### Name:

Title: Company: Sign Date: Name: Title: Company: Sign Date: Permitted Facility Representative / Date Testing Company Representative / Date Final Test Report for

/ / Based on information and belief formed after reasonable inquiry, I certify that the statements and information in this test report are true, accurate, and complete. I have reviewed all testing details and results in this test report and hereby certify that the test report is authentic and accurate.

Monday, March 07, 2011 Page 1 of 22

### Facility Information:

Costa Sur CS6 Carr. 165

Guayanilla PR Contact:Arsenio Reyes Phone:787-521-4988 Fax: Of above person Email: Of above person Testing Company: URS Corporation 1600 Perimeter Park Drive

Morrisville NC27560 Contact:Richard McMillan Phone:919-461-1217 Fax: Of above person Email:richard_mcmillan@urscorp.com

Air Permit Number: PR4 Permitted Source ID/Name: Enter the Boiler ID of the tested boiler (left) CS6 Permitted Maximum Process Rate: N/A Max. Normal Operation Process Rate: N/A Target Process Test Rate N/A

Description of the source (including control equipment). Please see the attachments for source or process flow diagram: This description should describe the process and associated controls to differentiate this facility from, or document similarity with others of same SCC. Industry/SCC/NAIS221112

Sampling Location Information:

Test Parameter Information: AFS #:Enter ARS ID FRS #:Enter FRS ID

SCC / Description10100401 External Combustion Boilers - Electric Generation - Residual Oil - Grade 6 Oil: Normal Firing

The following state and federal regulations that apply to the proposed testing:

Location Round

Duct Diam. Distance from upstream dist. Distance from

downstream dist. Number of

Traverse Ports Equiv. Diam Min.Travers Points Rect. Duct Length /Width Stack Exit 0 0 0 0 0 0 0 0

Target Parameter Test Method Number of

Test RunsTest Run

DurationSample

Points Comments Location% H2O Method 1 - 4 3 180 0 Stack Exit Carbon Monoxide Method 10 3 120 0 Stack Exit Formaldehyde Method 0011 3 120 0 Stack Exit 2,3,7,8-TCDD Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDD Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDD Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDD Method 23 3 480 0 Stack Exit



### Monday, March 07, 2011 Page 2 of 221,2,3,7,8,9-HxCDD Method 23 3 480 0

Stack Exit 1,2,3,4,6,7,8-HpCDD Method 23 3 480 0 Stack Exit OCDD Method 23 3 480 0 Stack Exit 2,3,7,8-TCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8-PeCDF Method 23 3 480 0 Stack Exit 2,3,4,7,8-PeCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 2,3,4,6,7,8-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,7,8,9-HxCDF Method 23 3 480 0 Stack Exit 1,2,3,4,6,7,8-HpCDF Method 23 3 480 0 Stack Exit 1,2,3,4,7,8,9-HpCDF Method 23 3 480 0 Stack Exit OCDF Method 23 3 480 0 Stack Exit Other TCDD Method 23 0 Stack Exit Other PeCDD Method 23 0 Stack Exit Other HxCDD Method 23 0 Stack Exit Other HpCDD Method 23 0 Stack Exit Other TCDF Method 23 0 Stack Exit Other PeCDF Method 23 0 Stack Exit Other HxCDF Method 23 0 Stack Exit Other HpCDF Method 23 0 Stack Exit Total Dioxins Method 23 3 480 0 Stack Exit Total Furans Method 23 3 480 0 Stack Exit 3,3',4,4'-TCB (PCB77) Method 23 3 480 0 Stack Exit 3,4,4',5-TCB (PCB81) Method 23 3 480 0 Stack Exit 2,3,3',4,4'-PeCB (PCB105) Method 23 3 480 0 Stack Exit 2,3,4,4',5-PeCB (PCB114) Method 23 3 480 0 Stack Exit 2,3',4,4',5-PeCB (PCB118) Method 23 3 480 0 Stack Exit 2',3,4,4',5-PeCB (PCB123) Method 23 3 480 0 Stack Exit 3,3',4,4',5-PeCB (PCB126) Method 23 3 480 0 Stack Exit 2,3,3',4,4',5/2,3,3',4,4',5'-

HxCB (PCBs156/157) Method 23 3 480 0 Stack Exit
2,3',4,4',5,5'-HxCB (PCB167)Method 23 3 480 0 Stack Exit 3,3',4,4',5,5'-HxCB (PCB169)Method 23 3 480 0 Stack Exit 2,3,3',4,4',5,5'-HpCB

(PCB189) Method 23 3 480 0 Stack Exit

Total PCBs Method 23 3 480 0 Stack Exit Total TEQ Method 23 3 480 0 Stack Exit Total organic compounds

(TOC) as Propane Method 25A 3 120 0 Stack Exit Hydrogen Chloride Method 26 3 180 0 Stack Exit Hydrogen Fluoride Method 26 3 180 0 Stack Exit Hydrogen Chloride Method 26A 3 180 0 Stack Exit Hydrogen Fluoride Method 26A 3 180 0 Stack Exit Inorganic (Aqueous)

Condensible Part. OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Filterable PM2.5 OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Organic Condensible

Particulate OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit



### Monday, March 07, 2011 Page 3 of 22

### The following describes any modifications and/or deviations to the applicable test

methods. If alternative methods were requested, see the attachments for documentation of request AND approval, including dates. In this section, identify the promulgation date of any specified test method that you use for determining the procedures followed. This field is also used to document any modifications that are necessary to conduct the emissions test if they are outside the requirements of the cited method. If this modification was approved verbally by a regulatory agency, the name and date of approval should be included. Written formal approval should be attached to this file using the "Attach File" button. Test procedures that are different from those published in the Federal Register should be attached using the "Attach File" button.

