a**  **- c**  **) Type(s) of Unit**  **Unit ID No.** 
* For example, afterburner, lime coated fabric filter, etc. ** Control &Capture E

fficiency a = Testing (specify method) b = Manufacturer's Specifications c = Engineering Estimate Please provide any additional info rmation concerning the Control Devices:

_______________________________________________________________________________________________________________

_________________________________________________________________________________________________________DRAFT 7/13/2010 Page 18 of 38

b. Add
- on air pollution control devices (use multiple lines if the same control device is used to control more than one pollutant). (Do not include Primary Aluminum Sources) Please provide the information below for sources not subject to subpart RRR MACT : **Control Devices Units**  **Controlled**
**Device Type*** **Device**

**ID No. Pollutant** 

**Controlled Capture** 

**Efficiency (if known)**  **(percent) Control** 

**Device Efficiency**  **(if k** **nown) (percent)**  **Overall**

**Efficiency (**  **if known**  **) (percent)**  **Me thods Used for** 

**Determ ining Capture**  **& Control**  **Efficiencies**(a -**  **c) Type(s) of Unit**  **Unit ID No.** 
* For example, afterburner, lime coated fabric filter, etc. ** Control &Capture Efficiency a = Testing (specify method) b = Manufac turer's Specifications c = Engineering Estimate Please provide any additional information concerning the Control Devices:

____________________________________________________________________________________________________________

__________________

__________________________________________________________________________________________

____________________________________________________________________________________________________________DRAFT 7/13/2010 Page 19 of 38

3 8 . a . For each stack/ control device exhaust point , ple ase provide the following information, if known , related to the information

in Item # 3 7 a above. (Subpart RRR MACT Sources
. )
**Unit ID No.**  **What C**  **ontrol**

**D evices are**  **V ented**  **at this P**  **oint? Height of stack** 

**or discharge (ft) Discharge**  **Exit Gas Temperature**  **(degre es F)**  **L atitude**  ***** **L ongitude**  ***** **Flow Rate (SCFM) Diam**  **eter (ft)**  **Area**

**(sq. ft.) Maximum**  **Minim um** 

* Longitude and Latitude should be specified out to 6 decimal places. If co ordinates are not known, p lease provide a scaled site diagram, with a latitude/longitude reference point, indicating stack locations
. b. For each stack/control device exhaust point, please provide the following information, if known, related to the info rmation in It em #3 7 b above. (Non
- Subpart RRR MACT Sources
. ) Do not include Primary Aluminum Sources
. If emissions from gas fired equipment were combined in question # 36c and discharged through different stacks, please estimate the fraction of the discharg e emitted through each stack.
**Unit ID No.**  **What C**  **ontrol**

**D evices are**  **V ented**  **at this P**  **oint? Height of stack** 

**or discharge (ft) Discharge**  **Exit Gas Temperature**  **(degrees F) Latitude** * **Longitude*** **Flow Rate (SCFM) Diam**  **eter (ft)**  **Area**

**(sq. ft.) Maximum**  **Minim um** 

* Longitude and Latitude should be specified out to 6 decimal places. If coordinates are not known, please provide a scaled site diagram, with a latitude/longitude reference point, indicating stack locations.DRAFT 7/13/2010 Page 20 of 38

3 9 . a. For each exhaust point/stack not associated with a control device for Subpart RRR MACT Sources , please provide the

following information :
**Unit ID No.**  **What C**  **ontrol**

**D evices are**  **V ented**  **at this P**  **oint? Height**  **of S**  **tack**

**or D**  **ischarge (ft) Discharge**  **Exit Gas Temperature**  **(degrees F) Latitude**  ***** **Longitude** ***** **Flow Rate (SCFM) Diam**  **eter (ft)**  **Area**

**(sq. ft.) Maximum**  **Minim um** 

* Longitude and Latitude should be specified out to 6 decimal places. If coordinates are not known, p lease provide a scaled site diagram, indicating stack locations. b. For each exhaust point/stack not associated with a control device for Non
- Subpart RRR MACT Sources , please provide the following information : (Do not include Primary Aluminum Sources
.)
**Unit ID No.**  **What C**  **ontrol**

