# Exhaust Emissions Sampling Daltile, Dallas, TX Plant 4 and Plant 213 Scrubber Exhausts

May 22 - 23, 2007 Armstrong Environmental, Inc. Project W-2527-07

Report Prepared For: Bob Hurt Daltile 7834 C. F. Hawn Freeway Dallas, TX 75217

Report Prepared May 26, 2007 By: Armstrong Erzvironmental, Inc. 1748 Hlavek Rd. Decatur, Texas 76234 (214) 631-0021

# TABLE OF CONTENTS Page

I. Introduction 1 U. Summary 2-4
IlI. Procedures 5-7 TV. Appendices
A. Calculation Summaries 8-13
B. Analytical Summaries 14-54

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# C. Field Data Sheets 51 - 58
D. Equipment Calibrations 59-68

# I. INTRODUCTION

A series of tests was performed on the exhausts associated with the Plant 4 scrubber and the Plant 2/3 Scrubber at the Daltile facility in Dallas, TX on May 26, 2007. The purpose of this test series was to determine the exhaust emission rate of Hydrogen Fluoride and Hydrogen Chloride in terms of lbs/hr. Testing followed procedures detailed in Title 40: Code of Federal Regulations (40:CFR). Sampling was performed by Richard Taylor, Gilbert Salinas and Tom Armstrong of Armstrong Environmental, Inc. using an Apex Method 5 sampling train. Present during the test series was Gabriel Perez of TCEQ. Three one hour test repetitions were performed on each source according to the following schedule:

° Date. Source:. Start Tiirne Finish T.ime 5/22/07 Plant 4 Scrubber 8:30 AM 12:02 PM 5/23/07 Plant 2/3 Scrubber 9:15 AM 12:46 PM Submitted by: 

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# II. SUMMARY

A series of tests was performed on the exhausts associated with the Plant 4 scrubber and the Plant 2/3 Scrubber at the Daltile facility in Dallas, TX on May 26, 2007. Sampling was performed following procedures detailed in Title 40: Code of Federal Regulations.
Results of this test series are summarized in Tables 1& 2. Results indicate the following emission rates for the Plant 4 Scrubber:

Avera e

- - HF, lbs/hr 0.0121 0.0120 0.0053 0.0098 

# HCI, lbs/hr 0.0078 0.0098 0.0079 0.0085 Results indicate the following emission rates for the Plant 2/3 Scrubber:

ver ~ e` HF, lbs/hr 0.00 0.0081 0.0079 0.0053 HCI, lbs/hr 0.00 0.0322 0.0072 0.0013 '-) a , 3



## 2

## SUMMARY OF EMISSIONS TEST DATA
Table : 1 Plant : Da(tile, Dallas, TX Location : Plant 4 Scrubber Operator : R. Taylor, G. Salinas, T. Armstrong Test Date : 22-May•07 Repetition : 1 2 3
STACK GAS Temperature, F 132.7 132.3 132.3 Velocity, fps 47.60 47.60 47.05 Volume Flow, acfm 15951.6 15952.0 15767.9

scfm 11983.0 12033.7 11718.7 scfh 718979 722022 703121 Moisture, 

# % 14.54% 14.25% 15.52% CO2, 

# % 3.00 3.00 3.00 02, 

# % 16.00 16.50 16.50
SAMPLE Start Time, hrs:min 

# ' 8:30 AM 9:45 AM 11:00 AM Finish Time, hrs:min 9:33 AM 10:48 AM 12:02 PM Sample Volume, scf 34.846 35.458 35.236 Isokinetic Ratio, 

# % 97.8333 99.13347 101.1615


## HYDROGEN FLUORIDE Sample Weight, mg 0.267 0.268 0.120 Concentration, ppm 0.325407 0.320983 0.144629 Emissions, Ibs/hr 0.012147 0.012033 0.00528


## HYDROGEN CHLORIDE Sample Weight, mg 0.171 0.218 0.179 Concentration, ppm 0.114195 0.143067 0.118213 Emissions, lbs/hr 0.00778 0.0097$$ 0.007$76

3

## SUMMARY OF EMISSIONS TEST DATA


# Table : 2 Plant : Daltile, Dallas, TX Location : Plant 2/3 Scrubber Operator : R. Taylor, G. Salinas, T. Armstrong Test Date : 23• May-07 Repetition : 1 2 3
STACK GAS Temperature, F 116.5 117.6 117.8 Velocity, fps 62.60 61.46 61.42 Volume Flow, acfm 15492.7 15210.1 15199.3

scfm 12606.8 12329.1 12214.9 scfh 756410 739749 732891 Moisture, % • 

## 10.11°J 10.28%

. 

## 11.03% CO2, °J o 1.50 1.50 1.50 02, °" J o 19.00 19.50 19.00
SAMPLE Start Time, hrs:min . 

## 9:15 AM 10:30 AM , 

## 11:45 AM Finish Time, hrs:min 10:16 AM 11:31 AM 12:46 PM Sample Volume, scf 37.267 36.466 36.272 lsokinetic Ratio, °J

o 100.4018 100.4551 100.8556
HYDROGEN FLUORIDE Sample Weight, mg 0.00 0.181 0.177 Concentration, ppm 0 0.210795 0.207239 Emi ssions, I bs/hr 0 0.008096 0.007886
HYDROGEN CHLORIDE Sample Weight, mg 0.00 0.720 0.162 Concentration, pprn 0 0.459464 0.103932 Emissions, !bs/hr 0 0.032206 0.007218

0

# III . PRO CEDUURES

The procedure for emissions sampling followed USEPA test methods as detailed in Title 40: Code of Federal Regulations. The following methods were used:
Method Title 1 Sample and Velocity Traverses for Stationary Sources
2 Determination of Stack Gas Velocity and Volumetric Flow Rate (Type S

Pitot Tube)
3 Gas Analysis for the Determination of Dry Molecular VVeight -
26A Determination of Hydrogen Halides and Halogens Emissions from

Stationary Sources 02 and CO2 were determined using FyRite Analyzers. HF and HCl sampling was performed on the Plant 4 scrubber exhaust for 2.5 minutes at each of 24 points, 12 points per traverse, making a total run duration of 60 minutes. HF and HCl was performed on the Plant 2l3 scrubber exhaust for 5 minutes at each of 12 points, six points per traverse. A schematic of each sampling location is shown in Figures 1 and 2. The sampling train was configured as follows: Glass Sampling Nozzle Heated Glass Lined Probe Heated teflon filter Impinger # 1- 100 mis 0.1 N H2S 04 Impinger #2 - 100 mis 0.1 N H2SO4 Impinger #3 - Empty Impinger #4 - 200 grams silica Gel Analysis for HF and HCl was performed on the solution frorn impingers 1- 3. Analysis was performed using a Dionex LC20 Ion Chromatograph. Standards were made from a 999 rnglL chloride in H20 and a 995 mg/L fluoride in H20 certified standards. 200 ul, 400 ul, 600 ul, and $00 ul of each solution was added to 100 mis of 0.1 N H2SO4.

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# Fzgure 2

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# Plant 2/3 Scrubrer

84 ir7clies

Lto Stack Diameter

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## ir

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## l It1 -1.2 iric

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## es Pair•ik #2 - 4.0 inclles Poilit h3 - 8.1 iriches ('oiiit M



### - 19.4 iticlies 

## Point 115 - 23.5 iiiches Pair

- it 06 - 2E.3 inches

# Figure :t -- Plant 4 Scubber

s34 iriches

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### 4 ireches 6 tacE; D iametei - 32 inches Poirlt #1 ;1. Q inches Point #2 - 2-1 inches Pcint 03 - 30 inches Point ##4 - 5.7 inctins Point 145 

### -

$ inches 

### - 

## Point 116 -11. 4 inches Poit

- it # 7 - 20.1 inciies Point 118 - 24 inches F'oir

- it I#9 - 26.3 inches Point 410 - 28.2 inches Point #t1'I - 23.9 incf7es Poirit tt12 - 31 inches

### EMISSION TEST SUMMARY

PLANT : Dattile. Datlas, TX DATE : 22•May07 PLACE : Plant 4 Scrubber RUN# : 1 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 126 

### NOZZLE DIAMETER (INCH.) : 0.2253 PARTICULATE WEIGHT (Front hatf mg) : 0 METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.34 GAS METER VOL.(Cu.Ft.) : 36.083 PERCENT CO2 3 BAROMETRIC PRESSURE 29.55 PERCENT 02 16 PERCENT CO 0
FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 32 STACK LENGTH(inchs) : 

### STACK AREA (Sq.Ft.) : 5.585054 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000277 STACK AREA (Sq.Ft.) : 0
ENTER THE STACK AREA SHOWN ABOVE: 5.585054
FLOwS SAMPLED VOLUME (STD. CU .FT.): ' 34.8458 VOLUME OF WATER VAPOR (STD. CU .FT.): 5.9308 FRACTIONAL MOISTURE CONTENT 0.1454

DRY BASE: 81.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1200 MOLECULAR WT. OF STACK GAS (WET BASE): 27.5026 STACK PRESSURE (inch Hg): 29.5250 STACK GAS VELOCITY (ft/sec.): 47.6021 ACTUAL STACK GAS FLOW RATE`(ACFM): 15951.6184 STANDARD STACK GAS FLOW RATE (SCFH): 718979.224