Total PM2.5 OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Total Particulate OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Filterable Particulate OTM - 27/28 3 240 0 Use only for dry stacks. Delete Method 5/OTM28 tests. Stack Exit

Arsenic Method 29 3 240 0 Stack Exit Nickel Method 29 3 240 0 Stack Exit Selenium Method 29 3 240 0 Stack Exit Lead Method 29 3 240 0 Stack Exit Chromium Method 29 3 240 0 Stack Exit Cadmium Method 29 3 240 0 Stack Exit Manganese Method 29 3 240 0 Stack Exit Beryllium Method 29 3 240 0 Stack Exit Filterable Particulate Method 29 3 240 0 Stack Exit Antimony Method 29 3 240 0 Stack Exit Co2 Method 3A CO2 3 120 0 Stack Exit Co2 Method 3A CO2 3 240 0 Stack Exit O2 Method 3A O2 3 240 0 Stack Exit O2 Method 3A O2 3 480 0 Stack Exit Co2 Method 3A CO2 3 480 0 Stack Exit O2 Method 3A O2 3 120 0 Stack Exit Inorganic (Aqueous)

Condensible Part. Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Organic Condensible

Particulate Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Total Particulate Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Filterable Particulate Method 5 3 240 0 Stack Exit Filterable Particulate Method 5/OTM-28 3 240 0 Use only for wet stacks. Delete OTM27/OTM28 test. Stack Exit

Sulfur Dioxide Method 6C 3 180 0 Stack Exit Nitrogen oxides (NOx) Method 7E 3 180 0 Stack Exit



### Monday, March 07, 2011 Page 4 of 22

### Sampling / Stack Data Results Summary



### LocationStack Exit - Method 23 Average Run Number 1 2 3 Test Date 6/16/20106/17/2010 6/18/2010 Run Start Time 8:53:00 AM 9:45:00 AM8:53:00 AM

Run Finish Time 6:04:00 PM7:31:00 PM6:04:00 PM Net Run Time, minutes 480 480 480 Dry Gas Meter Volume Sampled, dscf 301.133 276.847 301.133 293.038 Moisture Content of Stack Gas, % 11.42 10.69 11.42 11.177 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Carbon Dioxide, % 12.6 12.5 12.6 12.567 Oxygen, % 5 5.2 5 5.067 Average Stack Gas Temperature, °F 301.67 296.50 301.67 299.947 Dry Volumetric Flow Rate, dry scfm 0.0 0.0 0.0 0.000 Actual Wet Volumetric Flue Gas Flow Rate, acfm 0.0 0.0 0.0 0.000 Percent Isokinetic of Sampling Rate, % 99.4 99.9 99.4 99.567 F-Factor, dscfm/MMBtu @ %O2 9190 9190 9190 9,190.000 Fw 10320 10320 10320 10,320.000 Fc 1420 1420 1420 1,420.000



### Monday, March 07, 2011 Page 5 of 22

### LocationStack Exit - Method 29 Average

Run Number Test Date Run Start Time Run Finish Time Net Run Time, minutes Dry Gas Meter Volume Sampled, dscf Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Carbon Dioxide, % Oxygen, % Average Stack Gas Temperature, °F Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % F-Factor, dscfm/MMBtu @ %O2 Fw Fc



### LocationStack Exit - OTM - 27/28 Average Run Number Test Date Run Start Time Run Finish Time Net Run Time, minutes Stack ExitStack Exit Stack Exit Dry Gas Meter Volume Sampled, dscf 0.153 0.153 0.153 0.153 Moisture Content of Stack Gas, % 29.84 29.85 29.76 29.817 Moisture Saturation at Stack Gas Temperature, % 0.45 0.46 0.46 0.457 Carbon Dioxide, % 89.96 93.29 95.33 92.860 Oxygen, % 45.498 44.973 41.642 44.038 Average Stack Gas Temperature, °F 6.4 5.9 5 5.767 Dry Volumetric Flow Rate, dry scfm 310.00 307.29 307.65 308.313 Actual Wet Volumetric Flue Gas Flow Rate, acfm 1.343523401 236161.27024763

1595531.133735073

99612 1.249

Percent Isokinetic of Sampling Rate, % 78.91 76.41 72.27 75.863 F-Factor, dscfm/MMBtu @ %O2 0 0 0 0.000 Fw 0.000 0.000 0.000 0.000 Fc 0 0 0 0.000



### Monday, March 07, 2011 Page 6 of 22

### Emissions Summary



### Location: Stack Exit - Method 23 Compound: 1,2,3,4,6,7,8-HpCDD Average RunNumber 1 2 3 Mass_mg 0.0000000132 0.0000000077 0.0000000103 0.000 lb/mmBtuO2 1.17E-12 7.50E-13 9.11E-13 0.000 ng/dscm 1.55E-03 9.82E-04 1.21E-03 0.001 ng/dscm@7%O2 1.36E-03 8.69E-04 1.06E-03 0.001 

### Compound: 1,2,3,4,6,7,8-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000084 0.0000000053 0.0000000051 0.000 lb/mmBtuO2 7.43E-13 5.16E-13 4.51E-13 0.000 ng/dscm 9.85E-04 6.76E-04 5.98E-04 0.001 ng/dscm@7%O2 8.61E-04 5.98E-04 5.23E-04 0.001 

### Compound: 1,2,3,4,7,8,9-HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000045 0.0000000057 0.0000000048 0.000 lb/mmBtuO2 3.98E-13 5.55E-13 4.25E-13 0.000 ng/dscm 5.28E-04 7.27E-04 5.63E-04 0.001 ng/dscm@7%O2 4.62E-04 6.44E-04 4.92E-04 0.001 

### Compound: 1,2,3,4,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000001773 0.0000000025 0.0000000017 0.000 lb/mmBtuO2 1.57E-11 2.44E-13 1.50E-13 0.000 ng/dscm 2.08E-02 3.19E-04 1.99E-04 0.007 ng/dscm@7%O2 1.82E-02 2.82E-04 1.74E-04 0.006 