**D evices are**  **V ented**  **at this point? Height of**  **S tack** 

**or D**  **ischarge (ft) Discharge**  **Exit Gas Temperature**  **(degrees F) Latitude** * **Longitude*** **Flow Rate (SCFM) Diam**  **eter (ft)**  **Area**

**(sq. ft.) Maximum**  **Minim um** 

* Longitude and Latitude should be specified out to 6 decimal places. If coordinates are not known, please provide a scaled site diagram, indicating stack locations.DRAFT 7/13/2010 Page 21 of 38

40 . For each affected source listed in [ Section B , above ] , identify the date(s) of latest NESHAP compliance testing. **Date Tested**  **Emission Unit Test Method**  **Used Pollutant(s)** 

**Tested Emission**  **Rate**

**(Specify Units) Unit**  **Type Unit ID No.** 

a. For each Group 1 furnace for which a performance test was conducted: **Furnace ID*** ID of other furnaces for which this test was used to determine representative emission rates Is this furnace operated continuously or batch
-by
-batch? Does the furnace process metal other than clean charge? How many runs were included in the test? What was the length of each performance test run? How many minutes during each run was the charging door open? What steps were taken during the test to minimize air emissions escaping from the furnace doors, etc.? What period of time during each run was metal tapped from the furnace? Is this a sidewell (scrapwell) furnace? Is this a me lting or holding furnace? * Where two or more co
- controlled furnaces were tested simultaneously , list all furnace IDs.DRAFT 7/13/2010 Page 22 of 38

b. For each sidewell (scrapwell) furnace **Furnace ID** Was reactive flux used in the sidewell, hearth, both, or neither? W as the level of molten metal maintained above the top of the passage between the sidewell and hearth continuously? Was the level of molten metal maintained above the top of the passage between the sidewell and hearth during periods of reactive fluxing ? How was the molten metal level monitored? c. For each Group 1 furnace **that is not ducted to a control device** : **Furnace ID** Is the furnace equipped with a hood or other type of enclosure as part of the emissions collection system? If yes, please describe. What steps were taken during the test to minimize emissions from the furnace doors, etc.? Were visible emissions monitored during the performance test? Were visible emissions observed during the performance test? d. For each Group 1 furnace that is **ducted to a control device** : **Furnace ID** Is the furnace equipped with a capture system to limit fugitive emissions? If yes, please describe. Are visible emissions present during charging? What, if any, monito ring and inspection is conducted to minimize leakage from the duct leading to the control device? What steps were taken during the test to minimize air emissions escaping from the furnace doors, etc.?DRAFT 7/13/2010 Page 23 of 38

e. For each thermal chip dryer, scrap dryer/del acquering kiln/decoating kiln, sweat furnace, dross onl y furnace and rotary dross cooler: **Equipment ID & Type**  Is this unit equipped with a hood or other capture devices as part of the emissions collection system? If yes, please describe. We re visible emissions monitored during the performance test? Were visible emissions observed during the performance test? Are visible emissions present during loading and unloading of the unit? What steps were taken during the test to minimiz e air emissions escaping from the furnace doors, etc.? 4 1 . For affected sources at your facility subject to subpart RRR that are ducted to add
- on control devices: a. Are these sources equipped with capture s ys tems designed and installed in accord ance with the standard (i. e. sections 3 and 5 of the ACGIH manual)?

___________________________________________________________________________

___________________________________________________________________________

_____________________________________ ______________________________________ b. What design parameters were measured to confirm this? ________________________

___________________________________________________________________________

__________________________________________________________ _________________ c. What , if any , modifications to the capture s ys tems of existing sources were made to demonstrate compliance with this standard (e. g. extending hoods, increasing exhaust rate, modifying operating procedures, etc.)?

