### Instructions for completing the Fuel Material Analysis Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Data for multiple boilers should be handled by using separate spreadsheets. Fields that are highlighted in yellow are required fields. Green highlighted cells should be filled using the drop

- down boxes, included. Gray fields are automatically filled from other fields.

Please name each resulting spreadsheet with the following naming convention: [FacilityID]_Unit_[BoilerID]_Fuels_Testing.xls (example: 8100_Unit_2_Fuels_Testing.xls).

Please refer to the following steps when using these spreadsheets.

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet. 2. Please enter the test date on the Boiler Information worksheet. 3. Please choose the type of fuel being sampled using the drop

- down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865 04". 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. 6. Select the HAPs Test Group (i.e., HAP surrogate) for which the tab's data reflects (o range highlighted cell) 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

more. 8. Provide the results of the analyses for each constituent requested. Use the drop

- down boxes to fill in the units of

measure.

### Information

This Information Collection Request (ICR) spreadsheet is intended to collect information about chemical analyses of fuels used fossil fuel burning power plants. Constituents of concern are: mercury, chlorine, fluorine, and metals, such as antimony, beryllium, cadmium, chromium, cobalt, lead, manganese, nickel, and selenium. This spreadsheet is intended to be used for one boiler of one facility but is designed to allow multiple (up to 4) fuel analyses at that specific boiler. Th is number of analyses would coincide with one boiler where emissions testing for all 4 HAP surrogates were being tested. Fields that are highlighted in yellow are down boxes, included. Gray fields are automatically

1. Please enter the EIA Facility Code, Facility Name and Boiler ID of your boiler on the Boiler Information worksheet.

down in the fuel column of the Boiler Information worksheet. If you choose "other", please provide a description of the fuel in the Other Fuel Description column. 4. Please provide the analysis method for each constituent in the Analysis Methods worksheet. For example: "ASTM D5865

- 5. Please check the Units of Measure tables for HHV, Metals, and Cl/Fl in the Picklist worksheet (orange tab). If the units of

measure that you plan to report are not found in the Units of measure table, please fill them in the blank, orange highlighted, cell in each table. This allows you to choose the units of measure in the Fuels Sample Results worksheet. range highlighted cell)

. 7. Provide the Sample Number and Sample Date on the Fuels Sample Results worksheet. You must provide a minimum of 3 composite samples consisting of 3 combined grab samples each, but you are not limited to that number if you have collected

down boxes to fill in the units ofEIA

Facility Code Facility Name Boiler ID Fuel Type 1

708 Hammond Unit 1,2,3,4 

### bituminousFuel Type 2 Fuel Type 3 Other Fuel DescriptionEIA

Facility Code Facility Name Boiler ID Basis An alyte



### 708 Hammond Unit 1,2,3,4 As Received Higher Heating Value 

### 708 Hammond Unit 1,2,3,4 As Received % Moisture 

### 708 Hammond Unit 1,2,3,4 As Received % Ash 

### 708 Hammond Unit 1,2,3,4 As Received % Sulfur 

### 708 Hammond Unit 1,2,3,4 Dry basis Higher Heating Value 

### 708 Hammond Unit 1,2,3,4 Dry basis % Ash 

### 708 Hammond Unit 1,2,3,4 Dry basis % Sulfur 

### 708 Hammond Unit 1,2,3,4 Dry basis Antim ony 

### 708 Hammond Unit 1,2,3,4 Dry basis Arsenic 

### 708 Hammond Unit 1,2,3,4 Dry basis Bery llium 

### 708 Hammond Unit 1,2,3,4 Dry basis Cadmium 

### 708 Hammond Unit 1,2,3,4 Dry basis Chlorine 

### 708 Hammond Unit 1,2,3,4 Dry basis Chromium 

### 708 Hammond Unit 1,2,3,4 Dry basis Cobalt 

### 708 Hammond Unit 1,2,3,4 Dry basis Fluorine 

### 708 Hammond Unit 1,2,3,4 Dry basis Lead 

### 708 Hammond Unit 1,2,3,4 Dry basis Manganese 

### 708 Hammond Unit 1,2,3,4 Dry basis Mercury 

### 708 Hammond Unit 1,2,3,4 Dry basis Nickel 

### 708 Hammond Unit 1,2,3,4 Dry basis SeleniumAn alysis M ethod for each A nalyte

(example: ASTM D5865-04) 

### ASTM D5865 ASTM D5142 ASTM D5142 ASTM D4239 ASTM D5865 ASTM D5142 ASTM D4239 ASTM D3683 ASTM D3683 ASTM D3683 ASTM D3683 ASTM D4208 ASTM D3683 ASTM D3683 ASTM D3761 ASTM D3683 ASTM D3683 ASTM D6722 ASTM D3683 ASTM D4606EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 708 Hammond Unit 1,2,3,4 Mercury and non-mercury metalic HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units 1 