ISOKINETIC RATIO (%): 97.8333
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T.

deg F INLET It

METER T. Meter Point Point Point Point Iso OUTLET Votume VMSTD Velocity Moisture

1 138 0.65 0.806226 0.97 77 76 2 138 0.66 0.812404 0.98 78 76 3 138 0.69 0.830662 1.00 80 75 4 138 0.68 0.824621 1.00 80 75 5 138 0.68 0.824621 1.00 82 76 6 134 0.67 0.818535 1.00 83 76 7 134 0.64 0.8 0.95 83 76 8 132 0.61 0.781025 0.91 83 7 6 9 132 0.57 0.754983 0.85 83 77 10 132 0.53 0.728011 0.79 84 77 11 133 0.50 0.707107 0.74 84 78 12 331 0.42 0.648074 0.62 84 77 13 132 0.65 0.806226 0.97 79 77 14 132 0.69 0.830662 1.00 82 77 15 131 0.68 0.824621 1.00 84 77 16 130 0.69 0.830662 1.00 85 77 17 130 0.6E 0.824621 1.00 85 78 18 130 0.67 0.818535 1.00 85 78 19 130 0.62 0.787401 0.93 85 78 20 129 0.60 0.774597 0.91 81 78 21 129 0.55 0.748331 0.85 8r 78 22 130 0.52 0.72111 0.79 84 78 23 132 0.47 0.685565 0.71 84 78 24 132 0.40 0.632456 0.61 84 78
132.70833 0.7759 0.8992 82.8333 76.9583 mis 182 1.5552 49.6844 5.63101 183.6 1.4567 50.0651 5.27429 185.1 1.5524 51.1903 5.62095 186.7 1.5524 50.818 5.62095 188.3 1.5481 50.818 5.60531 189.9 1.5467 50274 5.60011 191.5 1.4498 49.1355 5.24945 193 1.4497 47.8893 5.24893 194.5 1.4481 46.2925 5.24329 196 1.3501 44.6387 4.88848 197.4 1.3487 43.3935 4.88336 198.8 1.2001 39.7037 4.34542 200.045 1.5072 49.4345 5.45738 201.6 1.5467 50.9328 5.60011 203.2 1.6403 50.5197 5.93911 204.9 1.446 50.8467 5.23555 206.4 1.5409 50.4769 5.57943 208 1.5409 50.1044 5.57943 209.6 1.4444 48.1986 5.22981 211.1 1.4443 47.3746 5.22955 212.6 1.4441 45.7682 5.22877 214.1 1.3489 44.1408 4.88397 215.5 1.2523 42.0361 4.53421 216.8 1.2356 38.7796 4.4738 218.083 79.8958 101.3172 94.1771 98.1610 98.8801 98.6049 98.9135 94.8681 96.9996 100.2375 96.9170 99.7617 96.6950 97.6992 97.3052 103.8637 90.8169 97.4910 98.2158 95.7015 

### 97.1961 100.5926 97.5888 95.4589 102.0965



## i ~

### EMISSION TEST SUMMARY

PLANT : rJaltile. De.11as. TX DATE : 22•May07 PLACE : PIan14 Scruaber RUN#: 2 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 125.2 NOZZLE DIAMETER (INCH_) : 0.2253 PARTlCULATE WEIGHT (Front half mg) : 0 METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mf{) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.34 GAS METER VOL.(Cu.Ft.) : 36.803 PERCENT CO2 3 BAROMETRIC PRESSURE 29.55 PERCENT 02 16.5 PERCENT CO 0
FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 32 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 5.585054, STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000277 STACK AREA (Sq.Ft.) : 0
ENTER THE STACK AREA SHOWN ABOVE: 5.585054


### FLOwS SAMPLED VOLUME (STD. CU .FT.): 35.4583 VOLUME OF WATER VAPOR (STD. CU .FT.): 5.8932 FRACTIONAL MOISTURE CONTENT (%): 0.1425

DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1400 MOLECULAR WT. OF STACK GAS (WET BASE): 27.5524 STACK PRESSURE (inch Hg): 29.5250 STACK GAS VELOCITY (ft/sec.): 47.6032 ACTUAL STACK GAS FLOW RATE (ACFM): 15951.9895 ° STANDARD STACK GAS FLOW RATE (SCFH): 722021.736

JSOKINETIC RATIO (%): 99.1335
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point Point Iso

deg F INLET

1 131 0.65 0.806226 0.98 78 2 132 0.66 0.812404 0.99 81 3 132 0.68 0.824621 1.00 82 4 132 0.70 0.83666 1.10 83 5 133 0.69 0.830662 1.00 84 6 133 0.68 0.824621 1.00 84 7 133 0.65 0.806226 0.98 85 8 133 0.62 0.787401 0.94 84 9 132 0.59 0.76B115 0.89 84 10 130 0.56 0.748331 0.85 85 11 130 0.55 0.74162 0.83 85 12 129 0.46 0.678233 0.70 85 13 130 0.65 0.806226 1.00 80 14 132 0.68 0.824621 1.10 84 15 134 0.67 0.818535 1.10 85 16 133 0.68 0.824621 1.10 86 17 134 0.66 0.812404 1.00 86 18 134 0.67 0.818535 1.10 85 19 134 0.64 0.8 1.00 86 20 135 0.58 0.761577 0.92 86 21 134 0.54 0.734847 0.86 86 22 132 0.51 0.714143 0.81 86 23 132 0.40 0.632456 0.63 86 24 130 040 0.632456 0.63 86

132.25 0.7769. 0.9379 84.2500 OUTLET Volume VMSTD Velocity Moisture mis 78 218.3 1.5509 49.3481 5.483405 77 219.9 1.5481 49.7683 5.473368 77 221.5 1.5467 50.5167 5.468431 77 223.1 1.5456 51.2542 5.464723 77 224.7 1.5438 50.9298 5.458313 77 226.3 1.5438 50.5594 5.458313 78 227.9 1.5409 49.4315 5.447963 77 229.5 1.4471 48.2773 5.116407 78 231 1.4456 47.0551 5.111043 78 232.5 1.4441 45.7657 5.105817 78 234 1.3478 45.3552 4.765193 78 235.4 1.3059 41.4435 4.617342 78 236.757 1.5897 49.3063 5.620604 78 238.4 1.5428 50.5167 5.454622 78 240 1.6377 50.2285 5.790185 78 241.7 1.5399 50.5594 5.444558 79 243.3 1.5381 49.8523 5.43819 79 244.9 1.6362 50.2285 5.784843 79 246.6 1.442 49.0911 5.098304 79 248.1 1.5378 46.7727 5.437111 80 249.7 1.4401 45.0931 5.091839 79 251.2 1.3452 43.7488 4.756173 80 252.6 1.1515 38.7446 4.071145 79 253.8 1.2514 38.6791 4.424659 255.103 78.1667 81.2083 100.1906 99.3306 97.7707 96.2985 96.9619 97.6722 99.7113 95.8618 98.1034 100.4239 94.5725 100.1176 102.6106 97.5238 104.4691 97.4261 98.8588 104.3728 94.1171 105.5243 102.3318 98.1913 94.9046 102.9711

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### EMlSSION TEST SUMMARY

PLANT : Daltile. Dallas, TX DATE : 22•May07 PLACE : Plant 4 Scrubber RUN3s : 3 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 137.5 NOZZLE DIAMETER (INCH.) : 0.2253 PARTICULATE WEIGHT (Front half mg) : 0 METER COEFFiCIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : •0.33 GAS METER VOL.(Cu.Ft.) : 36.805 PERCENT CO2 3 BAROMETRIC PRESSURE 29.55 PERCENT 02 16.5 PERCENT CO 0
FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 32 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 5.585054 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000277 STACK AREA (Sq.Ft.) : 0
ENTER THE STACK AREA SHOWN ABOVE: 5.585054 

### FLOWS SAMPLED VOLUME (STD. CU .FT.): 35.2364 VOLUME OF WATER VAPOR (STD. CU .FT.): 6.4721 FRACTIONAL MOISTURE CONTENT (g6): 0.1552

DRY BASE: 80.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.1400 MOLECULAR WT. OF STACK GAS (WET BASE): 27.4113 STACK PRESSURE (inch Hg): 29.5257 STACK GAS VELOCITY (ft/sec.): 47.0540 ACTUAL STACK GAS FLOW RATE (ACFM): 15787.938