____________________ _______________________

**___________________________________________________________________________**

**___________________________________________________________________________** d. Were there any problems that were encountered during the permitting process or operation of your facility due to the way the rule is written in subpart RRR?

_____________

___________________________________________________________________________

___________________________________________________________________________

___________

________________________________________________________________DRAFT 7/13/2010 Page 24 of 38

**Part G. Facility**  **Operation s**  4 2 . General Questions for Subpart RRR MACT Sources
a . What ty

pe of pretreatment ( including, but not limited to air drying, centrifugal drying, etc.) t akes places to get the charge ready for processing?

________________________________ ________________________________ _____ b. Do you track the amount of aluminum produced as well as the amount of charge?

________________________________ ________________________________ _____ c . Could you develop and report your emission rates in terms of amount of emissions per unit of aluminum produced? I f not, what prevents you from doing so?

________________________________ ________________________________ _____ d
. How do you ensure that the molten metal in the sidewell furnace remains above the top of the passage between the sidewell and the hearth during reactive fluxing ?

________________________________ ________________________________ _____ 4 3 . Flux ing for Subpart RRR MACT Sources
a. What fluxes were used during the representative year used in Part F ? Please attach MSDS for each flux:

**Flux Identification**  **Flux Still** 

**in Use? (Yes or No)**  **Reactive = R**

**Non -**  **reactive = N Mass Used** 

**(lb s.**  **/yr) Furnace or** 

**I n**  **- line**  **F luxer**  **ID in which F**  **lux was U**  **sed Purpose** 

**(e.g. ,**  **cover, degassing,**  **demagging, etc.)**

b
. If you have sidewell (scrapwell) furnaces, did you use reactive f lux in the sidewell and the hearth? If so, did you test emissions from both sources?

________________________________ ________________________________ _____ c. D o you use different types or quantities of flux for different flux applications? If so, how do the procedures differ?DRAFT 7/13/2010 Page 25 of 38 ________________________________ ________________________________ _____ d
. What are your flux rate operatin g and monitoring procedures?

________________________________ ________________________________ _____ e . Do you have any hydrogen fluoride emis sion s data for Subpart RRR MACT Sources ? If so, please provide the data reports or other supporting data for the following:

__________ Maximum tons/y r of hydrogen fluoride emissions

__________ Pounds of hydrogen fluoride emitted per ton of charge ( lb s. H F /ton

charge) __________ Maximum lbs./hr of hydrogen fluoride emitted

__________ What fraction of the fluorine content of the flux used was emitted as

either HF, F 2 , or particulate fluoride (%)? 4 4 . Alternative controls, monitoring, or operating conditions for Subpart RRR MACT S ources a . Please provide details for any **alternative control devices** ( e.g . control devices other than fabric filters, lime
- coated fabric filters, or afterburners) , **monitoring** (including particulate matter or HCl continuous emissions monitors) , or **operating conditions** at this facility for equipment regulated under 40 CFR 63, subpart RRR.

________________________________ ________________________________ _____

________________________________ ________________________________ _____ For the control technologies identified in question 44a above, please provide cost information:

**Unit ID No.**  **Control Device Tot**  **al Capital Investment**  **Total Annual**

**Operating and Maintenance**  **Costs Base Year for** 

**Operating Costs**  **Type/Description Device ID. No.** 

b
. Have you injected activated carbon or other type of carbon for HAP control (excluding res earch efforts) ? What barriers do you envision to addi ng carbon injection to fabric filters for HAP control (check as many as appl y) ? □ Cost of activated carbon □ Creates problems with disposal of material collected by baghouse □ Other (specify): ____________________________________________DRAFT 7/13/2010 Page 26 of 38

c . Do you use cataly

tic filters for dioxin control (e.g., http://www.donaldson.com/en/industrialair/literature/051754.pdf ) ?

________________________________ ________________________________ _____ d. Do you have any plans to install any new higher eff

iciency rated control devices or have any pending applications to add on any new controls? I f so, please specify and include any copies of pending p ermit applications as requested in Part A, item #17.