### 2/2/2010 2/2/2010 12201 Btu/lb 2 2/2/2010 2/2/2010 12232 Btu/lb 3 

### 2/3/2010 2/3/2010 12161 Btu/lb 4 2/3/2010 2/3/2010 12208 Btu/lb 5 

### 2/11/2010 2/11/2010 12353 Btu/lb 6 2/11/2010 2/11/2010 12349 Btu/lb Fuel Testing Results

### Mercury and non-mercury metalic HAPs

% Moisture (as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 8.14 11.64 1.00 13283 Btu/lb 12.67 1.09 8.14 11.41 1.01 13316 Btu/lb 12.42 1.10 8.63 11.34 1.03 13310 Btu/lb 12.41 1.12 8.30 11.39 1.03 13313 Btu/lb 12.42 1.12 7.88 11.15 1.24 13410 Btu/lb 12.11 1.34 7.88 11.35 1.24 13404 Btu/lb 12.32 1.34Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 0.04 % 0.08 μg/g <2 μg/g 8 μg/g 2 0.04 % 0.09 μg/g <2 μg/g 8 μg/g 2 0.04 % 0.09 μg/g <2 μg/g 10 μg/g 2 0.04 % 0.09 μg/g <2 μg/g 8 μg/g 2 0.06 % 0.09 μg/g <2 μg/g 16 μg/g 2 0.06 % 0.10 μg/g <2 μg/g 16 μg/g 2Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

Units 

### μg/g <2 μg/g 26 μg/g 10 μg/g 34 μg/g μg/g <2 μg/g 18 μg/g 10 μg/g 37 μg/g μg/g <2 μg/g 18 μg/g 10 μg/g 35 μg/g μg/g <2 μg/g 17 μg/g 10 μg/g 35 μg/g μg/g <2 μg/g 16 μg/g 9 μg/g 55 μg/g μg/g <2 μg/g 16 μg/g 9 μg/g 50 μg/gNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture 

### 17 μg/g <2 μg/g 10 μg/g 8.14 15 μg/g <2 μg/g 10 μg/g 8.14 14 μg/g <2 μg/g 9 μg/g 8.63 14 μg/g <2 μg/g 9 μg/g 8.30 13 μg/g <2 μg/g 9 μg/g 7.88 13 μg/g <2 μg/g 10 μg/g 7.88 Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 31.81 12.67 55.53 70.87 4.50 1.55 1.09 32.14 12.42 55.45 74.73 4.64 1.52 1.10 32.17 12.41 55.42 74.54 4.62 1.43 1.12 31.18 12.42 56.40 74.11 4.67 1.48 1.12 30.85 12.11 57.04 72.17 4.46 1.56 1.34 30.81 12.32 56.87 76.84 4.71 1.54 1.34 Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtOxygen



### 9.32 5.60 5.89 6.21 8.36 3.25EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 708 Hammond Unit 1,2,3,4 Acid gas HAPs

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating

Value (HHV) (as received) HHV Units 1 

### 2/3/2010 2/3/2010 12265 Btu/lb 2 2/8/2010 2/8/2010 11989 Btu/lb 3 2/8/2010 2/8/2010 12013 Btu/lb Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis) 

### 8.18 11.21 1.00 13358 Btu/lb 12.21 1.09 8.66 11.47 1.34 13126 Btu/lb 12.55 1.47 8.71 11.51 1.31 13160 Btu/lb 12.61 1.44Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis) 

### 0.04 % 0.03 % 0.02 %Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units 

### 147 ppm 110 ppm 129 ppmNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Total Moisture Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur 

### 8.18 30.61 12.21 57.17 75.14 4.65 1.46 1.09 8.66 32.06 12.55 55.39 74.06 4.72 1.52 1.47 8.71 32.88 12.61 54.51 73.18 4.59 1.48 1.44

Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Oxygen 

### 5.46 5.68 6.70EIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 708 Hammond Unit 1,2,3,4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date (MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy

ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtEIA

Facility Code Facility

Name Boiler ID HA Ps Test Group 

### 708 Hammond Unit 1,2,3,4

Sample Number (minimum of 3 composite samples) Test Start Date

(MM/DD/YYYY) Test Stop Date

(MM/DD/YYYY) Higher Heating Value (HHV) (as received) HHV Units Fuel Testing Results% Moisture

(as received) % A

sh (as received) % Sulfur

(as received) Higher

Heating Value (HHV) (Dry Basis) HHV Units % A sh (Dry Basis) % Sulfur

(Dry Basis)Chlorine

(Dry Basis) Chlorine

Units Mercury

(Dry Basis) Mercury

Units An timony

(Dry Basis) An timony

Units Arsenic (Dry

Basis) Arsenic

Units Beryllium

(Dry Basis)Beryllium

Units Cadmium

(Dry Basis) Cadmium

Units Chromium

(Dry Basis) Chromium

Units Lead (Dry

Basis) Lead Units Manganese (Dry Basis) Manganese

UnitsNickel (Dry

Basis) Nickel Units Selenium (Dry Basis) Selenium

Units Fluorine

(Dry Basis) Fluorine

Units Cobalt (Dry

Basis) Cobalt Units Total Moisture Proximate Analy ses, % by

wtNote the Proximate/Ultimate data below should be recorded on a dry basis (including ash).

Volatiles As h Fixed Carbon Carbon Hydrogen Nitrogen Total Sulfur Oxygen Proximate Analy

ses, % by

wt Ultimate Analy ses, % by

wtUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the

Fuel Units of Measure - HHV anthracite Btu/lb bitum inous Btu/gallon subbituminous lignite coal refuse (culm or gob) No.2 Fuel Oil (distillate) No.6 Fuel Oil (residual or bunker C) Units of Measure - Metals sy nfuel mg /g petroleum coke μg/g other mg /KgUnits of Measure Tables: Please do not modify these tables, except to add your own unit of measure to the orangehightlighted cell, if necessary

.

Units of Measure - Cl, Fl % ppm