~ STANDARD STACK GAS FLOW RATE (SCFH): 703121.263

1SOKINETIC RAT10 (gf,): 101.1615
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Paint Point Point Point Iso

deg F 1NLET OUTLET Volume VMSTD Velocity Moisture mis 1 133 0.65 0.806226 1.00 80 79 255.4 1.5467 49.5579 6.043488 101.3263 2 133 0.66 0.812404 1.00 82 79 257 1.5438 49.9377 6.032306 100.3697 3 133 0.67 0.818535 1.10 84 79 256.6 1.6377 50.3146 6.399077 105.6748 4 130 0.67 0.818535 1.10 85 79 260.3 1.5399 50.1871 6.017105 99.1152 5 13G 0.67 0.818535 1.10 85 79 261.9 1.5399 50.1871 6.017105 99.1152 6 130 0.65 0.806226 1.00 87 80 263.5 1.5353 49.4324 5.999009 100.3258 7 130 0.62 0.787401 0.99 87 80 265.1 1.5352 48.2782 5.99886 102.7219 8 129 0.60 0.774597 0.96 87 80 266.7 1.5351 47.4529 5.998414 104.3236 9 130 0.57 0.754983 0.91 88 80 268.3 1.4377 46.2906 5.617647 100.3245 10 131 0.54 0.734847 0.86 88 81 269.8 1.4362 45.0941 5.611792 103.0534 11 132 0.49 0.7 0.78 89 81 271.3 1.3389 42.992 5.231828 100.9439 12 132 0.50 0.707107 0.80 89 81 272.7 1.3237 43.4285 5.172292 98.7922 13 133 0.65 0.806226 1.00 85 82 274.084 1.5506 49.5579 6.058999 301.5864 14 136 0.65 0.806226 1.00 B9 82 275.7 1.5296 49.6831 5.977015 100.4650 15 1

.34 0.65 0.806226 1.00 89 82 277.3 1.5296 49.5997 5.977015 100.2963 16 134 0.66 0.812404 1.05 90 83 278.9 1.6225 49.9798 6.339744 105.5740 17 133 0.65 0.806226 1.00 90 83 280.6 1.5268 49.5579 5.966078 100.0284 18 133 0.64 0.8 1.00 90 83 282.2 1.5268 49.1752 5.966078 100.8069 19 134 0.61 0.781025 0.97 91 83 283.8 1.43 48.0493 5.587669 96.7883 20 134 0.55 0.74162 0.89 91 83 285.3 1.4297 45.6251 5.58656 101.9108 21 133 0.54 0.734847 0.86 91 84 286.8 1.4283 45.1703 5.581042 102.6620 22 133 0.48 0.69282 0.77 91 84 288.3 1.3328 42.587 5.207809 101.6075 23 132 0.43 0.655744 0.68 91 83 289.7 1.2384 40.2739 4.839161 99.6691 24 133 0.36 0.6 0.68 90 84 291 1.1479 36.8814 4.48553 101.0541 292.205 132.29167 0.7659 0.9375 87.8750 81.4167 84.6458FLOWS SAMPLED VOLUME (STD. CU .FT.): 37.2671 VOLUME OF WATER VAPOR (STD. CU .FT.): 4.1892 FRACTIONAL MOISTURE CONTENT 

## M; 0.1011

DRY BASE: 79.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0000 MOLECULAR WT. OF STACK GAS (WET BASE): 27.8884 STACK PRESSURE (inch Hg): 29.5713 STACK GAS VELOCITY (ft/sec.): 62.6013 It ACTUAL STACK GAS FLOW RATE (ACFM): 15492.7089 STANDARD STACK GAS FLOW RATE (SCFH): 756409.784

ISOKINETIC RATIO (%): 100.4018
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T

deg F INLET OUTLET

1 118 1.20 1.095445 1.10 2 118 1.30 1.140175 1.20 3 116 1.30 1.140175 1.20 4 115 1.00 1 0.94 5 117 0.79 0.888819 0.74 6 117 0.57 0.754983 0.54 7 118 1.30 1.140175 1.20 8 117 1.30 1.140175 1.20 9 117 1.30 1.140175 1.20 10 115 .1. 20 1.095445 1.10 11 114 1.10 1.048809 1.00 12 116 0.86 0.927362 0.81

116.5 1.0426 1.0192 

### c

75 75 76 76 77 78 78 79 79 

### ao ao 80 76 79 

### sl 82 84 84 

### sl 85 85 66 87 86
83.0000 77.7500 0

Meter Point Point Point Volume VMSTD Velocity Moisture mis 292.6 3.22 65.857 7.70028 295.9 3.5038 68.5461 8.37892 299.5 3.397 68.4274 8.12348 303 3.004 59.9627 7.18378 306.1 2.6 079 53.3886 6.23638 308.8 2.2666 45.3495 5.42026 311.15 3.4391 68.5461 8.22425 314.7 3.3751 68.4868 8.07102 318.2 3.3751 68.4868 8.07102 321.7 3.2718 65.6858 7.82404 325.1 3.0757 62.8347 7.35521 328.3 2.7386 55.6554 6.54908 331.148 80.3750 Point Iso

99.2262 103.7353 100.3987 101.1424 98.9586 101.2551 101.8205 99.8369 99.8369 100.5590 98.6509 99.5150 

### EMISSiON TEST SUiYIMARY

PLANT : Daltile. Dallas. TX DATE : 23-klay•07 PLACE : Plant 2/3 Scrubber RUN#: I TEST OURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : NOZZLE DIAMETER (1NCH.) : 0.1927 PARTICULATE WEIGHT (Front half mg) : METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : GAS METER VOL.(Cu.Ft.) : 38.548 PERCENT CO2 BAROMETRIC PRESSURE : 29.6 PERCENT 02 PERCENT CO
FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 27.5 STACK LENGTH(inchs) : STACK AREA (Sq.Ft.) ; 4.124704 STACK WIDTH(inchs) : NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) :
ENTER THE STACK AREA SHOWN ABOVE: 4.124704 89 0 0 •0.39 1.5 19 0

0



# 11

### EMISSION TEST SUMMARY

PLANT : Daltile. Daltas, TX DATE : 23•May07 PLACE : PIrnt 2+'3 Scrubber RUN# : 2 TEST DURATION (MINUTES) : NOZZLE DIAMETER (INCH.) : METER COEFFICIENT (Y) : PITOT COEFFICIENT (Cp) : GAS METER VOL.(Cu.Ft.) : BAROMETRIC PRESSURE 60 LIQUID COLLECTED (mis) : 0.1927 PARTICULATE WEIGHT (Front half mg) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0.84 STATIC PRESSURE (in. 1120) : 38.067 PERCENT CO2 29.5 PERCENT 02 PERCENT CO 88.8 0 D •0.39 1.5 19.5 0
FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 27. 5 1 STACK LENGTH(fnches) : STACK AREA (Sq.Ft.) : 4.124704 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 0
ENTER THE STACK AREA SHOWN ABOVE: 4.124704


### FLOwS SAMPLED VOLUME (STD. CU .FT.): 36.4656 VOLUME OF WATER VAPOR (STD. CU .FT.): 4.1798 FRACTIONAL MOISTURE CONTENT 

### (%): 0.1028

DRY BASE: 79.0000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0200 MOLECULAR WT. OF STACK GAS (WET BASE): 27.8867 STACK PRESSURE (inch Hg): 29.5713 STACK GAS VELOCITY (ft/sec.): 61.4595 AC7UAL STACK GAS FLOW RATE (ACFM): 15210.1293 STANDARD STACK GAS FLOW RATE (SCFH): 739748.969

ISOKINETIC RATIO 

### (%

a ): 100.4551
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T. METER T. Meter Point Point Point

deg F INLET OUTLET Volume VMSTD Velocity Moisture mis 1 119 1.20 1.095445 1.15 81 81 331.3 3.2843 65.9159 8.008531 2 118 1.30 1.140175 1.20 86 81 334.7 3.3658 68.5482 8.207171 3 117 1.30 1.140175 1.20 83 81 338.2 3.4556 68.4889 8.426158 4 l i6 1.05 1.024695 1.00 89 82 341.8 2.9687 61.4987 7.23897 5 1i7 0.82 0.905539 0.78 89 82 344.9 2.7757 54.3945 6.768248 6 118 0.74 0.860233 0.71 88 82 347.8 2.5306 51.7178 6.170693 7 118 1.00 1 0.96 85 83 350.442 2.9363 60.1207 7.159873 8 119 1.20 1.095445 1.15 89 82 353.5 3.2572 65.9159 7.942466 9 119 1.30 1.140175 1.20 91 84 356.9 3.3412 68.6074 8.14721 10 119 1.30 1.140175 1.20 91 84 360.4 3.4366 68.6074 8.379987 11 116 0.83 0.911043 0.79 91 84 364 2.6702 54.6777 6.51115 12 115 0.67 0.818535 0.64 90 84 366.8 2.4493 49.0831 5.972563 369.367 117.58333 1.0226 0.9983 88.1667 82.5000 85.3333 Point Iso

101.4925 99.8431 102.4184 97.8196 103.5833 99.4980 99.3120 100.6552 99.1994 102.0336 98.9606 100.9461



# - 12

### EMlSSION TEST SUMMARY

PLANT : DaItile. Dallas. TX DATE : 2-

3 •May07 PLACE : Plarit 2: 3 Scrubber RUN#: 3 TEST DURATION (MINUTES) : 60 LIQUID COLLECTED (mis) : 95.5 NOZZLE DIAMETER (tNCH.) : 0.1927 PARTICULATE WEIGH7 (Front half mg) : 0 METER COEFFICIENT (Y) : 0.998 PARTICULATE WEIGHT (Back half mg) : 0 PITOT COEFFICIENT (Cp) : 0.84 STATIC PRESSURE (in. H20) : 0.39 GAS METER VOL.(Cu.Ft.) : 38.139 PERCENT CO2 1.5 BAROMETRIC PRESSURE 29.6 PERCENT 02 i9 PERCENT CO 0
FOR CIRCULAR STACK FOR RECTANGULAR STACK STACK DIAMETER (inch): 27.5 STACK LENGTH(inches) : STACK AREA (Sq.Ft.) : 4.124704 STACK WIDTH(inches) : NOZZLE AREA (feet): 0.000203 STACK AREA (Sq.Ft.) : 0
ENTER THE STACK AREA SHOWN ABOVE: 4.124704