_____________________________________________________________________

_______________________________________________ ______________________

_____________________________________________________________________ e. Do you have any plans to use any alternative monitoring or operating conditions ? If so, please provide detail s :

_____________________________________________ _________________________

______________________________________________________________________

___________________________________________________________________ 4 5 . Pollution p revention for Subpart RRR MACT sources A. Describe any procedures or work practice standards used at your facility to prevent or reduce emissions of Hazardous Air Pollutants (HAP). (A s opposed to controlling po llution after it is formed)
.

_______________________________________________ _______________________________

**___________**

**___________________________________________________________________**

**______________________________________________________________________________**

**______________________________________________________________________________**

**________________________________ ______________________________________________** 

**______________________________________________________________________________**

**______________________________________________________________________________**

**____________________________________________________ __________________________** 

**______________________________________________________________________________**

**______________________________________________________________________________**DRAFT 7/13/2010 Page 27 of 38

**Part H. Startup**  **and Shutdown**  **for Subpart RRR MACT Sources** 46. For e ach startup and shutdown event for which you did not follow your Startup/Shutdown plan or that resulted in an exceedance of any applicable emission limitation during the past 2 ye ars, please provide the requested information in the table below. If this in formation is contained in periodic and immediate SSM reports (either stand
- alone or contained within the periodic excess emissions report) submitted to your permitting authority, you may submit copies of those reports instead. Please provide **any** emissions data during startup or shutdown, if available. Startup/Shutdown* D escription of the event, including identification of the emissions source or sources [unit ID(s)] associated with the startup or shutdown Was any permit condition exceeded and, if so, what permit condition was exceeded ? Was the event covered by any contingency plan for controlling emissions during startup or shutdown events and, if so, whether the plan was followed; if the plan was not followed, why not ? Ty pical d uration of an event A ctions taken to minimize emissions during the event, including the use of any backup control sy stems Estimates or measurements, if any , of emissions during the event; if you did not have the ability

to quantify

emission s during the event, please explain why For affected sources ducted to afterburners, did any startups or shutdowns take place while the afterburner was not operating, or operating outside of the operating temperature established during the performanc e test? For affected sources ducted to control devices and monitored by

continuous opacity

monitors, did opacity

exceed 10% during any startup or shutdown events? List performance test data collected during each period of startup or shutdown, the test method used for each event; when the testing was conducted and why; the test conditions at the time of testing; and whether the tests were associated with a routine startup or shutdownDRAFT 7/13/2010 Page 28 of 38

* Startup : the commencement of operation of an affect ed source or portion of an affected source for any purpose ; Shutdown : the cessation of operation of an affected source or portion of an affected source for any purpose 47. Are there any types of startup or shutdown events that you have been able to eliminate: if so, please describe the type of event and explain how these events were eliminated? 48 . Optional: Please recommend a standard that would apply during startup and/or shutdown
. D escribe the ty

pe of event (e.g., defining the beginning and durati on of a start
- up period and sim il arly for a shutdown) to which the standard would apply ; the recommended standard (this could be an emission limitation, work practice, or operational standard) that would apply during the period; the basis for the recommend ed standard; why and how the standard would minimize emissions during the event; and how compliance would be determined and/or monitored.DRAFT 7/13/2010 Page 2 9 of 38

**Part I. C**  **riteria Air Pollutants (CAP) for**  **subpart RRR MACT sources and non**  **- subpart RRR MACT sources**  Please prov ide the information below for all regulated equipment at your facility; Use information for this section from 2004 or later, whichever year has the highest production rate
. _________(please specify year ) 49. a. C AP emissions by unit for each emission unit subject to 40 CFR 63, subpart RRR MACT sources
. (Please include fugitive emissions
. )
**Unit ID No.**  **Emission**

