Exhaust Emissions Sampling 

Daltile, Dallas, TX 

Plant 4 and Plant 213 Scrubber Exhausts 

May 22 - 23, 2007 

Armstrong Environmental, Inc. 

Project W-2527-07 

Report Prepared For: 

Bob Hurt 

Daltile 

7834 C. F. Hawn Freeway 

Dallas, TX 75217 

Report Prepared May 26, 2007 By: 

Armstrong Erzvironmental, Inc. 

1748 Hlavek Rd. 

Decatur, Texas 76234 

(214) 631-0021 
TABLE OF CONTENTS 

Page 

I. Introduction 1 

U. Summary 2-4 

IlI. Procedures 5-7 

TV. Appendices 

A. Calculation Summaries 8-13 

B. Analytical Summaries 14-54 

t 

C. Field Data Sheets 51 - 58 

D. Equipment Calibrations 59-68 
I. INTRODUCTION 

A series of tests was performed on the exhausts associated with the Plant 4 scrubber and 

the Plant 2/3 Scrubber at the Daltile facility in Dallas, TX on May 26, 2007. 

The purpose of this test series was to determine the exhaust emission rate of Hydrogen 

Fluoride and Hydrogen Chloride in terms of lbs/hr. 

Testing followed procedures detailed in Title 40: Code of Federal Regulations (40:CFR). 

Sampling was performed by Richard Taylor, Gilbert Salinas and Tom Armstrong of 

Armstrong Environmental, Inc. using an Apex Method 5 sampling train. 

Present during the test series was Gabriel Perez of TCEQ. 

Three one hour test repetitions were performed on each source according to the following 

schedule: 

° Date. Source:. Start Tiirne Finish T.ime 

5/22/07 Plant 4 Scrubber 8:30 AM 12:02 PM 

5/23/07 Plant 2/3 Scrubber 9:15 AM 12:46 PM 

Submitted by: 

Armstronr~rn 

d orn Arn 

President 
II. SUMMARY 

A series of tests was performed on the exhausts associated with the Plant 4 scrubber and 

the Plant 2/3 Scrubber at the Daltile facility in Dallas, TX on May 26, 2007. 

Sampling was performed following procedures detailed in Title 40: Code of Federal 

Regulations. 

Results of this test series are summarized in Tables 1& 2. 

Results indicate the following emission rates for the Plant 4 Scrubber: 

Avera e -- HF, lbs/hr 0.0121 0.0120 0.0053 0.0098 

HCI, lbs/hr 0.0078 0.0098 0.0079 0.0085 

Results indicate the following emission rates for the Plant 2/3 Scrubber: 

ver~ e` 

HF, lbs/hr 0.00 0.0081 0.0079 0.0053 

HCI, lbs/hr 0.00 0.0322 0.0072 0.0013 

'-) a , 3 

2 
SUMMARY OF EMISSIONS TEST DATA 

Table : 1 

Plant : Da(tile, Dallas, TX 

Location : Plant 4 Scrubber 

Operator : R. Taylor, G. Salinas, T. Armstrong 

Test Date : 22-May•07 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 132.7 132.3 132.3 

Velocity, fps 47.60 47.60 47.05 

Volume Flow, acfm 15951.6 15952.0 15767.9 

scfm 11983.0 12033.7 11718.7 

scfh 718979 722022 703121 

Moisture, % 14.54% 14.25% 15.52% 

CO2, % 3.00 3.00 3.00 

02, % 16.00 16.50 16.50 

SAMPLE 

Start Time, hrs:min ' 8:30 AM 9:45 AM 11:00 AM 

Finish Time, hrs:min 9:33 AM 10:48 AM 12:02 PM 

Sample Volume, scf 34.846 35.458 35.236 

Isokinetic Ratio, % 97.8333 99.13347 101.1615 

HYDROGEN FLUORIDE 

Sample Weight, mg 0.267 0.268 0.120 

Concentration, ppm 0.325407 0.320983 0.144629 

Emissions, Ibs/hr 0.012147 0.012033 0.00528 

HYDROGEN CHLORIDE 

Sample Weight, mg 0.171 0.218 0.179 

Concentration, ppm 0.114195 0.143067 0.118213 

Emissions, lbs/hr 0.00778 0.0097$$ 0.007$76 

3 
SUMMARY OF EMISSIONS TEST DATA 

Table : 2 

Plant : Daltile, Dallas, TX 

Location : Plant 2/3 Scrubber 

Operator : R. Taylor, G. Salinas, T. Armstrong 

Test Date : 23• May-07 

Repetition : 1 2 3 

STACK GAS 

Temperature, F 116.5 117.6 117.8 

Velocity, fps 62.60 61.46 61.42 

Volume Flow, acfm 15492.7 15210.1 15199.3 

scfm 12606.8 12329.1 12214.9 

scfh 756410 739749 732891 

Moisture, % • 10.11°J 10.28% . 11.03% 

CO2, °Jo 1.50 1.50 1.50 

02, °"Jo 19.00 19.50 19.00 

SAMPLE 

Start Time, hrs:min 

. 

9:15 AM 10:30 AM 

, 

11:45 AM 

Finish Time, hrs:min 10:16 AM 11:31 AM 12:46 PM 

Sample Volume, scf 37.267 36.466 36.272 

lsokinetic Ratio, °Jo 100.4018 100.4551 100.8556 

HYDROGEN FLUORIDE 

Sample Weight, mg 0.00 0.181 0.177 

Concentration, ppm 0 0.210795 0.207239 

Emi ssions, I bs/hr 0 0.008096 0.007886 

HYDROGEN CHLORIDE 

Sample Weight, mg 0.00 0.720 0.162 

Concentration, pprn 0 0.459464 0.103932 

Emissions, !bs/hr 0 0.032206 0.007218 

0 
III . PRO CEDUURES 

The procedure for emissions sampling followed USEPA test methods as detailed in Title 

40: Code of Federal Regulations. The following methods were used: 

Method Title 

1 Sample and Velocity Traverses for Stationary Sources 

2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S 

Pitot Tube) 

3 Gas Analysis for the Determination of Dry Molecular VVeight - 

26A Determination of Hydrogen Halides and Halogens Emissions from 

Stationary Sources 

02 and CO2 were determined using FyRite Analyzers. 

HF and HCl sampling was performed on the Plant 4 scrubber exhaust for 2.5 minutes at 

each of 24 points, 12 points per traverse, making a total run duration of 60 minutes. HF 

and HCl was performed on the Plant 2l3 scrubber exhaust for 5 minutes at each of 12 

points, six points per traverse. A schematic of each sampling location is shown in Figures 

1 and 2. The sampling train was configured as follows: 

Glass Sampling Nozzle 

Heated Glass Lined Probe 

Heated teflon filter 

Impinger # 1- 100 mis 0.1 N H2S 04 

Impinger #2 - 100 mis 0.1 N H2SO4 

Impinger #3 - Empty 

Impinger #4 - 200 grams silica Gel 

Analysis for HF and HCl was performed on the solution frorn impingers 1- 3. Analysis 

was performed using a Dionex LC20 Ion Chromatograph. Standards were made from a 

999 rnglL chloride in H20 and a 995 mg/L fluoride in H20 certified standards. 200 ul, 

400 ul, 600 ul, and $00 ul of each solution was added to 100 mis of 0.1 N H2SO4. 

5 
Fzgure 2 —Plant 2/3 Scrubrer 

84 ir7clies 

Lto 

Stack Diameter ~7.5 irlches 

1:t ~ ii ~ches Pc~ ir~ l It1 -1.2 iric ~ es 

Pair•ik #2 - 4.0 inclles 

Poilit h3 - 8.1 iriches 

('oiiit M - 19.4 iticlies 

Point 115 - 23.5 iiiches 

Pair-it 06 - 2E.3 inches 
Figure :t -- Plant 4 Scubber 

s34 iriches 

~ 

t_~4 ireches 6 tacE; D iametei - 32 inches 

Poirlt #1 ;1. Q inches 

Point #2 - 2-1 inches 

Pcint 03 - 30 inches 

Point ##4 - 5.7 inctins 

Point 145 - $ inches - 

Point 116 -11. 4 inches 

Poit-it # 7 - 20.1 inciies 

Point 118 - 24 inches 

F'oir-it I#9 - 26.3 inches 

Point 410 - 28.2 inches 

Point #t1'I - 23.9 incf7es 

Poirit tt12 - 31 inches 

EMISSION TEST SUMMARY 

PLANT : Dattile. Datlas, TX 

DATE : 22•May07 

PLACE : Plant 4 Scrubber 

RUN# : 1 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 126 

NOZZLE DIAMETER (INCH.) : 0.2253 PARTICULATE WEIGHT (Front hatf mg) : 0 

METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.34 

GAS METER VOL.(Cu.Ft.) : 36.083 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.55 PERCENT 02 16 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 32 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) : 5.585054 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000277 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 5.585054 

FLOwS 

SAMPLED VOLUME (STD. CU .FT.): ' 34.8458 

VOLUME OF WATER VAPOR (STD. CU .FT.): 5.9308 

FRACTIONAL MOISTURE CONTENT 0.1454 

DRY BASE: 81.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.5026 

STACK PRESSURE (inch Hg): 29.5250 

STACK GAS VELOCITY (ft/sec.): 47.6021 

ACTUAL STACK GAS FLOW RATE`(ACFM): 15951.6184 

STANDARD STACK GAS FLOW RATE (SCFH): 718979.224 

ISOKINETIC RATIO (%): 97.8333 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. 

deg F INLET 

It 

METER T. Meter Point Point Point Point Iso 

OUTLET Votume VMSTD Velocity Moisture 

1 138 0.65 0.806226 0.97 77 76 

2 138 0.66 0.812404 0.98 78 76 

3 138 0.69 0.830662 1.00 80 75 

4 138 0.68 0.824621 1.00 80 75 

5 138 0.68 0.824621 1.00 82 76 

6 134 0.67 0.818535 1.00 83 76 

7 134 0.64 0.8 0.95 83 76 

8 132 0.61 0.781025 0.91 83 7 6 

9 132 0.57 0.754983 0.85 83 77 

10 132 0.53 0.728011 0.79 84 77 

11 133 0.50 0.707107 0.74 84 78 

12 331 0.42 0.648074 0.62 84 77 

13 132 0.65 0.806226 0.97 79 77 

14 132 0.69 0.830662 1.00 82 77 

15 131 0.68 0.824621 1.00 84 77 

16 130 0.69 0.830662 1.00 85 77 

17 130 0.6E 0.824621 1.00 85 78 

18 130 0.67 0.818535 1.00 85 78 

19 130 0.62 0.787401 0.93 85 78 

20 129 0.60 0.774597 0.91 81 78 

21 129 0.55 0.748331 0.85 8r 78 

22 130 0.52 0.72111 0.79 84 78 

23 132 0.47 0.685565 0.71 84 78 

24 132 0.40 0.632456 0.61 84 78 

132.70833 0.7759 0.8992 82.8333 76.9583 

mis 

182 1.5552 49.6844 5.63101 

183.6 1.4567 50.0651 5.27429 

185.1 1.5524 51.1903 5.62095 

186.7 1.5524 50.818 5.62095 

188.3 1.5481 50.818 5.60531 

189.9 1.5467 50274 5.60011 

191.5 1.4498 49.1355 5.24945 

193 1.4497 47.8893 5.24893 

194.5 1.4481 46.2925 5.24329 

196 1.3501 44.6387 4.88848 

197.4 1.3487 43.3935 4.88336 

198.8 1.2001 39.7037 4.34542 

200.045 1.5072 49.4345 5.45738 

201.6 1.5467 50.9328 5.60011 

203.2 1.6403 50.5197 5.93911 

204.9 1.446 50.8467 5.23555 

206.4 1.5409 50.4769 5.57943 

208 1.5409 50.1044 5.57943 

209.6 1.4444 48.1986 5.22981 

211.1 1.4443 47.3746 5.22955 

212.6 1.4441 45.7682 5.22877 

214.1 1.3489 44.1408 4.88397 

215.5 1.2523 42.0361 4.53421 

216.8 1.2356 38.7796 4.4738 

218.083 

79.8958 

101.3172 

94.1771 

98.1610 

98.8801 

98.6049 

98.9135 

94.8681 

96.9996 

100.2375 

96.9170 

99.7617 

96.6950 

97.6992 

97.3052 

103.8637 

90.8169 

97.4910 

98.2158 

95.7015 

97.1961 

100.5926 

97.5888 

95.4589 

102.0965 

i ~ 
EMISSION TEST SUMMARY 

PLANT : rJaltile. De.11as. TX 

DATE : 22•May07 

PLACE : PIan14 Scruaber 

RUN#: 2 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 125.2 

NOZZLE DIAMETER (INCH_) : 0.2253 PARTlCULATE WEIGHT (Front half mg) : 0 

METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mf{) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.34 