### FLOwS SAMPLED VOLUME (STD. CU .FT.): 36.2715 VOLUME OF WATER VAPOR (STD. CU .FT.): 4.4952 FRACTIONAL MOISTURE CONTENT {q o }: 0.1103 DRY BASE: 79.5000 MOLECULAR WT. OF STACK GAS (DRY BASE): 29.0000 MOLECULAR WT. OF STACK GAS (WET BASE): 27.7871 STACK PRESSURE (inch Hg): 29.5713 STACK GAS VELOCITY (ft/sec.): 61.4159 ACTUAL STACK +GAS FLOW RATE (ACFM): 15199.3481 STANDARD STACK GAS FLOW RATE (SCFH): 732891.184

ISOKINETIC RATIO (g(,): 100.8556
POINTS STACK T. DELTA P SQUAR D.P DELTA H METER T_

deR F INLET
1 118 1.30 1.140175 1.20 85 2 119 1.30 1.140175 1.25 90 3 119 1.20 1.095445 1.20 92 4 i i 6 1.10 1.048809 1.10 92 5 116 0.81 0.9 0.79 93 6 117 0.68 0.824621 0.66 93 7 118 1.20 1.095445 1.20 90 8 119 1.30 1.140175 1.30 94 9 I i 9 1.20 1.095445 1.20 94 10 118 0.97 0.984886 0.94 94 11 119 0.89 0.943398 0.87 94 12 115 0.69 0.830662 0.67 94

117.75 1.0199 1.0317 92.0833 n

METER T. Meter Point Point Point Point Iso OUTLET Volume VMSTD Veiocity Moisture mis 85 370.4 3.3565 68.671 8.849206 100.2214 85 373.9 3.437 68.7304 9.061601 102.7156 86 377.5 3.2368 66.034 8.533739 100.6820 86 380.9 3.1409 63.0588 8.280695 101.7760 86 384.2 2.6605 54.1117 7.014261 100.4649 87 387 2.4086 49.6227 6.350099 99.3522 87 389.538 3.2989 65.977 8.697275 102.5227 87 393 3.3238 68.7304 8.762965 99.3304 87 396.5 3.228 66.034 8.510486 100.4076 87 399.9 2.9413 59.3182 7.754564 101.6715 88 403 2.6538 56.8685 6.996553 95.8500 88 405.8 2.5899 49.8995 6.828247 105.8723 408.534 86.5833 89.3333

~

## 0.31 0.130572 0.25 0.1053 i 0.35 0.14742 ; 0.23: 0.0 

## 96876 ae { 0.120042 0.43 

## ~ 0.176816 0.193264 

## 0.481 0.197376 0.361 0.148032 - 1 0.178872

ml i L HF, 

## _mg - CI-, uglml jHCI 

## , mg _

~ - 

## 0



## - i -- - - 0 o' - - 

# 0 01 0 0 

# ~ 0 ✓



## - -- - 01 - - i -- 0
0.42 0.176904 

## 0.44 0.185328 pe 0.181116
0. 34' 0. 

## 1 43208 

## 0. 42 ; 

## 0. 176904 0.421 0.176904 0. 

## 51 0. 2106 3ge , - r 0.176904 1. 

## 76 0 .723712



## 1.74 0.715488 i 0.7196

_ 0.45 ! 

## _0. 18504



## _ 0.41 i 0.168592 0.341 0 

## .139808

~ 

## 0.38 j 0. 156256 

## j 0.162424 Sheet1

Summary of HF and HCI Anal 

## ys is


## Pl ant: 

## ; D altile, Dailas, 

## TX Date: i 5 /22 - 512 

## 3/07
--- - ~ 

## - -- ----- ~ 

## -_.

~



# - Locati _ _on_ - : ;Plan_t 4 Scrubber --, Run # 1Imps Volume Dilut

1 

## --- ------- i- 1 &2

, 

## --- ,



## _ 400;

~ 

## 400 ,

-- - - --- -- __ ~ ~ 

## ----- -
---...._-- 2 '------__

. 4001 1 !


## - ------ - -- _ _- - -- -

21 1 & 2 ~ 

## 400 1 i



## ._...._.__ _.. ~ 

## .. .- ---- -

2:1 &2 

## 400 11 - - - -- - 2 :1 & 2 4001 

## ----- --1 _- ( 

## - Aver
3 1 L & 2 

## 400 _ 1 i _._._._3 11_ & 2

~_



## 400 

## ! _-- - 1-- 

## 3 (1 & 2
--- --- - -- ~ 

## -- ---- - - ~ 

## -

- - 3 ~~ 

## & 2 1

-~ 

## ----

- -- - ; 

## _ 4 00 i 

## Aver

. ~
r



## crubb e 

## Plant 213 Location: ; S

., ~ 

## _ :..

-- - - ---- Run # ;I mps 

## !Volume ,Dilution -- !Fl-, ~



## _ _ _- -- ---,-- 1 !1 & 2 40 0j 

## 1 1;1 & 2 ; _.. _ 4001 

## - --- ~ 

## ;-

_. .. - -- - -- _ ---- Aver 

## . .. .----- - ._ -- ---- ---__ _ - ---

_ 2 i 1 &_.2______._

~ 

## - --400 __.__....1

~

- 2 I 1 

## &- 2 __. L_-- 400 1 ~



## ; ; Aver


## 3+ 1& 2' 400 1 ~ 

## __- 3 ; 1 & 2 

## 4 00i 

## - --- 1 _3 j 1_ & ? 

## - - ~ 

## - --. 400 

## 1 i

.. 3 L1 &_2_.-. 4 001 

# IAver

~ 

## 0.791 0.3327481 0.561 0.235872



## !! 0.67; 

## 0.282204 1

1 0.53 0.223236 

## ae 1 0.2685151 H CI, mg 0.176816



## _ 0.16448 

## 0 .1706 

## 48 0.58 j 0.238496 0.54 0.222048

- 

## 0.52 0.213824 0.48 0.197376 

## { 0.217936 ---- ~ 

## --- ~ 

## -- 1

i 

## on FI-, uglml j HF, mg `CI-, uglml i 11 0.641 0.269568 0.43 1 

## 11 0.631 0.265356 0.4 

## ! , !A 

## veraae I 0.267462 - i

Page 1 1 14

# l

. ~ C

l 2to.Qs



# ,

~ 00 23/. 2-1'

o 

# , 318 8 236.

~ 

# b'

70 6'00

~ 

# a52 3

~ 

# fS.oC
~



# 9-oo

~



# - ?A's Ls ©



# 1~

# conditions = 1.99 ug/ml. Fl-- in H2SO4 = 2.0 ug/m.l C1-- in H2SO4 Date » 05/25/2007 Time - 07'-03:15

--25 :600mV 

# Component Retenti

1.

1.58 F1-

Cl-

. 

## 256.00OmV 

# Area Externa

210.85 M



# 119.20 M

~

Compo ne nt 

# Fl•- 

# c i --

2 

# Number Retention Area External Units
1 .1 . G25 210.85 M 2.1.8 ug/ml 

## 2 J. . 583 119.20 NI 1 . 82 ug/m l

330.05 4.01



## ~ ~,

## Conditions 

# : 1.99 ug/ml Fl- in 

## H2SO4 : 2.0 ug/ml Cl— in H2504 Date : 05/25/2007 T2Lme z 07:15:13

-25.6OOmV COMPDnept 

## Retenti 256.00OmV 

# ATea Eyternal

Fl- 

# 1. ci- 1.58
2

41



# 5

61



# ~ ...»...».... 

# ._..... .. .. ....... . ........... . ............ . .............. ....... ..... 206.20 

# M 2. 1'4`



# 124.53 M 1.91

It



## Component Number Retention Area Exter-nal Units
Fl- 

# 1 1.016 206.20 M 

# 2.13 ug/ml 

# ci- 2 

# 1.583 124.53 M 

# 1.91 ug/ml

VA 

# 330.73 4.04

## Conditions 

## : H2SO4 Blank. Date 

## : 05/25/2007 Time 

## 07:31:27

-25.600MV 

# Component Ret*eition 256.00OmV 

# ATea External

.. ........... ...... .............. .. ..... .. ................. ....... ...... . .............................. . ............ .. . .. .................... .. ...................

~ ~~

..... !



## 2

~ .».».. : i



## 31

41

0

6'.



## ................. .... ......... ............ . .... ........ . . ....... ...... .. ..... ....... .. ............ ......................................... ...... .... .. ..... .. ..... ..................... ............
Component Number Retention Area External Units

0 

## 0.00 . 0.00



# „ 18

# 25h.00qmV —25.60C}mV ' 

# Component Retenti

Fl- 1.