**Unit CAP Emissions** * **(tons per year) Lead**  **VOC PM**  **PM10 PM2.5**  **CO SOx**  **NOx**

*** Pleas e provide any test data along with**  **this section**  **for sources subject to 40 CFR 63,**  **subpart RRR MACT sources .**  b
. Please list estimated CAP emissions from collocated sources at your facility that are not regulated under 40 CFR 63, subpart RRR
. (Please include fugitive emissions , but not emissions from Primary Aluminum sources
. ) **T**

**est reports are**  **not required to be submitted**  **for sources not subject to 40 CFR 63, subpart RRR. Unit**  **ID No. Emission** 

**Unit CAP Emissions**  **(tons per year) Lead**  **VOC PM**  **PM10 PM2.5**  **C O**  **SOx NOx** DRAFT 7/13/2010 Page 30 of 38

50. Control devices used for CAP emission control for Subpart RRR MACT sources & Non - Subpart RRR MACT sources (Excluding Primary

Aluminum) **Control Device ID Type of Device**  **ID(s) of Units Controlled**  **Pollutants Controlled Control Efficiency (%)** 

**Part J**  **. Energy Usage**  51 . Please list total annual energy consumption. **Combustion Units ( Ex**  **clude Emergency Combustion Equipment) Unit**  **Unit Unit**  **Unit Unit**  Process Unit ID: Equipment ID: Type of Combustion Equipment: Year Built: Number of Operating Hours per Year: Design Capacity (Heat Input) (MMBtu/hr): Fuel Type: Heat Release Rate (Btu/scf): Is the unit subject to NSPS? If yes, indicate the year: **Start -**  **up Fuel/Material** Start -up fuel: Typical Start
-up fuel amount ( s pecify units) Typical length of time for start
-up (hours): Higher heating value (HHV):DRAFT 7/13/2010 Page 31 of 38

**Fuels/Materials Combusted Du ring**  **Production (include solid, liquid, and gas waste**  **streams)** Fuel #1 u sage: ( s pecify units) Hours used per year: Higher heating value (HHV): Fuel #2 u sage: ( s pecify units) Hours used per year: Higher heating value (HHV): Fuel # 3 u sage: (specify units ) Hours used per year: Higher heating value (HHV): Please note: In the excel version this chart will be vertical and allow for facility totals, if individual unit information is not known. 52 . Are any

Co generation units listed above, if so please list the unit and describe the process for each?

____________________________________________________________________________________ _____

_________________________________________________________________________ ________________

_________________________________________________________________________________________ 53. Electricity

Usage **Normal Operating Annual Electricity Usage**  **Year Total Facility**  **Usage (Specify Unit**  **of Measurement )** 

**K. Miscellaneo**  **us Information** 5 4 . What specific improvements or rule changes would you like to see that would help your facility with compliance or better rule interpretation?NESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 32 of 38 **Attachment A. Definitions**  **for subpart RRR**  **MACT sources** Afterburner means an air polluti on control device that uses controlled flame combustion to convert combustible materials to noncombustible gases; also known as an incinerator or a thermal oxidizer. Aluminum scrap means fragments of aluminum stock removed during manufacturing (i.e., machining), manufactured aluminum articles or parts rejected or discarded and useful only as material for reprocessing, and waste and discarded material made of aluminum. Aluminum scrap shredder means a unit that crushes, grinds, or breaks aluminum scrap int o a more uniform size prior to processing or charging to a scrap dryer/delacquering kiln/decoating kiln, or furnace. A bale breaker is not an aluminum scrap shredder. Clean charge means furnace charge materials, including molten aluminum; T
- bar; sow; in got; billet; pig; alloying elements; aluminum scrap known by the owner or operator to be entirely free of paints, coatings, and lubricants; uncoated/unpainted aluminum chips that have been thermally dried or treated by a centrifugal cleaner; aluminum scrap dried at 343 °C (650 °F) or higher; aluminum scrap delacquered/ decoated at 482 °C (900 °F) or higher, and runaround scrap Cover flux means salt added to the surface of molten aluminum in a group 1 or group 2 furnace, without agitation of the molten alum inum, for the purpose of preventing oxidation. Dross - only