GAS METER VOL.(Cu.Ft.) : 36.803 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.55 PERCENT 02 16.5 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 32 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 5.585054, STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000277 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 5.585054 

FLOwS 

SAMPLED VOLUME (STD. CU .FT.): 35.4583 

VOLUME OF WATER VAPOR (STD. CU .FT.): 5.8932 

FRACTIONAL MOISTURE CONTENT (%): 0.1425 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1400 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.5524 

STACK PRESSURE (inch Hg): 29.5250 

STACK GAS VELOCITY (ft/sec.): 47.6032 

ACTUAL STACK GAS FLOW RATE (ACFM): 15951.9895 ° 

STANDARD STACK GAS FLOW RATE (SCFH): 722021.736 

JSOKINETIC RATIO (%): 99.1335 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso 

deg F INLET 

1 131 0.65 0.806226 0.98 78 

2 132 0.66 0.812404 0.99 81 

3 132 0.68 0.824621 1.00 82 

4 132 0.70 0.83666 1.10 83 

5 133 0.69 0.830662 1.00 84 

6 133 0.68 0.824621 1.00 84 

7 133 0.65 0.806226 0.98 85 

8 133 0.62 0.787401 0.94 84 

9 132 0.59 0.76B115 0.89 84 

10 130 0.56 0.748331 0.85 85 

11 130 0.55 0.74162 0.83 85 

12 129 0.46 0.678233 0.70 85 

13 130 0.65 0.806226 1.00 80 

14 132 0.68 0.824621 1.10 84 

15 134 0.67 0.818535 1.10 85 

16 133 0.68 0.824621 1.10 86 

17 134 0.66 0.812404 1.00 86 

18 134 0.67 0.818535 1.10 85 

19 134 0.64 0.8 1.00 86 

20 135 0.58 0.761577 0.92 86 

21 134 0.54 0.734847 0.86 86 

22 132 0.51 0.714143 0.81 86 

23 132 0.40 0.632456 0.63 86 

24 130 040 0.632456 0.63 86 

132.25 0.7769. 0.9379 84.2500 

OUTLET Volume VMSTD Velocity Moisture 

mis 

78 218.3 1.5509 49.3481 5.483405 

77 219.9 1.5481 49.7683 5.473368 

77 221.5 1.5467 50.5167 5.468431 

77 223.1 1.5456 51.2542 5.464723 

77 224.7 1.5438 50.9298 5.458313 

77 226.3 1.5438 50.5594 5.458313 

78 227.9 1.5409 49.4315 5.447963 

77 229.5 1.4471 48.2773 5.116407 

78 231 1.4456 47.0551 5.111043 

78 232.5 1.4441 45.7657 5.105817 

78 234 1.3478 45.3552 4.765193 

78 235.4 1.3059 41.4435 4.617342 

78 236.757 1.5897 49.3063 5.620604 

78 238.4 1.5428 50.5167 5.454622 

78 240 1.6377 50.2285 5.790185 

78 241.7 1.5399 50.5594 5.444558 

79 243.3 1.5381 49.8523 5.43819 

79 244.9 1.6362 50.2285 5.784843 

79 246.6 1.442 49.0911 5.098304 

79 248.1 1.5378 46.7727 5.437111 

80 249.7 1.4401 45.0931 5.091839 

79 251.2 1.3452 43.7488 4.756173 

80 252.6 1.1515 38.7446 4.071145 

79 253.8 1.2514 38.6791 4.424659 

255.103 

78.1667 81.2083 

100.1906 

99.3306 

97.7707 

96.2985 

96.9619 

97.6722 

99.7113 

95.8618 

98.1034 

100.4239 

94.5725 

100.1176 

102.6106 

97.5238 

104.4691 

97.4261 

98.8588 

104.3728 

94.1171 

105.5243 

102.3318 

98.1913 

94.9046 

102.9711 

.i ~ • ci. 
EMlSSION TEST SUMMARY 

PLANT : Daltile. Dallas, TX 

DATE : 22•May07 

PLACE : Plant 4 Scrubber 

RUN3s : 3 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 137.5 

NOZZLE DIAMETER (INCH.) : 0.2253 PARTICULATE WEIGHT (Front half mg) : 0 

METER COEFFiCIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.33 

GAS METER VOL.(Cu.Ft.) : 36.805 PERCENT CO2 3 

BAROMETRIC PRESSURE 29.55 PERCENT 02 16.5 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 32 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 5.585054 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000277 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 5.585054 

FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 35.2364 

VOLUME OF WATER VAPOR (STD. CU .FT.): 6.4721 

FRACTIONAL MOISTURE CONTENT (g6): 0.1552 

DRY BASE: 80.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1400 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.4113 

STACK PRESSURE (inch Hg): 29.5257 

STACK GAS VELOCITY (ft/sec.): 47.0540 

ACTUAL STACK GAS FLOW RATE (ACFM): 15787.938 ~ 

STANDARD STACK GAS FLOW RATE (SCFH): 703121.263 

1SOKINETIC RAT10 (gf,): 101.1615 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Paint Point Point Point Iso 

deg F 1NLET OUTLET Volume VMSTD Velocity Moisture 

mis 

1 133 0.65 0.806226 1.00 80 79 255.4 1.5467 49.5579 6.043488 101.3263 

2 133 0.66 0.812404 1.00 82 79 257 1.5438 49.9377 6.032306 100.3697 

3 133 0.67 0.818535 1.10 84 79 256.6 1.6377 50.3146 6.399077 105.6748 

4 130 0.67 0.818535 1.10 85 79 260.3 1.5399 50.1871 6.017105 99.1152 

5 13G 0.67 0.818535 1.10 85 79 261.9 1.5399 50.1871 6.017105 99.1152 

6 130 0.65 0.806226 1.00 87 80 263.5 1.5353 49.4324 5.999009 100.3258 

7 130 0.62 0.787401 0.99 87 80 265.1 1.5352 48.2782 5.99886 102.7219 

8 129 0.60 0.774597 0.96 87 80 266.7 1.5351 47.4529 5.998414 104.3236 

9 130 0.57 0.754983 0.91 88 80 268.3 1.4377 46.2906 5.617647 100.3245 

10 131 0.54 0.734847 0.86 88 81 269.8 1.4362 45.0941 5.611792 103.0534 

11 132 0.49 0.7 0.78 89 81 271.3 1.3389 42.992 5.231828 100.9439 

12 132 0.50 0.707107 0.80 89 81 272.7 1.3237 43.4285 5.172292 98.7922 

13 133 0.65 0.806226 1.00 85 82 274.084 1.5506 49.5579 6.058999 301.5864 

14 136 0.65 0.806226 1.00 B9 82 275.7 1.5296 49.6831 5.977015 100.4650 

15 .34 1 0.65 0.806226 1.00 89 82 277.3 1.5296 49.5997 5.977015 100.2963 

16 134 0.66 0.812404 1.05 90 83 278.9 1.6225 49.9798 6.339744 105.5740 

17 133 0.65 0.806226 1.00 90 83 280.6 1.5268 49.5579 5.966078 100.0284 

18 133 0.64 0.8 1.00 90 83 282.2 1.5268 49.1752 5.966078 100.8069 

19 134 0.61 0.781025 0.97 91 83 283.8 1.43 48.0493 5.587669 96.7883 

20 134 0.55 0.74162 0.89 91 83 285.3 1.4297 45.6251 5.58656 101.9108 

21 133 0.54 0.734847 0.86 91 84 286.8 1.4283 45.1703 5.581042 102.6620 

22 133 0.48 0.69282 0.77 91 84 288.3 1.3328 42.587 5.207809 101.6075 

23 132 0.43 0.655744 0.68 91 83 289.7 1.2384 40.2739 4.839161 99.6691 

24 133 0.36 0.6 0.68 90 84 291 1.1479 36.8814 4.48553 101.0541 

292.205 

132.29167 0.7659 0.9375 87.8750 81.4167 84.6458 
FLOWS 

SAMPLED VOLUME (STD. CU .FT.): 37.2671 

VOLUME OF WATER VAPOR (STD. CU .FT.): 4.1892 

FRACTIONAL MOISTURE CONTENT M; 0.1011 

DRY BASE: 79.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0000 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.8884 

STACK PRESSURE (inch Hg): 29.5713 

STACK GAS VELOCITY (ft/sec.): 62.6013 

It 

ACTUAL STACK GAS FLOW RATE (ACFM): 15492.7089 

STANDARD STACK GAS FLOW RATE (SCFH): 756409.784 

ISOKINETIC RATIO (%): 100.4018 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T 

deg F INLET OUTLET 

1 118 1.20 1.095445 1.10 

2 118 1.30 1.140175 1.20 

3 116 1.30 1.140175 1.20 

4 115 1.00 1 0.94 

5 117 0.79 0.888819 0.74 

6 117 0.57 0.754983 0.54 

7 118 1.30 1.140175 1.20 

8 117 1.30 1.140175 1.20 

9 117 1.30 1.140175 1.20 

10 115 .1. 20 1.095445 1.10 

11 114 1.10 1.048809 1.00 

12 116 0.86 0.927362 0.81 

116.5 1.0426 1.0192 

c 

75 

75 

76 

76 

77 

78 

78 

79 

79 

ao 

ao 

80 

76 

79 

sl 

82 

84 

84 

sl 

85 

85 

66 

87 

86 

83.0000 77.7500 

0 

Meter Point Point Point 

Volume VMSTD Velocity Moisture 

mis 

292.6 3.22 65.857 7.70028 

295.9 3.5038 68.5461 8.37892 

299.5 3.397 68.4274 8.12348 

303 3.004 59.9627 7.18378 

306.1 2.6 079 53.3886 6.23638 

308.8 2.2666 45.3495 5.42026 

311.15 3.4391 68.5461 8.22425 

314.7 3.3751 68.4868 8.07102 

318.2 3.3751 68.4868 8.07102 

321.7 3.2718 65.6858 7.82404 

325.1 3.0757 62.8347 7.35521 

328.3 2.7386 55.6554 6.54908 

331.148 

80.3750 

Point Iso 

99.2262 

103.7353 

100.3987 

101.1424 

98.9586 

101.2551 

101.8205 

99.8369 

99.8369 

100.5590 

98.6509 

99.5150 

EMISSiON TEST SUiYIMARY 

PLANT : Daltile. Dallas. TX 

DATE : 23-klay•07 

PLACE : Plant 2/3 Scrubber 

RUN#: I 

TEST OURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 

NOZZLE DIAMETER (1NCH.) : 0.1927 PARTICULATE WEIGHT (Front half mg) : 

METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : 

GAS METER VOL.(Cu.Ft.) : 38.548 PERCENT CO2 

BAROMETRIC PRESSURE : 29.6 PERCENT 02 

PERCENT CO 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 27.5 STACK LENGTH(inchs) : 

STACK AREA (Sq.Ft.) ; 4.124704 STACK WIDTH(inchs) : 

NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 

ENTER THE STACK AREA SHOWN ABOVE: 4.124704 

89 

0 

0 

•0.39 

1.5 

19 

0 

0 

11 
EMISSION TEST SUMMARY 

PLANT : Daltile. Daltas, TX 

DATE : 23•May07 

PLACE : PIrnt 2+'3 Scrubber 

RUN# : 2 

TEST DURATION (MINUTES) : 

NOZZLE DIAMETER (INCH.) : 

METER COEFFICIENT (Y) : 

PITOT COEFFICIENT (Cp) : 

GAS METER VOL.(Cu.Ft.) : 

BAROMETRIC PRESSURE 

60 LIQUID COLLECTED (mis) : 

0.1927 PARTICULATE WEIGHT (Front half mg) : 

0.998 PARTICULATE WEIGHT (Back half mg) : 

0.84 STATIC PRESSURE (in. 1120) : 

38.067 PERCENT CO2 

29.5 PERCENT 02 

PERCENT CO 

88.8 

0 

D 

•0.39 

1.5 

19.5 

0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 27. 51 STACK LENGTH(fnches) : 

STACK AREA (Sq.Ft.) : 4.124704 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 4.124704 

FLOwS 

SAMPLED VOLUME (STD. CU .FT.): 36.4656 

VOLUME OF WATER VAPOR (STD. CU .FT.): 4.1798 

FRACTIONAL MOISTURE CONTENT (%): 0.1028 

DRY BASE: 79.0000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0200 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.8867 

STACK PRESSURE (inch Hg): 29.5713 

STACK GAS VELOCITY (ft/sec.): 61.4595 

AC7UAL STACK GAS FLOW RATE (ACFM): 15210.1293 

STANDARD STACK GAS FLOW RATE (SCFH): 739748.969 

ISOKINETIC RATIO (%a): 100.4551 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point 

deg F INLET OUTLET Volume VMSTD Velocity Moisture 

mis 

1 119 1.20 1.095445 1.15 81 81 331.3 3.2843 65.9159 8.008531 

2 118 1.30 1.140175 1.20 86 81 334.7 3.3658 68.5482 8.207171 

3 117 1.30 1.140175 1.20 83 81 338.2 3.4556 68.4889 8.426158 

4 l i6 1.05 1.024695 1.00 89 82 341.8 2.9687 61.4987 7.23897 

5 1i7 0.82 0.905539 0.78 89 82 344.9 2.7757 54.3945 6.768248 

6 118 0.74 0.860233 0.71 88 82 347.8 2.5306 51.7178 6.170693 

7 118 1.00 1 0.96 85 83 350.442 2.9363 60.1207 7.159873 

8 119 1.20 1.095445 1.15 89 82 353.5 3.2572 65.9159 7.942466 

9 119 1.30 1.140175 1.20 91 84 356.9 3.3412 68.6074 8.14721 

10 119 1.30 1.140175 1.20 91 84 360.4 3.4366 68.6074 8.379987 

11 116 0.83 0.911043 0.79 91 84 364 2.6702 54.6777 6.51115 

12 115 0.67 0.818535 0.64 90 84 366.8 2.4493 49.0831 5.972563 

369.367 

117.58333 1.0226 0.9983 88.1667 82.5000 85.3333 

Point Iso 

101.4925 

99.8431 

102.4184 

97.8196 

103.5833 

99.4980 

99.3120 

100.6552 

99.1994 

102.0336 

98.9606 

100.9461 

- 12 
EMlSSION TEST SUMMARY 

PLANT : DaItile. Dallas. TX 

DATE : 2-3 •May07 

PLACE : Plarit 2: 3 Scrubber 

RUN#: 3 

TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 95.5 

NOZZLE DIAMETER (tNCH.) : 0.1927 PARTICULATE WEIGH7 (Front half mg) : 0 

METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0 

PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : 0.39 

GAS METER VOL.(Cu.Ft.) : 38.139 PERCENT CO2 1.5 

BAROMETRIC PRESSURE 29.6 PERCENT 02 i9 

PERCENT CO 0 

FOR CIRCULAR STACK FOR RECTANGULAR STACK 

STACK DIAMETER (inch): 27.5 STACK LENGTH(inches) : 

STACK AREA (Sq.Ft.) : 4.124704 STACK WIDTH(inches) : 

NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 0 

ENTER THE STACK AREA SHOWN ABOVE: 4.124704 

FLOwS 

SAMPLED VOLUME (STD. CU .FT.): 36.2715 

VOLUME OF WATER VAPOR (STD. CU .FT.): 4.4952 

FRACTIONAL MOISTURE CONTENT {qo}: 0.1103 

DRY BASE: 79.5000 

MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0000 

MOLECULAR WT. OF STACK GAS (WET BASE): 27.7871 

STACK PRESSURE (inch Hg): 29.5713 

STACK GAS VELOCITY (ft/sec.): 61.4159 

ACTUAL STACK +GAS FLOW RATE (ACFM): 15199.3481 

STANDARD STACK GAS FLOW RATE (SCFH): 732891.184 

ISOKINETIC RATIO (g(,): 100.8556 

POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T_ 

deR F INLET 

1 118 1.30 1.140175 1.20 85 

2 119 1.30 1.140175 1.25 90 

3 119 1.20 1.095445 1.20 92 

4 i i 6 1.10 1.048809 1.10 92 

5 116 0.81 0.9 0.79 93 

6 117 0.68 0.824621 0.66 93 

7 118 1.20 1.095445 1.20 90 

8 119 1.30 1.140175 1.30 94 

9 I i 9 1.20 1.095445 1.20 94 

10 118 0.97 0.984886 0.94 94 

11 119 0.89 0.943398 0.87 94 

12 115 0.69 0.830662 0.67 94 

117.75 1.0199 1.0317 92.0833 

n 

METER T. Meter Point Point Point Point Iso 

OUTLET Volume VMSTD Veiocity Moisture 

mis 

85 370.4 3.3565 68.671 8.849206 100.2214 

85 373.9 3.437 68.7304 9.061601 102.7156 

86 377.5 3.2368 66.034 8.533739 100.6820 

86 380.9 3.1409 63.0588 8.280695 101.7760 

86 384.2 2.6605 54.1117 7.014261 100.4649 

87 387 2.4086 49.6227 6.350099 99.3522 

87 389.538 3.2989 65.977 8.697275 102.5227 

87 393 3.3238 68.7304 8.762965 99.3304 

87 396.5 3.228 66.034 8.510486 100.4076 

87 399.9 2.9413 59.3182 7.754564 101.6715 

88 403 2.6538 56.8685 6.996553 95.8500 

88 405.8 2.5899 49.8995 6.828247 105.8723 

408.534 

86.5833 89.3333 

~ 

0.31 0.130572 

0.25 0.1053 i 

0.35 0.14742 ; 

0.23: 0.096876 

ae { 0.120042 

0.43 ~ 0.176816 

0.193264 

0.481 0.197376 

0.361 0.148032 

- 1 0.178872 

ml iLHF,_mg - CI-, uglml jHCI, mg _ 

~ - 

0-

i-- - - 0 o' - - 0 

01 0 0 ~ 0 ✓ 

 - -- - 01- -i--0 

0.42 0.176904 

0.44 0.185328 

pe 0.181116 

0.34' 0. 1 43208 

0.42 ; 0. 176904 

0.421 0.176904 

0. 51 0.2106 

3ge -r , 0.176904 

1.76 0.723712 

1.74 0.715488 

i 0.7196 

_0.45 !_0. 18504 

_0.41 i 0.168592 

0.3410.139808 

~ 0.38 j 0. 156256 

j 0.162424 

Sheet1 

Summary of HF and HCI Analys is 

Plant: ; D altile, Dailas,TX 

Date: i 5/22 - 5123/07 

--- - ~ - -- ----- ~ -_. 

~ 

-Locati

_ _on_ -

: ;Plan_t 4 Scrubber 

--, 

Run # 1Imps Volume Dilut 

1 

--- ------- 

i-1 &2 

, --- , ~ _ 400; 

400 , 

-- - - --- -- __~ ~ ----- - 

---...._-- 2 '------__ . 4001 1 ! 

- ------ - -- _ _- - -- - 

21 1 & 2 ~ 400 1 i 

._...._.__ _..~ .. .- ---- - 

2:1 &2 400 11 - - - -- - 2 :1 & 2 

4001 ----- --1_-(

- 

Aver 

3 L & 2 1 400 _ 1 i 

_._._._3 11_& 2~_400! _---1-- 

3 (1 & 2 

--- --- - --~-- ---- --~ - 

- - 3 ~~ & 2 

1-~---- 

- -- -; _ 400 i 

Aver 

. ~ Location: ; Plant 213 S crubbe r _ :.. ., ~ 

-- - - ---- 

Run # ;Imps !Volume,Dilution

-- 

 !Fl-, ~ _ _ _- -- ---,-- 

1 !1 & 2 400j 1 

1;1 & 2 

; _.. _ 

4001 

 - --- ~ ;- 

_. .. - -- - -- _ ---- 

Aver 

. .. .----- - ._ -- ---- ---__ _ - --- 

_2 i 1 &_.2______._ ~ - --400 

__.__....1 

~ 

-

2

I 1 &- 2 __. L_-- 400 1 ~ 

; ; Aver 

3+ 1& 2' 400 1 ~ __- 

3 ; 1 & 2 400i - --- 1 

_3 j 1_ & ? - -~- --.

400 1 i.. 

3 L1 &_2_.-. 4001 

~ IAver 

0.791 0.3327481 

0.561 0.235872 !! 

0.67; 0.28220411 

0.53 0.223236 

ae 1 0.2685151 

HCI, mg 

0.176816 

_ 0.16448 

0.170648 

0.58 j 0.238496 

0.54 0.222048 

-0.52 0.213824 

0.48 0.197376 

{ 0.217936 

---- ~ --- ~ -- 

1 

ion FI-, uglml j HF, mg `CI-, uglml i 

11 0.641 0.269568 0.43 1 

11 0.631 0.265356 0.4!, 

!Averaae I 0.267462 - i 

Page 1 1 14 
l .~Cl 2to.Qs 

, 

~ 00 23/. 2-1' 

o, 

318 8 236. ~ b' 

70 6'00 

~a523 ~fS.oC~ 

9-oo 

~ 

-?A's Ls 

© 

1~ 
conditions = 1.99 ug/ml. Fl-- in H2SO4 

= 2.0 ug/m.l C1-- in H2SO4 

Date » 05/25/2007 

Time - 07'-03:15 

--25 :600mV 

Component Retenti 

1. 

1.58 

F1- 

Cl- 

. 

256.00OmV 

Area Externa 

210.85 M 

119.20 M 

~ 

Compo ne nt 

Fl•- 

c i -- 

2 

Number Retention Area External Units 

1 .1 . G25 210.85 M 2.1.8 ug/ml 

2 J. . 583 119.20 NI 1 . 82 ug/m l 

330.05 4.01 

~ ~, 
Conditions : 1.99 ug/ml Fl- in H2SO4 

: 2.0 ug/ml Cl— in H2504 

Date : 05/25/2007 

T2Lme z 07:15:13 

-25.6OOmV 

COMPDnept Retenti 

256.00OmV 

ATea Eyternal 

Fl- 1. 

ci- 1.58 

2 

41 

5 

61 

~...»...»....._..... .. .. ....... . ........... . ............ . .............. ....... ..... 