C1- 1.50

A 

# Conditions : 3.98 ug/ml F1— in H2SO4

= 4.00 ug/mI C1— in H2SO4 Date : 05125/2007 Time = 07 = 46 ". 42



# Area Er.ternal

375.50 M 4.07

231, 2a H 3.54



## Component
F1-- C1.-

2 

# Number Retention
1 1.033 2 1.600 

# Area External Units
375.50 M 4.07 (ag/ml 

# 231.28 M 3.54 ug/mJ.

606 . 78 7.61

~ ,

# Conditions = 3.98 ug/ml Fl-- in H2SO4 = 4.00 ug/ml Cl-- i n H2SO4 Date = 05/25/2007 Time - 07 : 4,9 - 37

-25 . 6OOmV 

# Component Retenti

C1- 1.64 255 .00OmV 

# Area External

382.10 M 4.15

242.68 h1 3.74



# .Component Number Retention Area External Units
Fl- 1 1.033 382.10 Ni 4.15 ug/ml 

## Cl-- 2 1.600 242.68 M 3.70 

# ug/mJ.

2 624.78 7 _ 86

~ 

# 20

.~ .

## Conditions 

## : 5.97 ug/ml Fl— in H2504 

## : 6.00 ug/ail 

## Cl— in H2SO4 Date 

## : 05/25/2007 Time 

## : 08:00:07

—25.6OOmV 

# 256,OOOmV ComponeRt Reti 

# on

.......... . ...... ............ ....... ......

Fl- 1• ' 

# ~ • • i



## ci- 

# 1.61 ...........

............ ....... . ..................

........... . 

## 21;



# j

~ ; 

## 41

~ : ~ ~



## 6; -

............. . .. . ..... ........ ...... 

# Component Number Retention Area External Units Fl- 1 1-.033 580.70 11 

# 6.34 ug/ml Cl - 

## 2 

# 1.616 

# 348.33 M 5.65 

# ug/ml

2 929.03 11.99 

## Area bfternal

580.70 M 6.34

348.33 M 5.65



# 21

## Conditions
: 

## 0 5.97 ug/ml Fl- in H2SO4 

## : 6.00 ug/ml 

## Cl- i n H2SO4 Date 

## : 05/25/2007 Ti'me 

## : 08:03:26

-25.6OOmV uomponeRL ReLe 

## 256.000mV 

# Area External

Fl- 1.

ci- 1.60 

# l

! ';.._.. I

..... 

# 0 ..

. ....... ......

. .. . 

# 1 ........ .... 

# 2 - 

# 31 . . .....



# ~~ »..»_ : 

# ~

6 552.20 

# H 6.01


# 345 .46 m 5.60

0

Component 

## Number Retention Area •xternal Units 

# Fl- 1 1.033 552.20 M 

## 6.01 tig/ml 

# ci- 2 

## 1..660 345-06 M 

## 5.60 ug/ml



# 2 897.26 11-61



# 24

# 23 2 1219.75 15 .97 

# Conditions = 7_96 ug/ml F1- in H2SO4

= 8.00 ug/m i C I-- i n F12SQ4 Date = 05/25/2007 

## T.i.tne = 08 :12 : 17

Component 

## F1-- 

# c i -- 

# hlumber Retention Area
1 1.016 774.55 2 1.616 445,20 

# External Units 8.18 ug/m l 7.80 ug/m l 

# F1-


# ci1.

1.6] --25 . 6pOmV 256 . OOOmV 

# Camponent Re'Lention 

# Area External

774.55



# 445.20



# =

~ 

# ' , 

# 8.18

7.80

## Conc{itions : 7.96 ug/m3. F1— in H2SO4 : 8.00 ug/m 1 C 1-- i n H2SO4 Date = 05/25/2007 3"ime = 08-.14-=55

—25.6OOmV 25b.00UmV Conpanept Retentian Area Eztei

- nal

FlC1- l.

I.64 162,54 8.45

434 .42 h! 7.60

Component Number Retention Area External Units
F1— 1 1.016 762.50 8.05 ug/ml 

# c I '_ 2 1.600 4:34 ., 42 M - 7.60 ug/ml

2 114b . 

## g2 15.65

Y 

# ' 24

# AMC3UNT INJECTED

AREA 0.000 

# o . OaC

768.525 7.960


# 1

2

3

4

5 s 

# Calibration file = F1--.cal

Avg slope of curve = 96.55 Y-ax a. s i ntercep t= 0.00 Coeff of 1. i. n regr - 0.92 

# No. Area Amourit CF
0: 0.000 0.000 0.000 1 : 208 . 525 1.990 104 . 786* 2: 378.800 3.980 95.176 3: 566.450 5.970 94.883 

# 4" 768.525 7.960 96.548

~ y •~ ~ ~

# AMf,3Uh4T INJECTEQ

AREA 0.000 0.000

439.810 M ~ 

# 1

~ 

# M ,

3

4-

5 

# Calibration f i ie = Cl- .ca l

Avg s:lope of curwe - 54.98 Y-ax i si ntercept = 0.00 

# Coeff of J.in rc:gr : 0.90
No . A•rea Amaunt CF
0: 0.000 0.000 0.000 

# 1= 121.865 2.000 60.932 2-' 236.980 4.000 59.245 3= 346 k b95 6.000 57.782 4: 439,810 8.000 54 ,.976



# _ 26

## 256.00OmV 

# --25 .600mV 

# Componer.t Reten .


# unknown) 4. unknown) o. 

# Area Ey.tQrna]

34,74 N/A. 

# 32.55 M N/P, 67:50 M 0,64

25.90 h4 4.43 

# Corsditions = Dalfi.i.Le , Dallas s TX Plant 4• Scrubber

= Run #1 Tmps 1&2 = volume 400 Dilution 1/1 Date = 05/25/2007 Time = 08 = 31 - 4-6



## Component Number Retention Area External Units 

# ( u n know n) 0 0.483 34.70 N/A 

# ( unknown ) O 0 

# .8 50 32 .:.

~ 

# 5 M !

~ 

# !/ p 

# ; = 1-- 1

~ 

## . .016 h7' . 50

~ 

## i 0.64 ug/m1 

# r.l-- 2 1.616 25.90 M 0.43 tic/m.l_

4 160.65 1 .G7



# r ' 27

# --25 .600mV

Conpanent * itetentian

(unknawn) o.s F1- 1.

C1- 1.6 Area External

34.20 N/A 66.15 M 4.63

24.60 M 0.40

, 25b.000mV Conditions = Daltile, Dallas, TX Plant 4 Scrubber

: Run #1 ImPs 18:2 = Volume 400 Diluti on 1/1 Date = 05/25/2007 Time = 08 = 4,0 = 53

ComPonent
( E.1nItT1Wvv1"t ) 

# F1__ D Iw.

3 Number Retentian Area External Units
0 0.850 34.20 N/fi .3. .1 .(33 3 66.15 M 0.63 ug/m .!w 

# ? 1.650 24 .6d 11 n. 40 ug/ml

124.95 1.04

i

# 25.00 H N/A 82.60 « 0.75 

# 35.15 H 0.56

n 

# Co nditions : Daltile, Dallas, TX Plant 4 Scrubber

= Run #2 Imps 1&2 : Volume 400 Dilution 1/1 Date : 05/25/2007 Time - 08.49=40



# --25 .600mV 256 .00OmV 

# Component Rptention • 4rea External

(unknown) 0. F1- 1.16 C1- 1.66

m 

# _._-.._ ....... _ ..... ................... ----------- 

# ~

6

6 

### 2

~



# . ;

. ;

, • ~



## 4



# • ;

. i 6 . ....

. ~ ~ 

# : !

~ 

# ._..........__._.._:_.. . , .._ ....__ ...._._..._._.--_....._..._-_ _:---._ .._..__._-._.. -.__..._......_....._.._..--.. ..._.. ........ .. ... ..... ........... - ..... .... .._..._. .. ~ 

# Component Nutmber Retention AreaE External Units ( u nknown ) 0 0.883 25.00 11 N%A F J.— 1 1 -166 82.60 M 0.79 ug/ml. Cl— 2 1.666 35 .1.5 iH 0.58 ug/ml

3 142.75 1.37



# 2 S

# Conditions = Daltile, Dallas, Tn Plant 4 Scrubber = Run #2 Imps 1&2 

# = Volume 400 Dilution 1/1 Qa.te. = 05/25/2007 

## Time - 08:52=09

— 

## 25..600mV 2-56 .00OmV 

# Componeat Reten'' (unknokn) 0.

(unknown)

# FIC1- 

# 4.

1.

~

. 

# Area External 13.00 NiA



## 48.20 M 

# NiA 58.20 M 0.55 

# 32.65 M 0.54

Component 

# ( unknown ) ( unl<nown ) F l -- 

# r_ ]. Number 

# P.etention
0 0.133 0 0 .e83 1 1.150 2 1.633 

# Area External Units
13.00 N / A 

# 48.20 M i•!/A 58.20 lvI 0.56 ug/m 1 32 _65 M 0.54 ug/m 1



# 4 152.05 1.04

© 

# JQ

# Conditions : 

# Daltile, Dallas, TX Plant 4 Scrubber : 

# Run #2 Imps 1&2 : 

# Volume 400 Dilution 1/1 

# Date : 05/25/2007 

# Time : 

# 09:00:49

-25.600mV 256.00ORiV 

# Component ReLention 

# Area Eyternal

0. 

# Fl ci 1 65 .......... 

# i . . ............................................. . ................... . . .... . . ...... . ........................................... . ......... ...................