### Compound: 1,2,3,4,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000039 0.0000000032 0.0000000018 0.000 lb/mmBtuO2 3.45E-13 3.12E-13 1.59E-13 0.000 ng/dscm 4.57E-04 4.08E-04 2.11E-04 0.000 ng/dscm@7%O2 4.00E-04 3.61E-04 1.84E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000032 0.0000000026 0.0000000018 0.000 lb/mmBtuO2 2.83E-13 2.53E-13 1.59E-13 0.000 ng/dscm 3.75E-04 3.32E-04 2.11E-04 0.000 ng/dscm@7%O2 3.28E-04 2.94E-04 1.84E-04 0.000 

### Compound: 1,2,3,6,7,8-HxCDF Average



### Monday, March 07, 2011 Page 7 of 22RunNumber 1 2 3 Mass_mg 0.0000000048 0.000000004 0.0000000017 0.000 lb/mmBtuO2 4.25E-13 3.90E-13 1.50E-13 0.000 ng/dscm 5.63E-04 5.10E-04 1.99E-04 0.000 ng/dscm@7%O2 4.92E-04 4.52E-04 1.74E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000034 0.0000000027 0.0000000018 0.000 lb/mmBtuO2 3.01E-13 2.63E-13 1.59E-13 0.000 ng/dscm 3.99E-04 3.44E-04 2.11E-04 0.000 ng/dscm@7%O2 3.49E-04 3.05E-04 1.84E-04 0.000 

### Compound: 1,2,3,7,8,9-HxCDF Average RunNumber 1 2 3 Mass_mg 0.000000002 0.000000002 0.0000000019 0.000 lb/mmBtuO2 1.77E-13 1.95E-13 1.68E-13 0.000 ng/dscm 2.35E-04 2.55E-04 2.23E-04 0.000 ng/dscm@7%O2 2.05E-04 2.26E-04 1.95E-04 0.000 

### Compound: 1,2,3,7,8-PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000036 0.0000000036 0.0000000028 0.000 lb/mmBtuO2 3.18E-13 3.51E-13 2.48E-13 0.000 ng/dscm 4.22E-04 4.59E-04 3.28E-04 0.000 ng/dscm@7%O2 3.69E-04 4.06E-04 2.87E-04 0.000 

### Compound: 1,2,3,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.000000003 0.0000000049 0.0000000026 0.000 lb/mmBtuO2 2.65E-13 4.77E-13 2.30E-13 0.000 ng/dscm 3.52E-04 6.25E-04 3.05E-04 0.000 ng/dscm@7%O2 3.08E-04 5.53E-04 2.67E-04 0.000 

### Compound:2,3,3',4,4',5,5'-HpCB (PCB189) Average RunNumber 1 2 3 Mass_mg 0.0000000538 0.0000000302 0.0000002223 0.000 lb/mmBtuO2 4.76E-12 2.94E-12 1.97E-11 0.000 ng/dscm 6.31E-03 3.85E-03 2.61E-02 0.012 ng/dscm@7%O2 5.52E-03 3.41E-03 2.28E-02 0.011 

### Compound:2,3,3',4,4',5/2,3,3',4,4',5'-HxCB (PC Average RunNumber 1 2 3 Mass_mg 0.00000138617 0.00000060362 0.00000613904 0.000 lb/mmBtuO2 1.23E-10 5.88E-11 5.43E-10 0.000 ng/dscm 1.63E-01 7.70E-02 7.20E-01 0.320 ng/dscm@7%O2 1.42E-01 6.82E-02 6.29E-01 0.280



### Monday, March 07, 2011 Page 8 of 22

### Compound:2,3,3',4,4'-PeCB (PCB105) Average RunNumber 1 2 3 Mass_mg 0.0000052663 0.00000240275 0.00002131948 0.000 lb/mmBtuO2 4.66E-10 2.34E-10 1.89E-09 0.000 ng/dscm 6.18E-01 3.07E-01 2.50E+00 1.142 ng/dscm@7%O2 5.40E-01 2.72E-01 2.19E+00 1.001 

### Compound:2,3',4,4',5,5'-HxCB (PCB167) Average RunNumber 1 2 3 Mass_mg 0.00000067746 0.00000029329 0.00000307175 0.000 lb/mmBtuO2 5.99E-11 2.86E-11 2.72E-10 0.000 ng/dscm 7.95E-02 3.74E-02 3.60E-01 0.159 ng/dscm@7%O2 6.95E-02 3.31E-02 3.15E-01 0.139 

### Compound:2,3,4,4',5-PeCB (PCB114) Average RunNumber 1 2 3 Mass_mg 0.00000025867 0.00000013541 0.00000102012 0.000 lb/mmBtuO2 2.29E-11 1.32E-11 9.02E-11 0.000 ng/dscm 3.03E-02 1.73E-02 1.20E-01 0.056 ng/dscm@7%O2 2.65E-02 1.53E-02 1.05E-01 0.049 

### Compound:2,3',4,4',5-PeCB (PCB118) Average RunNumber 1 2 3 Mass_mg 0.0000141047 0.0000066382 0.0000570141 0.000 lb/mmBtuO2 1.25E-09 6.47E-10 5.04E-09 0.000 ng/dscm 1.65E+00 8.47E-01 6.69E+00 3.062 ng/dscm@7%O2 1.44E+00 7.50E-01 5.85E+00 2.680 

### Compound:2',3,4,4',5-PeCB (PCB123) Average RunNumber 1 2 3 Mass_mg 0.00000049219 0.00000023194 0.00000181191 0.000 lb/mmBtuO2 4.35E-11 2.26E-11 1.60E-10 0.000 ng/dscm 5.77E-02 2.96E-02 2.13E-01 0.100 ng/dscm@7%O2 5.04E-02 2.62E-02 1.86E-01 0.088 