furnace means a furnace, typicall y of rotary barrel design, dedicated to the reclamation of aluminum from dross formed during melting, holding, fluxing, or alloying operations carried out in other process units. Dross and salt flux are the sole feedstocks to this ty pe of furnace. Group 1 furnace means a furnace of any design that melts, holds, or processes aluminum that contains paint, lubricants, coatings, or other foreign materials with or witho ut reactive fluxing, or processes clean charge with reactive fluxing. Group 2 furnace means a furnace of any design that melts, holds, or processes only clean charge and that performs no fluxing or performs fluxing using only nonreactive, non
- HAP - containing/non
- HAP generating gases or agents. In - line fluxer means a device exterior to a furnace, located in a transfer line from a furnace, used to refine (flux) molten aluminum; also known as a flux box, degassing box, or demagging box. Melting/holding furn ace , or melter/holder, means a group 1 furnace that processes onl y clean charge, performs melting, holding, and fluxing functions, and does not transfer molten aluminum to or from another furnace. Rotary dross cooler means a water - cooled rotary barrel dev ice that accelerates cooling of dross. Runaround scrap means scrap materials generated on
- site by aluminum casting, extruding, rolling, scalping, forging, forming/stamping, cutting, and trimming operations and that do not contain paint or solid coatings . Uncoated/unpainted aluminum chips generated by turning, boring, milling, and similarNESHAP for Secondary Aluminum (40 CFR part 63, subpart RRR)

DRAFT 7/13/2010 Page 33 of 38 machining operations may be clean charge if they

have been thermall y dried or treated b y a centrifugal cleaner, but are not considered to be runaround scrap. Scrap drye r/delacquering kiln/decoating kiln means a unit used primarily to remove various organic contaminants such as oil, paint, lacquer, ink, plastic, and/or rubber from aluminum scrap (including used beverage containers) prior to melting. Secondary

aluminum processing unit (SAPU): an existing SAPU means all existing group 1 furnaces and all existing in
- line fluxers within a secondary aluminum production facility . Each existing group 1 furnace or existing in
- line fluxer is considered an emission unit within a secondary aluminum processing unit. A new SAPU means any combination of group 1 furnaces and in
- line fluxers which are simultaneously

constructed after February 11, 1999. Each of the group 1 furnaces or in
- line fluxers within a new SAPU is considered an emission unit within that secondary aluminum processing unit. Sidewell means an open well adjacent to the hearth of a furnace with connecting arches between the hearth and the open well through which molten aluminum is circulated between the hearth, where heat is applied by

burners, and the open well, which is used for charging scrap and solid flux or salt to the furnace, injecting fluxing agents, and skimming dross. Sweat furnace means a furnace used exclusively to reclaim aluminum from scrap that contains substantial quantities of iron by using heat to separate the low
- melting point aluminum from the scrap while the higher melting
- point iron remains in solid form. Thermal chip dryer means a device that uses heat to evaporate water, oil, or oil/water mixtures from unpainted/uncoated aluminum chips.DRAFT 7/13/2010 Page 34 of 38

**Appendix B** 

### Section 112(b) List of Hazardous Air Pollutants (HAP) U.S. Code Title 42, Chapter 85, Subchapter 1, Part A, § 7412 **CAS Number**  **Chemical Name**  75070 Acetaldehyde 60355 Acetamide 75058 Ac etonitrile 98862 Acetophenone 53963 2 - Acetylaminofluorene 107028 Acrolein 79061 Acrylamide 79107 Acrylic acid 107131 Acrylonitrile 107051 Allyl chloride 92671 4 - Aminobiphenyl 62533 Aniline 90040 o - Anisidine 1332214 Asbestos 71432 Be nzene (including benzene from gasoline) 92875 Benzidine 98077 Benzotrichloride 100447 Benzyl chloride 92524 Biphenyl 117817 Bis(2 - ethylhexyl)phthalate (DEHP) 542881 Bis(chloromethyl)ether 75252 Bromoform 106990 1,3 - Butadiene 156627 Calciu m cyanamide 133062 Captan 63252 Carbaryl 75150 Carbon disulfide 56235 Carbon tetrachloride 463581 Carbonyl sulfide 120809 Catechol 133904 Chloramben 57749 Chlordane 7782505 Chlorine 79118 Chloroacetic acid 532274 2 - Chloroacetophenone 108907 ChlorobenzeneDRAFT 7/13/2010 Page 35 of 38