206.20 M 2. 1'4` 

124.53 M 1.91 

It 

Component Number Retention Area Exter-nal Units 

Fl- 1 1.016 206.20 M 2.13 ug/ml 

ci- 2 1.583 124.53 M 1.91 ug/ml 

VA 330.73 4.04 
Conditions : H2SO4 Blank. 

Date : 05/25/2007 

Time 07:31:27 

-25.600MV 

Component Ret*eition 

256.00OmV 

.. ........... ...... .............. .. ..... .. ................. ....... ...... . .............................. . ............ .. . .. .................... .. ................... ATea External 

~ ~~..... ! 

2~.».».. : 

i 

31 

41 

0 

6'. 

................. .... ......... ............ . .... ........ . . ....... ...... .. ..... ....... .. ............ ......................................... ...... .... .. ..... .. ..... ..................... ............ 

Component Number Retention Area External Units 

0 0.00 . 0.00 

„ 18 
—25.60C}mV ' 25h.00qmV 

Component Retenti 

Fl- 1. 

C1- 1.50 

A 

Conditions : 3.98 ug/ml F1— in H2SO4 

= 4.00 ug/mI C1— in H2SO4 

Date : 05125/2007 

Time = 07 = 46 ". 42 

Area Er.ternal 

375.50 M 4.07 

231, 2a H 3.54 

Component 

F1-- 

C1.- 

2 

Number Retention 

1 1.033 

2 1.600 

Area External Units 

375.50 M 4.07 (ag/ml 

231.28 M 3.54 ug/mJ. 

606 . 78 7.61 

~, 
Conditions = 3.98 ug/ml Fl-- in H2SO4 

= 4.00 ug/ml Cl-- i n H2SO4 

Date = 05/25/2007 

Time - 07 : 4,9 - 37 

-25 . 6OOmV 

Component Retenti 

C1- 1.64 

255 .00OmV 

Area External 

382.10 M 4.15 

242.68 h1 3.74 

.Component Number Retention Area External Units 

Fl- 1 1.033 382.10 Ni 4.15 ug/ml 

Cl-- 2 1.600 242.68 M 3.70 ug/mJ. 

2 624.78 7 _ 86 

.~ . 

~ 20 
Conditions : 5.97 ug/ml Fl— in H2504 

: 6.00 ug/ail Cl— in H2SO4 

Date : 05/25/2007 

Time : 08:00:07 

—25.6OOmV 256,OOOmV 

ComponeRt Reti on 

.......... . ...... ............ ....... ...... 

Fl- 1• 

' ~• • i 

ci- 1.61 

...........

............

....... . .................. 

........... . 

21; 

j ~ ; 

41 

~ : ~ ~ 

6; - 

............. . .. . ..... ........ ...... 

Component Number Retention Area External Units 

Fl- 1 1-.033 580.70 11 6.34 ug/ml 

Cl - 2 1.616 348.33 M 5.65 ug/ml 

2 929.03 11.99 

Area bfternal 

580.70 M 6.34 

348.33 M 5.65 

21 
Conditions : 05.97 ug/ml Fl- in H2SO4 

: 6.00 ug/ml Cl- i n H2SO4 

Date : 05/25/2007 

Ti'me : 08:03:26 

-25.6OOmV 

uomponeRL ReLe 

256.000mV 

Area External 

Fl- 1. 

ci- 1.60 

l ! ';.._.. I 

..... 

0 

.. 

. .......

...... 

. .. . 

1 

........ 

.... 

2 - 

31 . . ..... 

~~ »..»_ : ~ 

6 

552.20 H 6.01 

345 .46 m 5.60 

0 

Component Number Retention Area •xternal Units 

Fl- 1 1.033 552.20 M 6.01 tig/ml 

ci- 2 1..660 345-06 M 5.60 ug/ml 

2 897.26 11-61 

24 
23 

2 1219.75 15 .97 

Conditions = 7_96 ug/ml F1- in H2SO4 

= 8.00 ug/m i C I-- i n F12SQ4 

Date = 05/25/2007 

T.i.tne = 08 :12 : 17 

Component 

F1-- 

c i -- 

hlumber Retention Area 

1 1.016 774.55 

2 1.616 445,20 

External Units 

8.18 ug/m l 

7.80 ug/m l 

F1- 

ci1. 

1.6] 

--25 . 6pOmV 256 . OOOmV 

Camponent Re'Lention Area External 

774.55 

445.20 

= ~ ' 

, 

8.18 

7.80 
Conc{itions : 7.96 ug/m3. F1— in H2SO4 

: 8.00 ug/m 1 C 1-- i n H2SO4 

Date = 05/25/2007 

3"ime = 08-.14-=55 

—25.6OOmV 25b.00UmV 

Conpanept Retentian Area Eztei- nal 

FlC1- 

l. 

I.64 

162,54 8.45 

434 .42 h! 7.60 

Component Number Retention Area External Units 

F1— 1 1.016 762.50 8.05 ug/ml 

c I '_ 2 1.600 4:34 ., 42 M - 7.60 ug/ml 

2 114b . g2 15.65 

Y ' 24 
AMC3UNT INJECTED 

AREA 0.000 

o . OaC 

768.525 

7.960 

1 

2 

3 

4 

5 s 

Calibration file = F1--.cal 

Avg slope of curve = 96.55 

Y-ax a. s i ntercep t= 0.00 

Coeff of 1. i. n regr - 0.92 

No. Area Amourit CF 

0: 0.000 0.000 0.000 

1 : 208 . 525 1.990 104 . 786* 

2: 378.800 3.980 95.176 

3: 566.450 5.970 94.883 

4" 768.525 7.960 96.548 

~ y •~ ~ ~ 
AMf,3Uh4T INJECTEQ 

AREA 0.000 

0.000 

439.810 

M ~ 

1 

~M, 

3 

4- 

5 

Calibration f i ie = Cl- .ca l 

Avg s:lope of curwe - 54.98 

Y-ax i si ntercept = 0.00 

Coeff of J.in rc:gr : 0.90 

No . A•rea Amaunt CF 

0: 0.000 0.000 0.000 

1= 121.865 2.000 60.932 

2-' 236.980 4.000 59.245 

3= 346 k b95 6.000 57.782 

4: 439,810 8.000 54 ,.976 

_ 26 
--25 .600mV 256.00OmV 

Componer.t Reten . 

unknown) 4. 

unknown) o. 

Area Ey.tQrna] 

34,74 N/A. 

32.55 M N/P, 

67:50 M 0,64 

25.90 h4 4.43 

Corsditions = Dalfi.i.Le , Dallas sTX Plant 4• Scrubber 

= Run #1 Tmps 1&2 

= volume 400 Dilution 1/1 

Date = 05/25/2007 

Time = 08 = 31 - 4-6 

Component Number Retention Area External Units 

( u n know n) 0 0.483 34.70 N/A 

( unknown ) O 0 .8 50 32 .:.~ 5 M !~!/ p; 

= 1-- 1 ~. .016 h7' . 50 ~i 0.64 ug/m1 

r.l-- 2 1.616 25.90 M 0.43 tic/m.l_ 

4 160.651 .G7 

r ' 27 
--25 .600mV 

Conpanent * itetentian 

(unknawn) o.s 

F1- 1. 

C1- 1.6 

Area External 

34.20 N/A 

66.15 M 4.63 

24.60 M 0.40 

, 

25b.000mV 

Conditions = Daltile, Dallas, TX Plant 4 Scrubber 

: Run #1 ImPs 18:2 

= Volume 400 Diluti on 1/1 

Date = 05/25/2007 

Time = 08 = 4,0 = 53 

ComPonent 

( E.1nItT1Wvv1"t ) 

F1__ 

D Iw. 

3 

Number Retentian Area External Units 

0 0.850 34.20 N/fi 

.3. .1 .(33 3 66.15 M 0.63 ug/m .!w 

? 1.650 24 .6d 11 n. 40 ug/ml 

124.95 1.04 

i 
25.00 H N/A 

82.60 « 0.75 

35.15 H 0.56 

n 

Co nditions : Daltile, Dallas, TX Plant 4 Scrubber 

= Run #2 Imps 1&2 

: Volume 400 Dilution 1/1 

Date : 05/25/2007 

Time - 08.49=40 

--25 .600mV 256 .00OmV 

Component Rptention • 4rea External 

(unknown) 0. 

F1- 1.16 

C1- 1.66 

m 

_._-.._ ....... _ ..... ................... ----------- ~ 

6 

6 

2 

~ 

. ; . ; 

, • ~ 

4 

• ; . i 

6 . .... 

. ~ ~ : ! 

~ ._..........__._.._:_.. . , .._ ....__ ...._._..._._.--_....._..._-_ _:---._ .._..__._-._.. -.__..._......_....._.._..--.. ..._.. ........ .. ... ..... ........... - ..... .... .._..._. ..~ 

Component Nutmber Retention AreaE External Units 

( u nknown ) 0 0.883 25.00 11 N%A 

F J.— 1 1 -166 82.60 M 0.79 ug/ml. 

Cl— 2 1.666 35 .1.5 iH 0.58 ug/ml 

3 142.75 1.37 

2 S 
Conditions = Daltile, Dallas, Tn Plant 4 Scrubber 

= Run #2 Imps 1&2 

= Volume 400 Dilution 1/1 

Qa.te. = 05/25/2007 

Time - 08:52=09 

— 25..600mV 2-56 .00OmV 

Componeat Reten'' 

(unknokn) 0. 

(unknown) 

FIC1- 

4. 

1. 

~ . 

Area External 

13.00 NiA 

48.20 M NiA 

58.20 M 0.55 

32.65 M 0.54 

Component 

( unknown ) 

( unl<nown ) 

F l -- r_ ]. 

Number P.etention 

0 0.133 

0 0 .e83 

1 1.150 

2 1.633 

Area External Units 

13.00 N / A 

48.20 M i•!/A 

58.20 lvI 0.56 ug/m 1 

32 _65 M 0.54 ug/m 1 

4 152.05 1.04 

© 

JQ 
Conditions : Daltile, Dallas, TX Plant 4 Scrubber 

: Run #2 Imps 1&2 

: Volume 400 Dilution 1/1 

Date : 05/25/2007 

Time : 09:00:49 

-25.600mV 256.00ORiV 

Component ReLention Area Eyternal 

0. 

Fl 

ci 1 65 

.......... i . . ............................................. . ................... . . .... . . ...... ........................................... . ......... ................... . 

0 

ol 

2

r.».... ; 

! 

3j ....... 

4 ........ 

61 

............ .... ........................... ... .......................... . . . . . . . ..... ......... ........................... . .......... ................. .... ... ..... ...... .................. ..................................... 

32.20 N/A 

70.20 14 0.67 

31.58 K 0.52 

Number Retention Area External Units 

0 0.866 32.20 N/A 

1 • 1.150 70.20 lvi 0.67 Ug/M.I. 

2 1.650 31.58 11 O~ 52 ug/ml 

133.98 1.19 

Component 

(unknown) 

Fl— 

CI — 

3 

31 
~

unknown ~ 0. 

iiDknown 1.2 

C1- 1.5 

62.40 

11.70 14 

: 28.95 M 

. , 

N/R 

N!A 

0.48 

0©nditions -- Daltile, Dallas, TX Plant 4 Scrubber 

= P.un #? Imps 1&2 

: Volume 400 Dilution 1/1 

Date :. 05/25/2007 

Time - 09-03-21 

—25 . bOOmU 256 . OOOmV 

Component ReLeniion Rrea External 

Number Retention Area External units 

0 62.40 N/A 

1 1.15055 . ?5 11 0.53 ua/m.l. 