### Compound:2,3,4,6,7,8-HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000039 0.0000000037 0.0000000017 0.000 lb/mmBtuO2 3.45E-13 3.60E-13 1.50E-13 0.000 ng/dscm 4.57E-04 4.72E-04 1.99E-04 0.000 ng/dscm@7%O2 4.00E-04 4.18E-04 1.74E-04 0.000 

### Compound:2,3,4,7,8-PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000077 0.0000000072 0.0000000036 0.000 lb/mmBtuO2 6.81E-13 7.01E-13 3.18E-13 0.000



### Monday, March 07, 2011 Page 9 of 22ng/dscm 9.03E-04 9.19E-04 4.22E-04 0.001 ng/dscm@7%O2 7.89E-04 8.14E-04 3.69E-04 0.001 

### Compound:2,3,7,8-TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000027 0.0000000025 0.0000000023 0.000 lb/mmBtuO2 2.39E-13 2.44E-13 2.03E-13 0.000 ng/dscm 3.17E-04 3.19E-04 2.70E-04 0.000 ng/dscm@7%O2 2.77E-04 2.82E-04 2.36E-04 0.000 

### Compound:2,3,7,8-TCDF Average RunNumber 1 2 3 Mass_mg 0.0000000026 0.0000000033 0.0000000031 0.000 lb/mmBtuO2 2.30E-13 3.21E-13 2.74E-13 0.000 ng/dscm 3.05E-04 4.21E-04 3.64E-04 0.000 ng/dscm@7%O2 2.67E-04 3.73E-04 3.18E-04 0.000 

### Compound: 3,3',4,4',5,5'-HxCB (PCB169) Average RunNumber 1 2 3 Mass_mg 0.00000001586 0.00000001126 0.00000006164 0.000 lb/mmBtuO2 1.40E-12 1.10E-12 5.45E-12 0.000 ng/dscm 1.86E-03 1.44E-03 7.23E-03 0.004 ng/dscm@7%O2 1.63E-03 1.27E-03 6.32E-03 0.003 

### Compound: 3,3',4,4',5-PeCB (PCB126) Average RunNumber 1 2 3 Mass_mg 0.00000062637 0.00000025637 0.00000289642 0.000 lb/mmBtuO2 5.54E-11 2.50E-11 2.56E-10 0.000 ng/dscm 7.35E-02 3.27E-02 3.40E-01 0.149 ng/dscm@7%O2 6.43E-02 2.90E-02 2.97E-01 0.130 

### Compound: 3,3',4,4'-TCB (PCB77) Average RunNumber 1 2 3 Mass_mg 0.00000529663 0.00000231531 0.00002455616 0.000 lb/mmBtuO2 4.68E-10 2.26E-10 2.17E-09 0.000 ng/dscm 6.21E-01 2.95E-01 2.88E+00 1.265 ng/dscm@7%O2 5.43E-01 2.61E-01 2.52E+00 1.108 

### Compound: 3,4,4',5-TCB (PCB81) Average RunNumber 1 2 3 Mass_mg 0.00000024353 0.00000010789 0.00000107416 0.000 lb/mmBtuO2 2.15E-11 1.05E-11 9.50E-11 0.000 ng/dscm 2.86E-02 1.38E-02 1.26E-01 0.056 ng/dscm@7%O2 2.50E-02 1.22E-02 1.10E-01 0.049 

### Compound:OCDD Average RunNumber 1 2 3 

### Monday, March 07, 2011 Page 10 of 22Mass_mg 0.0000000881 0.0000000507 0.0000000673 0.000 lb/mmBtuO2 7.79E-12 4.94E-12 5.95E-12 0.000 ng/dscm 1.03E-02 6.47E-03 7.89E-03 0.008 ng/dscm@7%O2 9.00E-03 5.73E-03 6.90E-03 0.007 

### Compound:OCDF Average RunNumber 1 2 3 Mass_mg 0.000000017 0.0000000095 0.0000000131 0.000 lb/mmBtuO2 1.50E-12 9.26E-13 1.16E-12 0.000 ng/dscm 1.99E-03 1.21E-03 1.54E-03 0.002 ng/dscm@7%O2 1.74E-03 1.07E-03 1.35E-03 0.001 

### Compound:Other HpCDD Average RunNumber 1 2 3 Mass_mg 0.0000000162 0.0000000126 0.0000000221 0.000 lb/mmBtuO2 1.43E-12 1.23E-12 1.95E-12 0.000 ng/dscm 1.90E-03 1.61E-03 2.59E-03 0.002 ng/dscm@7%O2 1.66E-03 1.43E-03 2.26E-03 0.002 

### Compound:Other HpCDF Average RunNumber 1 2 3 Mass_mg 0.0000000048 0 0 0.000 lb/mmBtuO2 4.25E-13 0.00E+00 0.00E+00 0.000 ng/dscm 5.63E-04 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 4.92E-04 0.00E+00 0.00E+00 0.000 

### Compound:Other HxCDD Average RunNumber 1 2 3 Mass_mg 0.0000000176 0.0000000118 0.0000000356 0.000 lb/mmBtuO2 1.56E-12 1.15E-12 3.15E-12 0.000 ng/dscm 2.06E-03 1.51E-03 4.18E-03 0.003 ng/dscm@7%O2 1.80E-03 1.34E-03 3.65E-03 0.002 

### Compound:Other HxCDF Average RunNumber 1 2 3 Mass_mg 0.0000000109 0.0000000073 0.0000000032 0.000 lb/mmBtuO2 9.64E-13 7.11E-13 2.83E-13 0.000 ng/dscm 1.28E-03 9.31E-04 3.75E-04 0.001 ng/dscm@7%O2 1.12E-03 8.24E-04 3.28E-04 0.001 