510156 Chlorobenzilate 67663 Chloroform 107302 Chloromethyl methyl ether 126998 Chloroprene 1319773 Cresols/Cresylic acid (isomers and mixture) 95487 o - Cresol 108394 m - Cresol 106445 p - Cresol 98828 Cumene 94757 2,4 - D, salts and esters 3547044 DDE 334883 Diazomethane 132649 Dibenzofurans 96128 1,2 - Dibromo - 3 - chloropropane 84742 Dibutylphthalate 106467 1,4 - Dichlorobenzene(p) 91941 3,3 - Dichlorobenzidene 111444 Dichloroethyl ether (Bis(2 - chloroethyl)ether ) 542756 1,3 - Dichloropropene 62737 Dichlorvos 111422 Diethanolamine 121697 N,N - Diethyl aniline (N,N - Dimethylaniline) 64675 Diethyl sulfate 119904 3,3 - Dimethoxybenzidine 60117 Dimethyl aminoazobenzene 119937 3,3 - Dimethyl benzidine 79447 Di methyl carbamoyl chloride 68122 Dimethyl formamide 57147 1,1 - Dimethyl hydrazine 131113 Dimethyl phthalate 77781 Dimethyl sulfate 534521 4,6 - Dinitro - o - cresol, and salts 51285 2,4 - Dinitrophenol 121142 2,4 - Dinitrotoluene 123911 1,4 - Dioxane (1, 4 - Diethyleneoxide) 122667 1,2 - Diphenylhydrazine 106898 Epichlorohydrin (l - Chloro - 2,3 - epoxypropane) 106887 1,2 - Epoxybutane 140885 Ethyl acrylate 100414 Ethyl benzene 51796 Ethyl carbamate (Urethane) 75003 Ethyl chloride (Chloroethane)DRAFT 7/13/2010 Page 36 of 38

106934 Ethylene dibromide (Dibromoethane) 107062 Ethylene dichloride (1,2 - Dichloroethane) 107211 Ethylene glycol 151564 Ethylene imine (Aziridine) 75218 Ethylene oxide 96457 Ethylene thiourea 75343 Ethylidene dichloride (1,1 - Dichloroethane) 50000 F ormaldehyde 76448 Heptachlor 118741 Hexachlorobenzene 87683 Hexachlorobutadiene 77474 Hexachlorocyclopentadiene 67721 Hexachloroethane 822060 Hexamethylene - 1,6 - diis ocyanate 680319 Hexamethylphosphoramide 110543 Hexane 302012 Hydrazine 76 47010 Hydrochloric acid 7664393 Hydrogen fluoride (Hydrofluoric acid) 123319 Hydroquinone 78591 Isophorone 58899 Lindane (all isomers) 108316 Maleic anhydride 67561 Methanol 72435 Methoxychlor 74839 Methyl bromide (Bromomethane) 74873 Me thyl chloride (Chloromethane) 71556 Methyl chloroform (1,1,1 - Trichloroethane) 60344 Methyl hydrazine 74884 Methyl iodide (Iodomethane) 108101 Methyl isobutyl ketone (Hexone) 624839 Methyl isocyanate 80626 Methyl methacrylate 1634044 Methyl te rt butyl ether 101144 4,4 - Methylene bis(2 - chloroaniline) 75092 Methylene chloride (Dichloromethane) 101688 Methylene diphenyl diisocyanate (MDI) 101779 4,4 - Methylenedianiline 91203 Naphthalene 98953 Nitrobenzene 92933 4 - Nitrobiphenyl 100027 4 - NitrophenolDRAFT 7/13/2010 Page 37 of 38