Q 1.25611..7O M N/ A 

2 1.650 28.95 11 O.. {•S Lt9/m:l 

158 _ 4 0 1.00 

CarnponAnt 

( unl:riown ) 

F I - 

( unknown ) 

Ci— 

4 

34, ~~ , 
N/A 

0.31 

N/P 

0.43 

0. 

1. 

1.: 

1. ~ 

--25 . 600mV 

ComponeRt Reten'' 

(unknown) 0. 

(unknown) 

F1- 

(unknown) 

Cl256.00OmV 

Area External 

10.00 II/A 

20.05 

32.35 

28.10 

26.20 N 

Conditions = Daltile, Dallas, TX Plant 4 Scrubber 

- Pu n #3 Irinps I &2 

= Volume 400 Dilution 1/1 

Date : 05/25/2007 

Time = 09 :13. : 53 

Component Number Retenta.o.n Area External Units 

( unknown ) 0 0.083 3.o .00 nI/A 

( u n k now n) 0 0.850 20.05 N/A 

F'l— 2 1.033 3.2 .35 0.31 u.9/mI 

( u r ~ k. r ~ s.~ w n) i) 1.250 28.10 Iw! r A 

Cl -- 2 1.633 26 _20 P1 0.4.3 ug/mJ. 

5 116.70 0.74 

~ 
Component 

(unknown) 

(unknawn) 

F1 - 

( unknawn ) 

C1- 

—25.600mV 

Reten ~ ion 

0.3 

1,2 

1.5 

Area Externa ► 

33.90 N/A 

22.50 H Nra 

26.20 H 0.25 

41.50 M NrA 

28.80 N 0.47 

256.00OmV 

Conditions : Daltile, Dallas, TX Plant 4 5crubber 

: Run #3 Irnps 1&2 

= Volume 400 Dilution 1/1 

Date = 05/25/2007 

Time = 09= 14=56 

Component Number Retention Area External Units 

( unknovin ) 0 0.366 33.90 N/A 

( u n f<now n) n 0.850 22.50 h1 N/A 

F1— 1 1.033 26.20 111 0.25 ug/ml 

( u n know n) 0 1.250 41.50 M N/A 

C].— 2 1. 63? 28.80 Mi 0.4.7 ug/ml_ 

5 152 . 90 0.72 

.14 
Conditions : Daltile,,Da 

' 

Ilas, TX Plant 4 Scrubber 

: Run #3 Imps 1&2 

: V61ume •00 Dilution 1/1 

Date : 05/25/2007 

Time : 09:23:39 

(unknown) 0 

Fl- I 

(uflknown) I 

ci• I 

-25.6.00mV 256.00OmV 

OMPOneRL l(etf ATea ExterDal 

21.75 N/A 

36.35 0.35 

24.90 N/A 

29.30 H 0.48 

ld 

.on . ............ . . ... 

. ...... 

0 

oi 

4 ..... ~ : 

~ . i 

6 . ....... 

................... . I ................ . . ......... ............................. ....... ......... . ............... . ......... . 

Area External Units 

21..75 N/A 

36.35 0.35 ug/ml 

24.90 N/A 

29.30 M 0.48 ug`/ml 

112.30 0.83 

Component Number Retention 

(unknown) 0 0..850 

Fl- 1 1.050 

(unknown) 0 1.250 

ci- 2 1.650 

4 
Area 

33.55 

23.60 

40.00 

22.05 N! 

Externa? 

; NlA ; i 

0.23 ' 

NlA 

0.36 i 

Conditions : Daltile, Oailas, TX Plartt 4 Scrubber 

: Run #3 Imps 1C*X2 

: Volume 400,Dilution 1/1 

Date = 05/25/2007 

Time : 09:26=38 , 

--25 . e00mV 256 .00OmV 

Component Retention 

(unknown) 0.4 

F'1- 1. 

( unknoin ) 1.2 

cl- 1.6 

t 

,........._......._....~ _._....»..__......___.._.................___..._._._»__....._...._..._.._.._.__..._............._......._.._.._.............._..._._._.__._._......_.._._....._.._......_... 

,:. 16 

50 : ;_" ~ ~~ • ,.~ 

33 

• ~ . ; 

; • _ 

3~........ : 

4` 

• ~ ~ 

1 • t ~ . . ; 

! : ~ f • ~ ~ ~ • ; 

61

...,..... 

I.».............»._ _...»........._.__.._ ....... ...... ._. ................................................ ». ........ ....._.._.......................».._......._........_..._......._._........__..._.._ _. ».__.._............... . ~ 

Number Retention 

0 0.416 

(3 0.866 

1 1.033 

0 1.250 

2 1.633 

Area. External Units 

33.55 Ni/A 

20.45 N/A 

23 » 60 0.23 ug/m l - 

40.00N/A 

22.05 M 0.36 ug/ml 

139 .d5 0.59 

Component 

( unknown ) ' 

(ur known) 

Fl- 

( unknown ) 

ci-- 

5 

49

. ar 
Conditions z Daltile sDa11as , TX Plant 2!3 rcrubber 

: Run #S - Imps 1&2 

: Volume 400 Di.].ution 1/1 

Date : 05f2512007 

Time = 09 : 46 : 55 

—25 . 640m'J 256 . U4OmV 

Component Retention Area Extern4l 

Cornponent 

~ unk'novin ~ 

( uri known ) 

2 

Number Retention Area Extcrnal. Unitw 

0 0 . 866 10.40 N/A 

a 1 . 25d 48.85 N/A 

59.25 0.00 

~

unknoEan} 4. 

ll1l ~~ i10 4~ 11 ) 1. 

la 

10.40 N!A 

48.85 NlA 
Conditions : Daltile, Dallas, Tn Plant 2/3 Scrubber 

= Run #1 Imps 1&2 

= Volume 400 Di lution 1/1 

Date = 05/25/2007 

Tirne : '09-49-57 

--25 . b00mV 

Component Ratent' 

( unkrown ) 0.3 

(unknown) 0.8 

(unknowfl 1.2 

256..00OmV 

ion I_.~........._.....» ; ...~.»._»......._._...__...»»...._»..._w...._.............._..._._.._._..». ~........_..._.»»_......._........_._.........._....._...._.._..»...._....._.....».._.»._...»....»_,.._. : •} ~ 

83~ ~•. ~ 

50 ,`1 1. ...... i;~ 50 ry ~:••!: ~ • 

:• ~ 

~ 

~ ~' ..... . : ~ ~• • I 

~ ~ • I 

i • I 

, . , 

s

........ : I 

: ! 

4 

: • ~ 5l....... : ~ ~ 

i ~ # . ; 

6 

 , ...... ; . 

( ~ i 

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Rrea Externa] 

34.°0 H/R 

17.90 NIR 

29.25 N N/fi 

Number Retention Rrea External Units 

0 0.383 34.90 N!l•a 

0 0.8501,7.90 N/A 

0 1.2-15 C) 29 . 2 5 Ni N /A. 

82.05 0.00 

Companent 

( unknown ) 

unknown ) 

!inknown ) 

3 

, 

J~ •.~ ~ 
Area External 

44.50 0.42 

30.70 NIP. 

107.20 H 1.76 

Fl- 1. 

(Upholn ) , 1.2 

ci- 13 

Conditions : Daltile, Dallas, TX Plant 2/3 Scrubber 

: Run #2 imps 1&,2 

: Volume 400 Dilution 1/1 

Date : 05/25/2007 

Time : 09:58:44 

-25.6OOmV 256,OOOmV 

GOMPODent Pi-etent 

........ ......... ............. .. .............. ........... . .................... ...... .......... ................................. ....................... .. ............................. ........... ............ ...... 

so 

50 

21 . ....... 

........... ............... . .... ...... . ................. .... ..................... ............. .. ......... ....... .... ................ . ........................ 

31 

4 

 . »»» ; ~ 

6 .... 

: 

 . . ................ ........ ................. . ..... . ....... . ...... ...... . . . ...... ..................... ............ ... 

Component 

( u..n 1- now n 

Fl- 

( Ll 71 k now n 

c 1 — 

Ei 

Number Re•tention Ai-ea 

0 0.866 11.75 

1 1.033 44.50 

0 1.250 30..70 

2 1.650 107.20 M 

194.15 

External Units. 

N/A 

0.4-2 ug/ml 

IN! / A 

1.76 ug / rri 1 

2-18 
NIA 

0.44 

N!A 

1.74 

Component Retenti 

(unknown) 0.85 rl` k . 

(unknown) 1.23 

C1- 1.63 

Area External 

15.70 

46.50 

24.80 

106.30 N 

Conditions : Daltile, Dallas, TX-Plant 2/3 Scrubber 

: Run #2 Imps 1&2 

: Volume 400 Dilution -1/1. 

Date : 05/25.l2007 

Time : 10=10-41 

--25 .60OmV 256 .00OmV 

Component 

( unknown ) 

FI - 

( un{;nown ) 

f"; ] - 

Number Retention 

n 0.850 

1 :1.,033 

0 1.233 

?_ 1.633 

Area External Units 

15.70 N/A 

41.6 .50 () .,441. u rn.l. 

24.80 Iq/A 

1.06.30 M 1.74 ug/m:l 

4 193.30 2.19 

9 40 
Conditions : Daltile., Dallas, TX Plant 2/3 Scrubber 

: Run #3 Imps.1&2' 

: Volume 4.00 Dilution 1/1 

Date : 05/25/2007 

Time : 10:19:24 

-25.6OOmV 256.00OmV 

Component Retent 

(uuknown) 0.8 

(unknown) 1.2 

ci- 1.6 

Area External 

36.70 NIP 

13.70 M NI A. 

27.50 P, 0.45 

ion 

........ .. ............... ...................... .......... ................... ........ ......... .......... .. ..... .. .......... ..... .. ... ............. .. .......... 

I 

50 :? 

16 

».. ~ •I•.~~~ ~ 2 

3 ....... 

4 

I : t ~ ~ 

51 

.................. 

Component Number Retention Area Exteri-ial Unit-s 

(uriknown) 0 0.850 36.70 N/A 

Fl- 1 1.166 35.30 M 0.34 ug/rnl 

( ui-il-no vi-i-i 0 1.250 13.70 Ivi N / A. 

ci-- 2 1. .616 27.50 Ivi 0.45 ug/ml 

4 113.20 0-79 
Area External Units 

18.00i !,~ ~ 

42.50 N/A 

43.55 ' M 0.42 ug/ml 

25.00 M 0.41 ug/rn .l. 

129.05 0.83 

Number Retention 

0 0.166 

0r~ V .\✓ b ',! 

 .y. 1 . 150 

2 1.600 

Com¢onent 

( unknown ) 

(unknown) 

F1— 

c t — 

4 

Conditions `- Daltile, Dallas, TX Plant 2/3 5crubber 

z Run #3 Imps 1&2 

: Volume 400 DiZution 1.t1. 

Dete = 05/25/2007 

Tirne = 10=22=40 

~ 

, --25 . b00mV 256 . OOOmU 

Component Reten" 

( unknown ) 0. 

(unknown) 0. 

F1- 1. 

ci- 1. 