### Compound:Other PeCDD Average RunNumber 1 2 3 Mass_mg 0.0000000131 0.0000000085 0.0000000375 0.000 lb/mmBtuO2 1.16E-12 8.28E-13 3.32E-12 0.000 ng/dscm 1.54E-03 1.08E-03 4.40E-03 0.002 ng/dscm@7%O2 1.35E-03 9.56E-04 3.85E-03 0.002



### Monday, March 07, 2011 Page 11 of 22

### Compound:Other PeCDF Average RunNumber 1 2 3 Mass_mg 0.0000000362 0.0000000318 0 0.000 lb/mmBtuO2 3.20E-12 3.10E-12 0.00E+00 0.000 ng/dscm 4.25E-03 4.06E-03 0.00E+00 0.003 ng/dscm@7%O2 3.72E-03 3.59E-03 0.00E+00 0.002 

### Compound:Other TCDD Average RunNumber 1 2 3 Mass_mg 0.0000000265 0.0000000234 0.0000000606 0.000 lb/mmBtuO2 2.34E-12 2.28E-12 5.36E-12 0.000 ng/dscm 3.11E-03 2.99E-03 7.11E-03 0.004 ng/dscm@7%O2 2.72E-03 2.65E-03 6.22E-03 0.004 

### Compound:Other TCDF Average RunNumber 1 2 3 Mass_mg 0.0000001116 0.0000000853 0.0000000183 0.000 lb/mmBtuO2 9.87E-12 8.31E-12 1.62E-12 0.000 ng/dscm 1.31E-02 1.09E-02 2.15E-03 0.009 ng/dscm@7%O2 1.15E-02 9.65E-03 1.88E-03 0.008 

### Compound:Total Dioxins Average RunNumber 1 2 3 Mass_mg 0.0000002915 0.000000072197 0.00000008807 0.000 lb/mmBtuO2 2.58E-11 7.03E-12 7.79E-12 0.000 ng/dscm 3.42E-02 9.21E-03 1.03E-02 0.018 ng/dscm@7%O2 2.99E-02 8.15E-03 9.00E-03 0.016 

### Compound:Total Furans Average RunNumber 1 2 3 Mass_mg 0.0000000577 0.000000048965 0.00000003931 0.000 lb/mmBtuO2 5.10E-12 4.77E-12 3.48E-12 0.000 ng/dscm 6.77E-03 6.25E-03 4.61E-03 0.006 ng/dscm@7%O2 5.92E-03 5.53E-03 4.03E-03 0.005 

### Compound:Total PCBs Average RunNumber 1 2 3 Mass_mg 0.0000284217 0.0000130262 0.0001191871 0.000 lb/mmBtuO2 2.51E-09 1.27E-09 1.05E-08 0.000 ng/dscm 3.33E+00 1.66E+00 1.40E+01 6.330 ng/dscm@7%O2 2.91E+00 1.47E+00 1.22E+01 5.527 

### Compound:Total TEQ Average RunNumber 1 2 3 Mass_mg 0 0 0 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.00E+00 0.000



### Monday, March 07, 2011 Page 12 of 22ng/dscm 0.00E+00 0.00E+00 0.00E+00 0.000 ng/dscm@7%O2 0.00E+00 0.00E+00 0.00E+00 0.000



### Location: Stack Exit - Method 29 Compound:Antimony Average RunNumber 1 2 3 Mass_mg 0.0214 0.01619 0.019847 0.019 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 4.02E-06 3.27E-06 3.76E-06 0.000 mg/dscm 5.20E-03 4.25E-03 5.01E-03 0.005 mg/dscm@7%O2 4.66E-03 3.79E-03 4.35E-03 0.004 

### Compound:Arsenic Average RunNumber 1 2 3 Mass_mg 0.035 0.02748 0.0328 0.032 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 6.58E-06 5.54E-06 6.21E-06 0.000 mg/dscm 8.50E-03 7.21E-03 8.29E-03 0.008 mg/dscm@7%O2 7.62E-03 6.42E-03 7.20E-03 0.007 

### Compound:Beryllium Average RunNumber 1 2 3 Mass_mg 0.0014 0.001125 0.001412 0.001 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 2.63E-07 2.27E-07 2.67E-07 0.000 mg/dscm 3.40E-04 2.95E-04 3.57E-04 0.000 mg/dscm@7%O2 3.05E-04 2.63E-04 3.10E-04 0.000 

### Compound:Cadmium Average RunNumber 1 2 3 Mass_mg 0.0003 0.00036 0.00031 0.000 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 5.64E-08 7.26E-08 5.87E-08 0.000 mg/dscm 7.29E-05 9.45E-05 7.83E-05 0.000 mg/dscm@7%O2 6.54E-05 8.42E-05 6.80E-05 0.000 

### Compound:Chromium Average RunNumber 1 2 3 Mass_mg 0.027 0.01858 0.02068 0.022 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 5.07E-06 3.75E-06 3.91E-06 0.000 mg/dscm 6.56E-03 4.88E-03 5.22E-03 0.006 mg/dscm@7%O2 5.88E-03 4.35E-03 4.53E-03 0.005 

### Compound:Filterable Particulate Average RunNumber 1 2 3 Mass_mg 139.4 108.9 131.2 126.500



### Monday, March 07, 2011 Page 13 of 22Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 2.62E-02 2.20E-02 2.48E-02 0.024 mg/dscm 3.39E+01 2.86E+01 3.31E+01 31.867 mg/dscm@7%O2 3.04E+01 2.55E+01 2.88E+01 28.233 

### Compound:Lead Average RunNumber 1 2 3 Mass_mg 0.0181 0.01339 0.01603 0.016 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 3.40E-06 2.70E-06 3.03E-06 0.000 mg/dscm 4.40E-03 3.52E-03 4.05E-03 0.004 mg/dscm@7%O2 3.95E-03 3.14E-03 3.52E-03 0.004 