# 0 

# ol
2 r .».... ;

!



## 3 

# j

.......



# 4

........



# 61

............ .... ........................... ... .......................... . . . . . . . ..... ......... ........................... . .......... ................. .... ... ..... ...... .................. ..................................... 

# 32.20 N/A 70.20 14 0.67 31.58 K 0.52

Number Retention Area External Units
0 0.866 32.20 

# N/A 1 • 1.150 70.20 lvi 

# 0.67 

# Ug/M.I. 2 1.650 31.58 

# 11 O~ 

## 52 

# ug/ml

133.98 1.19 

# Component (unknown) Fl— CI —

3



# 31

# ~ unknown 

# ~ 0.

iiDknown 1.2 

# C1- 1.5 62.40 11.70 14 

# : 28.95 M

. , 

# N/R

N!A 0.48 

# 0©nditions -- Daltile, Dallas, TX Plant 4 Scrubber

= P.un #? Imps 1&2 

# : Volume 400 Dilution 1/1 Date :. 05/25/2007 Time - 09-03-21

—25 . bOOmU 256 . OOOmV 

# Component ReLeniion Rrea External

Number Retention Area External units
0 62.40 N/A 1 1.150 55 . ?5 11 0.53 ua/m.l. Q 1.256 11..7O M N/ A 2 1.650 28.95 11 O.. {•S Lt9/m:l

158 _ 4 0 1.00 

# CarnponAnt 

# ( unl:riown ) F I - ( unknown ) Ci—

4



## 34, ~~ ,

# N/A 0.31 

# N/P
0.43 

# 0. 1. 1.: 1.

~ 

## --25 . 600mV 

# ComponeRt Reten'' (unknown) 0.
(unknown) F1- 

# (unknown)Cl256.00OmV 

# Area External 10.00 II/A



# 20.05 32.35 28.10 26.20 N 

# Conditions = Daltile, Dallas, TX Plant 4 Scrubber

- Pu n #3 Irinps I &2 

# = Volume 400 Dilution 1/1 Date : 05/25/2007 Time = 09 :13. : 53



# Component Number Retenta.o.n Area External Units ( unknown ) 0 0.083 3.o .00 nI/A 

# ( u n k now n) 0 0.850 20.05 N/A F'l— 2 1.033 3.2 .35 0.31 u.9/mI 

# ( u r

~ 

# k. r ~ s.~ 

# w n) i) 1.250 28.10 Iw! r A Cl -- 2 1.633 26 _20 P1 0.4.3 ug/mJ.



# 5 116.70 0.74

~

## Component



# (unknown) (unknawn) F1

- 

# ( unknawn ) C1- —25.600mV



# Reten

~ 

# ion
0.3



## 1,2 

# 1.5 Area Externa

# ► 33.90 N/A 

# 22.50 H Nra 26.20 H 0.25 41.50 M NrA 28.80 N 0.47 

# 256.00OmV 

# Conditions : Daltile, Dallas, TX Plant 4 5crubber

: Run #3 Irnps 1&2 = Volume 400 Dilution 1/1 Date = 05/25/2007 

## Time = 09= 14=56



# Component Number Retention Area External Units ( unknovin ) 0 0.366 33.90 N/A ( u n f<now n) n 0.850 22.50 h1 N/A F1— 1 1.033 26.20 111 0.25 ug/ml ( u n know n) 0 1.250 41.50 M N/A C].— 2 1. 63? 28.80 Mi 0.4.7 ug/ml_

5 152 . 90 0.72



# .14

## Conditions : Daltile,,Da ' Ilas, TX Plant 4 Scrubber : Run #3 Imps 1&2 : V61ume •00 Dilution 1/1 Date : 05/25/2007 Time : 09:23:39



# (unknown) 0 Fl- 

## I 

# (uflknown) I ci• I -25.6.00mV 256.00OmV OMPOneRL l(etf 

## ATea ExterDal



## 21.75 N/A 36.35 0.35 24.90 

## N/A
29.30 H 0.48



## ld 

# .on

. ............ . . ...



## . ......



# 0 

# oi

4 

# ..... ~ :

~ 

# . i

6

. .......

. ................... I 

## ................ . . ......... ............................. ....... ......... . ............... . ......... .

Area External Units
21..75 N/A 36.35 0.35 ug/ml 24.90 N/A 29.30 M 0.48 ug`/ml

112.30 0.83 Component Number Retention (unknown) 0 0..850 Fl- 1 1.050 (unknown) 0 

## 1.250 ci- 2 1.650



# 4

# Area

33.55
23.60 40.00 

# 22.05 N! 

# Externa?
;



# NlA ; 

# i 0.23 ' 

# NlA
0.36 i 

# Conditions : Daltile, Oailas, TX Plartt 4 Scrubber

: Run #3 Imps 1C*X2 

# : Volume 400,Dilution 1/1 Date = 05/25/2007 Time : 09:26=38 , 

# --25 . e00mV 256 .00OmV Component Retention


# (unknown) 0.4 F'1- 1. ( unknoin ) 1.2 cl- 1.6

t 

# ,........._......._.... ~ 

# _._....»..__......___.._.................___..._._._»__....._...._..._.._.._.__..._............._......._.._.._.............._..._._._.__._._......_.._._....._.._......_...

,:. 16 50 "

~ 

# : ;_

~~ 

# •
,. ~ 

# 33

• ~ 

# . ;
; •

_ 3~ 

# ........ :

4`

• ~ ~ 1 • t ~ 

## . . ;

! : ~ 

## f • ~ ~ ~ 

## • ; 

# 61 ...,..... 

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# ~

Number Retention 

# 0 0.416 (3 0.866 1 1.033 0 1.250 

## 2 1.633 

# Area. External Units
33.55 Ni/A 

# 20.45 N/A 23 » 60 0.23 ug/m l - 40.00 N/A 

## 22.05 M 0.36 ug/ml

139 .d5 0.59 

## Component 

# ( unknown ) ' (ur known) Fl- ( unknown ) 

# ci--


# 5

49 . 

# a r

# Conditions z Daltile s Da11as , TX Plant 2!3 rcrubber : Run #S - Imps 1&2 : Volume 400 Di.].ution 1/1 Date : 05f2512007 Time = 09 : 46 : 55



# —25 . 640m'J 256 . U4OmV 

# Component Retention Area Extern4l

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~ 

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# ( uri known )

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## 10.40 N!A 48.85 NlA

# Conditions : Daltile, Dallas, Tn Plant 2/3 Scrubber = Run #1 Imps 1&2 = Volume 400 Di lution 1/1 Date = 05/25/2007 Tirne : '09-49-57

--25 . b00mV 

# Component Ratent' ( unkrown ) 0.3 (unknown) 0.8 

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# Conditions : 

# Daltile, Dallas, TX Plant 2/3 

# Scrubber

: Run #2 imps 1&,2 : 

# Volume 400 Dilution 1/1 

# Date : 05/25/2007 

# Time : 

# 09:58:44

-25.6OOmV 256,OOOmV GOMPODent 

## Pi-etent

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# 44.50 0 1.250 30..70 

# 2 1.650 107.20 

# M

194.15 

# External Units.
N/A 

# 0.4-2 ug/ml IN! / A 

# 1.76 ug 

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## 1

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# NIA 0.44 N!A 1.74 Component Retenti

(unknown) 0.85 

# rl` k . (unknown) 1.23 C1- 1.63 

# Area External

15.70 46.50 24.80 106.30 N 

# Conditions : Daltile, Dallas, TX - Plant 2/3 Scrubber

: Run #2 Imps 1&2 : Volume 400 Dilution - 1/1. Date : 05/25.l2007 Time : 10=10-41

--25 .60OmV 256 .00OmV



## Component ( unknown ) FI - ( un{;nown ) 

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4 193.30 2.19

9 

# 40

# Conditions : 

# Daltile., Dallas, TX Plant 2/3 

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: 

# Run #3 

# Imps.1&2' : 

# Volume 4.00 Dilution 1/1 

# Date : 05/25/2007 

# Time : 

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# Ivi N / 

## A. ci-- 

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4 113.20 0-79

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18.00 i !, ~ ~ 

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# 25.00 M 0.41 ug/rn .l.

129.05 0.83 

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# (unknown) 0. F1- 1. ci- 1. 

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# 42.50 NlA 43,55 M 0.42
25.00 M 0.41



## s



# .~ ~ ~

# Conditions Daltile, Dallas, TX Plant 2/3 

# Scrubber Run #3 

# imps 1&2 Volume 400 Dilution 1/1 

# Date = 05/25/2007 

# Time = 10:31:30



# -25.600mV 256.00OMV Componerit Reteition Area External



## ( 

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105.75 0.75 

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# Conditions = Daltile, Da11as,'TX Plant 2/3 Scrubber = Run #3 Imps 1&2 = Volume 400 Dzlution 1./1 

# Date = 65/25/2007 Time = 10-34=03

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## 39.80 ri 239.02 M 22.07 14 3,81

NiA 4.04 

# N/A Conditions = 3.98 ug/ml F1- in H2SO4



# = 4.6 ug/m 1 C 1'-- i n H2SO4 Date = 05/25/2007 Time = 11=09=37

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# n 1_ 233 39.80 M N/A 2 i. .56b 239.02 11 4.04 ug/m:f. 0 1.916 22.07 11 N/ A



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# Comno.nent ' 

# Concentration

(mg/Lj . ' -Chloride 999 -4- 4

The .concentration i value is based on proven - r.eliable methods of analysis. The estimated uncertainties are two standard'deviations of the concentration:values. The concentration value is warranted to be stable for three months

- from the date of shipment.