Rrea External 

18.00 Nra 

42.50 NlA 

43,55 M 0.42 

25.00 M 0.41 

s 

.~ ~ ~ 
Conditions Daltile, Dallas, TX Plant 2/3 Scrubber 

Run #3 imps 1&2 

Volume 400 Dilution 1/1 

Date = 05/25/2007 

Time = 10:31:30 

-25.600mV 256.00OMV 

Componerit Reteition Area External 

( unknown-) 0. 

Fl- 1.1 

ci- 1.6 

. ................................ ..................... . .... w ........................ . .............................................................................................................. ........ ......... 

66 

50 1' 

21 

J~ . ..... : 

~ 

4 

61 ~ ; ~ 

................... ..................... . ......... ........................................ ................... ....... ........ ............ .... .. .................................. ................ .............. . ....... ............ . .......... 

41.65 il/A 

43.60 K 0,42 

20.50 M 0.34 

Number Retention 

0 0.8,66 

1 1.1.66 

2 1.650 

Area External tinits 

4 1. .65 N/A 

.1. 3.60 m 0.42 ug/ml 

20.50 M 0.34 ug/ml 

105.75 0.75 

. Component 

(unkriown) 

F.1 — 

ci3 
Conditions = Daltile, Da11as,'TX Plant 2/3 Scrubber 

= Run #3 Imps 1&2 

= Volume 400 Dzlution 1./1 

Date = 65/25/2007 

Time = 10-34=03 

-25.600mV 256.00OmV 

Componen~ Retenti 

(unknot~ n) 0.19 

( iinknown ) 0. 

F1- i .lb 

C1- 1.5c 

t 

Component Number Retention Area External Units 

~ unknown ) 0 0.116 12 M80 N/A 

( unknown ) 0 0.866 52.20 N/A 

F1- 1 1.166 52.00 11 0.50 ug/m1 

r1 ~- 2 1_650 23.35 11 0.38 ug/m]. 

0 140.35 0.88 

firea External 

12.80 N/A 

52.20 NJA 

52.00 M 0.50 

23.35 M 0.?6 

44 
1. 

1. 

1. 

1. 

F1- 

( unknown ) 

ci° 

(unknowrn) 

GOmpOSlent fteCei1 

(unknown) 0.. 

Area External 

21.50 N/A 

364.40 H 

39.80 ri 

239.02 M 

22.07 14 

3,81 

NiA 

4.04 

N/A 

Conditions = 3.98 ug/ml F1- in H2SO4 

= 4.6 ug/m 1 C 1'-- i n H2SO4 

Date = 05/25/2007 

Time = 11=09=37 

-25.b00mV 25G .00OmV 

Component 

( unknown ) 

(unknown) 

F1 

( unknown ~ ci— 

( unkn©wn ) 

b 

Number Retention Area External Units 

0 0.050 21.50 N/A 

0 0.866 69.45 N/A 

1 1.016 364.40 M 3.81 ug/ml 

n 1_ 233 39.80 M N/A 

2 i. .56b 239.02 11 4.04 ug/m:f. 

0 1.91622.07 11 N/ A 

756.24 7 _ F5 

~.~ ~ 
Conditions = H2504 Slank 

Date = 05/25/2007 

Time = 11=06'-53 

—25 , 600mV 

Conponent. RQtentioh' 

256 .00OmV 

Area External 

Nnknown) 0. 

(un k nown) 1.26 

(unknown) 1.93. 

.._ti..._ i,. ._.._._._._._._.. ~ _....._..__.._._.._.___._..._._........_._._.M._.___...._... ~.............M_.... ~__....__..__._...._._._._._.._...... ~......._._._ ~._.._...... ~_ 

:I 

i r 

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1 ~ ' 

31 ...... 

i . 

~ 

; . 

: • 

5 (_.._.. ; - t 

. • ~ ~ i • . ' 

I : . 

79.50 N/A 

55.85 M N/A 

94.30. M N/A 

ComQonent Numher Retention Area External Units 

; unE:nown ) 0 0.866 79.50 N/ ~1 -

~- u n k now n) 0 1.266 55.85 M N/A 

( un known ) 0 1.933 94.30 Nf N/A 

3 229.65 0. 00 

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PHONE NO ~ Armstrong Environmental, Inc. (21 jj ),6 ,3 -1-002 -1. 

1748 Hlavek Rd 

Decatur, TX 76234 

CHAIN OF CUSTODY RECORD 

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Chloride Standtard 

Comno.nent ' Concentration 

(mg/Lj . 

' -Chloride 999 -4- 4 

The .concentration i value is based on proven - r.eliable methods of analysis. The estimated 

uncertainties are two standard'deviations of the concentration:values. The concentration value is 

warranted to be stable for three months - from the date of shipment. 

 •• . t 

The preparation and analyses of the Chloride Standard was performed with extreme care by the 

D?ONEX Corporation Consumables Manufacturir.g Department. 

Document No. 034 ) 84-2 4a 20'v;ay 1998 

tiicnax Carporation Dionox U.S. Regianal 0!Ilcas 

228 7ftan 14r,. 3•ain;ywe, Ck (4G)131•:522 

i3or. 3G03 Y.~ smcrd. L (G3Y) 185•35:0 

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;(! c5•3S03 !;!1wt'r.. Gk (770) {3?•8t,r,3 

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5a't l.tb! CY;. UT (801) O12•9252 

dianex lnlernatianal Suhsidiariec 

~us!riziGl)G1G ~i2: f•eR•,am•{C5i2G)5?t-0 

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:. 

, t r .r,,: , r , :, •r' t _I`at T ~ onal lnstitute :of ~tandards .&: Technolo ~G ST' Standard Refer nc M n,. e e= ate 1 SRM a -gY ~~ )~ 

,•..` ~ - _ 

y :3183 (Fluonde ~tandard Sblution) . ,~ KThe actual; concentration alue ~ v ~1 ermin et ed `:for 

, 

com

p 

onent ~ ori: is :listed below ` t .. ~:. - t :~ t t:; • _ 

• _ t~ ' ~' ~ - . 

' '• _ . . . . ' ; - 

. - . Fluorid'e.Standard 

Component Concentration 

~mg~~ 

Fluoride 995 f 2 

The concentration value is based. on ,proven , reliable . methods of analysis. The .estimated 

uncertainties are two standard •deviatioris of the concentration values. The conceritration value is 

warranted to be stable for three months from the date of shipment. 

The preparation and analyses of the Fluoride Standard was performed with extreme care by• 

DIONEX Corporation Consumables Manufacturing Department. 

Jocu:neni No. 0341 83• 15 13-Dec-02 

50 

ionex Carporation Dloaex U.S. Hegional Dltiees 

'.2E T:tan Y,'r}' SunT~ti2,t, Cl~ (403) 737•8:21 

4 Box 3y03 Y:es:mor4. IL (63017E9•355C 

'•r•ti'alt, CA. Hodnt:rt. iX (2E1)847•35:i2 

)86-353'e At1t,•~a, GR ;770) 432-610D 

81 ?37-07C9 r+Szrtton, A,! (856)59a-M 

Sa! laDr '.it• t!7 (8?1)972•9292 

Dionexlnternational SoDsidiaries 

Auilrir (01) 616 5125 Ge mter(t5125) 831-0 

n-qliu'n 41130, 42 94 trah•IR:) &Fi 51 t,fi;>? 

C=L- (8D5) 844-SE50 J4~n (O6) 698: 1213 

Cnr'as (852) 2426 3282 Koiea (2) 265: -25E,1 

r7:.7rtN.•k (45) 3C 35 93 90 Tf19 A~.rlhC/' JdS (0151) 43 0 G3 

Fxu co1) 39 3D o110 Sa~ffCrttd (Oo2) 205 9: 65 

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LPN 031318•031DAS 3{9d 

® 2004 Otmu Coeporztion 

- FXELD DATA 

PLANT: ' ~ 

DATE: ~ 2~t3 ~' 

REPETITIO : ~ 

LOCATION (SOURCE n): Plemot-t ~ ~C'(,Wbbt 'r 

OPERATOR: j2--r (,S r 

SAIvIPLE TR.,6 IN : 

METER BOX 

BA.ROMETRIC PRESSURE: 

4M0IENT TEMPERATURE: 1S;0 

ASSUMED MOISTTJ-RE:1 7 

PROBE LENGTH: ,$ib' 

NOZZLE DL4METER: . ?~•~ 3 

STACK DYAMETER: 

METER H: /. yI y 

C FACTOR: . T q 

METER CO-EFFTCLENT: 

FILTER TARE: ~ 

PRE-TEST LEAK CHECK j 

Meter: 0 4~6 cu ft. @ 1 ~{ in. HG 

p;t„te. ~i n .s~• ~ ;., u,)n 

~ IMPm GERS 

Initial Fin,al 

~ ~ I ! ~ > ~s •! ~•~'y GG~ 

~ ,• 42 l w ~ 

94 

V .U ' ~ 

n3 

' 01 6 -one- 

~. 

C C1_ 02 

3 1 g 

POST-TEST LEAK CHECK 

Meter: b, p0'O cu.ft. @0' iiL. izCr 

Pitnts' ✓~ (a~ ~ ` in_ H2C~ 

S 

La • t 

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S =30 3 13 ?3 

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PLANT: aa I.A'!e 

FIELD DATA 

PATE: 

iZEPETITIIYN : 2.- 

LOCATION (SOURCE ~): ~~`~ ~j ~ ~'''~~i

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OPERATOR: P.4" E S 

SF,NiPLE TR.AIN r: 1 71, 

METER BOX ~ : ! a 

BAROMETRIC PRESSURE: Lj.r-' 

AMB IENT TEMPER.A.TURE : * ° 

ASSUMED MOISTURE: 1 -3L 

PROBE LENGTH: 5'v 

NOZZLE DL4METER: . ZL4 73 

STACK DIA,METER:; L 

METER H: !. ql V 

C FACTOR: , a ul 

METER CO-EFIi'ICIENT: . 7 -7S 

FILTER TARE: -- 

PRE-TEST LEAK CHECK 

IMPINGERS 

Initial 

.u I 

rr3 

#4 

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197- 

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scrjb~)Gr 

PLAWIT: Dfe) ~J 

D,kTF-: 5 12, 2- 

REPETITIO N: 3 

LOCA,TION (SQ9RCE, 

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METF-R BOX 'rr:) 

BA-ROMETRIC PRESSURE: 

A]vM MNT TENPERATURE: 

ASSUIvMD MOISTURE: I 

PROBE LENGTH. 6-0 

NOZZLE DIAM-ETER: 

STACK DIA-ME-TER,

. 3 

 

METER El: 1 . q 

C FACTOR: 46 

METER CO-EFFICEENT.. 

FU,TER TARE: 

PRE-TEST LEAK CELECK 

Meter: ~ . 000 ca-ft W ?- in. HG 

Pitots: t, A.e (&, '5; 1 ,, in. H20 

rWRiGERS 

Initial Final 

Jrr-'l 100 'z I f 

-42 00 (L3 

cr 44 

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CO2 02 

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Meter. 0• OV-1 cu. ft. in. HG 

Pitots: (a, in. k20 

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DATE:,S'"/?J 

REPETI T iUN' ( , 

LOCATION (SOURCE ~): {(•~ L ~3 Sc.*~~'~ 

OPERATOR: K;rSAMPLE TRA.IN 

METER BOX ~: l0 

BAROMETRTC PRESSURE:Z J.~ 

AMBIENT TEMPERATURE: 

ASSUMED MOISTURE: 

PROBE LENGTH: 3 

NOZZLE DLANIETER: , 

STACK DLAMETER: 7, 17. ~(~•.`r 

METER H: 1. `!~ `! ~ n~ ~ ~t ' 

C FACTOR: . $ 4 

h7ETER CO-EF'FICIENT: . `j g$ 

FILTER TARE: f J 

PRE-TEST LEAK CHECK 

Meter:~ a Qrcu.ft. a~ t""in. HG 

Pitots- (a 4 in H?_0 

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rri 

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Meter: 0,00 0 cu.ft. in. HG 

in_ H2O 

 FIELD DATA 

PLAI~TT: ,~~ ~~{ 

DATE: 

REPETITION: ? 