### Compound:Manganese Average RunNumber 1 2 3 Mass_mg 0.283 0.229072 0.273652 0.262 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 5.32E-05 4.62E-05 5.18E-05 0.000 mg/dscm 6.88E-02 6.01E-02 6.91E-02 0.066 mg/dscm@7%O2 6.17E-02 5.36E-02 6.00E-02 0.058 

### Compound:Nickel Average RunNumber 1 2 3 Mass_mg 2.5704 1.97611 2.32351 2.290 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 4.83E-04 3.99E-04 4.40E-04 0.000 mg/dscm 6.25E-01 5.19E-01 5.87E-01 0.577 mg/dscm@7%O2 5.60E-01 4.62E-01 5.10E-01 0.511 

### Compound: Selenium Average RunNumber 1 2 3 Mass_mg 0.0105 0.00811 0.01841 0.012 Elb/hr 0.00E+00 0.00E+00 0.00E+00 0.000 lb/mmBtuO2 1.97E-06 1.64E-06 3.49E-06 0.000 mg/dscm 2.55E-03 2.13E-03 4.65E-03 0.003 mg/dscm@7%O2 2.29E-03 1.90E-03 4.04E-03 0.003



### Location: Stack Exit - OTM - 27/28 Compound:Filterable Particulate Average RunNumber 1 2 3 Mass_mg 0 0 0 0.000 lb/mmBtuO2 0.00E+00 0.00E+00 0.00E+00 0.000 

### Compound:Filterable PM2.5 Average RunNumber 1 2 3 Mass_mg 144.3 34.8 10.8 63.300 lb/mmBtuO2 9.26E-02 2.18E-02 6.91E-03 0.040



### Monday, March 07, 2011 Page 14 of 22

### Process Run Data

Compound:Inorganic (Aqueous) Condensible Pa Average RunNumber 1 2 3 Mass_mg 3.3 3.3 5.9 4.167 lb/mmBtuO2 2.12E-03 2.07E-03 3.77E-03 0.003 

### Compound:Organic Condensible Particulate Average RunNumber 1 2 3 Mass_mg 28.6 14.2 26.7 23.167 lb/mmBtuO2 1.84E-02 8.91E-03 1.71E-02 0.015 

### Compound:Total Particulate Average RunNumber 1 2 3 Mass_mg 223 89.3 76.4 129.567 lb/mmBtuO2 1.43E-01 5.61E-02 4.89E-02 0.083 

### Compound:Total PM2.5 Average RunNumber 1 2 3 Mass_mg 78.7 54.5 65.6 66.267 lb/mmBtuO2 5.05E-02 3.42E-02 4.20E-02 0.042



### Monday, March 07, 2011 Page 15 of 22

### Process Run Data



### Run Name Value UOM Comments Target Value 1 Residual Oil (No. 6) Burned 164.3 1000 Gallons/million BTU using O2 0 

### 2Residual Oil (No. 6) Burned 159.9 1000 Gallons/million BTU using O2 0 3 Residual Oil (No. 6) Burned 165.2 1000 Gallons/million BTU using O2 0 4 Residual Oil (No. 6) Burned 177.6 1000 Gallons/million BTU using O2 0 

### 5 Residual Oil (No. 6) Burned 173 1000 Gallons/million BTU using O2 0 1 Average Heat Input 3086.2MMBtu/hr 0 2 Average Heat Input 3003.6MMBtu/hr 0 

### 3 Average Heat Input 3103.1MMBtu/hr 0 4 Average Heat Input 3336 MMBtu/hr 0 5 Average Heat Input 3249.6MMBtu/hr 0 

### 1 Steam Output 20211000 lb steam/hr 0 2 Steam Output 19281000 lb steam/hr 0 3 Steam Output 20641000 lb steam/hr 0 

### 4 Steam Output 22461000 lb steam/hr 0 5 Steam Output 20431000 lb steam/hr 0 1 Synfuel Firing Rate 0 0 

### 2 Synfuel Firing Rate 0 0 3 Synfuel Firing Rate 0 0 4 Synfuel Firing Rate 0 0 

### 5 Synfuel Firing Rate 0 0 1 Petroleum Coke Firing Rate 0 0 2Petroleum Coke Firing Rate 0 0 

### 3 Petroleum Coke Firing Rate 0 0 4Petroleum Coke Firing Rate 0 0 

### 5 Petroleum Coke Firing Rate 0 0 1 Coal Gas Firing Rate 0 0 2 Coal Gas Firing Rate 0 0 

### 3 Coal Gas Firing Rate 0 0 4 Coal Gas Firing Rate 0 0 5 Coal Gas Firing Rate 0 0 

### 1 Fuel Oil Firing Rate 0 0 2Fuel Oil Firing Rate 0 0 3 Fuel Oil Firing Rate 0 0



### Monday, March 07, 2011 Page 16 of 22

### 4 Fuel Oil Firing Rate 0 0



### 5 Fuel Oil Firing Rate 0 0 1 Flue Gas Flow Rate 0 dscfm 0 2Flue Gas Flow Rate 0 dscfm 0 

### 3 Flue Gas Flow Rate 0 dscfm 0 4 Flue Gas Flow Rate 0 dscfm 0 5 Flue Gas Flow Rate 0 dscfm 0 

### 1 Pressure Drop Across FGD (if applicable) 0 in H20 0 2 Pressure Drop Across FGD (if applicable) 0 in H20 0 3 Pressure Drop Across FGD (if applicable) 0 in H20 0 

### 4 Pressure Drop Across FGD (if applicable) 0 in H20 0 5 Pressure Drop Across FGD (if applicable) 0 in H20 0 1 FGD Scrubber Liquor pH 0 pH 0 