•• . t 

# The preparation and analyses of the Chloride Standard was performed with extreme care by the D?ONEX Corporation Consumables Manufacturir.g Department.

Document No. 034 ) 84-2 4

a 20'v;ay 1998

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The concentration value is based. on ,proven , reliable . methods of analysis. The .estimated uncertainties are two standard •deviatioris of the concentration values. The conceritration value is warranted to be stable for three months from the date of shipment. The preparation and analyses of the Fluoride Standard was performed with extreme care by• DIONEX Corporation Consumables Manufacturing Department.

Jocu:neni No. 0341 83• 15 13-Dec-02 

# 50

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# DAPE Armslrong Environrrnenial Inc. CONVERSION FACTORS EPA Melhod 5 522 SerPes Meter Box Calibralion i mtn Hg = 0.13330 kPa Pre-Test Orifice Method 1 cm - 0.39370 inch Encilish Meter Box Units, English K' Factor 1 mm = 0.03937 inch

r i cu 11 = 28.32 lilers Box t, 10 Date: ---------------- -- ------- ? 02109/07
><: 30272 Barontclric Pressure: ----------> 29.35 (in. Hg) - Theorelical Critical Vacuurn: --> 13.84 (in. Hg)



### RTAh For valid lesl resulls, flhe Acltral Vacutrrn should be 1 to 2 in. Hg grealer than Ihe Theoretical Critical Vacuunt shown above. RTAI\ The Crilical Orifice Coefficienl, IC, musl be entered in English uttils, (ft) 1 3'(deg R) 1 0.5!((in.Hg)'(min)).

~

---------------- DRY GAS METER READINGS --------- ------ -CRITICAL ORIFICE READINGS- -- Average Tentperatures -- 

### Voltrrne Volume Volume lnitial Ternps, Final Ternps. Orirrce K' OriGce Actual -- Ambiorc! Temperature -- DGM DGM Ambienl i Tinic Inilial Finat Tolal In1e( Outlet Inlet Outiet Seriall! Coefficient Vacuum htilial Fina1 Average Outlet Overali Temp O) (rnin) (ctr (l) (cu (l) (ctr fl) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.24 5.00 475.500 477.062 1.562 62.0 61.0 62.0 62.0 40 0.242 22.0 61.0 61.0 61.0 521.5 521.8 521.0 0.49 6.00 477.800 480.490 2.690 62.0 62.0 64.0 63.0 48 0.344 20.5 61.0 f 62.0 61.5 522.5 522.8 521.5 0.90 8.00 481.300 486.132 4.832 64.0 63.0 65.0 63.0 55 0.464 19.0 63.0 63.0 63.0 523.0 523.8 523.0 1_50 5.00 486.800 490.670 3.870 65.0 64.0 66.0 64.0 63 0.593 17.0 63.0 63.0 63.0 524.0 524.8 523.0 2.90 5.00 491.900 497.218 5.318 65.0 64.0 66.0 64.0 73 0.824 14.5 63.0 63.0 63.0 524.0 524.8 523.0

........................................... RESULTS ...................................................
Y GAS f11L=TER -- --------- ORIFICE -------- -- DRY GAS METER -- ------- ORIFICE -------


### vIL VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR CALIBRATION FACTOR ECT COf2P.ECTED CORRECT CORRECT NOMINAL Y dH@ (std) Vm(sk!) Vcr(std) Vcr(std) Vcr Valuc Varialiort Valuo Variation :u (1) (liters) (cu (t) (liters) (cu fl) (number) (nurnber) (in H20) (in H20) _551 0.1 1.558 0.1 1.568 1.004 0.007 1.381 -0.0330 ' 667 0.1 2.655 0.1 2.674 0.995 -0.002 1.395 -0.019 .787 0.2 4.763 0.2 4.811 0.995 -0.003 1.414 0.000 .833 0.2 3.808 0.1 3.847 0.994 -0.004 1.438 0.024 285 0.2 5.286 0.2 5.340 1.000 0.003 1.442 0.028 

## Average Y ------- > 0.998 1.414 <------- Average dH@

For Calihralion Faclor Y. tlie ralio of the readirtg of the calibration meler to lhe dry gas meter, 

### r.eptable tolerance of individtral values from the average is +-0.02. •r Orificr. C:+libralion Faclor dH@, ttie orifice differential pressure in inches of H201he1 equales to 0.75 cfni ol air 68 F and 29.92 inchea of Hg,_a,cceptable loleranc.rof individual value

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### s from the average is +-0.2.
Ic ! : S3t E D

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### :,31 C-..1

## Temperature Nleter Calibrations



# Meter Box #: 10 Date: 02/09/07 

## Calibrated By: RT

Emtech 42312 

# Degrees F Calibrator Probe Stack Oven Exit Auxillary
Point 1 32 31 32 32 31 31
Point 2 212 211 212 213 211 211
Point 3 752 752 752 752 751 752

Cmtech 42312 

# Degrees R Caiibrator Probe Stack Oven Exit AuxilEary
Point 1

~



## .. S



## 492 491 492 492

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## ` 491

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## 491
Point 2 o72 671 672 673 671 671
Point 3 1212 1212 1212 1212 1211 1212



# Percent Dir'ference Probe Stack Oven Exit Auxillary
Point 1 0.203252 0 0 0.203252 0.203252
Point 2 0.14881 0 0.148588 0.14881 0.14881
Point 3 0 0 0 0.082508 0



# 60Armstrong Environmental Inc. CONVERSION FACTORS EPA Method 5 511 Series Meter Box Calibration 1 mm Hg = 0.13330 kPa Post-Test Oririce Mathod 1 cm 0.39370 inch English Meter Box Units, English K' Factor 1 mm - 0.03937 inch 1 cu ft= 28.32 liters er Box A 10 Date: ---------------------> 05125/07 ial #: 30272 Barometric Pressure: ----------> 29.40 (in. Hg) Theoretical Critical Vacuum:---> 13.87 (in. Hg)

III

. 'ORTAN For vatid test results, the Actual Vacuum should be 1 to 2 in. Hg greater than the Theoretical Critica! Vacuum shown above. 'ORTAN The Critical Oriflce Coefficient, K', must be entered in English units, (ft)^3 6 (deg R) 1 0.51((in.Hg)'(min)). tll

..

---- ----------- DRY GAS ME'f'ER READINGS ------------•-•- -CRITICAL ORIFICE READINGSTheoretical Critical Vacuum:---> 13.87 (in. Hg) 

### Vofume Volume Volume lnitial Temps. Final Temps. Oririce K' Orifice Actual -- Ambient Temperature -- DGM DGM Ambient dH Time Initial Final Total Inlet - Outlet In1et Outlet Serial# Coefiicient Vacuum Initia) Final Average Outlet Overali Temp 420) (min) (cu ft) (cu ft) (cu ft) (deg F) (deg F) (deg F) (deg F) (number) (see above) (in Hg) (deg F) (deg F) (deg F) (deg R) (deg R) (deg R) 0.90 5.00 495.500 498.536 3.036 73.0 71.0 73.0 72.0 55 0.464 19.0 74.0 74.0 74.0 531.5 532.3 534.0 0.90 5.00 498.536 501.584 3.048 73.0 72.0 74.0 73.0 55 0.464 19.0 74.0 74.0 74.0 532.5 533.0 534.0 0.90 5.00 501.584 504.630 3.046 74.0 73.0 75.0 74.0 55 0.464 19.0 74.0 74.0 74.0 533.5 534.0 534.0

............................................... RESULTS ..................,.......,.....,............ ...... )RY GAS METER --- --------- ORIFICE --------- -- DRY GAS METER --

LUME VOLUME VOLUME VOLUME VOLUME CALIBRATION FACTOR RRECTICORRECTED CORRECTICORRECTI NOMINAL Y /m(std) Vm(std) Vcr(std) Vcr(std) Vcr Value Variation 

### (cu ft) (liters) (cu ft) (liters) (cu ft) (number) (number) 2.965 0.1 2.951 0.1 3.039 0.995 0.001 2.972 0.1 2.951 0.1 3.039 0.993 -0.002 2.965 0.1 2.951 0.1 3.039 0.995 0.001 

# Average Y -------> 0.994

e: For Calibration Factor Y. the ratio of the reading of the calibration meter to the dry gas meter, acceptabie tolerance of individual values from the average is +-0.02. ORIFICE --------

CALIBRATION FACTOR dH@ 

### Vaiue Variatlon (in H20) (in H20) 1.419 0.0027 1.416 -0.000 1.413 -0.003 ID 

# 1.416 - <------- Average dH a?

For Oririce Calibration Factor dH cLD, the_=ifice-d ? entiI pressur n inches of H20 that equates to 0.75 cim of air at 68 F and 29.92 inchesQf-H c' eptable to ranindivid values from the average is +-0.2.