LOCAiION (SOURCE u): fjbJ p- j 

OPERATOR: ~T rr- F S 

SAMPLE TRAIN 

METER BOX a. -•~e u 

B:4.ROI12ETRIC PRESSURE: If1 • r ~ 

A1vIBIENT TEMPERATURE: ~° & 

ASSUMED MOISTURE: J n 

PROBE LENGTH:' 3 5— 

NOZZLE DZAMETER:. 

STACK DrAMETER:?,'~ 4 

. 

ME T ER H: f.Y/ y 

C FACTOR: . I1 ~ 

METER CO-EFFICI'ENT: 

FILTER TARE: -- 

PRE-TEST LEAK CHECK 

Meter: o. o 00 cu.ft. @! z- in. HG 

Pitntc• '!~ tnl ~ -/ in T-T')O 

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#2 L!! 

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!. ; " 1 15 

POST-TEST LEAK CHECK 

Meter: p . o4X7.u.ft. @ j5r izL HG 

Pitats- 'f .. n Z •l inTd7n 

Fr—ELD DATA 

PLANT: A l ~l t 

DATE: S"~L3m 

REPETTTTON: 3 

LocATrOU (SOTJRCE #): 

OPERATOR: ,tt~T— 7-Pt f'S 

SAMPLE TRAIN #: IL 

IviETER BOX #: I o 

BAROl TETRTC PRESSURE: Ll . t 

AMl3IENT TENI'PERATURE: ~ 

ASSVMED MOIszURE:10 

PROBB LENGTH: 3r 

NOZZLE DIANETER: . I I z ~' 

STACK DLA.ME R: 

METER H: 1.'117 

C FACTOR: , a4 

METER CO=EFF'IC7ENT:. 

FII,TER TARE: " 

PRE-TEST LEAK CHECK 

Meter: O. 000 cu.ft. [a~ 1~ in. HG 

Pi.tots: ✓ ~u, ~', in. H20 

~ 

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z 1 
App~endisx' D 
APE Armslrong Environrrnenial Inc. CONVERSION FACTORS 

EPA Melhod 5 

522 SerPes Meter Box Calibralion i mtn Hg = 0.13330 kPa 

Pre-Test Orifice Method 1 cm - 0.39370 inch 

Encilish Meter Box Units, English K' Factor 1 mm = 0.03937 inch 

r i cu 11 = 28.32 lilers 

Box t, 10 Date: ---------------- -- ------- ? 02109/07 

><: 30272 Barontclric Pressure: ----------> 29.35 (in. Hg) - 

Theorelical Critical Vacuurn: --> 13.84 (in. Hg) 

RTAh For valid lesl resulls, flhe Acltral Vacutrrn should be 1 to 2 in. Hg grealer than Ihe Theoretical Critical Vacuunt shown above. 

RTAI\ The Crilical Orifice Coefficienl, IC, musl be entered in English uttils, (ft) 13'(deg R)10.5!((in.Hg)'(min)). 

~ 

---------------- DRY GAS METER READINGS --------- ------ -CRITICAL ORIFICE READINGS- 

-- Average Tentperatures -- 

Voltrrne Volume Volume lnitial Ternps, Final Ternps. Orirrce K' OriGce Actual -- Ambiorc! Temperature -- DGM DGM Ambienl 

i Tinic Inilial Finat Tolal In1e( Outlet Inlet Outiet Seriall! Coefficient Vacuum htilial Fina1 Average Outlet Overali Temp 

O) (rnin) (ctr (l) (cu (l) (ctr fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.24 5.00 475.500 477.062 1.562 62.0 61.0 62.0 62.0 40 0.242 22.0 61.0 61.0 61.0 521.5 521.8 521.0 

0.49 6.00 477.800 480.490 2.690 62.0 62.0 64.0 63.0 48 0.344 20.5 61.0 f 62.0 61.5 522.5 522.8 521.5 

0.90 8.00 481.300 486.132 4.832 64.0 63.0 65.0 63.0 55 0.464 19.0 63.0 63.0 63.0 523.0 523.8 523.0 

1_50 5.00 486.800 490.670 3.870 65.0 64.0 66.0 64.0 63 0.593 17.0 63.0 63.0 63.0 524.0 524.8 523.0 

2.90 5.00 491.900 497.218 5.318 65.0 64.0 66.0 64.0 73 0.824 14.5 63.0 63.0 63.0 524.0 524.8 523.0 

........................................... 

RESULTS 

 ................................................... 

Y GAS f11L=TER -- --------- ORIFICE -------- -- DRY GAS METER -- ------- ORIFICE ------- 

vIL VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR CALIBRATION FACTOR 

ECT COf2P.ECTED CORRECT CORRECT NOMINAL Y dH@ 

(std) Vm(sk!) Vcr(std) Vcr(std) Vcr Valuc Varialiort Valuo Variation 

:u (1) (liters) (cu (t) (liters) (cu fl) (number) (nurnber) (in H20) (in H20) 

_551 0.1 1.558 0.1 1.568 1.004 0.007 1.381 -0.0330 ' 

667 0.1 2.655 0.1 2.674 0.995 -0.002 1.395 -0.019 

.787 0.2 4.763 0.2 4.811 0.995 -0.003 1.414 0.000 

.833 0.2 3.808 0.1 3.847 0.994 -0.004 1.438 0.024 

285 0.2 5.286 0.2 5.340 1.000 0.003 1.442 0.028 

Average Y ------- > 0.998 1.414 <------- Average dH@ 

For Calihralion Faclor Y. tlie ralio of the readirtg of the calibration meler to lhe dry gas meter, 

r.eptable tolerance of individtral values from the average is +-0.02. 

•r Orificr. C:+libralion Faclor dH@, ttie orifice differential pressure in inches of H201he1 equales to 0.75 cfni ol air 

68 F and 29.92 inchea of Hg,_a,cceptable loleranc.rof individual value ~s from the average is +-0.2. 

S3t E D Ic ! : ~ 

 

Date: 

:,31 

C-..1 
Temperature Nleter Calibrations 

Meter Box #: 10 

Date: 02/09/07 

Calibrated By: RT 

Emtech 42312 

Degrees F Calibrator Probe Stack Oven Exit Auxillary 

Point 1 32 31 32 32 31 31 

Point 2 212 211 212 213 211 211 

Point 3 752 752 752 752 751 752 

Cmtech 42312 

Degrees R Caiibrator Probe Stack Oven Exit AuxilEary 

Point 1 ~ 

.. 

S492 491 492 492 

~ 

` 491 ~ 491 

Point 2 o72 671 672 673 671 671 

Point 3 1212 1212 1212 1212 1211 1212 

Percent Dir'ference 

Probe Stack Oven Exit Auxillary 

Point 1 0.203252 0 0 0.203252 0.203252 

Point 2 0.14881 0 0.148588 0.14881 0.14881 

Point 3 0 0 0 0.082508 0 

60 
Armstrong Environmental Inc. CONVERSION FACTORS 

EPA Method 5 

511 Series Meter Box Calibration 1 mm Hg = 0.13330 kPa 

Post-Test Oririce Mathod 1 cm 0.39370 inch 

English Meter Box Units, English K' Factor 1 mm - 0.03937 inch 

1 cu ft= 28.32 liters 

er Box A 10 Date: ---------------------> 05125/07 

ial #: 30272 Barometric Pressure: ----------> 29.40 (in. Hg) 

Theoretical Critical Vacuum:---> 13.87 (in. Hg) 

III . 

'ORTAN For vatid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critica! Vacuum shown above. 

'ORTAN The Critical Oriflce Coefficient, K', must be entered in English units, (ft)^3 6 (deg R)10.51((in.Hg)'(min)). 

tll 

.. 

---- ----------- DRY GAS ME'f'ER READINGS ------------•-•- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 13.87 (in. Hg) 

Vofume Volume Volume lnitial Temps. Final Temps. Oririce K' Orifice Actual -- Ambient Temperature -- DGM DGM Ambient 

dH Time Initial Final Total Inlet - Outlet In1et Outlet Serial# Coefiicient Vacuum Initia) Final Average Outlet Overali Temp 

420) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 

0.90 5.00 495.500 498.536 3.036 73.0 71.0 73.0 72.0 55 0.464 19.0 74.0 74.0 74.0 531.5 532.3 534.0 

0.90 5.00 498.536 501.584 3.048 73.0 72.0 74.0 73.0 55 0.464 19.0 74.0 74.0 74.0 532.5 533.0 534.0 

0.90 5.00 501.584 504.630 3.046 74.0 73.0 75.0 74.0 55 0.464 19.0 74.0 74.0 74.0 533.5 534.0 534.0 

............................................... RESULTS ..................,.......,.....,............ ...... 

)RY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER -- 

LUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR 

RRECTICORRECTED CORRECTICORRECTI NOMINAL Y 

/m(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variation 

(cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 

2.965 0.1 2.951 0.1 3.039 0.995 0.001 

2.972 0.1 2.951 0.1 3.039 0.993 -0.002 

2.965 0.1 2.951 0.1 3.039 0.995 0.001 

Average Y -------> 0.994 

e: For Calibration Factor Y. the ratio of the reading of the calibration meter to the dry gas meter, 

acceptabie tolerance of individual values from the average is +-0.02. 

ORIFICE -------- 

CALIBRATION FACTOR 

dH@ 

Vaiue Variatlon 

(in H20) (in H20) 

1.419 0.0027 

1.416 -0.000 

1.413 -0.003 ID 

1.416 - <------- Average dH a? 

For Oririce Calibration Factor dH cLD, the_=ifice-d ? entiI pressur n inches of H20 that equates to 0.75 cim of air 

at 68 F and 29.92 inchesQf-H c' eptable to ranindivid values from the average is +-0.2. 

SIGNED: t% Date: ~12-.IC) 

(M 

J-' 
Temperature M11leter Calibrations 

Meter Box #: 10 

Date: 05/27I07 

Calibrated By: TA 

Emtech Thermo 

Degrees F Checker Probe Stack Oven Exit Auxillary 

Point 1 32 34.9 34 35 34.3 33.8 

Point 2 212 215.1 213.6 214 213.8 213.4 

Point 3 752 754 753.2 755 752.7 754 

Emtech Thermo 

Degrees R Checker Probe Stack Oven Exit Auxillary 

, , 

Point 1 492 494.9 494 495 494.3 493.8 

Point 2 672 675.1 673.6 674 673.8 673.4 

Point 3 1212 1214 1213.2 1215 1212.7 1214 

Percent Difference 

Probe Stack Oven Exit Auxillary 

Point 1 -0.58943 -0.4065 -0.60976 -0.46748 -0.36585 

Point 2 -0.46131 -0.2381 -0.29762 -0.26786 -0.20833 

Point 3 -0.16502 -0.09901 -0.24752 -0.05776 -0.16502 

8? ~ 
lo7 

?. I 1O i TU3t-IhSPEC i I Oy DP. i A S'r-!t=T , r • 

Company Name : i(t~, Pre-s ~ 1 D1 e 'os ~ Samol e 

I J:L: D ~ DCLe •- ~i/ O ~ 

t►( w ~r ( I~ 

I: 1::K 

1 evel ? 