### 2FGD Scrubber Liquor pH 0 pH 0 3 FGD Scrubber Liquor pH 0 pH 0 4 FGD Scrubber Liquor pH 0 pH 0 

### 5 FGD Scrubber Liquor pH 0 pH 0 1 FGD Scrubber Liquor Flow Rate 0 gal/min 0 2FGD Scrubber Liquor Flow Rate 0 gal/min 0 

### 3 FGD Scrubber Liquor Flow Rate 0 gal/min 0 4 FGD Scrubber Liquor Flow Rate 0 gal/min 0 

### 5 FGD Scrubber Liquor Flow Rate 0 gal/min 0 1 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0

2 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0



### 3 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0

4 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0

5 Sorbent Type and Sorbent Injection Rate (if applicable) 0 lb/hr 0



### 1 Flue Gas Oxygen Content 2 % 0 2Flue Gas Oxygen Content 1.6 % 0 3 Flue Gas Oxygen Content 1.7 % 0 

### 4Flue Gas Oxygen Content 1.9 % 0 5 Flue Gas Oxygen Content 1.9 % 0 1 Flue Gas Carbon Dioxide Content 0 % 0



### Monday, March 07, 2011 Page 17 of 22

### 2Flue Gas Carbon Dioxide Content 0 % 0



### 3 Flue Gas Carbon Dioxide Content 0 % 0 4 Flue Gas Carbon Dioxide Content 0 % 0 5 Flue Gas Carbon Dioxide Content 0 % 0 

### 1 Flue Gas Moisture Content 0 % 0 2Flue Gas Moisture Content 0 % 0 3 Flue Gas Moisture Content 0 % 0 

### 4Flue Gas Moisture Content 0 % 0 5 Flue Gas Moisture Content 0 % 0 1 Flue Gas Sampling Point Temperature 0 Deg F 0 

### 2Flue Gas Sampling Point Temperature 0 Deg F 0 3 Flue Gas Sampling Point Temperature 0 Deg F 0 4 Flue Gas Sampling Point Temperature 0 Deg F 0 

### 5 Flue Gas Sampling Point Temperature 0 Deg F 0 1 Flue Gas Pressure 0 atm 0 2Flue Gas Pressure 0 atm 0 

### 3 Flue Gas Pressure 0 atm 0 4 Flue Gas Pressure 0 atm 0 5 Flue Gas Pressure 0 atm 0 

### 1 Standard Pressure 0 atm 0 2 Standard Pressure 0 atm 0 

### 3 Standard Pressure 0 atm 0 4 Standard Pressure 0 atm 0 5 Standard Pressure 0 atm 0 

### 1 Standard Temperature 0 Deg F 0 2 Standard Temperature 0 Deg F 0 3 Standard Temperature 0 Deg F 0 

### 4 Standard Temperature 0 Deg F 0 5 Standard Temperature 0 Deg F 0 1 Unit Gross Electrical Output 340 MW 0 

### 2Unit Gross Electrical Output 327 MW 0 3 Unit Gross Electrical Output 344 MW 0 4 Unit Gross Electrical Output 363 MW 0 

### 5 Unit Gross Electrical Output 356 MW 0 1 Unit Net Electric Generation 0 MWh 0 2 Unit Net Electric Generation 0 MWh 0



### Monday, March 07, 2011 Page 18 of 22

### APCD Run Data

Process Lab Run Data 3 Unit Net Electric Generation 0 MWh 0 

### 4Unit Net Electric Generation 0 MWh 0 5 Unit Net Electric Generation 0 MWh 0

Run Name Value UOM Comments Target Value 

### 1 List all emissions control devices in order of process flow. Choose from 0 0

1 drop down lists. If not on list add description and provide detailed 0 0



### 1 desription in section 5a. 0 0

Run Name ValueUOM Comments 1 See 4b Comments. 0



### Monday, March 07, 2011 Page 19 of 22

### Sampling / Stack Data Results Detail



### LocationStack Exit - Method 23 Average Run Number 1 2 3 Test Date 6/16/2010 6/17/2010 6/18/2010 Run Start Time 8:53:00 AM9:45:00 AM8:53:00 AM Run Finish Time 6:04:00 PM7:31:00 PM6:04:00 PM Net Traversing Points 49 49 49 Net Run Time, minutes 480 480 480 Nozzle Diameter, inches 0.22 0.22 0.22 0.220 Pitot Tube Coefficient 0.84 0.84 0.84 0.840 Dry Gas Meter Calibration Factor 1.032 1.032 1.032 1.032 Barometric Pressure, inches of Mercury 29.8 29.85 29.8 29.817 Average Orifice Meter Differential, inches H2O 1.42 1.17 1.42 1.337 Dry Gas Meter Volume Sampled, cubic feet 315.746 281.352 315.746 304.281 Average Dry Gas Meter Temperature, °F 111.04 94.06 111.04 105.380 Dry Gas Meter Volume Sampled, dscf 301.133 276.847 301.133 293.038 Total Moisture Liquid collected, g 825.2 703.8 825.2 784.733 Volume of Water Vapor, standard cubic feet 38.84 33.13 38.84 36.937 Moisture Content of Stack Gas, % 11.42 10.69 11.42 11.177 Moisture Saturation at Stack Gas Temperature, % 100.00 100.00 100.00 100.000 Dry Mole Fraction 0.8858 0.8931 0.8858 0.888 Carbon Dioxide, % 12.6 12.5 12.6 12.567 Oxygen, % 5 5.2 5 5.067 Carbon Monoxide & Nitrogen, % 82.4 82.3 82.4 82.367 Fuel Factor 1.26 1.26 1.26 Dry Molecular Weight, lb/lb-Mole 30.22 30.21 30.22 30.217 Wet Molecular weight, lb/lb-Mole 28.82 28.90 28.82 28.847 Flue Gas Static Pressure, inches of H2O 0.2 0.2 0.2 0.200 Absolute Flue Gas Pressure, inches of Mercury 29.81 29.86 29.81 29.827 Average Stack Gas Temperature, °F 301.67 296.50 301.67 299.947 Average Velocity Head, inches of H2O 0.9272984167 819370.760113675