79469 2 - Nitropropane 684935 N - Nitroso - N - methylurea 62759 N - Nitrosodimethylamine 59892 N - Nitrosomorpholine 56382 Parathion 82688 Pentachloronitrobenzene (Quintobenzene) 87865 Pentachlorophenol 108952 Phenol 106503 p - Phenylen ediamine 75445 Phosgene 7803512 Phosphine 7723140 Phosphorus 85449 Phthalic anhydride 1336363 Polychlorinated biphenyls (Aroclors) 1120714 1,3 - Propane sultone 57578 beta - Propiolactone 123386 Propionaldehyde 114261 Propoxur (Baygon) 78875 Propylene dichloride (1,2 - Dichloropropane) 75569 Propylene oxide 75558 1,2 - Propylenimine (2 - Methyl aziridine) 91225 Quinoline 106514 Quinone 100425 Styrene 96093 Styrene oxide 1746016 2,3,7,8 - Tetrachlorodibenzo - p - dioxin 79345 1,1,2,2 - Tetr achloroethane 127184 Tetrachloroethylene (Perchloroethylene) 7550450 Titanium tetrachloride 108883 Toluene 95807 2,4 - Toluene diamine 584849 2,4 - Toluene diisocyanate 95534 o - Toluidine 8001352 Toxaphene (chlorinated camphene) 120821 1,2,4 - Tri chlorobenzene 79005 1,1,2 - Trichloroethane 79016 Trichloroethylene 95954 2,4,5 - Trichlorophenol 88062 2,4,6 - Trichlorophenol 121448 Triethylamine 1582098 Trifluralin 540841 2,2,4 - TrimethylpentaneDRAFT 7/13/2010 Page 38 of 38

108054 Vinyl acetate 593602 Vinyl bromide 75 014 Vinyl chloride 75354 Vinylidene chloride (1,1 - Dichloroethylene) 1330207 Xylenes (isomers and mixture) 95476 o - Xylenes 108383 m - Xylenes 106423 p - Xylenes 0 Antimony Compounds 0 Arsenic Compounds (inorganic including arsine) 0 Beryllium C ompounds 0 Cadmium Compounds 0 Chromium Compounds 0 Cobalt Compounds 0 Coke Oven Emissions 0 Cyanide Compounds 1 0 Certain Glycol ethers 2 0 Lead Compounds 0 Manganese Compounds 0 Mercury Compounds 0 Fine mineral fibers 3 0 Nickel Compounds 0 Polycyclic Organic Matter 4 0 Radionuclides (including radon) 5 0 Selenium Compounds NOTE: For all listings above which contain the word “compounds” and for glycol ethers, the following applies: Unless otherwise specified, these l istings are defined as including any unique chemical substance that contains the named chemical (i.e., antimony, arsenic, etc.) as part of that chemical’s infrastructure. 1 XCN where X = H or any other group where a formal dissociation may occur. For exam ple KCN or Ca(CN) 2 . 2 Includes mono - and di - ethers of ethylene glycol (except for ethylene glycol monobutyl ether (CAS Number 111 – 76 – 2) , diethylene glycol, and triethylene glycol R – (OCH 2 CH 2 )n – OR where n = 1, 2, or 3 R = alkyl or aryl groups R = R, H, or groups which, when removed, yield glycol ethers with the structure: R – (OCH 2 CH)n – OH. Polymers are excluded from the glycol category. 3 Includes mineral fiber emissions from facilities manufacturing or processing glass, rock, or slag fibers (or other min eral derived fibers) of average diameter 1 micrometer or less. 4 Includes organic compounds with more than one benzene ring, and which have a boiling point greater than or equal to 100°C. 5 A type of atom which spontaneously undergoes radioactive decay.