~ ~ 1,: 

r ~ • I ,~.- =1~ ~::L[ ~G 

obs ~.ructions? 

damaaed . -7 

~~ + ., s .1:- .. . 

i► 

1'[ •n'y-T ttSiW[ : [MIrG r,u~ [ Df T)Q 1 7:T :A( I ( — ~ 0° < < ~ 

100 

3MLi Lt (rt• V.I. OW •v0.( [..( 0:2Lt tvtr+ r,~at. ~ 

 ~ 

~ Y~ ~ ~ I ~ -10 0 < a 2 <~.l 00 Z 1 

I ~ < ~ ; < 

Li 

I -2. _;° <W2 < ° 3 

eYtc[L 1•vltarl.t LZrtt vtl:la 

ioa Dttt+~ l.l.: T. T ~ t« CaatYL:tlK :. etGt[ Iaa1C+r1.L ltKl I I J 

.~tTlo. /oa ut(+ ~ 1•I.c ~ ` 

Z~—•—• ~ ~,I -- 1; --`~=~~i'— • r ~ __ ~ t 

. 

_ 

I . ^ 

Y . ~1 A l 

1 ~ ► Zg l 

- - ,.Z ~7~ 1.05D ~,<Pa<1.5 D ~ , 

1 

Zl ( 1.0 ~ D< P• < 1. ~ D~. ~ Z~ 5 ~ 

~ ~ 

~ o ~ 

i - Z.~ ~z~ ( 3/16 ~~ .< DL~ 3/8 11 

C[L.t[ 1qIL ~ IK LtY.1 

O[Illti fD4 ~ (T(.+1 I.C. 

•~ .•. ~• ~ 

:.~~i~ ~. C~ ( Z n 6an Y< 0. i ZS" 

~ •~~ ~ 

.— — .J 1 

.-r-• . 0-1•Z- CJ - I A 

. 

Lan p< 0-03125" 

~ 

-- —• ~~ • ~S Pa = Pb = 0. 063" ~~5 

~• • • L~ . . , . .. .. 

0(,-j(( • 1.p1(ytl ~C L(•I(L ftylTlOn 

Comment-s: 

Pi Lo ~ t:~ be/aroDe n ~lmGer 3-~ 

me a~ ;- ----1_ _„ ~ .,,..._; ~ ,-;,,,, ~ 

cri ~.eria and/or appl icabi e design f e? ture<. 

pi ~ o -Lo iube ca] i bration ► ac tor o; 0.84. 

Sigratu ~ 

D? `O 

'•.e 40 C'r 60 •V:i• 4, :, No. 2. Vpr • fV ihe 1[11 ~1V^I 

2 incn se::.zcz oi the : ~.e^~o.ovaie anc :np tni i. ... ~ /< inch 

separt::on be.veea :he tnd :"e ::cc_}e ts z: 

:ne :".r o` -."• i1 ;tst. 

63- 
P i T ~JT TU3E If~ SP"cC T ~ Oti DFT ~ Si~ EE T 

Comp ~ ny I~ at~e: ~~ (71 Pre-sample Post famQ,1e 

e0c t ~ `' c ~ ""~ ~ ~ ~' 'a t ~ 

,,,...,,~ ~ t , • 

,:e+ :s; 

~ ~ ~ .1 ~a i e ~ el ? I ti(~ 5 ~ ~ ,it ,.. 

S~••itK +C::it \v . 

obs truc -L-.i ons? 

E~ . 

damaged? ~ 

~ 

t 

M :ra;. ►tCSSwC o"f■n.0 riMC r iM ri!t' rst 

Swμ: It tvt. .::. a a&p.0 t.[ +of$C twttt r,yri. 

Y , ~ ~/ rr 

ect.rr Lo ~ urt e tzrtt •csttto, 

/Oa OCSIM ~~ 1.: !, '>,t• [+aCttLitlK :. 

}~ 

~n!~' ~ ► .... 

~ 

oKUtt Isorun.t itKt 

r41ttt0.~ rOl {[TSMI.I.L ~ 

U • ~ ~I (t — 

-tewrf t.attitlrc itYi 

res.trc. ra a't• ~ . .r.c 

... .. 

. ..~,, 

.~ ~. 

OC'~Kt ,r ~ttLTtK ltvCi r':'fIT 1 0. 

< 31 < _5 ° ~ 

.m} 

_50 < ~ 2 < 

Y 

9 ' 

A 

! 

1 1.05 Dt, < P a< 1.5 D ~ 

11.0S ~Jt<Pb<1.5 D. 

 .~ 3/16 11 •< Dt ,< 3/8tt 

'r 

A t.a n Y 

A tan 8<.0 

P a - P b 

< 0 . ~ 2 5 (t 

. 03125 tt 

_ 0. 063 , t 

~I 

~ 

I i I 

I ~ I 

y i 

t 

., •-~ 

1 

~ 

~~ 

-10 0< C. < =1 ~7° 

... i_ 

-10° < az < ~-10° 

Commenis: 

......~.:~

:. 

i~ i 1`.oi. ~ ;; b e/Probe n1amGer ~~~ _ meets or eXceadS al1 speci i iCc ~ iOnS 

cri ~ eria ?nd/or appl ica51 e desiQn i~ eai.lir°S" c, ~~'":1r5"" ereh assiqn_ed;"a 

.• ~ ,.•' <<~ 

pi ~ot tube cal ibra tion ; ac tor of 0.84. 

; ~.•. 

S i o, i a t'tl r° ° 

~ aC: 

'SeE =0 C>: 60, vo,. 42, yo. 155, hSe:nec 2. V°ri`y :!+t ninitnu:- 

2 tinvi se_zack o.' :ne - h er-ao ;~uvle arc :.~ e .~ ini.:..,-, 3/ 4 inc ~: 

seDara:ion ~ e:wee n .`e ' ~ P'.:_. _s.e arn ~ :."•e nc_Zie as s ~o~ a: 

:!+° :op o.` :"zs sace. 

F~ 
PITOT TUaE INSPECTION DATA SHEET 

Comparly Name : Pre-sampl e Post Sample 

Iw•o[artt "14— 1 

Date Date 9124 p 

LI 14. 

sralr! [ruuc 

!_ ~ . -V)-,, 

TK la ACT luisw[t 0 t.laG 1NrK Of M 1101 Rr[ I 

1wA 19 tKe r•Iis p Nrw( 1K niAi Litt[ 1LtlL. ~ 

Y~ 

« . . . 

rGi[[ 1611I[M49 lcltt MtITIN ~ 

IM uTles1.[IK I. t1Li W[W 1[O t. !f[itt t..IcITI.G l[Kt 

. M1/1«I !Y /1iWUsllit a 

~ • 

~. ....r t~~ J~..~L~.i:. 

~- 

. . 

.. Y 

c-- 

.1 ,~- 

lfGJM! ININfIrG l[1I~ t ' 

..111~ /.. Kn«I..1•~ 

M K y 

•~ ..,.._.,. 

._.. .—._. ~. 

-- - =~ 

~lG~t[ .IWt1T11t tl1Kl IN/t!• 

Comments: 

level? 

obstructions? 

.. . . 

damaged? 

-100< a l< +100 

-100 < az< +100 

-50 < $1 < +50. 

-50< 

a

Z< +50 

" Y 

 • • s 

A 

1.05 Ot < Pa < 1.5 Dt 

1.05 Dt < Pb < 1.5 Dt 

. 3/16 11 .< Dt .< 3/811 

AtanY<0.125" 

A tan @< 0. 03125" 

Pa = Pb ± 0.063 11 

D 

~ 

'L 

~ 

j 

0 

`2, 

l 

63~ 

a 32-0 

Z~ ' 

~e ~ 

Pitot tube/probe number ~~ meets or• exceeds all .specifications 

criteria and/or appl icab e design features* and is here ned a, : 

pitot tube cal ibratjon factor of 0.84. =a , 

 . • . . Signature - . 

. ,. 

Da te 

CPR 60. Yo . T2, No. 160, Method 2. Yerify the einicum ' 

2 inch setback of the thermocouple &nd the ninilt:usa 3/4 inctl 

ssparatlon bct.csen the pltot tubs and the nozzle +s shown it 

the top of thls paqt. 

fl ~ 
ir'OZLL ~ 1~\SJEC I!ON ~•Nl7 i'i_nsliR'CMEV I DH IA S1iEET 

Cor:rany Name , ~~ ~. Da,te Sam?led .S ~?i ~ ~ - Nozzle Nunber 

, 

Presample Inspection 

i hereby certi fy tnat -the above re -F erenced no-zzle appears to be 

round, sharp-ed•g•ed, `F ree ol nicks and dents and is judged accept- able 

Tor use at thi st.ime. . Zz,s' , zL6 ZLS~ . ZZ 3) 

Last P revi ously Measured 

Nozzl e A•reflp; do02.~ ~ t 2 s i anature • 

Dat- n Me?sured 

. 

, 

d • Z eS" 

~ . 

Post'sample Measurement 

Measure three didrieters as shown; me.asurernerit ;s 

in inches; record belov:; aer -l"orm calculati-ons. t 

3. , 27,,57~ 

~ • Z ~3 ~•'•I ~ rdCe ~ Uid.T, ~~~r • ~i ~ 

z D2 _ —T c ~- ~ o o 0 2? ~ 2 

, 

This ar_a s;h ' c 0sed i -, data reduCtion. 

~^? =:1 ~ ~ 

^ y 

•'~~ ~=~~/ '~ 

~ * ~:zr. ~~;,• ' _J ~• ..~ •iii L: i.7:•!C L: ~ ~ 1 i C i G ~~: ~ (:G ~ 

:i ? ~ :'•E ~ 
NOZ ZL;: I NSPtC i i ON /=.hD h9EA.SUR ~ Et~ = N► DA i A S ~-~~ r i 

 , 

Company Nane Def'U. DaT e Sampl ed ozzi e NumL~ er 

Presample Inspection 

~ hereby cerLi -','y tnai the above ref er?nced nQzzl e a?aears to 5e . 

roLnd, Shara-?dged, f ree of i-iickS and denLs 3nd is• jueged cccepicble 

Tor use at. ~ his t ime . . ~~.3 ~ . IfZ . l 53 .(, rl~~ :. 

, i 

L asZ' Previ ously Measur?d ' 

Nozzl e A ~rea,~o i~o3 ~ IZ s i gin aiur? 

Dal-- e ~eas!rad. . 0 da t A L' o S' m 

Pos tsampl e Measurement 

Measure three. di a mieters as snotiqn; me.asuremen't is 

i n i ~nches; record bel ovr; perforrn cal cul Qt; i ons. 

2. ~ .( ~12 3. :^ 

A -veraro- jl i?mnItcr a 192-7 

r,~ ~ 3 = r, D2 

---T L ), :? 

_ ' Z :. ^ ^ r ~ 

~h ~ ~r~~ ~ Tlat L (,t ~ ..v ~ rt JL`:G r ~ vJr:iU11. 

d V{ 

~ ♦ 

_~ 

j 

il` 

r • ~~"~""',~li/ ...~ 

t , 

, •~•~ 

i"iunl ;.Il7'vlc ~ !?: 

ai10 smc 
Barometer Calibrations 

Reference Barometer - Prrinco Instruments Hg in Glass - Model 9453 - Serial 41003 0 

Date Time Temp, F Watch Actual Difl', % 4wner 

I ~. 0'7 I Z' a ,~~ ~U Z.y : ~ Z~'. ~ ~--- 2 ..1 ~~ ~~ r 

2-1 „ 3 L`~ .~.~ ~~ 0~ aro ~ l~ r►1S~row 

V`i ~ ~( '2 ~l ~ `~ ' ~'~ {~ r,~~'~ 

t ~ 

~ 

~i a