2220320.927298416

781938 0.872 Average Stack Gas Velocity, feet/second 65.11 58.62 65.11 62.947 Stack Cross-Sectional Area, square feet 0.000 0.000 0.000 0.000 Dry Volumetric Flow Rate, dry scfm 0.0 0.0 0.0 0.000 Actual Wet Volumetric Flue Gas Flow Rate, acfm 0.0 0.0 0.0 0.000 Percent Isokinetic of Sampling Rate, % 99.4 99.9 99.4 99.567 Percent Excess Air, % 29.8 31.5 29.8 30.367 F-Factor, dscfm/MMBtu @ %O2 9190 9190 91909,190.000 Round Duct Diameter, inches 0 0 0 Rectangular Duct Width, inches 0 0 0 Rectangular Duct Length, inches 0 0 0 Fw 10320 10320 1032010,320.000 Fc 1420 1420 14201,420.000



### Monday, March 07, 2011 Page 20 of 22

### LocationStack Exit - Method 29 Average

Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Nozzle Diameter, inches Pitot Tube Coefficient Dry Gas Meter Calibration Factor Barometric Pressure, inches of Mercury Average Orifice Meter Differential, inches H2O Dry Gas Meter Volume Sampled, cubic feet Average Dry Gas Meter Temperature, °F Dry Gas Meter Volume Sampled, dscf Total Moisture Liquid collected, g Volume of Water Vapor, standard cubic feet Moisture Content of Stack Gas, % Moisture Saturation at Stack Gas Temperature, % Dry Mole Fraction Carbon Dioxide, % Oxygen, % Carbon Monoxide & Nitrogen, % Fuel Factor Dry Molecular Weight, lb/lb-Mole Wet Molecular weight, lb/lb-Mole Flue Gas Static Pressure, inches of H2O Absolute Flue Gas Pressure, inches of Mercury Average Stack Gas Temperature, °F Average Velocity Head, inches of H2O Average Stack Gas Velocity, feet/second Stack Cross-Sectional Area, square feet Dry Volumetric Flow Rate, dry scfm Actual Wet Volumetric Flue Gas Flow Rate, acfm Percent Isokinetic of Sampling Rate, % Percent Excess Air, % F-Factor, dscfm/MMBtu @ %O2 Round Duct Diameter, inches Rectangular Duct Width, inches Rectangular Duct Length, inches Fw Fc



### Monday, March 07, 2011 Page 21 of 22

### LocationStack Exit - OTM - 27/28 Average

Run Number Test Date Run Start Time Run Finish Time Net Traversing Points Net Run Time, minutes Stack Exit Stack Exit Stack Exit Nozzle Diameter, inches 8/18/2010 8/18/2010 8/19/2010 Pitot Tube Coefficient OTM - 27/28OTM - 27/28OTM - 27/28 Dry Gas Meter Calibration Factor 1 2 3 2.000 Barometric Pressure, inches of Mercury 10:30:00 AM9:30:00 AM12:00:00 PM Average Orifice Meter Differential, inches H2O 1:16:00 PM2:58:15 PM3:45:00 PM Dry Gas Meter Volume Sampled, cubic feet 25 24 24 24.333 Average Dry Gas Meter Temperature, °F 150 120 115 128.333 Dry Gas Meter Volume Sampled, dscf 0.153 0.153 0.153 0.153 Total Moisture Liquid collected, g 0.84 0.84 0.84 0.840 Volume of Water Vapor, standard cubic feet 1.0039 1.0039 1.0039 1.004 Moisture Content of Stack Gas, % 29.84 29.85 29.76 29.817 Moisture Saturation at Stack Gas Temperature, % 0.45 0.46 0.46 0.457 Dry Mole Fraction 47.280 47.001 43.812 46.031 Carbon Dioxide, % 89.96 93.29 95.33 92.860 Oxygen, % 45.498 44.973 41.642 44.038 Carbon Monoxide & Nitrogen, % 128 118.6 118.1 121.567 Fuel Factor 6.02 5.58 5.56 Dry Molecular Weight, lb/lb-Mole 11.69 11.04 11.78 11.503 Wet Molecular weight, lb/lb-Mole 100.00 100.00 100.00 100.000 Flue Gas Static Pressure, inches of H2O 0.8831 0.8896 0.8822 0.885 Absolute Flue Gas Pressure, inches of Mercury 11.6 12 12.7 12.100 Average Stack Gas Temperature, °F 6.4 5.9 5 5.767 Average Velocity Head, inches of H2O 82 82.1 82.3 82.133 Average Stack Gas Velocity, feet/second 1.25 1.25 1.25 1.250 Stack Cross-Sectional Area, square feet 29.86 29.87 29.85 29.860 Dry Volumetric Flow Rate, dry scfm 310.00 307.29 307.65 308.313 Actual Wet Volumetric Flue Gas Flow Rate, acfm 1.3435234012 36161.270247631

595531.133735073

99612 1.249 Percent Isokinetic of Sampling Rate, % 78.91 76.41 72.27 75.863 Percent Excess Air, % 0 0 0 0.000 F-Factor, dscfm/MMBtu @ %O2 0 0 0 0.000 Round Duct Diameter, inches 30.11 30.16 30.23 Rectangular Duct Width, inches 28.69 28.82 28.79 Rectangular Duct Length, inches 0.3 0.3 1.2 Fw 0.000 0.000 0.000 0.000 Fc 0 0 0 0.000



### Monday, March 07, 2011 Page 22 of 22