SIGNED: 

## t% Date: 

# ~ 

# 12- .IC)

(M 

# J-'

## Temperature M11leter Calibrations

Meter Box #: 10 Date: 05/27I07 Calibrated By: TA

Emtech Thermo Degrees F Checker Probe Stack Oven Exit Auxillary
Point 1 32 34.9 34 35 34.3 33.8
Point 2 212 215.1 213.6 214 213.8 213.4
Point 3 752 754 753.2 755 752.7 754

Emtech Thermo Degrees R Checker Probe Stack Oven Exit Auxillary

, , Point 1 492 494.9 494 495 494.3 493.8
Point 2 672 675.1 673.6 674 673.8 673.4
Point 3 1212 1214 1213.2 1215 1212.7 1214

Percent Difference Probe Stack Oven Exit Auxillary
Point 1 -0.58943 -0.4065 -0.60976 -0.46748 -0.36585
Point 2 -0.46131 -0.2381 -0.29762 -0.26786 -0.20833
Point 3 -0.16502 -0.09901 -0.24752 -0.05776 -0.16502



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~ ttLTtK ltvCi r':'fIT 1 0. 

## < 31 < _ 5 ° 

# ~

.m } 

## _50 <

~ 

## 2 <



# Y
9 ' A ! 

# 1 1.05 Dt, < P a < 1.5 D
~ 

## 11.0S

~ 

## Jt<Pb<1.5 D.

. ~ 

## 3/16 11 •< Dt ,< 3/8tt

'r 

## A t.a n Y
A tan 8<.0
P a - P 

## b < 0 . ~ 

## 2 5 (t

. 03125 tt _ 0. 063 , t 

# ~ 

# I

~ 

# I i 

# I I

~ 

# I y i

t

., •- ~ 

## 1

~



# ~~ -10 0 < C. < =1

~



## 7°

... 

# i_ -10° < az <

~ 

## -10°



# Commenis:

...... ~ .: ~ :. i~ 

## i 1`.oi.

~ 

## ;; 

## b e 

## /Probe n1amGer ~~~ 

## _ meets or eXceadS al1 speci i iCc ~ 

### iOnS 

# cri

~ 

# eria ?nd/or appl ica51 e desiQn i

~ 

# eai.lir°S" c,

~~ 

# '":1 r 5"" ereh assiqn_ed;"a

.• ~ 

### ,.•' << ~ 

# pi

~ 

# ot tube cal ibra tion ; ac tor of 0.84. ;

~ 

### .•. 

# S i o, i a t'tl r° °

~ 

## aC: 'SeE =0 C>: 60, vo,. 42, yo. 155, hSe:nec 2. V°ri`y :!+t ninitnu:- 2 tinvi se_zack o.' :ne - 

### h er-a 

### o ;~ uvle arc :.

~ e .

~ ini.:..,-, 3/ 4 inc

~ : seDara:ion

~ e:wee 

### n .`e 

### '

~ P'.:_. _s.e arn ~ :."•e nc_Zie as s ~o~ a: :!+° :op o.` :"zs sace.



# F~

# PITOT TUaE INSPECTION DATA SHEET Comparly Name : Pre-sampl e Post Sample

Iw•o[artt " 1

4 — 1 

# Date Date 9124 p

LI 14.

sralr! [ruuc 

# !_ ~ 

# . - V

)- ,,

TK la ACT luisw[t 0 t.laG 1NrK Of M 1101 Rr[ I 1wA 19 tKe r•Iis p Nrw( 1K niAi Litt[ 1LtlL.

~ 

# Y~
«

. . .

rGi[[ 1611I[M49 lcltt MtITIN ~ IM uTles1.[IK I. t1Li W[W 1[O t. !f[itt t..IcITI.G l[Kt

. M1/1«I !Y /1iWUsllit a

~ •

~ . ....r t~~ J

~ ..~L~ .i:.

~ -

. .

.. 

# Y



# c

--

. 1 ,~ 

# -

lfGJM! ININfIrG l[1I

~ t ' ..111 ~ /.. Kn«I..1• ~ M K y



## •~

. 

# .,.._.,. ._.. .—._. ~ 

# . -- - = ~

~ lG

~ t[ .IWt1T11t tl1Kl IN/t!• 

# Comments: level? obstructions?

.. . . damaged? 

# -10 0 < a l < +10 0
-10 0 < a z < +10 0 -50 < $1 < +50. -50 

# <
a Z < +50


# " Y

• • s



# A

1.05 Ot < Pa < 1.5 Dt
1.05 Dt < Pb < 1.5 D t

. 3/16 11 .< Dt .< 3/8 11

AtanY<0.125" 

# A tan @< 0. 03125" 

# Pa = Pb ± 0.063 11 D



# ~ 'L

~ 

# j

0 

# `2,

l 

# 63~

a 3 2 -0 

# Z~ '

~e ~



# Pitot tube/probe number ~~ meets or• exceeds all .specifications criteria and/or appl icab e design features* and is here ned a, : pitot tube cal ibratjon factor of 0.84. =a ,

. •
. . 

# Signature -

.

. ,. 

# Da te CPR 60. Yo . T2, No. 160, Method 2. Yerify the einicum ' 

### 2 inch setback of the thermocouple &nd the ninilt:usa 3/4 inctl 

## ssparatlon bct.csen the pltot tubs and the nozzle +s shown it the top of thls paqt.

fl 

# ~

## ir'OZLL ~ 1~ 

## \SJEC I!ON

~ 

## •Nl7 i'i_nsliR'CMEV I DH IA S1 

# iEET

Cor:rany Name 

# , ~~ ~. Da,te Sam?led .S ~?i ~ ~ 

## - Nozzle Nunber

,


# Presample Inspection i hereby certi fy tnat

- the above re

- F erenced no

- zzle appears to be round, sharp-ed•g•ed, `F ree ol nicks and dents and is judged accept

- able Tor use at thi st.ime. 

# . Zz,s' , zL6 ZLS

~ 

# . ZZ 3) Last P revi ously Measured Nozzl e A•reflp ; do02. 

# ~ ~ t 2 

# s i anature •


# Dat

- n Me?sured

.
, 

# d 

# • Z eS"

~ .



## Post'sample Measurement 

# Measure three didrieters as shown; me.asurernerit ;s in inches; record belov:; aer

- l"orm calculati-ons. t 3. 

# , 27,,57

~

~ • 

# Z

~ 

# 3

~ 

### •'•I

~ 

### rdCe ~ 

### Uid.T, ~~~r 

### • ~ i ~ 

# z D 2

_ 2 c 

# —T

~ 

# - ~ o 

# o 0 2 

# ? ~ 

# , This ar_a s;h ' c 0sed i

- , data reduCtion.

~ 

# ^? =:1

~ ~

^ y •'~~ ~=~~/ '~

~ 

# *

~ 

# :zr.

~~ 

# ;,• '

_ J

~ 

# •

..~ •iii L: i.7:•!C L: ~ ~ 1 i C i G ~~: ~ (:G ~

:i ?

~ :'•E ~

# NOZ ZL;: I NSPtC i i ON /=.hD h9EA.SUR

~ 

# Et

~ 

# = N► 

# DA i A S

~-~~ 

# r i

, 

# Company Nane 

# D ef'U. DaT e Sampl ed ozzi e NumL

~ 

# er



# Presample Inspection

~ 

# hereby cerLi

- ','y tnai the above ref er?nced nQzzl e a?aears to 5e . roLnd, Shara-?dged, f ree of i-iickS and denLs 3nd is• jueged cccepicble Tor use at.

~ 

## his t ime

. 

## . ~~.3 ~ 

# . IfZ

. l 53 .(, 

# rl ~~ 

# :.

, i 

# L asZ' Previ ously M 

# easur?d ' Nozzl e A

~ 

# rea,

~ 

# o i

~ 

## o3
~ 

# IZ s i gin aiur?
Dal-

- e ~ 

## eas! rad. . 0 

## da t A 

# L' o S' m



# Pos tsampl e Measurement Measure three. di a mieters as snotiqn; me.asuremen't is i n i

~ 

# nches; record bel ovr; perforrn cal cul Qt; i ons.

2.

~ 

# .(

~ 

# 12 3. :^ 

## A - veraro- jl i?mnItcr a 192-7


# r,~

~ 

# 3 = r, D2

---T 

### L ), 

# :?

_ ' Z :. ^ ^ r

~ ~h ~ ~r~~ ~ Tlat L (, t
~ ..v ~ rt JL`:G r

~ vJr:iU11.



## d V{

~

### ♦ _ ~ 

### j

i l` 

# r • ~~"~ 

# ""' , ~ 

# l i / ...

~

t ,
, •~•~ i"iunl ;.Il7'vlc

~ !?: 

### ai10 smc

# Barometer Calibrations

Reference Barometer - Prrinco Instruments Hg in Glass - Model 9453 - Serial 41003 0 Date Time Temp, F Watch Actual Difl', % 4wner
I

~ 

# . 0'7 I Z' a , ~~ ~U 

# Z.y :
~ Z~'. ~ ~ 

# --- 2 ..1 ~~ ~~ r 

# 2-1 „ 3 L`

~ .~.~ ~~ 0 ~ a

ro ~ l~ r►1S
~ ro w 

# V`i ~ ~( 

# '2 ~l ~ `~ ' ~'~ {~ r,~~'~

t ~

~

~ 

# i a